OBSP Determination:
ACETONITRILE
METHOD: 4437 , TESTIDCODE: 76997GM016

 Analysis Date = 09/28/16 
 SpikeMix = Accu 216041354: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl 
 Pct Recovery = 295%  Analysis Date = 07/15/16 
 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl 
 Pct Recovery = 141%  Analysis Date = 09/23/16 
 SpikeMix = Phenova B20160303: 40 µl & Accu 216041354: 40 µl 
 Pct Recovery = 149%  Analysis Date = 11/29/16 
 SpikeMix = Accu 216041354: 40 µl & Abs 060916HVOC: 40 µl 
 Pct Recovery = 157%  Analysis Date = 12/23/16 
 SpikeMix = ChemService 5082800: 25 µl & Accu 216041354: 25 µl & NSI 041416HVOC: 25 µl 
 Pct Recovery = 165%  Analysis Date = 01/22/16 
 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl 
 Pct Recovery = 107%  Analysis Date = 08/16/17 
 SpikeMix = ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 
 Pct Recovery = 106%  Analysis Date = 07/06/16 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl 
 Pct Recovery = 172%  Analysis Date = 08/12/16 
 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl 
 Pct Recovery = 154%  Analysis Date = 02/24/17 
 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 176%  Analysis Date = 07/14/17 
 SpikeMix = Accu 216041354: 15 µl & ChemService 5082800: 15 µl & Accu 216041225: 15 µl 
 Pct Recovery = 119%  Analysis Date = 04/09/16 
 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl 
 Pct Recovery = 109%  Analysis Date = 03/22/16 
 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl 
 Pct Recovery = 117%  Analysis Date = 08/16/17 
 Pct Recovery = 109%  Analysis Date = 08/13/17 
 Pct Recovery = 110%  Analysis Date = 08/13/17 
 Pct Recovery = 110%  Analysis Date = 08/10/17 
 Pct Recovery = 111%  Analysis Date = 08/10/17 
 Pct Recovery = 111%  Analysis Date = 08/07/17 
 Pct Recovery = 112%  Analysis Date = 08/07/17 
 Pct Recovery = 112%  Analysis Date = 08/04/17 
 Pct Recovery = 113%  Analysis Date = 08/04/17 
 Pct Recovery = 113%  Analysis Date = 08/01/17 
 Pct Recovery = 113%  Analysis Date = 08/01/17 
 Pct Recovery = 113%  Analysis Date = 07/29/17 
 Pct Recovery = 114%  Analysis Date = 07/29/17 
 Pct Recovery = 114%  Analysis Date = 07/26/17 
 Pct Recovery = 115%  Analysis Date = 07/26/17 
 Pct Recovery = 115%  Analysis Date = 07/24/17 
 Pct Recovery = 116%  Analysis Date = 07/24/17 
 Pct Recovery = 116%  Analysis Date = 07/21/17 
 Pct Recovery = 117%  Analysis Date = 07/21/17 
 Pct Recovery = 117%  Analysis Date = 07/18/17 
 Pct Recovery = 118%  Analysis Date = 07/18/17 
 Pct Recovery = 118%  Analysis Date = 07/15/17 
 Pct Recovery = 119%  Analysis Date = 07/15/17 
 Pct Recovery = 119%  Analysis Date = 07/12/17 
 Pct Recovery = 120%  Analysis Date = 07/12/17 
 Pct Recovery = 120%  Analysis Date = 07/09/17 
 Pct Recovery = 120%  Analysis Date = 07/09/17 
 Pct Recovery = 120%  Analysis Date = 07/06/17 
 Pct Recovery = 121%  Analysis Date = 07/06/17 
 Pct Recovery = 121%  Analysis Date = 07/04/17 
 Pct Recovery = 122%  Analysis Date = 07/04/17 
 Pct Recovery = 122%  Analysis Date = 07/01/17 
 Pct Recovery = 123%  Analysis Date = 07/01/17 
 Pct Recovery = 123%  Analysis Date = 06/28/17 
 Pct Recovery = 124%  Analysis Date = 06/28/17 
 Pct Recovery = 124%  Analysis Date = 06/25/17 
 Pct Recovery = 125%  Analysis Date = 06/25/17 
 Pct Recovery = 125%  Analysis Date = 06/22/17 
 Pct Recovery = 126%  Analysis Date = 06/22/17 
 Pct Recovery = 126%  Analysis Date = 06/19/17 
 Pct Recovery = 127%  Analysis Date = 06/19/17 
 Pct Recovery = 127%  Analysis Date = 06/16/17 
 Pct Recovery = 128%  Analysis Date = 06/16/17 
 Pct Recovery = 128%  Analysis Date = 06/14/17 
 Pct Recovery = 129%  Analysis Date = 06/14/17 
 Pct Recovery = 129%  Analysis Date = 06/11/17 
 Pct Recovery = 129%  Analysis Date = 06/11/17 
 Pct Recovery = 129%  Analysis Date = 06/08/17 
 Pct Recovery = 130%  Analysis Date = 06/08/17 
 Pct Recovery = 130%  Analysis Date = 06/05/17 
 Pct Recovery = 131%  Analysis Date = 06/05/17 
 Pct Recovery = 131%  Analysis Date = 06/02/17 
 Pct Recovery = 132%  Analysis Date = 06/02/17 
 Pct Recovery = 132%  Analysis Date = 05/30/17 
 Pct Recovery = 133%  Analysis Date = 05/30/17 
 Pct Recovery = 133%  Analysis Date = 05/27/17 
 Pct Recovery = 134%  Analysis Date = 05/27/17 
 Pct Recovery = 134%  Analysis Date = 05/25/17 
 Pct Recovery = 135%  Analysis Date = 05/25/17 
 Pct Recovery = 135%  Analysis Date = 05/22/17 
 Pct Recovery = 136%  Analysis Date = 05/22/17 
 Pct Recovery = 136%  Analysis Date = 05/19/17 
 Pct Recovery = 137%  Analysis Date = 05/19/17 
 Pct Recovery = 137%  Analysis Date = 05/16/17 
 Pct Recovery = 138%  Analysis Date = 05/16/17 
 Pct Recovery = 138%  Analysis Date = 05/13/17 
 Pct Recovery = 139%  Analysis Date = 05/13/17 
 Pct Recovery = 139%  Analysis Date = 05/10/17 
 Pct Recovery = 139%  Analysis Date = 05/10/17 
 Pct Recovery = 139%  Analysis Date = 05/07/17 
 Pct Recovery = 140%  Analysis Date = 05/07/17 
 Pct Recovery = 140%  Analysis Date = 05/05/17 
 Pct Recovery = 141%  Analysis Date = 05/05/17 
 Pct Recovery = 141%  Analysis Date = 05/02/17 
 Pct Recovery = 142%  Analysis Date = 05/02/17 
 Pct Recovery = 142%  Analysis Date = 04/29/17 
 Pct Recovery = 143%  Analysis Date = 04/29/17 
 Pct Recovery = 143%  Analysis Date = 04/26/17 
 Pct Recovery = 144%  Analysis Date = 04/26/17 
 Pct Recovery = 144%  Analysis Date = 04/23/17 
 Pct Recovery = 145%  Analysis Date = 04/23/17 
 Pct Recovery = 145%  Analysis Date = 04/20/17 
 Pct Recovery = 146%  Analysis Date = 04/20/17 
 Pct Recovery = 146%  Analysis Date = 04/17/17 
 Pct Recovery = 147%  Analysis Date = 04/17/17 
 Pct Recovery = 147%  Analysis Date = 04/15/17 
 Pct Recovery = 148%  Analysis Date = 04/15/17 
 Pct Recovery = 148%  Analysis Date = 04/12/17 
 Pct Recovery = 149%  Analysis Date = 04/12/17 
 Pct Recovery = 149%  Analysis Date = 04/09/17 
 Pct Recovery = 149%  Analysis Date = 04/09/17 
 Pct Recovery = 149%  Analysis Date = 04/06/17 
 Pct Recovery = 150%  Analysis Date = 04/06/17 
 Pct Recovery = 150%  Analysis Date = 04/03/17 
 Pct Recovery = 151%  Analysis Date = 04/03/17 
 Pct Recovery = 151%  Analysis Date = 03/31/17 
 Pct Recovery = 152%  Analysis Date = 03/31/17 
 Pct Recovery = 152%  Analysis Date = 03/28/17 
 Pct Recovery = 153%  Analysis Date = 03/28/17 
 Pct Recovery = 153%  Analysis Date = 03/26/17 
 Pct Recovery = 154%  Analysis Date = 03/26/17 
 Pct Recovery = 154%  Analysis Date = 03/23/17 
 Pct Recovery = 155%  Analysis Date = 03/23/17 
 Pct Recovery = 155%  Analysis Date = 03/20/17 
 Pct Recovery = 156%  Analysis Date = 03/20/17 
 Pct Recovery = 156%  Analysis Date = 03/17/17 
 Pct Recovery = 157%  Analysis Date = 03/17/17 
 Pct Recovery = 157%  Analysis Date = 03/14/17 
 Pct Recovery = 158%  Analysis Date = 03/14/17 
 Pct Recovery = 158%  Analysis Date = 03/11/17 
 Pct Recovery = 159%  Analysis Date = 03/11/17 
 Pct Recovery = 159%  Analysis Date = 03/08/17 
 Pct Recovery = 159%  Analysis Date = 03/08/17 
 Pct Recovery = 159%  Analysis Date = 03/05/17 
 Pct Recovery = 160%  Analysis Date = 03/05/17 
 Pct Recovery = 160%  Analysis Date = 03/03/17 
 Pct Recovery = 161%  Analysis Date = 03/03/17 
 Pct Recovery = 161%  Analysis Date = 02/28/17 
 Pct Recovery = 162%  Analysis Date = 02/28/17 
 Pct Recovery = 162%  Analysis Date = 02/25/17 
 Pct Recovery = 163%  Analysis Date = 02/25/17 
 Pct Recovery = 163%  Analysis Date = 02/22/17 
 Pct Recovery = 164%  Analysis Date = 02/22/17 
 Pct Recovery = 164%  Analysis Date = 02/19/17 
 Pct Recovery = 164%  Analysis Date = 02/19/17 
 Pct Recovery = 164%  Analysis Date = 02/16/17 
 Pct Recovery = 165%  Analysis Date = 02/16/17 
 Pct Recovery = 165%  Analysis Date = 02/13/17 
 Pct Recovery = 166%  Analysis Date = 02/13/17 
 Pct Recovery = 166%  Analysis Date = 02/11/17 
 Pct Recovery = 166%  Analysis Date = 02/11/17 
 Pct Recovery = 166%  Analysis Date = 02/08/17 
 Pct Recovery = 167%  Analysis Date = 02/08/17 
 Pct Recovery = 167%  Analysis Date = 02/05/17 
 Pct Recovery = 167%  Analysis Date = 02/05/17 
 Pct Recovery = 167%  Analysis Date = 02/02/17 
 Pct Recovery = 168%  Analysis Date = 02/02/17 
 Pct Recovery = 168%  Analysis Date = 01/30/17 
 Pct Recovery = 168%  Analysis Date = 01/30/17 
 Pct Recovery = 168%  Analysis Date = 01/27/17 
 Pct Recovery = 169%  Analysis Date = 01/27/17 
 Pct Recovery = 169%  Analysis Date = 01/24/17 
 Pct Recovery = 170%  Analysis Date = 01/24/17 
 Pct Recovery = 170%  Analysis Date = 01/22/17 
 Pct Recovery = 170%  Analysis Date = 01/22/17 
 Pct Recovery = 170%  Analysis Date = 01/19/17 
 Pct Recovery = 171%  Analysis Date = 01/19/17 
 Pct Recovery = 171%  Analysis Date = 01/16/17 
 Pct Recovery = 171%  Analysis Date = 01/16/17 
 Pct Recovery = 171%  Analysis Date = 01/13/17 
 Pct Recovery = 172%  Analysis Date = 01/13/17 
 Pct Recovery = 172%  Analysis Date = 01/10/17 
 Pct Recovery = 173%  Analysis Date = 01/10/17 
 Pct Recovery = 173%  Analysis Date = 01/07/17 
 Pct Recovery = 173%  Analysis Date = 01/07/17 
 Pct Recovery = 173%  Analysis Date = 01/04/17 
 Pct Recovery = 174%  Analysis Date = 01/04/17 
 Pct Recovery = 174%  Analysis Date = 01/02/17 
 Pct Recovery = 174%  Analysis Date = 01/02/17 
 Pct Recovery = 174%  Analysis Date = 12/30/16 
 Pct Recovery = 175%  Analysis Date = 12/30/16 
 Pct Recovery = 175%  Analysis Date = 12/27/16 
 Pct Recovery = 176%  Analysis Date = 12/27/16 
 Pct Recovery = 176%  Analysis Date = 12/24/16 
 Pct Recovery = 176%  Analysis Date = 12/24/16 
 Pct Recovery = 176%  Analysis Date = 12/21/16 
 Pct Recovery = 177%  Analysis Date = 12/21/16 
 Pct Recovery = 177%  Analysis Date = 12/18/16 
 Pct Recovery = 177%  Analysis Date = 12/18/16 
 Pct Recovery = 177%  Analysis Date = 12/15/16 
 Pct Recovery = 178%  Analysis Date = 12/15/16 
 Pct Recovery = 178%  Analysis Date = 12/13/16 
 Pct Recovery = 178%  Analysis Date = 12/13/16 
 Pct Recovery = 178%  Analysis Date = 12/10/16 
 Pct Recovery = 179%  Analysis Date = 12/10/16 
 Pct Recovery = 179%  Analysis Date = 12/07/16 
 Pct Recovery = 180%  Analysis Date = 12/07/16 
 Pct Recovery = 180%  Analysis Date = 12/04/16 
 Pct Recovery = 180%  Analysis Date = 12/04/16 
 Pct Recovery = 180%  Analysis Date = 12/01/16 
 Pct Recovery = 181%  Analysis Date = 12/01/16 
 Pct Recovery = 181%  Analysis Date = 11/28/16 
 Pct Recovery = 181%  Analysis Date = 11/28/16 
 Pct Recovery = 181%  Analysis Date = 11/25/16 
 Pct Recovery = 183%  Analysis Date = 11/25/16 
 Pct Recovery = 183%  Analysis Date = 11/23/16 
 Pct Recovery = 184%  Analysis Date = 11/23/16 
 Pct Recovery = 184%  Analysis Date = 11/20/16 
 Pct Recovery = 185%  Analysis Date = 11/20/16 
 Pct Recovery = 185%  Analysis Date = 11/17/16 
 Pct Recovery = 186%  Analysis Date = 11/17/16 
 Pct Recovery = 186%  Analysis Date = 11/14/16 
 Pct Recovery = 187%  Analysis Date = 11/14/16 
 Pct Recovery = 187%  Analysis Date = 11/11/16 
 Pct Recovery = 188%  Analysis Date = 11/11/16 
 Pct Recovery = 188%  Analysis Date = 11/08/16 
 Pct Recovery = 189%  Analysis Date = 11/08/16 
 Pct Recovery = 189%  Analysis Date = 11/05/16 
 Pct Recovery = 190%  Analysis Date = 11/05/16 
 Pct Recovery = 190%  Analysis Date = 11/03/16 
 Pct Recovery = 191%  Analysis Date = 11/03/16 
 Pct Recovery = 191%  Analysis Date = 10/31/16 
 Pct Recovery = 192%  Analysis Date = 10/31/16 
 Pct Recovery = 192%  Analysis Date = 10/28/16 
 Pct Recovery = 193%  Analysis Date = 10/28/16 
 Pct Recovery = 193%  Analysis Date = 10/25/16 
 Pct Recovery = 194%  Analysis Date = 10/25/16 
 Pct Recovery = 194%  Analysis Date = 10/22/16 
 Pct Recovery = 195%  Analysis Date = 10/22/16 
 Pct Recovery = 195%  Analysis Date = 10/19/16 
 Pct Recovery = 196%  Analysis Date = 10/19/16 
 Pct Recovery = 196%  Analysis Date = 10/16/16 
 Pct Recovery = 197%  Analysis Date = 10/16/16 
 Pct Recovery = 197%  Analysis Date = 10/13/16 
 Pct Recovery = 198%  Analysis Date = 10/13/16 
 Pct Recovery = 198%  Analysis Date = 10/11/16 
 Pct Recovery = 200%  Analysis Date = 10/11/16 
 Pct Recovery = 200%  Analysis Date = 10/08/16 
 Pct Recovery = 201%  Analysis Date = 10/08/16 
 Pct Recovery = 201%  Analysis Date = 10/05/16 
 Pct Recovery = 202%  Analysis Date = 10/05/16 
 Pct Recovery = 202%  Analysis Date = 10/02/16 
 Pct Recovery = 203%  Analysis Date = 10/02/16 
 Pct Recovery = 203%  Analysis Date = 09/29/16 
 Pct Recovery = 204%  Analysis Date = 09/29/16 
 Pct Recovery = 204%  Analysis Date = 09/26/16 
 Pct Recovery = 204%  Analysis Date = 09/26/16 
 Pct Recovery = 204%  Analysis Date = 09/23/16 
 Pct Recovery = 202%  Analysis Date = 09/23/16 
 Pct Recovery = 202%  Analysis Date = 09/21/16 
 Pct Recovery = 201%  Analysis Date = 09/21/16 
 Pct Recovery = 201%  Analysis Date = 09/18/16 
 Pct Recovery = 199%  Analysis Date = 09/18/16 
 Pct Recovery = 199%  Analysis Date = 09/15/16 
 Pct Recovery = 197%  Analysis Date = 09/15/16 
 Pct Recovery = 197%  Analysis Date = 09/12/16 
 Pct Recovery = 195%  Analysis Date = 09/12/16 
 Pct Recovery = 195%  Analysis Date = 09/09/16 
 Pct Recovery = 193%  Analysis Date = 09/09/16 
 Pct Recovery = 193%  Analysis Date = 09/06/16 
 Pct Recovery = 192%  Analysis Date = 09/06/16 
 Pct Recovery = 192%  Analysis Date = 09/03/16 
 Pct Recovery = 190%  Analysis Date = 09/03/16 
 Pct Recovery = 190%  Analysis Date = 09/01/16 
 Pct Recovery = 188%  Analysis Date = 09/01/16 
 Pct Recovery = 188%  Analysis Date = 08/29/16 
 Pct Recovery = 186%  Analysis Date = 08/29/16 
 Pct Recovery = 186%  Analysis Date = 08/26/16 
 Pct Recovery = 185%  Analysis Date = 08/26/16 
 Pct Recovery = 185%  Analysis Date = 08/23/16 
 Pct Recovery = 183%  Analysis Date = 08/23/16 
 Pct Recovery = 183%  Analysis Date = 08/20/16 
 Pct Recovery = 181%  Analysis Date = 08/20/16 
 Pct Recovery = 181%  Analysis Date = 08/17/16 
 Pct Recovery = 179%  Analysis Date = 08/17/16 
 Pct Recovery = 179%  Analysis Date = 08/14/16 
 Pct Recovery = 178%  Analysis Date = 08/14/16 
 Pct Recovery = 178%  Analysis Date = 08/12/16 
 Pct Recovery = 176%  Analysis Date = 08/12/16 
 Pct Recovery = 176%  Analysis Date = 08/09/16 
 Pct Recovery = 174%  Analysis Date = 08/09/16 
 Pct Recovery = 174%  Analysis Date = 08/06/16 
 Pct Recovery = 172%  Analysis Date = 08/06/16 
 Pct Recovery = 172%  Analysis Date = 08/03/16 
 Pct Recovery = 170%  Analysis Date = 08/03/16 
 Pct Recovery = 170%  Analysis Date = 07/31/16 
 Pct Recovery = 168%  Analysis Date = 07/31/16 
 Pct Recovery = 168%  Analysis Date = 07/28/16 
 Pct Recovery = 165%  Analysis Date = 07/28/16 
 Pct Recovery = 165%  Analysis Date = 07/25/16 
 Pct Recovery = 163%  Analysis Date = 07/25/16 
 Pct Recovery = 163%  Analysis Date = 07/23/16 
 Pct Recovery = 161%  Analysis Date = 07/23/16 
 Pct Recovery = 161%  Analysis Date = 07/20/16 
 Pct Recovery = 159%  Analysis Date = 07/20/16 
 Pct Recovery = 159%  Analysis Date = 07/17/16 
 Pct Recovery = 157%  Analysis Date = 07/17/16 
 Pct Recovery = 157%  Analysis Date = 07/14/16 
 Pct Recovery = 155%  Analysis Date = 07/14/16 
 Pct Recovery = 155%  Analysis Date = 07/11/16 
 Pct Recovery = 154%  Analysis Date = 07/11/16 
 Pct Recovery = 154%  Analysis Date = 07/08/16 
 Pct Recovery = 153%  Analysis Date = 07/08/16 
 Pct Recovery = 153%  Analysis Date = 07/05/16 
 Pct Recovery = 151%  Analysis Date = 07/05/16 
 Pct Recovery = 151%  Analysis Date = 07/03/16 
 Pct Recovery = 150%  Analysis Date = 07/03/16 
 Pct Recovery = 150%  Analysis Date = 06/30/16 
 Pct Recovery = 149%  Analysis Date = 06/30/16 
 Pct Recovery = 149%  Analysis Date = 06/27/16 
 Pct Recovery = 148%  Analysis Date = 06/27/16 
 Pct Recovery = 148%  Analysis Date = 06/24/16 
 Pct Recovery = 148%  Analysis Date = 06/24/16 
 Pct Recovery = 148%  Analysis Date = 06/21/16 
 Pct Recovery = 147%  Analysis Date = 06/21/16 
 Pct Recovery = 147%  Analysis Date = 06/18/16 
 Pct Recovery = 146%  Analysis Date = 06/18/16 
 Pct Recovery = 146%  Analysis Date = 06/15/16 
 Pct Recovery = 145%  Analysis Date = 06/15/16 
 Pct Recovery = 145%  Analysis Date = 06/13/16 
 Pct Recovery = 144%  Analysis Date = 06/13/16 
 Pct Recovery = 144%  Analysis Date = 06/10/16 
 Pct Recovery = 143%  Analysis Date = 06/10/16 
 Pct Recovery = 143%  Analysis Date = 06/07/16 
 Pct Recovery = 142%  Analysis Date = 06/07/16 
 Pct Recovery = 142%  Analysis Date = 06/04/16 
 Pct Recovery = 141%  Analysis Date = 06/04/16 
 Pct Recovery = 141%  Analysis Date = 06/01/16 
 Pct Recovery = 140%  Analysis Date = 06/01/16 
 Pct Recovery = 140%  Analysis Date = 05/29/16 
 Pct Recovery = 139%  Analysis Date = 05/29/16 
 Pct Recovery = 139%  Analysis Date = 05/26/16 
 Pct Recovery = 138%  Analysis Date = 05/26/16 
 Pct Recovery = 138%  Analysis Date = 05/23/16 
 Pct Recovery = 137%  Analysis Date = 05/23/16 
 Pct Recovery = 137%  Analysis Date = 05/21/16 
 Pct Recovery = 136%  Analysis Date = 05/21/16 
 Pct Recovery = 136%  Analysis Date = 05/18/16 
 Pct Recovery = 135%  Analysis Date = 05/18/16 
 Pct Recovery = 135%  Analysis Date = 05/15/16 
 Pct Recovery = 134%  Analysis Date = 05/15/16 
 Pct Recovery = 134%  Analysis Date = 05/12/16 
 Pct Recovery = 133%  Analysis Date = 05/12/16 
 Pct Recovery = 133%  Analysis Date = 05/09/16 
 Pct Recovery = 132%  Analysis Date = 05/09/16 
 Pct Recovery = 132%  Analysis Date = 05/06/16 
 Pct Recovery = 131%  Analysis Date = 05/06/16 
 Pct Recovery = 131%  Analysis Date = 05/03/16 
 Pct Recovery = 130%  Analysis Date = 05/03/16 
 Pct Recovery = 130%  Analysis Date = 05/01/16 
 Pct Recovery = 129%  Analysis Date = 05/01/16 
 Pct Recovery = 129%  Analysis Date = 04/28/16 
 Pct Recovery = 129%  Analysis Date = 04/28/16 
 Pct Recovery = 129%  Analysis Date = 04/25/16 
 Pct Recovery = 128%  Analysis Date = 04/25/16 
 Pct Recovery = 128%  Analysis Date = 04/22/16 
 Pct Recovery = 127%  Analysis Date = 04/22/16 
 Pct Recovery = 127%  Analysis Date = 04/19/16 
 Pct Recovery = 126%  Analysis Date = 04/19/16 
 Pct Recovery = 126%  Analysis Date = 04/16/16 
 Pct Recovery = 125%  Analysis Date = 04/16/16 
 Pct Recovery = 125%  Analysis Date = 04/13/16 
 Pct Recovery = 124%  Analysis Date = 04/13/16 
 Pct Recovery = 124%  Analysis Date = 04/11/16 
 Pct Recovery = 123%  Analysis Date = 04/11/16 
 Pct Recovery = 123%  Analysis Date = 04/08/16 
 Pct Recovery = 122%  Analysis Date = 04/08/16 
 Pct Recovery = 122%  Analysis Date = 04/05/16 
 Pct Recovery = 121%  Analysis Date = 04/05/16 
 Pct Recovery = 121%  Analysis Date = 04/02/16 
 Pct Recovery = 120%  Analysis Date = 04/02/16 
 Pct Recovery = 120%  Analysis Date = 03/30/16 
 Pct Recovery = 119%  Analysis Date = 03/30/16 
 Pct Recovery = 119%  Analysis Date = 03/27/16 
 Pct Recovery = 119%  Analysis Date = 03/27/16 
 Pct Recovery = 119%  Analysis Date = 03/24/16 
 Pct Recovery = 118%  Analysis Date = 03/24/16 
 Pct Recovery = 118%  Analysis Date = 03/22/16 
 Pct Recovery = 117%  Analysis Date = 03/22/16 
 Pct Recovery = 117%  Analysis Date = 03/19/16 
 Pct Recovery = 116%  Analysis Date = 03/19/16 
 Pct Recovery = 116%  Analysis Date = 03/16/16 
 Pct Recovery = 115%  Analysis Date = 03/16/16 
 Pct Recovery = 115%  Analysis Date = 03/13/16 
 Pct Recovery = 115%  Analysis Date = 03/13/16 
 Pct Recovery = 115%  Analysis Date = 03/10/16 
 Pct Recovery = 114%  Analysis Date = 03/10/16 
 Pct Recovery = 114%  Analysis Date = 03/07/16 
 Pct Recovery = 113%  Analysis Date = 03/07/16 
 Pct Recovery = 113%  Analysis Date = 03/04/16 
 Pct Recovery = 112%  Analysis Date = 03/04/16 
 Pct Recovery = 112%  Analysis Date = 03/02/16 
 Pct Recovery = 111%  Analysis Date = 03/02/16 
 Pct Recovery = 111%  Analysis Date = 02/28/16 
 Pct Recovery = 111%  Analysis Date = 02/28/16 
 Pct Recovery = 111%  Analysis Date = 02/25/16 
 Pct Recovery = 110%  Analysis Date = 02/25/16 
 Pct Recovery = 110%  Analysis Date = 02/22/16 
 Pct Recovery = 109%  Analysis Date = 02/22/16 
 Pct Recovery = 109%  Analysis Date = 02/19/16 
 Pct Recovery = 108%  Analysis Date = 02/19/16 
 Pct Recovery = 108%  Analysis Date = 02/16/16 
 Pct Recovery = 107%  Analysis Date = 02/16/16 
 Pct Recovery = 107%  Analysis Date = 02/13/16 
 Pct Recovery = 107%  Analysis Date = 02/13/16 
 Pct Recovery = 107%  Analysis Date = 02/11/16 
 Pct Recovery = 106%  Analysis Date = 02/11/16 
 Pct Recovery = 106%  Analysis Date = 02/08/16 
 Pct Recovery = 105%  Analysis Date = 02/08/16 
 Pct Recovery = 105%  Analysis Date = 02/05/16 
 Pct Recovery = 104%  Analysis Date = 02/05/16 
 Pct Recovery = 104%  Analysis Date = 02/02/16 
 Pct Recovery = 103%  Analysis Date = 02/02/16 
 Pct Recovery = 103%  Analysis Date = 01/30/16 
 Pct Recovery = 103%  Analysis Date = 01/30/16 
 Pct Recovery = 103%  Analysis Date = 01/27/16 
 Pct Recovery = 102%  Analysis Date = 01/27/16 
 Pct Recovery = 102%  Analysis Date = 01/24/16 
 Pct Recovery = 101%  Analysis Date = 01/24/16 
 Pct Recovery = 101%  Analysis Date = 01/22/16 
 Pct Recovery = 100%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 151% 50% 149% 36%
Total 13 151% 50% 149% 36%

Sample Statistics
ACETONITRILE

Characteristic N % % Basis
Plotted 13 100% Spiked
Estimated Values 1 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 13 .  
False Negatives 0 0% 0 out of 13
Not Spiked 14 .  
False Positives 3 21% 3 out of 14