BQS OBSP Determination:
IMAZAQUIN
METHOD: 2060 , TESTIDCODE: 50356LCM29
Open Data Set

 Analysis Date = 11/27/13 
 SpikeMix = ChemService 1448600: 50 µl & NSI 050613: 50 µl & Supelco LC01386: 50 µl 
 Pct Recovery = 338%  Analysis Date = 07/18/13 
 SpikeMix = Abs 042513: 50 µl & ChemService 1448600: 50 µl 
 Pct Recovery = 209%  Analysis Date = 06/10/04 
 SpikeMix = Protocol R1030930017: 150 µl 
 Pct Recovery = 252%  Analysis Date = 12/21/12 
 SpikeMix = Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl 
 Pct Recovery = 204%  Analysis Date = 02/12/14 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl 
 Pct Recovery = 236%  Analysis Date = 06/04/13 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µl 
 Pct Recovery = 288%  Analysis Date = 05/23/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 225%  Analysis Date = 09/15/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 259%  Analysis Date = 07/01/10 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 225%  Analysis Date = 12/29/09 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 309%  Analysis Date = 12/21/03 
 SpikeMix = ERA 0825-03-01HPLC: 60 µl 
 Pct Recovery = 215%  Analysis Date = 08/03/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 234%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 200%  Analysis Date = 03/17/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 313%  Analysis Date = 08/07/12 
 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 235%  Analysis Date = 08/22/12 
 SpikeMix = Abs 052312: 20 µl & Restek A088383: 20 µl 
 Pct Recovery = 303%  Analysis Date = 12/05/12 
 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 216%  Analysis Date = 03/26/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 370%  Analysis Date = 11/19/09 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 209%  Analysis Date = 05/06/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 268%  Analysis Date = 06/19/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 227%  Analysis Date = 06/17/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 274%  Analysis Date = 02/13/12 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 201%  Analysis Date = 11/29/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 201%  Analysis Date = 08/11/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 226%  Analysis Date = 06/28/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 211%  Analysis Date = 09/22/09 
 SpikeMix = ERA 0813-08-07Polar: 50 µl 
 Pct Recovery = 234%  Analysis Date = 10/22/03 
 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl 
 Pct Recovery = 535%  Analysis Date = 05/03/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 206%  Analysis Date = 08/30/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 227%  Analysis Date = 04/10/09 
 SpikeMix = Restek A063332: 30 µl & Restek A062398: 30 µl 
 Pct Recovery = 283%  Analysis Date = 05/28/09 
 SpikeMix = ERA 0813-08-07Polar: 30 µl 
 Pct Recovery = 232%  Analysis Date = 08/06/09 
 SpikeMix = ERA 0813-08-07Polar: 30 µl 
 Pct Recovery = 244%  Analysis Date = 08/28/04 
 SpikeMix = Absolute 082503HPLC: 20 µl 
 Pct Recovery = 210%  Analysis Date = 01/18/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 308%  Analysis Date = 12/21/03 
 SpikeMix = Absolute 082503HPLC: 20 µl 
 Pct Recovery = 211%  Analysis Date = 03/03/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 231%  Analysis Date = 07/19/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 200%  Analysis Date = 02/25/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 314%  Analysis Date = 01/05/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 211%  Analysis Date = 09/22/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 235%  Analysis Date = 03/07/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 300%  Analysis Date = 05/16/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 290%  Analysis Date = 08/22/04 
 SpikeMix = ERA 0825-03-01HPLC: 10 µl 
 Pct Recovery = 201%  Analysis Date = 06/16/01 
 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl 
 Pct Recovery = 234%  Analysis Date = 07/03/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 219%  Analysis Date = 05/16/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 305%  Analysis Date = 01/21/02 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 239%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 362%  Analysis Date = 09/19/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 271%  Analysis Date = 08/08/03 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 211%  Analysis Date = 05/03/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 370%  Analysis Date = 04/10/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 325%  Analysis Date = 10/04/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 223%  Analysis Date = 11/27/13 
 SpikeMix = ChemService 1448600: 50 µl & NSI 050613: 50 µl & Supelco LC01386: 50 µl 
 Pct Recovery = 338%  Analysis Date = 07/18/13 
 SpikeMix = Abs 042513: 50 µl & ChemService 1448600: 50 µl 
 Pct Recovery = 209%  Analysis Date = 06/10/04 
 SpikeMix = Protocol R1030930017: 150 µl 
 Pct Recovery = 252%  Analysis Date = 12/21/12 
 SpikeMix = Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl 
 Pct Recovery = 204%  Analysis Date = 09/28/13 
 SpikeMix = Accu 213041030: 20 µl & NSI 050613: 20 µl & Supelco LC01386: 20 µl 
 Pct Recovery = .  Analysis Date = 02/12/14 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl 
 Pct Recovery = 236%  Analysis Date = 06/04/13 
 SpikeMix = NSI 042213HPLC: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µl 
 Pct Recovery = 288%  Analysis Date = 05/23/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 225%  Analysis Date = 09/15/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 259%  Analysis Date = 07/01/10 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 225%  Analysis Date = 12/29/09 
 SpikeMix = NSI 090309-01HPLC: 80 µl 
 Pct Recovery = 309%  Analysis Date = 12/21/03 
 SpikeMix = ERA 0825-03-01HPLC: 60 µl 
 Pct Recovery = 215%  Analysis Date = 08/03/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 234%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 200%  Analysis Date = 03/17/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 313%  Analysis Date = 08/07/12 
 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 235%  Analysis Date = 08/22/12 
 SpikeMix = Abs 052312: 20 µl & Restek A088383: 20 µl 
 Pct Recovery = 303%  Analysis Date = 12/05/12 
 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 216%  Analysis Date = 03/26/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 370%  Analysis Date = 11/19/09 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 209%  Analysis Date = 05/06/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 268%  Analysis Date = 06/19/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 227%  Analysis Date = 06/17/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 274%  Analysis Date = 02/13/12 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 201%  Analysis Date = 11/29/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 201%  Analysis Date = 08/11/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 226%  Analysis Date = 06/28/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 211%  Analysis Date = 09/22/09 
 SpikeMix = ERA 0813-08-07Polar: 50 µl 
 Pct Recovery = 234%  Analysis Date = 10/22/03 
 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl 
 Pct Recovery = 535%  Analysis Date = 05/03/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 206%  Analysis Date = 08/30/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 227%  Analysis Date = 04/10/09 
 SpikeMix = Restek A063332: 30 µl & Restek A062398: 30 µl 
 Pct Recovery = 283%  Analysis Date = 05/28/09 
 SpikeMix = ERA 0813-08-07Polar: 30 µl 
 Pct Recovery = 232%  Analysis Date = 08/06/09 
 SpikeMix = ERA 0813-08-07Polar: 30 µl 
 Pct Recovery = 244%  Analysis Date = 08/28/04 
 SpikeMix = Absolute 082503HPLC: 20 µl 
 Pct Recovery = 210%  Analysis Date = 01/18/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 308%  Analysis Date = 12/21/03 
 SpikeMix = Absolute 082503HPLC: 20 µl 
 Pct Recovery = 211%  Analysis Date = 03/03/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 231%  Analysis Date = 07/19/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 200%  Analysis Date = 02/25/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 314%  Analysis Date = 01/05/03 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 211%  Analysis Date = 09/22/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 235%  Analysis Date = 03/07/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 300%  Analysis Date = 05/16/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 290%  Analysis Date = 08/22/04 
 SpikeMix = ERA 0825-03-01HPLC: 10 µl 
 Pct Recovery = 201%  Analysis Date = 06/16/01 
 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl 
 Pct Recovery = 234%  Analysis Date = 07/03/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 219%  Analysis Date = 05/16/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 305%  Analysis Date = 01/21/02 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 239%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 362%  Analysis Date = 09/19/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 271%  Analysis Date = 08/08/03 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 211%  Analysis Date = 05/03/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 370%  Analysis Date = 04/10/12 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 325%  Analysis Date = 10/04/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 223%  Analysis Date = 07/18/13 
 SpikeMix = Abs 042513: 50 µl & ChemService 1448600: 50 µl 
 Pct Recovery = 209%  Analysis Date = 03/12/13 
 SpikeMix = Abs 052312: 100 µl & ChemService 396400: 100 µl 
 Pct Recovery = 144%  Analysis Date = 03/04/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 173%  Analysis Date = 06/01/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 84%  Analysis Date = 12/14/05 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 170%  Analysis Date = 07/28/06 
 SpikeMix = Crescent 07EE046: 200 µl 
 Pct Recovery = 81%  Analysis Date = 12/20/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 105%  Analysis Date = 05/16/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 107%  Analysis Date = 10/05/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 138%  Analysis Date = 11/07/01 
 SpikeMix = Crescent 12M-005: 100 µl & Crescent 11L-031A: 100 µl & Crescent 04M-058A: 100 µl 
 Pct Recovery = 93%  Analysis Date = 04/24/04 
 SpikeMix = Protocol R1030930017: 150 µl 
 Pct Recovery = 144%  Analysis Date = 04/11/03 
 SpikeMix = Crescent 08BB071: 100 µl & Crescent 09BB025: 100 µl & Crescent 09BL026: 100 µl 
 Pct Recovery = 117%  Analysis Date = 09/12/04 
 SpikeMix = Protocol R1030930017: 150 µl 
 Pct Recovery = 111%  Analysis Date = 01/09/04 
 SpikeMix = Protocol R1030930017: 150 µl 
 Pct Recovery = 108%  Analysis Date = 05/01/03 
 SpikeMix = Supelco LA99123: 200 µl & Supelco LA99124: 200 µl 
 Pct Recovery = 77%  Analysis Date = 06/04/13 
 SpikeMix = Restek A088383: 50 µl & NSI 062612-01: 50 µl & NSI 718L-01-01: 50 µl 
 Pct Recovery = 199%  Analysis Date = 04/10/13 
 SpikeMix = Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl 
 Pct Recovery = 166%  Analysis Date = 12/21/12 
 SpikeMix = Spex Organics T1120525009: 50 µl & Restek A088383: 50 µl 
 Pct Recovery = 204%  Analysis Date = 11/13/12 
 SpikeMix = Abs 052312: 50 µl & ChemService 396400: 50 µl 
 Pct Recovery = 154%  Analysis Date = 11/07/13 
 SpikeMix = Abs 042513: 20 µl & Accu 213041030: 20 µl & NSI 050613: 20 µl 
 Pct Recovery = 167%  Analysis Date = 04/01/14 
 SpikeMix = Supelco LC01386: 20 µl & Accu 213041030: 20 µl 
 Pct Recovery = 125%  Analysis Date = 04/24/14 
 SpikeMix = Spex Organics T1130601011: 20 µl & Accu 213041030: 20 µl 
 Pct Recovery = 137%  Analysis Date = 03/04/14 
 SpikeMix = Abs 042513: 20 µl & ChemService 1448600: 20 µl & Supelco LC00372: 20 µl 
 Pct Recovery = 118%  Analysis Date = 01/16/14 
 SpikeMix = Spex Organics T1130601011: 20 µl & ChemService 1448600: 20 µl & NSI 050613: 20 µ 
 Pct Recovery = 126%  Analysis Date = 01/05/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 186%  Analysis Date = 05/14/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 183%  Analysis Date = 10/20/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 142%  Analysis Date = 06/28/02 
 SpikeMix = Crescent 09AA026: 40 µl & Crescent 09AM034: 40 µl & Crescent 09AL035: 40 µl 
 Pct Recovery = 121%  Analysis Date = 10/28/10 
 SpikeMix = Crescent 08LL073: 80 µl 
 Pct Recovery = 133%  Analysis Date = 10/05/04 
 SpikeMix = Ultra U1419: 75 µl 
 Pct Recovery = 139%  Analysis Date = 07/03/04 
 SpikeMix = Absolute 082503HPLC: 100 µl 
 Pct Recovery = 142%  Analysis Date = 07/18/04 
 SpikeMix = Ultra U1419: 75 µl 
 Pct Recovery = 120%  Analysis Date = 11/17/03 
 SpikeMix = Absolute 082503HPLC: 100 µl 
 Pct Recovery = 126%  Analysis Date = 03/25/04 
 SpikeMix = Ultra U1419: 75 µl 
 Pct Recovery = 126%  Analysis Date = 10/15/04 
 SpikeMix = Absolute 082503HPLC: 100 µl 
 Pct Recovery = 124%  Analysis Date = 03/06/04 
 SpikeMix = Absolute 082503HPLC: 100 µl 
 Pct Recovery = 137%  Analysis Date = 12/21/03 
 SpikeMix = Ultra U1419: 75 µl 
 Pct Recovery = 160%  Analysis Date = 09/15/04 
 SpikeMix = ERA 0825-03-01HPLC: 60 µl 
 Pct Recovery = 146%  Analysis Date = 04/24/04 
 SpikeMix = ERA 0825-03-01HPLC: 60 µl 
 Pct Recovery = 136%  Analysis Date = 06/16/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 200%  Analysis Date = 10/01/01 
 SpikeMix = NWQL LCL8SP091A: 100 µl & NWQL LCL8SP092A: 100 µl & NWQL LCL8SP093A: 100 µl 
 Pct Recovery = 101%  Analysis Date = 02/27/07 
 SpikeMix = Protocol F1060804006: 75 µl 
 Pct Recovery = 98%  Analysis Date = 01/05/07 
 SpikeMix = Protocol F1060804006: 75 µl 
 Pct Recovery = 121%  Analysis Date = 09/12/07 
 SpikeMix = Restek A046748: 75 µl 
 Pct Recovery = 62%  Analysis Date = 06/02/07 
 SpikeMix = Restek A046748: 75 µl 
 Pct Recovery = 85%  Analysis Date = 07/25/07 
 SpikeMix = Restek A046748: 75 µl 
 Pct Recovery = 81%  Analysis Date = 04/26/07 
 SpikeMix = Protocol F1060804006: 75 µl 
 Pct Recovery = 78%  Analysis Date = 06/15/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 194%  Analysis Date = 09/28/12 
 SpikeMix = NSI 062612-01: 20 µl & NSI 718L-01-01: 20 µl & Restek A088383: 20 µl 
 Pct Recovery = 188%  Analysis Date = 02/13/13 
 SpikeMix = Supelco LB92941: 20 µl & ChemService 396400: 20 µl 
 Pct Recovery = 113%  Analysis Date = 05/20/10 
 SpikeMix = NSI 090309-01HPLC: 40 µl 
 Pct Recovery = 168%  Analysis Date = 11/19/09 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 209%  Analysis Date = 09/01/10 
 SpikeMix = NSI 090309-01HPLC: 40 µl 
 Pct Recovery = 151%  Analysis Date = 07/26/10 
 SpikeMix = Crescent 08LL073: 40 µl 
 Pct Recovery = 168%  Analysis Date = 07/28/09 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 185%  Analysis Date = 04/30/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 149%  Analysis Date = 06/18/07 
 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl 
 Pct Recovery = 115%  Analysis Date = 11/30/06 
 SpikeMix = NWQL ABS94077: 75 µl & NWQL ABS94078: 75 µl 
 Pct Recovery = 110%  Analysis Date = 02/27/07 
 SpikeMix = NWQL ABS94078: 75 µl & NWQL ABS94077: 75 µl 
 Pct Recovery = 117%  Analysis Date = 07/30/08 
 SpikeMix = NWQL LCL10SP087A: 75 µl & NWQL LCL10SP087B: 75 µl 
 Pct Recovery = 135%  Analysis Date = 02/13/12 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 201%  Analysis Date = 09/12/11 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 163%  Analysis Date = 01/27/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 130%  Analysis Date = 08/29/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 91%  Analysis Date = 04/07/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 183%  Analysis Date = 06/10/11 
 SpikeMix = Abs 090910HPLC: 100 µl 
 Pct Recovery = 199%  Analysis Date = 11/29/11 
 SpikeMix = ChemService 448-45B: 100 µl 
 Pct Recovery = 201%  Analysis Date = 05/01/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 124%  Analysis Date = 09/22/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 170%  Analysis Date = 06/27/06 
 SpikeMix = Crescent 07EE046: 40 µl 
 Pct Recovery = 120%  Analysis Date = 10/18/06 
 SpikeMix = Protocol F1060804006: 50 µl 
 Pct Recovery = 103%  Analysis Date = 09/12/07 
 SpikeMix = Restek A046748: 50 µl 
 Pct Recovery = 73%  Analysis Date = 06/25/07 
 SpikeMix = Protocol F1060804006: 50 µl 
 Pct Recovery = 78%  Analysis Date = 08/07/07 
 SpikeMix = Restek A046748: 50 µl 
 Pct Recovery = 80%  Analysis Date = 12/31/08 
 SpikeMix = Restek A063332: 50 µl & Restek A062398: 50 µl 
 Pct Recovery = 169%  Analysis Date = 12/09/08 
 SpikeMix = ERA 0813-08-07Polar: 50 µl 
 Pct Recovery = 168%  Analysis Date = 09/01/09 
 SpikeMix = Restek A063332: 50 µl & Restek A062398: 50 µl 
 Pct Recovery = 194%  Analysis Date = 08/14/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 132%  Analysis Date = 05/18/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 162%  Analysis Date = 09/26/02 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 187%  Analysis Date = 06/14/03 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 113%  Analysis Date = 02/10/03 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 159%  Analysis Date = 07/09/04 
 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl 
 Pct Recovery = 129%  Analysis Date = 07/20/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 112%  Analysis Date = 08/13/03 
 SpikeMix = Supelco LA99123: 50 µl & Supelco LA99124: 50 µl 
 Pct Recovery = 175%  Analysis Date = 09/22/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 170%  Analysis Date = 03/06/04 
 SpikeMix = NWQL LCL9SP117A: 50 µl & NWQL LCL9SP117B: 50 µl 
 Pct Recovery = 139%  Analysis Date = 10/31/04 
 SpikeMix = Protocol R1030930017: 30 µl 
 Pct Recovery = 84%  Analysis Date = 02/27/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 106%  Analysis Date = 06/25/04 
 SpikeMix = Protocol R1030930017: 30 µl 
 Pct Recovery = 111%  Analysis Date = 05/03/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 206%  Analysis Date = 08/24/06 
 SpikeMix = NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl 
 Pct Recovery = 137%  Analysis Date = 04/13/04 
 SpikeMix = Protocol R1030930017: 30 µl 
 Pct Recovery = 111%  Analysis Date = 09/21/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 181%  Analysis Date = 07/27/10 
 SpikeMix = NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl 
 Pct Recovery = 185%  Analysis Date = 04/26/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 101%  Analysis Date = 07/31/07 
 SpikeMix = NWQL ABS94078: 50 µl & NWQL ABS94077: 50 µl 
 Pct Recovery = 110%  Analysis Date = 06/10/04 
 SpikeMix = Ultra U1419: 25 µl 
 Pct Recovery = 135%  Analysis Date = 09/18/04 
 SpikeMix = Ultra U1419: 25 µl 
 Pct Recovery = 123%  Analysis Date = 03/06/04 
 SpikeMix = Ultra U1419: 25 µl 
 Pct Recovery = 144%  Analysis Date = 12/04/03 
 SpikeMix = Ultra U1419: 25 µl 
 Pct Recovery = 111%  Analysis Date = 11/01/02 
 SpikeMix = Supelco LA99123: 40 µl & Supelco LA99124: 40 µl 
 Pct Recovery = 111%  Analysis Date = 05/27/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 166%  Analysis Date = 03/03/02 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 158%  Analysis Date = 12/04/01 
 SpikeMix = Crescent 09AA026: 10 µl & Crescent 09AM034: 10 µl & Crescent 09AL035: 10 µl 
 Pct Recovery = 150%  Analysis Date = 12/10/08 
 SpikeMix = Restek A063332: 30 µl & Restek A062398: 30 µl 
 Pct Recovery = 150%  Analysis Date = 07/11/09 
 SpikeMix = Restek A063332: 30 µl & Restek A062398: 30 µl 
 Pct Recovery = 185%  Analysis Date = 12/09/08 
 SpikeMix = ERA 0813-08-07Polar: 30 µl 
 Pct Recovery = 131%  Analysis Date = 09/08/04 
 SpikeMix = Protocol R1030930017: 20 µl 
 Pct Recovery = 142%  Analysis Date = 05/14/04 
 SpikeMix = Protocol R1030930017: 20 µl 
 Pct Recovery = 141%  Analysis Date = 01/27/04 
 SpikeMix = Protocol R1030930017: 20 µl 
 Pct Recovery = 167%  Analysis Date = 03/29/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 106%  Analysis Date = 03/25/04 
 SpikeMix = Absolute 082503HPLC: 20 µl 
 Pct Recovery = 151%  Analysis Date = 08/25/01 
 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl 
 Pct Recovery = 136%  Analysis Date = 05/14/04 
 SpikeMix = Ultra U1419: 15 µl 
 Pct Recovery = 123%  Analysis Date = 10/31/03 
 SpikeMix = Ultra U1419: 15 µl 
 Pct Recovery = 142%  Analysis Date = 08/26/04 
 SpikeMix = Ultra U1419: 15 µl 
 Pct Recovery = 151%  Analysis Date = 02/19/04 
 SpikeMix = Ultra U1419: 15 µl 
 Pct Recovery = 104%  Analysis Date = 02/02/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 154%  Analysis Date = 07/19/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 200%  Analysis Date = 04/12/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 193%  Analysis Date = 10/13/01 
 SpikeMix = Crescent 12M-005: 10 µl & Crescent 11L-031A: 10 µl & Crescent 04M-058A: 10 µl 
 Pct Recovery = 137%  Analysis Date = 07/26/02 
 SpikeMix = Supelco LA99123: 25 µl & Supelco LA99124: 25 µl 
 Pct Recovery = 130%  Analysis Date = 05/05/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 170%  Analysis Date = 01/04/11 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 140%  Analysis Date = 08/09/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 107%  Analysis Date = 05/01/03 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 111%  Analysis Date = 12/29/02 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 146%  Analysis Date = 06/27/06 
 SpikeMix = NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl 
 Pct Recovery = 137%  Analysis Date = 08/03/03 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 174%  Analysis Date = 09/25/03 
 SpikeMix = Crescent 08BB071: 10 µl & Crescent 09BB025: 10 µl & Crescent 09BL026: 10 µl 
 Pct Recovery = 151%  Analysis Date = 08/29/07 
 SpikeMix = Protocol F1060804006: 20 µl 
 Pct Recovery = 137%  Analysis Date = 01/22/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 131%  Analysis Date = 06/18/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 166%  Analysis Date = 02/09/07 
 SpikeMix = Restek A046748: 20 µl 
 Pct Recovery = 97%  Analysis Date = 11/28/07 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 101%  Analysis Date = 11/30/06 
 SpikeMix = Restek A046748: 20 µl 
 Pct Recovery = 106%  Analysis Date = 02/12/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 83%  Analysis Date = 04/30/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 162%  Analysis Date = 03/12/07 
 SpikeMix = Protocol F1060804006: 20 µl 
 Pct Recovery = 75%  Analysis Date = 11/06/07 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 91%  Analysis Date = 04/04/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 140%  Analysis Date = 09/09/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 119%  Analysis Date = 04/04/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 153%  Analysis Date = 11/28/07 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 103%  Analysis Date = 07/08/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 117%  Analysis Date = 07/24/08 
 SpikeMix = Ultra CD-2088: 50 µl 
 Pct Recovery = 129%  Analysis Date = 08/27/08 
 SpikeMix = Crescent 07GG007: 50 µl 
 Pct Recovery = 174%  Analysis Date = 11/20/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 200%  Analysis Date = 07/13/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 176%  Analysis Date = 03/29/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 142%  Analysis Date = 05/18/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 175%  Analysis Date = 11/17/03 
 SpikeMix = ERA 0825-03-01HPLC: 10 µl 
 Pct Recovery = 138%  Analysis Date = 08/03/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 123%  Analysis Date = 02/19/04 
 SpikeMix = ERA 0825-03-01HPLC: 10 µl 
 Pct Recovery = 105%  Analysis Date = 08/22/04 
 SpikeMix = ERA 0825-03-01HPLC: 10 µl 
 Pct Recovery = 201%  Analysis Date = 09/25/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 117%  Analysis Date = 08/31/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 141%  Analysis Date = 07/22/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 140%  Analysis Date = 07/07/05 
 SpikeMix = Crescent 07DD034: 50 µl 
 Pct Recovery = 185%  Analysis Date = 02/09/02 
 SpikeMix = Crescent 09AA026: 5 µl & Crescent 09AM034: 5 µl & Crescent 09AL035: 5 µl 
 Pct Recovery = 191%  Analysis Date = 08/03/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 144%  Analysis Date = 10/28/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 120%  Analysis Date = 11/03/05 
 SpikeMix = Crescent 07EE046: 10 µl 
 Pct Recovery = 92%  Analysis Date = 09/14/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 192%  Analysis Date = 02/22/02 
 SpikeMix = Supelco LA99123: 15 µl & Supelco LA99124: 15 µl 
 Pct Recovery = 126%  Analysis Date = 06/05/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 128%  Analysis Date = 10/13/05 
 SpikeMix = Crescent 07DD034: 40 µl 
 Pct Recovery = 124%  Analysis Date = 05/10/06 
 SpikeMix = Crescent 07EE046: 10 µl 
 Pct Recovery = 160%  Analysis Date = 09/25/01 
 SpikeMix = Crescent 12M-005: 5 µl & Crescent 11L-031A: 5 µl & Crescent 04M-058A: 5 µl 
 Pct Recovery = 163%  Analysis Date = 02/10/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 175%  Analysis Date = 09/05/03 
 SpikeMix = Crescent 08BB071: 5 µl & Crescent 09BB025: 5 µl & Crescent 09BL026: 5 µl 
 Pct Recovery = 129%  Analysis Date = 09/08/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 137%  Analysis Date = 11/30/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 150%  Analysis Date = 06/16/02 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 141%  Analysis Date = 04/13/03 
 SpikeMix = Supelco LA99123: 10 µl & Supelco LA99124: 10 µl 
 Pct Recovery = 118%  Analysis Date = 07/23/01 
 SpikeMix = NWQL LCL8SP091A: 10 µl & NWQL LCL8SP092A: 10 µl & NWQL LCL8SP093A: 10 µl 
 Pct Recovery = 142%  Analysis Date = 11/28/11 
 SpikeMix = Abs 090910HPLC: 40 µl 
 Pct Recovery = 189%  Analysis Date = 03/26/12 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 189%  Analysis Date = 02/02/12 
 SpikeMix = ChemService 448-45B: 40 µl 
 Pct Recovery = 173%  Analysis Date = 04/15/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 160%  Analysis Date = 06/19/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 133%  Analysis Date = 07/24/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 153%  Analysis Date = 08/18/05 
 SpikeMix = Crescent 07DD034: 10 µl 
 Pct Recovery = 164%  Analysis Date = 08/17/12 
 Pct Recovery = 209%  Analysis Date = 08/17/12 
 Pct Recovery = 209%  Analysis Date = 07/25/12 
 Pct Recovery = 208%  Analysis Date = 07/25/12 
 Pct Recovery = 208%  Analysis Date = 07/01/12 
 Pct Recovery = 208%  Analysis Date = 07/01/12 
 Pct Recovery = 208%  Analysis Date = 06/07/12 
 Pct Recovery = 207%  Analysis Date = 06/07/12 
 Pct Recovery = 207%  Analysis Date = 05/15/12 
 Pct Recovery = 206%  Analysis Date = 05/15/12 
 Pct Recovery = 206%  Analysis Date = 04/21/12 
 Pct Recovery = 206%  Analysis Date = 04/21/12 
 Pct Recovery = 206%  Analysis Date = 03/28/12 
 Pct Recovery = 205%  Analysis Date = 03/28/12 
 Pct Recovery = 205%  Analysis Date = 03/05/12 
 Pct Recovery = 205%  Analysis Date = 03/05/12 
 Pct Recovery = 205%  Analysis Date = 02/10/12 
 Pct Recovery = 204%  Analysis Date = 02/10/12 
 Pct Recovery = 204%  Analysis Date = 01/18/12 
 Pct Recovery = 204%  Analysis Date = 01/18/12 
 Pct Recovery = 204%  Analysis Date = 12/25/11 
 Pct Recovery = 203%  Analysis Date = 12/25/11 
 Pct Recovery = 203%  Analysis Date = 12/01/11 
 Pct Recovery = 203%  Analysis Date = 12/01/11 
 Pct Recovery = 203%  Analysis Date = 11/08/11 
 Pct Recovery = 202%  Analysis Date = 11/08/11 
 Pct Recovery = 202%  Analysis Date = 10/15/11 
 Pct Recovery = 201%  Analysis Date = 10/15/11 
 Pct Recovery = 201%  Analysis Date = 09/21/11 
 Pct Recovery = 201%  Analysis Date = 09/21/11 
 Pct Recovery = 201%  Analysis Date = 08/29/11 
 Pct Recovery = 200%  Analysis Date = 08/29/11 
 Pct Recovery = 200%  Analysis Date = 08/05/11 
 Pct Recovery = 200%  Analysis Date = 08/05/11 
 Pct Recovery = 200%  Analysis Date = 07/13/11 
 Pct Recovery = 199%  Analysis Date = 07/13/11 
 Pct Recovery = 199%  Analysis Date = 06/19/11 
 Pct Recovery = 198%  Analysis Date = 06/19/11 
 Pct Recovery = 198%  Analysis Date = 05/26/11 
 Pct Recovery = 198%  Analysis Date = 05/26/11 
 Pct Recovery = 198%  Analysis Date = 05/03/11 
 Pct Recovery = 197%  Analysis Date = 05/03/11 
 Pct Recovery = 197%  Analysis Date = 04/09/11 
 Pct Recovery = 197%  Analysis Date = 04/09/11 
 Pct Recovery = 197%  Analysis Date = 03/16/11 
 Pct Recovery = 196%  Analysis Date = 03/16/11 
 Pct Recovery = 196%  Analysis Date = 02/21/11 
 Pct Recovery = 195%  Analysis Date = 02/21/11 
 Pct Recovery = 195%  Analysis Date = 01/28/11 
 Pct Recovery = 195%  Analysis Date = 01/28/11 
 Pct Recovery = 195%  Analysis Date = 01/04/11 
 Pct Recovery = 194%  Analysis Date = 01/04/11 
 Pct Recovery = 194%  Analysis Date = 12/12/10 
 Pct Recovery = 194%  Analysis Date = 12/12/10 
 Pct Recovery = 194%  Analysis Date = 11/18/10 
 Pct Recovery = 193%  Analysis Date = 11/18/10 
 Pct Recovery = 193%  Analysis Date = 10/26/10 
 Pct Recovery = 192%  Analysis Date = 10/26/10 
 Pct Recovery = 192%  Analysis Date = 10/02/10 
 Pct Recovery = 192%  Analysis Date = 10/02/10 
 Pct Recovery = 192%  Analysis Date = 09/08/10 
 Pct Recovery = 191%  Analysis Date = 09/08/10 
 Pct Recovery = 191%  Analysis Date = 08/16/10 
 Pct Recovery = 191%  Analysis Date = 08/16/10 
 Pct Recovery = 191%  Analysis Date = 07/23/10 
 Pct Recovery = 190%  Analysis Date = 07/23/10 
 Pct Recovery = 190%  Analysis Date = 06/29/10 
 Pct Recovery = 189%  Analysis Date = 06/29/10 
 Pct Recovery = 189%  Analysis Date = 06/06/10 
 Pct Recovery = 189%  Analysis Date = 06/06/10 
 Pct Recovery = 189%  Analysis Date = 05/13/10 
 Pct Recovery = 188%  Analysis Date = 05/13/10 
 Pct Recovery = 188%  Analysis Date = 04/20/10 
 Pct Recovery = 187%  Analysis Date = 04/20/10 
 Pct Recovery = 187%  Analysis Date = 03/27/10 
 Pct Recovery = 186%  Analysis Date = 03/27/10 
 Pct Recovery = 186%  Analysis Date = 03/03/10 
 Pct Recovery = 186%  Analysis Date = 03/03/10 
 Pct Recovery = 186%  Analysis Date = 02/08/10 
 Pct Recovery = 185%  Analysis Date = 02/08/10 
 Pct Recovery = 185%  Analysis Date = 01/15/10 
 Pct Recovery = 184%  Analysis Date = 01/15/10 
 Pct Recovery = 184%  Analysis Date = 12/22/09 
 Pct Recovery = 184%  Analysis Date = 12/22/09 
 Pct Recovery = 184%  Analysis Date = 11/29/09 
 Pct Recovery = 183%  Analysis Date = 11/29/09 
 Pct Recovery = 183%  Analysis Date = 11/05/09 
 Pct Recovery = 182%  Analysis Date = 11/05/09 
 Pct Recovery = 182%  Analysis Date = 10/13/09 
 Pct Recovery = 181%  Analysis Date = 10/13/09 
 Pct Recovery = 181%  Analysis Date = 09/19/09 
 Pct Recovery = 181%  Analysis Date = 09/19/09 
 Pct Recovery = 181%  Analysis Date = 08/26/09 
 Pct Recovery = 180%  Analysis Date = 08/26/09 
 Pct Recovery = 180%  Analysis Date = 08/03/09 
 Pct Recovery = 179%  Analysis Date = 08/03/09 
 Pct Recovery = 179%  Analysis Date = 07/10/09 
 Pct Recovery = 179%  Analysis Date = 07/10/09 
 Pct Recovery = 179%  Analysis Date = 06/16/09 
 Pct Recovery = 178%  Analysis Date = 06/16/09 
 Pct Recovery = 178%  Analysis Date = 05/24/09 
 Pct Recovery = 177%  Analysis Date = 05/24/09 
 Pct Recovery = 177%  Analysis Date = 04/30/09 
 Pct Recovery = 176%  Analysis Date = 04/30/09 
 Pct Recovery = 176%  Analysis Date = 04/07/09 
 Pct Recovery = 175%  Analysis Date = 04/07/09 
 Pct Recovery = 175%  Analysis Date = 03/14/09 
 Pct Recovery = 174%  Analysis Date = 03/14/09 
 Pct Recovery = 174%  Analysis Date = 02/18/09 
 Pct Recovery = 173%  Analysis Date = 02/18/09 
 Pct Recovery = 173%  Analysis Date = 01/26/09 
 Pct Recovery = 172%  Analysis Date = 01/26/09 
 Pct Recovery = 172%  Analysis Date = 01/02/09 
 Pct Recovery = 171%  Analysis Date = 01/02/09 
 Pct Recovery = 171%  Analysis Date = 12/09/08 
 Pct Recovery = 170%  Analysis Date = 12/09/08 
 Pct Recovery = 170%  Analysis Date = 11/16/08 
 Pct Recovery = 169%  Analysis Date = 11/16/08 
 Pct Recovery = 169%  Analysis Date = 10/23/08 
 Pct Recovery = 168%  Analysis Date = 10/23/08 
 Pct Recovery = 168%  Analysis Date = 09/30/08 
 Pct Recovery = 167%  Analysis Date = 09/30/08 
 Pct Recovery = 167%  Analysis Date = 09/06/08 
 Pct Recovery = 165%  Analysis Date = 09/06/08 
 Pct Recovery = 165%  Analysis Date = 08/13/08 
 Pct Recovery = 164%  Analysis Date = 08/13/08 
 Pct Recovery = 164%  Analysis Date = 07/21/08 
 Pct Recovery = 163%  Analysis Date = 07/21/08 
 Pct Recovery = 163%  Analysis Date = 06/27/08 
 Pct Recovery = 162%  Analysis Date = 06/27/08 
 Pct Recovery = 162%  Analysis Date = 06/03/08 
 Pct Recovery = 161%  Analysis Date = 06/03/08 
 Pct Recovery = 161%  Analysis Date = 05/11/08 
 Pct Recovery = 160%  Analysis Date = 05/11/08 
 Pct Recovery = 160%  Analysis Date = 04/17/08 
 Pct Recovery = 159%  Analysis Date = 04/17/08 
 Pct Recovery = 159%  Analysis Date = 03/24/08 
 Pct Recovery = 158%  Analysis Date = 03/24/08 
 Pct Recovery = 158%  Analysis Date = 03/01/08 
 Pct Recovery = 156%  Analysis Date = 03/01/08 
 Pct Recovery = 156%  Analysis Date = 02/06/08 
 Pct Recovery = 155%  Analysis Date = 02/06/08 
 Pct Recovery = 155%  Analysis Date = 01/14/08 
 Pct Recovery = 154%  Analysis Date = 01/14/08 
 Pct Recovery = 154%  Analysis Date = 12/21/07 
 Pct Recovery = 153%  Analysis Date = 12/21/07 
 Pct Recovery = 153%  Analysis Date = 11/27/07 
 Pct Recovery = 152%  Analysis Date = 11/27/07 
 Pct Recovery = 152%  Analysis Date = 11/04/07 
 Pct Recovery = 150%  Analysis Date = 11/04/07 
 Pct Recovery = 150%  Analysis Date = 10/11/07 
 Pct Recovery = 149%  Analysis Date = 10/11/07 
 Pct Recovery = 149%  Analysis Date = 09/17/07 
 Pct Recovery = 148%  Analysis Date = 09/17/07 
 Pct Recovery = 148%  Analysis Date = 08/25/07 
 Pct Recovery = 147%  Analysis Date = 08/25/07 
 Pct Recovery = 147%  Analysis Date = 08/01/07 
 Pct Recovery = 146%  Analysis Date = 08/01/07 
 Pct Recovery = 146%  Analysis Date = 07/09/07 
 Pct Recovery = 145%  Analysis Date = 07/09/07 
 Pct Recovery = 145%  Analysis Date = 06/15/07 
 Pct Recovery = 144%  Analysis Date = 06/15/07 
 Pct Recovery = 144%  Analysis Date = 05/22/07 
 Pct Recovery = 143%  Analysis Date = 05/22/07 
 Pct Recovery = 143%  Analysis Date = 04/29/07 
 Pct Recovery = 142%  Analysis Date = 04/29/07 
 Pct Recovery = 142%  Analysis Date = 04/05/07 
 Pct Recovery = 141%  Analysis Date = 04/05/07 
 Pct Recovery = 141%  Analysis Date = 03/12/07 
 Pct Recovery = 140%  Analysis Date = 03/12/07 
 Pct Recovery = 140%  Analysis Date = 02/17/07 
 Pct Recovery = 139%  Analysis Date = 02/17/07 
 Pct Recovery = 139%  Analysis Date = 01/24/07 
 Pct Recovery = 138%  Analysis Date = 01/24/07 
 Pct Recovery = 138%  Analysis Date = 01/01/07 
 Pct Recovery = 137%  Analysis Date = 01/01/07 
 Pct Recovery = 137%  Analysis Date = 12/08/06 
 Pct Recovery = 136%  Analysis Date = 12/08/06 
 Pct Recovery = 136%  Analysis Date = 11/14/06 
 Pct Recovery = 135%  Analysis Date = 11/14/06 
 Pct Recovery = 135%  Analysis Date = 10/22/06 
 Pct Recovery = 135%  Analysis Date = 10/22/06 
 Pct Recovery = 135%  Analysis Date = 09/28/06 
 Pct Recovery = 134%  Analysis Date = 09/28/06 
 Pct Recovery = 134%  Analysis Date = 09/04/06 
 Pct Recovery = 134%  Analysis Date = 09/04/06 
 Pct Recovery = 134%  Analysis Date = 08/12/06 
 Pct Recovery = 134%  Analysis Date = 08/12/06 
 Pct Recovery = 134%  Analysis Date = 07/19/06 
 Pct Recovery = 133%  Analysis Date = 07/19/06 
 Pct Recovery = 133%  Analysis Date = 06/26/06 
 Pct Recovery = 133%  Analysis Date = 06/26/06 
 Pct Recovery = 133%  Analysis Date = 06/02/06 
 Pct Recovery = 132%  Analysis Date = 06/02/06 
 Pct Recovery = 132%  Analysis Date = 05/09/06 
 Pct Recovery = 132%  Analysis Date = 05/09/06 
 Pct Recovery = 132%  Analysis Date = 04/16/06 
 Pct Recovery = 132%  Analysis Date = 04/16/06 
 Pct Recovery = 132%  Analysis Date = 03/23/06 
 Pct Recovery = 132%  Analysis Date = 03/23/06 
 Pct Recovery = 132%  Analysis Date = 02/27/06 
 Pct Recovery = 132%  Analysis Date = 02/27/06 
 Pct Recovery = 132%  Analysis Date = 02/04/06 
 Pct Recovery = 133%  Analysis Date = 02/04/06 
 Pct Recovery = 133%  Analysis Date = 01/11/06 
 Pct Recovery = 134%  Analysis Date = 01/11/06 
 Pct Recovery = 134%  Analysis Date = 12/19/05 
 Pct Recovery = 134%  Analysis Date = 12/19/05 
 Pct Recovery = 134%  Analysis Date = 11/25/05 
 Pct Recovery = 135%  Analysis Date = 11/25/05 
 Pct Recovery = 135%  Analysis Date = 11/01/05 
 Pct Recovery = 135%  Analysis Date = 11/01/05 
 Pct Recovery = 135%  Analysis Date = 10/09/05 
 Pct Recovery = 136%  Analysis Date = 10/09/05 
 Pct Recovery = 136%  Analysis Date = 09/15/05 
 Pct Recovery = 136%  Analysis Date = 09/15/05 
 Pct Recovery = 136%  Analysis Date = 08/22/05 
 Pct Recovery = 137%  Analysis Date = 08/22/05 
 Pct Recovery = 137%  Analysis Date = 07/30/05 
 Pct Recovery = 137%  Analysis Date = 07/30/05 
 Pct Recovery = 137%  Analysis Date = 07/06/05 
 Pct Recovery = 138%  Analysis Date = 07/06/05 
 Pct Recovery = 138%  Analysis Date = 06/13/05 
 Pct Recovery = 139%  Analysis Date = 06/13/05 
 Pct Recovery = 139%  Analysis Date = 05/20/05 
 Pct Recovery = 140%  Analysis Date = 05/20/05 
 Pct Recovery = 140%  Analysis Date = 04/26/05 
 Pct Recovery = 141%  Analysis Date = 04/26/05 
 Pct Recovery = 141%  Analysis Date = 04/03/05 
 Pct Recovery = 142%  Analysis Date = 04/03/05 
 Pct Recovery = 142%  Analysis Date = 03/10/05 
 Pct Recovery = 142%  Analysis Date = 03/10/05 
 Pct Recovery = 142%  Analysis Date = 02/14/05 
 Pct Recovery = 143%  Analysis Date = 02/14/05 
 Pct Recovery = 143%  Analysis Date = 01/22/05 
 Pct Recovery = 144%  Analysis Date = 01/22/05 
 Pct Recovery = 144%  Analysis Date = 12/29/04 
 Pct Recovery = 145%  Analysis Date = 12/29/04 
 Pct Recovery = 145%  Analysis Date = 12/05/04 
 Pct Recovery = 146%  Analysis Date = 12/05/04 
 Pct Recovery = 146%  Analysis Date = 11/12/04 
 Pct Recovery = 147%  Analysis Date = 11/12/04 
 Pct Recovery = 147%  Analysis Date = 10/19/04 
 Pct Recovery = 148%  Analysis Date = 10/19/04 
 Pct Recovery = 148%  Analysis Date = 09/26/04 
 Pct Recovery = 149%  Analysis Date = 09/26/04 
 Pct Recovery = 149%  Analysis Date = 09/02/04 
 Pct Recovery = 150%  Analysis Date = 09/02/04 
 Pct Recovery = 150%  Analysis Date = 08/09/04 
 Pct Recovery = 150%  Analysis Date = 08/09/04 
 Pct Recovery = 150%  Analysis Date = 07/17/04 
 Pct Recovery = 151%  Analysis Date = 07/17/04 
 Pct Recovery = 151%  Analysis Date = 06/23/04 
 Pct Recovery = 152%  Analysis Date = 06/23/04 
 Pct Recovery = 152%  Analysis Date = 05/30/04 
 Pct Recovery = 152%  Analysis Date = 05/30/04 
 Pct Recovery = 152%  Analysis Date = 05/07/04 
 Pct Recovery = 153%  Analysis Date = 05/07/04 
 Pct Recovery = 153%  Analysis Date = 04/13/04 
 Pct Recovery = 154%  Analysis Date = 04/13/04 
 Pct Recovery = 154%  Analysis Date = 03/21/04 
 Pct Recovery = 154%  Analysis Date = 03/21/04 
 Pct Recovery = 154%  Analysis Date = 02/26/04 
 Pct Recovery = 155%  Analysis Date = 02/26/04 
 Pct Recovery = 155%  Analysis Date = 02/02/04 
 Pct Recovery = 155%  Analysis Date = 02/02/04 
 Pct Recovery = 155%  Analysis Date = 01/10/04 
 Pct Recovery = 156%  Analysis Date = 01/10/04 
 Pct Recovery = 156%  Analysis Date = 12/17/03 
 Pct Recovery = 156%  Analysis Date = 12/17/03 
 Pct Recovery = 156%  Analysis Date = 11/23/03 
 Pct Recovery = 157%  Analysis Date = 11/23/03 
 Pct Recovery = 157%  Analysis Date = 10/31/03 
 Pct Recovery = 158%  Analysis Date = 10/31/03 
 Pct Recovery = 158%  Analysis Date = 10/07/03 
 Pct Recovery = 158%  Analysis Date = 10/07/03 
 Pct Recovery = 158%  Analysis Date = 09/14/03 
 Pct Recovery = 159%  Analysis Date = 09/14/03 
 Pct Recovery = 159%  Analysis Date = 08/21/03 
 Pct Recovery = 159%  Analysis Date = 08/21/03 
 Pct Recovery = 159%  Analysis Date = 07/28/03 
 Pct Recovery = 160%  Analysis Date = 07/28/03 
 Pct Recovery = 160%  Analysis Date = 07/05/03 
 Pct Recovery = 161%  Analysis Date = 07/05/03 
 Pct Recovery = 161%  Analysis Date = 06/11/03 
 Pct Recovery = 161%  Analysis Date = 06/11/03 
 Pct Recovery = 161%  Analysis Date = 05/18/03 
 Pct Recovery = 162%  Analysis Date = 05/18/03 
 Pct Recovery = 162%  Analysis Date = 04/25/03 
 Pct Recovery = 163%  Analysis Date = 04/25/03 
 Pct Recovery = 163%  Analysis Date = 04/01/03 
 Pct Recovery = 163%  Analysis Date = 04/01/03 
 Pct Recovery = 163%  Analysis Date = 03/09/03 
 Pct Recovery = 164%  Analysis Date = 03/09/03 
 Pct Recovery = 164%  Analysis Date = 02/13/03 
 Pct Recovery = 164%  Analysis Date = 02/13/03 
 Pct Recovery = 164%  Analysis Date = 01/20/03 
 Pct Recovery = 165%  Analysis Date = 01/20/03 
 Pct Recovery = 165%  Analysis Date = 12/28/02 
 Pct Recovery = 166%  Analysis Date = 12/28/02 
 Pct Recovery = 166%  Analysis Date = 12/04/02 
 Pct Recovery = 166%  Analysis Date = 12/04/02 
 Pct Recovery = 166%  Analysis Date = 11/10/02 
 Pct Recovery = 167%  Analysis Date = 11/10/02 
 Pct Recovery = 167%  Analysis Date = 10/18/02 
 Pct Recovery = 168%  Analysis Date = 10/18/02 
 Pct Recovery = 168%  Analysis Date = 09/24/02 
 Pct Recovery = 168%  Analysis Date = 09/24/02 
 Pct Recovery = 168%  Analysis Date = 09/01/02 
 Pct Recovery = 169%  Analysis Date = 09/01/02 
 Pct Recovery = 169%  Analysis Date = 08/08/02 
 Pct Recovery = 170%  Analysis Date = 08/08/02 
 Pct Recovery = 170%  Analysis Date = 07/15/02 
 Pct Recovery = 170%  Analysis Date = 07/15/02 
 Pct Recovery = 170%  Analysis Date = 06/22/02 
 Pct Recovery = 171%  Analysis Date = 06/22/02 
 Pct Recovery = 171%  Analysis Date = 05/29/02 
 Pct Recovery = 172%  Analysis Date = 05/29/02 
 Pct Recovery = 172%  Analysis Date = 05/05/02 
 Pct Recovery = 172%  Analysis Date = 05/05/02 
 Pct Recovery = 172%  Analysis Date = 04/12/02 
 Pct Recovery = 173%  Analysis Date = 04/12/02 
 Pct Recovery = 173%  Analysis Date = 03/19/02 
 Pct Recovery = 174%  Analysis Date = 03/19/02 
 Pct Recovery = 174%  Analysis Date = 02/23/02 
 Pct Recovery = 174%  Analysis Date = 02/23/02 
 Pct Recovery = 174%  Analysis Date = 01/31/02 
 Pct Recovery = 175%  Analysis Date = 01/31/02 
 Pct Recovery = 175%  Analysis Date = 01/07/02 
 Pct Recovery = 175%  Analysis Date = 01/07/02 
 Pct Recovery = 175%  Analysis Date = 12/15/01 
 Pct Recovery = 176%  Analysis Date = 12/15/01 
 Pct Recovery = 176%  Analysis Date = 11/21/01 
 Pct Recovery = 177%  Analysis Date = 11/21/01 
 Pct Recovery = 177%  Analysis Date = 10/28/01 
 Pct Recovery = 177%  Analysis Date = 10/28/01 
 Pct Recovery = 177%  Analysis Date = 10/05/01 
 Pct Recovery = 178%  Analysis Date = 10/05/01 
 Pct Recovery = 178%  Analysis Date = 09/11/01 
 Pct Recovery = 179%  Analysis Date = 09/11/01 
 Pct Recovery = 179%  Analysis Date = 08/18/01 
 Pct Recovery = 179%  Analysis Date = 08/18/01 
 Pct Recovery = 179%  Analysis Date = 07/26/01 
 Pct Recovery = 180%  Analysis Date = 07/26/01 
 Pct Recovery = 180%  Analysis Date = 07/02/01 
 Pct Recovery = 181%  Analysis Date = 07/02/01 
 Pct Recovery = 181%  Analysis Date = 06/09/01 
 Pct Recovery = 181%  Analysis Date = 06/09/01 
 Pct Recovery = 181%  Analysis Date = 05/16/01 
 Pct Recovery = 182%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
IMAZAQUIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 208% 78% 181% 47%
>= Reporting Level 219 164% 64% 146% 55%
Total 229 166% 65% 150% 53%

Sample Statistics
IMAZAQUIN

Characteristic N % % Basis
Plotted 229 100% Spiked
Estimated Values 229 100% Spiked
Deleted Values 4 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 232 .  
False Negatives 0 0% 0 out of 229
Not Spiked 203 .  
False Positives 0 0% 0 out of 202