BQS OBSP Determination:
DILTIAZEM
METHOD: 2080 , TESTIDCODE: 6200800021
DATES: 03/03/08 - 09/24/10

Expected Conc. = 0.2829 Median Pct Recovery = 31% Expected Conc. = 0.2822 Median Pct Recovery = 31% Expected Conc. = 0.2822 Median Pct Recovery = 31% Expected Conc. = 0.2767 Median Pct Recovery = 31% Expected Conc. = 0.2767 Median Pct Recovery = 31% Expected Conc. = 0.2729 Median Pct Recovery = 31% Expected Conc. = 0.2729 Median Pct Recovery = 31% Expected Conc. = 0.2498 Median Pct Recovery = 31% Expected Conc. = 0.2498 Median Pct Recovery = 31% Expected Conc. = 0.2228 Median Pct Recovery = 31% Expected Conc. = 0.2228 Median Pct Recovery = 31% Expected Conc. = 0.2201 Median Pct Recovery = 31% Expected Conc. = 0.2201 Median Pct Recovery = 31% Expected Conc. = 0.2187 Median Pct Recovery = 31% Expected Conc. = 0.2187 Median Pct Recovery = 31% Expected Conc. = 0.2008 Median Pct Recovery = 31% Expected Conc. = 0.2008 Median Pct Recovery = 31% Expected Conc. = 0.1983 Median Pct Recovery = 31% Expected Conc. = 0.1983 Median Pct Recovery = 31% Expected Conc. = 0.1968 Median Pct Recovery = 31% Expected Conc. = 0.1968 Median Pct Recovery = 31% Expected Conc. = 0.1498 Median Pct Recovery = 31% Expected Conc. = 0.1498 Median Pct Recovery = 31% Expected Conc. = 0.148 Median Pct Recovery = 31% Expected Conc. = 0.148 Median Pct Recovery = 31% Expected Conc. = 0.1472 Median Pct Recovery = 31% Expected Conc. = 0.1472 Median Pct Recovery = 31% Expected Conc. = 0.1433 Median Pct Recovery = 31% Expected Conc. = 0.1433 Median Pct Recovery = 31% Expected Conc. = 0.1418 Median Pct Recovery = 31% Expected Conc. = 0.1418 Median Pct Recovery = 31% Expected Conc. = 0.1408 Median Pct Recovery = 31% Expected Conc. = 0.1408 Median Pct Recovery = 31% Expected Conc. = 0.1407 Median Pct Recovery = 31% Expected Conc. = 0.1407 Median Pct Recovery = 31% Expected Conc. = 0.14 Median Pct Recovery = 31% Expected Conc. = 0.14 Median Pct Recovery = 31% Expected Conc. = 0.1384 Median Pct Recovery = 31% Expected Conc. = 0.1384 Median Pct Recovery = 31% Expected Conc. = 0.1383 Median Pct Recovery = 31% Expected Conc. = 0.1383 Median Pct Recovery = 31% Expected Conc. = 0.1377 Median Pct Recovery = 31% Expected Conc. = 0.1377 Median Pct Recovery = 31% Expected Conc. = 0.1374 Median Pct Recovery = 31% Expected Conc. = 0.1374 Median Pct Recovery = 31% Expected Conc. = 0.1365 Median Pct Recovery = 31% Expected Conc. = 0.1365 Median Pct Recovery = 31% Expected Conc. = 0.1279 Median Pct Recovery = 31% Expected Conc. = 0.1279 Median Pct Recovery = 31% Expected Conc. = 0.1277 Median Pct Recovery = 31% Expected Conc. = 0.1277 Median Pct Recovery = 31% Expected Conc. = 0.1275 Median Pct Recovery = 31% Expected Conc. = 0.1275 Median Pct Recovery = 31% Expected Conc. = 0.1257 Median Pct Recovery = 31% Expected Conc. = 0.1257 Median Pct Recovery = 31% Expected Conc. = 0.1242 Median Pct Recovery = 31% Expected Conc. = 0.1242 Median Pct Recovery = 31% Expected Conc. = 0.0575 Median Pct Recovery = 31% Expected Conc. = 0.0575 Median Pct Recovery = 31% Expected Conc. = 0.0564 Median Pct Recovery = 31% Expected Conc. = 0.0564 Median Pct Recovery = 31% Expected Conc. = 0.0557 Median Pct Recovery = 31% Expected Conc. = 0.0557 Median Pct Recovery = 31% Expected Conc. = 0.0555 Median Pct Recovery = 31% Expected Conc. = 0.0555 Median Pct Recovery = 31% Expected Conc. = 0.0553 Median Pct Recovery = 31% Expected Conc. = 0.0553 Median Pct Recovery = 31% Expected Conc. = 0.0553 Median Pct Recovery = 31% Expected Conc. = 0.0553 Median Pct Recovery = 31% Expected Conc. = 0.0551 Median Pct Recovery = 31% Expected Conc. = 0.0551 Median Pct Recovery = 31% Expected Conc. = 0.055 Median Pct Recovery = 31% Expected Conc. = 0.055 Median Pct Recovery = 31% Expected Conc. = 0.0546 Median Pct Recovery = 31% Expected Conc. = 0.0546 Median Pct Recovery = 31% Expected Conc. = 0.0542 Median Pct Recovery = 31% Expected Conc. = 0.0542 Median Pct Recovery = 31% Expected Conc. = 0.0538 Median Pct Recovery = 31% Expected Conc. = 0.0538 Median Pct Recovery = 31% Expected Conc. = 0.0545 Median Pct Recovery = 31% Expected Conc. = 0.0545 Median Pct Recovery = 31% Expected Conc. = 0.1985 Median Pct Recovery = 31% Expected Conc. = 0.1985 Median Pct Recovery = 31% Expected Conc. = 0.1388 Median Pct Recovery = 31% Analysis Date = 06/15/10 SpikeMix = Restek A069729: 50 µl Pct Recovery = 42% Analysis Date = 08/17/10 SpikeMix = Restek A069729: 50 µl Pct Recovery = 38% Analysis Date = 07/20/10 SpikeMix = Spex Organics T1090819006: 50 µl Pct Recovery = 36% Analysis Date = 09/08/10 SpikeMix = Spex Organics T1090819006: 50 µl Pct Recovery = 33% Analysis Date = 08/19/09 SpikeMix = NWQL LCL11SP078A: 100 µl Pct Recovery = 16% Analysis Date = 09/17/09 SpikeMix = Restek A063896: 40 µl Pct Recovery = 17% Analysis Date = 11/04/08 SpikeMix = Protocol T1080910002: 40 µl Pct Recovery = 38% Analysis Date = 06/22/09 SpikeMix = Protocol T1080910002: 40 µl Pct Recovery = 10% Analysis Date = 05/28/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 29% Analysis Date = 06/25/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 22% Analysis Date = 07/27/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 17% Analysis Date = 03/10/09 SpikeMix = Restek A063896: 25 µl Pct Recovery = 31% Analysis Date = 02/23/09 SpikeMix = Restek A063896: 25 µl Pct Recovery = 12% Analysis Date = 03/25/09 SpikeMix = Protocol T1080910002: 25 µl Pct Recovery = 14% Analysis Date = 09/24/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 20% Analysis Date = 05/06/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 41% Analysis Date = 09/24/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 18% Analysis Date = 12/16/08 SpikeMix = Restek A063896: 25 µl Pct Recovery = 26% Analysis Date = 11/20/08 SpikeMix = Protocol T1080910002: 25 µl Pct Recovery = 61% Analysis Date = 05/25/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 35% Analysis Date = 12/14/09 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 33% Analysis Date = 11/12/09 SpikeMix = Restek A069729: 25 µl Pct Recovery = 19% Analysis Date = 02/08/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 41% Analysis Date = 04/08/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 35% Analysis Date = 06/23/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 41% Analysis Date = 09/10/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 73% Analysis Date = 04/08/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 29% Analysis Date = 06/02/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 55% Analysis Date = 07/21/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 48% Analysis Date = 03/03/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 21% Analysis Date = 04/16/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 18% Analysis Date = 06/18/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 29% Analysis Date = 07/23/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 32% Analysis Date = 05/14/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 38% Analysis Date = 08/14/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 33% Analysis Date = 05/20/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 18% Analysis Date = 06/18/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 38% Analysis Date = 06/30/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 24% Analysis Date = 08/26/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 33% Analysis Date = 08/05/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 20% Analysis Date = 10/01/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 9% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Median Pct Recovery = 31% Y = 1
The SGPlot Procedure