OBSP Determination:
TIOTROPIUM
METHOD: 2440 , TESTIDCODE: 67508LCM56

Analysis Date = 09/09/17 SpikeMix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Pct Recovery = 208% Analysis Date = 09/21/17 SpikeMix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Pct Recovery = 103% Analysis Date = 08/28/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 072517Pharm2: 50 µl Pct Recovery = 111% Analysis Date = 08/26/17 SpikeMix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Pct Recovery = 43% Analysis Date = 11/08/17 SpikeMix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Pct Recovery = 32% Analysis Date = 09/23/17 SpikeMix = Abs 072517Pharm1: 20 µl & Abs 072517Pharm2: 20 µl Pct Recovery = 34% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 15% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 17% Analysis Date = 07/15/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 7% Analysis Date = 06/17/17 SpikeMix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 39% Analysis Date = 06/08/17 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 30% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 18% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 7% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 3% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 4% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 50% Analysis Date = 02/07/17 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 45% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 08/11/17 SpikeMix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Pct Recovery = 57% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 31% Analysis Date = 11/07/17 Pct Recovery = 87% Analysis Date = 11/05/17 Pct Recovery = 86% Analysis Date = 11/05/17 Pct Recovery = 86% Analysis Date = 11/02/17 Pct Recovery = 85% Analysis Date = 11/02/17 Pct Recovery = 85% Analysis Date = 10/30/17 Pct Recovery = 85% Analysis Date = 10/30/17 Pct Recovery = 85% Analysis Date = 10/27/17 Pct Recovery = 84% Analysis Date = 10/27/17 Pct Recovery = 84% Analysis Date = 10/24/17 Pct Recovery = 83% Analysis Date = 10/24/17 Pct Recovery = 83% Analysis Date = 10/21/17 Pct Recovery = 83% Analysis Date = 10/21/17 Pct Recovery = 83% Analysis Date = 10/18/17 Pct Recovery = 82% Analysis Date = 10/18/17 Pct Recovery = 82% Analysis Date = 10/15/17 Pct Recovery = 81% Analysis Date = 10/15/17 Pct Recovery = 81% Analysis Date = 10/12/17 Pct Recovery = 81% Analysis Date = 10/12/17 Pct Recovery = 81% Analysis Date = 10/10/17 Pct Recovery = 80% Analysis Date = 10/10/17 Pct Recovery = 80% Analysis Date = 10/07/17 Pct Recovery = 79% Analysis Date = 10/07/17 Pct Recovery = 79% Analysis Date = 10/04/17 Pct Recovery = 79% Analysis Date = 10/04/17 Pct Recovery = 79% Analysis Date = 10/01/17 Pct Recovery = 78% Analysis Date = 10/01/17 Pct Recovery = 78% Analysis Date = 09/28/17 Pct Recovery = 77% Analysis Date = 09/28/17 Pct Recovery = 77% Analysis Date = 09/25/17 Pct Recovery = 77% Analysis Date = 09/25/17 Pct Recovery = 77% Analysis Date = 09/22/17 Pct Recovery = 76% Analysis Date = 09/22/17 Pct Recovery = 76% Analysis Date = 09/19/17 Pct Recovery = 75% Analysis Date = 09/19/17 Pct Recovery = 75% Analysis Date = 09/16/17 Pct Recovery = 75% Analysis Date = 09/16/17 Pct Recovery = 75% Analysis Date = 09/14/17 Pct Recovery = 74% Analysis Date = 09/14/17 Pct Recovery = 74% Analysis Date = 09/11/17 Pct Recovery = 73% Analysis Date = 09/11/17 Pct Recovery = 73% Analysis Date = 09/08/17 Pct Recovery = 73% Analysis Date = 09/08/17 Pct Recovery = 73% Analysis Date = 09/05/17 Pct Recovery = 72% Analysis Date = 09/05/17 Pct Recovery = 72% Analysis Date = 09/02/17 Pct Recovery = 71% Analysis Date = 09/02/17 Pct Recovery = 71% Analysis Date = 08/30/17 Pct Recovery = 71% Analysis Date = 08/30/17 Pct Recovery = 71% Analysis Date = 08/27/17 Pct Recovery = 70% Analysis Date = 08/27/17 Pct Recovery = 70% Analysis Date = 08/24/17 Pct Recovery = 70% Analysis Date = 08/24/17 Pct Recovery = 70% Analysis Date = 08/21/17 Pct Recovery = 69% Analysis Date = 08/21/17 Pct Recovery = 69% Analysis Date = 08/19/17 Pct Recovery = 68% Analysis Date = 08/19/17 Pct Recovery = 68% Analysis Date = 08/16/17 Pct Recovery = 68% Analysis Date = 08/16/17 Pct Recovery = 68% Analysis Date = 08/13/17 Pct Recovery = 67% Analysis Date = 08/13/17 Pct Recovery = 67% Analysis Date = 08/10/17 Pct Recovery = 67% Analysis Date = 08/10/17 Pct Recovery = 67% Analysis Date = 08/07/17 Pct Recovery = 66% Analysis Date = 08/07/17 Pct Recovery = 66% Analysis Date = 08/04/17 Pct Recovery = 65% Analysis Date = 08/04/17 Pct Recovery = 65% Analysis Date = 08/01/17 Pct Recovery = 65% Analysis Date = 08/01/17 Pct Recovery = 65% Analysis Date = 07/29/17 Pct Recovery = 64% Analysis Date = 07/29/17 Pct Recovery = 64% Analysis Date = 07/26/17 Pct Recovery = 64% Analysis Date = 07/26/17 Pct Recovery = 64% Analysis Date = 07/24/17 Pct Recovery = 63% Analysis Date = 07/24/17 Pct Recovery = 63% Analysis Date = 07/21/17 Pct Recovery = 63% Analysis Date = 07/21/17 Pct Recovery = 63% Analysis Date = 07/18/17 Pct Recovery = 62% Analysis Date = 07/18/17 Pct Recovery = 62% Analysis Date = 07/15/17 Pct Recovery = 61% Analysis Date = 07/15/17 Pct Recovery = 61% Analysis Date = 07/12/17 Pct Recovery = 61% Analysis Date = 07/12/17 Pct Recovery = 61% Analysis Date = 07/09/17 Pct Recovery = 60% Analysis Date = 07/09/17 Pct Recovery = 60% Analysis Date = 07/06/17 Pct Recovery = 60% Analysis Date = 07/06/17 Pct Recovery = 60% Analysis Date = 07/03/17 Pct Recovery = 59% Analysis Date = 07/03/17 Pct Recovery = 59% Analysis Date = 06/30/17 Pct Recovery = 59% Analysis Date = 06/30/17 Pct Recovery = 59% Analysis Date = 06/28/17 Pct Recovery = 58% Analysis Date = 06/28/17 Pct Recovery = 58% Analysis Date = 06/25/17 Pct Recovery = 58% Analysis Date = 06/25/17 Pct Recovery = 58% Analysis Date = 06/22/17 Pct Recovery = 57% Analysis Date = 06/22/17 Pct Recovery = 57% Analysis Date = 06/19/17 Pct Recovery = 57% Analysis Date = 06/19/17 Pct Recovery = 57% Analysis Date = 06/16/17 Pct Recovery = 56% Analysis Date = 06/16/17 Pct Recovery = 56% Analysis Date = 06/13/17 Pct Recovery = 56% Analysis Date = 06/13/17 Pct Recovery = 56% Analysis Date = 06/10/17 Pct Recovery = 55% Analysis Date = 06/10/17 Pct Recovery = 55% Analysis Date = 06/07/17 Pct Recovery = 54% Analysis Date = 06/07/17 Pct Recovery = 54% Analysis Date = 06/04/17 Pct Recovery = 54% Analysis Date = 06/04/17 Pct Recovery = 54% Analysis Date = 06/02/17 Pct Recovery = 53% Analysis Date = 06/02/17 Pct Recovery = 53% Analysis Date = 05/30/17 Pct Recovery = 53% Analysis Date = 05/30/17 Pct Recovery = 53% Analysis Date = 05/27/17 Pct Recovery = 52% Analysis Date = 05/27/17 Pct Recovery = 52% Analysis Date = 05/24/17 Pct Recovery = 52% Analysis Date = 05/24/17 Pct Recovery = 52% Analysis Date = 05/21/17 Pct Recovery = 51% Analysis Date = 05/21/17 Pct Recovery = 51% Analysis Date = 05/18/17 Pct Recovery = 51% Analysis Date = 05/18/17 Pct Recovery = 51% Analysis Date = 05/15/17 Pct Recovery = 50% Analysis Date = 05/15/17 Pct Recovery = 50% Analysis Date = 05/12/17 Pct Recovery = 50% Analysis Date = 05/12/17 Pct Recovery = 50% Analysis Date = 05/09/17 Pct Recovery = 49% Analysis Date = 05/09/17 Pct Recovery = 49% Analysis Date = 05/07/17 Pct Recovery = 49% Analysis Date = 05/07/17 Pct Recovery = 49% Analysis Date = 05/04/17 Pct Recovery = 48% Analysis Date = 05/04/17 Pct Recovery = 48% Analysis Date = 05/01/17 Pct Recovery = 48% Analysis Date = 05/01/17 Pct Recovery = 48% Analysis Date = 04/28/17 Pct Recovery = 47% Analysis Date = 04/28/17 Pct Recovery = 47% Analysis Date = 04/25/17 Pct Recovery = 47% Analysis Date = 04/25/17 Pct Recovery = 47% Analysis Date = 04/22/17 Pct Recovery = 46% Analysis Date = 04/22/17 Pct Recovery = 46% Analysis Date = 04/19/17 Pct Recovery = 46% Analysis Date = 04/19/17 Pct Recovery = 46% Analysis Date = 04/16/17 Pct Recovery = 45% Analysis Date = 04/16/17 Pct Recovery = 45% Analysis Date = 04/13/17 Pct Recovery = 44% Analysis Date = 04/13/17 Pct Recovery = 44% Analysis Date = 04/11/17 Pct Recovery = 44% Analysis Date = 04/11/17 Pct Recovery = 44% Analysis Date = 04/08/17 Pct Recovery = 43% Analysis Date = 04/08/17 Pct Recovery = 43% Analysis Date = 04/05/17 Pct Recovery = 43% Analysis Date = 04/05/17 Pct Recovery = 43% Analysis Date = 04/02/17 Pct Recovery = 42% Analysis Date = 04/02/17 Pct Recovery = 42% Analysis Date = 03/30/17 Pct Recovery = 42% Analysis Date = 03/30/17 Pct Recovery = 42% Analysis Date = 03/27/17 Pct Recovery = 41% Analysis Date = 03/27/17 Pct Recovery = 41% Analysis Date = 03/24/17 Pct Recovery = 41% Analysis Date = 03/24/17 Pct Recovery = 41% Analysis Date = 03/21/17 Pct Recovery = 40% Analysis Date = 03/21/17 Pct Recovery = 40% Analysis Date = 03/18/17 Pct Recovery = 40% Analysis Date = 03/18/17 Pct Recovery = 40% Analysis Date = 03/16/17 Pct Recovery = 39% Analysis Date = 03/16/17 Pct Recovery = 39% Analysis Date = 03/13/17 Pct Recovery = 39% Analysis Date = 03/13/17 Pct Recovery = 39% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/07/17 Pct Recovery = 38% Analysis Date = 03/07/17 Pct Recovery = 38% Analysis Date = 03/04/17 Pct Recovery = 37% Analysis Date = 03/04/17 Pct Recovery = 37% Analysis Date = 03/01/17 Pct Recovery = 37% Analysis Date = 03/01/17 Pct Recovery = 37% Analysis Date = 02/26/17 Pct Recovery = 36% Analysis Date = 02/26/17 Pct Recovery = 36% Analysis Date = 02/23/17 Pct Recovery = 35% Analysis Date = 02/23/17 Pct Recovery = 35% Analysis Date = 02/20/17 Pct Recovery = 35% Analysis Date = 02/20/17 Pct Recovery = 35% Analysis Date = 02/18/17 Pct Recovery = 34% Analysis Date = 02/18/17 Pct Recovery = 34% Analysis Date = 02/15/17 Pct Recovery = 34% Analysis Date = 02/15/17 Pct Recovery = 34% Analysis Date = 02/12/17 Pct Recovery = 33% Analysis Date = 02/12/17 Pct Recovery = 33% Analysis Date = 02/09/17 Pct Recovery = 33% Analysis Date = 02/09/17 Pct Recovery = 33% Analysis Date = 02/06/17 Pct Recovery = 32% Analysis Date = 02/06/17 Pct Recovery = 32% Analysis Date = 02/03/17 Pct Recovery = 32% Analysis Date = 02/03/17 Pct Recovery = 32% Analysis Date = 01/31/17 Pct Recovery = 33% Analysis Date = 01/31/17 Pct Recovery = 33% Analysis Date = 01/28/17 Pct Recovery = 33% Analysis Date = 01/28/17 Pct Recovery = 33% Analysis Date = 01/25/17 Pct Recovery = 33% Analysis Date = 01/25/17 Pct Recovery = 33% Analysis Date = 01/22/17 Pct Recovery = 33% Analysis Date = 01/22/17 Pct Recovery = 33% Analysis Date = 01/20/17 Pct Recovery = 33% Analysis Date = 01/20/17 Pct Recovery = 33% Analysis Date = 01/17/17 Pct Recovery = 33% Analysis Date = 01/17/17 Pct Recovery = 33% Analysis Date = 01/14/17 Pct Recovery = 32% Analysis Date = 01/14/17 Pct Recovery = 32% Analysis Date = 01/11/17 Pct Recovery = 32% Analysis Date = 01/11/17 Pct Recovery = 32% Analysis Date = 01/08/17 Pct Recovery = 32% Analysis Date = 01/08/17 Pct Recovery = 32% Analysis Date = 01/05/17 Pct Recovery = 32% Analysis Date = 01/05/17 Pct Recovery = 32% Analysis Date = 01/02/17 Pct Recovery = 32% Analysis Date = 01/02/17 Pct Recovery = 32% Analysis Date = 12/30/16 Pct Recovery = 32% Analysis Date = 12/30/16 Pct Recovery = 32% Analysis Date = 12/27/16 Pct Recovery = 31% Analysis Date = 12/27/16 Pct Recovery = 31% Analysis Date = 12/25/16 Pct Recovery = 31% Analysis Date = 12/25/16 Pct Recovery = 31% Analysis Date = 12/22/16 Pct Recovery = 31% Analysis Date = 12/22/16 Pct Recovery = 31% Analysis Date = 12/19/16 Pct Recovery = 31% Analysis Date = 12/19/16 Pct Recovery = 31% Analysis Date = 12/16/16 Pct Recovery = 31% Analysis Date = 12/16/16 Pct Recovery = 31% Analysis Date = 12/13/16 Pct Recovery = 31% Analysis Date = 12/13/16 Pct Recovery = 31% Analysis Date = 12/10/16 Pct Recovery = 30% Analysis Date = 12/10/16 Pct Recovery = 30% Analysis Date = 12/07/16 Pct Recovery = 30% Analysis Date = 12/07/16 Pct Recovery = 30% Analysis Date = 12/04/16 Pct Recovery = 30% Analysis Date = 12/04/16 Pct Recovery = 30% Analysis Date = 12/01/16 Pct Recovery = 30% Analysis Date = 12/01/16 Pct Recovery = 30% Analysis Date = 11/29/16 Pct Recovery = 30% Analysis Date = 11/29/16 Pct Recovery = 30% Analysis Date = 11/26/16 Pct Recovery = 29% Analysis Date = 11/26/16 Pct Recovery = 29% Analysis Date = 11/23/16 Pct Recovery = 29% Analysis Date = 11/23/16 Pct Recovery = 29% Analysis Date = 11/20/16 Pct Recovery = 29% Analysis Date = 11/20/16 Pct Recovery = 29% Analysis Date = 11/17/16 Pct Recovery = 29% Analysis Date = 11/17/16 Pct Recovery = 29% Analysis Date = 11/14/16 Pct Recovery = 29% Analysis Date = 11/14/16 Pct Recovery = 29% Analysis Date = 11/11/16 Pct Recovery = 29% Analysis Date = 11/11/16 Pct Recovery = 29% Analysis Date = 11/08/16 Pct Recovery = 28% Analysis Date = 11/08/16 Pct Recovery = 28% Analysis Date = 11/05/16 Pct Recovery = 28% Analysis Date = 11/05/16 Pct Recovery = 28% Analysis Date = 11/03/16 Pct Recovery = 28% Analysis Date = 11/03/16 Pct Recovery = 28% Analysis Date = 10/31/16 Pct Recovery = 28% Analysis Date = 10/31/16 Pct Recovery = 28% Analysis Date = 10/28/16 Pct Recovery = 28% Analysis Date = 10/28/16 Pct Recovery = 28% Analysis Date = 10/25/16 Pct Recovery = 28% Analysis Date = 10/25/16 Pct Recovery = 28% Analysis Date = 10/22/16 Pct Recovery = 27% Analysis Date = 10/22/16 Pct Recovery = 27% Analysis Date = 10/19/16 Pct Recovery = 27% Analysis Date = 10/19/16 Pct Recovery = 27% Analysis Date = 10/16/16 Pct Recovery = 27% Analysis Date = 10/16/16 Pct Recovery = 27% Analysis Date = 10/13/16 Pct Recovery = 27% Analysis Date = 10/13/16 Pct Recovery = 27% Analysis Date = 10/10/16 Pct Recovery = 27% Analysis Date = 10/10/16 Pct Recovery = 27% Analysis Date = 10/08/16 Pct Recovery = 27% Analysis Date = 10/08/16 Pct Recovery = 27% Analysis Date = 10/05/16 Pct Recovery = 27% Analysis Date = 10/05/16 Pct Recovery = 27% Analysis Date = 10/02/16 Pct Recovery = 26% Analysis Date = 10/02/16 Pct Recovery = 26% Analysis Date = 09/29/16 Pct Recovery = 26% Analysis Date = 09/29/16 Pct Recovery = 26% Analysis Date = 09/26/16 Pct Recovery = 26% Analysis Date = 09/26/16 Pct Recovery = 26% Analysis Date = 09/23/16 Pct Recovery = 26% Analysis Date = 09/23/16 Pct Recovery = 26% Analysis Date = 09/20/16 Pct Recovery = 26% Analysis Date = 09/20/16 Pct Recovery = 26% Analysis Date = 09/17/16 Pct Recovery = 26% Analysis Date = 09/17/16 Pct Recovery = 26% Analysis Date = 09/14/16 Pct Recovery = 26% Analysis Date = 09/14/16 Pct Recovery = 26% Analysis Date = 09/12/16 Pct Recovery = 26% Analysis Date = 09/12/16 Pct Recovery = 26% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/06/16 Pct Recovery = 25% Analysis Date = 09/06/16 Pct Recovery = 25% Analysis Date = 09/03/16 Pct Recovery = 25% Analysis Date = 09/03/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/28/16 Pct Recovery = 25% Analysis Date = 08/28/16 Pct Recovery = 25% Analysis Date = 08/25/16 Pct Recovery = 25% Analysis Date = 08/25/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/19/16 Pct Recovery = 25% Analysis Date = 08/19/16 Pct Recovery = 25% Analysis Date = 08/17/16 Pct Recovery = 25% Analysis Date = 08/17/16 Pct Recovery = 25% Analysis Date = 08/14/16 Pct Recovery = 25% Analysis Date = 08/14/16 Pct Recovery = 25% Analysis Date = 08/11/16 Pct Recovery = 25% Analysis Date = 08/11/16 Pct Recovery = 25% Analysis Date = 08/08/16 Pct Recovery = 25% Analysis Date = 08/08/16 Pct Recovery = 25% Analysis Date = 08/05/16 Pct Recovery = 26% Analysis Date = 08/05/16 Pct Recovery = 26% Analysis Date = 08/02/16 Pct Recovery = 26% Analysis Date = 08/02/16 Pct Recovery = 26% Analysis Date = 07/30/16 Pct Recovery = 26% Analysis Date = 07/30/16 Pct Recovery = 26% Analysis Date = 07/27/16 Pct Recovery = 26% Analysis Date = 07/27/16 Pct Recovery = 26% Analysis Date = 07/24/16 Pct Recovery = 27% Analysis Date = 07/24/16 Pct Recovery = 27% Analysis Date = 07/22/16 Pct Recovery = 27% Analysis Date = 07/22/16 Pct Recovery = 27% Analysis Date = 07/19/16 Pct Recovery = 27% Analysis Date = 07/19/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/13/16 Pct Recovery = 28% Analysis Date = 07/13/16 Pct Recovery = 28% Analysis Date = 07/10/16 Pct Recovery = 28% Analysis Date = 07/10/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/04/16 Pct Recovery = 28% Analysis Date = 07/04/16 Pct Recovery = 28% Analysis Date = 07/01/16 Pct Recovery = 29% Analysis Date = 07/01/16 Pct Recovery = 29% Analysis Date = 06/28/16 Pct Recovery = 29% Analysis Date = 06/28/16 Pct Recovery = 29% Analysis Date = 06/26/16 Pct Recovery = 29% Analysis Date = 06/26/16 Pct Recovery = 29% Analysis Date = 06/23/16 Pct Recovery = 29% Analysis Date = 06/23/16 Pct Recovery = 29% Analysis Date = 06/20/16 Pct Recovery = 30% Analysis Date = 06/20/16 Pct Recovery = 30% Analysis Date = 06/17/16 Pct Recovery = 30% Analysis Date = 06/17/16 Pct Recovery = 30% Analysis Date = 06/14/16 Pct Recovery = 30% Analysis Date = 06/14/16 Pct Recovery = 30% Analysis Date = 06/11/16 Pct Recovery = 30% Analysis Date = 06/11/16 Pct Recovery = 30% Analysis Date = 06/08/16 Pct Recovery = 31% Analysis Date = 06/08/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 06/02/16 Pct Recovery = 31% Analysis Date = 06/02/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/28/16 Pct Recovery = 32% Analysis Date = 05/28/16 Pct Recovery = 32% Analysis Date = 05/25/16 Pct Recovery = 32% Analysis Date = 05/25/16 Pct Recovery = 32% Analysis Date = 05/22/16 Pct Recovery = 32% Analysis Date = 05/22/16 Pct Recovery = 32% Analysis Date = 05/19/16 Pct Recovery = 32% Analysis Date = 05/19/16 Pct Recovery = 32% Analysis Date = 05/16/16 Pct Recovery = 33% Analysis Date = 05/16/16 Pct Recovery = 33% Analysis Date = 05/13/16 Pct Recovery = 33% Analysis Date = 05/13/16 Pct Recovery = 33% Analysis Date = 05/10/16 Pct Recovery = 33% Analysis Date = 05/10/16 Pct Recovery = 33% Analysis Date = 05/07/16 Pct Recovery = 33% Analysis Date = 05/07/16 Pct Recovery = 33% Analysis Date = 05/05/16 Pct Recovery = 34% Analysis Date = 05/05/16 Pct Recovery = 34% Analysis Date = 05/02/16 Pct Recovery = 34% Analysis Date = 05/02/16 Pct Recovery = 34% Analysis Date = 04/29/16 Pct Recovery = 34% Analysis Date = 04/29/16 Pct Recovery = 34% Analysis Date = 04/26/16 Pct Recovery = 34% Analysis Date = 04/26/16 Pct Recovery = 34% Analysis Date = 04/23/16 Pct Recovery = 35% Analysis Date = 04/23/16 Pct Recovery = 35% Analysis Date = 04/20/16 Pct Recovery = 35% Analysis Date = 04/20/16 Pct Recovery = 35% Analysis Date = 04/17/16 Pct Recovery = 35% Analysis Date = 04/17/16 Pct Recovery = 35% Analysis Date = 04/14/16 Pct Recovery = 35% Analysis Date = 04/14/16 Pct Recovery = 35% Analysis Date = 04/11/16 Pct Recovery = 36% Analysis Date = 04/11/16 Pct Recovery = 36% Analysis Date = 04/09/16 Pct Recovery = 36% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TIOTROPIUM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 42% 10% 41% 13%
>= Reporting Level 22 42% 47% 30% 21%
Total 28 42% 41% 32% 22%

Sample Statistics
TIOTROPIUM

Characteristic N % % Basis
Plotted 28 82% Spiked
Estimated Values 28 82% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 35 .  
False Negatives 5 15% 5 out of 34
Not Spiked 51 .  
False Positives 0 0% 0 out of 51