BQS OBSP Determination:
ANTIPYRENE
METHOD: LC9017 , TESTIDCODE: 67477LCM56
Open Data Set

Analysis Date = 01/24/13 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl Pct Recovery = 83% Analysis Date = 01/24/13 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl Pct Recovery = 83% Analysis Date = 05/02/13 SpikeMix = ERA 0823-11-05.1: 40 µl Pct Recovery = 68% Analysis Date = 05/02/13 SpikeMix = ERA 0823-11-05.1: 40 µl Pct Recovery = 68% Analysis Date = 05/01/12 SpikeMix = ERA 0823-11-05.1: 40 µl Pct Recovery = 140% Analysis Date = 05/01/12 SpikeMix = ERA 0823-11-05.1: 40 µl Pct Recovery = 140% Analysis Date = 12/14/12 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Pct Recovery = 82% Analysis Date = 12/14/12 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Pct Recovery = 82% Analysis Date = 05/03/13 SpikeMix = Spex Organics T1120802015: 40 µl Pct Recovery = 75% Analysis Date = 05/03/13 SpikeMix = Spex Organics T1120802015: 40 µl Pct Recovery = 75% Analysis Date = 03/21/14 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Pct Recovery = 76% Analysis Date = 03/21/14 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Pct Recovery = 76% Analysis Date = 07/26/12 SpikeMix = ERA 0823-11-05.1: 20 µl Pct Recovery = 193% Analysis Date = 07/26/12 SpikeMix = ERA 0823-11-05.1: 20 µl Pct Recovery = 193% Analysis Date = 04/10/12 SpikeMix = ERA 0823-11-05.1: 20 µl Pct Recovery = 65% Analysis Date = 04/10/12 SpikeMix = ERA 0823-11-05.1: 20 µl Pct Recovery = 65% Analysis Date = 08/29/13 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Pct Recovery = 92% Analysis Date = 08/29/13 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Pct Recovery = 92% Analysis Date = 02/20/14 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 76% Analysis Date = 02/20/14 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 76% Analysis Date = 02/28/13 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 79% Analysis Date = 02/28/13 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 79% Analysis Date = 09/27/12 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 93% Analysis Date = 09/27/12 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Pct Recovery = 93% Analysis Date = 11/20/13 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Pct Recovery = 63% Analysis Date = 11/20/13 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Pct Recovery = 63% Analysis Date = 01/16/14 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl Pct Recovery = 71% Analysis Date = 01/16/14 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl Pct Recovery = 71% Analysis Date = 02/19/14 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl Pct Recovery = 69% Analysis Date = 02/19/14 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl Pct Recovery = 69% Analysis Date = 06/15/12 SpikeMix = ERA 0823-11-05.1: 10 µl Pct Recovery = 67% Analysis Date = 06/15/12 SpikeMix = ERA 0823-11-05.1: 10 µl Pct Recovery = 67% Analysis Date = 10/25/12 SpikeMix = Abs 060112: 10 µl & Spex Organics T1120802015: 10 µl Pct Recovery = 84% Analysis Date = 10/25/12 SpikeMix = Abs 060112: 10 µl & Spex Organics T1120802015: 10 µl Pct Recovery = 84% Analysis Date = 03/20/14 Pct Recovery = 72% Analysis Date = 03/17/14 Pct Recovery = 72% Analysis Date = 03/17/14 Pct Recovery = 72% Analysis Date = 03/13/14 Pct Recovery = 72% Analysis Date = 03/13/14 Pct Recovery = 72% Analysis Date = 03/10/14 Pct Recovery = 72% Analysis Date = 03/10/14 Pct Recovery = 72% Analysis Date = 03/06/14 Pct Recovery = 72% Analysis Date = 03/06/14 Pct Recovery = 72% Analysis Date = 03/03/14 Pct Recovery = 72% Analysis Date = 03/03/14 Pct Recovery = 72% Analysis Date = 02/27/14 Pct Recovery = 72% Analysis Date = 02/27/14 Pct Recovery = 72% Analysis Date = 02/24/14 Pct Recovery = 72% Analysis Date = 02/24/14 Pct Recovery = 72% Analysis Date = 02/20/14 Pct Recovery = 72% Analysis Date = 02/20/14 Pct Recovery = 72% Analysis Date = 02/17/14 Pct Recovery = 72% Analysis Date = 02/17/14 Pct Recovery = 72% Analysis Date = 02/13/14 Pct Recovery = 72% Analysis Date = 02/13/14 Pct Recovery = 72% Analysis Date = 02/09/14 Pct Recovery = 72% Analysis Date = 02/09/14 Pct Recovery = 72% Analysis Date = 02/06/14 Pct Recovery = 73% Analysis Date = 02/06/14 Pct Recovery = 73% Analysis Date = 02/02/14 Pct Recovery = 73% Analysis Date = 02/02/14 Pct Recovery = 73% Analysis Date = 01/30/14 Pct Recovery = 73% Analysis Date = 01/30/14 Pct Recovery = 73% Analysis Date = 01/26/14 Pct Recovery = 73% Analysis Date = 01/26/14 Pct Recovery = 73% Analysis Date = 01/23/14 Pct Recovery = 73% Analysis Date = 01/23/14 Pct Recovery = 73% Analysis Date = 01/19/14 Pct Recovery = 73% Analysis Date = 01/19/14 Pct Recovery = 73% Analysis Date = 01/16/14 Pct Recovery = 73% Analysis Date = 01/16/14 Pct Recovery = 73% Analysis Date = 01/12/14 Pct Recovery = 73% Analysis Date = 01/12/14 Pct Recovery = 73% Analysis Date = 01/08/14 Pct Recovery = 73% Analysis Date = 01/08/14 Pct Recovery = 73% Analysis Date = 01/05/14 Pct Recovery = 73% Analysis Date = 01/05/14 Pct Recovery = 73% Analysis Date = 01/01/14 Pct Recovery = 73% Analysis Date = 01/01/14 Pct Recovery = 73% Analysis Date = 12/29/13 Pct Recovery = 73% Analysis Date = 12/29/13 Pct Recovery = 73% Analysis Date = 12/25/13 Pct Recovery = 73% Analysis Date = 12/25/13 Pct Recovery = 73% Analysis Date = 12/22/13 Pct Recovery = 74% Analysis Date = 12/22/13 Pct Recovery = 74% Analysis Date = 12/18/13 Pct Recovery = 74% Analysis Date = 12/18/13 Pct Recovery = 74% Analysis Date = 12/15/13 Pct Recovery = 74% Analysis Date = 12/15/13 Pct Recovery = 74% Analysis Date = 12/11/13 Pct Recovery = 74% Analysis Date = 12/11/13 Pct Recovery = 74% Analysis Date = 12/08/13 Pct Recovery = 74% Analysis Date = 12/08/13 Pct Recovery = 74% Analysis Date = 12/04/13 Pct Recovery = 74% Analysis Date = 12/04/13 Pct Recovery = 74% Analysis Date = 11/30/13 Pct Recovery = 74% Analysis Date = 11/30/13 Pct Recovery = 74% Analysis Date = 11/27/13 Pct Recovery = 74% Analysis Date = 11/27/13 Pct Recovery = 74% Analysis Date = 11/23/13 Pct Recovery = 74% Analysis Date = 11/23/13 Pct Recovery = 74% Analysis Date = 11/20/13 Pct Recovery = 74% Analysis Date = 11/20/13 Pct Recovery = 74% Analysis Date = 11/16/13 Pct Recovery = 74% Analysis Date = 11/16/13 Pct Recovery = 74% Analysis Date = 11/13/13 Pct Recovery = 74% Analysis Date = 11/13/13 Pct Recovery = 74% Analysis Date = 11/09/13 Pct Recovery = 75% Analysis Date = 11/09/13 Pct Recovery = 75% Analysis Date = 11/06/13 Pct Recovery = 75% Analysis Date = 11/06/13 Pct Recovery = 75% Analysis Date = 11/02/13 Pct Recovery = 75% Analysis Date = 11/02/13 Pct Recovery = 75% Analysis Date = 10/29/13 Pct Recovery = 75% Analysis Date = 10/29/13 Pct Recovery = 75% Analysis Date = 10/26/13 Pct Recovery = 75% Analysis Date = 10/26/13 Pct Recovery = 75% Analysis Date = 10/22/13 Pct Recovery = 75% Analysis Date = 10/22/13 Pct Recovery = 75% Analysis Date = 10/19/13 Pct Recovery = 75% Analysis Date = 10/19/13 Pct Recovery = 75% Analysis Date = 10/15/13 Pct Recovery = 75% Analysis Date = 10/15/13 Pct Recovery = 75% Analysis Date = 10/12/13 Pct Recovery = 75% Analysis Date = 10/12/13 Pct Recovery = 75% Analysis Date = 10/08/13 Pct Recovery = 75% Analysis Date = 10/08/13 Pct Recovery = 75% Analysis Date = 10/05/13 Pct Recovery = 75% Analysis Date = 10/05/13 Pct Recovery = 75% Analysis Date = 10/01/13 Pct Recovery = 75% Analysis Date = 10/01/13 Pct Recovery = 75% Analysis Date = 09/28/13 Pct Recovery = 75% Analysis Date = 09/28/13 Pct Recovery = 75% Analysis Date = 09/24/13 Pct Recovery = 76% Analysis Date = 09/24/13 Pct Recovery = 76% Analysis Date = 09/20/13 Pct Recovery = 76% Analysis Date = 09/20/13 Pct Recovery = 76% Analysis Date = 09/17/13 Pct Recovery = 76% Analysis Date = 09/17/13 Pct Recovery = 76% Analysis Date = 09/13/13 Pct Recovery = 76% Analysis Date = 09/13/13 Pct Recovery = 76% Analysis Date = 09/10/13 Pct Recovery = 76% Analysis Date = 09/10/13 Pct Recovery = 76% Analysis Date = 09/06/13 Pct Recovery = 76% Analysis Date = 09/06/13 Pct Recovery = 76% Analysis Date = 09/03/13 Pct Recovery = 76% Analysis Date = 09/03/13 Pct Recovery = 76% Analysis Date = 08/30/13 Pct Recovery = 76% Analysis Date = 08/30/13 Pct Recovery = 76% Analysis Date = 08/27/13 Pct Recovery = 76% Analysis Date = 08/27/13 Pct Recovery = 76% Analysis Date = 08/23/13 Pct Recovery = 76% Analysis Date = 08/23/13 Pct Recovery = 76% Analysis Date = 08/19/13 Pct Recovery = 76% Analysis Date = 08/19/13 Pct Recovery = 76% Analysis Date = 08/16/13 Pct Recovery = 76% Analysis Date = 08/16/13 Pct Recovery = 76% Analysis Date = 08/12/13 Pct Recovery = 76% Analysis Date = 08/12/13 Pct Recovery = 76% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 08/09/13 Pct Recovery = 77% Analysis Date = 08/05/13 Pct Recovery = 77% Analysis Date = 08/05/13 Pct Recovery = 77% Analysis Date = 08/02/13 Pct Recovery = 77% Analysis Date = 08/02/13 Pct Recovery = 77% Analysis Date = 07/29/13 Pct Recovery = 77% Analysis Date = 07/29/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/22/13 Pct Recovery = 77% Analysis Date = 07/19/13 Pct Recovery = 77% Analysis Date = 07/19/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/11/13 Pct Recovery = 77% Analysis Date = 07/11/13 Pct Recovery = 77% Analysis Date = 07/08/13 Pct Recovery = 77% Analysis Date = 07/08/13 Pct Recovery = 77% Analysis Date = 07/04/13 Pct Recovery = 77% Analysis Date = 07/04/13 Pct Recovery = 77% Analysis Date = 07/01/13 Pct Recovery = 77% Analysis Date = 07/01/13 Pct Recovery = 77% Analysis Date = 06/27/13 Pct Recovery = 78% Analysis Date = 06/27/13 Pct Recovery = 78% Analysis Date = 06/24/13 Pct Recovery = 78% Analysis Date = 06/24/13 Pct Recovery = 78% Analysis Date = 06/20/13 Pct Recovery = 78% Analysis Date = 06/20/13 Pct Recovery = 78% Analysis Date = 06/17/13 Pct Recovery = 78% Analysis Date = 06/17/13 Pct Recovery = 78% Analysis Date = 06/13/13 Pct Recovery = 78% Analysis Date = 06/13/13 Pct Recovery = 78% Analysis Date = 06/09/13 Pct Recovery = 78% Analysis Date = 06/09/13 Pct Recovery = 78% Analysis Date = 06/06/13 Pct Recovery = 78% Analysis Date = 06/06/13 Pct Recovery = 78% Analysis Date = 06/02/13 Pct Recovery = 78% Analysis Date = 06/02/13 Pct Recovery = 78% Analysis Date = 05/30/13 Pct Recovery = 78% Analysis Date = 05/30/13 Pct Recovery = 78% Analysis Date = 05/26/13 Pct Recovery = 78% Analysis Date = 05/26/13 Pct Recovery = 78% Analysis Date = 05/23/13 Pct Recovery = 78% Analysis Date = 05/23/13 Pct Recovery = 78% Analysis Date = 05/19/13 Pct Recovery = 78% Analysis Date = 05/19/13 Pct Recovery = 78% Analysis Date = 05/16/13 Pct Recovery = 78% Analysis Date = 05/16/13 Pct Recovery = 78% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/09/13 Pct Recovery = 79% Analysis Date = 05/09/13 Pct Recovery = 79% Analysis Date = 05/05/13 Pct Recovery = 79% Analysis Date = 05/05/13 Pct Recovery = 79% Analysis Date = 05/01/13 Pct Recovery = 79% Analysis Date = 05/01/13 Pct Recovery = 79% Analysis Date = 04/28/13 Pct Recovery = 79% Analysis Date = 04/28/13 Pct Recovery = 79% Analysis Date = 04/24/13 Pct Recovery = 79% Analysis Date = 04/24/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/17/13 Pct Recovery = 79% Analysis Date = 04/17/13 Pct Recovery = 79% Analysis Date = 04/14/13 Pct Recovery = 79% Analysis Date = 04/14/13 Pct Recovery = 79% Analysis Date = 04/10/13 Pct Recovery = 79% Analysis Date = 04/10/13 Pct Recovery = 79% Analysis Date = 04/07/13 Pct Recovery = 79% Analysis Date = 04/07/13 Pct Recovery = 79% Analysis Date = 04/03/13 Pct Recovery = 79% Analysis Date = 04/03/13 Pct Recovery = 79% Analysis Date = 03/30/13 Pct Recovery = 79% Analysis Date = 03/30/13 Pct Recovery = 79% Analysis Date = 03/27/13 Pct Recovery = 79% Analysis Date = 03/27/13 Pct Recovery = 79% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/16/13 Pct Recovery = 80% Analysis Date = 03/16/13 Pct Recovery = 80% Analysis Date = 03/13/13 Pct Recovery = 80% Analysis Date = 03/13/13 Pct Recovery = 80% Analysis Date = 03/09/13 Pct Recovery = 80% Analysis Date = 03/09/13 Pct Recovery = 80% Analysis Date = 03/06/13 Pct Recovery = 80% Analysis Date = 03/06/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 02/27/13 Pct Recovery = 80% Analysis Date = 02/27/13 Pct Recovery = 80% Analysis Date = 02/23/13 Pct Recovery = 81% Analysis Date = 02/23/13 Pct Recovery = 81% Analysis Date = 02/19/13 Pct Recovery = 81% Analysis Date = 02/19/13 Pct Recovery = 81% Analysis Date = 02/16/13 Pct Recovery = 82% Analysis Date = 02/16/13 Pct Recovery = 82% Analysis Date = 02/12/13 Pct Recovery = 82% Analysis Date = 02/12/13 Pct Recovery = 82% Analysis Date = 02/09/13 Pct Recovery = 83% Analysis Date = 02/09/13 Pct Recovery = 83% Analysis Date = 02/05/13 Pct Recovery = 83% Analysis Date = 02/05/13 Pct Recovery = 83% Analysis Date = 02/02/13 Pct Recovery = 84% Analysis Date = 02/02/13 Pct Recovery = 84% Analysis Date = 01/29/13 Pct Recovery = 84% Analysis Date = 01/29/13 Pct Recovery = 84% Analysis Date = 01/26/13 Pct Recovery = 85% Analysis Date = 01/26/13 Pct Recovery = 85% Analysis Date = 01/22/13 Pct Recovery = 85% Analysis Date = 01/22/13 Pct Recovery = 85% Analysis Date = 01/18/13 Pct Recovery = 86% Analysis Date = 01/18/13 Pct Recovery = 86% Analysis Date = 01/15/13 Pct Recovery = 86% Analysis Date = 01/15/13 Pct Recovery = 86% Analysis Date = 01/11/13 Pct Recovery = 87% Analysis Date = 01/11/13 Pct Recovery = 87% Analysis Date = 01/08/13 Pct Recovery = 87% Analysis Date = 01/08/13 Pct Recovery = 87% Analysis Date = 01/04/13 Pct Recovery = 88% Analysis Date = 01/04/13 Pct Recovery = 88% Analysis Date = 01/01/13 Pct Recovery = 88% Analysis Date = 01/01/13 Pct Recovery = 88% Analysis Date = 12/28/12 Pct Recovery = 89% Analysis Date = 12/28/12 Pct Recovery = 89% Analysis Date = 12/25/12 Pct Recovery = 89% Analysis Date = 12/25/12 Pct Recovery = 89% Analysis Date = 12/21/12 Pct Recovery = 90% Analysis Date = 12/21/12 Pct Recovery = 90% Analysis Date = 12/18/12 Pct Recovery = 90% Analysis Date = 12/18/12 Pct Recovery = 90% Analysis Date = 12/14/12 Pct Recovery = 91% Analysis Date = 12/14/12 Pct Recovery = 91% Analysis Date = 12/10/12 Pct Recovery = 91% Analysis Date = 12/10/12 Pct Recovery = 91% Analysis Date = 12/07/12 Pct Recovery = 92% Analysis Date = 12/07/12 Pct Recovery = 92% Analysis Date = 12/03/12 Pct Recovery = 92% Analysis Date = 12/03/12 Pct Recovery = 92% Analysis Date = 11/30/12 Pct Recovery = 93% Analysis Date = 11/30/12 Pct Recovery = 93% Analysis Date = 11/26/12 Pct Recovery = 94% Analysis Date = 11/26/12 Pct Recovery = 94% Analysis Date = 11/23/12 Pct Recovery = 94% Analysis Date = 11/23/12 Pct Recovery = 94% Analysis Date = 11/19/12 Pct Recovery = 95% Analysis Date = 11/19/12 Pct Recovery = 95% Analysis Date = 11/16/12 Pct Recovery = 95% Analysis Date = 11/16/12 Pct Recovery = 95% Analysis Date = 11/12/12 Pct Recovery = 96% Analysis Date = 11/12/12 Pct Recovery = 96% Analysis Date = 11/08/12 Pct Recovery = 96% Analysis Date = 11/08/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 97% Analysis Date = 11/05/12 Pct Recovery = 97% Analysis Date = 11/01/12 Pct Recovery = 97% Analysis Date = 11/01/12 Pct Recovery = 97% Analysis Date = 10/29/12 Pct Recovery = 98% Analysis Date = 10/29/12 Pct Recovery = 98% Analysis Date = 10/25/12 Pct Recovery = 99% Analysis Date = 10/25/12 Pct Recovery = 99% Analysis Date = 10/22/12 Pct Recovery = 99% Analysis Date = 10/22/12 Pct Recovery = 99% Analysis Date = 10/18/12 Pct Recovery = 100% Analysis Date = 10/18/12 Pct Recovery = 100% Analysis Date = 10/15/12 Pct Recovery = 100% Analysis Date = 10/15/12 Pct Recovery = 100% Analysis Date = 10/11/12 Pct Recovery = 101% Analysis Date = 10/11/12 Pct Recovery = 101% Analysis Date = 10/08/12 Pct Recovery = 101% Analysis Date = 10/08/12 Pct Recovery = 101% Analysis Date = 10/04/12 Pct Recovery = 102% Analysis Date = 10/04/12 Pct Recovery = 102% Analysis Date = 09/30/12 Pct Recovery = 102% Analysis Date = 09/30/12 Pct Recovery = 102% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/23/12 Pct Recovery = 103% Analysis Date = 09/23/12 Pct Recovery = 103% Analysis Date = 09/20/12 Pct Recovery = 103% Analysis Date = 09/20/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/13/12 Pct Recovery = 104% Analysis Date = 09/13/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 09/06/12 Pct Recovery = 104% Analysis Date = 09/06/12 Pct Recovery = 104% Analysis Date = 09/02/12 Pct Recovery = 104% Analysis Date = 09/02/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/22/12 Pct Recovery = 104% Analysis Date = 08/22/12 Pct Recovery = 104% Analysis Date = 08/19/12 Pct Recovery = 104% Analysis Date = 08/19/12 Pct Recovery = 104% Analysis Date = 08/15/12 Pct Recovery = 105% Analysis Date = 08/15/12 Pct Recovery = 105% Analysis Date = 08/12/12 Pct Recovery = 105% Analysis Date = 08/12/12 Pct Recovery = 105% Analysis Date = 08/08/12 Pct Recovery = 105% Analysis Date = 08/08/12 Pct Recovery = 105% Analysis Date = 08/05/12 Pct Recovery = 105% Analysis Date = 08/05/12 Pct Recovery = 105% Analysis Date = 08/01/12 Pct Recovery = 105% Analysis Date = 08/01/12 Pct Recovery = 105% Analysis Date = 07/29/12 Pct Recovery = 105% Analysis Date = 07/29/12 Pct Recovery = 105% Analysis Date = 07/25/12 Pct Recovery = 105% Analysis Date = 07/25/12 Pct Recovery = 105% Analysis Date = 07/21/12 Pct Recovery = 106% Analysis Date = 07/21/12 Pct Recovery = 106% Analysis Date = 07/18/12 Pct Recovery = 106% Analysis Date = 07/18/12 Pct Recovery = 106% Analysis Date = 07/14/12 Pct Recovery = 106% Analysis Date = 07/14/12 Pct Recovery = 106% Analysis Date = 07/11/12 Pct Recovery = 106% Analysis Date = 07/11/12 Pct Recovery = 106% Analysis Date = 07/07/12 Pct Recovery = 106% Analysis Date = 07/07/12 Pct Recovery = 106% Analysis Date = 07/04/12 Pct Recovery = 106% Analysis Date = 07/04/12 Pct Recovery = 106% Analysis Date = 06/30/12 Pct Recovery = 106% Analysis Date = 06/30/12 Pct Recovery = 106% Analysis Date = 06/27/12 Pct Recovery = 106% Analysis Date = 06/27/12 Pct Recovery = 106% Analysis Date = 06/23/12 Pct Recovery = 107% Analysis Date = 06/23/12 Pct Recovery = 107% Analysis Date = 06/19/12 Pct Recovery = 107% Analysis Date = 06/19/12 Pct Recovery = 107% Analysis Date = 06/16/12 Pct Recovery = 107% Analysis Date = 06/16/12 Pct Recovery = 107% Analysis Date = 06/12/12 Pct Recovery = 107% Analysis Date = 06/12/12 Pct Recovery = 107% Analysis Date = 06/09/12 Pct Recovery = 107% Analysis Date = 06/09/12 Pct Recovery = 107% Analysis Date = 06/05/12 Pct Recovery = 107% Analysis Date = 06/05/12 Pct Recovery = 107% Analysis Date = 06/02/12 Pct Recovery = 107% Analysis Date = 06/02/12 Pct Recovery = 107% Analysis Date = 05/29/12 Pct Recovery = 107% Analysis Date = 05/29/12 Pct Recovery = 107% Analysis Date = 05/26/12 Pct Recovery = 108% Analysis Date = 05/26/12 Pct Recovery = 108% Analysis Date = 05/22/12 Pct Recovery = 108% Analysis Date = 05/22/12 Pct Recovery = 108% Analysis Date = 05/19/12 Pct Recovery = 108% Analysis Date = 05/19/12 Pct Recovery = 108% Analysis Date = 05/15/12 Pct Recovery = 108% Analysis Date = 05/15/12 Pct Recovery = 108% Analysis Date = 05/11/12 Pct Recovery = 108% Analysis Date = 05/11/12 Pct Recovery = 108% Analysis Date = 05/08/12 Pct Recovery = 108% Analysis Date = 05/08/12 Pct Recovery = 108% Analysis Date = 05/04/12 Pct Recovery = 108% Analysis Date = 05/04/12 Pct Recovery = 108% Analysis Date = 05/01/12 Pct Recovery = 108% Analysis Date = 05/01/12 Pct Recovery = 108% Analysis Date = 04/27/12 Pct Recovery = 108% Analysis Date = 04/27/12 Pct Recovery = 108% Analysis Date = 04/24/12 Pct Recovery = 108% Analysis Date = 04/24/12 Pct Recovery = 108% Analysis Date = 04/20/12 Pct Recovery = 108% Analysis Date = 04/20/12 Pct Recovery = 108% Analysis Date = 04/17/12 Pct Recovery = 108% Analysis Date = 04/17/12 Pct Recovery = 108% Analysis Date = 04/13/12 Pct Recovery = 109% Analysis Date = 04/13/12 Pct Recovery = 109% Analysis Date = 04/10/12 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ANTIPYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 84% 0% 84% 0%
>= Reporting Level 32 87% 33% 76% 14%
Total 34 87% 32% 76% 11%

Sample Statistics
ANTIPYRENE

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 34
Not Spiked 54 .  
False Positives 0 0% 0 out of 54