BQS OBSP Determination:
3-CHLOROPROPENE
METHOD: 2021 , TESTIDCODE: 78109GCM66
Open Data Set

Analysis Date = 05/02/06 SpikeMix = NSI 080405-01VOC: 20 µl & Ultra CB-1578: 50 µl Pct Recovery = 109% Analysis Date = 01/27/06 SpikeMix = NSI 080405-01VOC: 20 µl & Supelco LB31918: 30 µl Pct Recovery = 131% Analysis Date = 04/07/06 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl Pct Recovery = 122% Analysis Date = 08/12/05 SpikeMix = Supelco LB22064: 15 µl Pct Recovery = 102% Analysis Date = 07/14/05 SpikeMix = Supelco LB22064: 15 µl Pct Recovery = 96% Analysis Date = 05/20/05 SpikeMix = Supelco LB22064: 15 µl Pct Recovery = 106% Analysis Date = 12/22/12 SpikeMix = NSI 062112-01VOA: 40 µl & Supelco LB92787: 40 µl Pct Recovery = 100% Analysis Date = 01/19/13 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl Pct Recovery = 115% Analysis Date = 09/19/07 SpikeMix = Restek A046581: 40 µl Pct Recovery = 101% Analysis Date = 07/27/07 SpikeMix = Restek A046581: 40 µl Pct Recovery = 121% Analysis Date = 05/31/07 SpikeMix = Restek A046581: 40 µl Pct Recovery = 117% Analysis Date = 04/03/07 SpikeMix = Restek A046581: 40 µl Pct Recovery = 101% Analysis Date = 01/09/07 SpikeMix = Restek A046581: 40 µl Pct Recovery = 103% Analysis Date = 10/14/06 SpikeMix = Restek A046581: 40 µl Pct Recovery = 108% Analysis Date = 02/26/99 SpikeMix = NSI Q-16750-50 101497: 25 µl Pct Recovery = 106% Analysis Date = 11/20/98 SpikeMix = NSI Q-16750-50 101497: 25 µl Pct Recovery = 104% Analysis Date = 09/11/12 SpikeMix = NSI 062112-01VOA: 20 µl & Supelco LB92787: 20 µl Pct Recovery = 91% Analysis Date = 07/30/12 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl Pct Recovery = 101% Analysis Date = 11/08/12 SpikeMix = Crescent 05BB048: 20 µl & Accu 212051193: 20 µl Pct Recovery = 102% Analysis Date = 11/02/01 SpikeMix = Ultra S0039: 8 µl Pct Recovery = 107% Analysis Date = 09/20/01 SpikeMix = Ultra S0039: 8 µl Pct Recovery = 109% Analysis Date = 06/09/01 SpikeMix = Ultra S0039: 8 µl Pct Recovery = 93% Analysis Date = 03/14/01 SpikeMix = Ultra S0039: 8 µl Pct Recovery = 97% Analysis Date = 08/25/05 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl Pct Recovery = 99% Analysis Date = 06/27/05 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl Pct Recovery = 100% Analysis Date = 07/26/05 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl Pct Recovery = 102% Analysis Date = 03/09/05 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl Pct Recovery = 112% Analysis Date = 04/15/05 SpikeMix = Supelco LB22064: 5 µl Pct Recovery = 102% Analysis Date = 02/11/05 SpikeMix = Supelco LB22064: 5 µl Pct Recovery = 99% Analysis Date = 08/13/06 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 101% Analysis Date = 03/15/06 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 109% Analysis Date = 05/17/06 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 103% Analysis Date = 12/08/05 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 101% Analysis Date = 02/14/06 SpikeMix = NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl Pct Recovery = 107% Analysis Date = 11/15/05 SpikeMix = NSI 080405-01VOC: 5 µl & Supelco LB31918: 5 µl Pct Recovery = 100% Analysis Date = 06/06/06 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl Pct Recovery = 112% Analysis Date = 05/03/13 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl Pct Recovery = 95% Analysis Date = 03/29/13 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl Pct Recovery = 113% Analysis Date = 02/28/13 SpikeMix = NSI 062112-01VOA: 10 µl & Accu 212051193: 10 µl Pct Recovery = 105% Analysis Date = 07/19/12 SpikeMix = Crescent 05BB048: 10 µl & Accu 212051193: 10 µl Pct Recovery = 97% Analysis Date = 05/24/02 SpikeMix = NSI Q-3183: 20 µl Pct Recovery = 104% Analysis Date = 02/22/02 SpikeMix = NSI Q-3183: 20 µl Pct Recovery = 105% Analysis Date = 06/17/10 SpikeMix = Accu 209081198: 30 µl Pct Recovery = 89% Analysis Date = 03/26/10 SpikeMix = Accu 209081198: 30 µl Pct Recovery = 79% Analysis Date = 12/24/09 SpikeMix = Accu 209081198: 30 µl Pct Recovery = 98% Analysis Date = 08/11/10 SpikeMix = Restek A069860: 30 µl Pct Recovery = 93% Analysis Date = 05/22/10 SpikeMix = Restek A069860: 30 µl Pct Recovery = 83% Analysis Date = 03/11/10 SpikeMix = Restek A069860: 30 µl Pct Recovery = 89% Analysis Date = 12/04/09 SpikeMix = Restek A069860: 30 µl Pct Recovery = 116% Analysis Date = 03/31/99 SpikeMix = NSI Q-16750-50 101497: 10 µl Pct Recovery = 126% Analysis Date = 01/20/99 SpikeMix = NSI Q-16750-50 101497: 10 µl Pct Recovery = 109% Analysis Date = 08/24/02 SpikeMix = Ultra S1214: 25 µl Pct Recovery = 97% Analysis Date = 05/09/02 SpikeMix = Ultra S1214: 25 µl Pct Recovery = 103% Analysis Date = 12/07/01 SpikeMix = Ultra S1214: 25 µl Pct Recovery = 117% Analysis Date = 12/20/08 SpikeMix = NSI 021408-01: 20 µl Pct Recovery = 92% Analysis Date = 12/03/08 SpikeMix = NSI 021408-01: 20 µl Pct Recovery = 89% Analysis Date = 08/30/08 SpikeMix = NSI 021408-01: 20 µl Pct Recovery = 89% Analysis Date = 06/25/08 SpikeMix = NSI 021408-01: 20 µl Pct Recovery = 113% Analysis Date = 05/16/08 SpikeMix = NSI 021408-01: 20 µl Pct Recovery = 103% Analysis Date = 07/24/08 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 134% Analysis Date = 07/17/08 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 89% Analysis Date = 06/06/08 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 106% Analysis Date = 04/18/08 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 99% Analysis Date = 01/17/08 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 103% Analysis Date = 11/10/07 SpikeMix = ERA 0709-07-04VOC: 20 µl Pct Recovery = 99% Analysis Date = 04/04/02 SpikeMix = NSI Q-3183: 10 µl Pct Recovery = 101% Analysis Date = 01/04/02 SpikeMix = NSI Q-3183: 10 µl Pct Recovery = 105% Analysis Date = 05/25/12 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 96% Analysis Date = 05/08/12 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 87% Analysis Date = 11/24/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 90% Analysis Date = 06/10/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 93% Analysis Date = 04/13/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 86% Analysis Date = 01/22/11 SpikeMix = NSI 062310-01: 40 µl Pct Recovery = 86% Analysis Date = 04/21/09 SpikeMix = Abs 080408VOC: 40 µl Pct Recovery = 125% Analysis Date = 01/27/09 SpikeMix = Abs 080408VOC: 40 µl Pct Recovery = 94% Analysis Date = 03/01/14 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 83% Analysis Date = 07/24/13 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 96% Analysis Date = 09/17/13 SpikeMix = Crescent 04CC151: 20 µl & Supelco LC00154: 20 µl Pct Recovery = 86% Analysis Date = 01/29/14 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 97% Analysis Date = 09/17/13 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 108% Analysis Date = 08/06/13 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl Pct Recovery = 91% Analysis Date = 11/01/13 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl Pct Recovery = 83% Analysis Date = 12/12/13 SpikeMix = NSI 053013: 20 µl & Accu 213041120: 20 µl Pct Recovery = 95% Analysis Date = 06/30/09 SpikeMix = Ultra CE-2869: 40 µl Pct Recovery = 93% Analysis Date = 06/17/09 SpikeMix = Ultra CE-2869: 40 µl Pct Recovery = 93% Analysis Date = 09/01/10 SpikeMix = Accu 209081198: 10 µl Pct Recovery = 96% Analysis Date = 07/16/10 SpikeMix = Accu 209081198: 10 µl Pct Recovery = 95% Analysis Date = 05/05/10 SpikeMix = Accu 209081198: 10 µl Pct Recovery = 86% Analysis Date = 02/19/10 SpikeMix = Accu 209081198: 10 µl Pct Recovery = 98% Analysis Date = 11/10/09 SpikeMix = Accu 209081198: 10 µl Pct Recovery = 96% Analysis Date = 09/21/10 SpikeMix = Restek A069860: 10 µl Pct Recovery = 92% Analysis Date = 07/09/10 SpikeMix = Restek A069860: 10 µl Pct Recovery = 99% Analysis Date = 04/13/10 SpikeMix = Restek A069860: 10 µl Pct Recovery = 87% Analysis Date = 01/26/10 SpikeMix = Restek A069860: 10 µl Pct Recovery = 91% Analysis Date = 10/22/09 SpikeMix = Restek A069860: 10 µl Pct Recovery = 108% Analysis Date = 09/10/02 SpikeMix = Ultra S1214: 10 µl Pct Recovery = 93% Analysis Date = 06/21/02 SpikeMix = Ultra S1214: 10 µl Pct Recovery = 93% Analysis Date = 03/16/02 SpikeMix = Ultra S1214: 10 µl Pct Recovery = 122% Analysis Date = 02/02/02 SpikeMix = Ultra S1214: 10 µl Pct Recovery = 127% Analysis Date = 03/10/12 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 92% Analysis Date = 10/18/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 93% Analysis Date = 09/17/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 96% Analysis Date = 05/03/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 97% Analysis Date = 03/01/11 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 103% Analysis Date = 11/05/10 SpikeMix = NSI 062310-01: 20 µl Pct Recovery = 94% Analysis Date = 08/29/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 104% Analysis Date = 07/17/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 94% Analysis Date = 06/09/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 94% Analysis Date = 03/14/09 SpikeMix = Abs 080408VOC: 20 µl Pct Recovery = 83% Analysis Date = 09/17/13 SpikeMix = Crescent 04CC151: 10 µl & Supelco LC00154: 10 µl Pct Recovery = 89% Analysis Date = 12/12/13 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl Pct Recovery = 116% Analysis Date = 12/31/13 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl Pct Recovery = 91% Analysis Date = 01/15/14 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl Pct Recovery = 82% Analysis Date = 05/22/13 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl Pct Recovery = 93% Analysis Date = 03/19/14 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl Pct Recovery = 101% Analysis Date = 06/08/13 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl Pct Recovery = 96% Analysis Date = 08/11/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 112% Analysis Date = 03/31/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 112% Analysis Date = 02/18/09 SpikeMix = Ultra CE-2869: 20 µl Pct Recovery = 87% Analysis Date = 11/29/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 97% Analysis Date = 09/17/06 SpikeMix = NSI 080405-01VOC: 2 µl Pct Recovery = 108% Analysis Date = 03/23/06 SpikeMix = NSI 080405-01VOC: 2 µl Pct Recovery = 123% Analysis Date = 09/19/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 114% Analysis Date = 08/02/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 103% Analysis Date = 07/06/00 SpikeMix = NSI 053100-01: 2 µl Pct Recovery = 99% Analysis Date = 03/18/14 Pct Recovery = 96% Analysis Date = 02/19/14 Pct Recovery = 96% Analysis Date = 02/19/14 Pct Recovery = 96% Analysis Date = 01/22/14 Pct Recovery = 96% Analysis Date = 01/22/14 Pct Recovery = 96% Analysis Date = 12/25/13 Pct Recovery = 96% Analysis Date = 12/25/13 Pct Recovery = 96% Analysis Date = 11/27/13 Pct Recovery = 96% Analysis Date = 11/27/13 Pct Recovery = 96% Analysis Date = 10/30/13 Pct Recovery = 96% Analysis Date = 10/30/13 Pct Recovery = 96% Analysis Date = 10/02/13 Pct Recovery = 96% Analysis Date = 10/02/13 Pct Recovery = 96% Analysis Date = 09/04/13 Pct Recovery = 96% Analysis Date = 09/04/13 Pct Recovery = 96% Analysis Date = 08/07/13 Pct Recovery = 96% Analysis Date = 08/07/13 Pct Recovery = 96% Analysis Date = 07/10/13 Pct Recovery = 96% Analysis Date = 07/10/13 Pct Recovery = 96% Analysis Date = 06/12/13 Pct Recovery = 96% Analysis Date = 06/12/13 Pct Recovery = 96% Analysis Date = 05/15/13 Pct Recovery = 96% Analysis Date = 05/15/13 Pct Recovery = 96% Analysis Date = 04/17/13 Pct Recovery = 96% Analysis Date = 04/17/13 Pct Recovery = 96% Analysis Date = 03/20/13 Pct Recovery = 96% Analysis Date = 03/20/13 Pct Recovery = 96% Analysis Date = 02/20/13 Pct Recovery = 96% Analysis Date = 02/20/13 Pct Recovery = 96% Analysis Date = 01/23/13 Pct Recovery = 96% Analysis Date = 01/23/13 Pct Recovery = 96% Analysis Date = 12/26/12 Pct Recovery = 96% Analysis Date = 12/26/12 Pct Recovery = 96% Analysis Date = 11/28/12 Pct Recovery = 96% Analysis Date = 11/28/12 Pct Recovery = 96% Analysis Date = 10/31/12 Pct Recovery = 95% Analysis Date = 10/31/12 Pct Recovery = 95% Analysis Date = 10/03/12 Pct Recovery = 95% Analysis Date = 10/03/12 Pct Recovery = 95% Analysis Date = 09/05/12 Pct Recovery = 95% Analysis Date = 09/05/12 Pct Recovery = 95% Analysis Date = 08/08/12 Pct Recovery = 95% Analysis Date = 08/08/12 Pct Recovery = 95% Analysis Date = 07/11/12 Pct Recovery = 95% Analysis Date = 07/11/12 Pct Recovery = 95% Analysis Date = 06/13/12 Pct Recovery = 95% Analysis Date = 06/13/12 Pct Recovery = 95% Analysis Date = 05/16/12 Pct Recovery = 95% Analysis Date = 05/16/12 Pct Recovery = 95% Analysis Date = 04/18/12 Pct Recovery = 95% Analysis Date = 04/18/12 Pct Recovery = 95% Analysis Date = 03/21/12 Pct Recovery = 95% Analysis Date = 03/21/12 Pct Recovery = 95% Analysis Date = 02/22/12 Pct Recovery = 95% Analysis Date = 02/22/12 Pct Recovery = 95% Analysis Date = 01/25/12 Pct Recovery = 95% Analysis Date = 01/25/12 Pct Recovery = 95% Analysis Date = 12/28/11 Pct Recovery = 95% Analysis Date = 12/28/11 Pct Recovery = 95% Analysis Date = 11/30/11 Pct Recovery = 95% Analysis Date = 11/30/11 Pct Recovery = 95% Analysis Date = 11/02/11 Pct Recovery = 95% Analysis Date = 11/02/11 Pct Recovery = 95% Analysis Date = 10/05/11 Pct Recovery = 95% Analysis Date = 10/05/11 Pct Recovery = 95% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 08/10/11 Pct Recovery = 95% Analysis Date = 08/10/11 Pct Recovery = 95% Analysis Date = 07/13/11 Pct Recovery = 95% Analysis Date = 07/13/11 Pct Recovery = 95% Analysis Date = 06/15/11 Pct Recovery = 95% Analysis Date = 06/15/11 Pct Recovery = 95% Analysis Date = 05/18/11 Pct Recovery = 95% Analysis Date = 05/18/11 Pct Recovery = 95% Analysis Date = 04/20/11 Pct Recovery = 96% Analysis Date = 04/20/11 Pct Recovery = 96% Analysis Date = 03/23/11 Pct Recovery = 96% Analysis Date = 03/23/11 Pct Recovery = 96% Analysis Date = 02/23/11 Pct Recovery = 96% Analysis Date = 02/23/11 Pct Recovery = 96% Analysis Date = 01/26/11 Pct Recovery = 96% Analysis Date = 01/26/11 Pct Recovery = 96% Analysis Date = 12/29/10 Pct Recovery = 96% Analysis Date = 12/29/10 Pct Recovery = 96% Analysis Date = 12/01/10 Pct Recovery = 96% Analysis Date = 12/01/10 Pct Recovery = 96% Analysis Date = 11/03/10 Pct Recovery = 96% Analysis Date = 11/03/10 Pct Recovery = 96% Analysis Date = 10/06/10 Pct Recovery = 96% Analysis Date = 10/06/10 Pct Recovery = 96% Analysis Date = 09/08/10 Pct Recovery = 96% Analysis Date = 09/08/10 Pct Recovery = 96% Analysis Date = 08/11/10 Pct Recovery = 96% Analysis Date = 08/11/10 Pct Recovery = 96% Analysis Date = 07/14/10 Pct Recovery = 96% Analysis Date = 07/14/10 Pct Recovery = 96% Analysis Date = 06/16/10 Pct Recovery = 96% Analysis Date = 06/16/10 Pct Recovery = 96% Analysis Date = 05/19/10 Pct Recovery = 96% Analysis Date = 05/19/10 Pct Recovery = 96% Analysis Date = 04/21/10 Pct Recovery = 96% Analysis Date = 04/21/10 Pct Recovery = 96% Analysis Date = 03/24/10 Pct Recovery = 96% Analysis Date = 03/24/10 Pct Recovery = 96% Analysis Date = 02/24/10 Pct Recovery = 96% Analysis Date = 02/24/10 Pct Recovery = 96% Analysis Date = 01/27/10 Pct Recovery = 97% Analysis Date = 01/27/10 Pct Recovery = 97% Analysis Date = 12/30/09 Pct Recovery = 97% Analysis Date = 12/30/09 Pct Recovery = 97% Analysis Date = 12/02/09 Pct Recovery = 97% Analysis Date = 12/02/09 Pct Recovery = 97% Analysis Date = 11/04/09 Pct Recovery = 97% Analysis Date = 11/04/09 Pct Recovery = 97% Analysis Date = 10/07/09 Pct Recovery = 97% Analysis Date = 10/07/09 Pct Recovery = 97% Analysis Date = 09/09/09 Pct Recovery = 98% Analysis Date = 09/09/09 Pct Recovery = 98% Analysis Date = 08/12/09 Pct Recovery = 98% Analysis Date = 08/12/09 Pct Recovery = 98% Analysis Date = 07/15/09 Pct Recovery = 98% Analysis Date = 07/15/09 Pct Recovery = 98% Analysis Date = 06/17/09 Pct Recovery = 98% Analysis Date = 06/17/09 Pct Recovery = 98% Analysis Date = 05/20/09 Pct Recovery = 99% Analysis Date = 05/20/09 Pct Recovery = 99% Analysis Date = 04/22/09 Pct Recovery = 99% Analysis Date = 04/22/09 Pct Recovery = 99% Analysis Date = 03/25/09 Pct Recovery = 99% Analysis Date = 03/25/09 Pct Recovery = 99% Analysis Date = 02/25/09 Pct Recovery = 100% Analysis Date = 02/25/09 Pct Recovery = 100% Analysis Date = 01/28/09 Pct Recovery = 100% Analysis Date = 01/28/09 Pct Recovery = 100% Analysis Date = 12/31/08 Pct Recovery = 100% Analysis Date = 12/31/08 Pct Recovery = 100% Analysis Date = 12/03/08 Pct Recovery = 100% Analysis Date = 12/03/08 Pct Recovery = 100% Analysis Date = 11/05/08 Pct Recovery = 100% Analysis Date = 11/05/08 Pct Recovery = 100% Analysis Date = 10/08/08 Pct Recovery = 101% Analysis Date = 10/08/08 Pct Recovery = 101% Analysis Date = 09/10/08 Pct Recovery = 101% Analysis Date = 09/10/08 Pct Recovery = 101% Analysis Date = 08/13/08 Pct Recovery = 101% Analysis Date = 08/13/08 Pct Recovery = 101% Analysis Date = 07/16/08 Pct Recovery = 101% Analysis Date = 07/16/08 Pct Recovery = 101% Analysis Date = 06/18/08 Pct Recovery = 101% Analysis Date = 06/18/08 Pct Recovery = 101% Analysis Date = 05/21/08 Pct Recovery = 102% Analysis Date = 05/21/08 Pct Recovery = 102% Analysis Date = 04/23/08 Pct Recovery = 102% Analysis Date = 04/23/08 Pct Recovery = 102% Analysis Date = 03/26/08 Pct Recovery = 102% Analysis Date = 03/26/08 Pct Recovery = 102% Analysis Date = 02/27/08 Pct Recovery = 102% Analysis Date = 02/27/08 Pct Recovery = 102% Analysis Date = 01/30/08 Pct Recovery = 102% Analysis Date = 01/30/08 Pct Recovery = 102% Analysis Date = 01/02/08 Pct Recovery = 103% Analysis Date = 01/02/08 Pct Recovery = 103% Analysis Date = 12/05/07 Pct Recovery = 103% Analysis Date = 12/05/07 Pct Recovery = 103% Analysis Date = 11/07/07 Pct Recovery = 103% Analysis Date = 11/07/07 Pct Recovery = 103% Analysis Date = 10/11/07 Pct Recovery = 103% Analysis Date = 10/11/07 Pct Recovery = 103% Analysis Date = 09/13/07 Pct Recovery = 103% Analysis Date = 09/13/07 Pct Recovery = 103% Analysis Date = 08/16/07 Pct Recovery = 104% Analysis Date = 08/16/07 Pct Recovery = 104% Analysis Date = 07/19/07 Pct Recovery = 104% Analysis Date = 07/19/07 Pct Recovery = 104% Analysis Date = 06/21/07 Pct Recovery = 104% Analysis Date = 06/21/07 Pct Recovery = 104% Analysis Date = 05/24/07 Pct Recovery = 104% Analysis Date = 05/24/07 Pct Recovery = 104% Analysis Date = 04/26/07 Pct Recovery = 104% Analysis Date = 04/26/07 Pct Recovery = 104% Analysis Date = 03/29/07 Pct Recovery = 104% Analysis Date = 03/29/07 Pct Recovery = 104% Analysis Date = 03/01/07 Pct Recovery = 105% Analysis Date = 03/01/07 Pct Recovery = 105% Analysis Date = 02/01/07 Pct Recovery = 105% Analysis Date = 02/01/07 Pct Recovery = 105% Analysis Date = 01/04/07 Pct Recovery = 105% Analysis Date = 01/04/07 Pct Recovery = 105% Analysis Date = 12/07/06 Pct Recovery = 105% Analysis Date = 12/07/06 Pct Recovery = 105% Analysis Date = 11/09/06 Pct Recovery = 105% Analysis Date = 11/09/06 Pct Recovery = 105% Analysis Date = 10/12/06 Pct Recovery = 105% Analysis Date = 10/12/06 Pct Recovery = 105% Analysis Date = 09/14/06 Pct Recovery = 105% Analysis Date = 09/14/06 Pct Recovery = 105% Analysis Date = 08/17/06 Pct Recovery = 106% Analysis Date = 08/17/06 Pct Recovery = 106% Analysis Date = 07/20/06 Pct Recovery = 106% Analysis Date = 07/20/06 Pct Recovery = 106% Analysis Date = 06/22/06 Pct Recovery = 106% Analysis Date = 06/22/06 Pct Recovery = 106% Analysis Date = 05/25/06 Pct Recovery = 106% Analysis Date = 05/25/06 Pct Recovery = 106% Analysis Date = 04/27/06 Pct Recovery = 106% Analysis Date = 04/27/06 Pct Recovery = 106% Analysis Date = 03/30/06 Pct Recovery = 106% Analysis Date = 03/30/06 Pct Recovery = 106% Analysis Date = 03/02/06 Pct Recovery = 106% Analysis Date = 03/02/06 Pct Recovery = 106% Analysis Date = 02/02/06 Pct Recovery = 106% Analysis Date = 02/02/06 Pct Recovery = 106% Analysis Date = 01/05/06 Pct Recovery = 106% Analysis Date = 01/05/06 Pct Recovery = 106% Analysis Date = 12/08/05 Pct Recovery = 106% Analysis Date = 12/08/05 Pct Recovery = 106% Analysis Date = 11/10/05 Pct Recovery = 106% Analysis Date = 11/10/05 Pct Recovery = 106% Analysis Date = 10/13/05 Pct Recovery = 106% Analysis Date = 10/13/05 Pct Recovery = 106% Analysis Date = 09/15/05 Pct Recovery = 106% Analysis Date = 09/15/05 Pct Recovery = 106% Analysis Date = 08/18/05 Pct Recovery = 106% Analysis Date = 08/18/05 Pct Recovery = 106% Analysis Date = 07/21/05 Pct Recovery = 106% Analysis Date = 07/21/05 Pct Recovery = 106% Analysis Date = 06/23/05 Pct Recovery = 106% Analysis Date = 06/23/05 Pct Recovery = 106% Analysis Date = 05/26/05 Pct Recovery = 106% Analysis Date = 05/26/05 Pct Recovery = 106% Analysis Date = 04/28/05 Pct Recovery = 106% Analysis Date = 04/28/05 Pct Recovery = 106% Analysis Date = 03/31/05 Pct Recovery = 106% Analysis Date = 03/31/05 Pct Recovery = 106% Analysis Date = 03/03/05 Pct Recovery = 106% Analysis Date = 03/03/05 Pct Recovery = 106% Analysis Date = 02/03/05 Pct Recovery = 106% Analysis Date = 02/03/05 Pct Recovery = 106% Analysis Date = 01/06/05 Pct Recovery = 106% Analysis Date = 01/06/05 Pct Recovery = 106% Analysis Date = 12/09/04 Pct Recovery = 106% Analysis Date = 12/09/04 Pct Recovery = 106% Analysis Date = 11/11/04 Pct Recovery = 106% Analysis Date = 11/11/04 Pct Recovery = 106% Analysis Date = 10/14/04 Pct Recovery = 106% Analysis Date = 10/14/04 Pct Recovery = 106% Analysis Date = 09/16/04 Pct Recovery = 106% Analysis Date = 09/16/04 Pct Recovery = 106% Analysis Date = 08/19/04 Pct Recovery = 106% Analysis Date = 08/19/04 Pct Recovery = 106% Analysis Date = 07/22/04 Pct Recovery = 106% Analysis Date = 07/22/04 Pct Recovery = 106% Analysis Date = 06/24/04 Pct Recovery = 106% Analysis Date = 06/24/04 Pct Recovery = 106% Analysis Date = 05/27/04 Pct Recovery = 106% Analysis Date = 05/27/04 Pct Recovery = 106% Analysis Date = 04/29/04 Pct Recovery = 106% Analysis Date = 04/29/04 Pct Recovery = 106% Analysis Date = 04/01/04 Pct Recovery = 106% Analysis Date = 04/01/04 Pct Recovery = 106% Analysis Date = 03/04/04 Pct Recovery = 106% Analysis Date = 03/04/04 Pct Recovery = 106% Analysis Date = 02/05/04 Pct Recovery = 106% Analysis Date = 02/05/04 Pct Recovery = 106% Analysis Date = 01/08/04 Pct Recovery = 106% Analysis Date = 01/08/04 Pct Recovery = 106% Analysis Date = 12/11/03 Pct Recovery = 106% Analysis Date = 12/11/03 Pct Recovery = 106% Analysis Date = 11/13/03 Pct Recovery = 106% Analysis Date = 11/13/03 Pct Recovery = 106% Analysis Date = 10/16/03 Pct Recovery = 106% Analysis Date = 10/16/03 Pct Recovery = 106% Analysis Date = 09/18/03 Pct Recovery = 106% Analysis Date = 09/18/03 Pct Recovery = 106% Analysis Date = 08/21/03 Pct Recovery = 106% Analysis Date = 08/21/03 Pct Recovery = 106% Analysis Date = 07/24/03 Pct Recovery = 106% Analysis Date = 07/24/03 Pct Recovery = 106% Analysis Date = 06/26/03 Pct Recovery = 106% Analysis Date = 06/26/03 Pct Recovery = 106% Analysis Date = 05/29/03 Pct Recovery = 106% Analysis Date = 05/29/03 Pct Recovery = 106% Analysis Date = 05/01/03 Pct Recovery = 106% Analysis Date = 05/01/03 Pct Recovery = 106% Analysis Date = 04/03/03 Pct Recovery = 106% Analysis Date = 04/03/03 Pct Recovery = 106% Analysis Date = 03/06/03 Pct Recovery = 106% Analysis Date = 03/06/03 Pct Recovery = 106% Analysis Date = 02/06/03 Pct Recovery = 106% Analysis Date = 02/06/03 Pct Recovery = 106% Analysis Date = 01/09/03 Pct Recovery = 106% Analysis Date = 01/09/03 Pct Recovery = 106% Analysis Date = 12/12/02 Pct Recovery = 106% Analysis Date = 12/12/02 Pct Recovery = 106% Analysis Date = 11/14/02 Pct Recovery = 106% Analysis Date = 11/14/02 Pct Recovery = 106% Analysis Date = 10/17/02 Pct Recovery = 106% Analysis Date = 10/17/02 Pct Recovery = 106% Analysis Date = 09/19/02 Pct Recovery = 106% Analysis Date = 09/19/02 Pct Recovery = 106% Analysis Date = 08/22/02 Pct Recovery = 106% Analysis Date = 08/22/02 Pct Recovery = 106% Analysis Date = 07/25/02 Pct Recovery = 106% Analysis Date = 07/25/02 Pct Recovery = 106% Analysis Date = 06/27/02 Pct Recovery = 106% Analysis Date = 06/27/02 Pct Recovery = 106% Analysis Date = 05/30/02 Pct Recovery = 106% Analysis Date = 05/30/02 Pct Recovery = 106% Analysis Date = 05/02/02 Pct Recovery = 106% Analysis Date = 05/02/02 Pct Recovery = 106% Analysis Date = 04/04/02 Pct Recovery = 106% Analysis Date = 04/04/02 Pct Recovery = 106% Analysis Date = 03/07/02 Pct Recovery = 106% Analysis Date = 03/07/02 Pct Recovery = 106% Analysis Date = 02/07/02 Pct Recovery = 106% Analysis Date = 02/07/02 Pct Recovery = 106% Analysis Date = 01/10/02 Pct Recovery = 106% Analysis Date = 01/10/02 Pct Recovery = 106% Analysis Date = 12/13/01 Pct Recovery = 106% Analysis Date = 12/13/01 Pct Recovery = 106% Analysis Date = 11/15/01 Pct Recovery = 106% Analysis Date = 11/15/01 Pct Recovery = 106% Analysis Date = 10/18/01 Pct Recovery = 106% Analysis Date = 10/18/01 Pct Recovery = 106% Analysis Date = 09/20/01 Pct Recovery = 106% Analysis Date = 09/20/01 Pct Recovery = 106% Analysis Date = 08/23/01 Pct Recovery = 106% Analysis Date = 08/23/01 Pct Recovery = 106% Analysis Date = 07/26/01 Pct Recovery = 106% Analysis Date = 07/26/01 Pct Recovery = 106% Analysis Date = 06/28/01 Pct Recovery = 106% Analysis Date = 06/28/01 Pct Recovery = 106% Analysis Date = 05/31/01 Pct Recovery = 106% Analysis Date = 05/31/01 Pct Recovery = 106% Analysis Date = 05/04/01 Pct Recovery = 106% Analysis Date = 05/04/01 Pct Recovery = 106% Analysis Date = 04/06/01 Pct Recovery = 106% Analysis Date = 04/06/01 Pct Recovery = 106% Analysis Date = 03/09/01 Pct Recovery = 106% Analysis Date = 03/09/01 Pct Recovery = 106% Analysis Date = 02/09/01 Pct Recovery = 106% Analysis Date = 02/09/01 Pct Recovery = 106% Analysis Date = 01/12/01 Pct Recovery = 106% Analysis Date = 01/12/01 Pct Recovery = 106% Analysis Date = 12/15/00 Pct Recovery = 106% Analysis Date = 12/15/00 Pct Recovery = 106% Analysis Date = 11/17/00 Pct Recovery = 106% Analysis Date = 11/17/00 Pct Recovery = 106% Analysis Date = 10/20/00 Pct Recovery = 106% Analysis Date = 10/20/00 Pct Recovery = 106% Analysis Date = 09/22/00 Pct Recovery = 106% Analysis Date = 09/22/00 Pct Recovery = 106% Analysis Date = 08/25/00 Pct Recovery = 106% Analysis Date = 08/25/00 Pct Recovery = 106% Analysis Date = 07/28/00 Pct Recovery = 106% Analysis Date = 07/28/00 Pct Recovery = 106% Analysis Date = 06/30/00 Pct Recovery = 106% Analysis Date = 06/30/00 Pct Recovery = 106% Analysis Date = 06/02/00 Pct Recovery = 106% Analysis Date = 06/02/00 Pct Recovery = 106% Analysis Date = 05/05/00 Pct Recovery = 106% Analysis Date = 05/05/00 Pct Recovery = 106% Analysis Date = 04/07/00 Pct Recovery = 106% Analysis Date = 04/07/00 Pct Recovery = 106% Analysis Date = 03/10/00 Pct Recovery = 106% Analysis Date = 03/10/00 Pct Recovery = 106% Analysis Date = 02/11/00 Pct Recovery = 106% Analysis Date = 02/11/00 Pct Recovery = 106% Analysis Date = 01/14/00 Pct Recovery = 106% Analysis Date = 01/14/00 Pct Recovery = 106% Analysis Date = 12/17/99 Pct Recovery = 106% Analysis Date = 12/17/99 Pct Recovery = 106% Analysis Date = 11/19/99 Pct Recovery = 106% Analysis Date = 11/19/99 Pct Recovery = 106% Analysis Date = 10/22/99 Pct Recovery = 106% Analysis Date = 10/22/99 Pct Recovery = 106% Analysis Date = 09/24/99 Pct Recovery = 106% Analysis Date = 09/24/99 Pct Recovery = 106% Analysis Date = 08/27/99 Pct Recovery = 106% Analysis Date = 08/27/99 Pct Recovery = 106% Analysis Date = 07/30/99 Pct Recovery = 106% Analysis Date = 07/30/99 Pct Recovery = 106% Analysis Date = 07/02/99 Pct Recovery = 106% Analysis Date = 07/02/99 Pct Recovery = 106% Analysis Date = 06/04/99 Pct Recovery = 106% Analysis Date = 06/04/99 Pct Recovery = 106% Analysis Date = 05/07/99 Pct Recovery = 106% Analysis Date = 05/07/99 Pct Recovery = 106% Analysis Date = 04/09/99 Pct Recovery = 107% Analysis Date = 04/09/99 Pct Recovery = 107% Analysis Date = 03/12/99 Pct Recovery = 107% Analysis Date = 03/12/99 Pct Recovery = 107% Analysis Date = 02/12/99 Pct Recovery = 107% Analysis Date = 02/12/99 Pct Recovery = 107% Analysis Date = 01/15/99 Pct Recovery = 107% Analysis Date = 01/15/99 Pct Recovery = 107% Analysis Date = 12/18/98 Pct Recovery = 107% Analysis Date = 12/18/98 Pct Recovery = 107% Analysis Date = 11/20/98 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-CHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 109% 10% 108% 9%
>= Reporting Level 120 100% 11% 99% 10%
Total 125 101% 11% 99% 10%

Sample Statistics
3-CHLOROPROPENE

Characteristic N % % Basis
Plotted 125 98% Spiked
Estimated Values 125 98% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 132 .  
False Negatives 1 1% 1 out of 127
Not Spiked 365 .  
False Positives 1 0% 1 out of 337