OBSP Determination:
BETA-SITOSTEROL
METHOD: 4433 , TESTIDCODE: 62815GCM99

 Analysis Date = 09/26/16 
 SpikeMix = Abs 061716WW: 100 µl & NSI 042916WW: 100 µl 
 Pct Recovery = 20%  Analysis Date = 04/11/17 
 SpikeMix = Crescent 03FF070: 100 µl & Phenova B20160306: 100 µl 
 Pct Recovery = 77%  Analysis Date = 01/10/17 
 SpikeMix = ChemService 5016000: 100 µl & Crescent 03FF070: 100 µl 
 Pct Recovery = 11%  Analysis Date = 08/15/17 
 SpikeMix = ChemService 5016000: 80 µl & NSI 042916WW: 80 µl 
 Pct Recovery = 22%  Analysis Date = 12/06/16 
 SpikeMix = Abs 061716WW: 80 µl & NSI 042916WW: 80 µl 
 Pct Recovery = 44%  Analysis Date = 12/06/16 
 SpikeMix = NSI 042916WW: 80 µl & Supelco LC20139V: 80 µl 
 Pct Recovery = 30%  Analysis Date = 06/30/17 
 SpikeMix = Phenova B20160306: 80 µl & Crescent 03FF070: 80 µl 
 Pct Recovery = 21%  Analysis Date = 01/05/17 
 SpikeMix = Abs 061716WW: 80 µl & Crescent 03FF070: 80 µl 
 Pct Recovery = 49%  Analysis Date = 12/06/16 
 SpikeMix = Crescent 03FF070: 80 µl & Supelco LC20139V: 80 µl 
 Pct Recovery = 55%  Analysis Date = 08/10/16 
 SpikeMix = ChemService 5016000: 80 µl & Crescent 03FF070: 80 µl 
 Pct Recovery = 68%  Analysis Date = 01/11/18 
 SpikeMix = Abs 071317WWUF: 60 µl & Abs 071717WWUF: 60 µl 
 Pct Recovery = 1%  Analysis Date = 06/29/17 
 SpikeMix = Phenova B20160306: 40 µl & NSI 042916WW: 40 µl 
 Pct Recovery = 33%  Analysis Date = 04/12/17 
 SpikeMix = Abs 061716WW: 40 µl & NSI 042916WW: 40 µl 
 Pct Recovery = 27%  Analysis Date = 04/12/17 
 SpikeMix = NSI 042916WW: 40 µl & Supelco LC20139V: 40 µl 
 Pct Recovery = 37%  Analysis Date = 01/06/17 
 SpikeMix = NSI 042916WW: 40 µl & Phenova B20160306: 40 µl 
 Pct Recovery = 32%  Analysis Date = 12/07/16 
 SpikeMix = ChemService 5016000: 40 µl & NSI 042916WW: 40 µl 
 Pct Recovery = 42%  Analysis Date = 09/27/16 
 SpikeMix = NSI 042916WW: 40 µl & Phenova B20160306: 40 µl 
 Pct Recovery = 32%  Analysis Date = 08/03/16 
 SpikeMix = NSI 042916WW: 40 µl & Supelco LC20139V: 40 µl 
 Pct Recovery = 55%  Analysis Date = 05/25/17 
 SpikeMix = ChemService 5016000: 40 µl & Crescent 03FF070: 40 µl 
 Pct Recovery = 90%  Analysis Date = 10/06/16 
 SpikeMix = Crescent 03FF070: 40 µl & Supelco LC20139V: 40 µl 
 Pct Recovery = 24%  Analysis Date = 09/28/16 
 SpikeMix = Abs 061716WW: 40 µl & Crescent 03FF070: 40 µl 
 Pct Recovery = 37%  Analysis Date = 08/24/16 
 SpikeMix = Crescent 03FF070: 40 µl & Phenova B20160306: 40 µl 
 Pct Recovery = 71%  Analysis Date = 06/16/16 
 SpikeMix = Phenova B20160306: 40 µl & Crescent 03FF070: 40 µl 
 Pct Recovery = 20%  Analysis Date = 06/14/16 
 SpikeMix = ChemService 5016000: 40 µl & Crescent 03FF070: 40 µl 
 Pct Recovery = 26%  Analysis Date = 08/16/17 
 SpikeMix = Abs 071717WWUF: 30 µl & Abs 071417WWUF: 30 µl 
 Pct Recovery = 77%  Analysis Date = 02/25/16 
 SpikeMix = ERA 0406-15-02: 20 µl & Spex Organics EN150529012: 20 µl 
 Pct Recovery = 28%  Analysis Date = 02/24/16 
 SpikeMix = Abs 041615: 20 µl & Supelco LC13546: 20 µl 
 Pct Recovery = 30%  Analysis Date = 01/11/18 
 Pct Recovery = 9%  Analysis Date = 01/07/18 
 Pct Recovery = 10%  Analysis Date = 01/07/18 
 Pct Recovery = 10%  Analysis Date = 01/04/18 
 Pct Recovery = 10%  Analysis Date = 01/04/18 
 Pct Recovery = 10%  Analysis Date = 12/31/17 
 Pct Recovery = 11%  Analysis Date = 12/31/17 
 Pct Recovery = 11%  Analysis Date = 12/28/17 
 Pct Recovery = 12%  Analysis Date = 12/28/17 
 Pct Recovery = 12%  Analysis Date = 12/24/17 
 Pct Recovery = 12%  Analysis Date = 12/24/17 
 Pct Recovery = 12%  Analysis Date = 12/21/17 
 Pct Recovery = 13%  Analysis Date = 12/21/17 
 Pct Recovery = 13%  Analysis Date = 12/17/17 
 Pct Recovery = 14%  Analysis Date = 12/17/17 
 Pct Recovery = 14%  Analysis Date = 12/14/17 
 Pct Recovery = 14%  Analysis Date = 12/14/17 
 Pct Recovery = 14%  Analysis Date = 12/11/17 
 Pct Recovery = 15%  Analysis Date = 12/11/17 
 Pct Recovery = 15%  Analysis Date = 12/07/17 
 Pct Recovery = 16%  Analysis Date = 12/07/17 
 Pct Recovery = 16%  Analysis Date = 12/04/17 
 Pct Recovery = 16%  Analysis Date = 12/04/17 
 Pct Recovery = 16%  Analysis Date = 11/30/17 
 Pct Recovery = 17%  Analysis Date = 11/30/17 
 Pct Recovery = 17%  Analysis Date = 11/27/17 
 Pct Recovery = 18%  Analysis Date = 11/27/17 
 Pct Recovery = 18%  Analysis Date = 11/23/17 
 Pct Recovery = 18%  Analysis Date = 11/23/17 
 Pct Recovery = 18%  Analysis Date = 11/20/17 
 Pct Recovery = 19%  Analysis Date = 11/20/17 
 Pct Recovery = 19%  Analysis Date = 11/17/17 
 Pct Recovery = 20%  Analysis Date = 11/17/17 
 Pct Recovery = 20%  Analysis Date = 11/13/17 
 Pct Recovery = 20%  Analysis Date = 11/13/17 
 Pct Recovery = 20%  Analysis Date = 11/10/17 
 Pct Recovery = 21%  Analysis Date = 11/10/17 
 Pct Recovery = 21%  Analysis Date = 11/06/17 
 Pct Recovery = 22%  Analysis Date = 11/06/17 
 Pct Recovery = 22%  Analysis Date = 11/03/17 
 Pct Recovery = 22%  Analysis Date = 11/03/17 
 Pct Recovery = 22%  Analysis Date = 10/30/17 
 Pct Recovery = 23%  Analysis Date = 10/30/17 
 Pct Recovery = 23%  Analysis Date = 10/27/17 
 Pct Recovery = 24%  Analysis Date = 10/27/17 
 Pct Recovery = 24%  Analysis Date = 10/23/17 
 Pct Recovery = 24%  Analysis Date = 10/23/17 
 Pct Recovery = 24%  Analysis Date = 10/20/17 
 Pct Recovery = 25%  Analysis Date = 10/20/17 
 Pct Recovery = 25%  Analysis Date = 10/17/17 
 Pct Recovery = 26%  Analysis Date = 10/17/17 
 Pct Recovery = 26%  Analysis Date = 10/13/17 
 Pct Recovery = 26%  Analysis Date = 10/13/17 
 Pct Recovery = 26%  Analysis Date = 10/10/17 
 Pct Recovery = 27%  Analysis Date = 10/10/17 
 Pct Recovery = 27%  Analysis Date = 10/06/17 
 Pct Recovery = 28%  Analysis Date = 10/06/17 
 Pct Recovery = 28%  Analysis Date = 10/03/17 
 Pct Recovery = 28%  Analysis Date = 10/03/17 
 Pct Recovery = 28%  Analysis Date = 09/29/17 
 Pct Recovery = 29%  Analysis Date = 09/29/17 
 Pct Recovery = 29%  Analysis Date = 09/26/17 
 Pct Recovery = 30%  Analysis Date = 09/26/17 
 Pct Recovery = 30%  Analysis Date = 09/23/17 
 Pct Recovery = 30%  Analysis Date = 09/23/17 
 Pct Recovery = 30%  Analysis Date = 09/19/17 
 Pct Recovery = 31%  Analysis Date = 09/19/17 
 Pct Recovery = 31%  Analysis Date = 09/16/17 
 Pct Recovery = 32%  Analysis Date = 09/16/17 
 Pct Recovery = 32%  Analysis Date = 09/12/17 
 Pct Recovery = 32%  Analysis Date = 09/12/17 
 Pct Recovery = 32%  Analysis Date = 09/09/17 
 Pct Recovery = 33%  Analysis Date = 09/09/17 
 Pct Recovery = 33%  Analysis Date = 09/05/17 
 Pct Recovery = 34%  Analysis Date = 09/05/17 
 Pct Recovery = 34%  Analysis Date = 09/02/17 
 Pct Recovery = 34%  Analysis Date = 09/02/17 
 Pct Recovery = 34%  Analysis Date = 08/30/17 
 Pct Recovery = 35%  Analysis Date = 08/30/17 
 Pct Recovery = 35%  Analysis Date = 08/26/17 
 Pct Recovery = 36%  Analysis Date = 08/26/17 
 Pct Recovery = 36%  Analysis Date = 08/23/17 
 Pct Recovery = 36%  Analysis Date = 08/23/17 
 Pct Recovery = 36%  Analysis Date = 08/19/17 
 Pct Recovery = 37%  Analysis Date = 08/19/17 
 Pct Recovery = 37%  Analysis Date = 08/16/17 
 Pct Recovery = 38%  Analysis Date = 08/16/17 
 Pct Recovery = 38%  Analysis Date = 08/12/17 
 Pct Recovery = 38%  Analysis Date = 08/12/17 
 Pct Recovery = 38%  Analysis Date = 08/09/17 
 Pct Recovery = 39%  Analysis Date = 08/09/17 
 Pct Recovery = 39%  Analysis Date = 08/05/17 
 Pct Recovery = 40%  Analysis Date = 08/05/17 
 Pct Recovery = 40%  Analysis Date = 08/02/17 
 Pct Recovery = 40%  Analysis Date = 08/02/17 
 Pct Recovery = 40%  Analysis Date = 07/30/17 
 Pct Recovery = 41%  Analysis Date = 07/30/17 
 Pct Recovery = 41%  Analysis Date = 07/26/17 
 Pct Recovery = 42%  Analysis Date = 07/26/17 
 Pct Recovery = 42%  Analysis Date = 07/23/17 
 Pct Recovery = 42%  Analysis Date = 07/23/17 
 Pct Recovery = 42%  Analysis Date = 07/19/17 
 Pct Recovery = 43%  Analysis Date = 07/19/17 
 Pct Recovery = 43%  Analysis Date = 07/16/17 
 Pct Recovery = 44%  Analysis Date = 07/16/17 
 Pct Recovery = 44%  Analysis Date = 07/12/17 
 Pct Recovery = 44%  Analysis Date = 07/12/17 
 Pct Recovery = 44%  Analysis Date = 07/09/17 
 Pct Recovery = 45%  Analysis Date = 07/09/17 
 Pct Recovery = 45%  Analysis Date = 07/06/17 
 Pct Recovery = 46%  Analysis Date = 07/06/17 
 Pct Recovery = 46%  Analysis Date = 07/02/17 
 Pct Recovery = 46%  Analysis Date = 07/02/17 
 Pct Recovery = 46%  Analysis Date = 06/29/17 
 Pct Recovery = 47%  Analysis Date = 06/29/17 
 Pct Recovery = 47%  Analysis Date = 06/25/17 
 Pct Recovery = 47%  Analysis Date = 06/25/17 
 Pct Recovery = 47%  Analysis Date = 06/22/17 
 Pct Recovery = 47%  Analysis Date = 06/22/17 
 Pct Recovery = 47%  Analysis Date = 06/18/17 
 Pct Recovery = 46%  Analysis Date = 06/18/17 
 Pct Recovery = 46%  Analysis Date = 06/15/17 
 Pct Recovery = 46%  Analysis Date = 06/15/17 
 Pct Recovery = 46%  Analysis Date = 06/12/17 
 Pct Recovery = 46%  Analysis Date = 06/12/17 
 Pct Recovery = 46%  Analysis Date = 06/08/17 
 Pct Recovery = 46%  Analysis Date = 06/08/17 
 Pct Recovery = 46%  Analysis Date = 06/05/17 
 Pct Recovery = 46%  Analysis Date = 06/05/17 
 Pct Recovery = 46%  Analysis Date = 06/01/17 
 Pct Recovery = 46%  Analysis Date = 06/01/17 
 Pct Recovery = 46%  Analysis Date = 05/29/17 
 Pct Recovery = 46%  Analysis Date = 05/29/17 
 Pct Recovery = 46%  Analysis Date = 05/25/17 
 Pct Recovery = 46%  Analysis Date = 05/25/17 
 Pct Recovery = 46%  Analysis Date = 05/22/17 
 Pct Recovery = 46%  Analysis Date = 05/22/17 
 Pct Recovery = 46%  Analysis Date = 05/18/17 
 Pct Recovery = 46%  Analysis Date = 05/18/17 
 Pct Recovery = 46%  Analysis Date = 05/15/17 
 Pct Recovery = 46%  Analysis Date = 05/15/17 
 Pct Recovery = 46%  Analysis Date = 05/12/17 
 Pct Recovery = 45%  Analysis Date = 05/12/17 
 Pct Recovery = 45%  Analysis Date = 05/08/17 
 Pct Recovery = 45%  Analysis Date = 05/08/17 
 Pct Recovery = 45%  Analysis Date = 05/05/17 
 Pct Recovery = 45%  Analysis Date = 05/05/17 
 Pct Recovery = 45%  Analysis Date = 05/01/17 
 Pct Recovery = 45%  Analysis Date = 05/01/17 
 Pct Recovery = 45%  Analysis Date = 04/28/17 
 Pct Recovery = 45%  Analysis Date = 04/28/17 
 Pct Recovery = 45%  Analysis Date = 04/24/17 
 Pct Recovery = 45%  Analysis Date = 04/24/17 
 Pct Recovery = 45%  Analysis Date = 04/21/17 
 Pct Recovery = 45%  Analysis Date = 04/21/17 
 Pct Recovery = 45%  Analysis Date = 04/18/17 
 Pct Recovery = 45%  Analysis Date = 04/18/17 
 Pct Recovery = 45%  Analysis Date = 04/14/17 
 Pct Recovery = 45%  Analysis Date = 04/14/17 
 Pct Recovery = 45%  Analysis Date = 04/11/17 
 Pct Recovery = 45%  Analysis Date = 04/11/17 
 Pct Recovery = 45%  Analysis Date = 04/07/17 
 Pct Recovery = 44%  Analysis Date = 04/07/17 
 Pct Recovery = 44%  Analysis Date = 04/04/17 
 Pct Recovery = 44%  Analysis Date = 04/04/17 
 Pct Recovery = 44%  Analysis Date = 03/31/17 
 Pct Recovery = 44%  Analysis Date = 03/31/17 
 Pct Recovery = 44%  Analysis Date = 03/28/17 
 Pct Recovery = 44%  Analysis Date = 03/28/17 
 Pct Recovery = 44%  Analysis Date = 03/25/17 
 Pct Recovery = 43%  Analysis Date = 03/25/17 
 Pct Recovery = 43%  Analysis Date = 03/21/17 
 Pct Recovery = 43%  Analysis Date = 03/21/17 
 Pct Recovery = 43%  Analysis Date = 03/18/17 
 Pct Recovery = 43%  Analysis Date = 03/18/17 
 Pct Recovery = 43%  Analysis Date = 03/14/17 
 Pct Recovery = 43%  Analysis Date = 03/14/17 
 Pct Recovery = 43%  Analysis Date = 03/11/17 
 Pct Recovery = 42%  Analysis Date = 03/11/17 
 Pct Recovery = 42%  Analysis Date = 03/07/17 
 Pct Recovery = 42%  Analysis Date = 03/07/17 
 Pct Recovery = 42%  Analysis Date = 03/04/17 
 Pct Recovery = 42%  Analysis Date = 03/04/17 
 Pct Recovery = 42%  Analysis Date = 02/28/17 
 Pct Recovery = 42%  Analysis Date = 02/28/17 
 Pct Recovery = 42%  Analysis Date = 02/25/17 
 Pct Recovery = 42%  Analysis Date = 02/25/17 
 Pct Recovery = 42%  Analysis Date = 02/22/17 
 Pct Recovery = 41%  Analysis Date = 02/22/17 
 Pct Recovery = 41%  Analysis Date = 02/18/17 
 Pct Recovery = 41%  Analysis Date = 02/18/17 
 Pct Recovery = 41%  Analysis Date = 02/15/17 
 Pct Recovery = 41%  Analysis Date = 02/15/17 
 Pct Recovery = 41%  Analysis Date = 02/11/17 
 Pct Recovery = 41%  Analysis Date = 02/11/17 
 Pct Recovery = 41%  Analysis Date = 02/08/17 
 Pct Recovery = 40%  Analysis Date = 02/08/17 
 Pct Recovery = 40%  Analysis Date = 02/04/17 
 Pct Recovery = 40%  Analysis Date = 02/04/17 
 Pct Recovery = 40%  Analysis Date = 02/01/17 
 Pct Recovery = 40%  Analysis Date = 02/01/17 
 Pct Recovery = 40%  Analysis Date = 01/29/17 
 Pct Recovery = 40%  Analysis Date = 01/29/17 
 Pct Recovery = 40%  Analysis Date = 01/25/17 
 Pct Recovery = 39%  Analysis Date = 01/25/17 
 Pct Recovery = 39%  Analysis Date = 01/22/17 
 Pct Recovery = 39%  Analysis Date = 01/22/17 
 Pct Recovery = 39%  Analysis Date = 01/18/17 
 Pct Recovery = 39%  Analysis Date = 01/18/17 
 Pct Recovery = 39%  Analysis Date = 01/15/17 
 Pct Recovery = 39%  Analysis Date = 01/15/17 
 Pct Recovery = 39%  Analysis Date = 01/11/17 
 Pct Recovery = 39%  Analysis Date = 01/11/17 
 Pct Recovery = 39%  Analysis Date = 01/08/17 
 Pct Recovery = 38%  Analysis Date = 01/08/17 
 Pct Recovery = 38%  Analysis Date = 01/05/17 
 Pct Recovery = 38%  Analysis Date = 01/05/17 
 Pct Recovery = 38%  Analysis Date = 01/01/17 
 Pct Recovery = 38%  Analysis Date = 01/01/17 
 Pct Recovery = 38%  Analysis Date = 12/29/16 
 Pct Recovery = 37%  Analysis Date = 12/29/16 
 Pct Recovery = 37%  Analysis Date = 12/25/16 
 Pct Recovery = 37%  Analysis Date = 12/25/16 
 Pct Recovery = 37%  Analysis Date = 12/22/16 
 Pct Recovery = 37%  Analysis Date = 12/22/16 
 Pct Recovery = 37%  Analysis Date = 12/18/16 
 Pct Recovery = 37%  Analysis Date = 12/18/16 
 Pct Recovery = 37%  Analysis Date = 12/15/16 
 Pct Recovery = 36%  Analysis Date = 12/15/16 
 Pct Recovery = 36%  Analysis Date = 12/11/16 
 Pct Recovery = 36%  Analysis Date = 12/11/16 
 Pct Recovery = 36%  Analysis Date = 12/08/16 
 Pct Recovery = 36%  Analysis Date = 12/08/16 
 Pct Recovery = 36%  Analysis Date = 12/05/16 
 Pct Recovery = 36%  Analysis Date = 12/05/16 
 Pct Recovery = 36%  Analysis Date = 12/01/16 
 Pct Recovery = 36%  Analysis Date = 12/01/16 
 Pct Recovery = 36%  Analysis Date = 11/28/16 
 Pct Recovery = 37%  Analysis Date = 11/28/16 
 Pct Recovery = 37%  Analysis Date = 11/24/16 
 Pct Recovery = 37%  Analysis Date = 11/24/16 
 Pct Recovery = 37%  Analysis Date = 11/21/16 
 Pct Recovery = 37%  Analysis Date = 11/21/16 
 Pct Recovery = 37%  Analysis Date = 11/17/16 
 Pct Recovery = 38%  Analysis Date = 11/17/16 
 Pct Recovery = 38%  Analysis Date = 11/14/16 
 Pct Recovery = 38%  Analysis Date = 11/14/16 
 Pct Recovery = 38%  Analysis Date = 11/11/16 
 Pct Recovery = 38%  Analysis Date = 11/11/16 
 Pct Recovery = 38%  Analysis Date = 11/07/16 
 Pct Recovery = 39%  Analysis Date = 11/07/16 
 Pct Recovery = 39%  Analysis Date = 11/04/16 
 Pct Recovery = 39%  Analysis Date = 11/04/16 
 Pct Recovery = 39%  Analysis Date = 10/31/16 
 Pct Recovery = 39%  Analysis Date = 10/31/16 
 Pct Recovery = 39%  Analysis Date = 10/28/16 
 Pct Recovery = 40%  Analysis Date = 10/28/16 
 Pct Recovery = 40%  Analysis Date = 10/24/16 
 Pct Recovery = 40%  Analysis Date = 10/24/16 
 Pct Recovery = 40%  Analysis Date = 10/21/16 
 Pct Recovery = 40%  Analysis Date = 10/21/16 
 Pct Recovery = 40%  Analysis Date = 10/18/16 
 Pct Recovery = 41%  Analysis Date = 10/18/16 
 Pct Recovery = 41%  Analysis Date = 10/14/16 
 Pct Recovery = 41%  Analysis Date = 10/14/16 
 Pct Recovery = 41%  Analysis Date = 10/11/16 
 Pct Recovery = 41%  Analysis Date = 10/11/16 
 Pct Recovery = 41%  Analysis Date = 10/07/16 
 Pct Recovery = 42%  Analysis Date = 10/07/16 
 Pct Recovery = 42%  Analysis Date = 10/04/16 
 Pct Recovery = 42%  Analysis Date = 10/04/16 
 Pct Recovery = 42%  Analysis Date = 09/30/16 
 Pct Recovery = 42%  Analysis Date = 09/30/16 
 Pct Recovery = 42%  Analysis Date = 09/27/16 
 Pct Recovery = 42%  Analysis Date = 09/27/16 
 Pct Recovery = 42%  Analysis Date = 09/23/16 
 Pct Recovery = 42%  Analysis Date = 09/23/16 
 Pct Recovery = 42%  Analysis Date = 09/20/16 
 Pct Recovery = 42%  Analysis Date = 09/20/16 
 Pct Recovery = 42%  Analysis Date = 09/17/16 
 Pct Recovery = 42%  Analysis Date = 09/17/16 
 Pct Recovery = 42%  Analysis Date = 09/13/16 
 Pct Recovery = 42%  Analysis Date = 09/13/16 
 Pct Recovery = 42%  Analysis Date = 09/10/16 
 Pct Recovery = 42%  Analysis Date = 09/10/16 
 Pct Recovery = 42%  Analysis Date = 09/06/16 
 Pct Recovery = 42%  Analysis Date = 09/06/16 
 Pct Recovery = 42%  Analysis Date = 09/03/16 
 Pct Recovery = 41%  Analysis Date = 09/03/16 
 Pct Recovery = 41%  Analysis Date = 08/30/16 
 Pct Recovery = 41%  Analysis Date = 08/30/16 
 Pct Recovery = 41%  Analysis Date = 08/27/16 
 Pct Recovery = 41%  Analysis Date = 08/27/16 
 Pct Recovery = 41%  Analysis Date = 08/24/16 
 Pct Recovery = 41%  Analysis Date = 08/24/16 
 Pct Recovery = 41%  Analysis Date = 08/20/16 
 Pct Recovery = 41%  Analysis Date = 08/20/16 
 Pct Recovery = 41%  Analysis Date = 08/17/16 
 Pct Recovery = 41%  Analysis Date = 08/17/16 
 Pct Recovery = 41%  Analysis Date = 08/13/16 
 Pct Recovery = 41%  Analysis Date = 08/13/16 
 Pct Recovery = 41%  Analysis Date = 08/10/16 
 Pct Recovery = 40%  Analysis Date = 08/10/16 
 Pct Recovery = 40%  Analysis Date = 08/06/16 
 Pct Recovery = 40%  Analysis Date = 08/06/16 
 Pct Recovery = 40%  Analysis Date = 08/03/16 
 Pct Recovery = 40%  Analysis Date = 08/03/16 
 Pct Recovery = 40%  Analysis Date = 07/31/16 
 Pct Recovery = 40%  Analysis Date = 07/31/16 
 Pct Recovery = 40%  Analysis Date = 07/27/16 
 Pct Recovery = 39%  Analysis Date = 07/27/16 
 Pct Recovery = 39%  Analysis Date = 07/24/16 
 Pct Recovery = 39%  Analysis Date = 07/24/16 
 Pct Recovery = 39%  Analysis Date = 07/20/16 
 Pct Recovery = 39%  Analysis Date = 07/20/16 
 Pct Recovery = 39%  Analysis Date = 07/17/16 
 Pct Recovery = 39%  Analysis Date = 07/17/16 
 Pct Recovery = 39%  Analysis Date = 07/13/16 
 Pct Recovery = 39%  Analysis Date = 07/13/16 
 Pct Recovery = 39%  Analysis Date = 07/10/16 
 Pct Recovery = 38%  Analysis Date = 07/10/16 
 Pct Recovery = 38%  Analysis Date = 07/06/16 
 Pct Recovery = 38%  Analysis Date = 07/06/16 
 Pct Recovery = 38%  Analysis Date = 07/03/16 
 Pct Recovery = 38%  Analysis Date = 07/03/16 
 Pct Recovery = 38%  Analysis Date = 06/30/16 
 Pct Recovery = 38%  Analysis Date = 06/30/16 
 Pct Recovery = 38%  Analysis Date = 06/26/16 
 Pct Recovery = 37%  Analysis Date = 06/26/16 
 Pct Recovery = 37%  Analysis Date = 06/23/16 
 Pct Recovery = 37%  Analysis Date = 06/23/16 
 Pct Recovery = 37%  Analysis Date = 06/19/16 
 Pct Recovery = 37%  Analysis Date = 06/19/16 
 Pct Recovery = 37%  Analysis Date = 06/16/16 
 Pct Recovery = 37%  Analysis Date = 06/16/16 
 Pct Recovery = 37%  Analysis Date = 06/12/16 
 Pct Recovery = 37%  Analysis Date = 06/12/16 
 Pct Recovery = 37%  Analysis Date = 06/09/16 
 Pct Recovery = 36%  Analysis Date = 06/09/16 
 Pct Recovery = 36%  Analysis Date = 06/06/16 
 Pct Recovery = 36%  Analysis Date = 06/06/16 
 Pct Recovery = 36%  Analysis Date = 06/02/16 
 Pct Recovery = 36%  Analysis Date = 06/02/16 
 Pct Recovery = 36%  Analysis Date = 05/30/16 
 Pct Recovery = 35%  Analysis Date = 05/30/16 
 Pct Recovery = 35%  Analysis Date = 05/26/16 
 Pct Recovery = 35%  Analysis Date = 05/26/16 
 Pct Recovery = 35%  Analysis Date = 05/23/16 
 Pct Recovery = 35%  Analysis Date = 05/23/16 
 Pct Recovery = 35%  Analysis Date = 05/19/16 
 Pct Recovery = 35%  Analysis Date = 05/19/16 
 Pct Recovery = 35%  Analysis Date = 05/16/16 
 Pct Recovery = 34%  Analysis Date = 05/16/16 
 Pct Recovery = 34%  Analysis Date = 05/13/16 
 Pct Recovery = 34%  Analysis Date = 05/13/16 
 Pct Recovery = 34%  Analysis Date = 05/09/16 
 Pct Recovery = 34%  Analysis Date = 05/09/16 
 Pct Recovery = 34%  Analysis Date = 05/06/16 
 Pct Recovery = 33%  Analysis Date = 05/06/16 
 Pct Recovery = 33%  Analysis Date = 05/02/16 
 Pct Recovery = 33%  Analysis Date = 05/02/16 
 Pct Recovery = 33%  Analysis Date = 04/29/16 
 Pct Recovery = 33%  Analysis Date = 04/29/16 
 Pct Recovery = 33%  Analysis Date = 04/25/16 
 Pct Recovery = 33%  Analysis Date = 04/25/16 
 Pct Recovery = 33%  Analysis Date = 04/22/16 
 Pct Recovery = 32%  Analysis Date = 04/22/16 
 Pct Recovery = 32%  Analysis Date = 04/18/16 
 Pct Recovery = 32%  Analysis Date = 04/18/16 
 Pct Recovery = 32%  Analysis Date = 04/15/16 
 Pct Recovery = 32%  Analysis Date = 04/15/16 
 Pct Recovery = 32%  Analysis Date = 04/12/16 
 Pct Recovery = 32%  Analysis Date = 04/12/16 
 Pct Recovery = 32%  Analysis Date = 04/08/16 
 Pct Recovery = 31%  Analysis Date = 04/08/16 
 Pct Recovery = 31%  Analysis Date = 04/05/16 
 Pct Recovery = 31%  Analysis Date = 04/05/16 
 Pct Recovery = 31%  Analysis Date = 04/01/16 
 Pct Recovery = 31%  Analysis Date = 04/01/16 
 Pct Recovery = 31%  Analysis Date = 03/29/16 
 Pct Recovery = 30%  Analysis Date = 03/29/16 
 Pct Recovery = 30%  Analysis Date = 03/25/16 
 Pct Recovery = 30%  Analysis Date = 03/25/16 
 Pct Recovery = 30%  Analysis Date = 03/22/16 
 Pct Recovery = 30%  Analysis Date = 03/22/16 
 Pct Recovery = 30%  Analysis Date = 03/19/16 
 Pct Recovery = 30%  Analysis Date = 03/19/16 
 Pct Recovery = 30%  Analysis Date = 03/15/16 
 Pct Recovery = 29%  Analysis Date = 03/15/16 
 Pct Recovery = 29%  Analysis Date = 03/12/16 
 Pct Recovery = 29%  Analysis Date = 03/12/16 
 Pct Recovery = 29%  Analysis Date = 03/08/16 
 Pct Recovery = 29%  Analysis Date = 03/08/16 
 Pct Recovery = 29%  Analysis Date = 03/05/16 
 Pct Recovery = 29%  Analysis Date = 03/05/16 
 Pct Recovery = 29%  Analysis Date = 03/01/16 
 Pct Recovery = 28%  Analysis Date = 03/01/16 
 Pct Recovery = 28%  Analysis Date = 02/27/16 
 Pct Recovery = 28%  Analysis Date = 02/27/16 
 Pct Recovery = 28%  Analysis Date = 02/24/16 
 Pct Recovery = 28%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
BETA-SITOSTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 27 39% 22% 32% 23%
Total 27 39% 22% 32% 23%

Sample Statistics
BETA-SITOSTEROL

Characteristic N % % Basis
Plotted 27 93% Spiked
Estimated Values 27 93% Spiked
Deleted Values 2 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 2 7% 2 out of 29
Not Spiked 24 .  
False Positives 3 13% 3 out of 24