OBSP Determination:
TAMOXIFEN
METHOD: LC9017 , TESTIDCODE: 68015LCM56

Analysis Date = 01/24/13 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl Pct Recovery = 7% Analysis Date = 01/24/13 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl Pct Recovery = 14% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TAMOXIFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 10% 5% 10% 6%
Total 2 10% 5% 10% 6%

Sample Statistics
TAMOXIFEN

Characteristic N % % Basis
Plotted 2 22% Spiked
Estimated Values 2 22% Spiked
Deleted Values 12 38% Spiked + Not Spiked
Spiked, Censored 2 22% Spiked
Spiked 14 .  
False Negatives 5 56% 5 out of 9
Not Spiked 18 .  
False Positives 0 0% 0 out of 11