BQS OBSP Determination:
ALDICARB SULFOXIDE
METHOD: 2060 , TESTIDCODE: 49314LCM29
Open Data Set

 Analysis Date = 06/17/09 
 SpikeMix = ChemService 406-113B: 50 µl 
 Pct Recovery = 241%  Analysis Date = 06/17/09 
 SpikeMix = ChemService 406-113B: 50 µl 
 Pct Recovery = 241%  Analysis Date = 06/20/04 
 SpikeMix = NSI 100303HPLC: 200 µl 
 Pct Recovery = 60%  Analysis Date = 09/09/04 
 SpikeMix = NSI 100303HPLC: 200 µl 
 Pct Recovery = 92%  Analysis Date = 03/25/04 
 SpikeMix = NSI 100303HPLC: 200 µl 
 Pct Recovery = 46%  Analysis Date = 01/18/13 
 SpikeMix = Spex Organics T1120525009: 100 µl & NSI 062612-01: 100 µl & NSI 718L-01-01: 100 
 Pct Recovery = 83%  Analysis Date = 04/11/03 
 SpikeMix = Crescent 08BB071: 100 µl & Crescent 09BB025: 100 µl & Crescent 09BL026: 100 µl 
 Pct Recovery = 22%  Analysis Date = 03/13/02 
 SpikeMix = Supelco LA-88006: 75 µl & Supelco LA-88007: 75 µl 
 Pct Recovery = 27%  Analysis Date = 12/20/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 32%  Analysis Date = 05/16/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 39%  Analysis Date = 11/10/01 
 SpikeMix = Supelco LA-88006: 75 µl & Supelco LA-88007: 75 µl 
 Pct Recovery = 59%  Analysis Date = 10/05/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 8%  Analysis Date = 11/07/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 43%  Analysis Date = 11/17/04 
 SpikeMix = NSI 100303HPLC: 100 µl 
 Pct Recovery = 29%  Analysis Date = 01/29/05 
 SpikeMix = NSI 100303HPLC: 100 µl 
 Pct Recovery = 16%  Analysis Date = 03/08/05 
 SpikeMix = NSI 100303HPLC: 100 µl 
 Pct Recovery = 68%  Analysis Date = 12/01/04 
 SpikeMix = NSI 100303HPLC: 100 µl 
 Pct Recovery = 46%  Analysis Date = 08/17/13 
 SpikeMix = Spex Organics T1130601011: 50 µl & NSI 050613: 50 µl & Supelco LC01386: 50 µl 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 SpikeMix = ChemService 1448600: 50 µl & NSI 050613: 50 µl & Supelco LC01386: 50 µl 
 Pct Recovery = 74%  Analysis Date = 07/18/12 
 SpikeMix = Spex Organics T1120525009: 50 µl & Supelco LB92941: 50 µl 
 Pct Recovery = 74%  Analysis Date = 05/02/13 
 SpikeMix = Abs 052312: 50 µl & Supelco LB92941: 50 µl 
 Pct Recovery = 73%  Analysis Date = 03/12/13 
 SpikeMix = Abs 052312: 50 µl & Supelco LB92941: 50 µl 
 Pct Recovery = 76%  Analysis Date = 09/27/13 
 SpikeMix = NSI 042213HPLC: 50 µl & Accu 213041030: 50 µl & Supelco LC00372: 50 µl 
 Pct Recovery = 66%  Analysis Date = 06/26/13 
 SpikeMix = Abs 042513: 50 µl & NSI 042213HPLC: 50 µl & NSI 050613: 50 µl 
 Pct Recovery = 80%  Analysis Date = 06/04/13 
 SpikeMix = Restek A088383: 50 µl & NSI 062612-01: 50 µl & NSI 718L-01-01: 50 µl 
 Pct Recovery = 65%  Analysis Date = 01/05/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 46%  Analysis Date = 05/14/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 23%  Analysis Date = 05/23/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 18%  Analysis Date = 10/20/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 65%  Analysis Date = 06/28/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 45%  Analysis Date = 09/15/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 48%  Analysis Date = 08/16/01 
 SpikeMix = Supelco LA-88006: 30 µl & Supelco LA-88007: 30 µl 
 Pct Recovery = 68%  Analysis Date = 10/15/01 
 SpikeMix = Supelco LA-88006: 30 µl & Supelco LA-88007: 30 µl 
 Pct Recovery = 5%  Analysis Date = 08/03/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 36%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 83%  Analysis Date = 10/01/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 35%  Analysis Date = 07/01/10 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 81%  Analysis Date = 12/29/09 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 77%  Analysis Date = 10/28/10 
 SpikeMix = Crescent 08LL073: 80 µl 
 Pct Recovery = 9%  Analysis Date = 10/31/08 
 SpikeMix = Abs 081508Polar: 50 µl 
 Pct Recovery = 137%  Analysis Date = 09/01/09 
 SpikeMix = Abs 081508Polar: 50 µl 
 Pct Recovery = 146%  Analysis Date = 03/04/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 86%  Analysis Date = 06/01/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 82%  Analysis Date = 11/19/08 
 SpikeMix = ChemService 406-113B: 50 µl 
 Pct Recovery = 131%  Analysis Date = 12/14/05 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 73%  Analysis Date = 06/06/04 
 SpikeMix = Crescent 09CC036: 40 µl 
 Pct Recovery = 91%  Analysis Date = 09/25/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 97%  Analysis Date = 08/31/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 85%  Analysis Date = 07/22/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 59%  Analysis Date = 10/31/03 
 SpikeMix = Crescent 09CC036: 40 µl 
 Pct Recovery = 11%  Analysis Date = 07/07/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 87%  Analysis Date = 07/28/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 78%  Analysis Date = 09/27/13 
 SpikeMix = Accu 213041030: 20 µl & NSI 050613: 20 µl & Supelco LC01386: 20 µl 
 Pct Recovery = 88%  Analysis Date = 03/04/14 
 SpikeMix = Spex Organics T1130601011: 20 µl & Supelco LC01386: 20 µl & Supelco LC00372: 20 
 Pct Recovery = 68%  Analysis Date = 01/16/14 
 SpikeMix = Abs 042513: 20 µl & Supelco LC01386: 20 µl & NSI 050613: 20 µl 
 Pct Recovery = 34%  Analysis Date = 04/01/14 
 SpikeMix = Supelco LC01386: 20 µl & Accu 213041030: 20 µl 
 Pct Recovery = 86%  Analysis Date = 02/13/13 
 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 90%  Analysis Date = 12/05/12 
 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 98%  Analysis Date = 07/09/12 
 SpikeMix = Supelco LB92941: 20 µl 
 Pct Recovery = 53%  Analysis Date = 02/12/14 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl 
 Pct Recovery = 81%  Analysis Date = 06/04/13 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µl 
 Pct Recovery = 75%  Analysis Date = 11/07/13 
 SpikeMix = Abs 042513: 20 µl & NSI 042213HPLC: 20 µl 
 Pct Recovery = 72%  Analysis Date = 09/28/12 
 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & Restek A088383: 20 µl 
 Pct Recovery = 86%  Analysis Date = 09/13/12 
 SpikeMix = Spex Organics T1120525009: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl 
 Pct Recovery = 81%  Analysis Date = 12/05/12 
 SpikeMix = Abs 052312: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl 
 Pct Recovery = 72%  Analysis Date = 08/07/12 
 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 97%  Analysis Date = 11/13/06 
 SpikeMix = Supelco LB40676: 75 µl 
 Pct Recovery = 103%  Analysis Date = 03/26/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 130%  Analysis Date = 07/25/07 
 SpikeMix = Ultra CC-2418: 75 µl 
 Pct Recovery = 83%  Analysis Date = 04/10/07 
 SpikeMix = Ultra CC-2418: 75 µl 
 Pct Recovery = 37%  Analysis Date = 05/11/07 
 SpikeMix = Supelco LB40676: 75 µl 
 Pct Recovery = 104%  Analysis Date = 06/02/07 
 SpikeMix = Ultra CC-2418: 75 µl 
 Pct Recovery = 94%  Analysis Date = 06/25/07 
 SpikeMix = Supelco LB40676: 75 µl 
 Pct Recovery = 99%  Analysis Date = 05/06/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 128%  Analysis Date = 07/28/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 68%  Analysis Date = 06/19/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 88%  Analysis Date = 04/30/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 103%  Analysis Date = 06/18/07 
 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl 
 Pct Recovery = 118%  Analysis Date = 06/17/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 125%  Analysis Date = 11/30/06 
 SpikeMix = NWQL ABS94077: 75 µl & NWQL ABS94078: 75 µl 
 Pct Recovery = 106%  Analysis Date = 02/27/07 
 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl 
 Pct Recovery = 115%  Analysis Date = 07/30/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 109%  Analysis Date = 02/13/12 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 121%  Analysis Date = 09/12/11 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 131%  Analysis Date = 11/29/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 113%  Analysis Date = 08/11/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 100%  Analysis Date = 06/10/11 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 120%  Analysis Date = 06/28/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 99%  Analysis Date = 08/03/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 103%  Analysis Date = 10/28/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 78%  Analysis Date = 09/14/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 75%  Analysis Date = 06/05/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 113%  Analysis Date = 10/13/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 119%  Analysis Date = 08/14/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 81%  Analysis Date = 05/18/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 81%  Analysis Date = 09/26/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 62%  Analysis Date = 03/03/09 
 SpikeMix = ChemService 406-113B: 30 µl 
 Pct Recovery = 157%  Analysis Date = 09/24/07 
 SpikeMix = Supelco LB40676: 50 µl 
 Pct Recovery = 85%  Analysis Date = 02/10/03 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 13%  Analysis Date = 07/09/04 
 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl 
 Pct Recovery = 76%  Analysis Date = 07/20/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 98%  Analysis Date = 08/13/03 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 60%  Analysis Date = 04/30/09 
 SpikeMix = Abs 081508Polar: 30 µl 
 Pct Recovery = 126%  Analysis Date = 12/30/08 
 SpikeMix = Abs 081508Polar: 30 µl 
 Pct Recovery = 170%  Analysis Date = 09/22/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 107%  Analysis Date = 02/09/07 
 SpikeMix = Ultra CC-2418: 50 µl 
 Pct Recovery = 113%  Analysis Date = 07/28/09 
 SpikeMix = Abs 081508Polar: 30 µl 
 Pct Recovery = 76%  Analysis Date = 03/28/07 
 SpikeMix = Ultra CC-2418: 50 µl 
 Pct Recovery = 74%  Analysis Date = 08/23/07 
 SpikeMix = Supelco LB40676: 50 µl 
 Pct Recovery = 67%  Analysis Date = 09/23/09 
 SpikeMix = ChemService 406-113B: 30 µl 
 Pct Recovery = 148%  Analysis Date = 08/13/09 
 SpikeMix = ChemService 406-113B: 30 µl 
 Pct Recovery = 141%  Analysis Date = 02/27/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 119%  Analysis Date = 05/03/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 134%  Analysis Date = 08/24/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 113%  Analysis Date = 09/21/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 124%  Analysis Date = 07/27/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 131%  Analysis Date = 04/26/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 121%  Analysis Date = 07/31/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 101%  Analysis Date = 05/20/10 
 SpikeMix = NSI 090309-01HPLC: 40 µl 
 Pct Recovery = 86%  Analysis Date = 06/15/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 81%  Analysis Date = 03/17/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 110%  Analysis Date = 09/01/10 
 SpikeMix = NSI 090309-01HPLC: 40 µl 
 Pct Recovery = 63%  Analysis Date = 11/19/09 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 85%  Analysis Date = 07/26/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 111%  Analysis Date = 11/01/02 
 SpikeMix = Supelco LA99123: 40 µl & Supelco LA99124: 40 µl 
 Pct Recovery = 4%  Analysis Date = 08/20/04 
 SpikeMix = Crescent 09CC036: 20 µl 
 Pct Recovery = 19%  Analysis Date = 05/14/04 
 SpikeMix = Crescent 09CC036: 20 µl 
 Pct Recovery = 70%  Analysis Date = 05/27/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 71%  Analysis Date = 03/03/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 53%  Analysis Date = 05/01/03 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 7%  Analysis Date = 12/04/01 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 20%  Analysis Date = 12/29/02 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 25%  Analysis Date = 08/03/03 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 64%  Analysis Date = 08/30/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 9%  Analysis Date = 09/25/01 
 SpikeMix = Supelco LA-88006: 8 µl & Supelco LA-88007: 8 µl 
 Pct Recovery = 41%  Analysis Date = 08/25/01 
 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl 
 Pct Recovery = 33%  Analysis Date = 01/08/05 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 58%  Analysis Date = 11/10/04 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 16%  Analysis Date = 04/01/05 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 87%  Analysis Date = 02/16/05 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 19%  Analysis Date = 05/06/04 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 58%  Analysis Date = 10/21/04 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 18%  Analysis Date = 07/18/04 
 SpikeMix = NSI 100303HPLC: 15 µl 
 Pct Recovery = 52%  Analysis Date = 10/13/01 
 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl 
 Pct Recovery = 58%  Analysis Date = 03/29/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 54%  Analysis Date = 01/18/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 77%  Analysis Date = 03/03/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 77%  Analysis Date = 02/02/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 154%  Analysis Date = 07/19/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 101%  Analysis Date = 07/26/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 29%  Analysis Date = 02/25/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 102%  Analysis Date = 04/12/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 135%  Analysis Date = 05/05/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 117%  Analysis Date = 01/05/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 63%  Analysis Date = 01/04/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 125%  Analysis Date = 03/07/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 136%  Analysis Date = 05/23/02 
 SpikeMix = Supelco LA-88006: 5 µl & Supelco LA-88007: 5 µl 
 Pct Recovery = 34%  Analysis Date = 01/21/02 
 SpikeMix = Supelco LA-88006: 5 µl & Supelco LA-88007: 5 µl 
 Pct Recovery = 47%  Analysis Date = 08/29/07 
 SpikeMix = Ultra CC-2418: 20 µl 
 Pct Recovery = 101%  Analysis Date = 02/27/07 
 SpikeMix = Supelco LB40676: 20 µl 
 Pct Recovery = 134%  Analysis Date = 05/11/07 
 SpikeMix = Supelco LB40676: 20 µl 
 Pct Recovery = 108%  Analysis Date = 11/20/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 18%  Analysis Date = 07/13/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 11%  Analysis Date = 03/29/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 48%  Analysis Date = 05/18/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 61%  Analysis Date = 08/03/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 42%  Analysis Date = 02/09/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 43%  Analysis Date = 01/27/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 115%  Analysis Date = 02/22/02 
 SpikeMix = Supelco LA99123: 15 µl & Supelco LA99124: 15 µl 
 Pct Recovery = 7%  Analysis Date = 04/15/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 101%  Analysis Date = 06/19/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 83%  Analysis Date = 07/24/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 110%  Analysis Date = 08/18/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 81%  Analysis Date = 06/16/01 
 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl 
 Pct Recovery = 69%  Analysis Date = 09/25/01 
 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl 
 Pct Recovery = 56%  Analysis Date = 01/21/02 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 38%  Analysis Date = 09/08/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 76%  Analysis Date = 11/30/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 22%  Analysis Date = 06/16/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 108%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 45%  Analysis Date = 04/13/03 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 25%  Analysis Date = 09/19/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 88%  Analysis Date = 07/23/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 54%  Analysis Date = 05/03/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 113%  Analysis Date = 04/10/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 112%  Analysis Date = 11/28/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 150%  Analysis Date = 03/26/12 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 125%  Analysis Date = 02/02/12 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 115%  Analysis Date = 10/04/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 65%  Analysis Date = 08/09/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 105%  Analysis Date = 06/27/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 101%  Analysis Date = 01/22/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 130%  Analysis Date = 06/18/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 112%  Analysis Date = 11/28/07 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 93%  Analysis Date = 04/30/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 140%  Analysis Date = 11/06/07 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 77%  Analysis Date = 04/04/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 138%  Analysis Date = 09/09/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 141%  Analysis Date = 04/04/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 69%  Analysis Date = 05/16/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 107%  Analysis Date = 07/08/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 145%  Analysis Date = 07/24/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 94%  Analysis Date = 08/27/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 158%  Analysis Date = 08/29/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 97%  Analysis Date = 04/07/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 71%  Analysis Date = 05/01/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 124%  Analysis Date = 09/22/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 84%  Analysis Date = 06/27/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 96%  Analysis Date = 05/10/06 
 SpikeMix = Crescent 07EE046: 10 µl 
 Pct Recovery = 115%  Analysis Date = 03/31/14 
 Pct Recovery = 77%  Analysis Date = 03/08/14 
 Pct Recovery = 78%  Analysis Date = 03/08/14 
 Pct Recovery = 78%  Analysis Date = 02/12/14 
 Pct Recovery = 78%  Analysis Date = 02/12/14 
 Pct Recovery = 78%  Analysis Date = 01/20/14 
 Pct Recovery = 79%  Analysis Date = 01/20/14 
 Pct Recovery = 79%  Analysis Date = 12/27/13 
 Pct Recovery = 79%  Analysis Date = 12/27/13 
 Pct Recovery = 79%  Analysis Date = 12/04/13 
 Pct Recovery = 80%  Analysis Date = 12/04/13 
 Pct Recovery = 80%  Analysis Date = 11/10/13 
 Pct Recovery = 80%  Analysis Date = 11/10/13 
 Pct Recovery = 80%  Analysis Date = 10/18/13 
 Pct Recovery = 81%  Analysis Date = 10/18/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 82%  Analysis Date = 09/24/13 
 Pct Recovery = 82%  Analysis Date = 09/01/13 
 Pct Recovery = 82%  Analysis Date = 09/01/13 
 Pct Recovery = 82%  Analysis Date = 08/08/13 
 Pct Recovery = 83%  Analysis Date = 08/08/13 
 Pct Recovery = 83%  Analysis Date = 07/16/13 
 Pct Recovery = 83%  Analysis Date = 07/16/13 
 Pct Recovery = 83%  Analysis Date = 06/22/13 
 Pct Recovery = 84%  Analysis Date = 06/22/13 
 Pct Recovery = 84%  Analysis Date = 05/30/13 
 Pct Recovery = 84%  Analysis Date = 05/30/13 
 Pct Recovery = 84%  Analysis Date = 05/06/13 
 Pct Recovery = 85%  Analysis Date = 05/06/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 03/20/13 
 Pct Recovery = 86%  Analysis Date = 03/20/13 
 Pct Recovery = 86%  Analysis Date = 02/25/13 
 Pct Recovery = 87%  Analysis Date = 02/25/13 
 Pct Recovery = 87%  Analysis Date = 02/01/13 
 Pct Recovery = 87%  Analysis Date = 02/01/13 
 Pct Recovery = 87%  Analysis Date = 01/09/13 
 Pct Recovery = 88%  Analysis Date = 01/09/13 
 Pct Recovery = 88%  Analysis Date = 12/16/12 
 Pct Recovery = 88%  Analysis Date = 12/16/12 
 Pct Recovery = 88%  Analysis Date = 11/23/12 
 Pct Recovery = 89%  Analysis Date = 11/23/12 
 Pct Recovery = 89%  Analysis Date = 10/30/12 
 Pct Recovery = 89%  Analysis Date = 10/30/12 
 Pct Recovery = 89%  Analysis Date = 10/07/12 
 Pct Recovery = 90%  Analysis Date = 10/07/12 
 Pct Recovery = 90%  Analysis Date = 09/13/12 
 Pct Recovery = 90%  Analysis Date = 09/13/12 
 Pct Recovery = 90%  Analysis Date = 08/21/12 
 Pct Recovery = 91%  Analysis Date = 08/21/12 
 Pct Recovery = 91%  Analysis Date = 07/28/12 
 Pct Recovery = 91%  Analysis Date = 07/28/12 
 Pct Recovery = 91%  Analysis Date = 07/05/12 
 Pct Recovery = 92%  Analysis Date = 07/05/12 
 Pct Recovery = 92%  Analysis Date = 06/11/12 
 Pct Recovery = 92%  Analysis Date = 06/11/12 
 Pct Recovery = 92%  Analysis Date = 05/19/12 
 Pct Recovery = 93%  Analysis Date = 05/19/12 
 Pct Recovery = 93%  Analysis Date = 04/25/12 
 Pct Recovery = 93%  Analysis Date = 04/25/12 
 Pct Recovery = 93%  Analysis Date = 04/02/12 
 Pct Recovery = 94%  Analysis Date = 04/02/12 
 Pct Recovery = 94%  Analysis Date = 03/09/12 
 Pct Recovery = 94%  Analysis Date = 03/09/12 
 Pct Recovery = 94%  Analysis Date = 02/15/12 
 Pct Recovery = 95%  Analysis Date = 02/15/12 
 Pct Recovery = 95%  Analysis Date = 01/22/12 
 Pct Recovery = 95%  Analysis Date = 01/22/12 
 Pct Recovery = 95%  Analysis Date = 12/30/11 
 Pct Recovery = 96%  Analysis Date = 12/30/11 
 Pct Recovery = 96%  Analysis Date = 12/06/11 
 Pct Recovery = 96%  Analysis Date = 12/06/11 
 Pct Recovery = 96%  Analysis Date = 11/13/11 
 Pct Recovery = 97%  Analysis Date = 11/13/11 
 Pct Recovery = 97%  Analysis Date = 10/20/11 
 Pct Recovery = 97%  Analysis Date = 10/20/11 
 Pct Recovery = 97%  Analysis Date = 09/27/11 
 Pct Recovery = 98%  Analysis Date = 09/27/11 
 Pct Recovery = 98%  Analysis Date = 09/03/11 
 Pct Recovery = 98%  Analysis Date = 09/03/11 
 Pct Recovery = 98%  Analysis Date = 08/10/11 
 Pct Recovery = 99%  Analysis Date = 08/10/11 
 Pct Recovery = 99%  Analysis Date = 07/18/11 
 Pct Recovery = 99%  Analysis Date = 07/18/11 
 Pct Recovery = 99%  Analysis Date = 06/24/11 
 Pct Recovery = 100%  Analysis Date = 06/24/11 
 Pct Recovery = 100%  Analysis Date = 06/01/11 
 Pct Recovery = 100%  Analysis Date = 06/01/11 
 Pct Recovery = 100%  Analysis Date = 05/08/11 
 Pct Recovery = 101%  Analysis Date = 05/08/11 
 Pct Recovery = 101%  Analysis Date = 04/15/11 
 Pct Recovery = 101%  Analysis Date = 04/15/11 
 Pct Recovery = 101%  Analysis Date = 03/22/11 
 Pct Recovery = 101%  Analysis Date = 03/22/11 
 Pct Recovery = 101%  Analysis Date = 02/27/11 
 Pct Recovery = 102%  Analysis Date = 02/27/11 
 Pct Recovery = 102%  Analysis Date = 02/03/11 
 Pct Recovery = 102%  Analysis Date = 02/03/11 
 Pct Recovery = 102%  Analysis Date = 01/11/11 
 Pct Recovery = 103%  Analysis Date = 01/11/11 
 Pct Recovery = 103%  Analysis Date = 12/18/10 
 Pct Recovery = 103%  Analysis Date = 12/18/10 
 Pct Recovery = 103%  Analysis Date = 11/25/10 
 Pct Recovery = 104%  Analysis Date = 11/25/10 
 Pct Recovery = 104%  Analysis Date = 11/01/10 
 Pct Recovery = 104%  Analysis Date = 11/01/10 
 Pct Recovery = 104%  Analysis Date = 10/09/10 
 Pct Recovery = 105%  Analysis Date = 10/09/10 
 Pct Recovery = 105%  Analysis Date = 09/15/10 
 Pct Recovery = 105%  Analysis Date = 09/15/10 
 Pct Recovery = 105%  Analysis Date = 08/23/10 
 Pct Recovery = 106%  Analysis Date = 08/23/10 
 Pct Recovery = 106%  Analysis Date = 07/30/10 
 Pct Recovery = 106%  Analysis Date = 07/30/10 
 Pct Recovery = 106%  Analysis Date = 07/07/10 
 Pct Recovery = 107%  Analysis Date = 07/07/10 
 Pct Recovery = 107%  Analysis Date = 06/13/10 
 Pct Recovery = 107%  Analysis Date = 06/13/10 
 Pct Recovery = 107%  Analysis Date = 05/21/10 
 Pct Recovery = 108%  Analysis Date = 05/21/10 
 Pct Recovery = 108%  Analysis Date = 04/27/10 
 Pct Recovery = 108%  Analysis Date = 04/27/10 
 Pct Recovery = 108%  Analysis Date = 04/04/10 
 Pct Recovery = 109%  Analysis Date = 04/04/10 
 Pct Recovery = 109%  Analysis Date = 03/11/10 
 Pct Recovery = 109%  Analysis Date = 03/11/10 
 Pct Recovery = 109%  Analysis Date = 02/16/10 
 Pct Recovery = 109%  Analysis Date = 02/16/10 
 Pct Recovery = 109%  Analysis Date = 01/23/10 
 Pct Recovery = 110%  Analysis Date = 01/23/10 
 Pct Recovery = 110%  Analysis Date = 12/31/09 
 Pct Recovery = 110%  Analysis Date = 12/31/09 
 Pct Recovery = 110%  Analysis Date = 12/07/09 
 Pct Recovery = 110%  Analysis Date = 12/07/09 
 Pct Recovery = 110%  Analysis Date = 11/14/09 
 Pct Recovery = 110%  Analysis Date = 11/14/09 
 Pct Recovery = 110%  Analysis Date = 10/21/09 
 Pct Recovery = 111%  Analysis Date = 10/21/09 
 Pct Recovery = 111%  Analysis Date = 09/28/09 
 Pct Recovery = 111%  Analysis Date = 09/28/09 
 Pct Recovery = 111%  Analysis Date = 09/04/09 
 Pct Recovery = 111%  Analysis Date = 09/04/09 
 Pct Recovery = 111%  Analysis Date = 08/12/09 
 Pct Recovery = 111%  Analysis Date = 08/12/09 
 Pct Recovery = 111%  Analysis Date = 07/19/09 
 Pct Recovery = 111%  Analysis Date = 07/19/09 
 Pct Recovery = 111%  Analysis Date = 06/26/09 
 Pct Recovery = 111%  Analysis Date = 06/26/09 
 Pct Recovery = 111%  Analysis Date = 06/02/09 
 Pct Recovery = 111%  Analysis Date = 06/02/09 
 Pct Recovery = 111%  Analysis Date = 05/10/09 
 Pct Recovery = 111%  Analysis Date = 05/10/09 
 Pct Recovery = 111%  Analysis Date = 04/16/09 
 Pct Recovery = 111%  Analysis Date = 04/16/09 
 Pct Recovery = 111%  Analysis Date = 03/24/09 
 Pct Recovery = 111%  Analysis Date = 03/24/09 
 Pct Recovery = 111%  Analysis Date = 02/28/09 
 Pct Recovery = 111%  Analysis Date = 02/28/09 
 Pct Recovery = 111%  Analysis Date = 02/04/09 
 Pct Recovery = 111%  Analysis Date = 02/04/09 
 Pct Recovery = 111%  Analysis Date = 01/12/09 
 Pct Recovery = 111%  Analysis Date = 01/12/09 
 Pct Recovery = 111%  Analysis Date = 12/19/08 
 Pct Recovery = 111%  Analysis Date = 12/19/08 
 Pct Recovery = 111%  Analysis Date = 11/26/08 
 Pct Recovery = 111%  Analysis Date = 11/26/08 
 Pct Recovery = 111%  Analysis Date = 11/02/08 
 Pct Recovery = 111%  Analysis Date = 11/02/08 
 Pct Recovery = 111%  Analysis Date = 10/10/08 
 Pct Recovery = 110%  Analysis Date = 10/10/08 
 Pct Recovery = 110%  Analysis Date = 09/16/08 
 Pct Recovery = 110%  Analysis Date = 09/16/08 
 Pct Recovery = 110%  Analysis Date = 08/24/08 
 Pct Recovery = 110%  Analysis Date = 08/24/08 
 Pct Recovery = 110%  Analysis Date = 07/31/08 
 Pct Recovery = 110%  Analysis Date = 07/31/08 
 Pct Recovery = 110%  Analysis Date = 07/08/08 
 Pct Recovery = 110%  Analysis Date = 07/08/08 
 Pct Recovery = 110%  Analysis Date = 06/14/08 
 Pct Recovery = 109%  Analysis Date = 06/14/08 
 Pct Recovery = 109%  Analysis Date = 05/22/08 
 Pct Recovery = 109%  Analysis Date = 05/22/08 
 Pct Recovery = 109%  Analysis Date = 04/28/08 
 Pct Recovery = 109%  Analysis Date = 04/28/08 
 Pct Recovery = 109%  Analysis Date = 04/05/08 
 Pct Recovery = 109%  Analysis Date = 04/05/08 
 Pct Recovery = 109%  Analysis Date = 03/12/08 
 Pct Recovery = 108%  Analysis Date = 03/12/08 
 Pct Recovery = 108%  Analysis Date = 02/18/08 
 Pct Recovery = 108%  Analysis Date = 02/18/08 
 Pct Recovery = 108%  Analysis Date = 01/25/08 
 Pct Recovery = 107%  Analysis Date = 01/25/08 
 Pct Recovery = 107%  Analysis Date = 01/02/08 
 Pct Recovery = 107%  Analysis Date = 01/02/08 
 Pct Recovery = 107%  Analysis Date = 12/09/07 
 Pct Recovery = 106%  Analysis Date = 12/09/07 
 Pct Recovery = 106%  Analysis Date = 11/16/07 
 Pct Recovery = 106%  Analysis Date = 11/16/07 
 Pct Recovery = 106%  Analysis Date = 10/23/07 
 Pct Recovery = 105%  Analysis Date = 10/23/07 
 Pct Recovery = 105%  Analysis Date = 09/30/07 
 Pct Recovery = 105%  Analysis Date = 09/30/07 
 Pct Recovery = 105%  Analysis Date = 09/06/07 
 Pct Recovery = 104%  Analysis Date = 09/06/07 
 Pct Recovery = 104%  Analysis Date = 08/14/07 
 Pct Recovery = 103%  Analysis Date = 08/14/07 
 Pct Recovery = 103%  Analysis Date = 07/21/07 
 Pct Recovery = 103%  Analysis Date = 07/21/07 
 Pct Recovery = 103%  Analysis Date = 06/28/07 
 Pct Recovery = 102%  Analysis Date = 06/28/07 
 Pct Recovery = 102%  Analysis Date = 06/04/07 
 Pct Recovery = 102%  Analysis Date = 06/04/07 
 Pct Recovery = 102%  Analysis Date = 05/12/07 
 Pct Recovery = 101%  Analysis Date = 05/12/07 
 Pct Recovery = 101%  Analysis Date = 04/18/07 
 Pct Recovery = 101%  Analysis Date = 04/18/07 
 Pct Recovery = 101%  Analysis Date = 03/26/07 
 Pct Recovery = 100%  Analysis Date = 03/26/07 
 Pct Recovery = 100%  Analysis Date = 03/02/07 
 Pct Recovery = 99%  Analysis Date = 03/02/07 
 Pct Recovery = 99%  Analysis Date = 02/07/07 
 Pct Recovery = 98%  Analysis Date = 02/07/07 
 Pct Recovery = 98%  Analysis Date = 01/14/07 
 Pct Recovery = 97%  Analysis Date = 01/14/07 
 Pct Recovery = 97%  Analysis Date = 12/22/06 
 Pct Recovery = 97%  Analysis Date = 12/22/06 
 Pct Recovery = 97%  Analysis Date = 11/28/06 
 Pct Recovery = 96%  Analysis Date = 11/28/06 
 Pct Recovery = 96%  Analysis Date = 11/05/06 
 Pct Recovery = 95%  Analysis Date = 11/05/06 
 Pct Recovery = 95%  Analysis Date = 10/12/06 
 Pct Recovery = 94%  Analysis Date = 10/12/06 
 Pct Recovery = 94%  Analysis Date = 09/19/06 
 Pct Recovery = 93%  Analysis Date = 09/19/06 
 Pct Recovery = 93%  Analysis Date = 08/26/06 
 Pct Recovery = 93%  Analysis Date = 08/26/06 
 Pct Recovery = 93%  Analysis Date = 08/02/06 
 Pct Recovery = 92%  Analysis Date = 08/02/06 
 Pct Recovery = 92%  Analysis Date = 07/10/06 
 Pct Recovery = 91%  Analysis Date = 07/10/06 
 Pct Recovery = 91%  Analysis Date = 06/16/06 
 Pct Recovery = 90%  Analysis Date = 06/16/06 
 Pct Recovery = 90%  Analysis Date = 05/24/06 
 Pct Recovery = 89%  Analysis Date = 05/24/06 
 Pct Recovery = 89%  Analysis Date = 04/30/06 
 Pct Recovery = 88%  Analysis Date = 04/30/06 
 Pct Recovery = 88%  Analysis Date = 04/07/06 
 Pct Recovery = 87%  Analysis Date = 04/07/06 
 Pct Recovery = 87%  Analysis Date = 03/14/06 
 Pct Recovery = 86%  Analysis Date = 03/14/06 
 Pct Recovery = 86%  Analysis Date = 02/19/06 
 Pct Recovery = 85%  Analysis Date = 02/19/06 
 Pct Recovery = 85%  Analysis Date = 01/26/06 
 Pct Recovery = 84%  Analysis Date = 01/26/06 
 Pct Recovery = 84%  Analysis Date = 01/03/06 
 Pct Recovery = 83%  Analysis Date = 01/03/06 
 Pct Recovery = 83%  Analysis Date = 12/10/05 
 Pct Recovery = 82%  Analysis Date = 12/10/05 
 Pct Recovery = 82%  Analysis Date = 11/17/05 
 Pct Recovery = 81%  Analysis Date = 11/17/05 
 Pct Recovery = 81%  Analysis Date = 10/24/05 
 Pct Recovery = 80%  Analysis Date = 10/24/05 
 Pct Recovery = 80%  Analysis Date = 10/01/05 
 Pct Recovery = 79%  Analysis Date = 10/01/05 
 Pct Recovery = 79%  Analysis Date = 09/07/05 
 Pct Recovery = 78%  Analysis Date = 09/07/05 
 Pct Recovery = 78%  Analysis Date = 08/15/05 
 Pct Recovery = 77%  Analysis Date = 08/15/05 
 Pct Recovery = 77%  Analysis Date = 07/22/05 
 Pct Recovery = 76%  Analysis Date = 07/22/05 
 Pct Recovery = 76%  Analysis Date = 06/29/05 
 Pct Recovery = 75%  Analysis Date = 06/29/05 
 Pct Recovery = 75%  Analysis Date = 06/05/05 
 Pct Recovery = 74%  Analysis Date = 06/05/05 
 Pct Recovery = 74%  Analysis Date = 05/13/05 
 Pct Recovery = 73%  Analysis Date = 05/13/05 
 Pct Recovery = 73%  Analysis Date = 04/19/05 
 Pct Recovery = 73%  Analysis Date = 04/19/05 
 Pct Recovery = 73%  Analysis Date = 03/27/05 
 Pct Recovery = 72%  Analysis Date = 03/27/05 
 Pct Recovery = 72%  Analysis Date = 03/03/05 
 Pct Recovery = 71%  Analysis Date = 03/03/05 
 Pct Recovery = 71%  Analysis Date = 02/08/05 
 Pct Recovery = 70%  Analysis Date = 02/08/05 
 Pct Recovery = 70%  Analysis Date = 01/15/05 
 Pct Recovery = 69%  Analysis Date = 01/15/05 
 Pct Recovery = 69%  Analysis Date = 12/23/04 
 Pct Recovery = 68%  Analysis Date = 12/23/04 
 Pct Recovery = 68%  Analysis Date = 11/29/04 
 Pct Recovery = 67%  Analysis Date = 11/29/04 
 Pct Recovery = 67%  Analysis Date = 11/06/04 
 Pct Recovery = 67%  Analysis Date = 11/06/04 
 Pct Recovery = 67%  Analysis Date = 10/13/04 
 Pct Recovery = 66%  Analysis Date = 10/13/04 
 Pct Recovery = 66%  Analysis Date = 09/20/04 
 Pct Recovery = 65%  Analysis Date = 09/20/04 
 Pct Recovery = 65%  Analysis Date = 08/27/04 
 Pct Recovery = 64%  Analysis Date = 08/27/04 
 Pct Recovery = 64%  Analysis Date = 08/04/04 
 Pct Recovery = 63%  Analysis Date = 08/04/04 
 Pct Recovery = 63%  Analysis Date = 07/11/04 
 Pct Recovery = 62%  Analysis Date = 07/11/04 
 Pct Recovery = 62%  Analysis Date = 06/18/04 
 Pct Recovery = 62%  Analysis Date = 06/18/04 
 Pct Recovery = 62%  Analysis Date = 05/25/04 
 Pct Recovery = 61%  Analysis Date = 05/25/04 
 Pct Recovery = 61%  Analysis Date = 05/02/04 
 Pct Recovery = 61%  Analysis Date = 05/02/04 
 Pct Recovery = 61%  Analysis Date = 04/08/04 
 Pct Recovery = 60%  Analysis Date = 04/08/04 
 Pct Recovery = 60%  Analysis Date = 03/16/04 
 Pct Recovery = 60%  Analysis Date = 03/16/04 
 Pct Recovery = 60%  Analysis Date = 02/21/04 
 Pct Recovery = 59%  Analysis Date = 02/21/04 
 Pct Recovery = 59%  Analysis Date = 01/28/04 
 Pct Recovery = 59%  Analysis Date = 01/28/04 
 Pct Recovery = 59%  Analysis Date = 01/05/04 
 Pct Recovery = 58%  Analysis Date = 01/05/04 
 Pct Recovery = 58%  Analysis Date = 12/12/03 
 Pct Recovery = 58%  Analysis Date = 12/12/03 
 Pct Recovery = 58%  Analysis Date = 11/19/03 
 Pct Recovery = 57%  Analysis Date = 11/19/03 
 Pct Recovery = 57%  Analysis Date = 10/26/03 
 Pct Recovery = 57%  Analysis Date = 10/26/03 
 Pct Recovery = 57%  Analysis Date = 10/03/03 
 Pct Recovery = 56%  Analysis Date = 10/03/03 
 Pct Recovery = 56%  Analysis Date = 09/09/03 
 Pct Recovery = 55%  Analysis Date = 09/09/03 
 Pct Recovery = 55%  Analysis Date = 08/17/03 
 Pct Recovery = 55%  Analysis Date = 08/17/03 
 Pct Recovery = 55%  Analysis Date = 07/24/03 
 Pct Recovery = 54%  Analysis Date = 07/24/03 
 Pct Recovery = 54%  Analysis Date = 07/01/03 
 Pct Recovery = 54%  Analysis Date = 07/01/03 
 Pct Recovery = 54%  Analysis Date = 06/07/03 
 Pct Recovery = 53%  Analysis Date = 06/07/03 
 Pct Recovery = 53%  Analysis Date = 05/15/03 
 Pct Recovery = 53%  Analysis Date = 05/15/03 
 Pct Recovery = 53%  Analysis Date = 04/21/03 
 Pct Recovery = 52%  Analysis Date = 04/21/03 
 Pct Recovery = 52%  Analysis Date = 03/29/03 
 Pct Recovery = 52%  Analysis Date = 03/29/03 
 Pct Recovery = 52%  Analysis Date = 03/05/03 
 Pct Recovery = 51%  Analysis Date = 03/05/03 
 Pct Recovery = 51%  Analysis Date = 02/10/03 
 Pct Recovery = 51%  Analysis Date = 02/10/03 
 Pct Recovery = 51%  Analysis Date = 01/17/03 
 Pct Recovery = 50%  Analysis Date = 01/17/03 
 Pct Recovery = 50%  Analysis Date = 12/25/02 
 Pct Recovery = 50%  Analysis Date = 12/25/02 
 Pct Recovery = 50%  Analysis Date = 12/01/02 
 Pct Recovery = 49%  Analysis Date = 12/01/02 
 Pct Recovery = 49%  Analysis Date = 11/08/02 
 Pct Recovery = 49%  Analysis Date = 11/08/02 
 Pct Recovery = 49%  Analysis Date = 10/15/02 
 Pct Recovery = 48%  Analysis Date = 10/15/02 
 Pct Recovery = 48%  Analysis Date = 09/22/02 
 Pct Recovery = 48%  Analysis Date = 09/22/02 
 Pct Recovery = 48%  Analysis Date = 08/29/02 
 Pct Recovery = 47%  Analysis Date = 08/29/02 
 Pct Recovery = 47%  Analysis Date = 08/06/02 
 Pct Recovery = 47%  Analysis Date = 08/06/02 
 Pct Recovery = 47%  Analysis Date = 07/13/02 
 Pct Recovery = 46%  Analysis Date = 07/13/02 
 Pct Recovery = 46%  Analysis Date = 06/20/02 
 Pct Recovery = 46%  Analysis Date = 06/20/02 
 Pct Recovery = 46%  Analysis Date = 05/27/02 
 Pct Recovery = 45%  Analysis Date = 05/27/02 
 Pct Recovery = 45%  Analysis Date = 05/04/02 
 Pct Recovery = 45%  Analysis Date = 05/04/02 
 Pct Recovery = 45%  Analysis Date = 04/10/02 
 Pct Recovery = 44%  Analysis Date = 04/10/02 
 Pct Recovery = 44%  Analysis Date = 03/18/02 
 Pct Recovery = 44%  Analysis Date = 03/18/02 
 Pct Recovery = 44%  Analysis Date = 02/22/02 
 Pct Recovery = 43%  Analysis Date = 02/22/02 
 Pct Recovery = 43%  Analysis Date = 01/30/02 
 Pct Recovery = 43%  Analysis Date = 01/30/02 
 Pct Recovery = 43%  Analysis Date = 01/06/02 
 Pct Recovery = 43%  Analysis Date = 01/06/02 
 Pct Recovery = 43%  Analysis Date = 12/14/01 
 Pct Recovery = 42%  Analysis Date = 12/14/01 
 Pct Recovery = 42%  Analysis Date = 11/20/01 
 Pct Recovery = 42%  Analysis Date = 11/20/01 
 Pct Recovery = 42%  Analysis Date = 10/28/01 
 Pct Recovery = 41%  Analysis Date = 10/28/01 
 Pct Recovery = 41%  Analysis Date = 10/04/01 
 Pct Recovery = 41%  Analysis Date = 10/04/01 
 Pct Recovery = 41%  Analysis Date = 09/11/01 
 Pct Recovery = 40%  Analysis Date = 09/11/01 
 Pct Recovery = 40%  Analysis Date = 08/18/01 
 Pct Recovery = 40%  Analysis Date = 08/18/01 
 Pct Recovery = 40%  Analysis Date = 07/25/01 
 Pct Recovery = 40%  Analysis Date = 07/25/01 
 Pct Recovery = 40%  Analysis Date = 07/02/01 
 Pct Recovery = 39%  Analysis Date = 07/02/01 
 Pct Recovery = 39%  Analysis Date = 06/08/01 
 Pct Recovery = 39%  Analysis Date = 06/08/01 
 Pct Recovery = 39%  Analysis Date = 05/16/01 
 Pct Recovery = 38%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALDICARB SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 26 111% 26% 112% 27%
>= Reporting Level 182 77% 39% 77% 40%
Total 208 81% 39% 81% 41%

Sample Statistics
ALDICARB SULFOXIDE

Characteristic N % % Basis
Plotted 208 92% Spiked
Estimated Values 175 78% Spiked
Deleted Values 3 1% Spiked + Not Spiked
Spiked, Censored 3 1% Spiked
Spiked 226 .  
False Negatives 14 6% 14 out of 225
Not Spiked 200 .  
False Positives 16 8% 16 out of 198