OBSP Determination:
OXAMYL OXIME
METHOD: 2437 , TESTIDCODE: 68665LCM60

Analysis Date = 07/12/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 404% Analysis Date = 05/17/17 SpikeMix = Spex Organics TS160511023: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 467% Analysis Date = 10/04/17 SpikeMix = Abs 071917Pest3: 50 µl & Abs 071717Pest3: 50 µl Pct Recovery = 98% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 138% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 140% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 105% Analysis Date = 02/01/17 SpikeMix = Spex Organics TS160603008: 100 µl & Spex Organics TS160511023: 100 µl Pct Recovery = 122% Analysis Date = 01/24/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 102% Analysis Date = 01/24/17 SpikeMix = ChemService 5154100: 100 µl & Spex Organics TS160603008: 100 µl Pct Recovery = 100% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 137% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 119% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 126% Analysis Date = 08/21/16 SpikeMix = Abs 071816: 80 µl & Abs 072516: 80 µl Pct Recovery = 142% Analysis Date = 08/08/17 SpikeMix = Abs 071917Pest3: 20 µl & Abs 071717Pest3: 20 µl Pct Recovery = 115% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 120% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 129% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 117% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 105% Analysis Date = 05/07/17 SpikeMix = Abs 071816: 40 µl & Abs 072516: 40 µl Pct Recovery = 130% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 106% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 88% Analysis Date = 05/11/17 Pct Recovery = 203% Analysis Date = 05/11/17 Pct Recovery = 203% Analysis Date = 05/08/17 Pct Recovery = 201% Analysis Date = 05/08/17 Pct Recovery = 201% Analysis Date = 05/05/17 Pct Recovery = 199% Analysis Date = 05/05/17 Pct Recovery = 199% Analysis Date = 05/02/17 Pct Recovery = 196% Analysis Date = 05/02/17 Pct Recovery = 196% Analysis Date = 04/29/17 Pct Recovery = 194% Analysis Date = 04/29/17 Pct Recovery = 194% Analysis Date = 04/26/17 Pct Recovery = 192% Analysis Date = 04/26/17 Pct Recovery = 192% Analysis Date = 04/23/17 Pct Recovery = 189% Analysis Date = 04/23/17 Pct Recovery = 189% Analysis Date = 04/21/17 Pct Recovery = 187% Analysis Date = 04/21/17 Pct Recovery = 187% Analysis Date = 04/18/17 Pct Recovery = 184% Analysis Date = 04/18/17 Pct Recovery = 184% Analysis Date = 04/15/17 Pct Recovery = 182% Analysis Date = 04/15/17 Pct Recovery = 182% Analysis Date = 04/12/17 Pct Recovery = 180% Analysis Date = 04/12/17 Pct Recovery = 180% Analysis Date = 04/09/17 Pct Recovery = 177% Analysis Date = 04/09/17 Pct Recovery = 177% Analysis Date = 04/06/17 Pct Recovery = 175% Analysis Date = 04/06/17 Pct Recovery = 175% Analysis Date = 04/03/17 Pct Recovery = 173% Analysis Date = 04/03/17 Pct Recovery = 173% Analysis Date = 04/01/17 Pct Recovery = 170% Analysis Date = 04/01/17 Pct Recovery = 170% Analysis Date = 03/29/17 Pct Recovery = 168% Analysis Date = 03/29/17 Pct Recovery = 168% Analysis Date = 03/26/17 Pct Recovery = 165% Analysis Date = 03/26/17 Pct Recovery = 165% Analysis Date = 03/23/17 Pct Recovery = 163% Analysis Date = 03/23/17 Pct Recovery = 163% Analysis Date = 03/20/17 Pct Recovery = 161% Analysis Date = 03/20/17 Pct Recovery = 161% Analysis Date = 03/17/17 Pct Recovery = 158% Analysis Date = 03/17/17 Pct Recovery = 158% Analysis Date = 03/14/17 Pct Recovery = 156% Analysis Date = 03/14/17 Pct Recovery = 156% Analysis Date = 03/12/17 Pct Recovery = 154% Analysis Date = 03/12/17 Pct Recovery = 154% Analysis Date = 03/09/17 Pct Recovery = 151% Analysis Date = 03/09/17 Pct Recovery = 151% Analysis Date = 03/06/17 Pct Recovery = 149% Analysis Date = 03/06/17 Pct Recovery = 149% Analysis Date = 03/03/17 Pct Recovery = 146% Analysis Date = 03/03/17 Pct Recovery = 146% Analysis Date = 02/28/17 Pct Recovery = 144% Analysis Date = 02/28/17 Pct Recovery = 144% Analysis Date = 02/25/17 Pct Recovery = 142% Analysis Date = 02/25/17 Pct Recovery = 142% Analysis Date = 02/22/17 Pct Recovery = 139% Analysis Date = 02/22/17 Pct Recovery = 139% Analysis Date = 02/20/17 Pct Recovery = 137% Analysis Date = 02/20/17 Pct Recovery = 137% Analysis Date = 02/17/17 Pct Recovery = 135% Analysis Date = 02/17/17 Pct Recovery = 135% Analysis Date = 02/14/17 Pct Recovery = 132% Analysis Date = 02/14/17 Pct Recovery = 132% Analysis Date = 02/11/17 Pct Recovery = 130% Analysis Date = 02/11/17 Pct Recovery = 130% Analysis Date = 02/08/17 Pct Recovery = 127% Analysis Date = 02/08/17 Pct Recovery = 127% Analysis Date = 02/05/17 Pct Recovery = 125% Analysis Date = 02/05/17 Pct Recovery = 125% Analysis Date = 02/02/17 Pct Recovery = 123% Analysis Date = 02/02/17 Pct Recovery = 123% Analysis Date = 01/31/17 Pct Recovery = 120% Analysis Date = 01/31/17 Pct Recovery = 120% Analysis Date = 01/28/17 Pct Recovery = 115% Analysis Date = 01/28/17 Pct Recovery = 115% Analysis Date = 01/25/17 Pct Recovery = 111% Analysis Date = 01/25/17 Pct Recovery = 111% Analysis Date = 01/22/17 Pct Recovery = 109% Analysis Date = 01/22/17 Pct Recovery = 109% Analysis Date = 01/19/17 Pct Recovery = 109% Analysis Date = 01/19/17 Pct Recovery = 109% Analysis Date = 01/16/17 Pct Recovery = 109% Analysis Date = 01/16/17 Pct Recovery = 109% Analysis Date = 01/13/17 Pct Recovery = 109% Analysis Date = 01/13/17 Pct Recovery = 109% Analysis Date = 01/11/17 Pct Recovery = 108% Analysis Date = 01/11/17 Pct Recovery = 108% Analysis Date = 01/08/17 Pct Recovery = 108% Analysis Date = 01/08/17 Pct Recovery = 108% Analysis Date = 01/05/17 Pct Recovery = 108% Analysis Date = 01/05/17 Pct Recovery = 108% Analysis Date = 01/02/17 Pct Recovery = 108% Analysis Date = 01/02/17 Pct Recovery = 108% Analysis Date = 12/30/16 Pct Recovery = 109% Analysis Date = 12/30/16 Pct Recovery = 109% Analysis Date = 12/27/16 Pct Recovery = 109% Analysis Date = 12/27/16 Pct Recovery = 109% Analysis Date = 12/24/16 Pct Recovery = 110% Analysis Date = 12/24/16 Pct Recovery = 110% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/19/16 Pct Recovery = 111% Analysis Date = 12/19/16 Pct Recovery = 111% Analysis Date = 12/16/16 Pct Recovery = 112% Analysis Date = 12/16/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 113% Analysis Date = 12/13/16 Pct Recovery = 113% Analysis Date = 12/10/16 Pct Recovery = 113% Analysis Date = 12/10/16 Pct Recovery = 113% Analysis Date = 12/07/16 Pct Recovery = 114% Analysis Date = 12/07/16 Pct Recovery = 114% Analysis Date = 12/04/16 Pct Recovery = 115% Analysis Date = 12/04/16 Pct Recovery = 115% Analysis Date = 12/01/16 Pct Recovery = 115% Analysis Date = 12/01/16 Pct Recovery = 115% Analysis Date = 11/29/16 Pct Recovery = 116% Analysis Date = 11/29/16 Pct Recovery = 116% Analysis Date = 11/26/16 Pct Recovery = 116% Analysis Date = 11/26/16 Pct Recovery = 116% Analysis Date = 11/23/16 Pct Recovery = 117% Analysis Date = 11/23/16 Pct Recovery = 117% Analysis Date = 11/20/16 Pct Recovery = 118% Analysis Date = 11/20/16 Pct Recovery = 118% Analysis Date = 11/17/16 Pct Recovery = 118% Analysis Date = 11/17/16 Pct Recovery = 118% Analysis Date = 11/14/16 Pct Recovery = 119% Analysis Date = 11/14/16 Pct Recovery = 119% Analysis Date = 11/11/16 Pct Recovery = 120% Analysis Date = 11/11/16 Pct Recovery = 120% Analysis Date = 11/09/16 Pct Recovery = 120% Analysis Date = 11/09/16 Pct Recovery = 120% Analysis Date = 11/06/16 Pct Recovery = 121% Analysis Date = 11/06/16 Pct Recovery = 121% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 10/31/16 Pct Recovery = 122% Analysis Date = 10/31/16 Pct Recovery = 122% Analysis Date = 10/28/16 Pct Recovery = 123% Analysis Date = 10/28/16 Pct Recovery = 123% Analysis Date = 10/25/16 Pct Recovery = 124% Analysis Date = 10/25/16 Pct Recovery = 124% Analysis Date = 10/22/16 Pct Recovery = 124% Analysis Date = 10/22/16 Pct Recovery = 124% Analysis Date = 10/20/16 Pct Recovery = 125% Analysis Date = 10/20/16 Pct Recovery = 125% Analysis Date = 10/17/16 Pct Recovery = 125% Analysis Date = 10/17/16 Pct Recovery = 125% Analysis Date = 10/14/16 Pct Recovery = 126% Analysis Date = 10/14/16 Pct Recovery = 126% Analysis Date = 10/11/16 Pct Recovery = 127% Analysis Date = 10/11/16 Pct Recovery = 127% Analysis Date = 10/08/16 Pct Recovery = 127% Analysis Date = 10/08/16 Pct Recovery = 127% Analysis Date = 10/05/16 Pct Recovery = 128% Analysis Date = 10/05/16 Pct Recovery = 128% Analysis Date = 10/02/16 Pct Recovery = 129% Analysis Date = 10/02/16 Pct Recovery = 129% Analysis Date = 09/30/16 Pct Recovery = 129% Analysis Date = 09/30/16 Pct Recovery = 129% Analysis Date = 09/27/16 Pct Recovery = 130% Analysis Date = 09/27/16 Pct Recovery = 130% Analysis Date = 09/24/16 Pct Recovery = 131% Analysis Date = 09/24/16 Pct Recovery = 131% Analysis Date = 09/21/16 Pct Recovery = 131% Analysis Date = 09/21/16 Pct Recovery = 131% Analysis Date = 09/18/16 Pct Recovery = 132% Analysis Date = 09/18/16 Pct Recovery = 132% Analysis Date = 09/15/16 Pct Recovery = 132% Analysis Date = 09/15/16 Pct Recovery = 132% Analysis Date = 09/12/16 Pct Recovery = 133% Analysis Date = 09/12/16 Pct Recovery = 133% Analysis Date = 09/10/16 Pct Recovery = 133% Analysis Date = 09/10/16 Pct Recovery = 133% Analysis Date = 09/07/16 Pct Recovery = 133% Analysis Date = 09/07/16 Pct Recovery = 133% Analysis Date = 09/04/16 Pct Recovery = 133% Analysis Date = 09/04/16 Pct Recovery = 133% Analysis Date = 09/01/16 Pct Recovery = 132% Analysis Date = 09/01/16 Pct Recovery = 132% Analysis Date = 08/29/16 Pct Recovery = 132% Analysis Date = 08/29/16 Pct Recovery = 132% Analysis Date = 08/26/16 Pct Recovery = 132% Analysis Date = 08/26/16 Pct Recovery = 132% Analysis Date = 08/23/16 Pct Recovery = 132% Analysis Date = 08/23/16 Pct Recovery = 132% Analysis Date = 08/21/16 Pct Recovery = 132% Analysis Date = 08/21/16 Pct Recovery = 132% Analysis Date = 08/18/16 Pct Recovery = 132% Analysis Date = 08/18/16 Pct Recovery = 132% Analysis Date = 08/15/16 Pct Recovery = 131% Analysis Date = 08/15/16 Pct Recovery = 131% Analysis Date = 08/12/16 Pct Recovery = 131% Analysis Date = 08/12/16 Pct Recovery = 131% Analysis Date = 08/09/16 Pct Recovery = 131% Analysis Date = 08/09/16 Pct Recovery = 131% Analysis Date = 08/06/16 Pct Recovery = 130% Analysis Date = 08/06/16 Pct Recovery = 130% Analysis Date = 08/03/16 Pct Recovery = 130% Analysis Date = 08/03/16 Pct Recovery = 130% Analysis Date = 08/01/16 Pct Recovery = 130% Analysis Date = 08/01/16 Pct Recovery = 130% Analysis Date = 07/29/16 Pct Recovery = 129% Analysis Date = 07/29/16 Pct Recovery = 129% Analysis Date = 07/26/16 Pct Recovery = 129% Analysis Date = 07/26/16 Pct Recovery = 129% Analysis Date = 07/23/16 Pct Recovery = 129% Analysis Date = 07/23/16 Pct Recovery = 129% Analysis Date = 07/20/16 Pct Recovery = 129% Analysis Date = 07/20/16 Pct Recovery = 129% Analysis Date = 07/17/16 Pct Recovery = 128% Analysis Date = 07/17/16 Pct Recovery = 128% Analysis Date = 07/14/16 Pct Recovery = 128% Analysis Date = 07/14/16 Pct Recovery = 128% Analysis Date = 07/11/16 Pct Recovery = 128% Analysis Date = 07/11/16 Pct Recovery = 128% Analysis Date = 07/09/16 Pct Recovery = 127% Analysis Date = 07/09/16 Pct Recovery = 127% Analysis Date = 07/06/16 Pct Recovery = 127% Analysis Date = 07/06/16 Pct Recovery = 127% Analysis Date = 07/03/16 Pct Recovery = 127% Analysis Date = 07/03/16 Pct Recovery = 127% Analysis Date = 06/30/16 Pct Recovery = 126% Analysis Date = 06/30/16 Pct Recovery = 126% Analysis Date = 06/27/16 Pct Recovery = 126% Analysis Date = 06/27/16 Pct Recovery = 126% Analysis Date = 06/24/16 Pct Recovery = 126% Analysis Date = 06/24/16 Pct Recovery = 126% Analysis Date = 06/21/16 Pct Recovery = 125% Analysis Date = 06/21/16 Pct Recovery = 125% Analysis Date = 06/19/16 Pct Recovery = 125% Analysis Date = 06/19/16 Pct Recovery = 125% Analysis Date = 06/16/16 Pct Recovery = 125% Analysis Date = 06/16/16 Pct Recovery = 125% Analysis Date = 06/13/16 Pct Recovery = 124% Analysis Date = 06/13/16 Pct Recovery = 124% Analysis Date = 06/10/16 Pct Recovery = 124% Analysis Date = 06/10/16 Pct Recovery = 124% Analysis Date = 06/07/16 Pct Recovery = 124% Analysis Date = 06/07/16 Pct Recovery = 124% Analysis Date = 06/04/16 Pct Recovery = 123% Analysis Date = 06/04/16 Pct Recovery = 123% Analysis Date = 06/01/16 Pct Recovery = 123% Analysis Date = 06/01/16 Pct Recovery = 123% Analysis Date = 05/30/16 Pct Recovery = 123% Analysis Date = 05/30/16 Pct Recovery = 123% Analysis Date = 05/27/16 Pct Recovery = 123% Analysis Date = 05/27/16 Pct Recovery = 123% Analysis Date = 05/24/16 Pct Recovery = 122% Analysis Date = 05/24/16 Pct Recovery = 122% Analysis Date = 05/21/16 Pct Recovery = 122% Analysis Date = 05/21/16 Pct Recovery = 122% Analysis Date = 05/18/16 Pct Recovery = 122% Analysis Date = 05/18/16 Pct Recovery = 122% Analysis Date = 05/15/16 Pct Recovery = 121% Analysis Date = 05/15/16 Pct Recovery = 121% Analysis Date = 05/12/16 Pct Recovery = 121% Analysis Date = 05/12/16 Pct Recovery = 121% Analysis Date = 05/10/16 Pct Recovery = 121% Analysis Date = 05/10/16 Pct Recovery = 121% Analysis Date = 05/07/16 Pct Recovery = 120% Analysis Date = 05/07/16 Pct Recovery = 120% Analysis Date = 05/04/16 Pct Recovery = 120% Analysis Date = 05/04/16 Pct Recovery = 120% Analysis Date = 05/01/16 Pct Recovery = 120% Analysis Date = 05/01/16 Pct Recovery = 120% Analysis Date = 04/28/16 Pct Recovery = 119% Analysis Date = 04/28/16 Pct Recovery = 119% Analysis Date = 04/25/16 Pct Recovery = 119% Analysis Date = 04/25/16 Pct Recovery = 119% Analysis Date = 04/22/16 Pct Recovery = 119% Analysis Date = 04/22/16 Pct Recovery = 119% Analysis Date = 04/20/16 Pct Recovery = 118% Analysis Date = 04/20/16 Pct Recovery = 118% Analysis Date = 04/17/16 Pct Recovery = 118% Analysis Date = 04/17/16 Pct Recovery = 118% Analysis Date = 04/14/16 Pct Recovery = 118% Analysis Date = 04/14/16 Pct Recovery = 118% Analysis Date = 04/11/16 Pct Recovery = 117% Analysis Date = 04/11/16 Pct Recovery = 117% Analysis Date = 04/08/16 Pct Recovery = 117% Analysis Date = 04/08/16 Pct Recovery = 117% Analysis Date = 04/05/16 Pct Recovery = 117% Analysis Date = 04/05/16 Pct Recovery = 117% Analysis Date = 04/02/16 Pct Recovery = 116% Analysis Date = 04/02/16 Pct Recovery = 116% Analysis Date = 03/31/16 Pct Recovery = 116% Analysis Date = 03/31/16 Pct Recovery = 116% Analysis Date = 03/28/16 Pct Recovery = 116% Analysis Date = 03/28/16 Pct Recovery = 116% Analysis Date = 03/25/16 Pct Recovery = 115% Analysis Date = 03/25/16 Pct Recovery = 115% Analysis Date = 03/22/16 Pct Recovery = 115% Analysis Date = 03/22/16 Pct Recovery = 115% Analysis Date = 03/19/16 Pct Recovery = 115% Analysis Date = 03/19/16 Pct Recovery = 115% Analysis Date = 03/16/16 Pct Recovery = 115% Analysis Date = 03/16/16 Pct Recovery = 115% Analysis Date = 03/13/16 Pct Recovery = 114% Analysis Date = 03/13/16 Pct Recovery = 114% Analysis Date = 03/11/16 Pct Recovery = 114% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXAMYL OXIME

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 21 148% 97% 120% 24%
Total 21 148% 97% 120% 24%

Sample Statistics
OXAMYL OXIME

Characteristic N % % Basis
Plotted 21 28% Spiked
Estimated Values 1 1% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 53 70% Spiked
Spiked 78 .  
False Negatives 2 3% 2 out of 76
Not Spiked 41 .  
False Positives 1 2% 1 out of 41