BQS OBSP Determination:
WARFARIN
METHOD: 2080 , TESTIDCODE: 6202400021
DATES: 03/03/08 - 09/16/11

Expected Conc. = 0.3335 Median Pct Recovery = 44% Expected Conc. = 0.3327 Median Pct Recovery = 44% Expected Conc. = 0.3327 Median Pct Recovery = 44% Expected Conc. = 0.327 Median Pct Recovery = 44% Expected Conc. = 0.327 Median Pct Recovery = 44% Expected Conc. = 0.3225 Median Pct Recovery = 44% Expected Conc. = 0.3225 Median Pct Recovery = 44% Expected Conc. = 0.2908 Median Pct Recovery = 44% Expected Conc. = 0.2908 Median Pct Recovery = 44% Expected Conc. = 0.2888 Median Pct Recovery = 44% Expected Conc. = 0.2888 Median Pct Recovery = 44% Expected Conc. = 0.2886 Median Pct Recovery = 44% Expected Conc. = 0.2886 Median Pct Recovery = 44% Expected Conc. = 0.2874 Median Pct Recovery = 44% Expected Conc. = 0.2874 Median Pct Recovery = 44% Expected Conc. = 0.2861 Median Pct Recovery = 44% Expected Conc. = 0.2861 Median Pct Recovery = 44% Expected Conc. = 0.2578 Median Pct Recovery = 44% Expected Conc. = 0.2578 Median Pct Recovery = 44% Expected Conc. = 0.2544 Median Pct Recovery = 44% Expected Conc. = 0.2544 Median Pct Recovery = 44% Expected Conc. = 0.2498 Median Pct Recovery = 44% Expected Conc. = 0.2498 Median Pct Recovery = 44% Expected Conc. = 0.2008 Median Pct Recovery = 44% Expected Conc. = 0.2008 Median Pct Recovery = 44% Expected Conc. = 0.1983 Median Pct Recovery = 44% Expected Conc. = 0.1983 Median Pct Recovery = 44% Expected Conc. = 0.1968 Median Pct Recovery = 44% Expected Conc. = 0.1968 Median Pct Recovery = 44% Expected Conc. = 0.182 Median Pct Recovery = 44% Expected Conc. = 0.182 Median Pct Recovery = 44% Expected Conc. = 0.1818 Median Pct Recovery = 44% Expected Conc. = 0.1818 Median Pct Recovery = 44% Expected Conc. = 0.1805 Median Pct Recovery = 44% Expected Conc. = 0.1805 Median Pct Recovery = 44% Expected Conc. = 0.1804 Median Pct Recovery = 44% Expected Conc. = 0.1804 Median Pct Recovery = 44% Expected Conc. = 0.1798 Median Pct Recovery = 44% Expected Conc. = 0.1798 Median Pct Recovery = 44% Expected Conc. = 0.1793 Median Pct Recovery = 44% Expected Conc. = 0.1793 Median Pct Recovery = 44% Expected Conc. = 0.1791 Median Pct Recovery = 44% Expected Conc. = 0.1791 Median Pct Recovery = 44% Expected Conc. = 0.1694 Median Pct Recovery = 44% Expected Conc. = 0.1694 Median Pct Recovery = 44% Expected Conc. = 0.1689 Median Pct Recovery = 44% Expected Conc. = 0.1689 Median Pct Recovery = 44% Expected Conc. = 0.1671 Median Pct Recovery = 44% Expected Conc. = 0.1671 Median Pct Recovery = 44% Expected Conc. = 0.1664 Median Pct Recovery = 44% Expected Conc. = 0.1664 Median Pct Recovery = 44% Expected Conc. = 0.1661 Median Pct Recovery = 44% Expected Conc. = 0.1661 Median Pct Recovery = 44% Expected Conc. = 0.1636 Median Pct Recovery = 44% Expected Conc. = 0.1636 Median Pct Recovery = 44% Expected Conc. = 0.1635 Median Pct Recovery = 44% Expected Conc. = 0.1635 Median Pct Recovery = 44% Expected Conc. = 0.1635 Median Pct Recovery = 44% Expected Conc. = 0.1635 Median Pct Recovery = 44% Expected Conc. = 0.1624 Median Pct Recovery = 44% Expected Conc. = 0.1624 Median Pct Recovery = 44% Expected Conc. = 0.1623 Median Pct Recovery = 44% Expected Conc. = 0.1623 Median Pct Recovery = 44% Expected Conc. = 0.1619 Median Pct Recovery = 44% Expected Conc. = 0.1619 Median Pct Recovery = 44% Expected Conc. = 0.1614 Median Pct Recovery = 44% Expected Conc. = 0.1614 Median Pct Recovery = 44% Expected Conc. = 0.1591 Median Pct Recovery = 44% Expected Conc. = 0.1591 Median Pct Recovery = 44% Expected Conc. = 0.1582 Median Pct Recovery = 44% Expected Conc. = 0.1582 Median Pct Recovery = 44% Expected Conc. = 0.158 Median Pct Recovery = 44% Expected Conc. = 0.158 Median Pct Recovery = 44% Expected Conc. = 0.1279 Median Pct Recovery = 44% Expected Conc. = 0.1279 Median Pct Recovery = 44% Expected Conc. = 0.1277 Median Pct Recovery = 44% Expected Conc. = 0.1277 Median Pct Recovery = 44% Expected Conc. = 0.1275 Median Pct Recovery = 44% Expected Conc. = 0.1275 Median Pct Recovery = 44% Expected Conc. = 0.1257 Median Pct Recovery = 44% Expected Conc. = 0.1257 Median Pct Recovery = 44% Expected Conc. = 0.1242 Median Pct Recovery = 44% Expected Conc. = 0.1242 Median Pct Recovery = 44% Expected Conc. = 0.1145 Median Pct Recovery = 44% Expected Conc. = 0.1145 Median Pct Recovery = 44% Expected Conc. = 0.1123 Median Pct Recovery = 44% Expected Conc. = 0.1123 Median Pct Recovery = 44% Expected Conc. = 0.1117 Median Pct Recovery = 44% Expected Conc. = 0.1117 Median Pct Recovery = 44% Expected Conc. = 0.1114 Median Pct Recovery = 44% Expected Conc. = 0.1114 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1109 Median Pct Recovery = 44% Expected Conc. = 0.1107 Median Pct Recovery = 44% Expected Conc. = 0.1107 Median Pct Recovery = 44% Expected Conc. = 0.1105 Median Pct Recovery = 44% Expected Conc. = 0.1105 Median Pct Recovery = 44% Expected Conc. = 0.1104 Median Pct Recovery = 44% Expected Conc. = 0.1104 Median Pct Recovery = 44% Expected Conc. = 0.1102 Median Pct Recovery = 44% Expected Conc. = 0.1102 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.11 Median Pct Recovery = 44% Expected Conc. = 0.1091 Median Pct Recovery = 44% Expected Conc. = 0.1091 Median Pct Recovery = 44% Expected Conc. = 0.2578 Median Pct Recovery = 44% Expected Conc. = 0.2578 Median Pct Recovery = 44% Expected Conc. = 0.1985 Median Pct Recovery = 44% Expected Conc. = 0.1985 Median Pct Recovery = 44% Expected Conc. = 0.1095 Median Pct Recovery = 44% Analysis Date = 06/15/10 SpikeMix = Restek A069729: 50 µl Pct Recovery = 79% Analysis Date = 08/17/10 SpikeMix = Restek A069729: 50 µl Pct Recovery = 50% Analysis Date = 07/20/10 SpikeMix = Spex Organics T1090819006: 50 µl Pct Recovery = 42% Analysis Date = 09/08/10 SpikeMix = Spex Organics T1090819006: 50 µl Pct Recovery = 39% Analysis Date = 06/15/11 SpikeMix = Accu 210061380: 80 µl Pct Recovery = 4% Analysis Date = 08/26/11 SpikeMix = Accu 210061380: 80 µl Pct Recovery = 38% Analysis Date = 08/03/11 SpikeMix = Supelco LB77166: 80 µl Pct Recovery = 53% Analysis Date = 05/12/11 SpikeMix = Supelco LB77166: 80 µl Pct Recovery = 34% Analysis Date = 12/14/10 SpikeMix = Supelco LB77166: 80 µl Pct Recovery = 28% Analysis Date = 04/13/09 SpikeMix = Accu B8080253: 40 µl Pct Recovery = 33% Analysis Date = 09/25/09 SpikeMix = Supelco LB60728: 40 µl Pct Recovery = 49% Analysis Date = 08/19/09 SpikeMix = NWQL LCL11SP078A: 100 µl Pct Recovery = 56% Analysis Date = 05/28/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 61% Analysis Date = 06/25/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 54% Analysis Date = 07/27/09 SpikeMix = NWQL LCL11SP078A: 80 µl Pct Recovery = 38% Analysis Date = 04/13/11 SpikeMix = Supelco LB77166: 50 µl Pct Recovery = 18% Analysis Date = 01/04/11 SpikeMix = Accu 210061380: 50 µl Pct Recovery = 34% Analysis Date = 09/16/11 SpikeMix = Accu 210061380: 50 µl Pct Recovery = 9% Analysis Date = 07/05/11 SpikeMix = Supelco LB77166: 50 µl Pct Recovery = 14% Analysis Date = 03/23/11 SpikeMix = Supelco LB77166: 50 µl Pct Recovery = 52% Analysis Date = 11/15/10 SpikeMix = Accu 210061380: 50 µl Pct Recovery = 66% Analysis Date = 04/26/11 SpikeMix = Accu 210061380: 50 µl Pct Recovery = 27% Analysis Date = 03/02/09 SpikeMix = Supelco LB60728: 25 µl Pct Recovery = 38% Analysis Date = 09/24/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 35% Analysis Date = 05/06/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 89% Analysis Date = 09/24/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 19% Analysis Date = 12/05/08 SpikeMix = Supelco LB60728: 25 µl Pct Recovery = 49% Analysis Date = 05/25/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 48% Analysis Date = 07/15/09 SpikeMix = Supelco LB60728: 25 µl Pct Recovery = 35% Analysis Date = 12/14/09 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 43% Analysis Date = 04/13/09 SpikeMix = Accu B8080253: 25 µl Pct Recovery = 25% Analysis Date = 11/12/09 SpikeMix = Restek A069729: 25 µl Pct Recovery = 32% Analysis Date = 02/08/10 SpikeMix = Restek A069729: 25 µl Pct Recovery = 65% Analysis Date = 04/08/10 SpikeMix = Spex Organics T1090819006: 25 µl Pct Recovery = 48% Analysis Date = 04/29/09 SpikeMix = Supelco LB60728: 25 µl Pct Recovery = 41% Analysis Date = 11/13/08 SpikeMix = Accu B8080253: 25 µl Pct Recovery = 24% Analysis Date = 08/28/09 SpikeMix = Accu B8080253: 25 µl Pct Recovery = 33% Analysis Date = 06/23/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 82% Analysis Date = 09/10/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 97% Analysis Date = 04/08/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 74% Analysis Date = 06/02/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 66% Analysis Date = 07/21/10 SpikeMix = NWQL LCL11SP081A: 50 µl Pct Recovery = 66% Analysis Date = 03/03/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 37% Analysis Date = 04/16/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 69% Analysis Date = 05/20/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 21% Analysis Date = 06/18/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 96% Analysis Date = 06/04/08 SpikeMix = ChemService 385-69B: 50 µl Pct Recovery = 52% Analysis Date = 06/18/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 39% Analysis Date = 04/23/08 SpikeMix = ChemService 385-69B: 50 µl Pct Recovery = 43% Analysis Date = 06/30/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 53% Analysis Date = 10/01/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 17% Analysis Date = 07/23/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 70% Analysis Date = 05/14/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 44% Analysis Date = 08/14/08 SpikeMix = ERA 0710-07-02Rx: 50 µl Pct Recovery = 83% Analysis Date = 08/25/08 SpikeMix = ChemService 385-69B: 50 µl Pct Recovery = 68% Analysis Date = 08/26/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 85% Analysis Date = 08/05/08 SpikeMix = Protocol M1070727011: 50 µl Pct Recovery = 76% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Median Pct Recovery = 44% Y = 1
The SGPlot Procedure