OBSP Determination:
DIMETHENAMID SULFONIC ACID
METHOD: 2437 , TESTIDCODE: 68582LCM60

Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 97% Analysis Date = 02/16/17 SpikeMix = Abs 071216: 100 µl & ChemService 5154100: 100 µl Pct Recovery = 91% Analysis Date = 01/28/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 92% Analysis Date = 01/28/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 103% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 123% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 104% Analysis Date = 07/11/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 104% Analysis Date = 06/21/17 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 90% Analysis Date = 02/28/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 95% Analysis Date = 02/28/17 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 98% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 120% Analysis Date = 01/17/17 SpikeMix = Spex Organics TS160511023: 80 µl & Abs 071816: 80 µl Pct Recovery = 99% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 96% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 109% Analysis Date = 08/20/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 90% Analysis Date = 08/20/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 88% Analysis Date = 06/13/17 SpikeMix = ChemService 5154100: 80 µl & Abs 072516: 80 µl Pct Recovery = 87% Analysis Date = 04/18/17 SpikeMix = Abs 071216: 80 µl & ChemService 5154100: 80 µl Pct Recovery = 86% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 95% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 98% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 90% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 78% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 94% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 90% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 86% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 99% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 90% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 86% Analysis Date = 07/26/17 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 122% Analysis Date = 05/27/17 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 93% Analysis Date = 05/06/17 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 80% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 87% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 130% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 84% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 130% Analysis Date = 10/21/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 101% Analysis Date = 10/21/16 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 96% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 101% Analysis Date = 09/07/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 87% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 88% Analysis Date = 08/31/16 SpikeMix = Abs 071216: 40 µl & Abs 071816: 40 µl Pct Recovery = 85% Analysis Date = 05/23/17 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 87% Analysis Date = 11/29/16 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 94% Analysis Date = 11/29/16 SpikeMix = ChemService 5154100: 40 µl & Abs 072516: 40 µl Pct Recovery = 109% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 88% Analysis Date = 09/21/16 SpikeMix = Abs 071216: 40 µl & ChemService 5154100: 40 µl Pct Recovery = 107% Analysis Date = 08/12/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 103% Analysis Date = 08/12/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 101% Analysis Date = 08/05/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 97% Analysis Date = 08/05/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 110% Analysis Date = 08/05/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 109% Analysis Date = 08/05/16 SpikeMix = ChemService 5154100: 40 µl & ChemService 5154200: 40 µl & Spex Organics TS160603 Pct Recovery = 77% Analysis Date = 07/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 79% Analysis Date = 07/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 81% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 95% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 97% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 118% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 84% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 85% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 83% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 76% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 80% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 81% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 110% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 84% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 107% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 88% Analysis Date = 10/20/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 112% Analysis Date = 10/20/16 SpikeMix = Abs 071216: 10 µl & Abs 071816: 10 µl Pct Recovery = 83% Analysis Date = 07/25/17 Pct Recovery = 94% Analysis Date = 07/23/17 Pct Recovery = 94% Analysis Date = 07/23/17 Pct Recovery = 94% Analysis Date = 07/20/17 Pct Recovery = 94% Analysis Date = 07/20/17 Pct Recovery = 94% Analysis Date = 07/17/17 Pct Recovery = 94% Analysis Date = 07/17/17 Pct Recovery = 94% Analysis Date = 07/15/17 Pct Recovery = 94% Analysis Date = 07/15/17 Pct Recovery = 94% Analysis Date = 07/12/17 Pct Recovery = 95% Analysis Date = 07/12/17 Pct Recovery = 95% Analysis Date = 07/09/17 Pct Recovery = 95% Analysis Date = 07/09/17 Pct Recovery = 95% Analysis Date = 07/06/17 Pct Recovery = 95% Analysis Date = 07/06/17 Pct Recovery = 95% Analysis Date = 07/04/17 Pct Recovery = 95% Analysis Date = 07/04/17 Pct Recovery = 95% Analysis Date = 07/01/17 Pct Recovery = 95% Analysis Date = 07/01/17 Pct Recovery = 95% Analysis Date = 06/28/17 Pct Recovery = 95% Analysis Date = 06/28/17 Pct Recovery = 95% Analysis Date = 06/25/17 Pct Recovery = 95% Analysis Date = 06/25/17 Pct Recovery = 95% Analysis Date = 06/23/17 Pct Recovery = 95% Analysis Date = 06/23/17 Pct Recovery = 95% Analysis Date = 06/20/17 Pct Recovery = 95% Analysis Date = 06/20/17 Pct Recovery = 95% Analysis Date = 06/17/17 Pct Recovery = 95% Analysis Date = 06/17/17 Pct Recovery = 95% Analysis Date = 06/15/17 Pct Recovery = 95% Analysis Date = 06/15/17 Pct Recovery = 95% Analysis Date = 06/12/17 Pct Recovery = 95% Analysis Date = 06/12/17 Pct Recovery = 95% Analysis Date = 06/09/17 Pct Recovery = 95% Analysis Date = 06/09/17 Pct Recovery = 95% Analysis Date = 06/06/17 Pct Recovery = 95% Analysis Date = 06/06/17 Pct Recovery = 95% Analysis Date = 06/04/17 Pct Recovery = 95% Analysis Date = 06/04/17 Pct Recovery = 95% Analysis Date = 06/01/17 Pct Recovery = 95% Analysis Date = 06/01/17 Pct Recovery = 95% Analysis Date = 05/29/17 Pct Recovery = 96% Analysis Date = 05/29/17 Pct Recovery = 96% Analysis Date = 05/26/17 Pct Recovery = 96% Analysis Date = 05/26/17 Pct Recovery = 96% Analysis Date = 05/24/17 Pct Recovery = 96% Analysis Date = 05/24/17 Pct Recovery = 96% Analysis Date = 05/21/17 Pct Recovery = 96% Analysis Date = 05/21/17 Pct Recovery = 96% Analysis Date = 05/18/17 Pct Recovery = 96% Analysis Date = 05/18/17 Pct Recovery = 96% Analysis Date = 05/16/17 Pct Recovery = 96% Analysis Date = 05/16/17 Pct Recovery = 96% Analysis Date = 05/13/17 Pct Recovery = 96% Analysis Date = 05/13/17 Pct Recovery = 96% Analysis Date = 05/10/17 Pct Recovery = 96% Analysis Date = 05/10/17 Pct Recovery = 96% Analysis Date = 05/07/17 Pct Recovery = 96% Analysis Date = 05/07/17 Pct Recovery = 96% Analysis Date = 05/05/17 Pct Recovery = 96% Analysis Date = 05/05/17 Pct Recovery = 96% Analysis Date = 05/02/17 Pct Recovery = 96% Analysis Date = 05/02/17 Pct Recovery = 96% Analysis Date = 04/29/17 Pct Recovery = 96% Analysis Date = 04/29/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/10/17 Pct Recovery = 96% Analysis Date = 04/10/17 Pct Recovery = 96% Analysis Date = 04/07/17 Pct Recovery = 96% Analysis Date = 04/07/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 97% Analysis Date = 04/02/17 Pct Recovery = 97% Analysis Date = 03/30/17 Pct Recovery = 97% Analysis Date = 03/30/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/22/17 Pct Recovery = 97% Analysis Date = 03/22/17 Pct Recovery = 97% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/16/17 Pct Recovery = 97% Analysis Date = 03/16/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/11/17 Pct Recovery = 97% Analysis Date = 03/11/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/06/17 Pct Recovery = 97% Analysis Date = 03/06/17 Pct Recovery = 97% Analysis Date = 03/03/17 Pct Recovery = 97% Analysis Date = 03/03/17 Pct Recovery = 97% Analysis Date = 02/28/17 Pct Recovery = 97% Analysis Date = 02/28/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/14/17 Pct Recovery = 98% Analysis Date = 02/14/17 Pct Recovery = 98% Analysis Date = 02/12/17 Pct Recovery = 98% Analysis Date = 02/12/17 Pct Recovery = 98% Analysis Date = 02/09/17 Pct Recovery = 98% Analysis Date = 02/09/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/24/17 Pct Recovery = 99% Analysis Date = 01/24/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/18/17 Pct Recovery = 99% Analysis Date = 01/18/17 Pct Recovery = 99% Analysis Date = 01/15/17 Pct Recovery = 99% Analysis Date = 01/15/17 Pct Recovery = 99% Analysis Date = 01/13/17 Pct Recovery = 99% Analysis Date = 01/13/17 Pct Recovery = 99% Analysis Date = 01/10/17 Pct Recovery = 99% Analysis Date = 01/10/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/04/17 Pct Recovery = 100% Analysis Date = 01/04/17 Pct Recovery = 100% Analysis Date = 01/02/17 Pct Recovery = 100% Analysis Date = 01/02/17 Pct Recovery = 100% Analysis Date = 12/30/16 Pct Recovery = 100% Analysis Date = 12/30/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/25/16 Pct Recovery = 100% Analysis Date = 12/25/16 Pct Recovery = 100% Analysis Date = 12/22/16 Pct Recovery = 100% Analysis Date = 12/22/16 Pct Recovery = 100% Analysis Date = 12/19/16 Pct Recovery = 101% Analysis Date = 12/19/16 Pct Recovery = 101% Analysis Date = 12/16/16 Pct Recovery = 101% Analysis Date = 12/16/16 Pct Recovery = 101% Analysis Date = 12/14/16 Pct Recovery = 101% Analysis Date = 12/14/16 Pct Recovery = 101% Analysis Date = 12/11/16 Pct Recovery = 101% Analysis Date = 12/11/16 Pct Recovery = 101% Analysis Date = 12/08/16 Pct Recovery = 101% Analysis Date = 12/08/16 Pct Recovery = 101% Analysis Date = 12/05/16 Pct Recovery = 101% Analysis Date = 12/05/16 Pct Recovery = 101% Analysis Date = 12/03/16 Pct Recovery = 101% Analysis Date = 12/03/16 Pct Recovery = 101% Analysis Date = 11/30/16 Pct Recovery = 101% Analysis Date = 11/30/16 Pct Recovery = 101% Analysis Date = 11/27/16 Pct Recovery = 101% Analysis Date = 11/27/16 Pct Recovery = 101% Analysis Date = 11/25/16 Pct Recovery = 101% Analysis Date = 11/25/16 Pct Recovery = 101% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/19/16 Pct Recovery = 100% Analysis Date = 11/19/16 Pct Recovery = 100% Analysis Date = 11/16/16 Pct Recovery = 100% Analysis Date = 11/16/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/11/16 Pct Recovery = 100% Analysis Date = 11/11/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/08/16 Pct Recovery = 100% Analysis Date = 11/05/16 Pct Recovery = 100% Analysis Date = 11/05/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 100% Analysis Date = 10/31/16 Pct Recovery = 100% Analysis Date = 10/31/16 Pct Recovery = 100% Analysis Date = 10/28/16 Pct Recovery = 100% Analysis Date = 10/28/16 Pct Recovery = 100% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/25/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/06/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/04/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/28/16 Pct Recovery = 98% Analysis Date = 09/28/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/25/16 Pct Recovery = 98% Analysis Date = 09/23/16 Pct Recovery = 98% Analysis Date = 09/23/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/12/16 Pct Recovery = 97% Analysis Date = 09/09/16 Pct Recovery = 97% Analysis Date = 09/09/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/06/16 Pct Recovery = 97% Analysis Date = 09/04/16 Pct Recovery = 96% Analysis Date = 09/04/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/26/16 Pct Recovery = 96% Analysis Date = 08/26/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/24/16 Pct Recovery = 96% Analysis Date = 08/21/16 Pct Recovery = 95% Analysis Date = 08/21/16 Pct Recovery = 95% Analysis Date = 08/18/16 Pct Recovery = 95% Analysis Date = 08/18/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/13/16 Pct Recovery = 95% Analysis Date = 08/13/16 Pct Recovery = 95% Analysis Date = 08/10/16 Pct Recovery = 95% Analysis Date = 08/10/16 Pct Recovery = 95% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/25/16 Pct Recovery = 94% Analysis Date = 07/25/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/19/16 Pct Recovery = 94% Analysis Date = 07/19/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/16/16 Pct Recovery = 94% Analysis Date = 07/14/16 Pct Recovery = 93% Analysis Date = 07/14/16 Pct Recovery = 93% Analysis Date = 07/11/16 Pct Recovery = 93% Analysis Date = 07/11/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 06/30/16 Pct Recovery = 93% Analysis Date = 06/30/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/19/16 Pct Recovery = 93% Analysis Date = 06/19/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/11/16 Pct Recovery = 93% Analysis Date = 06/11/16 Pct Recovery = 93% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/08/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 06/03/16 Pct Recovery = 92% Analysis Date = 05/31/16 Pct Recovery = 92% Analysis Date = 05/31/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 92% Analysis Date = 05/26/16 Pct Recovery = 92% Analysis Date = 05/26/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/23/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/15/16 Pct Recovery = 92% Analysis Date = 05/15/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/09/16 Pct Recovery = 92% Analysis Date = 05/07/16 Pct Recovery = 91% Analysis Date = 05/07/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/23/16 Pct Recovery = 91% Analysis Date = 04/23/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/20/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/15/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/09/16 Pct Recovery = 91% Analysis Date = 04/09/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/04/16 Pct Recovery = 91% Analysis Date = 04/04/16 Pct Recovery = 91% Analysis Date = 04/01/16 Pct Recovery = 90% Analysis Date = 04/01/16 Pct Recovery = 90% Analysis Date = 03/29/16 Pct Recovery = 90% Analysis Date = 03/29/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/21/16 Pct Recovery = 90% Analysis Date = 03/21/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/13/16 Pct Recovery = 90% Analysis Date = 03/13/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/07/16 Pct Recovery = 90% Analysis Date = 03/07/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 02/28/16 Pct Recovery = 89% Analysis Date = 02/28/16 Pct Recovery = 89% Analysis Date = 02/26/16 Pct Recovery = 89% Analysis Date = 02/26/16 Pct Recovery = 89% Analysis Date = 02/23/16 Pct Recovery = 89% Analysis Date = 02/23/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/12/16 Pct Recovery = 89% Analysis Date = 02/12/16 Pct Recovery = 89% Analysis Date = 02/09/16 Pct Recovery = 89% Analysis Date = 02/09/16 Pct Recovery = 89% Analysis Date = 02/06/16 Pct Recovery = 88% Analysis Date = 02/06/16 Pct Recovery = 88% Analysis Date = 02/04/16 Pct Recovery = 88% Analysis Date = 02/04/16 Pct Recovery = 88% Analysis Date = 02/01/16 Pct Recovery = 88% Analysis Date = 02/01/16 Pct Recovery = 88% Analysis Date = 01/29/16 Pct Recovery = 88% Analysis Date = 01/29/16 Pct Recovery = 88% Analysis Date = 01/27/16 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHENAMID SULFONIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 97% 21% 97% 22%
>= Reporting Level 72 95% 13% 93% 12%
Total 74 95% 13% 93% 12%

Sample Statistics
DIMETHENAMID SULFONIC ACID

Characteristic N % % Basis
Plotted 74 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 74 .  
False Negatives 0 0% 0 out of 74
Not Spiked 40 .  
False Positives 0 0% 0 out of 40