BQS OBSP Determination:
METHYL IODIDE
METHOD: 2021 , TESTIDCODE: 77424GCM66
Open Data Set

 Analysis Date = 10/23/12 
 SpikeMix = Crescent 05BB048: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 100%  Analysis Date = 01/19/13 
 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 103%  Analysis Date = 05/02/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Ultra CB-1578: 50 µl 
 Pct Recovery = 91%  Analysis Date = 01/27/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Supelco LB31918: 30 µl 
 Pct Recovery = 44%  Analysis Date = 04/07/06 
 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl 
 Pct Recovery = 114%  Analysis Date = 02/14/13 
 SpikeMix = Crescent 05BB048: 40 µl & ChemService 472200: 40 µl 
 Pct Recovery = 138%  Analysis Date = 08/14/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 127%  Analysis Date = 05/29/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 123%  Analysis Date = 03/11/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 104%  Analysis Date = 12/11/09 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 100%  Analysis Date = 09/08/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 140%  Analysis Date = 06/24/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 142%  Analysis Date = 04/02/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 123%  Analysis Date = 01/26/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 117%  Analysis Date = 08/12/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 86%  Analysis Date = 07/14/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 99%  Analysis Date = 05/20/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 97%  Analysis Date = 07/30/12 
 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl 
 Pct Recovery = 111%  Analysis Date = 06/12/12 
 SpikeMix = Abs 051712: 20 µl 
 Pct Recovery = 139%  Analysis Date = 08/28/12 
 SpikeMix = NSI 062112-01VOA: 20 µl & ChemService 472200: 20 µl 
 Pct Recovery = 96%  Analysis Date = 09/19/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 47%  Analysis Date = 07/27/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 105%  Analysis Date = 05/31/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 107%  Analysis Date = 04/03/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 84%  Analysis Date = 01/09/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 94%  Analysis Date = 10/14/06 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 75%  Analysis Date = 05/24/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 86%  Analysis Date = 02/22/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 86%  Analysis Date = 11/02/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 54%  Analysis Date = 06/09/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 64%  Analysis Date = 03/14/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 116%  Analysis Date = 02/26/99 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 77%  Analysis Date = 11/20/98 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 77%  Analysis Date = 07/08/09 
 SpikeMix = Supelco LB60727: 40 µl 
 Pct Recovery = 104%  Analysis Date = 04/08/09 
 SpikeMix = Supelco LB60727: 40 µl 
 Pct Recovery = 112%  Analysis Date = 07/25/09 
 SpikeMix = ERA 0804-08-02VOC: 40 µl 
 Pct Recovery = 99%  Analysis Date = 02/06/09 
 SpikeMix = ERA 0804-08-02VOC: 40 µl 
 Pct Recovery = 83%  Analysis Date = 07/09/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 126%  Analysis Date = 04/21/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 115%  Analysis Date = 02/03/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 116%  Analysis Date = 10/24/09 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 127%  Analysis Date = 07/27/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 106%  Analysis Date = 05/11/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 108%  Analysis Date = 02/19/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 124%  Analysis Date = 11/14/09 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 122%  Analysis Date = 02/24/12 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 110%  Analysis Date = 11/18/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 101%  Analysis Date = 05/28/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 111%  Analysis Date = 03/08/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 110%  Analysis Date = 11/16/10 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 113%  Analysis Date = 11/21/12 
 SpikeMix = Abs 051712: 10 µl 
 Pct Recovery = 108%  Analysis Date = 08/13/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 53%  Analysis Date = 03/15/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 116%  Analysis Date = 05/17/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 97%  Analysis Date = 12/08/05 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 116%  Analysis Date = 02/14/06 
 SpikeMix = NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 98%  Analysis Date = 11/15/05 
 SpikeMix = NSI 080405-01VOC: 5 µl & Supelco LB31918: 5 µl 
 Pct Recovery = 86%  Analysis Date = 06/06/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl 
 Pct Recovery = 109%  Analysis Date = 05/03/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 116%  Analysis Date = 03/29/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 104%  Analysis Date = 12/09/12 
 SpikeMix = NSI 062112-01VOA: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 108%  Analysis Date = 10/11/12 
 SpikeMix = Crescent 05BB048: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 131%  Analysis Date = 12/17/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 100%  Analysis Date = 08/10/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 115%  Analysis Date = 05/10/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 115%  Analysis Date = 12/03/10 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 107%  Analysis Date = 04/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 78%  Analysis Date = 01/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 115%  Analysis Date = 08/25/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 63%  Analysis Date = 06/27/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 130%  Analysis Date = 07/26/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 92%  Analysis Date = 03/09/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 58%  Analysis Date = 12/31/13 
 SpikeMix = Abs 051413: 20 µl & Crescent 04CC151: 20 µl 
 Pct Recovery = 117%  Analysis Date = 08/06/13 
 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl 
 Pct Recovery = 100%  Analysis Date = 04/15/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 83%  Analysis Date = 02/11/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 111%  Analysis Date = 03/19/14 
 SpikeMix = ChemService 1530700: 20 µl & NSI 053013: 20 µl 
 Pct Recovery = 134%  Analysis Date = 08/22/13 
 SpikeMix = ChemService 1530700: 20 µl & NSI 053013: 20 µl 
 Pct Recovery = 128%  Analysis Date = 01/29/14 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 130%  Analysis Date = 09/17/13 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 114%  Analysis Date = 11/01/13 
 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 114%  Analysis Date = 03/31/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 71%  Analysis Date = 01/20/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 67%  Analysis Date = 09/16/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 117%  Analysis Date = 06/03/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 142%  Analysis Date = 04/04/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 102%  Analysis Date = 08/12/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/22/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 117%  Analysis Date = 07/03/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/01/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 119%  Analysis Date = 02/06/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 100%  Analysis Date = 10/11/07 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 117%  Analysis Date = 09/19/07 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 75%  Analysis Date = 04/06/12 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 93%  Analysis Date = 01/26/12 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 108%  Analysis Date = 09/03/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 97%  Analysis Date = 07/20/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 114%  Analysis Date = 04/21/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 102%  Analysis Date = 01/22/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 101%  Analysis Date = 03/24/12 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 96%  Analysis Date = 02/24/12 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 107%  Analysis Date = 10/24/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 115%  Analysis Date = 06/18/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 97%  Analysis Date = 03/26/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 107%  Analysis Date = 02/14/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 106%  Analysis Date = 10/23/10 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 90%  Analysis Date = 09/27/13 
 SpikeMix = Abs 051413: 10 µl & NSI 053013: 10 µl 
 Pct Recovery = 119%  Analysis Date = 11/15/13 
 SpikeMix = Abs 051413: 10 µl & Crescent 04CC151: 10 µl 
 Pct Recovery = 131%  Analysis Date = 12/12/13 
 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 128%  Analysis Date = 03/19/14 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 132%  Analysis Date = 06/08/13 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 113%  Analysis Date = 02/22/14 
 SpikeMix = ChemService 1530700: 10 µl & NSI 053013: 10 µl 
 Pct Recovery = 104%  Analysis Date = 06/29/13 
 SpikeMix = ChemService 1530700: 10 µl & Crescent 04CC151: 10 µl 
 Pct Recovery = 113%  Analysis Date = 12/31/13 
 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl 
 Pct Recovery = 130%  Analysis Date = 05/09/02 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 42%  Analysis Date = 12/07/01 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 56%  Analysis Date = 09/19/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 78%  Analysis Date = 08/02/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 75%  Analysis Date = 07/06/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 57%  Analysis Date = 09/26/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 117%  Analysis Date = 08/19/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 117%  Analysis Date = 05/16/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 109%  Analysis Date = 02/27/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 114%  Analysis Date = 09/05/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 92%  Analysis Date = 06/17/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 86%  Analysis Date = 04/25/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 90%  Analysis Date = 03/14/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 86%  Analysis Date = 01/17/09 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 169%  Analysis Date = 12/16/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 98%  Analysis Date = 11/01/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 98%  Analysis Date = 09/17/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 116%  Analysis Date = 03/23/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 153%  Analysis Date = 02/02/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 25%  Analysis Date = 03/18/14 
 Pct Recovery = 119%  Analysis Date = 02/19/14 
 Pct Recovery = 118%  Analysis Date = 02/19/14 
 Pct Recovery = 118%  Analysis Date = 01/22/14 
 Pct Recovery = 118%  Analysis Date = 01/22/14 
 Pct Recovery = 118%  Analysis Date = 12/25/13 
 Pct Recovery = 118%  Analysis Date = 12/25/13 
 Pct Recovery = 118%  Analysis Date = 11/27/13 
 Pct Recovery = 118%  Analysis Date = 11/27/13 
 Pct Recovery = 118%  Analysis Date = 10/30/13 
 Pct Recovery = 117%  Analysis Date = 10/30/13 
 Pct Recovery = 117%  Analysis Date = 10/02/13 
 Pct Recovery = 117%  Analysis Date = 10/02/13 
 Pct Recovery = 117%  Analysis Date = 09/04/13 
 Pct Recovery = 117%  Analysis Date = 09/04/13 
 Pct Recovery = 117%  Analysis Date = 08/07/13 
 Pct Recovery = 117%  Analysis Date = 08/07/13 
 Pct Recovery = 117%  Analysis Date = 07/10/13 
 Pct Recovery = 116%  Analysis Date = 07/10/13 
 Pct Recovery = 116%  Analysis Date = 06/12/13 
 Pct Recovery = 116%  Analysis Date = 06/12/13 
 Pct Recovery = 116%  Analysis Date = 05/15/13 
 Pct Recovery = 116%  Analysis Date = 05/15/13 
 Pct Recovery = 116%  Analysis Date = 04/17/13 
 Pct Recovery = 116%  Analysis Date = 04/17/13 
 Pct Recovery = 116%  Analysis Date = 03/20/13 
 Pct Recovery = 115%  Analysis Date = 03/20/13 
 Pct Recovery = 115%  Analysis Date = 02/20/13 
 Pct Recovery = 115%  Analysis Date = 02/20/13 
 Pct Recovery = 115%  Analysis Date = 01/23/13 
 Pct Recovery = 115%  Analysis Date = 01/23/13 
 Pct Recovery = 115%  Analysis Date = 12/26/12 
 Pct Recovery = 115%  Analysis Date = 12/26/12 
 Pct Recovery = 115%  Analysis Date = 11/28/12 
 Pct Recovery = 115%  Analysis Date = 11/28/12 
 Pct Recovery = 115%  Analysis Date = 10/31/12 
 Pct Recovery = 114%  Analysis Date = 10/31/12 
 Pct Recovery = 114%  Analysis Date = 10/03/12 
 Pct Recovery = 114%  Analysis Date = 10/03/12 
 Pct Recovery = 114%  Analysis Date = 09/05/12 
 Pct Recovery = 114%  Analysis Date = 09/05/12 
 Pct Recovery = 114%  Analysis Date = 08/08/12 
 Pct Recovery = 114%  Analysis Date = 08/08/12 
 Pct Recovery = 114%  Analysis Date = 07/11/12 
 Pct Recovery = 114%  Analysis Date = 07/11/12 
 Pct Recovery = 114%  Analysis Date = 06/13/12 
 Pct Recovery = 113%  Analysis Date = 06/13/12 
 Pct Recovery = 113%  Analysis Date = 05/16/12 
 Pct Recovery = 113%  Analysis Date = 05/16/12 
 Pct Recovery = 113%  Analysis Date = 04/18/12 
 Pct Recovery = 113%  Analysis Date = 04/18/12 
 Pct Recovery = 113%  Analysis Date = 03/21/12 
 Pct Recovery = 113%  Analysis Date = 03/21/12 
 Pct Recovery = 113%  Analysis Date = 02/22/12 
 Pct Recovery = 113%  Analysis Date = 02/22/12 
 Pct Recovery = 113%  Analysis Date = 01/25/12 
 Pct Recovery = 112%  Analysis Date = 01/25/12 
 Pct Recovery = 112%  Analysis Date = 12/28/11 
 Pct Recovery = 112%  Analysis Date = 12/28/11 
 Pct Recovery = 112%  Analysis Date = 11/30/11 
 Pct Recovery = 112%  Analysis Date = 11/30/11 
 Pct Recovery = 112%  Analysis Date = 11/02/11 
 Pct Recovery = 112%  Analysis Date = 11/02/11 
 Pct Recovery = 112%  Analysis Date = 10/05/11 
 Pct Recovery = 112%  Analysis Date = 10/05/11 
 Pct Recovery = 112%  Analysis Date = 09/07/11 
 Pct Recovery = 111%  Analysis Date = 09/07/11 
 Pct Recovery = 111%  Analysis Date = 08/10/11 
 Pct Recovery = 111%  Analysis Date = 08/10/11 
 Pct Recovery = 111%  Analysis Date = 07/13/11 
 Pct Recovery = 111%  Analysis Date = 07/13/11 
 Pct Recovery = 111%  Analysis Date = 06/15/11 
 Pct Recovery = 111%  Analysis Date = 06/15/11 
 Pct Recovery = 111%  Analysis Date = 05/18/11 
 Pct Recovery = 111%  Analysis Date = 05/18/11 
 Pct Recovery = 111%  Analysis Date = 04/20/11 
 Pct Recovery = 111%  Analysis Date = 04/20/11 
 Pct Recovery = 111%  Analysis Date = 03/23/11 
 Pct Recovery = 111%  Analysis Date = 03/23/11 
 Pct Recovery = 111%  Analysis Date = 02/23/11 
 Pct Recovery = 111%  Analysis Date = 02/23/11 
 Pct Recovery = 111%  Analysis Date = 01/26/11 
 Pct Recovery = 111%  Analysis Date = 01/26/11 
 Pct Recovery = 111%  Analysis Date = 12/29/10 
 Pct Recovery = 111%  Analysis Date = 12/29/10 
 Pct Recovery = 111%  Analysis Date = 12/01/10 
 Pct Recovery = 111%  Analysis Date = 12/01/10 
 Pct Recovery = 111%  Analysis Date = 11/03/10 
 Pct Recovery = 111%  Analysis Date = 11/03/10 
 Pct Recovery = 111%  Analysis Date = 10/06/10 
 Pct Recovery = 111%  Analysis Date = 10/06/10 
 Pct Recovery = 111%  Analysis Date = 09/08/10 
 Pct Recovery = 111%  Analysis Date = 09/08/10 
 Pct Recovery = 111%  Analysis Date = 08/11/10 
 Pct Recovery = 111%  Analysis Date = 08/11/10 
 Pct Recovery = 111%  Analysis Date = 07/14/10 
 Pct Recovery = 111%  Analysis Date = 07/14/10 
 Pct Recovery = 111%  Analysis Date = 06/16/10 
 Pct Recovery = 110%  Analysis Date = 06/16/10 
 Pct Recovery = 110%  Analysis Date = 05/19/10 
 Pct Recovery = 110%  Analysis Date = 05/19/10 
 Pct Recovery = 110%  Analysis Date = 04/21/10 
 Pct Recovery = 110%  Analysis Date = 04/21/10 
 Pct Recovery = 110%  Analysis Date = 03/24/10 
 Pct Recovery = 110%  Analysis Date = 03/24/10 
 Pct Recovery = 110%  Analysis Date = 02/24/10 
 Pct Recovery = 110%  Analysis Date = 02/24/10 
 Pct Recovery = 110%  Analysis Date = 01/27/10 
 Pct Recovery = 110%  Analysis Date = 01/27/10 
 Pct Recovery = 110%  Analysis Date = 12/30/09 
 Pct Recovery = 110%  Analysis Date = 12/30/09 
 Pct Recovery = 110%  Analysis Date = 12/02/09 
 Pct Recovery = 110%  Analysis Date = 12/02/09 
 Pct Recovery = 110%  Analysis Date = 11/04/09 
 Pct Recovery = 110%  Analysis Date = 11/04/09 
 Pct Recovery = 110%  Analysis Date = 10/07/09 
 Pct Recovery = 110%  Analysis Date = 10/07/09 
 Pct Recovery = 110%  Analysis Date = 09/09/09 
 Pct Recovery = 109%  Analysis Date = 09/09/09 
 Pct Recovery = 109%  Analysis Date = 08/12/09 
 Pct Recovery = 109%  Analysis Date = 08/12/09 
 Pct Recovery = 109%  Analysis Date = 07/15/09 
 Pct Recovery = 109%  Analysis Date = 07/15/09 
 Pct Recovery = 109%  Analysis Date = 06/17/09 
 Pct Recovery = 109%  Analysis Date = 06/17/09 
 Pct Recovery = 109%  Analysis Date = 05/20/09 
 Pct Recovery = 108%  Analysis Date = 05/20/09 
 Pct Recovery = 108%  Analysis Date = 04/22/09 
 Pct Recovery = 108%  Analysis Date = 04/22/09 
 Pct Recovery = 108%  Analysis Date = 03/25/09 
 Pct Recovery = 108%  Analysis Date = 03/25/09 
 Pct Recovery = 108%  Analysis Date = 02/25/09 
 Pct Recovery = 107%  Analysis Date = 02/25/09 
 Pct Recovery = 107%  Analysis Date = 01/28/09 
 Pct Recovery = 107%  Analysis Date = 01/28/09 
 Pct Recovery = 107%  Analysis Date = 12/31/08 
 Pct Recovery = 107%  Analysis Date = 12/31/08 
 Pct Recovery = 107%  Analysis Date = 12/03/08 
 Pct Recovery = 106%  Analysis Date = 12/03/08 
 Pct Recovery = 106%  Analysis Date = 11/05/08 
 Pct Recovery = 106%  Analysis Date = 11/05/08 
 Pct Recovery = 106%  Analysis Date = 10/08/08 
 Pct Recovery = 106%  Analysis Date = 10/08/08 
 Pct Recovery = 106%  Analysis Date = 09/10/08 
 Pct Recovery = 105%  Analysis Date = 09/10/08 
 Pct Recovery = 105%  Analysis Date = 08/13/08 
 Pct Recovery = 105%  Analysis Date = 08/13/08 
 Pct Recovery = 105%  Analysis Date = 07/16/08 
 Pct Recovery = 105%  Analysis Date = 07/16/08 
 Pct Recovery = 105%  Analysis Date = 06/18/08 
 Pct Recovery = 104%  Analysis Date = 06/18/08 
 Pct Recovery = 104%  Analysis Date = 05/21/08 
 Pct Recovery = 104%  Analysis Date = 05/21/08 
 Pct Recovery = 104%  Analysis Date = 04/23/08 
 Pct Recovery = 104%  Analysis Date = 04/23/08 
 Pct Recovery = 104%  Analysis Date = 03/26/08 
 Pct Recovery = 103%  Analysis Date = 03/26/08 
 Pct Recovery = 103%  Analysis Date = 02/27/08 
 Pct Recovery = 103%  Analysis Date = 02/27/08 
 Pct Recovery = 103%  Analysis Date = 01/30/08 
 Pct Recovery = 103%  Analysis Date = 01/30/08 
 Pct Recovery = 103%  Analysis Date = 01/02/08 
 Pct Recovery = 102%  Analysis Date = 01/02/08 
 Pct Recovery = 102%  Analysis Date = 12/05/07 
 Pct Recovery = 102%  Analysis Date = 12/05/07 
 Pct Recovery = 102%  Analysis Date = 11/07/07 
 Pct Recovery = 102%  Analysis Date = 11/07/07 
 Pct Recovery = 102%  Analysis Date = 10/11/07 
 Pct Recovery = 102%  Analysis Date = 10/11/07 
 Pct Recovery = 102%  Analysis Date = 09/13/07 
 Pct Recovery = 101%  Analysis Date = 09/13/07 
 Pct Recovery = 101%  Analysis Date = 08/16/07 
 Pct Recovery = 101%  Analysis Date = 08/16/07 
 Pct Recovery = 101%  Analysis Date = 07/19/07 
 Pct Recovery = 101%  Analysis Date = 07/19/07 
 Pct Recovery = 101%  Analysis Date = 06/21/07 
 Pct Recovery = 100%  Analysis Date = 06/21/07 
 Pct Recovery = 100%  Analysis Date = 05/24/07 
 Pct Recovery = 100%  Analysis Date = 05/24/07 
 Pct Recovery = 100%  Analysis Date = 04/26/07 
 Pct Recovery = 100%  Analysis Date = 04/26/07 
 Pct Recovery = 100%  Analysis Date = 03/29/07 
 Pct Recovery = 99%  Analysis Date = 03/29/07 
 Pct Recovery = 99%  Analysis Date = 03/01/07 
 Pct Recovery = 99%  Analysis Date = 03/01/07 
 Pct Recovery = 99%  Analysis Date = 02/01/07 
 Pct Recovery = 99%  Analysis Date = 02/01/07 
 Pct Recovery = 99%  Analysis Date = 01/04/07 
 Pct Recovery = 98%  Analysis Date = 01/04/07 
 Pct Recovery = 98%  Analysis Date = 12/07/06 
 Pct Recovery = 98%  Analysis Date = 12/07/06 
 Pct Recovery = 98%  Analysis Date = 11/09/06 
 Pct Recovery = 98%  Analysis Date = 11/09/06 
 Pct Recovery = 98%  Analysis Date = 10/12/06 
 Pct Recovery = 97%  Analysis Date = 10/12/06 
 Pct Recovery = 97%  Analysis Date = 09/14/06 
 Pct Recovery = 97%  Analysis Date = 09/14/06 
 Pct Recovery = 97%  Analysis Date = 08/17/06 
 Pct Recovery = 97%  Analysis Date = 08/17/06 
 Pct Recovery = 97%  Analysis Date = 07/20/06 
 Pct Recovery = 96%  Analysis Date = 07/20/06 
 Pct Recovery = 96%  Analysis Date = 06/22/06 
 Pct Recovery = 96%  Analysis Date = 06/22/06 
 Pct Recovery = 96%  Analysis Date = 05/25/06 
 Pct Recovery = 96%  Analysis Date = 05/25/06 
 Pct Recovery = 96%  Analysis Date = 04/27/06 
 Pct Recovery = 95%  Analysis Date = 04/27/06 
 Pct Recovery = 95%  Analysis Date = 03/30/06 
 Pct Recovery = 95%  Analysis Date = 03/30/06 
 Pct Recovery = 95%  Analysis Date = 03/02/06 
 Pct Recovery = 94%  Analysis Date = 03/02/06 
 Pct Recovery = 94%  Analysis Date = 02/02/06 
 Pct Recovery = 94%  Analysis Date = 02/02/06 
 Pct Recovery = 94%  Analysis Date = 01/05/06 
 Pct Recovery = 94%  Analysis Date = 01/05/06 
 Pct Recovery = 94%  Analysis Date = 12/08/05 
 Pct Recovery = 93%  Analysis Date = 12/08/05 
 Pct Recovery = 93%  Analysis Date = 11/10/05 
 Pct Recovery = 93%  Analysis Date = 11/10/05 
 Pct Recovery = 93%  Analysis Date = 10/13/05 
 Pct Recovery = 92%  Analysis Date = 10/13/05 
 Pct Recovery = 92%  Analysis Date = 09/15/05 
 Pct Recovery = 92%  Analysis Date = 09/15/05 
 Pct Recovery = 92%  Analysis Date = 08/18/05 
 Pct Recovery = 91%  Analysis Date = 08/18/05 
 Pct Recovery = 91%  Analysis Date = 07/21/05 
 Pct Recovery = 91%  Analysis Date = 07/21/05 
 Pct Recovery = 91%  Analysis Date = 06/23/05 
 Pct Recovery = 91%  Analysis Date = 06/23/05 
 Pct Recovery = 91%  Analysis Date = 05/26/05 
 Pct Recovery = 90%  Analysis Date = 05/26/05 
 Pct Recovery = 90%  Analysis Date = 04/28/05 
 Pct Recovery = 90%  Analysis Date = 04/28/05 
 Pct Recovery = 90%  Analysis Date = 03/31/05 
 Pct Recovery = 90%  Analysis Date = 03/31/05 
 Pct Recovery = 90%  Analysis Date = 03/03/05 
 Pct Recovery = 89%  Analysis Date = 03/03/05 
 Pct Recovery = 89%  Analysis Date = 02/03/05 
 Pct Recovery = 89%  Analysis Date = 02/03/05 
 Pct Recovery = 89%  Analysis Date = 01/06/05 
 Pct Recovery = 89%  Analysis Date = 01/06/05 
 Pct Recovery = 89%  Analysis Date = 12/09/04 
 Pct Recovery = 89%  Analysis Date = 12/09/04 
 Pct Recovery = 89%  Analysis Date = 11/11/04 
 Pct Recovery = 88%  Analysis Date = 11/11/04 
 Pct Recovery = 88%  Analysis Date = 10/14/04 
 Pct Recovery = 88%  Analysis Date = 10/14/04 
 Pct Recovery = 88%  Analysis Date = 09/16/04 
 Pct Recovery = 88%  Analysis Date = 09/16/04 
 Pct Recovery = 88%  Analysis Date = 08/19/04 
 Pct Recovery = 87%  Analysis Date = 08/19/04 
 Pct Recovery = 87%  Analysis Date = 07/22/04 
 Pct Recovery = 87%  Analysis Date = 07/22/04 
 Pct Recovery = 87%  Analysis Date = 06/24/04 
 Pct Recovery = 87%  Analysis Date = 06/24/04 
 Pct Recovery = 87%  Analysis Date = 05/27/04 
 Pct Recovery = 86%  Analysis Date = 05/27/04 
 Pct Recovery = 86%  Analysis Date = 04/29/04 
 Pct Recovery = 86%  Analysis Date = 04/29/04 
 Pct Recovery = 86%  Analysis Date = 04/01/04 
 Pct Recovery = 86%  Analysis Date = 04/01/04 
 Pct Recovery = 86%  Analysis Date = 03/04/04 
 Pct Recovery = 86%  Analysis Date = 03/04/04 
 Pct Recovery = 86%  Analysis Date = 02/05/04 
 Pct Recovery = 85%  Analysis Date = 02/05/04 
 Pct Recovery = 85%  Analysis Date = 01/08/04 
 Pct Recovery = 85%  Analysis Date = 01/08/04 
 Pct Recovery = 85%  Analysis Date = 12/11/03 
 Pct Recovery = 85%  Analysis Date = 12/11/03 
 Pct Recovery = 85%  Analysis Date = 11/13/03 
 Pct Recovery = 84%  Analysis Date = 11/13/03 
 Pct Recovery = 84%  Analysis Date = 10/16/03 
 Pct Recovery = 84%  Analysis Date = 10/16/03 
 Pct Recovery = 84%  Analysis Date = 09/18/03 
 Pct Recovery = 84%  Analysis Date = 09/18/03 
 Pct Recovery = 84%  Analysis Date = 08/21/03 
 Pct Recovery = 83%  Analysis Date = 08/21/03 
 Pct Recovery = 83%  Analysis Date = 07/24/03 
 Pct Recovery = 83%  Analysis Date = 07/24/03 
 Pct Recovery = 83%  Analysis Date = 06/26/03 
 Pct Recovery = 83%  Analysis Date = 06/26/03 
 Pct Recovery = 83%  Analysis Date = 05/29/03 
 Pct Recovery = 83%  Analysis Date = 05/29/03 
 Pct Recovery = 83%  Analysis Date = 05/01/03 
 Pct Recovery = 82%  Analysis Date = 05/01/03 
 Pct Recovery = 82%  Analysis Date = 04/03/03 
 Pct Recovery = 82%  Analysis Date = 04/03/03 
 Pct Recovery = 82%  Analysis Date = 03/06/03 
 Pct Recovery = 82%  Analysis Date = 03/06/03 
 Pct Recovery = 82%  Analysis Date = 02/06/03 
 Pct Recovery = 81%  Analysis Date = 02/06/03 
 Pct Recovery = 81%  Analysis Date = 01/09/03 
 Pct Recovery = 81%  Analysis Date = 01/09/03 
 Pct Recovery = 81%  Analysis Date = 12/12/02 
 Pct Recovery = 81%  Analysis Date = 12/12/02 
 Pct Recovery = 81%  Analysis Date = 11/14/02 
 Pct Recovery = 80%  Analysis Date = 11/14/02 
 Pct Recovery = 80%  Analysis Date = 10/17/02 
 Pct Recovery = 80%  Analysis Date = 10/17/02 
 Pct Recovery = 80%  Analysis Date = 09/19/02 
 Pct Recovery = 80%  Analysis Date = 09/19/02 
 Pct Recovery = 80%  Analysis Date = 08/22/02 
 Pct Recovery = 80%  Analysis Date = 08/22/02 
 Pct Recovery = 80%  Analysis Date = 07/25/02 
 Pct Recovery = 79%  Analysis Date = 07/25/02 
 Pct Recovery = 79%  Analysis Date = 06/27/02 
 Pct Recovery = 79%  Analysis Date = 06/27/02 
 Pct Recovery = 79%  Analysis Date = 05/30/02 
 Pct Recovery = 79%  Analysis Date = 05/30/02 
 Pct Recovery = 79%  Analysis Date = 05/02/02 
 Pct Recovery = 78%  Analysis Date = 05/02/02 
 Pct Recovery = 78%  Analysis Date = 04/04/02 
 Pct Recovery = 78%  Analysis Date = 04/04/02 
 Pct Recovery = 78%  Analysis Date = 03/07/02 
 Pct Recovery = 78%  Analysis Date = 03/07/02 
 Pct Recovery = 78%  Analysis Date = 02/07/02 
 Pct Recovery = 78%  Analysis Date = 02/07/02 
 Pct Recovery = 78%  Analysis Date = 01/10/02 
 Pct Recovery = 77%  Analysis Date = 01/10/02 
 Pct Recovery = 77%  Analysis Date = 12/13/01 
 Pct Recovery = 77%  Analysis Date = 12/13/01 
 Pct Recovery = 77%  Analysis Date = 11/15/01 
 Pct Recovery = 77%  Analysis Date = 11/15/01 
 Pct Recovery = 77%  Analysis Date = 10/18/01 
 Pct Recovery = 76%  Analysis Date = 10/18/01 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 Pct Recovery = 76%  Analysis Date = 08/23/01 
 Pct Recovery = 76%  Analysis Date = 08/23/01 
 Pct Recovery = 76%  Analysis Date = 07/26/01 
 Pct Recovery = 76%  Analysis Date = 07/26/01 
 Pct Recovery = 76%  Analysis Date = 06/28/01 
 Pct Recovery = 75%  Analysis Date = 06/28/01 
 Pct Recovery = 75%  Analysis Date = 05/31/01 
 Pct Recovery = 75%  Analysis Date = 05/31/01 
 Pct Recovery = 75%  Analysis Date = 05/04/01 
 Pct Recovery = 75%  Analysis Date = 05/04/01 
 Pct Recovery = 75%  Analysis Date = 04/06/01 
 Pct Recovery = 74%  Analysis Date = 04/06/01 
 Pct Recovery = 74%  Analysis Date = 03/09/01 
 Pct Recovery = 74%  Analysis Date = 03/09/01 
 Pct Recovery = 74%  Analysis Date = 02/09/01 
 Pct Recovery = 74%  Analysis Date = 02/09/01 
 Pct Recovery = 74%  Analysis Date = 01/12/01 
 Pct Recovery = 74%  Analysis Date = 01/12/01 
 Pct Recovery = 74%  Analysis Date = 12/15/00 
 Pct Recovery = 73%  Analysis Date = 12/15/00 
 Pct Recovery = 73%  Analysis Date = 11/17/00 
 Pct Recovery = 73%  Analysis Date = 11/17/00 
 Pct Recovery = 73%  Analysis Date = 10/20/00 
 Pct Recovery = 73%  Analysis Date = 10/20/00 
 Pct Recovery = 73%  Analysis Date = 09/22/00 
 Pct Recovery = 72%  Analysis Date = 09/22/00 
 Pct Recovery = 72%  Analysis Date = 08/25/00 
 Pct Recovery = 72%  Analysis Date = 08/25/00 
 Pct Recovery = 72%  Analysis Date = 07/28/00 
 Pct Recovery = 72%  Analysis Date = 07/28/00 
 Pct Recovery = 72%  Analysis Date = 06/30/00 
 Pct Recovery = 72%  Analysis Date = 06/30/00 
 Pct Recovery = 72%  Analysis Date = 06/02/00 
 Pct Recovery = 71%  Analysis Date = 06/02/00 
 Pct Recovery = 71%  Analysis Date = 05/05/00 
 Pct Recovery = 71%  Analysis Date = 05/05/00 
 Pct Recovery = 71%  Analysis Date = 04/07/00 
 Pct Recovery = 71%  Analysis Date = 04/07/00 
 Pct Recovery = 71%  Analysis Date = 03/10/00 
 Pct Recovery = 70%  Analysis Date = 03/10/00 
 Pct Recovery = 70%  Analysis Date = 02/11/00 
 Pct Recovery = 70%  Analysis Date = 02/11/00 
 Pct Recovery = 70%  Analysis Date = 01/14/00 
 Pct Recovery = 70%  Analysis Date = 01/14/00 
 Pct Recovery = 70%  Analysis Date = 12/17/99 
 Pct Recovery = 70%  Analysis Date = 12/17/99 
 Pct Recovery = 70%  Analysis Date = 11/19/99 
 Pct Recovery = 69%  Analysis Date = 11/19/99 
 Pct Recovery = 69%  Analysis Date = 10/22/99 
 Pct Recovery = 69%  Analysis Date = 10/22/99 
 Pct Recovery = 69%  Analysis Date = 09/24/99 
 Pct Recovery = 69%  Analysis Date = 09/24/99 
 Pct Recovery = 69%  Analysis Date = 08/27/99 
 Pct Recovery = 68%  Analysis Date = 08/27/99 
 Pct Recovery = 68%  Analysis Date = 07/30/99 
 Pct Recovery = 68%  Analysis Date = 07/30/99 
 Pct Recovery = 68%  Analysis Date = 07/02/99 
 Pct Recovery = 68%  Analysis Date = 07/02/99 
 Pct Recovery = 68%  Analysis Date = 06/04/99 
 Pct Recovery = 68%  Analysis Date = 06/04/99 
 Pct Recovery = 68%  Analysis Date = 05/07/99 
 Pct Recovery = 67%  Analysis Date = 05/07/99 
 Pct Recovery = 67%  Analysis Date = 04/09/99 
 Pct Recovery = 67%  Analysis Date = 04/09/99 
 Pct Recovery = 67%  Analysis Date = 03/12/99 
 Pct Recovery = 67%  Analysis Date = 03/12/99 
 Pct Recovery = 67%  Analysis Date = 02/12/99 
 Pct Recovery = 67%  Analysis Date = 02/12/99 
 Pct Recovery = 67%  Analysis Date = 01/15/99 
 Pct Recovery = 66%  Analysis Date = 01/15/99 
 Pct Recovery = 66%  Analysis Date = 12/18/98 
 Pct Recovery = 66%  Analysis Date = 12/18/98 
 Pct Recovery = 66%  Analysis Date = 11/20/98 
 Pct Recovery = 66%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL IODIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 105% 33% 103% 20%
>= Reporting Level 120 103% 22% 106% 17%
Total 134 103% 23% 106% 18%

Sample Statistics
METHYL IODIDE

Characteristic N % % Basis
Plotted 134 96% Spiked
Estimated Values 134 96% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 4 3% Spiked
Spiked 156 .  
False Negatives 2 1% 2 out of 140
Not Spiked 341 .  
False Positives 19 6% 19 out of 324