SAS Output

WY2010 LTMDL Data Review for Pharmaceuticals

Last Updated 11/09/2009

Analyte	Lab Code	TestID
1,7-dimethylxanthine	12080	6203000021
Acetaminophen	12080	6200000021
Caffeine	12080	5030500021
Carbamazepine	12080	6279300021
Codeine	12080	6200300021
Cotinine	12080	6200500021
Dehydronifedipine	12080	6200400021
Diltiazem	12080	6200800021
Diphenhydramine	12080	6279600021
Salbutamol (Albuterol)	12080	6202000021
Sulfamethoxazole	12080	6202100021
Thiabendazole	12080	6280100021
Trimethoprim	12080	6202300021
Warfarin	12080	6202400021

2010 LTMDL for 1,7-dimethylxanthine

Test ID: 6203000021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0585	0.08	.	.	.	.	.	0.0104	irl	0.06	0.12
2008	05/01/07 - 04/30/08	26	0.0642	0.08	.	.	.	3	0.0265	0.05	lrl	0.06	0.12
2009	05/01/08 - 04/30/09	24	0.0521	0.08	.	.	.	2	0.0088	0.06	lrl	.	.
2010	05/01/09 - 04/30/10	13	0.0654	0.08	.	.	.	.	.	0.05	lrl	.	.

Measured in ug/L

2010 LTMDL for Acetaminophen

Test ID: 6200000021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	28	0.0421	0.08	.	.	.	7	0.0021	0.0119	irl	0.04	0.08
2008	05/01/07 - 04/30/08	25	0.0405	0.08	.	.	.	13	0.0447	0.04	lrl	.	.
2009	05/01/08 - 04/30/09	24	0.0555	0.08	.	.	.	2	0.0077	0.04	lrl	0.06	0.12
2010	05/01/09 - 04/30/10	13	0.0501	0.08	.	.	.	3	0.0054	0.06	lrl	.	.

Measured in ug/L

2010 LTMDL for Caffeine

Test ID: 5030500021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	28	0.0321	0.08	2	.	0.0026	15	0.0138	0.0075	irl	0.03	0.06
2008	05/01/07 - 04/30/08	25	0.0447	0.08	2	.	0.0026	24	0.1362	0.03	lrl	0.14	0.28
2009	05/01/08 - 04/30/09	24	0.0317	0.08	.	.	.	3	0.0064	0.1	lrl	0.03	0.06
2010	05/01/09 - 04/30/10	13	0.0338	0.08	.	.	.	4	0.0147	0.03	lrl	.	.

Measured in ug/L

2010 LTMDL for Carbamazepine

Test ID: 6279300021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0239	0.08	2	.	0.0043	9	0.006	0.0089	irl	0.024	0.048
2008	05/01/07 - 04/30/08	26	0.0206	0.08	2	.	0.0043	16	0.0125	0.02	lrl	.	.
2009	05/01/08 - 04/30/09	24	0.0273	0.08	.	.	.	2	0.0001	0.02	lrl	0.03	0.06
2010	05/01/09 - 04/30/10	14	0.0085	0.08	.	.	.	.	.	0.03	lrl	0.008	0.016

Measured in ug/L

2010 LTMDL for Codeine

Test ID: 6200300021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0190	0.08	.	.	.	.	.	0.0111	irl	0.019	0.038
2008	05/01/07 - 04/30/08	26	0.0219	0.08	.	.	.	.	.	0.02	lrl	.	.
2009	05/01/08 - 04/30/09	24	0.0234	0.08	.	.	.	.	.	0.02	lrl	.	.
2010	05/01/09 - 04/30/10	14	0.0143	0.08	.	.	.	.	.	0.023	lrl	.	.

Measured in ug/L

2010 LTMDL for Cotinine

Test ID: 6200500021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0153	0.08	.	.	.	23	0.017	0.0142	irl	.	.
2008	05/01/07 - 04/30/08	26	0.0165	0.08	.	.	.	7	0.0058	0.01	irl	0.017	0.034
2009	05/01/08 - 04/30/09	24	0.0192	0.08	.	.	.	3	0.0043	0.01	irl	0.019	0.038
2010	05/01/09 - 04/30/10	14	0.0125	0.08	.	.	.	.	.	0.019	lrl	.	.

Measured in ug/L

2010 LTMDL for Dehydronifedipine

Test ID: 6200400021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0367	0.08	.	.	.	4	0.0004	0.011	irl	0.04	0.08
2008	05/01/07 - 04/30/08	26	0.0429	0.08	.	.	.	3	0.0014	0.03	lrl	0.04	0.08
2009	05/01/08 - 04/30/09	24	0.0380	0.08	.	.	.	.	.	0.04	lrl	.	.
2010	05/01/09 - 04/30/10	14	0.0277	0.08	.	.	.	6	0.003	0.04	lrl	.	.

Measured in ug/L

2010 LTMDL for Diltiazem

Test ID: 6200800021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	28	0.0235	0.08	.	.	.	.	.	0.0089	irl	0.023	0.046
2008	05/01/07 - 04/30/08	25	0.0366	0.08	.	.	.	2	0.0002	0.02	lrl	0.04	0.08
2009	05/01/08 - 04/30/09	24	0.0296	0.08	.	.	.	.	.	0.04	lrl	.	.
2010	05/01/09 - 04/30/10	9	0.0287	0.08	.	.	.	6	0.0023	0.03	lrl	.	.

Measured in ug/L

2010 LTMDL for Diphenhydramine

Test ID: 6279600021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0135	0.08	7	0.0005	0.0004	45	0.0019	0.0115	irl	.	.
2008	05/01/07 - 04/30/08	25	0.0145	0.08	.	.	.	65	0.0108	0.01	irl	0.015	0.03
2009	05/01/08 - 04/30/09	24	0.0175	0.08	.	.	.	43	0.0033	0.02	irl	.	.
2010	05/01/09 - 04/30/10	14	0.0183	0.08	.	.	.	7	0.0022	0.018	lrl	.	.

Measured in ug/L

2010 LTMDL for Salbutamol (Albuterol)

Test ID: 6202000021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0259	0.08	.	.	.	8	0.0045	0.0069	irl	0.03	0.06
2008	05/01/07 - 04/30/08	26	0.0295	0.08	.	.	.	17	0.0298	0.02	lrl	0.03	0.06
2009	05/01/08 - 04/30/09	24	0.0391	0.08	.	.	.	6	0.0164	0.03	lrl	0.04	0.08
2010	05/01/09 - 04/30/10	14	0.0266	0.08	.	.	.	.	.	0.04	lrl	.	.

Measured in ug/L

2010 LTMDL for Sulfamethoxazole

Test ID: 6202100021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0646	0.08	2	.	0.0018	13	0.0133	0.0119	irl	0.06	0.12
2008	05/01/07 - 04/30/08	26	0.0754	0.08	2	.	0.0018	19	0.0133	0.05	lrl	0.08	0.16
2009	05/01/08 - 04/30/09	21	0.0789	0.08	.	.	.	.	.	0.08	lrl	.	.
2010	05/01/09 - 04/30/10	14	0.0492	0.08	.	.	.	.	.	0.08	lrl	0.05	0.1

Measured in ug/L

2010 LTMDL for Thiabendazole

Test ID: 6280100021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	29	0.0256	0.08	.	.	.	7	0.0086	0.0125	irl	0.03	0.06
2008	05/01/07 - 04/30/08	26	0.0335	0.08	.	.	.	6	0.0103	0.02	irl	0.03	0.06
2009	05/01/08 - 04/30/09	24	0.0296	0.08	.	.	.	4	0.0095	0.03	irl	.	.
2010	05/01/09 - 04/30/10	14	0.0331	0.08	.	.	.	.	.	0.03	lrl	.	.

Measured in ug/L

2010 LTMDL for Trimethoprim

Test ID: 6202300021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	28	0.0128	0.08	.	.	.	5	0.0012	0.0102	irl	.	.
2008	05/01/07 - 04/30/08	25	0.0140	0.08	.	.	.	3	0.001	0.01	irl	0.014	0.028
2009	05/01/08 - 04/30/09	24	0.0165	0.08	.	.	.	3	0.0005	0.01	irl	0.017	0.034
2010	05/01/09 - 04/30/10	14	0.0097	0.08	.	.	.	.	.	0.017	lrl	0.01	0.02

Measured in ug/L

2010 LTMDL for Warfarin

Test ID: 6202400021, Labcode: 12080

Sample Dates		Spike Data			Blind Blank Data			Set Blank Data		Previous Settings		Suggested New Settings
LTMDL Year	Dates	n	Calculated LTMDL Spikes	Spike Concentration	n	Calculated LTMDL BBP	99% LTMDL BBP	n	99% LTMDL Set Blanks	LTMDL In Use	LTMDL Type	Update LTMDL to:	Update RL to:
2007	10/01/06 - 09/30/07	28	0.0328	0.08	.	.	.	.	.	0.0094	irl	0.03	0.06
2008	05/01/07 - 04/30/08	26	0.0504	0.08	.	.	.	.	.	0.03	lrl	0.05	0.1
2009	05/01/08 - 04/30/09	24	0.0431	0.08	.	.	.	.	.	0.05	lrl	.	.
2010	05/01/09 - 04/30/10	14	0.0330	0.08	.	.	.	3	0.0011	0.04	lrl	.	.

Measured in ug/L