OBSP Determination:
RALOXIFENE
METHOD: 2440 , TESTIDCODE: 67530LCM56

Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 242% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 249% Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 54% Analysis Date = 11/09/17 SpikeMix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Pct Recovery = 94% Analysis Date = 10/21/17 SpikeMix = ERA 06281702: 50 µl & ERA 06281703: 50 µl Pct Recovery = 33% Analysis Date = 09/21/17 SpikeMix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Pct Recovery = 37% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 37% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 29% Analysis Date = 11/09/17 SpikeMix = ERA 06281702: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 73% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 16% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 26% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 22% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 23% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 41% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 25% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 43% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 7% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 20% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 14% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 19% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 30% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 37% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 41% Analysis Date = 02/07/17 SpikeMix = Abs 061416: 100 µl & ERA 04281603: 100 µl Pct Recovery = 53% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 32% Analysis Date = 06/17/17 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 38% Analysis Date = 06/17/17 SpikeMix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 44% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 28% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 20% Analysis Date = 08/11/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 25% Analysis Date = 04/06/17 SpikeMix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Pct Recovery = 40% Analysis Date = 04/06/17 SpikeMix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Pct Recovery = 56% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 03/14/17 SpikeMix = Crescent EN160610015: 40 µl & ERA 04281604: 40 µl Pct Recovery = 32% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 40% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 38% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 11/09/17 Pct Recovery = 45% Analysis Date = 11/06/17 Pct Recovery = 45% Analysis Date = 11/06/17 Pct Recovery = 45% Analysis Date = 11/03/17 Pct Recovery = 45% Analysis Date = 11/03/17 Pct Recovery = 45% Analysis Date = 10/31/17 Pct Recovery = 45% Analysis Date = 10/31/17 Pct Recovery = 45% Analysis Date = 10/29/17 Pct Recovery = 45% Analysis Date = 10/29/17 Pct Recovery = 45% Analysis Date = 10/26/17 Pct Recovery = 45% Analysis Date = 10/26/17 Pct Recovery = 45% Analysis Date = 10/23/17 Pct Recovery = 45% Analysis Date = 10/23/17 Pct Recovery = 45% Analysis Date = 10/20/17 Pct Recovery = 45% Analysis Date = 10/20/17 Pct Recovery = 45% Analysis Date = 10/18/17 Pct Recovery = 45% Analysis Date = 10/18/17 Pct Recovery = 45% Analysis Date = 10/15/17 Pct Recovery = 45% Analysis Date = 10/15/17 Pct Recovery = 45% Analysis Date = 10/12/17 Pct Recovery = 44% Analysis Date = 10/12/17 Pct Recovery = 44% Analysis Date = 10/09/17 Pct Recovery = 44% Analysis Date = 10/09/17 Pct Recovery = 44% Analysis Date = 10/07/17 Pct Recovery = 44% Analysis Date = 10/07/17 Pct Recovery = 44% Analysis Date = 10/04/17 Pct Recovery = 44% Analysis Date = 10/04/17 Pct Recovery = 44% Analysis Date = 10/01/17 Pct Recovery = 44% Analysis Date = 10/01/17 Pct Recovery = 44% Analysis Date = 09/28/17 Pct Recovery = 44% Analysis Date = 09/28/17 Pct Recovery = 44% Analysis Date = 09/26/17 Pct Recovery = 44% Analysis Date = 09/26/17 Pct Recovery = 44% Analysis Date = 09/23/17 Pct Recovery = 44% Analysis Date = 09/23/17 Pct Recovery = 44% Analysis Date = 09/20/17 Pct Recovery = 44% Analysis Date = 09/20/17 Pct Recovery = 44% Analysis Date = 09/18/17 Pct Recovery = 44% Analysis Date = 09/18/17 Pct Recovery = 44% Analysis Date = 09/15/17 Pct Recovery = 43% Analysis Date = 09/15/17 Pct Recovery = 43% Analysis Date = 09/12/17 Pct Recovery = 43% Analysis Date = 09/12/17 Pct Recovery = 43% Analysis Date = 09/09/17 Pct Recovery = 43% Analysis Date = 09/09/17 Pct Recovery = 43% Analysis Date = 09/07/17 Pct Recovery = 43% Analysis Date = 09/07/17 Pct Recovery = 43% Analysis Date = 09/04/17 Pct Recovery = 43% Analysis Date = 09/04/17 Pct Recovery = 43% Analysis Date = 09/01/17 Pct Recovery = 43% Analysis Date = 09/01/17 Pct Recovery = 43% Analysis Date = 08/29/17 Pct Recovery = 43% Analysis Date = 08/29/17 Pct Recovery = 43% Analysis Date = 08/27/17 Pct Recovery = 43% Analysis Date = 08/27/17 Pct Recovery = 43% Analysis Date = 08/24/17 Pct Recovery = 43% Analysis Date = 08/24/17 Pct Recovery = 43% Analysis Date = 08/21/17 Pct Recovery = 43% Analysis Date = 08/21/17 Pct Recovery = 43% Analysis Date = 08/18/17 Pct Recovery = 43% Analysis Date = 08/18/17 Pct Recovery = 43% Analysis Date = 08/16/17 Pct Recovery = 42% Analysis Date = 08/16/17 Pct Recovery = 42% Analysis Date = 08/13/17 Pct Recovery = 42% Analysis Date = 08/13/17 Pct Recovery = 42% Analysis Date = 08/10/17 Pct Recovery = 42% Analysis Date = 08/10/17 Pct Recovery = 42% Analysis Date = 08/08/17 Pct Recovery = 42% Analysis Date = 08/08/17 Pct Recovery = 42% Analysis Date = 08/05/17 Pct Recovery = 42% Analysis Date = 08/05/17 Pct Recovery = 42% Analysis Date = 08/02/17 Pct Recovery = 42% Analysis Date = 08/02/17 Pct Recovery = 42% Analysis Date = 07/30/17 Pct Recovery = 42% Analysis Date = 07/30/17 Pct Recovery = 42% Analysis Date = 07/28/17 Pct Recovery = 42% Analysis Date = 07/28/17 Pct Recovery = 42% Analysis Date = 07/25/17 Pct Recovery = 42% Analysis Date = 07/25/17 Pct Recovery = 42% Analysis Date = 07/22/17 Pct Recovery = 42% Analysis Date = 07/22/17 Pct Recovery = 42% Analysis Date = 07/19/17 Pct Recovery = 42% Analysis Date = 07/19/17 Pct Recovery = 42% Analysis Date = 07/17/17 Pct Recovery = 42% Analysis Date = 07/17/17 Pct Recovery = 42% Analysis Date = 07/14/17 Pct Recovery = 41% Analysis Date = 07/14/17 Pct Recovery = 41% Analysis Date = 07/11/17 Pct Recovery = 41% Analysis Date = 07/11/17 Pct Recovery = 41% Analysis Date = 07/08/17 Pct Recovery = 41% Analysis Date = 07/08/17 Pct Recovery = 41% Analysis Date = 07/06/17 Pct Recovery = 41% Analysis Date = 07/06/17 Pct Recovery = 41% Analysis Date = 07/03/17 Pct Recovery = 41% Analysis Date = 07/03/17 Pct Recovery = 41% Analysis Date = 06/30/17 Pct Recovery = 41% Analysis Date = 06/30/17 Pct Recovery = 41% Analysis Date = 06/27/17 Pct Recovery = 41% Analysis Date = 06/27/17 Pct Recovery = 41% Analysis Date = 06/25/17 Pct Recovery = 41% Analysis Date = 06/25/17 Pct Recovery = 41% Analysis Date = 06/22/17 Pct Recovery = 41% Analysis Date = 06/22/17 Pct Recovery = 41% Analysis Date = 06/19/17 Pct Recovery = 41% Analysis Date = 06/19/17 Pct Recovery = 41% Analysis Date = 06/17/17 Pct Recovery = 41% Analysis Date = 06/17/17 Pct Recovery = 41% Analysis Date = 06/14/17 Pct Recovery = 41% Analysis Date = 06/14/17 Pct Recovery = 41% Analysis Date = 06/11/17 Pct Recovery = 41% Analysis Date = 06/11/17 Pct Recovery = 41% Analysis Date = 06/08/17 Pct Recovery = 41% Analysis Date = 06/08/17 Pct Recovery = 41% Analysis Date = 06/06/17 Pct Recovery = 41% Analysis Date = 06/06/17 Pct Recovery = 41% Analysis Date = 06/03/17 Pct Recovery = 41% Analysis Date = 06/03/17 Pct Recovery = 41% Analysis Date = 05/31/17 Pct Recovery = 41% Analysis Date = 05/31/17 Pct Recovery = 41% Analysis Date = 05/28/17 Pct Recovery = 41% Analysis Date = 05/28/17 Pct Recovery = 41% Analysis Date = 05/26/17 Pct Recovery = 41% Analysis Date = 05/26/17 Pct Recovery = 41% Analysis Date = 05/23/17 Pct Recovery = 42% Analysis Date = 05/23/17 Pct Recovery = 42% Analysis Date = 05/20/17 Pct Recovery = 42% Analysis Date = 05/20/17 Pct Recovery = 42% Analysis Date = 05/17/17 Pct Recovery = 42% Analysis Date = 05/17/17 Pct Recovery = 42% Analysis Date = 05/15/17 Pct Recovery = 42% Analysis Date = 05/15/17 Pct Recovery = 42% Analysis Date = 05/12/17 Pct Recovery = 42% Analysis Date = 05/12/17 Pct Recovery = 42% Analysis Date = 05/09/17 Pct Recovery = 42% Analysis Date = 05/09/17 Pct Recovery = 42% Analysis Date = 05/07/17 Pct Recovery = 42% Analysis Date = 05/07/17 Pct Recovery = 42% Analysis Date = 05/04/17 Pct Recovery = 42% Analysis Date = 05/04/17 Pct Recovery = 42% Analysis Date = 05/01/17 Pct Recovery = 42% Analysis Date = 05/01/17 Pct Recovery = 42% Analysis Date = 04/28/17 Pct Recovery = 42% Analysis Date = 04/28/17 Pct Recovery = 42% Analysis Date = 04/26/17 Pct Recovery = 43% Analysis Date = 04/26/17 Pct Recovery = 43% Analysis Date = 04/23/17 Pct Recovery = 43% Analysis Date = 04/23/17 Pct Recovery = 43% Analysis Date = 04/20/17 Pct Recovery = 43% Analysis Date = 04/20/17 Pct Recovery = 43% Analysis Date = 04/17/17 Pct Recovery = 43% Analysis Date = 04/17/17 Pct Recovery = 43% Analysis Date = 04/15/17 Pct Recovery = 43% Analysis Date = 04/15/17 Pct Recovery = 43% Analysis Date = 04/12/17 Pct Recovery = 43% Analysis Date = 04/12/17 Pct Recovery = 43% Analysis Date = 04/09/17 Pct Recovery = 43% Analysis Date = 04/09/17 Pct Recovery = 43% Analysis Date = 04/06/17 Pct Recovery = 43% Analysis Date = 04/06/17 Pct Recovery = 43% Analysis Date = 04/04/17 Pct Recovery = 43% Analysis Date = 04/04/17 Pct Recovery = 43% Analysis Date = 04/01/17 Pct Recovery = 43% Analysis Date = 04/01/17 Pct Recovery = 43% Analysis Date = 03/29/17 Pct Recovery = 43% Analysis Date = 03/29/17 Pct Recovery = 43% Analysis Date = 03/26/17 Pct Recovery = 44% Analysis Date = 03/26/17 Pct Recovery = 44% Analysis Date = 03/24/17 Pct Recovery = 44% Analysis Date = 03/24/17 Pct Recovery = 44% Analysis Date = 03/21/17 Pct Recovery = 44% Analysis Date = 03/21/17 Pct Recovery = 44% Analysis Date = 03/18/17 Pct Recovery = 44% Analysis Date = 03/18/17 Pct Recovery = 44% Analysis Date = 03/16/17 Pct Recovery = 44% Analysis Date = 03/16/17 Pct Recovery = 44% Analysis Date = 03/13/17 Pct Recovery = 44% Analysis Date = 03/13/17 Pct Recovery = 44% Analysis Date = 03/10/17 Pct Recovery = 44% Analysis Date = 03/10/17 Pct Recovery = 44% Analysis Date = 03/07/17 Pct Recovery = 44% Analysis Date = 03/07/17 Pct Recovery = 44% Analysis Date = 03/05/17 Pct Recovery = 44% Analysis Date = 03/05/17 Pct Recovery = 44% Analysis Date = 03/02/17 Pct Recovery = 44% Analysis Date = 03/02/17 Pct Recovery = 44% Analysis Date = 02/27/17 Pct Recovery = 45% Analysis Date = 02/27/17 Pct Recovery = 45% Analysis Date = 02/24/17 Pct Recovery = 45% Analysis Date = 02/24/17 Pct Recovery = 45% Analysis Date = 02/22/17 Pct Recovery = 45% Analysis Date = 02/22/17 Pct Recovery = 45% Analysis Date = 02/19/17 Pct Recovery = 45% Analysis Date = 02/19/17 Pct Recovery = 45% Analysis Date = 02/16/17 Pct Recovery = 45% Analysis Date = 02/16/17 Pct Recovery = 45% Analysis Date = 02/13/17 Pct Recovery = 45% Analysis Date = 02/13/17 Pct Recovery = 45% Analysis Date = 02/11/17 Pct Recovery = 45% Analysis Date = 02/11/17 Pct Recovery = 45% Analysis Date = 02/08/17 Pct Recovery = 45% Analysis Date = 02/08/17 Pct Recovery = 45% Analysis Date = 02/05/17 Pct Recovery = 45% Analysis Date = 02/05/17 Pct Recovery = 45% Analysis Date = 02/03/17 Pct Recovery = 45% Analysis Date = 02/03/17 Pct Recovery = 45% Analysis Date = 01/31/17 Pct Recovery = 45% Analysis Date = 01/31/17 Pct Recovery = 45% Analysis Date = 01/28/17 Pct Recovery = 45% Analysis Date = 01/28/17 Pct Recovery = 45% Analysis Date = 01/25/17 Pct Recovery = 45% Analysis Date = 01/25/17 Pct Recovery = 45% Analysis Date = 01/23/17 Pct Recovery = 45% Analysis Date = 01/23/17 Pct Recovery = 45% Analysis Date = 01/20/17 Pct Recovery = 45% Analysis Date = 01/20/17 Pct Recovery = 45% Analysis Date = 01/17/17 Pct Recovery = 45% Analysis Date = 01/17/17 Pct Recovery = 45% Analysis Date = 01/14/17 Pct Recovery = 45% Analysis Date = 01/14/17 Pct Recovery = 45% Analysis Date = 01/12/17 Pct Recovery = 44% Analysis Date = 01/12/17 Pct Recovery = 44% Analysis Date = 01/09/17 Pct Recovery = 44% Analysis Date = 01/09/17 Pct Recovery = 44% Analysis Date = 01/06/17 Pct Recovery = 44% Analysis Date = 01/06/17 Pct Recovery = 44% Analysis Date = 01/03/17 Pct Recovery = 44% Analysis Date = 01/03/17 Pct Recovery = 44% Analysis Date = 01/01/17 Pct Recovery = 44% Analysis Date = 01/01/17 Pct Recovery = 44% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/26/16 Pct Recovery = 44% Analysis Date = 12/26/16 Pct Recovery = 44% Analysis Date = 12/24/16 Pct Recovery = 44% Analysis Date = 12/24/16 Pct Recovery = 44% Analysis Date = 12/21/16 Pct Recovery = 44% Analysis Date = 12/21/16 Pct Recovery = 44% Analysis Date = 12/18/16 Pct Recovery = 44% Analysis Date = 12/18/16 Pct Recovery = 44% Analysis Date = 12/15/16 Pct Recovery = 44% Analysis Date = 12/15/16 Pct Recovery = 44% Analysis Date = 12/13/16 Pct Recovery = 43% Analysis Date = 12/13/16 Pct Recovery = 43% Analysis Date = 12/10/16 Pct Recovery = 43% Analysis Date = 12/10/16 Pct Recovery = 43% Analysis Date = 12/07/16 Pct Recovery = 43% Analysis Date = 12/07/16 Pct Recovery = 43% Analysis Date = 12/04/16 Pct Recovery = 43% Analysis Date = 12/04/16 Pct Recovery = 43% Analysis Date = 12/02/16 Pct Recovery = 43% Analysis Date = 12/02/16 Pct Recovery = 43% Analysis Date = 11/29/16 Pct Recovery = 43% Analysis Date = 11/29/16 Pct Recovery = 43% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/23/16 Pct Recovery = 42% Analysis Date = 11/23/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/21/16 Pct Recovery = 42% Analysis Date = 11/18/16 Pct Recovery = 42% Analysis Date = 11/18/16 Pct Recovery = 42% Analysis Date = 11/15/16 Pct Recovery = 42% Analysis Date = 11/15/16 Pct Recovery = 42% Analysis Date = 11/12/16 Pct Recovery = 41% Analysis Date = 11/12/16 Pct Recovery = 41% Analysis Date = 11/10/16 Pct Recovery = 41% Analysis Date = 11/10/16 Pct Recovery = 41% Analysis Date = 11/07/16 Pct Recovery = 41% Analysis Date = 11/07/16 Pct Recovery = 41% Analysis Date = 11/04/16 Pct Recovery = 41% Analysis Date = 11/04/16 Pct Recovery = 41% Analysis Date = 11/02/16 Pct Recovery = 41% Analysis Date = 11/02/16 Pct Recovery = 41% Analysis Date = 10/30/16 Pct Recovery = 42% Analysis Date = 10/30/16 Pct Recovery = 42% Analysis Date = 10/27/16 Pct Recovery = 43% Analysis Date = 10/27/16 Pct Recovery = 43% Analysis Date = 10/24/16 Pct Recovery = 44% Analysis Date = 10/24/16 Pct Recovery = 44% Analysis Date = 10/22/16 Pct Recovery = 45% Analysis Date = 10/22/16 Pct Recovery = 45% Analysis Date = 10/19/16 Pct Recovery = 46% Analysis Date = 10/19/16 Pct Recovery = 46% Analysis Date = 10/16/16 Pct Recovery = 47% Analysis Date = 10/16/16 Pct Recovery = 47% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/13/16 Pct Recovery = 48% Analysis Date = 10/11/16 Pct Recovery = 49% Analysis Date = 10/11/16 Pct Recovery = 49% Analysis Date = 10/08/16 Pct Recovery = 50% Analysis Date = 10/08/16 Pct Recovery = 50% Analysis Date = 10/05/16 Pct Recovery = 51% Analysis Date = 10/05/16 Pct Recovery = 51% Analysis Date = 10/02/16 Pct Recovery = 52% Analysis Date = 10/02/16 Pct Recovery = 52% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/30/16 Pct Recovery = 53% Analysis Date = 09/27/16 Pct Recovery = 54% Analysis Date = 09/27/16 Pct Recovery = 54% Analysis Date = 09/24/16 Pct Recovery = 55% Analysis Date = 09/24/16 Pct Recovery = 55% Analysis Date = 09/22/16 Pct Recovery = 56% Analysis Date = 09/22/16 Pct Recovery = 56% Analysis Date = 09/19/16 Pct Recovery = 56% Analysis Date = 09/19/16 Pct Recovery = 56% Analysis Date = 09/16/16 Pct Recovery = 57% Analysis Date = 09/16/16 Pct Recovery = 57% Analysis Date = 09/13/16 Pct Recovery = 57% Analysis Date = 09/13/16 Pct Recovery = 57% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/08/16 Pct Recovery = 57% Analysis Date = 09/08/16 Pct Recovery = 57% Analysis Date = 09/05/16 Pct Recovery = 57% Analysis Date = 09/05/16 Pct Recovery = 57% Analysis Date = 09/02/16 Pct Recovery = 58% Analysis Date = 09/02/16 Pct Recovery = 58% Analysis Date = 08/31/16 Pct Recovery = 58% Analysis Date = 08/31/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/22/16 Pct Recovery = 58% Analysis Date = 08/22/16 Pct Recovery = 58% Analysis Date = 08/20/16 Pct Recovery = 58% Analysis Date = 08/20/16 Pct Recovery = 58% Analysis Date = 08/17/16 Pct Recovery = 58% Analysis Date = 08/17/16 Pct Recovery = 58% Analysis Date = 08/14/16 Pct Recovery = 58% Analysis Date = 08/14/16 Pct Recovery = 58% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/11/16 Pct Recovery = 59% Analysis Date = 08/09/16 Pct Recovery = 59% Analysis Date = 08/09/16 Pct Recovery = 59% Analysis Date = 08/06/16 Pct Recovery = 59% Analysis Date = 08/06/16 Pct Recovery = 59% Analysis Date = 08/03/16 Pct Recovery = 59% Analysis Date = 08/03/16 Pct Recovery = 59% Analysis Date = 08/01/16 Pct Recovery = 59% Analysis Date = 08/01/16 Pct Recovery = 59% Analysis Date = 07/29/16 Pct Recovery = 59% Analysis Date = 07/29/16 Pct Recovery = 59% Analysis Date = 07/26/16 Pct Recovery = 59% Analysis Date = 07/26/16 Pct Recovery = 59% Analysis Date = 07/23/16 Pct Recovery = 59% Analysis Date = 07/23/16 Pct Recovery = 59% Analysis Date = 07/21/16 Pct Recovery = 60% Analysis Date = 07/21/16 Pct Recovery = 60% Analysis Date = 07/18/16 Pct Recovery = 60% Analysis Date = 07/18/16 Pct Recovery = 60% Analysis Date = 07/15/16 Pct Recovery = 60% Analysis Date = 07/15/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/12/16 Pct Recovery = 60% Analysis Date = 07/10/16 Pct Recovery = 60% Analysis Date = 07/10/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/07/16 Pct Recovery = 60% Analysis Date = 07/04/16 Pct Recovery = 60% Analysis Date = 07/04/16 Pct Recovery = 60% Analysis Date = 07/01/16 Pct Recovery = 60% Analysis Date = 07/01/16 Pct Recovery = 60% Analysis Date = 06/29/16 Pct Recovery = 60% Analysis Date = 06/29/16 Pct Recovery = 60% Analysis Date = 06/26/16 Pct Recovery = 60% Analysis Date = 06/26/16 Pct Recovery = 60% Analysis Date = 06/23/16 Pct Recovery = 60% Analysis Date = 06/23/16 Pct Recovery = 60% Analysis Date = 06/21/16 Pct Recovery = 60% Analysis Date = 06/21/16 Pct Recovery = 60% Analysis Date = 06/18/16 Pct Recovery = 60% Analysis Date = 06/18/16 Pct Recovery = 60% Analysis Date = 06/15/16 Pct Recovery = 61% Analysis Date = 06/15/16 Pct Recovery = 61% Analysis Date = 06/12/16 Pct Recovery = 61% Analysis Date = 06/12/16 Pct Recovery = 61% Analysis Date = 06/10/16 Pct Recovery = 61% Analysis Date = 06/10/16 Pct Recovery = 61% Analysis Date = 06/07/16 Pct Recovery = 61% Analysis Date = 06/07/16 Pct Recovery = 61% Analysis Date = 06/04/16 Pct Recovery = 61% Analysis Date = 06/04/16 Pct Recovery = 61% Analysis Date = 06/01/16 Pct Recovery = 61% Analysis Date = 06/01/16 Pct Recovery = 61% Analysis Date = 05/30/16 Pct Recovery = 61% Analysis Date = 05/30/16 Pct Recovery = 61% Analysis Date = 05/27/16 Pct Recovery = 61% Analysis Date = 05/27/16 Pct Recovery = 61% Analysis Date = 05/24/16 Pct Recovery = 61% Analysis Date = 05/24/16 Pct Recovery = 61% Analysis Date = 05/21/16 Pct Recovery = 61% Analysis Date = 05/21/16 Pct Recovery = 61% Analysis Date = 05/19/16 Pct Recovery = 61% Analysis Date = 05/19/16 Pct Recovery = 61% Analysis Date = 05/16/16 Pct Recovery = 61% Analysis Date = 05/16/16 Pct Recovery = 61% Analysis Date = 05/13/16 Pct Recovery = 61% Analysis Date = 05/13/16 Pct Recovery = 61% Analysis Date = 05/11/16 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
RALOXIFENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 21 43% 13% 40% 14%
>= Reporting Level 23 53% 64% 33% 15%
Total 44 48% 47% 38% 19%

Sample Statistics
RALOXIFENE

Characteristic N % % Basis
Plotted 44 81% Spiked
Estimated Values 44 81% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 9 17% Spiked
Spiked 54 .  
False Negatives 1 2% 1 out of 54
Not Spiked 32 .  
False Positives 0 0% 0 out of 32