BQS OBSP Determination:
DICAMBA
METHOD: 2060 , TESTIDCODE: 38442LCM29
Open Data Set

Analysis Date = 06/20/04 SpikeMix = NSI 100303HPLC: 200 µl Pct Recovery = 108% Analysis Date = 09/09/04 SpikeMix = NSI 100303HPLC: 200 µl Pct Recovery = 128% Analysis Date = 03/25/04 SpikeMix = NSI 100303HPLC: 200 µl Pct Recovery = 87% Analysis Date = 04/11/03 SpikeMix = Crescent 08BB071: 100 µl & Crescent 09BB025: 100 µl & Crescent 09BL026: 100 µl Pct Recovery = 89% Analysis Date = 12/20/01 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl Pct Recovery = 104% Analysis Date = 05/16/01 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl Pct Recovery = 93% Analysis Date = 10/05/01 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl Pct Recovery = 87% Analysis Date = 11/07/01 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl Pct Recovery = 98% Analysis Date = 03/13/02 SpikeMix = Supelco LA-88006: 75 µl & Supelco LA-88007: 75 µl Pct Recovery = 95% Analysis Date = 11/10/01 SpikeMix = Supelco LA-88006: 75 µl & Supelco LA-88007: 75 µl Pct Recovery = 107% Analysis Date = 01/19/13 SpikeMix = Spex Organics T1120525009: 100 µl & NSI 062612-01: 100 µl & NSI 718L-01-01: 100 Pct Recovery = 62% Analysis Date = 11/17/04 SpikeMix = NSI 100303HPLC: 100 µl Pct Recovery = 110% Analysis Date = 01/29/05 SpikeMix = NSI 100303HPLC: 100 µl Pct Recovery = 111% Analysis Date = 03/08/05 SpikeMix = NSI 100303HPLC: 100 µl Pct Recovery = 105% Analysis Date = 04/24/04 SpikeMix = Protocol R1030930017: 150 µl Pct Recovery = 105% Analysis Date = 12/01/04 SpikeMix = NSI 100303HPLC: 100 µl Pct Recovery = 118% Analysis Date = 06/10/04 SpikeMix = Protocol R1030930017: 150 µl Pct Recovery = 118% Analysis Date = 09/12/04 SpikeMix = Protocol R1030930017: 150 µl Pct Recovery = 108% Analysis Date = 01/09/04 SpikeMix = Protocol R1030930017: 150 µl Pct Recovery = 113% Analysis Date = 05/01/03 SpikeMix = Supelco LA99123: 200 µl & Supelco LA99124: 200 µl Pct Recovery = 77% Analysis Date = 11/27/13 SpikeMix = ChemService 1448600: 50 µl & NSI 050613: 50 µl & Supelco LC01386: 50 µl Pct Recovery = 73% Analysis Date = 07/19/13 SpikeMix = Abs 042513: 50 µl & ChemService 1448600: 50 µl Pct Recovery = 54% Analysis Date = 09/27/13 SpikeMix = Spex Organics T1130601011: 50 µl & Accu 213041030: 50 µl & Supelco LC00372: 50 µ Pct Recovery = 53% Analysis Date = 09/27/13 SpikeMix = NSI 042213HPLC: 50 µl & Accu 213041030: 50 µl & Supelco LC00372: 50 µl Pct Recovery = 122% Analysis Date = 01/05/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 106% Analysis Date = 05/14/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 79% Analysis Date = 05/01/03 SpikeMix = Absolute 090902: 40 µl & Ultra T1235: 40 µl Pct Recovery = 79% Analysis Date = 07/03/03 SpikeMix = Absolute 090902: 40 µl & Ultra T1235: 40 µl Pct Recovery = 102% Analysis Date = 05/23/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 120% Analysis Date = 09/25/03 SpikeMix = Absolute 090902: 40 µl & Ultra T1235: 40 µl Pct Recovery = 114% Analysis Date = 10/20/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 122% Analysis Date = 06/28/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 112% Analysis Date = 09/15/02 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl Pct Recovery = 94% Analysis Date = 07/20/12 SpikeMix = Spex Organics T1120525009: 50 µl & Supelco LB92941: 50 µl Pct Recovery = 59% Analysis Date = 05/02/13 SpikeMix = Abs 052312: 50 µl & Supelco LB92941: 50 µl Pct Recovery = 62% Analysis Date = 03/13/13 SpikeMix = Abs 052312: 50 µl & Supelco LB92941: 50 µl Pct Recovery = 69% Analysis Date = 06/05/13 SpikeMix = Restek A088383: 50 µl & NSI 062612-01: 50 µl & NSI 718L-01-01: 50 µl Pct Recovery = 66% Analysis Date = 08/16/01 SpikeMix = Supelco LA-88006: 30 µl & Supelco LA-88007: 30 µl Pct Recovery = 113% Analysis Date = 10/05/04 SpikeMix = Ultra U1419: 75 µl Pct Recovery = 109% Analysis Date = 07/18/04 SpikeMix = Ultra U1419: 75 µl Pct Recovery = 96% Analysis Date = 10/15/01 SpikeMix = Supelco LA-88006: 30 µl & Supelco LA-88007: 30 µl Pct Recovery = 80% Analysis Date = 03/25/04 SpikeMix = Ultra U1419: 75 µl Pct Recovery = 85% Analysis Date = 12/21/03 SpikeMix = Ultra U1419: 75 µl Pct Recovery = 114% Analysis Date = 08/13/09 SpikeMix = Supelco LB60726: 50 µl Pct Recovery = 122% Analysis Date = 09/01/09 SpikeMix = NSI 081208-01Polar: 50 µl Pct Recovery = 77% Analysis Date = 12/14/05 SpikeMix = Absolute 091202HPLC: 30 µl & Absolute 090902: 30 µl Pct Recovery = 131% Analysis Date = 01/27/06 SpikeMix = Absolute 091202HPLC: 30 µl & Absolute 090902: 30 µl Pct Recovery = 136% Analysis Date = 11/19/08 SpikeMix = NSI 081208-01Polar: 50 µl Pct Recovery = 79% Analysis Date = 11/28/07 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 74% Analysis Date = 04/04/08 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 67% Analysis Date = 06/23/08 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 57% Analysis Date = 02/12/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 74% Analysis Date = 04/04/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 68% Analysis Date = 01/03/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 46% Analysis Date = 05/16/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 64% Analysis Date = 09/10/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 64% Analysis Date = 07/10/08 SpikeMix = Abs 071607LC: 50 µl Pct Recovery = 53% Analysis Date = 09/26/08 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 39% Analysis Date = 08/03/01 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl Pct Recovery = 117% Analysis Date = 09/26/08 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 66% Analysis Date = 07/31/08 SpikeMix = Accu B7070230: 50 µl Pct Recovery = 49% Analysis Date = 06/16/01 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl Pct Recovery = 105% Analysis Date = 10/01/01 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl Pct Recovery = 70% Analysis Date = 06/06/04 SpikeMix = Crescent 09CC036: 40 µl Pct Recovery = 110% Analysis Date = 02/19/04 SpikeMix = Crescent 09CC036: 40 µl Pct Recovery = 94% Analysis Date = 10/31/03 SpikeMix = Crescent 09CC036: 40 µl Pct Recovery = 114% Analysis Date = 03/04/06 SpikeMix = Crescent 07EE046: 200 µl Pct Recovery = 108% Analysis Date = 06/01/06 SpikeMix = Crescent 07EE046: 200 µl Pct Recovery = 68% Analysis Date = 12/14/05 SpikeMix = Crescent 07EE046: 200 µl Pct Recovery = 130% Analysis Date = 07/28/06 SpikeMix = Crescent 07EE046: 200 µl Pct Recovery = 60% Analysis Date = 02/13/14 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl Pct Recovery = 59% Analysis Date = 03/04/14 SpikeMix = Abs 042513: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl Pct Recovery = 67% Analysis Date = 01/17/14 SpikeMix = Spex Organics T1130601011: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µ Pct Recovery = 57% Analysis Date = 06/05/13 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µl Pct Recovery = 57% Analysis Date = 03/26/09 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 53% Analysis Date = 09/27/13 SpikeMix = Accu 213041030: 20 µl & NSI 050613: 20 µl & Supelco LC01386: 20 µl Pct Recovery = 55% Analysis Date = 11/07/13 SpikeMix = Abs 042513: 20 µl & Accu 213041030: 20 µl & NSI 050613: 20 µl Pct Recovery = 42% Analysis Date = 04/02/14 SpikeMix = Supelco LC01386: 20 µl & Accu 213041030: 20 µl Pct Recovery = 53% Analysis Date = 04/25/14 SpikeMix = Spex Organics T1130601011: 20 µl & Accu 213041030: 20 µl Pct Recovery = 64% Analysis Date = 01/05/12 SpikeMix = Crescent 163162: 100 µl Pct Recovery = 88% Analysis Date = 07/19/11 SpikeMix = Crescent 163162: 100 µl Pct Recovery = 63% Analysis Date = 04/14/11 SpikeMix = Crescent 163162: 100 µl Pct Recovery = 62% Analysis Date = 05/20/11 SpikeMix = Restek A075600: 100 µl Pct Recovery = 72% Analysis Date = 05/07/09 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 56% Analysis Date = 07/29/09 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 54% Analysis Date = 05/22/12 SpikeMix = Restek A075600: 100 µl Pct Recovery = 82% Analysis Date = 02/14/12 SpikeMix = Restek A075600: 100 µl Pct Recovery = 84% Analysis Date = 09/14/11 SpikeMix = Restek A075600: 100 µl Pct Recovery = 61% Analysis Date = 06/23/08 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 77% Analysis Date = 04/30/08 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 69% Analysis Date = 06/18/07 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl Pct Recovery = 77% Analysis Date = 06/18/09 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 61% Analysis Date = 11/30/06 SpikeMix = NWQL ABS94077: 75 µl & NWQL ABS94078: 75 µl Pct Recovery = 62% Analysis Date = 02/27/07 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl Pct Recovery = 61% Analysis Date = 07/31/08 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl Pct Recovery = 66% Analysis Date = 12/31/08 SpikeMix = Supelco LB60726: 30 µl Pct Recovery = 45% Analysis Date = 06/18/09 SpikeMix = NSI 081208-01Polar: 30 µl Pct Recovery = 46% Analysis Date = 05/28/09 SpikeMix = Supelco LB60726: 30 µl Pct Recovery = 43% Analysis Date = 10/31/08 SpikeMix = Supelco LB60726: 30 µl Pct Recovery = 68% Analysis Date = 04/10/09 SpikeMix = NSI 081208-01Polar: 30 µl Pct Recovery = 61% Analysis Date = 10/31/08 SpikeMix = NSI 081208-01Polar: 30 µl Pct Recovery = 62% Analysis Date = 09/25/05 SpikeMix = Crescent 07DD034: 50 µl Pct Recovery = 106% Analysis Date = 08/31/05 SpikeMix = Crescent 07DD034: 50 µl Pct Recovery = 115% Analysis Date = 07/22/05 SpikeMix = Crescent 07DD034: 50 µl Pct Recovery = 102% Analysis Date = 07/07/05 SpikeMix = Crescent 07DD034: 50 µl Pct Recovery = 113% Analysis Date = 02/27/07 SpikeMix = Protocol F1060804006: 75 µl Pct Recovery = 76% Analysis Date = 09/12/07 SpikeMix = Restek A046748: 75 µl Pct Recovery = 94% Analysis Date = 06/02/07 SpikeMix = Restek A046748: 75 µl Pct Recovery = 69% Analysis Date = 01/05/07 SpikeMix = Protocol F1060804006: 75 µl Pct Recovery = 63% Analysis Date = 02/13/13 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl Pct Recovery = 112% Analysis Date = 12/06/12 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl Pct Recovery = 47% Analysis Date = 07/10/12 SpikeMix = Supelco LB92941: 20 µl Pct Recovery = 77% Analysis Date = 09/29/12 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & Restek A088383: 20 µl Pct Recovery = 59% Analysis Date = 09/15/12 SpikeMix = Spex Organics T1120525009: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl Pct Recovery = 78% Analysis Date = 12/06/12 SpikeMix = Abs 052312: 20 µl & NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl Pct Recovery = 136% Analysis Date = 08/08/12 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl Pct Recovery = 65% Analysis Date = 07/25/07 SpikeMix = Restek A046748: 75 µl Pct Recovery = 75% Analysis Date = 04/26/07 SpikeMix = Protocol F1060804006: 75 µl Pct Recovery = 52% Analysis Date = 08/14/02 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 97% Analysis Date = 05/18/02 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 112% Analysis Date = 09/26/02 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 110% Analysis Date = 06/14/03 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 112% Analysis Date = 02/10/03 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 112% Analysis Date = 07/09/04 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl Pct Recovery = 131% Analysis Date = 07/20/06 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl Pct Recovery = 79% Analysis Date = 08/13/03 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl Pct Recovery = 97% Analysis Date = 09/22/06 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl Pct Recovery = 71% Analysis Date = 10/22/03 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl Pct Recovery = 98% Analysis Date = 03/06/04 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl Pct Recovery = 102% Analysis Date = 10/31/04 SpikeMix = Protocol R1030930017: 30 µl Pct Recovery = 91% Analysis Date = 02/27/07 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl Pct Recovery = 86% Analysis Date = 08/03/05 SpikeMix = Crescent 07DD034: 40 µl Pct Recovery = 114% Analysis Date = 10/28/05 SpikeMix = Crescent 07DD034: 40 µl Pct Recovery = 110% Analysis Date = 09/14/05 SpikeMix = Crescent 07DD034: 40 µl Pct Recovery = 104% Analysis Date = 06/25/04 SpikeMix = Protocol R1030930017: 30 µl Pct Recovery = 131% Analysis Date = 06/05/05 SpikeMix = Crescent 07DD034: 40 µl Pct Recovery = 115% Analysis Date = 05/04/10 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl Pct Recovery = 115% Analysis Date = 08/24/06 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl Pct Recovery = 78% Analysis Date = 10/13/05 SpikeMix = Crescent 07DD034: 40 µl Pct Recovery = 134% Analysis Date = 04/13/04 SpikeMix = Protocol R1030930017: 30 µl Pct Recovery = 113% Analysis Date = 09/22/10 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl Pct Recovery = 62% Analysis Date = 07/28/10 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl Pct Recovery = 71% Analysis Date = 04/26/07 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl Pct Recovery = 91% Analysis Date = 07/31/07 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl Pct Recovery = 85% Analysis Date = 09/01/10 SpikeMix = ChemService 430-40B: 80 µl Pct Recovery = 80% Analysis Date = 10/28/10 SpikeMix = ChemService 430-40B: 80 µl Pct Recovery = 66% Analysis Date = 08/20/04 SpikeMix = Crescent 09CC036: 20 µl Pct Recovery = 115% Analysis Date = 05/14/04 SpikeMix = Crescent 09CC036: 20 µl Pct Recovery = 100% Analysis Date = 12/04/03 SpikeMix = Crescent 09CC036: 20 µl Pct Recovery = 95% Analysis Date = 11/01/02 SpikeMix = Supelco LA99123: 40 µl & Supelco LA99124: 40 µl Pct Recovery = 107% Analysis Date = 06/11/10 SpikeMix = Accu 209081166: 80 µl Pct Recovery = 71% Analysis Date = 06/10/04 SpikeMix = Ultra U1419: 25 µl Pct Recovery = 133% Analysis Date = 09/18/04 SpikeMix = Ultra U1419: 25 µl Pct Recovery = 113% Analysis Date = 03/06/04 SpikeMix = Ultra U1419: 25 µl Pct Recovery = 97% Analysis Date = 12/04/03 SpikeMix = Ultra U1419: 25 µl Pct Recovery = 103% Analysis Date = 09/12/07 SpikeMix = Restek A046748: 50 µl Pct Recovery = 90% Analysis Date = 06/11/03 SpikeMix = Absolute 090902: 10 µl & Absolute 091202HPLC: 10 µl & Ultra T1235: 10 µl Pct Recovery = 128% Analysis Date = 08/07/07 SpikeMix = Restek A046748: 50 µl Pct Recovery = 95% Analysis Date = 10/18/06 SpikeMix = Protocol F1060804006: 50 µl Pct Recovery = 59% Analysis Date = 01/08/05 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 142% Analysis Date = 02/14/03 SpikeMix = Absolute 090902: 10 µl & Absolute 091202HPLC: 10 µl & Ultra T1235: 10 µl Pct Recovery = 90% Analysis Date = 01/07/06 SpikeMix = Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl Pct Recovery = 123% Analysis Date = 06/25/07 SpikeMix = Protocol F1060804006: 50 µl Pct Recovery = 65% Analysis Date = 01/09/06 SpikeMix = Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl Pct Recovery = 155% Analysis Date = 03/04/06 SpikeMix = Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl Pct Recovery = 146% Analysis Date = 11/10/04 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 155% Analysis Date = 09/24/03 SpikeMix = Absolute 090902: 10 µl & Absolute 091202HPLC: 10 µl & Ultra T1235: 10 µl Pct Recovery = 112% Analysis Date = 04/01/05 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 122% Analysis Date = 02/16/05 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 131% Analysis Date = 01/27/04 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 83% Analysis Date = 05/06/04 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 145% Analysis Date = 10/21/04 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 121% Analysis Date = 05/27/02 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl Pct Recovery = 120% Analysis Date = 03/03/02 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl Pct Recovery = 107% Analysis Date = 07/18/04 SpikeMix = NSI 100303HPLC: 15 µl Pct Recovery = 99% Analysis Date = 05/01/03 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl Pct Recovery = 81% Analysis Date = 12/04/01 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl Pct Recovery = 112% Analysis Date = 08/03/03 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl Pct Recovery = 90% Analysis Date = 08/30/02 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl Pct Recovery = 102% Analysis Date = 09/25/03 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl Pct Recovery = 119% Analysis Date = 08/25/01 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl Pct Recovery = 97% Analysis Date = 10/13/01 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl Pct Recovery = 106% Analysis Date = 09/08/04 SpikeMix = Protocol R1030930017: 20 µl Pct Recovery = 114% Analysis Date = 05/14/04 SpikeMix = Protocol R1030930017: 20 µl Pct Recovery = 98% Analysis Date = 09/25/01 SpikeMix = Supelco LA-88006: 8 µl & Supelco LA-88007: 8 µl Pct Recovery = 132% Analysis Date = 01/27/04 SpikeMix = Protocol R1030930017: 20 µl Pct Recovery = 106% Analysis Date = 06/21/12 SpikeMix = Crescent 163162: 40 µl Pct Recovery = 75% Analysis Date = 03/07/12 SpikeMix = Crescent 163162: 40 µl Pct Recovery = 47% Analysis Date = 07/20/11 SpikeMix = Crescent 163162: 40 µl Pct Recovery = 47% Analysis Date = 05/21/11 SpikeMix = Crescent 163162: 40 µl Pct Recovery = 57% Analysis Date = 05/03/12 SpikeMix = Restek A075600: 40 µl Pct Recovery = 76% Analysis Date = 03/27/12 SpikeMix = Restek A075600: 40 µl Pct Recovery = 71% Analysis Date = 11/29/11 SpikeMix = Restek A075600: 40 µl Pct Recovery = 57% Analysis Date = 02/25/11 SpikeMix = Crescent 163162: 40 µl Pct Recovery = 90% Analysis Date = 06/11/11 SpikeMix = Restek A075600: 40 µl Pct Recovery = 85% Analysis Date = 01/05/11 SpikeMix = Restek A075600: 40 µl Pct Recovery = 78% Analysis Date = 03/29/02 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl Pct Recovery = 125% Analysis Date = 01/18/02 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl Pct Recovery = 114% Analysis Date = 03/03/03 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl Pct Recovery = 102% Analysis Date = 07/26/02 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl Pct Recovery = 135% Analysis Date = 01/05/03 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl Pct Recovery = 123% Analysis Date = 09/22/06 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl Pct Recovery = 52% Analysis Date = 08/09/06 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl Pct Recovery = 87% Analysis Date = 05/14/04 SpikeMix = Ultra U1419: 15 µl Pct Recovery = 101% Analysis Date = 06/27/06 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl Pct Recovery = 76% Analysis Date = 10/31/03 SpikeMix = Ultra U1419: 15 µl Pct Recovery = 105% Analysis Date = 08/26/04 SpikeMix = Ultra U1419: 15 µl Pct Recovery = 83% Analysis Date = 02/19/04 SpikeMix = Ultra U1419: 15 µl Pct Recovery = 115% Analysis Date = 07/01/10 SpikeMix = ChemService 430-40B: 40 µl Pct Recovery = 55% Analysis Date = 05/23/02 SpikeMix = Supelco LA-88006: 5 µl & Supelco LA-88007: 5 µl Pct Recovery = 97% Analysis Date = 01/21/02 SpikeMix = Supelco LA-88006: 5 µl & Supelco LA-88007: 5 µl Pct Recovery = 112% Analysis Date = 10/03/03 SpikeMix = Absolute 090902: 5 µl & Absolute 091202HPLC: 5 µl Pct Recovery = 159% Analysis Date = 11/20/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 156% Analysis Date = 07/13/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 116% Analysis Date = 03/29/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 102% Analysis Date = 05/18/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 112% Analysis Date = 08/03/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 126% Analysis Date = 02/10/03 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl Pct Recovery = 88% Analysis Date = 07/03/03 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl Pct Recovery = 112% Analysis Date = 05/16/03 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl Pct Recovery = 115% Analysis Date = 02/09/02 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl Pct Recovery = 100% Analysis Date = 09/05/03 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl Pct Recovery = 119% Analysis Date = 06/16/01 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl Pct Recovery = 104% Analysis Date = 09/25/01 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl Pct Recovery = 126% Analysis Date = 02/22/02 SpikeMix = Supelco LA99123: 15 µl & Supelco LA99124: 15 µl Pct Recovery = 132% Analysis Date = 06/27/06 SpikeMix = Crescent 07EE046: 40 µl Pct Recovery = 104% Analysis Date = 01/21/02 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl Pct Recovery = 112% Analysis Date = 09/08/02 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl Pct Recovery = 147% Analysis Date = 11/30/02 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl Pct Recovery = 161% Analysis Date = 06/16/02 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl Pct Recovery = 142% Analysis Date = 06/16/01 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl Pct Recovery = 139% Analysis Date = 04/13/03 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl Pct Recovery = 112% Analysis Date = 09/19/01 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl Pct Recovery = 128% Analysis Date = 07/23/01 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl Pct Recovery = 156% Analysis Date = 08/08/03 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl Pct Recovery = 106% Analysis Date = 08/29/07 SpikeMix = Protocol F1060804006: 20 µl Pct Recovery = 84% Analysis Date = 02/09/07 SpikeMix = Restek A046748: 20 µl Pct Recovery = 74% Analysis Date = 04/15/05 SpikeMix = Crescent 07DD034: 10 µl Pct Recovery = 107% Analysis Date = 06/19/05 SpikeMix = Crescent 07DD034: 10 µl Pct Recovery = 101% Analysis Date = 07/24/05 SpikeMix = Crescent 07DD034: 10 µl Pct Recovery = 124% Analysis Date = 08/18/05 SpikeMix = Crescent 07DD034: 10 µl Pct Recovery = 96% Analysis Date = 11/03/05 SpikeMix = Crescent 07EE046: 10 µl Pct Recovery = 123% Analysis Date = 04/25/14 Pct Recovery = 67% Analysis Date = 04/01/14 Pct Recovery = 67% Analysis Date = 04/01/14 Pct Recovery = 67% Analysis Date = 03/08/14 Pct Recovery = 67% Analysis Date = 03/08/14 Pct Recovery = 67% Analysis Date = 02/13/14 Pct Recovery = 67% Analysis Date = 02/13/14 Pct Recovery = 67% Analysis Date = 01/20/14 Pct Recovery = 67% Analysis Date = 01/20/14 Pct Recovery = 67% Analysis Date = 12/27/13 Pct Recovery = 67% Analysis Date = 12/27/13 Pct Recovery = 67% Analysis Date = 12/04/13 Pct Recovery = 67% Analysis Date = 12/04/13 Pct Recovery = 67% Analysis Date = 11/10/13 Pct Recovery = 67% Analysis Date = 11/10/13 Pct Recovery = 67% Analysis Date = 10/17/13 Pct Recovery = 67% Analysis Date = 10/17/13 Pct Recovery = 67% Analysis Date = 09/24/13 Pct Recovery = 67% Analysis Date = 09/24/13 Pct Recovery = 67% Analysis Date = 08/31/13 Pct Recovery = 67% Analysis Date = 08/31/13 Pct Recovery = 67% Analysis Date = 08/08/13 Pct Recovery = 67% Analysis Date = 08/08/13 Pct Recovery = 67% Analysis Date = 07/15/13 Pct Recovery = 67% Analysis Date = 07/15/13 Pct Recovery = 67% Analysis Date = 06/21/13 Pct Recovery = 67% Analysis Date = 06/21/13 Pct Recovery = 67% Analysis Date = 05/29/13 Pct Recovery = 67% Analysis Date = 05/29/13 Pct Recovery = 67% Analysis Date = 05/05/13 Pct Recovery = 68% Analysis Date = 05/05/13 Pct Recovery = 68% Analysis Date = 04/11/13 Pct Recovery = 68% Analysis Date = 04/11/13 Pct Recovery = 68% Analysis Date = 03/19/13 Pct Recovery = 68% Analysis Date = 03/19/13 Pct Recovery = 68% Analysis Date = 02/23/13 Pct Recovery = 68% Analysis Date = 02/23/13 Pct Recovery = 68% Analysis Date = 01/30/13 Pct Recovery = 68% Analysis Date = 01/30/13 Pct Recovery = 68% Analysis Date = 01/07/13 Pct Recovery = 68% Analysis Date = 01/07/13 Pct Recovery = 68% Analysis Date = 12/14/12 Pct Recovery = 68% Analysis Date = 12/14/12 Pct Recovery = 68% Analysis Date = 11/21/12 Pct Recovery = 68% Analysis Date = 11/21/12 Pct Recovery = 68% Analysis Date = 10/28/12 Pct Recovery = 68% Analysis Date = 10/28/12 Pct Recovery = 68% Analysis Date = 10/04/12 Pct Recovery = 68% Analysis Date = 10/04/12 Pct Recovery = 68% Analysis Date = 09/11/12 Pct Recovery = 68% Analysis Date = 09/11/12 Pct Recovery = 68% Analysis Date = 08/18/12 Pct Recovery = 68% Analysis Date = 08/18/12 Pct Recovery = 68% Analysis Date = 07/25/12 Pct Recovery = 68% Analysis Date = 07/25/12 Pct Recovery = 68% Analysis Date = 07/02/12 Pct Recovery = 68% Analysis Date = 07/02/12 Pct Recovery = 68% Analysis Date = 06/08/12 Pct Recovery = 68% Analysis Date = 06/08/12 Pct Recovery = 68% Analysis Date = 05/16/12 Pct Recovery = 68% Analysis Date = 05/16/12 Pct Recovery = 68% Analysis Date = 04/22/12 Pct Recovery = 68% Analysis Date = 04/22/12 Pct Recovery = 68% Analysis Date = 03/29/12 Pct Recovery = 68% Analysis Date = 03/29/12 Pct Recovery = 68% Analysis Date = 03/06/12 Pct Recovery = 68% Analysis Date = 03/06/12 Pct Recovery = 68% Analysis Date = 02/11/12 Pct Recovery = 69% Analysis Date = 02/11/12 Pct Recovery = 69% Analysis Date = 01/18/12 Pct Recovery = 69% Analysis Date = 01/18/12 Pct Recovery = 69% Analysis Date = 12/26/11 Pct Recovery = 69% Analysis Date = 12/26/11 Pct Recovery = 69% Analysis Date = 12/02/11 Pct Recovery = 69% Analysis Date = 12/02/11 Pct Recovery = 69% Analysis Date = 11/08/11 Pct Recovery = 69% Analysis Date = 11/08/11 Pct Recovery = 69% Analysis Date = 10/16/11 Pct Recovery = 69% Analysis Date = 10/16/11 Pct Recovery = 69% Analysis Date = 09/22/11 Pct Recovery = 69% Analysis Date = 09/22/11 Pct Recovery = 69% Analysis Date = 08/30/11 Pct Recovery = 69% Analysis Date = 08/30/11 Pct Recovery = 69% Analysis Date = 08/06/11 Pct Recovery = 69% Analysis Date = 08/06/11 Pct Recovery = 69% Analysis Date = 07/13/11 Pct Recovery = 69% Analysis Date = 07/13/11 Pct Recovery = 69% Analysis Date = 06/20/11 Pct Recovery = 69% Analysis Date = 06/20/11 Pct Recovery = 69% Analysis Date = 05/27/11 Pct Recovery = 69% Analysis Date = 05/27/11 Pct Recovery = 69% Analysis Date = 05/03/11 Pct Recovery = 69% Analysis Date = 05/03/11 Pct Recovery = 69% Analysis Date = 04/10/11 Pct Recovery = 70% Analysis Date = 04/10/11 Pct Recovery = 70% Analysis Date = 03/17/11 Pct Recovery = 70% Analysis Date = 03/17/11 Pct Recovery = 70% Analysis Date = 02/21/11 Pct Recovery = 70% Analysis Date = 02/21/11 Pct Recovery = 70% Analysis Date = 01/29/11 Pct Recovery = 70% Analysis Date = 01/29/11 Pct Recovery = 70% Analysis Date = 01/05/11 Pct Recovery = 70% Analysis Date = 01/05/11 Pct Recovery = 70% Analysis Date = 12/13/10 Pct Recovery = 70% Analysis Date = 12/13/10 Pct Recovery = 70% Analysis Date = 11/19/10 Pct Recovery = 70% Analysis Date = 11/19/10 Pct Recovery = 70% Analysis Date = 10/26/10 Pct Recovery = 70% Analysis Date = 10/26/10 Pct Recovery = 70% Analysis Date = 10/03/10 Pct Recovery = 70% Analysis Date = 10/03/10 Pct Recovery = 70% Analysis Date = 09/09/10 Pct Recovery = 70% Analysis Date = 09/09/10 Pct Recovery = 70% Analysis Date = 08/16/10 Pct Recovery = 70% Analysis Date = 08/16/10 Pct Recovery = 70% Analysis Date = 07/24/10 Pct Recovery = 70% Analysis Date = 07/24/10 Pct Recovery = 70% Analysis Date = 06/30/10 Pct Recovery = 70% Analysis Date = 06/30/10 Pct Recovery = 70% Analysis Date = 06/07/10 Pct Recovery = 71% Analysis Date = 06/07/10 Pct Recovery = 71% Analysis Date = 05/14/10 Pct Recovery = 71% Analysis Date = 05/14/10 Pct Recovery = 71% Analysis Date = 04/20/10 Pct Recovery = 71% Analysis Date = 04/20/10 Pct Recovery = 71% Analysis Date = 03/28/10 Pct Recovery = 71% Analysis Date = 03/28/10 Pct Recovery = 71% Analysis Date = 03/04/10 Pct Recovery = 71% Analysis Date = 03/04/10 Pct Recovery = 71% Analysis Date = 02/08/10 Pct Recovery = 71% Analysis Date = 02/08/10 Pct Recovery = 71% Analysis Date = 01/16/10 Pct Recovery = 71% Analysis Date = 01/16/10 Pct Recovery = 71% Analysis Date = 12/23/09 Pct Recovery = 71% Analysis Date = 12/23/09 Pct Recovery = 71% Analysis Date = 11/29/09 Pct Recovery = 71% Analysis Date = 11/29/09 Pct Recovery = 71% Analysis Date = 11/06/09 Pct Recovery = 71% Analysis Date = 11/06/09 Pct Recovery = 71% Analysis Date = 10/13/09 Pct Recovery = 71% Analysis Date = 10/13/09 Pct Recovery = 71% Analysis Date = 09/20/09 Pct Recovery = 71% Analysis Date = 09/20/09 Pct Recovery = 71% Analysis Date = 08/27/09 Pct Recovery = 72% Analysis Date = 08/27/09 Pct Recovery = 72% Analysis Date = 08/03/09 Pct Recovery = 72% Analysis Date = 08/03/09 Pct Recovery = 72% Analysis Date = 07/11/09 Pct Recovery = 72% Analysis Date = 07/11/09 Pct Recovery = 72% Analysis Date = 06/17/09 Pct Recovery = 72% Analysis Date = 06/17/09 Pct Recovery = 72% Analysis Date = 05/24/09 Pct Recovery = 72% Analysis Date = 05/24/09 Pct Recovery = 72% Analysis Date = 05/01/09 Pct Recovery = 72% Analysis Date = 05/01/09 Pct Recovery = 72% Analysis Date = 04/07/09 Pct Recovery = 72% Analysis Date = 04/07/09 Pct Recovery = 72% Analysis Date = 03/15/09 Pct Recovery = 72% Analysis Date = 03/15/09 Pct Recovery = 72% Analysis Date = 02/19/09 Pct Recovery = 72% Analysis Date = 02/19/09 Pct Recovery = 72% Analysis Date = 01/26/09 Pct Recovery = 72% Analysis Date = 01/26/09 Pct Recovery = 72% Analysis Date = 01/03/09 Pct Recovery = 72% Analysis Date = 01/03/09 Pct Recovery = 72% Analysis Date = 12/10/08 Pct Recovery = 72% Analysis Date = 12/10/08 Pct Recovery = 72% Analysis Date = 11/16/08 Pct Recovery = 73% Analysis Date = 11/16/08 Pct Recovery = 73% Analysis Date = 10/24/08 Pct Recovery = 73% Analysis Date = 10/24/08 Pct Recovery = 73% Analysis Date = 09/30/08 Pct Recovery = 73% Analysis Date = 09/30/08 Pct Recovery = 73% Analysis Date = 09/06/08 Pct Recovery = 73% Analysis Date = 09/06/08 Pct Recovery = 73% Analysis Date = 08/14/08 Pct Recovery = 74% Analysis Date = 08/14/08 Pct Recovery = 74% Analysis Date = 07/21/08 Pct Recovery = 74% Analysis Date = 07/21/08 Pct Recovery = 74% Analysis Date = 06/28/08 Pct Recovery = 74% Analysis Date = 06/28/08 Pct Recovery = 74% Analysis Date = 06/04/08 Pct Recovery = 75% Analysis Date = 06/04/08 Pct Recovery = 75% Analysis Date = 05/11/08 Pct Recovery = 75% Analysis Date = 05/11/08 Pct Recovery = 75% Analysis Date = 04/18/08 Pct Recovery = 75% Analysis Date = 04/18/08 Pct Recovery = 75% Analysis Date = 03/25/08 Pct Recovery = 76% Analysis Date = 03/25/08 Pct Recovery = 76% Analysis Date = 03/01/08 Pct Recovery = 76% Analysis Date = 03/01/08 Pct Recovery = 76% Analysis Date = 02/07/08 Pct Recovery = 76% Analysis Date = 02/07/08 Pct Recovery = 76% Analysis Date = 01/14/08 Pct Recovery = 76% Analysis Date = 01/14/08 Pct Recovery = 76% Analysis Date = 12/21/07 Pct Recovery = 77% Analysis Date = 12/21/07 Pct Recovery = 77% Analysis Date = 11/28/07 Pct Recovery = 77% Analysis Date = 11/28/07 Pct Recovery = 77% Analysis Date = 11/04/07 Pct Recovery = 78% Analysis Date = 11/04/07 Pct Recovery = 78% Analysis Date = 10/12/07 Pct Recovery = 78% Analysis Date = 10/12/07 Pct Recovery = 78% Analysis Date = 09/18/07 Pct Recovery = 79% Analysis Date = 09/18/07 Pct Recovery = 79% Analysis Date = 08/25/07 Pct Recovery = 79% Analysis Date = 08/25/07 Pct Recovery = 79% Analysis Date = 08/02/07 Pct Recovery = 80% Analysis Date = 08/02/07 Pct Recovery = 80% Analysis Date = 07/09/07 Pct Recovery = 81% Analysis Date = 07/09/07 Pct Recovery = 81% Analysis Date = 06/15/07 Pct Recovery = 81% Analysis Date = 06/15/07 Pct Recovery = 81% Analysis Date = 05/23/07 Pct Recovery = 82% Analysis Date = 05/23/07 Pct Recovery = 82% Analysis Date = 04/29/07 Pct Recovery = 82% Analysis Date = 04/29/07 Pct Recovery = 82% Analysis Date = 04/06/07 Pct Recovery = 83% Analysis Date = 04/06/07 Pct Recovery = 83% Analysis Date = 03/13/07 Pct Recovery = 83% Analysis Date = 03/13/07 Pct Recovery = 83% Analysis Date = 02/17/07 Pct Recovery = 84% Analysis Date = 02/17/07 Pct Recovery = 84% Analysis Date = 01/25/07 Pct Recovery = 85% Analysis Date = 01/25/07 Pct Recovery = 85% Analysis Date = 01/01/07 Pct Recovery = 86% Analysis Date = 01/01/07 Pct Recovery = 86% Analysis Date = 12/08/06 Pct Recovery = 86% Analysis Date = 12/08/06 Pct Recovery = 86% Analysis Date = 11/15/06 Pct Recovery = 87% Analysis Date = 11/15/06 Pct Recovery = 87% Analysis Date = 10/22/06 Pct Recovery = 88% Analysis Date = 10/22/06 Pct Recovery = 88% Analysis Date = 09/28/06 Pct Recovery = 89% Analysis Date = 09/28/06 Pct Recovery = 89% Analysis Date = 09/05/06 Pct Recovery = 89% Analysis Date = 09/05/06 Pct Recovery = 89% Analysis Date = 08/12/06 Pct Recovery = 90% Analysis Date = 08/12/06 Pct Recovery = 90% Analysis Date = 07/20/06 Pct Recovery = 91% Analysis Date = 07/20/06 Pct Recovery = 91% Analysis Date = 06/26/06 Pct Recovery = 92% Analysis Date = 06/26/06 Pct Recovery = 92% Analysis Date = 06/02/06 Pct Recovery = 92% Analysis Date = 06/02/06 Pct Recovery = 92% Analysis Date = 05/10/06 Pct Recovery = 93% Analysis Date = 05/10/06 Pct Recovery = 93% Analysis Date = 04/16/06 Pct Recovery = 94% Analysis Date = 04/16/06 Pct Recovery = 94% Analysis Date = 03/23/06 Pct Recovery = 95% Analysis Date = 03/23/06 Pct Recovery = 95% Analysis Date = 02/28/06 Pct Recovery = 95% Analysis Date = 02/28/06 Pct Recovery = 95% Analysis Date = 02/04/06 Pct Recovery = 96% Analysis Date = 02/04/06 Pct Recovery = 96% Analysis Date = 01/12/06 Pct Recovery = 97% Analysis Date = 01/12/06 Pct Recovery = 97% Analysis Date = 12/19/05 Pct Recovery = 98% Analysis Date = 12/19/05 Pct Recovery = 98% Analysis Date = 11/25/05 Pct Recovery = 98% Analysis Date = 11/25/05 Pct Recovery = 98% Analysis Date = 11/02/05 Pct Recovery = 99% Analysis Date = 11/02/05 Pct Recovery = 99% Analysis Date = 10/09/05 Pct Recovery = 100% Analysis Date = 10/09/05 Pct Recovery = 100% Analysis Date = 09/15/05 Pct Recovery = 101% Analysis Date = 09/15/05 Pct Recovery = 101% Analysis Date = 08/23/05 Pct Recovery = 101% Analysis Date = 08/23/05 Pct Recovery = 101% Analysis Date = 07/30/05 Pct Recovery = 102% Analysis Date = 07/30/05 Pct Recovery = 102% Analysis Date = 07/06/05 Pct Recovery = 103% Analysis Date = 07/06/05 Pct Recovery = 103% Analysis Date = 06/13/05 Pct Recovery = 104% Analysis Date = 06/13/05 Pct Recovery = 104% Analysis Date = 05/20/05 Pct Recovery = 104% Analysis Date = 05/20/05 Pct Recovery = 104% Analysis Date = 04/27/05 Pct Recovery = 105% Analysis Date = 04/27/05 Pct Recovery = 105% Analysis Date = 04/03/05 Pct Recovery = 105% Analysis Date = 04/03/05 Pct Recovery = 105% Analysis Date = 03/10/05 Pct Recovery = 106% Analysis Date = 03/10/05 Pct Recovery = 106% Analysis Date = 02/15/05 Pct Recovery = 106% Analysis Date = 02/15/05 Pct Recovery = 106% Analysis Date = 01/22/05 Pct Recovery = 107% Analysis Date = 01/22/05 Pct Recovery = 107% Analysis Date = 12/29/04 Pct Recovery = 108% Analysis Date = 12/29/04 Pct Recovery = 108% Analysis Date = 12/06/04 Pct Recovery = 108% Analysis Date = 12/06/04 Pct Recovery = 108% Analysis Date = 11/12/04 Pct Recovery = 109% Analysis Date = 11/12/04 Pct Recovery = 109% Analysis Date = 10/19/04 Pct Recovery = 109% Analysis Date = 10/19/04 Pct Recovery = 109% Analysis Date = 09/26/04 Pct Recovery = 110% Analysis Date = 09/26/04 Pct Recovery = 110% Analysis Date = 09/02/04 Pct Recovery = 110% Analysis Date = 09/02/04 Pct Recovery = 110% Analysis Date = 08/10/04 Pct Recovery = 110% Analysis Date = 08/10/04 Pct Recovery = 110% Analysis Date = 07/17/04 Pct Recovery = 111% Analysis Date = 07/17/04 Pct Recovery = 111% Analysis Date = 06/23/04 Pct Recovery = 111% Analysis Date = 06/23/04 Pct Recovery = 111% Analysis Date = 05/31/04 Pct Recovery = 111% Analysis Date = 05/31/04 Pct Recovery = 111% Analysis Date = 05/07/04 Pct Recovery = 111% Analysis Date = 05/07/04 Pct Recovery = 111% Analysis Date = 04/13/04 Pct Recovery = 111% Analysis Date = 04/13/04 Pct Recovery = 111% Analysis Date = 03/21/04 Pct Recovery = 111% Analysis Date = 03/21/04 Pct Recovery = 111% Analysis Date = 02/26/04 Pct Recovery = 111% Analysis Date = 02/26/04 Pct Recovery = 111% Analysis Date = 02/03/04 Pct Recovery = 111% Analysis Date = 02/03/04 Pct Recovery = 111% Analysis Date = 01/10/04 Pct Recovery = 111% Analysis Date = 01/10/04 Pct Recovery = 111% Analysis Date = 12/17/03 Pct Recovery = 111% Analysis Date = 12/17/03 Pct Recovery = 111% Analysis Date = 11/24/03 Pct Recovery = 111% Analysis Date = 11/24/03 Pct Recovery = 111% Analysis Date = 10/31/03 Pct Recovery = 111% Analysis Date = 10/31/03 Pct Recovery = 111% Analysis Date = 10/07/03 Pct Recovery = 111% Analysis Date = 10/07/03 Pct Recovery = 111% Analysis Date = 09/14/03 Pct Recovery = 111% Analysis Date = 09/14/03 Pct Recovery = 111% Analysis Date = 08/21/03 Pct Recovery = 111% Analysis Date = 08/21/03 Pct Recovery = 111% Analysis Date = 07/28/03 Pct Recovery = 111% Analysis Date = 07/28/03 Pct Recovery = 111% Analysis Date = 07/05/03 Pct Recovery = 111% Analysis Date = 07/05/03 Pct Recovery = 111% Analysis Date = 06/11/03 Pct Recovery = 111% Analysis Date = 06/11/03 Pct Recovery = 111% Analysis Date = 05/19/03 Pct Recovery = 111% Analysis Date = 05/19/03 Pct Recovery = 111% Analysis Date = 04/25/03 Pct Recovery = 110% Analysis Date = 04/25/03 Pct Recovery = 110% Analysis Date = 04/01/03 Pct Recovery = 110% Analysis Date = 04/01/03 Pct Recovery = 110% Analysis Date = 03/09/03 Pct Recovery = 110% Analysis Date = 03/09/03 Pct Recovery = 110% Analysis Date = 02/13/03 Pct Recovery = 110% Analysis Date = 02/13/03 Pct Recovery = 110% Analysis Date = 01/20/03 Pct Recovery = 110% Analysis Date = 01/20/03 Pct Recovery = 110% Analysis Date = 12/28/02 Pct Recovery = 110% Analysis Date = 12/28/02 Pct Recovery = 110% Analysis Date = 12/04/02 Pct Recovery = 110% Analysis Date = 12/04/02 Pct Recovery = 110% Analysis Date = 11/11/02 Pct Recovery = 110% Analysis Date = 11/11/02 Pct Recovery = 110% Analysis Date = 10/18/02 Pct Recovery = 110% Analysis Date = 10/18/02 Pct Recovery = 110% Analysis Date = 09/24/02 Pct Recovery = 110% Analysis Date = 09/24/02 Pct Recovery = 110% Analysis Date = 09/01/02 Pct Recovery = 110% Analysis Date = 09/01/02 Pct Recovery = 110% Analysis Date = 08/08/02 Pct Recovery = 110% Analysis Date = 08/08/02 Pct Recovery = 110% Analysis Date = 07/15/02 Pct Recovery = 110% Analysis Date = 07/15/02 Pct Recovery = 110% Analysis Date = 06/22/02 Pct Recovery = 110% Analysis Date = 06/22/02 Pct Recovery = 110% Analysis Date = 05/29/02 Pct Recovery = 110% Analysis Date = 05/29/02 Pct Recovery = 110% Analysis Date = 05/05/02 Pct Recovery = 110% Analysis Date = 05/05/02 Pct Recovery = 110% Analysis Date = 04/12/02 Pct Recovery = 110% Analysis Date = 04/12/02 Pct Recovery = 110% Analysis Date = 03/19/02 Pct Recovery = 110% Analysis Date = 03/19/02 Pct Recovery = 110% Analysis Date = 02/24/02 Pct Recovery = 111% Analysis Date = 02/24/02 Pct Recovery = 111% Analysis Date = 01/31/02 Pct Recovery = 111% Analysis Date = 01/31/02 Pct Recovery = 111% Analysis Date = 01/07/02 Pct Recovery = 111% Analysis Date = 01/07/02 Pct Recovery = 111% Analysis Date = 12/15/01 Pct Recovery = 111% Analysis Date = 12/15/01 Pct Recovery = 111% Analysis Date = 11/21/01 Pct Recovery = 111% Analysis Date = 11/21/01 Pct Recovery = 111% Analysis Date = 10/28/01 Pct Recovery = 111% Analysis Date = 10/28/01 Pct Recovery = 111% Analysis Date = 10/05/01 Pct Recovery = 111% Analysis Date = 10/05/01 Pct Recovery = 111% Analysis Date = 09/11/01 Pct Recovery = 111% Analysis Date = 09/11/01 Pct Recovery = 111% Analysis Date = 08/18/01 Pct Recovery = 111% Analysis Date = 08/18/01 Pct Recovery = 111% Analysis Date = 07/26/01 Pct Recovery = 111% Analysis Date = 07/26/01 Pct Recovery = 111% Analysis Date = 07/02/01 Pct Recovery = 111% Analysis Date = 07/02/01 Pct Recovery = 111% Analysis Date = 06/09/01 Pct Recovery = 111% Analysis Date = 06/09/01 Pct Recovery = 111% Analysis Date = 05/16/01 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICAMBA

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 101% 19% 101% 29%
>= Reporting Level 235 94% 28% 97% 33%
Total 242 94% 28% 97% 32%

Sample Statistics
DICAMBA

Characteristic N % % Basis
Plotted 242 92% Spiked
Estimated Values 24 9% Spiked
Deleted Values 2 0% Spiked + Not Spiked
Spiked, Censored 3 1% Spiked
Spiked 264 .  
False Negatives 17 6% 17 out of 262
Not Spiked 171 .  
False Positives 0 0% 0 out of 171