OBSP Determination:
1-NAPHTHOL
METHOD: 2033 , TESTIDCODE: 49295GCM39

 Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 58%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 42%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 65%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 51%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 56%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 50%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 25%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 84%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 49%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 62%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 54%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 55%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 71%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 33%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 33%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 50%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 36%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 24%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 36%  Analysis Date = 05/10/17 
 Pct Recovery = 63%  Analysis Date = 05/08/17 
 Pct Recovery = 62%  Analysis Date = 05/08/17 
 Pct Recovery = 62%  Analysis Date = 05/06/17 
 Pct Recovery = 62%  Analysis Date = 05/06/17 
 Pct Recovery = 62%  Analysis Date = 05/04/17 
 Pct Recovery = 62%  Analysis Date = 05/04/17 
 Pct Recovery = 62%  Analysis Date = 05/01/17 
 Pct Recovery = 61%  Analysis Date = 05/01/17 
 Pct Recovery = 61%  Analysis Date = 04/29/17 
 Pct Recovery = 61%  Analysis Date = 04/29/17 
 Pct Recovery = 61%  Analysis Date = 04/27/17 
 Pct Recovery = 61%  Analysis Date = 04/27/17 
 Pct Recovery = 61%  Analysis Date = 04/25/17 
 Pct Recovery = 61%  Analysis Date = 04/25/17 
 Pct Recovery = 61%  Analysis Date = 04/22/17 
 Pct Recovery = 60%  Analysis Date = 04/22/17 
 Pct Recovery = 60%  Analysis Date = 04/20/17 
 Pct Recovery = 60%  Analysis Date = 04/20/17 
 Pct Recovery = 60%  Analysis Date = 04/18/17 
 Pct Recovery = 60%  Analysis Date = 04/18/17 
 Pct Recovery = 60%  Analysis Date = 04/15/17 
 Pct Recovery = 60%  Analysis Date = 04/15/17 
 Pct Recovery = 60%  Analysis Date = 04/13/17 
 Pct Recovery = 59%  Analysis Date = 04/13/17 
 Pct Recovery = 59%  Analysis Date = 04/11/17 
 Pct Recovery = 59%  Analysis Date = 04/11/17 
 Pct Recovery = 59%  Analysis Date = 04/09/17 
 Pct Recovery = 59%  Analysis Date = 04/09/17 
 Pct Recovery = 59%  Analysis Date = 04/06/17 
 Pct Recovery = 59%  Analysis Date = 04/06/17 
 Pct Recovery = 59%  Analysis Date = 04/04/17 
 Pct Recovery = 58%  Analysis Date = 04/04/17 
 Pct Recovery = 58%  Analysis Date = 04/02/17 
 Pct Recovery = 58%  Analysis Date = 04/02/17 
 Pct Recovery = 58%  Analysis Date = 03/30/17 
 Pct Recovery = 58%  Analysis Date = 03/30/17 
 Pct Recovery = 58%  Analysis Date = 03/28/17 
 Pct Recovery = 58%  Analysis Date = 03/28/17 
 Pct Recovery = 58%  Analysis Date = 03/26/17 
 Pct Recovery = 58%  Analysis Date = 03/26/17 
 Pct Recovery = 58%  Analysis Date = 03/24/17 
 Pct Recovery = 57%  Analysis Date = 03/24/17 
 Pct Recovery = 57%  Analysis Date = 03/21/17 
 Pct Recovery = 57%  Analysis Date = 03/21/17 
 Pct Recovery = 57%  Analysis Date = 03/19/17 
 Pct Recovery = 57%  Analysis Date = 03/19/17 
 Pct Recovery = 57%  Analysis Date = 03/17/17 
 Pct Recovery = 57%  Analysis Date = 03/17/17 
 Pct Recovery = 57%  Analysis Date = 03/14/17 
 Pct Recovery = 56%  Analysis Date = 03/14/17 
 Pct Recovery = 56%  Analysis Date = 03/12/17 
 Pct Recovery = 56%  Analysis Date = 03/12/17 
 Pct Recovery = 56%  Analysis Date = 03/10/17 
 Pct Recovery = 56%  Analysis Date = 03/10/17 
 Pct Recovery = 56%  Analysis Date = 03/08/17 
 Pct Recovery = 56%  Analysis Date = 03/08/17 
 Pct Recovery = 56%  Analysis Date = 03/05/17 
 Pct Recovery = 55%  Analysis Date = 03/05/17 
 Pct Recovery = 55%  Analysis Date = 03/03/17 
 Pct Recovery = 55%  Analysis Date = 03/03/17 
 Pct Recovery = 55%  Analysis Date = 03/01/17 
 Pct Recovery = 55%  Analysis Date = 03/01/17 
 Pct Recovery = 55%  Analysis Date = 02/26/17 
 Pct Recovery = 55%  Analysis Date = 02/26/17 
 Pct Recovery = 55%  Analysis Date = 02/24/17 
 Pct Recovery = 54%  Analysis Date = 02/24/17 
 Pct Recovery = 54%  Analysis Date = 02/22/17 
 Pct Recovery = 54%  Analysis Date = 02/22/17 
 Pct Recovery = 54%  Analysis Date = 02/20/17 
 Pct Recovery = 54%  Analysis Date = 02/20/17 
 Pct Recovery = 54%  Analysis Date = 02/17/17 
 Pct Recovery = 54%  Analysis Date = 02/17/17 
 Pct Recovery = 54%  Analysis Date = 02/15/17 
 Pct Recovery = 54%  Analysis Date = 02/15/17 
 Pct Recovery = 54%  Analysis Date = 02/13/17 
 Pct Recovery = 53%  Analysis Date = 02/13/17 
 Pct Recovery = 53%  Analysis Date = 02/10/17 
 Pct Recovery = 53%  Analysis Date = 02/10/17 
 Pct Recovery = 53%  Analysis Date = 02/08/17 
 Pct Recovery = 53%  Analysis Date = 02/08/17 
 Pct Recovery = 53%  Analysis Date = 02/06/17 
 Pct Recovery = 53%  Analysis Date = 02/06/17 
 Pct Recovery = 53%  Analysis Date = 02/04/17 
 Pct Recovery = 53%  Analysis Date = 02/04/17 
 Pct Recovery = 53%  Analysis Date = 02/01/17 
 Pct Recovery = 52%  Analysis Date = 02/01/17 
 Pct Recovery = 52%  Analysis Date = 01/30/17 
 Pct Recovery = 52%  Analysis Date = 01/30/17 
 Pct Recovery = 52%  Analysis Date = 01/28/17 
 Pct Recovery = 52%  Analysis Date = 01/28/17 
 Pct Recovery = 52%  Analysis Date = 01/25/17 
 Pct Recovery = 52%  Analysis Date = 01/25/17 
 Pct Recovery = 52%  Analysis Date = 01/23/17 
 Pct Recovery = 52%  Analysis Date = 01/23/17 
 Pct Recovery = 52%  Analysis Date = 01/21/17 
 Pct Recovery = 51%  Analysis Date = 01/21/17 
 Pct Recovery = 51%  Analysis Date = 01/19/17 
 Pct Recovery = 51%  Analysis Date = 01/19/17 
 Pct Recovery = 51%  Analysis Date = 01/16/17 
 Pct Recovery = 51%  Analysis Date = 01/16/17 
 Pct Recovery = 51%  Analysis Date = 01/14/17 
 Pct Recovery = 51%  Analysis Date = 01/14/17 
 Pct Recovery = 51%  Analysis Date = 01/12/17 
 Pct Recovery = 52%  Analysis Date = 01/12/17 
 Pct Recovery = 52%  Analysis Date = 01/09/17 
 Pct Recovery = 52%  Analysis Date = 01/09/17 
 Pct Recovery = 52%  Analysis Date = 01/07/17 
 Pct Recovery = 52%  Analysis Date = 01/07/17 
 Pct Recovery = 52%  Analysis Date = 01/05/17 
 Pct Recovery = 53%  Analysis Date = 01/05/17 
 Pct Recovery = 53%  Analysis Date = 01/03/17 
 Pct Recovery = 53%  Analysis Date = 01/03/17 
 Pct Recovery = 53%  Analysis Date = 12/31/16 
 Pct Recovery = 53%  Analysis Date = 12/31/16 
 Pct Recovery = 53%  Analysis Date = 12/29/16 
 Pct Recovery = 53%  Analysis Date = 12/29/16 
 Pct Recovery = 53%  Analysis Date = 12/27/16 
 Pct Recovery = 54%  Analysis Date = 12/27/16 
 Pct Recovery = 54%  Analysis Date = 12/24/16 
 Pct Recovery = 54%  Analysis Date = 12/24/16 
 Pct Recovery = 54%  Analysis Date = 12/22/16 
 Pct Recovery = 54%  Analysis Date = 12/22/16 
 Pct Recovery = 54%  Analysis Date = 12/20/16 
 Pct Recovery = 54%  Analysis Date = 12/20/16 
 Pct Recovery = 54%  Analysis Date = 12/18/16 
 Pct Recovery = 54%  Analysis Date = 12/18/16 
 Pct Recovery = 54%  Analysis Date = 12/15/16 
 Pct Recovery = 55%  Analysis Date = 12/15/16 
 Pct Recovery = 55%  Analysis Date = 12/13/16 
 Pct Recovery = 55%  Analysis Date = 12/13/16 
 Pct Recovery = 55%  Analysis Date = 12/11/16 
 Pct Recovery = 55%  Analysis Date = 12/11/16 
 Pct Recovery = 55%  Analysis Date = 12/08/16 
 Pct Recovery = 55%  Analysis Date = 12/08/16 
 Pct Recovery = 55%  Analysis Date = 12/06/16 
 Pct Recovery = 55%  Analysis Date = 12/06/16 
 Pct Recovery = 55%  Analysis Date = 12/04/16 
 Pct Recovery = 55%  Analysis Date = 12/04/16 
 Pct Recovery = 55%  Analysis Date = 12/02/16 
 Pct Recovery = 55%  Analysis Date = 12/02/16 
 Pct Recovery = 55%  Analysis Date = 11/29/16 
 Pct Recovery = 55%  Analysis Date = 11/29/16 
 Pct Recovery = 55%  Analysis Date = 11/27/16 
 Pct Recovery = 55%  Analysis Date = 11/27/16 
 Pct Recovery = 55%  Analysis Date = 11/25/16 
 Pct Recovery = 56%  Analysis Date = 11/25/16 
 Pct Recovery = 56%  Analysis Date = 11/22/16 
 Pct Recovery = 56%  Analysis Date = 11/22/16 
 Pct Recovery = 56%  Analysis Date = 11/20/16 
 Pct Recovery = 56%  Analysis Date = 11/20/16 
 Pct Recovery = 56%  Analysis Date = 11/18/16 
 Pct Recovery = 56%  Analysis Date = 11/18/16 
 Pct Recovery = 56%  Analysis Date = 11/16/16 
 Pct Recovery = 56%  Analysis Date = 11/16/16 
 Pct Recovery = 56%  Analysis Date = 11/13/16 
 Pct Recovery = 56%  Analysis Date = 11/13/16 
 Pct Recovery = 56%  Analysis Date = 11/11/16 
 Pct Recovery = 56%  Analysis Date = 11/11/16 
 Pct Recovery = 56%  Analysis Date = 11/09/16 
 Pct Recovery = 56%  Analysis Date = 11/09/16 
 Pct Recovery = 56%  Analysis Date = 11/06/16 
 Pct Recovery = 56%  Analysis Date = 11/06/16 
 Pct Recovery = 56%  Analysis Date = 11/04/16 
 Pct Recovery = 57%  Analysis Date = 11/04/16 
 Pct Recovery = 57%  Analysis Date = 11/02/16 
 Pct Recovery = 57%  Analysis Date = 11/02/16 
 Pct Recovery = 57%  Analysis Date = 10/31/16 
 Pct Recovery = 57%  Analysis Date = 10/31/16 
 Pct Recovery = 57%  Analysis Date = 10/28/16 
 Pct Recovery = 57%  Analysis Date = 10/28/16 
 Pct Recovery = 57%  Analysis Date = 10/26/16 
 Pct Recovery = 57%  Analysis Date = 10/26/16 
 Pct Recovery = 57%  Analysis Date = 10/24/16 
 Pct Recovery = 57%  Analysis Date = 10/24/16 
 Pct Recovery = 57%  Analysis Date = 10/21/16 
 Pct Recovery = 57%  Analysis Date = 10/21/16 
 Pct Recovery = 57%  Analysis Date = 10/19/16 
 Pct Recovery = 57%  Analysis Date = 10/19/16 
 Pct Recovery = 57%  Analysis Date = 10/17/16 
 Pct Recovery = 57%  Analysis Date = 10/17/16 
 Pct Recovery = 57%  Analysis Date = 10/15/16 
 Pct Recovery = 58%  Analysis Date = 10/15/16 
 Pct Recovery = 58%  Analysis Date = 10/12/16 
 Pct Recovery = 58%  Analysis Date = 10/12/16 
 Pct Recovery = 58%  Analysis Date = 10/10/16 
 Pct Recovery = 58%  Analysis Date = 10/10/16 
 Pct Recovery = 58%  Analysis Date = 10/08/16 
 Pct Recovery = 58%  Analysis Date = 10/08/16 
 Pct Recovery = 58%  Analysis Date = 10/05/16 
 Pct Recovery = 58%  Analysis Date = 10/05/16 
 Pct Recovery = 58%  Analysis Date = 10/03/16 
 Pct Recovery = 58%  Analysis Date = 10/03/16 
 Pct Recovery = 58%  Analysis Date = 10/01/16 
 Pct Recovery = 58%  Analysis Date = 10/01/16 
 Pct Recovery = 58%  Analysis Date = 09/29/16 
 Pct Recovery = 58%  Analysis Date = 09/29/16 
 Pct Recovery = 58%  Analysis Date = 09/26/16 
 Pct Recovery = 58%  Analysis Date = 09/26/16 
 Pct Recovery = 58%  Analysis Date = 09/24/16 
 Pct Recovery = 58%  Analysis Date = 09/24/16 
 Pct Recovery = 58%  Analysis Date = 09/22/16 
 Pct Recovery = 59%  Analysis Date = 09/22/16 
 Pct Recovery = 59%  Analysis Date = 09/19/16 
 Pct Recovery = 59%  Analysis Date = 09/19/16 
 Pct Recovery = 59%  Analysis Date = 09/17/16 
 Pct Recovery = 59%  Analysis Date = 09/17/16 
 Pct Recovery = 59%  Analysis Date = 09/15/16 
 Pct Recovery = 59%  Analysis Date = 09/15/16 
 Pct Recovery = 59%  Analysis Date = 09/13/16 
 Pct Recovery = 59%  Analysis Date = 09/13/16 
 Pct Recovery = 59%  Analysis Date = 09/10/16 
 Pct Recovery = 59%  Analysis Date = 09/10/16 
 Pct Recovery = 59%  Analysis Date = 09/08/16 
 Pct Recovery = 59%  Analysis Date = 09/08/16 
 Pct Recovery = 59%  Analysis Date = 09/06/16 
 Pct Recovery = 59%  Analysis Date = 09/06/16 
 Pct Recovery = 59%  Analysis Date = 09/03/16 
 Pct Recovery = 59%  Analysis Date = 09/03/16 
 Pct Recovery = 59%  Analysis Date = 09/01/16 
 Pct Recovery = 59%  Analysis Date = 09/01/16 
 Pct Recovery = 59%  Analysis Date = 08/30/16 
 Pct Recovery = 58%  Analysis Date = 08/30/16 
 Pct Recovery = 58%  Analysis Date = 08/28/16 
 Pct Recovery = 58%  Analysis Date = 08/28/16 
 Pct Recovery = 58%  Analysis Date = 08/25/16 
 Pct Recovery = 58%  Analysis Date = 08/25/16 
 Pct Recovery = 58%  Analysis Date = 08/23/16 
 Pct Recovery = 58%  Analysis Date = 08/23/16 
 Pct Recovery = 58%  Analysis Date = 08/21/16 
 Pct Recovery = 58%  Analysis Date = 08/21/16 
 Pct Recovery = 58%  Analysis Date = 08/18/16 
 Pct Recovery = 58%  Analysis Date = 08/18/16 
 Pct Recovery = 58%  Analysis Date = 08/16/16 
 Pct Recovery = 57%  Analysis Date = 08/16/16 
 Pct Recovery = 57%  Analysis Date = 08/14/16 
 Pct Recovery = 56%  Analysis Date = 08/14/16 
 Pct Recovery = 56%  Analysis Date = 08/12/16 
 Pct Recovery = 56%  Analysis Date = 08/12/16 
 Pct Recovery = 56%  Analysis Date = 08/09/16 
 Pct Recovery = 55%  Analysis Date = 08/09/16 
 Pct Recovery = 55%  Analysis Date = 08/07/16 
 Pct Recovery = 55%  Analysis Date = 08/07/16 
 Pct Recovery = 55%  Analysis Date = 08/05/16 
 Pct Recovery = 54%  Analysis Date = 08/05/16 
 Pct Recovery = 54%  Analysis Date = 08/02/16 
 Pct Recovery = 53%  Analysis Date = 08/02/16 
 Pct Recovery = 53%  Analysis Date = 07/31/16 
 Pct Recovery = 53%  Analysis Date = 07/31/16 
 Pct Recovery = 53%  Analysis Date = 07/29/16 
 Pct Recovery = 52%  Analysis Date = 07/29/16 
 Pct Recovery = 52%  Analysis Date = 07/27/16 
 Pct Recovery = 52%  Analysis Date = 07/27/16 
 Pct Recovery = 52%  Analysis Date = 07/24/16 
 Pct Recovery = 51%  Analysis Date = 07/24/16 
 Pct Recovery = 51%  Analysis Date = 07/22/16 
 Pct Recovery = 51%  Analysis Date = 07/22/16 
 Pct Recovery = 51%  Analysis Date = 07/20/16 
 Pct Recovery = 50%  Analysis Date = 07/20/16 
 Pct Recovery = 50%  Analysis Date = 07/17/16 
 Pct Recovery = 49%  Analysis Date = 07/17/16 
 Pct Recovery = 49%  Analysis Date = 07/15/16 
 Pct Recovery = 49%  Analysis Date = 07/15/16 
 Pct Recovery = 49%  Analysis Date = 07/13/16 
 Pct Recovery = 48%  Analysis Date = 07/13/16 
 Pct Recovery = 48%  Analysis Date = 07/11/16 
 Pct Recovery = 48%  Analysis Date = 07/11/16 
 Pct Recovery = 48%  Analysis Date = 07/08/16 
 Pct Recovery = 47%  Analysis Date = 07/08/16 
 Pct Recovery = 47%  Analysis Date = 07/06/16 
 Pct Recovery = 46%  Analysis Date = 07/06/16 
 Pct Recovery = 46%  Analysis Date = 07/04/16 
 Pct Recovery = 46%  Analysis Date = 07/04/16 
 Pct Recovery = 46%  Analysis Date = 07/01/16 
 Pct Recovery = 45%  Analysis Date = 07/01/16 
 Pct Recovery = 45%  Analysis Date = 06/29/16 
 Pct Recovery = 45%  Analysis Date = 06/29/16 
 Pct Recovery = 45%  Analysis Date = 06/27/16 
 Pct Recovery = 44%  Analysis Date = 06/27/16 
 Pct Recovery = 44%  Analysis Date = 06/25/16 
 Pct Recovery = 44%  Analysis Date = 06/25/16 
 Pct Recovery = 44%  Analysis Date = 06/22/16 
 Pct Recovery = 43%  Analysis Date = 06/22/16 
 Pct Recovery = 43%  Analysis Date = 06/20/16 
 Pct Recovery = 42%  Analysis Date = 06/20/16 
 Pct Recovery = 42%  Analysis Date = 06/18/16 
 Pct Recovery = 42%  Analysis Date = 06/18/16 
 Pct Recovery = 42%  Analysis Date = 06/15/16 
 Pct Recovery = 41%  Analysis Date = 06/15/16 
 Pct Recovery = 41%  Analysis Date = 06/13/16 
 Pct Recovery = 41%  Analysis Date = 06/13/16 
 Pct Recovery = 41%  Analysis Date = 06/11/16 
 Pct Recovery = 40%  Analysis Date = 06/11/16 
 Pct Recovery = 40%  Analysis Date = 06/09/16 
 Pct Recovery = 39%  Analysis Date = 06/09/16 
 Pct Recovery = 39%  Analysis Date = 06/06/16 
 Pct Recovery = 39%  Analysis Date = 06/06/16 
 Pct Recovery = 39%  Analysis Date = 06/04/16 
 Pct Recovery = 38%  Analysis Date = 06/04/16 
 Pct Recovery = 38%  Analysis Date = 06/02/16 
 Pct Recovery = 38%  Analysis Date = 06/02/16 
 Pct Recovery = 38%  Analysis Date = 05/30/16 
 Pct Recovery = 37%  Analysis Date = 05/30/16 
 Pct Recovery = 37%  Analysis Date = 05/28/16 
 Pct Recovery = 37%  Analysis Date = 05/28/16 
 Pct Recovery = 37%  Analysis Date = 05/26/16 
 Pct Recovery = 36%  Analysis Date = 05/26/16 
 Pct Recovery = 36%  Analysis Date = 05/24/16 
 Pct Recovery = 36%  Analysis Date = 05/24/16 
 Pct Recovery = 36%  Analysis Date = 05/21/16 
 Pct Recovery = 36%  Analysis Date = 05/21/16 
 Pct Recovery = 36%  Analysis Date = 05/19/16 
 Pct Recovery = 35%  Analysis Date = 05/19/16 
 Pct Recovery = 35%  Analysis Date = 05/17/16 
 Pct Recovery = 35%  Analysis Date = 05/17/16 
 Pct Recovery = 35%  Analysis Date = 05/14/16 
 Pct Recovery = 35%  Analysis Date = 05/14/16 
 Pct Recovery = 35%  Analysis Date = 05/12/16 
 Pct Recovery = 35%  Analysis Date = 05/12/16 
 Pct Recovery = 35%  Analysis Date = 05/10/16 
 Pct Recovery = 34%  Analysis Date = 05/10/16 
 Pct Recovery = 34%  Analysis Date = 05/08/16 
 Pct Recovery = 34%  Analysis Date = 05/08/16 
 Pct Recovery = 34%  Analysis Date = 05/05/16 
 Pct Recovery = 34%  Analysis Date = 05/05/16 
 Pct Recovery = 34%  Analysis Date = 05/03/16 
 Pct Recovery = 34%  Analysis Date = 05/03/16 
 Pct Recovery = 34%  Analysis Date = 05/01/16 
 Pct Recovery = 34%  Analysis Date = 05/01/16 
 Pct Recovery = 34%  Analysis Date = 04/28/16 
 Pct Recovery = 34%  Analysis Date = 04/28/16 
 Pct Recovery = 34%  Analysis Date = 04/26/16 
 Pct Recovery = 34%  Analysis Date = 04/26/16 
 Pct Recovery = 34%  Analysis Date = 04/24/16 
 Pct Recovery = 34%  Analysis Date = 04/24/16 
 Pct Recovery = 34%  Analysis Date = 04/22/16 
 Pct Recovery = 34%  Analysis Date = 04/22/16 
 Pct Recovery = 34%  Analysis Date = 04/19/16 
 Pct Recovery = 34%  Analysis Date = 04/19/16 
 Pct Recovery = 34%  Analysis Date = 04/17/16 
 Pct Recovery = 34%  Analysis Date = 04/17/16 
 Pct Recovery = 34%  Analysis Date = 04/15/16 
 Pct Recovery = 34%  Analysis Date = 04/15/16 
 Pct Recovery = 34%  Analysis Date = 04/12/16 
 Pct Recovery = 34%  Analysis Date = 04/12/16 
 Pct Recovery = 34%  Analysis Date = 04/10/16 
 Pct Recovery = 34%  Analysis Date = 04/10/16 
 Pct Recovery = 34%  Analysis Date = 04/08/16 
 Pct Recovery = 34%  Analysis Date = 04/08/16 
 Pct Recovery = 34%  Analysis Date = 04/06/16 
 Pct Recovery = 34%  Analysis Date = 04/06/16 
 Pct Recovery = 34%  Analysis Date = 04/03/16 
 Pct Recovery = 35%  Analysis Date = 04/03/16 
 Pct Recovery = 35%  Analysis Date = 04/01/16 
 Pct Recovery = 35%  Analysis Date = 04/01/16 
 Pct Recovery = 35%  Analysis Date = 03/30/16 
 Pct Recovery = 35%  Analysis Date = 03/30/16 
 Pct Recovery = 35%  Analysis Date = 03/27/16 
 Pct Recovery = 35%  Analysis Date = 03/27/16 
 Pct Recovery = 35%  Analysis Date = 03/25/16 
 Pct Recovery = 35%  Analysis Date = 03/25/16 
 Pct Recovery = 35%  Analysis Date = 03/23/16 
 Pct Recovery = 35%  Analysis Date = 03/23/16 
 Pct Recovery = 35%  Analysis Date = 03/21/16 
 Pct Recovery = 36%  Analysis Date = 03/21/16 
 Pct Recovery = 36%  Analysis Date = 03/18/16 
 Pct Recovery = 36%  Analysis Date = 03/18/16 
 Pct Recovery = 36%  Analysis Date = 03/16/16 
 Pct Recovery = 36%  Analysis Date = 03/16/16 
 Pct Recovery = 36%  Analysis Date = 03/14/16 
 Pct Recovery = 36%  Analysis Date = 03/14/16 
 Pct Recovery = 36%  Analysis Date = 03/11/16 
 Pct Recovery = 36%  Analysis Date = 03/11/16 
 Pct Recovery = 36%  Analysis Date = 03/09/16 
 Pct Recovery = 36%  Analysis Date = 03/09/16 
 Pct Recovery = 36%  Analysis Date = 03/07/16 
 Pct Recovery = 37%  Analysis Date = 03/07/16 
 Pct Recovery = 37%  Analysis Date = 03/05/16 
 Pct Recovery = 37%  Analysis Date = 03/05/16 
 Pct Recovery = 37%  Analysis Date = 03/02/16 
 Pct Recovery = 37%  Analysis Date = 03/02/16 
 Pct Recovery = 37%  Analysis Date = 02/29/16 
 Pct Recovery = 37%  Analysis Date = 02/29/16 
 Pct Recovery = 37%  Analysis Date = 02/27/16 
 Pct Recovery = 37%  Analysis Date = 02/27/16 
 Pct Recovery = 37%  Analysis Date = 02/24/16 
 Pct Recovery = 38%  Analysis Date = 02/24/16 
 Pct Recovery = 38%  Analysis Date = 02/22/16 
 Pct Recovery = 38%  Analysis Date = 02/22/16 
 Pct Recovery = 38%  Analysis Date = 02/20/16 
 Pct Recovery = 38%  Analysis Date = 02/20/16 
 Pct Recovery = 38%  Analysis Date = 02/18/16 
 Pct Recovery = 38%  Analysis Date = 02/18/16 
 Pct Recovery = 38%  Analysis Date = 02/15/16 
 Pct Recovery = 38%  Analysis Date = 02/15/16 
 Pct Recovery = 38%  Analysis Date = 02/13/16 
 Pct Recovery = 39%  Analysis Date = 02/13/16 
 Pct Recovery = 39%  Analysis Date = 02/11/16 
 Pct Recovery = 39%  Analysis Date = 02/11/16 
 Pct Recovery = 39%  Analysis Date = 02/09/16 
 Pct Recovery = 39%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-NAPHTHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 49% 16% 50% 16%
Total 19 49% 16% 50% 16%

Sample Statistics
1-NAPHTHOL

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 1 11% 1 out of 9

OBSP Determination:
2,6-DIETHYLANILINE
METHOD: 2033 , TESTIDCODE: 82660GCM35

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 105%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 92%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 109%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 85%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 69%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 102%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 91%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 92%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 79%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 91%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 82%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 108%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 97%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 104%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 101%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 94%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 89%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 82%  Analysis Date = 05/10/17 
 Pct Recovery = 85%  Analysis Date = 05/08/17 
 Pct Recovery = 86%  Analysis Date = 05/08/17 
 Pct Recovery = 86%  Analysis Date = 05/06/17 
 Pct Recovery = 86%  Analysis Date = 05/06/17 
 Pct Recovery = 86%  Analysis Date = 05/04/17 
 Pct Recovery = 87%  Analysis Date = 05/04/17 
 Pct Recovery = 87%  Analysis Date = 05/01/17 
 Pct Recovery = 87%  Analysis Date = 05/01/17 
 Pct Recovery = 87%  Analysis Date = 04/29/17 
 Pct Recovery = 88%  Analysis Date = 04/29/17 
 Pct Recovery = 88%  Analysis Date = 04/27/17 
 Pct Recovery = 88%  Analysis Date = 04/27/17 
 Pct Recovery = 88%  Analysis Date = 04/25/17 
 Pct Recovery = 89%  Analysis Date = 04/25/17 
 Pct Recovery = 89%  Analysis Date = 04/22/17 
 Pct Recovery = 89%  Analysis Date = 04/22/17 
 Pct Recovery = 89%  Analysis Date = 04/20/17 
 Pct Recovery = 90%  Analysis Date = 04/20/17 
 Pct Recovery = 90%  Analysis Date = 04/18/17 
 Pct Recovery = 90%  Analysis Date = 04/18/17 
 Pct Recovery = 90%  Analysis Date = 04/15/17 
 Pct Recovery = 91%  Analysis Date = 04/15/17 
 Pct Recovery = 91%  Analysis Date = 04/13/17 
 Pct Recovery = 91%  Analysis Date = 04/13/17 
 Pct Recovery = 91%  Analysis Date = 04/11/17 
 Pct Recovery = 91%  Analysis Date = 04/11/17 
 Pct Recovery = 91%  Analysis Date = 04/09/17 
 Pct Recovery = 92%  Analysis Date = 04/09/17 
 Pct Recovery = 92%  Analysis Date = 04/06/17 
 Pct Recovery = 92%  Analysis Date = 04/06/17 
 Pct Recovery = 92%  Analysis Date = 04/04/17 
 Pct Recovery = 93%  Analysis Date = 04/04/17 
 Pct Recovery = 93%  Analysis Date = 04/02/17 
 Pct Recovery = 93%  Analysis Date = 04/02/17 
 Pct Recovery = 93%  Analysis Date = 03/30/17 
 Pct Recovery = 94%  Analysis Date = 03/30/17 
 Pct Recovery = 94%  Analysis Date = 03/28/17 
 Pct Recovery = 94%  Analysis Date = 03/28/17 
 Pct Recovery = 94%  Analysis Date = 03/26/17 
 Pct Recovery = 95%  Analysis Date = 03/26/17 
 Pct Recovery = 95%  Analysis Date = 03/24/17 
 Pct Recovery = 95%  Analysis Date = 03/24/17 
 Pct Recovery = 95%  Analysis Date = 03/21/17 
 Pct Recovery = 96%  Analysis Date = 03/21/17 
 Pct Recovery = 96%  Analysis Date = 03/19/17 
 Pct Recovery = 96%  Analysis Date = 03/19/17 
 Pct Recovery = 96%  Analysis Date = 03/17/17 
 Pct Recovery = 97%  Analysis Date = 03/17/17 
 Pct Recovery = 97%  Analysis Date = 03/14/17 
 Pct Recovery = 97%  Analysis Date = 03/14/17 
 Pct Recovery = 97%  Analysis Date = 03/12/17 
 Pct Recovery = 97%  Analysis Date = 03/12/17 
 Pct Recovery = 97%  Analysis Date = 03/10/17 
 Pct Recovery = 98%  Analysis Date = 03/10/17 
 Pct Recovery = 98%  Analysis Date = 03/08/17 
 Pct Recovery = 98%  Analysis Date = 03/08/17 
 Pct Recovery = 98%  Analysis Date = 03/05/17 
 Pct Recovery = 99%  Analysis Date = 03/05/17 
 Pct Recovery = 99%  Analysis Date = 03/03/17 
 Pct Recovery = 99%  Analysis Date = 03/03/17 
 Pct Recovery = 99%  Analysis Date = 03/01/17 
 Pct Recovery = 100%  Analysis Date = 03/01/17 
 Pct Recovery = 100%  Analysis Date = 02/26/17 
 Pct Recovery = 100%  Analysis Date = 02/26/17 
 Pct Recovery = 100%  Analysis Date = 02/24/17 
 Pct Recovery = 100%  Analysis Date = 02/24/17 
 Pct Recovery = 100%  Analysis Date = 02/22/17 
 Pct Recovery = 101%  Analysis Date = 02/22/17 
 Pct Recovery = 101%  Analysis Date = 02/20/17 
 Pct Recovery = 101%  Analysis Date = 02/20/17 
 Pct Recovery = 101%  Analysis Date = 02/17/17 
 Pct Recovery = 101%  Analysis Date = 02/17/17 
 Pct Recovery = 101%  Analysis Date = 02/15/17 
 Pct Recovery = 101%  Analysis Date = 02/15/17 
 Pct Recovery = 101%  Analysis Date = 02/13/17 
 Pct Recovery = 101%  Analysis Date = 02/13/17 
 Pct Recovery = 101%  Analysis Date = 02/10/17 
 Pct Recovery = 101%  Analysis Date = 02/10/17 
 Pct Recovery = 101%  Analysis Date = 02/08/17 
 Pct Recovery = 101%  Analysis Date = 02/08/17 
 Pct Recovery = 101%  Analysis Date = 02/06/17 
 Pct Recovery = 101%  Analysis Date = 02/06/17 
 Pct Recovery = 101%  Analysis Date = 02/04/17 
 Pct Recovery = 101%  Analysis Date = 02/04/17 
 Pct Recovery = 101%  Analysis Date = 02/01/17 
 Pct Recovery = 101%  Analysis Date = 02/01/17 
 Pct Recovery = 101%  Analysis Date = 01/30/17 
 Pct Recovery = 101%  Analysis Date = 01/30/17 
 Pct Recovery = 101%  Analysis Date = 01/28/17 
 Pct Recovery = 101%  Analysis Date = 01/28/17 
 Pct Recovery = 101%  Analysis Date = 01/25/17 
 Pct Recovery = 101%  Analysis Date = 01/25/17 
 Pct Recovery = 101%  Analysis Date = 01/23/17 
 Pct Recovery = 102%  Analysis Date = 01/23/17 
 Pct Recovery = 102%  Analysis Date = 01/21/17 
 Pct Recovery = 102%  Analysis Date = 01/21/17 
 Pct Recovery = 102%  Analysis Date = 01/19/17 
 Pct Recovery = 102%  Analysis Date = 01/19/17 
 Pct Recovery = 102%  Analysis Date = 01/16/17 
 Pct Recovery = 101%  Analysis Date = 01/16/17 
 Pct Recovery = 101%  Analysis Date = 01/14/17 
 Pct Recovery = 101%  Analysis Date = 01/14/17 
 Pct Recovery = 101%  Analysis Date = 01/12/17 
 Pct Recovery = 101%  Analysis Date = 01/12/17 
 Pct Recovery = 101%  Analysis Date = 01/09/17 
 Pct Recovery = 101%  Analysis Date = 01/09/17 
 Pct Recovery = 101%  Analysis Date = 01/07/17 
 Pct Recovery = 101%  Analysis Date = 01/07/17 
 Pct Recovery = 101%  Analysis Date = 01/05/17 
 Pct Recovery = 100%  Analysis Date = 01/05/17 
 Pct Recovery = 100%  Analysis Date = 01/03/17 
 Pct Recovery = 100%  Analysis Date = 01/03/17 
 Pct Recovery = 100%  Analysis Date = 12/31/16 
 Pct Recovery = 100%  Analysis Date = 12/31/16 
 Pct Recovery = 100%  Analysis Date = 12/29/16 
 Pct Recovery = 100%  Analysis Date = 12/29/16 
 Pct Recovery = 100%  Analysis Date = 12/27/16 
 Pct Recovery = 99%  Analysis Date = 12/27/16 
 Pct Recovery = 99%  Analysis Date = 12/24/16 
 Pct Recovery = 99%  Analysis Date = 12/24/16 
 Pct Recovery = 99%  Analysis Date = 12/22/16 
 Pct Recovery = 99%  Analysis Date = 12/22/16 
 Pct Recovery = 99%  Analysis Date = 12/20/16 
 Pct Recovery = 99%  Analysis Date = 12/20/16 
 Pct Recovery = 99%  Analysis Date = 12/18/16 
 Pct Recovery = 98%  Analysis Date = 12/18/16 
 Pct Recovery = 98%  Analysis Date = 12/15/16 
 Pct Recovery = 98%  Analysis Date = 12/15/16 
 Pct Recovery = 98%  Analysis Date = 12/13/16 
 Pct Recovery = 98%  Analysis Date = 12/13/16 
 Pct Recovery = 98%  Analysis Date = 12/11/16 
 Pct Recovery = 98%  Analysis Date = 12/11/16 
 Pct Recovery = 98%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/06/16 
 Pct Recovery = 97%  Analysis Date = 12/06/16 
 Pct Recovery = 97%  Analysis Date = 12/04/16 
 Pct Recovery = 97%  Analysis Date = 12/04/16 
 Pct Recovery = 97%  Analysis Date = 12/02/16 
 Pct Recovery = 97%  Analysis Date = 12/02/16 
 Pct Recovery = 97%  Analysis Date = 11/29/16 
 Pct Recovery = 97%  Analysis Date = 11/29/16 
 Pct Recovery = 97%  Analysis Date = 11/27/16 
 Pct Recovery = 96%  Analysis Date = 11/27/16 
 Pct Recovery = 96%  Analysis Date = 11/25/16 
 Pct Recovery = 96%  Analysis Date = 11/25/16 
 Pct Recovery = 96%  Analysis Date = 11/22/16 
 Pct Recovery = 96%  Analysis Date = 11/22/16 
 Pct Recovery = 96%  Analysis Date = 11/20/16 
 Pct Recovery = 96%  Analysis Date = 11/20/16 
 Pct Recovery = 96%  Analysis Date = 11/18/16 
 Pct Recovery = 95%  Analysis Date = 11/18/16 
 Pct Recovery = 95%  Analysis Date = 11/16/16 
 Pct Recovery = 95%  Analysis Date = 11/16/16 
 Pct Recovery = 95%  Analysis Date = 11/13/16 
 Pct Recovery = 95%  Analysis Date = 11/13/16 
 Pct Recovery = 95%  Analysis Date = 11/11/16 
 Pct Recovery = 95%  Analysis Date = 11/11/16 
 Pct Recovery = 95%  Analysis Date = 11/09/16 
 Pct Recovery = 94%  Analysis Date = 11/09/16 
 Pct Recovery = 94%  Analysis Date = 11/06/16 
 Pct Recovery = 94%  Analysis Date = 11/06/16 
 Pct Recovery = 94%  Analysis Date = 11/04/16 
 Pct Recovery = 94%  Analysis Date = 11/04/16 
 Pct Recovery = 94%  Analysis Date = 11/02/16 
 Pct Recovery = 94%  Analysis Date = 11/02/16 
 Pct Recovery = 94%  Analysis Date = 10/31/16 
 Pct Recovery = 93%  Analysis Date = 10/31/16 
 Pct Recovery = 93%  Analysis Date = 10/28/16 
 Pct Recovery = 93%  Analysis Date = 10/28/16 
 Pct Recovery = 93%  Analysis Date = 10/26/16 
 Pct Recovery = 93%  Analysis Date = 10/26/16 
 Pct Recovery = 93%  Analysis Date = 10/24/16 
 Pct Recovery = 93%  Analysis Date = 10/24/16 
 Pct Recovery = 93%  Analysis Date = 10/21/16 
 Pct Recovery = 93%  Analysis Date = 10/21/16 
 Pct Recovery = 93%  Analysis Date = 10/19/16 
 Pct Recovery = 92%  Analysis Date = 10/19/16 
 Pct Recovery = 92%  Analysis Date = 10/17/16 
 Pct Recovery = 92%  Analysis Date = 10/17/16 
 Pct Recovery = 92%  Analysis Date = 10/15/16 
 Pct Recovery = 92%  Analysis Date = 10/15/16 
 Pct Recovery = 92%  Analysis Date = 10/12/16 
 Pct Recovery = 92%  Analysis Date = 10/12/16 
 Pct Recovery = 92%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/08/16 
 Pct Recovery = 91%  Analysis Date = 10/08/16 
 Pct Recovery = 91%  Analysis Date = 10/05/16 
 Pct Recovery = 91%  Analysis Date = 10/05/16 
 Pct Recovery = 91%  Analysis Date = 10/03/16 
 Pct Recovery = 91%  Analysis Date = 10/03/16 
 Pct Recovery = 91%  Analysis Date = 10/01/16 
 Pct Recovery = 90%  Analysis Date = 10/01/16 
 Pct Recovery = 90%  Analysis Date = 09/29/16 
 Pct Recovery = 90%  Analysis Date = 09/29/16 
 Pct Recovery = 90%  Analysis Date = 09/26/16 
 Pct Recovery = 90%  Analysis Date = 09/26/16 
 Pct Recovery = 90%  Analysis Date = 09/24/16 
 Pct Recovery = 90%  Analysis Date = 09/24/16 
 Pct Recovery = 90%  Analysis Date = 09/22/16 
 Pct Recovery = 89%  Analysis Date = 09/22/16 
 Pct Recovery = 89%  Analysis Date = 09/19/16 
 Pct Recovery = 89%  Analysis Date = 09/19/16 
 Pct Recovery = 89%  Analysis Date = 09/17/16 
 Pct Recovery = 89%  Analysis Date = 09/17/16 
 Pct Recovery = 89%  Analysis Date = 09/15/16 
 Pct Recovery = 89%  Analysis Date = 09/15/16 
 Pct Recovery = 89%  Analysis Date = 09/13/16 
 Pct Recovery = 89%  Analysis Date = 09/13/16 
 Pct Recovery = 89%  Analysis Date = 09/10/16 
 Pct Recovery = 89%  Analysis Date = 09/10/16 
 Pct Recovery = 89%  Analysis Date = 09/08/16 
 Pct Recovery = 89%  Analysis Date = 09/08/16 
 Pct Recovery = 89%  Analysis Date = 09/06/16 
 Pct Recovery = 89%  Analysis Date = 09/06/16 
 Pct Recovery = 89%  Analysis Date = 09/03/16 
 Pct Recovery = 89%  Analysis Date = 09/03/16 
 Pct Recovery = 89%  Analysis Date = 09/01/16 
 Pct Recovery = 89%  Analysis Date = 09/01/16 
 Pct Recovery = 89%  Analysis Date = 08/30/16 
 Pct Recovery = 89%  Analysis Date = 08/30/16 
 Pct Recovery = 89%  Analysis Date = 08/28/16 
 Pct Recovery = 89%  Analysis Date = 08/28/16 
 Pct Recovery = 89%  Analysis Date = 08/25/16 
 Pct Recovery = 89%  Analysis Date = 08/25/16 
 Pct Recovery = 89%  Analysis Date = 08/23/16 
 Pct Recovery = 89%  Analysis Date = 08/23/16 
 Pct Recovery = 89%  Analysis Date = 08/21/16 
 Pct Recovery = 89%  Analysis Date = 08/21/16 
 Pct Recovery = 89%  Analysis Date = 08/18/16 
 Pct Recovery = 89%  Analysis Date = 08/18/16 
 Pct Recovery = 89%  Analysis Date = 08/16/16 
 Pct Recovery = 89%  Analysis Date = 08/16/16 
 Pct Recovery = 89%  Analysis Date = 08/14/16 
 Pct Recovery = 89%  Analysis Date = 08/14/16 
 Pct Recovery = 89%  Analysis Date = 08/12/16 
 Pct Recovery = 90%  Analysis Date = 08/12/16 
 Pct Recovery = 90%  Analysis Date = 08/09/16 
 Pct Recovery = 90%  Analysis Date = 08/09/16 
 Pct Recovery = 90%  Analysis Date = 08/07/16 
 Pct Recovery = 90%  Analysis Date = 08/07/16 
 Pct Recovery = 90%  Analysis Date = 08/05/16 
 Pct Recovery = 90%  Analysis Date = 08/05/16 
 Pct Recovery = 90%  Analysis Date = 08/02/16 
 Pct Recovery = 90%  Analysis Date = 08/02/16 
 Pct Recovery = 90%  Analysis Date = 07/31/16 
 Pct Recovery = 90%  Analysis Date = 07/31/16 
 Pct Recovery = 90%  Analysis Date = 07/29/16 
 Pct Recovery = 90%  Analysis Date = 07/29/16 
 Pct Recovery = 90%  Analysis Date = 07/27/16 
 Pct Recovery = 90%  Analysis Date = 07/27/16 
 Pct Recovery = 90%  Analysis Date = 07/24/16 
 Pct Recovery = 90%  Analysis Date = 07/24/16 
 Pct Recovery = 90%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/22/16 
 Pct Recovery = 90%  Analysis Date = 07/20/16 
 Pct Recovery = 90%  Analysis Date = 07/20/16 
 Pct Recovery = 90%  Analysis Date = 07/17/16 
 Pct Recovery = 91%  Analysis Date = 07/17/16 
 Pct Recovery = 91%  Analysis Date = 07/15/16 
 Pct Recovery = 91%  Analysis Date = 07/15/16 
 Pct Recovery = 91%  Analysis Date = 07/13/16 
 Pct Recovery = 91%  Analysis Date = 07/13/16 
 Pct Recovery = 91%  Analysis Date = 07/11/16 
 Pct Recovery = 91%  Analysis Date = 07/11/16 
 Pct Recovery = 91%  Analysis Date = 07/08/16 
 Pct Recovery = 91%  Analysis Date = 07/08/16 
 Pct Recovery = 91%  Analysis Date = 07/06/16 
 Pct Recovery = 91%  Analysis Date = 07/06/16 
 Pct Recovery = 91%  Analysis Date = 07/04/16 
 Pct Recovery = 91%  Analysis Date = 07/04/16 
 Pct Recovery = 91%  Analysis Date = 07/01/16 
 Pct Recovery = 91%  Analysis Date = 07/01/16 
 Pct Recovery = 91%  Analysis Date = 06/29/16 
 Pct Recovery = 91%  Analysis Date = 06/29/16 
 Pct Recovery = 91%  Analysis Date = 06/27/16 
 Pct Recovery = 91%  Analysis Date = 06/27/16 
 Pct Recovery = 91%  Analysis Date = 06/25/16 
 Pct Recovery = 91%  Analysis Date = 06/25/16 
 Pct Recovery = 91%  Analysis Date = 06/22/16 
 Pct Recovery = 92%  Analysis Date = 06/22/16 
 Pct Recovery = 92%  Analysis Date = 06/20/16 
 Pct Recovery = 92%  Analysis Date = 06/20/16 
 Pct Recovery = 92%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/15/16 
 Pct Recovery = 92%  Analysis Date = 06/13/16 
 Pct Recovery = 92%  Analysis Date = 06/13/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/09/16 
 Pct Recovery = 92%  Analysis Date = 06/09/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/04/16 
 Pct Recovery = 92%  Analysis Date = 06/04/16 
 Pct Recovery = 92%  Analysis Date = 06/02/16 
 Pct Recovery = 92%  Analysis Date = 06/02/16 
 Pct Recovery = 92%  Analysis Date = 05/30/16 
 Pct Recovery = 92%  Analysis Date = 05/30/16 
 Pct Recovery = 92%  Analysis Date = 05/28/16 
 Pct Recovery = 93%  Analysis Date = 05/28/16 
 Pct Recovery = 93%  Analysis Date = 05/26/16 
 Pct Recovery = 93%  Analysis Date = 05/26/16 
 Pct Recovery = 93%  Analysis Date = 05/24/16 
 Pct Recovery = 93%  Analysis Date = 05/24/16 
 Pct Recovery = 93%  Analysis Date = 05/21/16 
 Pct Recovery = 93%  Analysis Date = 05/21/16 
 Pct Recovery = 93%  Analysis Date = 05/19/16 
 Pct Recovery = 93%  Analysis Date = 05/19/16 
 Pct Recovery = 93%  Analysis Date = 05/17/16 
 Pct Recovery = 93%  Analysis Date = 05/17/16 
 Pct Recovery = 93%  Analysis Date = 05/14/16 
 Pct Recovery = 93%  Analysis Date = 05/14/16 
 Pct Recovery = 93%  Analysis Date = 05/12/16 
 Pct Recovery = 93%  Analysis Date = 05/12/16 
 Pct Recovery = 93%  Analysis Date = 05/10/16 
 Pct Recovery = 93%  Analysis Date = 05/10/16 
 Pct Recovery = 93%  Analysis Date = 05/08/16 
 Pct Recovery = 93%  Analysis Date = 05/08/16 
 Pct Recovery = 93%  Analysis Date = 05/05/16 
 Pct Recovery = 93%  Analysis Date = 05/05/16 
 Pct Recovery = 93%  Analysis Date = 05/03/16 
 Pct Recovery = 93%  Analysis Date = 05/03/16 
 Pct Recovery = 93%  Analysis Date = 05/01/16 
 Pct Recovery = 93%  Analysis Date = 05/01/16 
 Pct Recovery = 93%  Analysis Date = 04/28/16 
 Pct Recovery = 93%  Analysis Date = 04/28/16 
 Pct Recovery = 93%  Analysis Date = 04/26/16 
 Pct Recovery = 93%  Analysis Date = 04/26/16 
 Pct Recovery = 93%  Analysis Date = 04/24/16 
 Pct Recovery = 93%  Analysis Date = 04/24/16 
 Pct Recovery = 93%  Analysis Date = 04/22/16 
 Pct Recovery = 93%  Analysis Date = 04/22/16 
 Pct Recovery = 93%  Analysis Date = 04/19/16 
 Pct Recovery = 93%  Analysis Date = 04/19/16 
 Pct Recovery = 93%  Analysis Date = 04/17/16 
 Pct Recovery = 93%  Analysis Date = 04/17/16 
 Pct Recovery = 93%  Analysis Date = 04/15/16 
 Pct Recovery = 93%  Analysis Date = 04/15/16 
 Pct Recovery = 93%  Analysis Date = 04/12/16 
 Pct Recovery = 93%  Analysis Date = 04/12/16 
 Pct Recovery = 93%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/08/16 
 Pct Recovery = 92%  Analysis Date = 04/08/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/03/16 
 Pct Recovery = 92%  Analysis Date = 04/03/16 
 Pct Recovery = 92%  Analysis Date = 04/01/16 
 Pct Recovery = 92%  Analysis Date = 04/01/16 
 Pct Recovery = 92%  Analysis Date = 03/30/16 
 Pct Recovery = 91%  Analysis Date = 03/30/16 
 Pct Recovery = 91%  Analysis Date = 03/27/16 
 Pct Recovery = 91%  Analysis Date = 03/27/16 
 Pct Recovery = 91%  Analysis Date = 03/25/16 
 Pct Recovery = 91%  Analysis Date = 03/25/16 
 Pct Recovery = 91%  Analysis Date = 03/23/16 
 Pct Recovery = 91%  Analysis Date = 03/23/16 
 Pct Recovery = 91%  Analysis Date = 03/21/16 
 Pct Recovery = 91%  Analysis Date = 03/21/16 
 Pct Recovery = 91%  Analysis Date = 03/18/16 
 Pct Recovery = 90%  Analysis Date = 03/18/16 
 Pct Recovery = 90%  Analysis Date = 03/16/16 
 Pct Recovery = 90%  Analysis Date = 03/16/16 
 Pct Recovery = 90%  Analysis Date = 03/14/16 
 Pct Recovery = 90%  Analysis Date = 03/14/16 
 Pct Recovery = 90%  Analysis Date = 03/11/16 
 Pct Recovery = 90%  Analysis Date = 03/11/16 
 Pct Recovery = 90%  Analysis Date = 03/09/16 
 Pct Recovery = 89%  Analysis Date = 03/09/16 
 Pct Recovery = 89%  Analysis Date = 03/07/16 
 Pct Recovery = 89%  Analysis Date = 03/07/16 
 Pct Recovery = 89%  Analysis Date = 03/05/16 
 Pct Recovery = 89%  Analysis Date = 03/05/16 
 Pct Recovery = 89%  Analysis Date = 03/02/16 
 Pct Recovery = 89%  Analysis Date = 03/02/16 
 Pct Recovery = 89%  Analysis Date = 02/29/16 
 Pct Recovery = 88%  Analysis Date = 02/29/16 
 Pct Recovery = 88%  Analysis Date = 02/27/16 
 Pct Recovery = 88%  Analysis Date = 02/27/16 
 Pct Recovery = 88%  Analysis Date = 02/24/16 
 Pct Recovery = 88%  Analysis Date = 02/24/16 
 Pct Recovery = 88%  Analysis Date = 02/22/16 
 Pct Recovery = 87%  Analysis Date = 02/22/16 
 Pct Recovery = 87%  Analysis Date = 02/20/16 
 Pct Recovery = 87%  Analysis Date = 02/20/16 
 Pct Recovery = 87%  Analysis Date = 02/18/16 
 Pct Recovery = 87%  Analysis Date = 02/18/16 
 Pct Recovery = 87%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/15/16 
 Pct Recovery = 86%  Analysis Date = 02/13/16 
 Pct Recovery = 86%  Analysis Date = 02/13/16 
 Pct Recovery = 86%  Analysis Date = 02/11/16 
 Pct Recovery = 86%  Analysis Date = 02/11/16 
 Pct Recovery = 86%  Analysis Date = 02/09/16 
 Pct Recovery = 85%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,6-DIETHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 93% 11% 92% 13%
Total 18 93% 11% 92% 13%

Sample Statistics
2,6-DIETHYLANILINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
2-CHLORO-2,6-DIETHYLACETANILIDE
METHOD: 2033 , TESTIDCODE: 61618GCM39

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 111%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 98%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 97%  Analysis Date = 04/19/16 
 SpikeMix = ERA 0406-15-01: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 84%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 80%  Analysis Date = 05/19/16 
 SpikeMix = ChemService 3851600: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 91%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 93%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 131%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 95%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 111%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 86%  Analysis Date = 05/02/17 
 Pct Recovery = 95%  Analysis Date = 04/30/17 
 Pct Recovery = 96%  Analysis Date = 04/30/17 
 Pct Recovery = 96%  Analysis Date = 04/28/17 
 Pct Recovery = 97%  Analysis Date = 04/28/17 
 Pct Recovery = 97%  Analysis Date = 04/26/17 
 Pct Recovery = 99%  Analysis Date = 04/26/17 
 Pct Recovery = 99%  Analysis Date = 04/24/17 
 Pct Recovery = 100%  Analysis Date = 04/24/17 
 Pct Recovery = 100%  Analysis Date = 04/22/17 
 Pct Recovery = 102%  Analysis Date = 04/22/17 
 Pct Recovery = 102%  Analysis Date = 04/20/17 
 Pct Recovery = 103%  Analysis Date = 04/20/17 
 Pct Recovery = 103%  Analysis Date = 04/18/17 
 Pct Recovery = 104%  Analysis Date = 04/18/17 
 Pct Recovery = 104%  Analysis Date = 04/15/17 
 Pct Recovery = 106%  Analysis Date = 04/15/17 
 Pct Recovery = 106%  Analysis Date = 04/13/17 
 Pct Recovery = 107%  Analysis Date = 04/13/17 
 Pct Recovery = 107%  Analysis Date = 04/11/17 
 Pct Recovery = 109%  Analysis Date = 04/11/17 
 Pct Recovery = 109%  Analysis Date = 04/09/17 
 Pct Recovery = 110%  Analysis Date = 04/09/17 
 Pct Recovery = 110%  Analysis Date = 04/07/17 
 Pct Recovery = 111%  Analysis Date = 04/07/17 
 Pct Recovery = 111%  Analysis Date = 04/05/17 
 Pct Recovery = 113%  Analysis Date = 04/05/17 
 Pct Recovery = 113%  Analysis Date = 04/03/17 
 Pct Recovery = 114%  Analysis Date = 04/03/17 
 Pct Recovery = 114%  Analysis Date = 03/31/17 
 Pct Recovery = 116%  Analysis Date = 03/31/17 
 Pct Recovery = 116%  Analysis Date = 03/29/17 
 Pct Recovery = 117%  Analysis Date = 03/29/17 
 Pct Recovery = 117%  Analysis Date = 03/27/17 
 Pct Recovery = 118%  Analysis Date = 03/27/17 
 Pct Recovery = 118%  Analysis Date = 03/25/17 
 Pct Recovery = 120%  Analysis Date = 03/25/17 
 Pct Recovery = 120%  Analysis Date = 03/23/17 
 Pct Recovery = 121%  Analysis Date = 03/23/17 
 Pct Recovery = 121%  Analysis Date = 03/21/17 
 Pct Recovery = 123%  Analysis Date = 03/21/17 
 Pct Recovery = 123%  Analysis Date = 03/19/17 
 Pct Recovery = 124%  Analysis Date = 03/19/17 
 Pct Recovery = 124%  Analysis Date = 03/17/17 
 Pct Recovery = 125%  Analysis Date = 03/17/17 
 Pct Recovery = 125%  Analysis Date = 03/14/17 
 Pct Recovery = 125%  Analysis Date = 03/14/17 
 Pct Recovery = 125%  Analysis Date = 03/12/17 
 Pct Recovery = 122%  Analysis Date = 03/12/17 
 Pct Recovery = 122%  Analysis Date = 03/10/17 
 Pct Recovery = 120%  Analysis Date = 03/10/17 
 Pct Recovery = 120%  Analysis Date = 03/08/17 
 Pct Recovery = 117%  Analysis Date = 03/08/17 
 Pct Recovery = 117%  Analysis Date = 03/06/17 
 Pct Recovery = 115%  Analysis Date = 03/06/17 
 Pct Recovery = 115%  Analysis Date = 03/04/17 
 Pct Recovery = 112%  Analysis Date = 03/04/17 
 Pct Recovery = 112%  Analysis Date = 03/02/17 
 Pct Recovery = 110%  Analysis Date = 03/02/17 
 Pct Recovery = 110%  Analysis Date = 02/27/17 
 Pct Recovery = 107%  Analysis Date = 02/27/17 
 Pct Recovery = 107%  Analysis Date = 02/25/17 
 Pct Recovery = 105%  Analysis Date = 02/25/17 
 Pct Recovery = 105%  Analysis Date = 02/23/17 
 Pct Recovery = 102%  Analysis Date = 02/23/17 
 Pct Recovery = 102%  Analysis Date = 02/21/17 
 Pct Recovery = 100%  Analysis Date = 02/21/17 
 Pct Recovery = 100%  Analysis Date = 02/19/17 
 Pct Recovery = 98%  Analysis Date = 02/19/17 
 Pct Recovery = 98%  Analysis Date = 02/17/17 
 Pct Recovery = 96%  Analysis Date = 02/17/17 
 Pct Recovery = 96%  Analysis Date = 02/15/17 
 Pct Recovery = 95%  Analysis Date = 02/15/17 
 Pct Recovery = 95%  Analysis Date = 02/13/17 
 Pct Recovery = 96%  Analysis Date = 02/13/17 
 Pct Recovery = 96%  Analysis Date = 02/10/17 
 Pct Recovery = 96%  Analysis Date = 02/10/17 
 Pct Recovery = 96%  Analysis Date = 02/08/17 
 Pct Recovery = 97%  Analysis Date = 02/08/17 
 Pct Recovery = 97%  Analysis Date = 02/06/17 
 Pct Recovery = 97%  Analysis Date = 02/06/17 
 Pct Recovery = 97%  Analysis Date = 02/04/17 
 Pct Recovery = 98%  Analysis Date = 02/04/17 
 Pct Recovery = 98%  Analysis Date = 02/02/17 
 Pct Recovery = 98%  Analysis Date = 02/02/17 
 Pct Recovery = 98%  Analysis Date = 01/31/17 
 Pct Recovery = 99%  Analysis Date = 01/31/17 
 Pct Recovery = 99%  Analysis Date = 01/29/17 
 Pct Recovery = 100%  Analysis Date = 01/29/17 
 Pct Recovery = 100%  Analysis Date = 01/26/17 
 Pct Recovery = 100%  Analysis Date = 01/26/17 
 Pct Recovery = 100%  Analysis Date = 01/24/17 
 Pct Recovery = 101%  Analysis Date = 01/24/17 
 Pct Recovery = 101%  Analysis Date = 01/22/17 
 Pct Recovery = 101%  Analysis Date = 01/22/17 
 Pct Recovery = 101%  Analysis Date = 01/20/17 
 Pct Recovery = 102%  Analysis Date = 01/20/17 
 Pct Recovery = 102%  Analysis Date = 01/18/17 
 Pct Recovery = 103%  Analysis Date = 01/18/17 
 Pct Recovery = 103%  Analysis Date = 01/16/17 
 Pct Recovery = 103%  Analysis Date = 01/16/17 
 Pct Recovery = 103%  Analysis Date = 01/14/17 
 Pct Recovery = 104%  Analysis Date = 01/14/17 
 Pct Recovery = 104%  Analysis Date = 01/11/17 
 Pct Recovery = 104%  Analysis Date = 01/11/17 
 Pct Recovery = 104%  Analysis Date = 01/09/17 
 Pct Recovery = 105%  Analysis Date = 01/09/17 
 Pct Recovery = 105%  Analysis Date = 01/07/17 
 Pct Recovery = 106%  Analysis Date = 01/07/17 
 Pct Recovery = 106%  Analysis Date = 01/05/17 
 Pct Recovery = 106%  Analysis Date = 01/05/17 
 Pct Recovery = 106%  Analysis Date = 01/03/17 
 Pct Recovery = 107%  Analysis Date = 01/03/17 
 Pct Recovery = 107%  Analysis Date = 01/01/17 
 Pct Recovery = 107%  Analysis Date = 01/01/17 
 Pct Recovery = 107%  Analysis Date = 12/30/16 
 Pct Recovery = 108%  Analysis Date = 12/30/16 
 Pct Recovery = 108%  Analysis Date = 12/28/16 
 Pct Recovery = 108%  Analysis Date = 12/28/16 
 Pct Recovery = 108%  Analysis Date = 12/25/16 
 Pct Recovery = 109%  Analysis Date = 12/25/16 
 Pct Recovery = 109%  Analysis Date = 12/23/16 
 Pct Recovery = 110%  Analysis Date = 12/23/16 
 Pct Recovery = 110%  Analysis Date = 12/21/16 
 Pct Recovery = 110%  Analysis Date = 12/21/16 
 Pct Recovery = 110%  Analysis Date = 12/19/16 
 Pct Recovery = 111%  Analysis Date = 12/19/16 
 Pct Recovery = 111%  Analysis Date = 12/17/16 
 Pct Recovery = 110%  Analysis Date = 12/17/16 
 Pct Recovery = 110%  Analysis Date = 12/15/16 
 Pct Recovery = 110%  Analysis Date = 12/15/16 
 Pct Recovery = 110%  Analysis Date = 12/13/16 
 Pct Recovery = 110%  Analysis Date = 12/13/16 
 Pct Recovery = 110%  Analysis Date = 12/10/16 
 Pct Recovery = 110%  Analysis Date = 12/10/16 
 Pct Recovery = 110%  Analysis Date = 12/08/16 
 Pct Recovery = 110%  Analysis Date = 12/08/16 
 Pct Recovery = 110%  Analysis Date = 12/06/16 
 Pct Recovery = 109%  Analysis Date = 12/06/16 
 Pct Recovery = 109%  Analysis Date = 12/04/16 
 Pct Recovery = 109%  Analysis Date = 12/04/16 
 Pct Recovery = 109%  Analysis Date = 12/02/16 
 Pct Recovery = 109%  Analysis Date = 12/02/16 
 Pct Recovery = 109%  Analysis Date = 11/30/16 
 Pct Recovery = 109%  Analysis Date = 11/30/16 
 Pct Recovery = 109%  Analysis Date = 11/28/16 
 Pct Recovery = 108%  Analysis Date = 11/28/16 
 Pct Recovery = 108%  Analysis Date = 11/26/16 
 Pct Recovery = 108%  Analysis Date = 11/26/16 
 Pct Recovery = 108%  Analysis Date = 11/23/16 
 Pct Recovery = 108%  Analysis Date = 11/23/16 
 Pct Recovery = 108%  Analysis Date = 11/21/16 
 Pct Recovery = 108%  Analysis Date = 11/21/16 
 Pct Recovery = 108%  Analysis Date = 11/19/16 
 Pct Recovery = 108%  Analysis Date = 11/19/16 
 Pct Recovery = 108%  Analysis Date = 11/17/16 
 Pct Recovery = 107%  Analysis Date = 11/17/16 
 Pct Recovery = 107%  Analysis Date = 11/15/16 
 Pct Recovery = 107%  Analysis Date = 11/15/16 
 Pct Recovery = 107%  Analysis Date = 11/13/16 
 Pct Recovery = 107%  Analysis Date = 11/13/16 
 Pct Recovery = 107%  Analysis Date = 11/11/16 
 Pct Recovery = 107%  Analysis Date = 11/11/16 
 Pct Recovery = 107%  Analysis Date = 11/08/16 
 Pct Recovery = 107%  Analysis Date = 11/08/16 
 Pct Recovery = 107%  Analysis Date = 11/06/16 
 Pct Recovery = 106%  Analysis Date = 11/06/16 
 Pct Recovery = 106%  Analysis Date = 11/04/16 
 Pct Recovery = 106%  Analysis Date = 11/04/16 
 Pct Recovery = 106%  Analysis Date = 11/02/16 
 Pct Recovery = 106%  Analysis Date = 11/02/16 
 Pct Recovery = 106%  Analysis Date = 10/31/16 
 Pct Recovery = 106%  Analysis Date = 10/31/16 
 Pct Recovery = 106%  Analysis Date = 10/29/16 
 Pct Recovery = 105%  Analysis Date = 10/29/16 
 Pct Recovery = 105%  Analysis Date = 10/27/16 
 Pct Recovery = 105%  Analysis Date = 10/27/16 
 Pct Recovery = 105%  Analysis Date = 10/24/16 
 Pct Recovery = 105%  Analysis Date = 10/24/16 
 Pct Recovery = 105%  Analysis Date = 10/22/16 
 Pct Recovery = 105%  Analysis Date = 10/22/16 
 Pct Recovery = 105%  Analysis Date = 10/20/16 
 Pct Recovery = 105%  Analysis Date = 10/20/16 
 Pct Recovery = 105%  Analysis Date = 10/18/16 
 Pct Recovery = 104%  Analysis Date = 10/18/16 
 Pct Recovery = 104%  Analysis Date = 10/16/16 
 Pct Recovery = 104%  Analysis Date = 10/16/16 
 Pct Recovery = 104%  Analysis Date = 10/14/16 
 Pct Recovery = 104%  Analysis Date = 10/14/16 
 Pct Recovery = 104%  Analysis Date = 10/12/16 
 Pct Recovery = 104%  Analysis Date = 10/12/16 
 Pct Recovery = 104%  Analysis Date = 10/10/16 
 Pct Recovery = 103%  Analysis Date = 10/10/16 
 Pct Recovery = 103%  Analysis Date = 10/07/16 
 Pct Recovery = 103%  Analysis Date = 10/07/16 
 Pct Recovery = 103%  Analysis Date = 10/05/16 
 Pct Recovery = 103%  Analysis Date = 10/05/16 
 Pct Recovery = 103%  Analysis Date = 10/03/16 
 Pct Recovery = 103%  Analysis Date = 10/03/16 
 Pct Recovery = 103%  Analysis Date = 10/01/16 
 Pct Recovery = 103%  Analysis Date = 10/01/16 
 Pct Recovery = 103%  Analysis Date = 09/29/16 
 Pct Recovery = 102%  Analysis Date = 09/29/16 
 Pct Recovery = 102%  Analysis Date = 09/27/16 
 Pct Recovery = 102%  Analysis Date = 09/27/16 
 Pct Recovery = 102%  Analysis Date = 09/25/16 
 Pct Recovery = 102%  Analysis Date = 09/25/16 
 Pct Recovery = 102%  Analysis Date = 09/22/16 
 Pct Recovery = 102%  Analysis Date = 09/22/16 
 Pct Recovery = 102%  Analysis Date = 09/20/16 
 Pct Recovery = 102%  Analysis Date = 09/20/16 
 Pct Recovery = 102%  Analysis Date = 09/18/16 
 Pct Recovery = 101%  Analysis Date = 09/18/16 
 Pct Recovery = 101%  Analysis Date = 09/16/16 
 Pct Recovery = 101%  Analysis Date = 09/16/16 
 Pct Recovery = 101%  Analysis Date = 09/14/16 
 Pct Recovery = 101%  Analysis Date = 09/14/16 
 Pct Recovery = 101%  Analysis Date = 09/12/16 
 Pct Recovery = 101%  Analysis Date = 09/12/16 
 Pct Recovery = 101%  Analysis Date = 09/10/16 
 Pct Recovery = 100%  Analysis Date = 09/10/16 
 Pct Recovery = 100%  Analysis Date = 09/08/16 
 Pct Recovery = 100%  Analysis Date = 09/08/16 
 Pct Recovery = 100%  Analysis Date = 09/05/16 
 Pct Recovery = 100%  Analysis Date = 09/05/16 
 Pct Recovery = 100%  Analysis Date = 09/03/16 
 Pct Recovery = 100%  Analysis Date = 09/03/16 
 Pct Recovery = 100%  Analysis Date = 09/01/16 
 Pct Recovery = 100%  Analysis Date = 09/01/16 
 Pct Recovery = 100%  Analysis Date = 08/30/16 
 Pct Recovery = 99%  Analysis Date = 08/30/16 
 Pct Recovery = 99%  Analysis Date = 08/28/16 
 Pct Recovery = 99%  Analysis Date = 08/28/16 
 Pct Recovery = 99%  Analysis Date = 08/26/16 
 Pct Recovery = 99%  Analysis Date = 08/26/16 
 Pct Recovery = 99%  Analysis Date = 08/24/16 
 Pct Recovery = 99%  Analysis Date = 08/24/16 
 Pct Recovery = 99%  Analysis Date = 08/21/16 
 Pct Recovery = 99%  Analysis Date = 08/21/16 
 Pct Recovery = 99%  Analysis Date = 08/19/16 
 Pct Recovery = 98%  Analysis Date = 08/19/16 
 Pct Recovery = 98%  Analysis Date = 08/17/16 
 Pct Recovery = 98%  Analysis Date = 08/17/16 
 Pct Recovery = 98%  Analysis Date = 08/15/16 
 Pct Recovery = 98%  Analysis Date = 08/15/16 
 Pct Recovery = 98%  Analysis Date = 08/13/16 
 Pct Recovery = 98%  Analysis Date = 08/13/16 
 Pct Recovery = 98%  Analysis Date = 08/11/16 
 Pct Recovery = 97%  Analysis Date = 08/11/16 
 Pct Recovery = 97%  Analysis Date = 08/09/16 
 Pct Recovery = 97%  Analysis Date = 08/09/16 
 Pct Recovery = 97%  Analysis Date = 08/06/16 
 Pct Recovery = 97%  Analysis Date = 08/06/16 
 Pct Recovery = 97%  Analysis Date = 08/04/16 
 Pct Recovery = 97%  Analysis Date = 08/04/16 
 Pct Recovery = 97%  Analysis Date = 08/02/16 
 Pct Recovery = 97%  Analysis Date = 08/02/16 
 Pct Recovery = 97%  Analysis Date = 07/31/16 
 Pct Recovery = 96%  Analysis Date = 07/31/16 
 Pct Recovery = 96%  Analysis Date = 07/29/16 
 Pct Recovery = 96%  Analysis Date = 07/29/16 
 Pct Recovery = 96%  Analysis Date = 07/27/16 
 Pct Recovery = 96%  Analysis Date = 07/27/16 
 Pct Recovery = 96%  Analysis Date = 07/25/16 
 Pct Recovery = 96%  Analysis Date = 07/25/16 
 Pct Recovery = 96%  Analysis Date = 07/23/16 
 Pct Recovery = 95%  Analysis Date = 07/23/16 
 Pct Recovery = 95%  Analysis Date = 07/20/16 
 Pct Recovery = 95%  Analysis Date = 07/20/16 
 Pct Recovery = 95%  Analysis Date = 07/18/16 
 Pct Recovery = 95%  Analysis Date = 07/18/16 
 Pct Recovery = 95%  Analysis Date = 07/16/16 
 Pct Recovery = 95%  Analysis Date = 07/16/16 
 Pct Recovery = 95%  Analysis Date = 07/14/16 
 Pct Recovery = 95%  Analysis Date = 07/14/16 
 Pct Recovery = 95%  Analysis Date = 07/12/16 
 Pct Recovery = 94%  Analysis Date = 07/12/16 
 Pct Recovery = 94%  Analysis Date = 07/10/16 
 Pct Recovery = 94%  Analysis Date = 07/10/16 
 Pct Recovery = 94%  Analysis Date = 07/08/16 
 Pct Recovery = 94%  Analysis Date = 07/08/16 
 Pct Recovery = 94%  Analysis Date = 07/05/16 
 Pct Recovery = 94%  Analysis Date = 07/05/16 
 Pct Recovery = 94%  Analysis Date = 07/03/16 
 Pct Recovery = 94%  Analysis Date = 07/03/16 
 Pct Recovery = 94%  Analysis Date = 07/01/16 
 Pct Recovery = 93%  Analysis Date = 07/01/16 
 Pct Recovery = 93%  Analysis Date = 06/29/16 
 Pct Recovery = 93%  Analysis Date = 06/29/16 
 Pct Recovery = 93%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/27/16 
 Pct Recovery = 93%  Analysis Date = 06/25/16 
 Pct Recovery = 93%  Analysis Date = 06/25/16 
 Pct Recovery = 93%  Analysis Date = 06/23/16 
 Pct Recovery = 92%  Analysis Date = 06/23/16 
 Pct Recovery = 92%  Analysis Date = 06/21/16 
 Pct Recovery = 92%  Analysis Date = 06/21/16 
 Pct Recovery = 92%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/16/16 
 Pct Recovery = 92%  Analysis Date = 06/16/16 
 Pct Recovery = 92%  Analysis Date = 06/14/16 
 Pct Recovery = 92%  Analysis Date = 06/14/16 
 Pct Recovery = 92%  Analysis Date = 06/12/16 
 Pct Recovery = 91%  Analysis Date = 06/12/16 
 Pct Recovery = 91%  Analysis Date = 06/10/16 
 Pct Recovery = 91%  Analysis Date = 06/10/16 
 Pct Recovery = 91%  Analysis Date = 06/08/16 
 Pct Recovery = 91%  Analysis Date = 06/08/16 
 Pct Recovery = 91%  Analysis Date = 06/06/16 
 Pct Recovery = 91%  Analysis Date = 06/06/16 
 Pct Recovery = 91%  Analysis Date = 06/03/16 
 Pct Recovery = 90%  Analysis Date = 06/03/16 
 Pct Recovery = 90%  Analysis Date = 06/01/16 
 Pct Recovery = 90%  Analysis Date = 06/01/16 
 Pct Recovery = 90%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/24/16 
 Pct Recovery = 89%  Analysis Date = 05/24/16 
 Pct Recovery = 89%  Analysis Date = 05/22/16 
 Pct Recovery = 89%  Analysis Date = 05/22/16 
 Pct Recovery = 89%  Analysis Date = 05/19/16 
 Pct Recovery = 89%  Analysis Date = 05/19/16 
 Pct Recovery = 89%  Analysis Date = 05/17/16 
 Pct Recovery = 89%  Analysis Date = 05/17/16 
 Pct Recovery = 89%  Analysis Date = 05/15/16 
 Pct Recovery = 89%  Analysis Date = 05/15/16 
 Pct Recovery = 89%  Analysis Date = 05/13/16 
 Pct Recovery = 88%  Analysis Date = 05/13/16 
 Pct Recovery = 88%  Analysis Date = 05/11/16 
 Pct Recovery = 88%  Analysis Date = 05/11/16 
 Pct Recovery = 88%  Analysis Date = 05/09/16 
 Pct Recovery = 88%  Analysis Date = 05/09/16 
 Pct Recovery = 88%  Analysis Date = 05/07/16 
 Pct Recovery = 88%  Analysis Date = 05/07/16 
 Pct Recovery = 88%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/02/16 
 Pct Recovery = 87%  Analysis Date = 05/02/16 
 Pct Recovery = 87%  Analysis Date = 04/30/16 
 Pct Recovery = 87%  Analysis Date = 04/30/16 
 Pct Recovery = 87%  Analysis Date = 04/28/16 
 Pct Recovery = 87%  Analysis Date = 04/28/16 
 Pct Recovery = 87%  Analysis Date = 04/26/16 
 Pct Recovery = 87%  Analysis Date = 04/26/16 
 Pct Recovery = 87%  Analysis Date = 04/24/16 
 Pct Recovery = 87%  Analysis Date = 04/24/16 
 Pct Recovery = 87%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/22/16 
 Pct Recovery = 86%  Analysis Date = 04/20/16 
 Pct Recovery = 86%  Analysis Date = 04/20/16 
 Pct Recovery = 86%  Analysis Date = 04/17/16 
 Pct Recovery = 86%  Analysis Date = 04/17/16 
 Pct Recovery = 86%  Analysis Date = 04/15/16 
 Pct Recovery = 86%  Analysis Date = 04/15/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/13/16 
 Pct Recovery = 86%  Analysis Date = 04/11/16 
 Pct Recovery = 85%  Analysis Date = 04/11/16 
 Pct Recovery = 85%  Analysis Date = 04/09/16 
 Pct Recovery = 85%  Analysis Date = 04/09/16 
 Pct Recovery = 85%  Analysis Date = 04/07/16 
 Pct Recovery = 85%  Analysis Date = 04/07/16 
 Pct Recovery = 85%  Analysis Date = 04/05/16 
 Pct Recovery = 85%  Analysis Date = 04/05/16 
 Pct Recovery = 85%  Analysis Date = 04/03/16 
 Pct Recovery = 85%  Analysis Date = 04/03/16 
 Pct Recovery = 85%  Analysis Date = 03/31/16 
 Pct Recovery = 84%  Analysis Date = 03/31/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/27/16 
 Pct Recovery = 84%  Analysis Date = 03/27/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/23/16 
 Pct Recovery = 84%  Analysis Date = 03/23/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 83%  Analysis Date = 03/21/16 
 Pct Recovery = 83%  Analysis Date = 03/19/16 
 Pct Recovery = 83%  Analysis Date = 03/19/16 
 Pct Recovery = 83%  Analysis Date = 03/16/16 
 Pct Recovery = 83%  Analysis Date = 03/16/16 
 Pct Recovery = 83%  Analysis Date = 03/14/16 
 Pct Recovery = 83%  Analysis Date = 03/14/16 
 Pct Recovery = 83%  Analysis Date = 03/12/16 
 Pct Recovery = 83%  Analysis Date = 03/12/16 
 Pct Recovery = 83%  Analysis Date = 03/10/16 
 Pct Recovery = 83%  Analysis Date = 03/10/16 
 Pct Recovery = 83%  Analysis Date = 03/08/16 
 Pct Recovery = 82%  Analysis Date = 03/08/16 
 Pct Recovery = 82%  Analysis Date = 03/06/16 
 Pct Recovery = 82%  Analysis Date = 03/06/16 
 Pct Recovery = 82%  Analysis Date = 03/04/16 
 Pct Recovery = 82%  Analysis Date = 03/04/16 
 Pct Recovery = 82%  Analysis Date = 03/02/16 
 Pct Recovery = 82%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 98% 15% 95% 19%
Total 11 98% 15% 95% 19%

Sample Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Characteristic N % % Basis
Plotted 11 92% Spiked
Estimated Values 1 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 8% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 12
Not Spiked 16 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
2-ETHYL-6-METHYLANILINE
METHOD: 2033 , TESTIDCODE: 61620GCM39

 Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 95%  Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 105%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 85%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 80%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 74%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 81%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 73%  Analysis Date = 05/19/16 
 SpikeMix = ChemService 3851600: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 80%  Analysis Date = 04/19/16 
 SpikeMix = ERA 0406-15-01: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 90%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 86%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 84%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 75%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 99%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 83%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 98%  Analysis Date = 04/14/16 
 SpikeMix = ChemService 3851600: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 94%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 87%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 73%  Analysis Date = 05/10/17 
 Pct Recovery = 78%  Analysis Date = 05/08/17 
 Pct Recovery = 79%  Analysis Date = 05/08/17 
 Pct Recovery = 79%  Analysis Date = 05/06/17 
 Pct Recovery = 79%  Analysis Date = 05/06/17 
 Pct Recovery = 79%  Analysis Date = 05/04/17 
 Pct Recovery = 80%  Analysis Date = 05/04/17 
 Pct Recovery = 80%  Analysis Date = 05/01/17 
 Pct Recovery = 80%  Analysis Date = 05/01/17 
 Pct Recovery = 80%  Analysis Date = 04/29/17 
 Pct Recovery = 80%  Analysis Date = 04/29/17 
 Pct Recovery = 80%  Analysis Date = 04/27/17 
 Pct Recovery = 81%  Analysis Date = 04/27/17 
 Pct Recovery = 81%  Analysis Date = 04/25/17 
 Pct Recovery = 81%  Analysis Date = 04/25/17 
 Pct Recovery = 81%  Analysis Date = 04/22/17 
 Pct Recovery = 82%  Analysis Date = 04/22/17 
 Pct Recovery = 82%  Analysis Date = 04/20/17 
 Pct Recovery = 82%  Analysis Date = 04/20/17 
 Pct Recovery = 82%  Analysis Date = 04/18/17 
 Pct Recovery = 82%  Analysis Date = 04/18/17 
 Pct Recovery = 82%  Analysis Date = 04/15/17 
 Pct Recovery = 83%  Analysis Date = 04/15/17 
 Pct Recovery = 83%  Analysis Date = 04/13/17 
 Pct Recovery = 83%  Analysis Date = 04/13/17 
 Pct Recovery = 83%  Analysis Date = 04/11/17 
 Pct Recovery = 83%  Analysis Date = 04/11/17 
 Pct Recovery = 83%  Analysis Date = 04/09/17 
 Pct Recovery = 84%  Analysis Date = 04/09/17 
 Pct Recovery = 84%  Analysis Date = 04/06/17 
 Pct Recovery = 84%  Analysis Date = 04/06/17 
 Pct Recovery = 84%  Analysis Date = 04/04/17 
 Pct Recovery = 85%  Analysis Date = 04/04/17 
 Pct Recovery = 85%  Analysis Date = 04/02/17 
 Pct Recovery = 85%  Analysis Date = 04/02/17 
 Pct Recovery = 85%  Analysis Date = 03/30/17 
 Pct Recovery = 85%  Analysis Date = 03/30/17 
 Pct Recovery = 85%  Analysis Date = 03/28/17 
 Pct Recovery = 86%  Analysis Date = 03/28/17 
 Pct Recovery = 86%  Analysis Date = 03/26/17 
 Pct Recovery = 86%  Analysis Date = 03/26/17 
 Pct Recovery = 86%  Analysis Date = 03/24/17 
 Pct Recovery = 87%  Analysis Date = 03/24/17 
 Pct Recovery = 87%  Analysis Date = 03/21/17 
 Pct Recovery = 87%  Analysis Date = 03/21/17 
 Pct Recovery = 87%  Analysis Date = 03/19/17 
 Pct Recovery = 87%  Analysis Date = 03/19/17 
 Pct Recovery = 87%  Analysis Date = 03/17/17 
 Pct Recovery = 88%  Analysis Date = 03/17/17 
 Pct Recovery = 88%  Analysis Date = 03/14/17 
 Pct Recovery = 88%  Analysis Date = 03/14/17 
 Pct Recovery = 88%  Analysis Date = 03/12/17 
 Pct Recovery = 88%  Analysis Date = 03/12/17 
 Pct Recovery = 88%  Analysis Date = 03/10/17 
 Pct Recovery = 89%  Analysis Date = 03/10/17 
 Pct Recovery = 89%  Analysis Date = 03/08/17 
 Pct Recovery = 89%  Analysis Date = 03/08/17 
 Pct Recovery = 89%  Analysis Date = 03/05/17 
 Pct Recovery = 89%  Analysis Date = 03/05/17 
 Pct Recovery = 89%  Analysis Date = 03/03/17 
 Pct Recovery = 90%  Analysis Date = 03/03/17 
 Pct Recovery = 90%  Analysis Date = 03/01/17 
 Pct Recovery = 90%  Analysis Date = 03/01/17 
 Pct Recovery = 90%  Analysis Date = 02/26/17 
 Pct Recovery = 90%  Analysis Date = 02/26/17 
 Pct Recovery = 90%  Analysis Date = 02/24/17 
 Pct Recovery = 91%  Analysis Date = 02/24/17 
 Pct Recovery = 91%  Analysis Date = 02/22/17 
 Pct Recovery = 91%  Analysis Date = 02/22/17 
 Pct Recovery = 91%  Analysis Date = 02/20/17 
 Pct Recovery = 91%  Analysis Date = 02/20/17 
 Pct Recovery = 91%  Analysis Date = 02/17/17 
 Pct Recovery = 91%  Analysis Date = 02/17/17 
 Pct Recovery = 91%  Analysis Date = 02/15/17 
 Pct Recovery = 92%  Analysis Date = 02/15/17 
 Pct Recovery = 92%  Analysis Date = 02/13/17 
 Pct Recovery = 92%  Analysis Date = 02/13/17 
 Pct Recovery = 92%  Analysis Date = 02/10/17 
 Pct Recovery = 92%  Analysis Date = 02/10/17 
 Pct Recovery = 92%  Analysis Date = 02/08/17 
 Pct Recovery = 92%  Analysis Date = 02/08/17 
 Pct Recovery = 92%  Analysis Date = 02/06/17 
 Pct Recovery = 92%  Analysis Date = 02/06/17 
 Pct Recovery = 92%  Analysis Date = 02/04/17 
 Pct Recovery = 93%  Analysis Date = 02/04/17 
 Pct Recovery = 93%  Analysis Date = 02/01/17 
 Pct Recovery = 93%  Analysis Date = 02/01/17 
 Pct Recovery = 93%  Analysis Date = 01/30/17 
 Pct Recovery = 93%  Analysis Date = 01/30/17 
 Pct Recovery = 93%  Analysis Date = 01/28/17 
 Pct Recovery = 93%  Analysis Date = 01/28/17 
 Pct Recovery = 93%  Analysis Date = 01/25/17 
 Pct Recovery = 93%  Analysis Date = 01/25/17 
 Pct Recovery = 93%  Analysis Date = 01/23/17 
 Pct Recovery = 93%  Analysis Date = 01/23/17 
 Pct Recovery = 93%  Analysis Date = 01/21/17 
 Pct Recovery = 94%  Analysis Date = 01/21/17 
 Pct Recovery = 94%  Analysis Date = 01/19/17 
 Pct Recovery = 94%  Analysis Date = 01/19/17 
 Pct Recovery = 94%  Analysis Date = 01/16/17 
 Pct Recovery = 94%  Analysis Date = 01/16/17 
 Pct Recovery = 94%  Analysis Date = 01/14/17 
 Pct Recovery = 94%  Analysis Date = 01/14/17 
 Pct Recovery = 94%  Analysis Date = 01/12/17 
 Pct Recovery = 93%  Analysis Date = 01/12/17 
 Pct Recovery = 93%  Analysis Date = 01/09/17 
 Pct Recovery = 93%  Analysis Date = 01/09/17 
 Pct Recovery = 93%  Analysis Date = 01/07/17 
 Pct Recovery = 93%  Analysis Date = 01/07/17 
 Pct Recovery = 93%  Analysis Date = 01/05/17 
 Pct Recovery = 93%  Analysis Date = 01/05/17 
 Pct Recovery = 93%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/24/16 
 Pct Recovery = 92%  Analysis Date = 12/24/16 
 Pct Recovery = 92%  Analysis Date = 12/22/16 
 Pct Recovery = 91%  Analysis Date = 12/22/16 
 Pct Recovery = 91%  Analysis Date = 12/20/16 
 Pct Recovery = 91%  Analysis Date = 12/20/16 
 Pct Recovery = 91%  Analysis Date = 12/18/16 
 Pct Recovery = 91%  Analysis Date = 12/18/16 
 Pct Recovery = 91%  Analysis Date = 12/15/16 
 Pct Recovery = 91%  Analysis Date = 12/15/16 
 Pct Recovery = 91%  Analysis Date = 12/13/16 
 Pct Recovery = 90%  Analysis Date = 12/13/16 
 Pct Recovery = 90%  Analysis Date = 12/11/16 
 Pct Recovery = 90%  Analysis Date = 12/11/16 
 Pct Recovery = 90%  Analysis Date = 12/08/16 
 Pct Recovery = 90%  Analysis Date = 12/08/16 
 Pct Recovery = 90%  Analysis Date = 12/06/16 
 Pct Recovery = 90%  Analysis Date = 12/06/16 
 Pct Recovery = 90%  Analysis Date = 12/04/16 
 Pct Recovery = 90%  Analysis Date = 12/04/16 
 Pct Recovery = 90%  Analysis Date = 12/02/16 
 Pct Recovery = 89%  Analysis Date = 12/02/16 
 Pct Recovery = 89%  Analysis Date = 11/29/16 
 Pct Recovery = 89%  Analysis Date = 11/29/16 
 Pct Recovery = 89%  Analysis Date = 11/27/16 
 Pct Recovery = 89%  Analysis Date = 11/27/16 
 Pct Recovery = 89%  Analysis Date = 11/25/16 
 Pct Recovery = 89%  Analysis Date = 11/25/16 
 Pct Recovery = 89%  Analysis Date = 11/22/16 
 Pct Recovery = 88%  Analysis Date = 11/22/16 
 Pct Recovery = 88%  Analysis Date = 11/20/16 
 Pct Recovery = 88%  Analysis Date = 11/20/16 
 Pct Recovery = 88%  Analysis Date = 11/18/16 
 Pct Recovery = 88%  Analysis Date = 11/18/16 
 Pct Recovery = 88%  Analysis Date = 11/16/16 
 Pct Recovery = 88%  Analysis Date = 11/16/16 
 Pct Recovery = 88%  Analysis Date = 11/13/16 
 Pct Recovery = 88%  Analysis Date = 11/13/16 
 Pct Recovery = 88%  Analysis Date = 11/11/16 
 Pct Recovery = 87%  Analysis Date = 11/11/16 
 Pct Recovery = 87%  Analysis Date = 11/09/16 
 Pct Recovery = 87%  Analysis Date = 11/09/16 
 Pct Recovery = 87%  Analysis Date = 11/06/16 
 Pct Recovery = 87%  Analysis Date = 11/06/16 
 Pct Recovery = 87%  Analysis Date = 11/04/16 
 Pct Recovery = 87%  Analysis Date = 11/04/16 
 Pct Recovery = 87%  Analysis Date = 11/02/16 
 Pct Recovery = 86%  Analysis Date = 11/02/16 
 Pct Recovery = 86%  Analysis Date = 10/31/16 
 Pct Recovery = 86%  Analysis Date = 10/31/16 
 Pct Recovery = 86%  Analysis Date = 10/28/16 
 Pct Recovery = 86%  Analysis Date = 10/28/16 
 Pct Recovery = 86%  Analysis Date = 10/26/16 
 Pct Recovery = 86%  Analysis Date = 10/26/16 
 Pct Recovery = 86%  Analysis Date = 10/24/16 
 Pct Recovery = 85%  Analysis Date = 10/24/16 
 Pct Recovery = 85%  Analysis Date = 10/21/16 
 Pct Recovery = 85%  Analysis Date = 10/21/16 
 Pct Recovery = 85%  Analysis Date = 10/19/16 
 Pct Recovery = 85%  Analysis Date = 10/19/16 
 Pct Recovery = 85%  Analysis Date = 10/17/16 
 Pct Recovery = 85%  Analysis Date = 10/17/16 
 Pct Recovery = 85%  Analysis Date = 10/15/16 
 Pct Recovery = 85%  Analysis Date = 10/15/16 
 Pct Recovery = 85%  Analysis Date = 10/12/16 
 Pct Recovery = 84%  Analysis Date = 10/12/16 
 Pct Recovery = 84%  Analysis Date = 10/10/16 
 Pct Recovery = 84%  Analysis Date = 10/10/16 
 Pct Recovery = 84%  Analysis Date = 10/08/16 
 Pct Recovery = 84%  Analysis Date = 10/08/16 
 Pct Recovery = 84%  Analysis Date = 10/05/16 
 Pct Recovery = 84%  Analysis Date = 10/05/16 
 Pct Recovery = 84%  Analysis Date = 10/03/16 
 Pct Recovery = 83%  Analysis Date = 10/03/16 
 Pct Recovery = 83%  Analysis Date = 10/01/16 
 Pct Recovery = 83%  Analysis Date = 10/01/16 
 Pct Recovery = 83%  Analysis Date = 09/29/16 
 Pct Recovery = 83%  Analysis Date = 09/29/16 
 Pct Recovery = 83%  Analysis Date = 09/26/16 
 Pct Recovery = 83%  Analysis Date = 09/26/16 
 Pct Recovery = 83%  Analysis Date = 09/24/16 
 Pct Recovery = 83%  Analysis Date = 09/24/16 
 Pct Recovery = 83%  Analysis Date = 09/22/16 
 Pct Recovery = 82%  Analysis Date = 09/22/16 
 Pct Recovery = 82%  Analysis Date = 09/19/16 
 Pct Recovery = 82%  Analysis Date = 09/19/16 
 Pct Recovery = 82%  Analysis Date = 09/17/16 
 Pct Recovery = 82%  Analysis Date = 09/17/16 
 Pct Recovery = 82%  Analysis Date = 09/15/16 
 Pct Recovery = 82%  Analysis Date = 09/15/16 
 Pct Recovery = 82%  Analysis Date = 09/13/16 
 Pct Recovery = 82%  Analysis Date = 09/13/16 
 Pct Recovery = 82%  Analysis Date = 09/10/16 
 Pct Recovery = 81%  Analysis Date = 09/10/16 
 Pct Recovery = 81%  Analysis Date = 09/08/16 
 Pct Recovery = 81%  Analysis Date = 09/08/16 
 Pct Recovery = 81%  Analysis Date = 09/06/16 
 Pct Recovery = 81%  Analysis Date = 09/06/16 
 Pct Recovery = 81%  Analysis Date = 09/03/16 
 Pct Recovery = 81%  Analysis Date = 09/03/16 
 Pct Recovery = 81%  Analysis Date = 09/01/16 
 Pct Recovery = 81%  Analysis Date = 09/01/16 
 Pct Recovery = 81%  Analysis Date = 08/30/16 
 Pct Recovery = 81%  Analysis Date = 08/30/16 
 Pct Recovery = 81%  Analysis Date = 08/28/16 
 Pct Recovery = 81%  Analysis Date = 08/28/16 
 Pct Recovery = 81%  Analysis Date = 08/25/16 
 Pct Recovery = 81%  Analysis Date = 08/25/16 
 Pct Recovery = 81%  Analysis Date = 08/23/16 
 Pct Recovery = 82%  Analysis Date = 08/23/16 
 Pct Recovery = 82%  Analysis Date = 08/21/16 
 Pct Recovery = 82%  Analysis Date = 08/21/16 
 Pct Recovery = 82%  Analysis Date = 08/18/16 
 Pct Recovery = 82%  Analysis Date = 08/18/16 
 Pct Recovery = 82%  Analysis Date = 08/16/16 
 Pct Recovery = 82%  Analysis Date = 08/16/16 
 Pct Recovery = 82%  Analysis Date = 08/14/16 
 Pct Recovery = 82%  Analysis Date = 08/14/16 
 Pct Recovery = 82%  Analysis Date = 08/12/16 
 Pct Recovery = 82%  Analysis Date = 08/12/16 
 Pct Recovery = 82%  Analysis Date = 08/09/16 
 Pct Recovery = 82%  Analysis Date = 08/09/16 
 Pct Recovery = 82%  Analysis Date = 08/07/16 
 Pct Recovery = 82%  Analysis Date = 08/07/16 
 Pct Recovery = 82%  Analysis Date = 08/05/16 
 Pct Recovery = 83%  Analysis Date = 08/05/16 
 Pct Recovery = 83%  Analysis Date = 08/02/16 
 Pct Recovery = 83%  Analysis Date = 08/02/16 
 Pct Recovery = 83%  Analysis Date = 07/31/16 
 Pct Recovery = 83%  Analysis Date = 07/31/16 
 Pct Recovery = 83%  Analysis Date = 07/29/16 
 Pct Recovery = 83%  Analysis Date = 07/29/16 
 Pct Recovery = 83%  Analysis Date = 07/27/16 
 Pct Recovery = 83%  Analysis Date = 07/27/16 
 Pct Recovery = 83%  Analysis Date = 07/24/16 
 Pct Recovery = 83%  Analysis Date = 07/24/16 
 Pct Recovery = 83%  Analysis Date = 07/22/16 
 Pct Recovery = 83%  Analysis Date = 07/22/16 
 Pct Recovery = 83%  Analysis Date = 07/20/16 
 Pct Recovery = 83%  Analysis Date = 07/20/16 
 Pct Recovery = 83%  Analysis Date = 07/17/16 
 Pct Recovery = 84%  Analysis Date = 07/17/16 
 Pct Recovery = 84%  Analysis Date = 07/15/16 
 Pct Recovery = 84%  Analysis Date = 07/15/16 
 Pct Recovery = 84%  Analysis Date = 07/13/16 
 Pct Recovery = 84%  Analysis Date = 07/13/16 
 Pct Recovery = 84%  Analysis Date = 07/11/16 
 Pct Recovery = 84%  Analysis Date = 07/11/16 
 Pct Recovery = 84%  Analysis Date = 07/08/16 
 Pct Recovery = 84%  Analysis Date = 07/08/16 
 Pct Recovery = 84%  Analysis Date = 07/06/16 
 Pct Recovery = 84%  Analysis Date = 07/06/16 
 Pct Recovery = 84%  Analysis Date = 07/04/16 
 Pct Recovery = 84%  Analysis Date = 07/04/16 
 Pct Recovery = 84%  Analysis Date = 07/01/16 
 Pct Recovery = 84%  Analysis Date = 07/01/16 
 Pct Recovery = 84%  Analysis Date = 06/29/16 
 Pct Recovery = 85%  Analysis Date = 06/29/16 
 Pct Recovery = 85%  Analysis Date = 06/27/16 
 Pct Recovery = 85%  Analysis Date = 06/27/16 
 Pct Recovery = 85%  Analysis Date = 06/25/16 
 Pct Recovery = 85%  Analysis Date = 06/25/16 
 Pct Recovery = 85%  Analysis Date = 06/22/16 
 Pct Recovery = 85%  Analysis Date = 06/22/16 
 Pct Recovery = 85%  Analysis Date = 06/20/16 
 Pct Recovery = 85%  Analysis Date = 06/20/16 
 Pct Recovery = 85%  Analysis Date = 06/18/16 
 Pct Recovery = 85%  Analysis Date = 06/18/16 
 Pct Recovery = 85%  Analysis Date = 06/15/16 
 Pct Recovery = 85%  Analysis Date = 06/15/16 
 Pct Recovery = 85%  Analysis Date = 06/13/16 
 Pct Recovery = 85%  Analysis Date = 06/13/16 
 Pct Recovery = 85%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/04/16 
 Pct Recovery = 86%  Analysis Date = 06/04/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 05/30/16 
 Pct Recovery = 86%  Analysis Date = 05/30/16 
 Pct Recovery = 86%  Analysis Date = 05/28/16 
 Pct Recovery = 86%  Analysis Date = 05/28/16 
 Pct Recovery = 86%  Analysis Date = 05/26/16 
 Pct Recovery = 86%  Analysis Date = 05/26/16 
 Pct Recovery = 86%  Analysis Date = 05/24/16 
 Pct Recovery = 87%  Analysis Date = 05/24/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/21/16 
 Pct Recovery = 87%  Analysis Date = 05/19/16 
 Pct Recovery = 87%  Analysis Date = 05/19/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/14/16 
 Pct Recovery = 87%  Analysis Date = 05/14/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/10/16 
 Pct Recovery = 87%  Analysis Date = 05/10/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/03/16 
 Pct Recovery = 88%  Analysis Date = 05/03/16 
 Pct Recovery = 88%  Analysis Date = 05/01/16 
 Pct Recovery = 88%  Analysis Date = 05/01/16 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 Pct Recovery = 87%  Analysis Date = 04/28/16 
 Pct Recovery = 87%  Analysis Date = 04/26/16 
 Pct Recovery = 87%  Analysis Date = 04/26/16 
 Pct Recovery = 87%  Analysis Date = 04/24/16 
 Pct Recovery = 87%  Analysis Date = 04/24/16 
 Pct Recovery = 87%  Analysis Date = 04/22/16 
 Pct Recovery = 87%  Analysis Date = 04/22/16 
 Pct Recovery = 87%  Analysis Date = 04/19/16 
 Pct Recovery = 87%  Analysis Date = 04/19/16 
 Pct Recovery = 87%  Analysis Date = 04/17/16 
 Pct Recovery = 87%  Analysis Date = 04/17/16 
 Pct Recovery = 87%  Analysis Date = 04/15/16 
 Pct Recovery = 87%  Analysis Date = 04/15/16 
 Pct Recovery = 87%  Analysis Date = 04/12/16 
 Pct Recovery = 87%  Analysis Date = 04/12/16 
 Pct Recovery = 87%  Analysis Date = 04/10/16 
 Pct Recovery = 87%  Analysis Date = 04/10/16 
 Pct Recovery = 87%  Analysis Date = 04/08/16 
 Pct Recovery = 86%  Analysis Date = 04/08/16 
 Pct Recovery = 86%  Analysis Date = 04/06/16 
 Pct Recovery = 86%  Analysis Date = 04/06/16 
 Pct Recovery = 86%  Analysis Date = 04/03/16 
 Pct Recovery = 86%  Analysis Date = 04/03/16 
 Pct Recovery = 86%  Analysis Date = 04/01/16 
 Pct Recovery = 86%  Analysis Date = 04/01/16 
 Pct Recovery = 86%  Analysis Date = 03/30/16 
 Pct Recovery = 86%  Analysis Date = 03/30/16 
 Pct Recovery = 86%  Analysis Date = 03/27/16 
 Pct Recovery = 85%  Analysis Date = 03/27/16 
 Pct Recovery = 85%  Analysis Date = 03/25/16 
 Pct Recovery = 85%  Analysis Date = 03/25/16 
 Pct Recovery = 85%  Analysis Date = 03/23/16 
 Pct Recovery = 85%  Analysis Date = 03/23/16 
 Pct Recovery = 85%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/18/16 
 Pct Recovery = 84%  Analysis Date = 03/18/16 
 Pct Recovery = 84%  Analysis Date = 03/16/16 
 Pct Recovery = 84%  Analysis Date = 03/16/16 
 Pct Recovery = 84%  Analysis Date = 03/14/16 
 Pct Recovery = 84%  Analysis Date = 03/14/16 
 Pct Recovery = 84%  Analysis Date = 03/11/16 
 Pct Recovery = 83%  Analysis Date = 03/11/16 
 Pct Recovery = 83%  Analysis Date = 03/09/16 
 Pct Recovery = 83%  Analysis Date = 03/09/16 
 Pct Recovery = 83%  Analysis Date = 03/07/16 
 Pct Recovery = 83%  Analysis Date = 03/07/16 
 Pct Recovery = 83%  Analysis Date = 03/05/16 
 Pct Recovery = 83%  Analysis Date = 03/05/16 
 Pct Recovery = 83%  Analysis Date = 03/02/16 
 Pct Recovery = 82%  Analysis Date = 03/02/16 
 Pct Recovery = 82%  Analysis Date = 02/29/16 
 Pct Recovery = 82%  Analysis Date = 02/29/16 
 Pct Recovery = 82%  Analysis Date = 02/27/16 
 Pct Recovery = 82%  Analysis Date = 02/27/16 
 Pct Recovery = 82%  Analysis Date = 02/24/16 
 Pct Recovery = 82%  Analysis Date = 02/24/16 
 Pct Recovery = 82%  Analysis Date = 02/22/16 
 Pct Recovery = 81%  Analysis Date = 02/22/16 
 Pct Recovery = 81%  Analysis Date = 02/20/16 
 Pct Recovery = 81%  Analysis Date = 02/20/16 
 Pct Recovery = 81%  Analysis Date = 02/18/16 
 Pct Recovery = 81%  Analysis Date = 02/18/16 
 Pct Recovery = 81%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/15/16 
 Pct Recovery = 81%  Analysis Date = 02/13/16 
 Pct Recovery = 80%  Analysis Date = 02/13/16 
 Pct Recovery = 80%  Analysis Date = 02/11/16 
 Pct Recovery = 80%  Analysis Date = 02/11/16 
 Pct Recovery = 80%  Analysis Date = 02/09/16 
 Pct Recovery = 80%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-ETHYL-6-METHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 86% 9% 85% 11%
Total 19 86% 9% 85% 11%

Sample Statistics
2-ETHYL-6-METHYLANILINE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
3,4-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61625GCM39

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 92%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 66%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 61%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 67%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 51%  Analysis Date = 05/19/16 
 SpikeMix = ChemService 3851600: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 71%  Analysis Date = 04/19/16 
 SpikeMix = ERA 0406-15-01: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 70%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 71%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 70%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 80%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 88%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 79%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 65%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 74%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 75%  Analysis Date = 04/14/16 
 SpikeMix = ChemService 3851600: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 84%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 70%  Analysis Date = 05/02/17 
 Pct Recovery = 69%  Analysis Date = 04/30/17 
 Pct Recovery = 69%  Analysis Date = 04/30/17 
 Pct Recovery = 69%  Analysis Date = 04/28/17 
 Pct Recovery = 69%  Analysis Date = 04/28/17 
 Pct Recovery = 69%  Analysis Date = 04/26/17 
 Pct Recovery = 69%  Analysis Date = 04/26/17 
 Pct Recovery = 69%  Analysis Date = 04/24/17 
 Pct Recovery = 70%  Analysis Date = 04/24/17 
 Pct Recovery = 70%  Analysis Date = 04/22/17 
 Pct Recovery = 70%  Analysis Date = 04/22/17 
 Pct Recovery = 70%  Analysis Date = 04/20/17 
 Pct Recovery = 70%  Analysis Date = 04/20/17 
 Pct Recovery = 70%  Analysis Date = 04/18/17 
 Pct Recovery = 70%  Analysis Date = 04/18/17 
 Pct Recovery = 70%  Analysis Date = 04/15/17 
 Pct Recovery = 71%  Analysis Date = 04/15/17 
 Pct Recovery = 71%  Analysis Date = 04/13/17 
 Pct Recovery = 71%  Analysis Date = 04/13/17 
 Pct Recovery = 71%  Analysis Date = 04/11/17 
 Pct Recovery = 71%  Analysis Date = 04/11/17 
 Pct Recovery = 71%  Analysis Date = 04/09/17 
 Pct Recovery = 72%  Analysis Date = 04/09/17 
 Pct Recovery = 72%  Analysis Date = 04/07/17 
 Pct Recovery = 72%  Analysis Date = 04/07/17 
 Pct Recovery = 72%  Analysis Date = 04/05/17 
 Pct Recovery = 72%  Analysis Date = 04/05/17 
 Pct Recovery = 72%  Analysis Date = 04/03/17 
 Pct Recovery = 72%  Analysis Date = 04/03/17 
 Pct Recovery = 72%  Analysis Date = 03/31/17 
 Pct Recovery = 73%  Analysis Date = 03/31/17 
 Pct Recovery = 73%  Analysis Date = 03/29/17 
 Pct Recovery = 73%  Analysis Date = 03/29/17 
 Pct Recovery = 73%  Analysis Date = 03/27/17 
 Pct Recovery = 73%  Analysis Date = 03/27/17 
 Pct Recovery = 73%  Analysis Date = 03/25/17 
 Pct Recovery = 73%  Analysis Date = 03/25/17 
 Pct Recovery = 73%  Analysis Date = 03/23/17 
 Pct Recovery = 74%  Analysis Date = 03/23/17 
 Pct Recovery = 74%  Analysis Date = 03/21/17 
 Pct Recovery = 74%  Analysis Date = 03/21/17 
 Pct Recovery = 74%  Analysis Date = 03/19/17 
 Pct Recovery = 74%  Analysis Date = 03/19/17 
 Pct Recovery = 74%  Analysis Date = 03/17/17 
 Pct Recovery = 75%  Analysis Date = 03/17/17 
 Pct Recovery = 75%  Analysis Date = 03/14/17 
 Pct Recovery = 75%  Analysis Date = 03/14/17 
 Pct Recovery = 75%  Analysis Date = 03/12/17 
 Pct Recovery = 75%  Analysis Date = 03/12/17 
 Pct Recovery = 75%  Analysis Date = 03/10/17 
 Pct Recovery = 75%  Analysis Date = 03/10/17 
 Pct Recovery = 75%  Analysis Date = 03/08/17 
 Pct Recovery = 76%  Analysis Date = 03/08/17 
 Pct Recovery = 76%  Analysis Date = 03/06/17 
 Pct Recovery = 76%  Analysis Date = 03/06/17 
 Pct Recovery = 76%  Analysis Date = 03/04/17 
 Pct Recovery = 76%  Analysis Date = 03/04/17 
 Pct Recovery = 76%  Analysis Date = 03/02/17 
 Pct Recovery = 77%  Analysis Date = 03/02/17 
 Pct Recovery = 77%  Analysis Date = 02/27/17 
 Pct Recovery = 77%  Analysis Date = 02/27/17 
 Pct Recovery = 77%  Analysis Date = 02/25/17 
 Pct Recovery = 77%  Analysis Date = 02/25/17 
 Pct Recovery = 77%  Analysis Date = 02/23/17 
 Pct Recovery = 77%  Analysis Date = 02/23/17 
 Pct Recovery = 77%  Analysis Date = 02/21/17 
 Pct Recovery = 78%  Analysis Date = 02/21/17 
 Pct Recovery = 78%  Analysis Date = 02/19/17 
 Pct Recovery = 78%  Analysis Date = 02/19/17 
 Pct Recovery = 78%  Analysis Date = 02/17/17 
 Pct Recovery = 78%  Analysis Date = 02/17/17 
 Pct Recovery = 78%  Analysis Date = 02/15/17 
 Pct Recovery = 79%  Analysis Date = 02/15/17 
 Pct Recovery = 79%  Analysis Date = 02/13/17 
 Pct Recovery = 79%  Analysis Date = 02/13/17 
 Pct Recovery = 79%  Analysis Date = 02/10/17 
 Pct Recovery = 79%  Analysis Date = 02/10/17 
 Pct Recovery = 79%  Analysis Date = 02/08/17 
 Pct Recovery = 79%  Analysis Date = 02/08/17 
 Pct Recovery = 79%  Analysis Date = 02/06/17 
 Pct Recovery = 79%  Analysis Date = 02/06/17 
 Pct Recovery = 79%  Analysis Date = 02/04/17 
 Pct Recovery = 80%  Analysis Date = 02/04/17 
 Pct Recovery = 80%  Analysis Date = 02/02/17 
 Pct Recovery = 80%  Analysis Date = 02/02/17 
 Pct Recovery = 80%  Analysis Date = 01/31/17 
 Pct Recovery = 80%  Analysis Date = 01/31/17 
 Pct Recovery = 80%  Analysis Date = 01/29/17 
 Pct Recovery = 80%  Analysis Date = 01/29/17 
 Pct Recovery = 80%  Analysis Date = 01/26/17 
 Pct Recovery = 81%  Analysis Date = 01/26/17 
 Pct Recovery = 81%  Analysis Date = 01/24/17 
 Pct Recovery = 81%  Analysis Date = 01/24/17 
 Pct Recovery = 81%  Analysis Date = 01/22/17 
 Pct Recovery = 81%  Analysis Date = 01/22/17 
 Pct Recovery = 81%  Analysis Date = 01/20/17 
 Pct Recovery = 81%  Analysis Date = 01/20/17 
 Pct Recovery = 81%  Analysis Date = 01/18/17 
 Pct Recovery = 82%  Analysis Date = 01/18/17 
 Pct Recovery = 82%  Analysis Date = 01/16/17 
 Pct Recovery = 82%  Analysis Date = 01/16/17 
 Pct Recovery = 82%  Analysis Date = 01/14/17 
 Pct Recovery = 82%  Analysis Date = 01/14/17 
 Pct Recovery = 82%  Analysis Date = 01/11/17 
 Pct Recovery = 82%  Analysis Date = 01/11/17 
 Pct Recovery = 82%  Analysis Date = 01/09/17 
 Pct Recovery = 82%  Analysis Date = 01/09/17 
 Pct Recovery = 82%  Analysis Date = 01/07/17 
 Pct Recovery = 83%  Analysis Date = 01/07/17 
 Pct Recovery = 83%  Analysis Date = 01/05/17 
 Pct Recovery = 83%  Analysis Date = 01/05/17 
 Pct Recovery = 83%  Analysis Date = 01/03/17 
 Pct Recovery = 83%  Analysis Date = 01/03/17 
 Pct Recovery = 83%  Analysis Date = 01/01/17 
 Pct Recovery = 83%  Analysis Date = 01/01/17 
 Pct Recovery = 83%  Analysis Date = 12/30/16 
 Pct Recovery = 84%  Analysis Date = 12/30/16 
 Pct Recovery = 84%  Analysis Date = 12/28/16 
 Pct Recovery = 84%  Analysis Date = 12/28/16 
 Pct Recovery = 84%  Analysis Date = 12/25/16 
 Pct Recovery = 84%  Analysis Date = 12/25/16 
 Pct Recovery = 84%  Analysis Date = 12/23/16 
 Pct Recovery = 84%  Analysis Date = 12/23/16 
 Pct Recovery = 84%  Analysis Date = 12/21/16 
 Pct Recovery = 85%  Analysis Date = 12/21/16 
 Pct Recovery = 85%  Analysis Date = 12/19/16 
 Pct Recovery = 85%  Analysis Date = 12/19/16 
 Pct Recovery = 85%  Analysis Date = 12/17/16 
 Pct Recovery = 84%  Analysis Date = 12/17/16 
 Pct Recovery = 84%  Analysis Date = 12/15/16 
 Pct Recovery = 84%  Analysis Date = 12/15/16 
 Pct Recovery = 84%  Analysis Date = 12/13/16 
 Pct Recovery = 84%  Analysis Date = 12/13/16 
 Pct Recovery = 84%  Analysis Date = 12/10/16 
 Pct Recovery = 83%  Analysis Date = 12/10/16 
 Pct Recovery = 83%  Analysis Date = 12/08/16 
 Pct Recovery = 83%  Analysis Date = 12/08/16 
 Pct Recovery = 83%  Analysis Date = 12/06/16 
 Pct Recovery = 83%  Analysis Date = 12/06/16 
 Pct Recovery = 83%  Analysis Date = 12/04/16 
 Pct Recovery = 82%  Analysis Date = 12/04/16 
 Pct Recovery = 82%  Analysis Date = 12/02/16 
 Pct Recovery = 82%  Analysis Date = 12/02/16 
 Pct Recovery = 82%  Analysis Date = 11/30/16 
 Pct Recovery = 82%  Analysis Date = 11/30/16 
 Pct Recovery = 82%  Analysis Date = 11/28/16 
 Pct Recovery = 81%  Analysis Date = 11/28/16 
 Pct Recovery = 81%  Analysis Date = 11/26/16 
 Pct Recovery = 81%  Analysis Date = 11/26/16 
 Pct Recovery = 81%  Analysis Date = 11/23/16 
 Pct Recovery = 81%  Analysis Date = 11/23/16 
 Pct Recovery = 81%  Analysis Date = 11/21/16 
 Pct Recovery = 81%  Analysis Date = 11/21/16 
 Pct Recovery = 81%  Analysis Date = 11/19/16 
 Pct Recovery = 80%  Analysis Date = 11/19/16 
 Pct Recovery = 80%  Analysis Date = 11/17/16 
 Pct Recovery = 80%  Analysis Date = 11/17/16 
 Pct Recovery = 80%  Analysis Date = 11/15/16 
 Pct Recovery = 80%  Analysis Date = 11/15/16 
 Pct Recovery = 80%  Analysis Date = 11/13/16 
 Pct Recovery = 79%  Analysis Date = 11/13/16 
 Pct Recovery = 79%  Analysis Date = 11/11/16 
 Pct Recovery = 79%  Analysis Date = 11/11/16 
 Pct Recovery = 79%  Analysis Date = 11/08/16 
 Pct Recovery = 79%  Analysis Date = 11/08/16 
 Pct Recovery = 79%  Analysis Date = 11/06/16 
 Pct Recovery = 78%  Analysis Date = 11/06/16 
 Pct Recovery = 78%  Analysis Date = 11/04/16 
 Pct Recovery = 78%  Analysis Date = 11/04/16 
 Pct Recovery = 78%  Analysis Date = 11/02/16 
 Pct Recovery = 78%  Analysis Date = 11/02/16 
 Pct Recovery = 78%  Analysis Date = 10/31/16 
 Pct Recovery = 77%  Analysis Date = 10/31/16 
 Pct Recovery = 77%  Analysis Date = 10/29/16 
 Pct Recovery = 77%  Analysis Date = 10/29/16 
 Pct Recovery = 77%  Analysis Date = 10/27/16 
 Pct Recovery = 77%  Analysis Date = 10/27/16 
 Pct Recovery = 77%  Analysis Date = 10/24/16 
 Pct Recovery = 76%  Analysis Date = 10/24/16 
 Pct Recovery = 76%  Analysis Date = 10/22/16 
 Pct Recovery = 76%  Analysis Date = 10/22/16 
 Pct Recovery = 76%  Analysis Date = 10/20/16 
 Pct Recovery = 76%  Analysis Date = 10/20/16 
 Pct Recovery = 76%  Analysis Date = 10/18/16 
 Pct Recovery = 75%  Analysis Date = 10/18/16 
 Pct Recovery = 75%  Analysis Date = 10/16/16 
 Pct Recovery = 75%  Analysis Date = 10/16/16 
 Pct Recovery = 75%  Analysis Date = 10/14/16 
 Pct Recovery = 75%  Analysis Date = 10/14/16 
 Pct Recovery = 75%  Analysis Date = 10/12/16 
 Pct Recovery = 74%  Analysis Date = 10/12/16 
 Pct Recovery = 74%  Analysis Date = 10/10/16 
 Pct Recovery = 74%  Analysis Date = 10/10/16 
 Pct Recovery = 74%  Analysis Date = 10/07/16 
 Pct Recovery = 74%  Analysis Date = 10/07/16 
 Pct Recovery = 74%  Analysis Date = 10/05/16 
 Pct Recovery = 74%  Analysis Date = 10/05/16 
 Pct Recovery = 74%  Analysis Date = 10/03/16 
 Pct Recovery = 73%  Analysis Date = 10/03/16 
 Pct Recovery = 73%  Analysis Date = 10/01/16 
 Pct Recovery = 73%  Analysis Date = 10/01/16 
 Pct Recovery = 73%  Analysis Date = 09/29/16 
 Pct Recovery = 73%  Analysis Date = 09/29/16 
 Pct Recovery = 73%  Analysis Date = 09/27/16 
 Pct Recovery = 72%  Analysis Date = 09/27/16 
 Pct Recovery = 72%  Analysis Date = 09/25/16 
 Pct Recovery = 72%  Analysis Date = 09/25/16 
 Pct Recovery = 72%  Analysis Date = 09/22/16 
 Pct Recovery = 72%  Analysis Date = 09/22/16 
 Pct Recovery = 72%  Analysis Date = 09/20/16 
 Pct Recovery = 71%  Analysis Date = 09/20/16 
 Pct Recovery = 71%  Analysis Date = 09/18/16 
 Pct Recovery = 71%  Analysis Date = 09/18/16 
 Pct Recovery = 71%  Analysis Date = 09/16/16 
 Pct Recovery = 71%  Analysis Date = 09/16/16 
 Pct Recovery = 71%  Analysis Date = 09/14/16 
 Pct Recovery = 70%  Analysis Date = 09/14/16 
 Pct Recovery = 70%  Analysis Date = 09/12/16 
 Pct Recovery = 70%  Analysis Date = 09/12/16 
 Pct Recovery = 70%  Analysis Date = 09/10/16 
 Pct Recovery = 70%  Analysis Date = 09/10/16 
 Pct Recovery = 70%  Analysis Date = 09/08/16 
 Pct Recovery = 69%  Analysis Date = 09/08/16 
 Pct Recovery = 69%  Analysis Date = 09/05/16 
 Pct Recovery = 69%  Analysis Date = 09/05/16 
 Pct Recovery = 69%  Analysis Date = 09/03/16 
 Pct Recovery = 69%  Analysis Date = 09/03/16 
 Pct Recovery = 69%  Analysis Date = 09/01/16 
 Pct Recovery = 68%  Analysis Date = 09/01/16 
 Pct Recovery = 68%  Analysis Date = 08/30/16 
 Pct Recovery = 68%  Analysis Date = 08/30/16 
 Pct Recovery = 68%  Analysis Date = 08/28/16 
 Pct Recovery = 68%  Analysis Date = 08/28/16 
 Pct Recovery = 68%  Analysis Date = 08/26/16 
 Pct Recovery = 69%  Analysis Date = 08/26/16 
 Pct Recovery = 69%  Analysis Date = 08/24/16 
 Pct Recovery = 69%  Analysis Date = 08/24/16 
 Pct Recovery = 69%  Analysis Date = 08/21/16 
 Pct Recovery = 69%  Analysis Date = 08/21/16 
 Pct Recovery = 69%  Analysis Date = 08/19/16 
 Pct Recovery = 69%  Analysis Date = 08/19/16 
 Pct Recovery = 69%  Analysis Date = 08/17/16 
 Pct Recovery = 69%  Analysis Date = 08/17/16 
 Pct Recovery = 69%  Analysis Date = 08/15/16 
 Pct Recovery = 69%  Analysis Date = 08/15/16 
 Pct Recovery = 69%  Analysis Date = 08/13/16 
 Pct Recovery = 69%  Analysis Date = 08/13/16 
 Pct Recovery = 69%  Analysis Date = 08/11/16 
 Pct Recovery = 69%  Analysis Date = 08/11/16 
 Pct Recovery = 69%  Analysis Date = 08/09/16 
 Pct Recovery = 69%  Analysis Date = 08/09/16 
 Pct Recovery = 69%  Analysis Date = 08/06/16 
 Pct Recovery = 69%  Analysis Date = 08/06/16 
 Pct Recovery = 69%  Analysis Date = 08/04/16 
 Pct Recovery = 69%  Analysis Date = 08/04/16 
 Pct Recovery = 69%  Analysis Date = 08/02/16 
 Pct Recovery = 69%  Analysis Date = 08/02/16 
 Pct Recovery = 69%  Analysis Date = 07/31/16 
 Pct Recovery = 70%  Analysis Date = 07/31/16 
 Pct Recovery = 70%  Analysis Date = 07/29/16 
 Pct Recovery = 70%  Analysis Date = 07/29/16 
 Pct Recovery = 70%  Analysis Date = 07/27/16 
 Pct Recovery = 70%  Analysis Date = 07/27/16 
 Pct Recovery = 70%  Analysis Date = 07/25/16 
 Pct Recovery = 70%  Analysis Date = 07/25/16 
 Pct Recovery = 70%  Analysis Date = 07/23/16 
 Pct Recovery = 70%  Analysis Date = 07/23/16 
 Pct Recovery = 70%  Analysis Date = 07/20/16 
 Pct Recovery = 70%  Analysis Date = 07/20/16 
 Pct Recovery = 70%  Analysis Date = 07/18/16 
 Pct Recovery = 70%  Analysis Date = 07/18/16 
 Pct Recovery = 70%  Analysis Date = 07/16/16 
 Pct Recovery = 70%  Analysis Date = 07/16/16 
 Pct Recovery = 70%  Analysis Date = 07/14/16 
 Pct Recovery = 70%  Analysis Date = 07/14/16 
 Pct Recovery = 70%  Analysis Date = 07/12/16 
 Pct Recovery = 70%  Analysis Date = 07/12/16 
 Pct Recovery = 70%  Analysis Date = 07/10/16 
 Pct Recovery = 70%  Analysis Date = 07/10/16 
 Pct Recovery = 70%  Analysis Date = 07/08/16 
 Pct Recovery = 71%  Analysis Date = 07/08/16 
 Pct Recovery = 71%  Analysis Date = 07/05/16 
 Pct Recovery = 71%  Analysis Date = 07/05/16 
 Pct Recovery = 71%  Analysis Date = 07/03/16 
 Pct Recovery = 71%  Analysis Date = 07/03/16 
 Pct Recovery = 71%  Analysis Date = 07/01/16 
 Pct Recovery = 71%  Analysis Date = 07/01/16 
 Pct Recovery = 71%  Analysis Date = 06/29/16 
 Pct Recovery = 71%  Analysis Date = 06/29/16 
 Pct Recovery = 71%  Analysis Date = 06/27/16 
 Pct Recovery = 71%  Analysis Date = 06/27/16 
 Pct Recovery = 71%  Analysis Date = 06/25/16 
 Pct Recovery = 71%  Analysis Date = 06/25/16 
 Pct Recovery = 71%  Analysis Date = 06/23/16 
 Pct Recovery = 71%  Analysis Date = 06/23/16 
 Pct Recovery = 71%  Analysis Date = 06/21/16 
 Pct Recovery = 71%  Analysis Date = 06/21/16 
 Pct Recovery = 71%  Analysis Date = 06/18/16 
 Pct Recovery = 71%  Analysis Date = 06/18/16 
 Pct Recovery = 71%  Analysis Date = 06/16/16 
 Pct Recovery = 71%  Analysis Date = 06/16/16 
 Pct Recovery = 71%  Analysis Date = 06/14/16 
 Pct Recovery = 71%  Analysis Date = 06/14/16 
 Pct Recovery = 71%  Analysis Date = 06/12/16 
 Pct Recovery = 72%  Analysis Date = 06/12/16 
 Pct Recovery = 72%  Analysis Date = 06/10/16 
 Pct Recovery = 72%  Analysis Date = 06/10/16 
 Pct Recovery = 72%  Analysis Date = 06/08/16 
 Pct Recovery = 72%  Analysis Date = 06/08/16 
 Pct Recovery = 72%  Analysis Date = 06/06/16 
 Pct Recovery = 72%  Analysis Date = 06/06/16 
 Pct Recovery = 72%  Analysis Date = 06/03/16 
 Pct Recovery = 72%  Analysis Date = 06/03/16 
 Pct Recovery = 72%  Analysis Date = 06/01/16 
 Pct Recovery = 72%  Analysis Date = 06/01/16 
 Pct Recovery = 72%  Analysis Date = 05/30/16 
 Pct Recovery = 72%  Analysis Date = 05/30/16 
 Pct Recovery = 72%  Analysis Date = 05/28/16 
 Pct Recovery = 72%  Analysis Date = 05/28/16 
 Pct Recovery = 72%  Analysis Date = 05/26/16 
 Pct Recovery = 72%  Analysis Date = 05/26/16 
 Pct Recovery = 72%  Analysis Date = 05/24/16 
 Pct Recovery = 72%  Analysis Date = 05/24/16 
 Pct Recovery = 72%  Analysis Date = 05/22/16 
 Pct Recovery = 73%  Analysis Date = 05/22/16 
 Pct Recovery = 73%  Analysis Date = 05/19/16 
 Pct Recovery = 73%  Analysis Date = 05/19/16 
 Pct Recovery = 73%  Analysis Date = 05/17/16 
 Pct Recovery = 73%  Analysis Date = 05/17/16 
 Pct Recovery = 73%  Analysis Date = 05/15/16 
 Pct Recovery = 73%  Analysis Date = 05/15/16 
 Pct Recovery = 73%  Analysis Date = 05/13/16 
 Pct Recovery = 73%  Analysis Date = 05/13/16 
 Pct Recovery = 73%  Analysis Date = 05/11/16 
 Pct Recovery = 73%  Analysis Date = 05/11/16 
 Pct Recovery = 73%  Analysis Date = 05/09/16 
 Pct Recovery = 73%  Analysis Date = 05/09/16 
 Pct Recovery = 73%  Analysis Date = 05/07/16 
 Pct Recovery = 73%  Analysis Date = 05/07/16 
 Pct Recovery = 73%  Analysis Date = 05/05/16 
 Pct Recovery = 73%  Analysis Date = 05/05/16 
 Pct Recovery = 73%  Analysis Date = 05/02/16 
 Pct Recovery = 73%  Analysis Date = 05/02/16 
 Pct Recovery = 73%  Analysis Date = 04/30/16 
 Pct Recovery = 73%  Analysis Date = 04/30/16 
 Pct Recovery = 73%  Analysis Date = 04/28/16 
 Pct Recovery = 73%  Analysis Date = 04/28/16 
 Pct Recovery = 73%  Analysis Date = 04/26/16 
 Pct Recovery = 73%  Analysis Date = 04/26/16 
 Pct Recovery = 73%  Analysis Date = 04/24/16 
 Pct Recovery = 73%  Analysis Date = 04/24/16 
 Pct Recovery = 73%  Analysis Date = 04/22/16 
 Pct Recovery = 73%  Analysis Date = 04/22/16 
 Pct Recovery = 73%  Analysis Date = 04/20/16 
 Pct Recovery = 73%  Analysis Date = 04/20/16 
 Pct Recovery = 73%  Analysis Date = 04/17/16 
 Pct Recovery = 73%  Analysis Date = 04/17/16 
 Pct Recovery = 73%  Analysis Date = 04/15/16 
 Pct Recovery = 73%  Analysis Date = 04/15/16 
 Pct Recovery = 73%  Analysis Date = 04/13/16 
 Pct Recovery = 73%  Analysis Date = 04/13/16 
 Pct Recovery = 73%  Analysis Date = 04/11/16 
 Pct Recovery = 73%  Analysis Date = 04/11/16 
 Pct Recovery = 73%  Analysis Date = 04/09/16 
 Pct Recovery = 73%  Analysis Date = 04/09/16 
 Pct Recovery = 73%  Analysis Date = 04/07/16 
 Pct Recovery = 73%  Analysis Date = 04/07/16 
 Pct Recovery = 73%  Analysis Date = 04/05/16 
 Pct Recovery = 73%  Analysis Date = 04/05/16 
 Pct Recovery = 73%  Analysis Date = 04/03/16 
 Pct Recovery = 73%  Analysis Date = 04/03/16 
 Pct Recovery = 73%  Analysis Date = 03/31/16 
 Pct Recovery = 73%  Analysis Date = 03/31/16 
 Pct Recovery = 73%  Analysis Date = 03/29/16 
 Pct Recovery = 73%  Analysis Date = 03/29/16 
 Pct Recovery = 73%  Analysis Date = 03/27/16 
 Pct Recovery = 73%  Analysis Date = 03/27/16 
 Pct Recovery = 73%  Analysis Date = 03/25/16 
 Pct Recovery = 73%  Analysis Date = 03/25/16 
 Pct Recovery = 73%  Analysis Date = 03/23/16 
 Pct Recovery = 73%  Analysis Date = 03/23/16 
 Pct Recovery = 73%  Analysis Date = 03/21/16 
 Pct Recovery = 73%  Analysis Date = 03/21/16 
 Pct Recovery = 73%  Analysis Date = 03/19/16 
 Pct Recovery = 73%  Analysis Date = 03/19/16 
 Pct Recovery = 73%  Analysis Date = 03/16/16 
 Pct Recovery = 73%  Analysis Date = 03/16/16 
 Pct Recovery = 73%  Analysis Date = 03/14/16 
 Pct Recovery = 73%  Analysis Date = 03/14/16 
 Pct Recovery = 73%  Analysis Date = 03/12/16 
 Pct Recovery = 73%  Analysis Date = 03/12/16 
 Pct Recovery = 73%  Analysis Date = 03/10/16 
 Pct Recovery = 73%  Analysis Date = 03/10/16 
 Pct Recovery = 73%  Analysis Date = 03/08/16 
 Pct Recovery = 73%  Analysis Date = 03/08/16 
 Pct Recovery = 73%  Analysis Date = 03/06/16 
 Pct Recovery = 73%  Analysis Date = 03/06/16 
 Pct Recovery = 73%  Analysis Date = 03/04/16 
 Pct Recovery = 73%  Analysis Date = 03/04/16 
 Pct Recovery = 73%  Analysis Date = 03/02/16 
 Pct Recovery = 73%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,4-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 73% 10% 71% 10%
Total 18 73% 10% 71% 10%

Sample Statistics
3,4-DICHLOROANILINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
3,5-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61627GCM39

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 104%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 92%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 93%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 82%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 69%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 76%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 88%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 77%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 92%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 82%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 107%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 87%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 95%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 96%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 93%  Analysis Date = 05/10/17 
 Pct Recovery = 81%  Analysis Date = 05/08/17 
 Pct Recovery = 81%  Analysis Date = 05/08/17 
 Pct Recovery = 81%  Analysis Date = 05/06/17 
 Pct Recovery = 82%  Analysis Date = 05/06/17 
 Pct Recovery = 82%  Analysis Date = 05/04/17 
 Pct Recovery = 82%  Analysis Date = 05/04/17 
 Pct Recovery = 82%  Analysis Date = 05/01/17 
 Pct Recovery = 82%  Analysis Date = 05/01/17 
 Pct Recovery = 82%  Analysis Date = 04/29/17 
 Pct Recovery = 83%  Analysis Date = 04/29/17 
 Pct Recovery = 83%  Analysis Date = 04/27/17 
 Pct Recovery = 83%  Analysis Date = 04/27/17 
 Pct Recovery = 83%  Analysis Date = 04/25/17 
 Pct Recovery = 84%  Analysis Date = 04/25/17 
 Pct Recovery = 84%  Analysis Date = 04/22/17 
 Pct Recovery = 84%  Analysis Date = 04/22/17 
 Pct Recovery = 84%  Analysis Date = 04/20/17 
 Pct Recovery = 84%  Analysis Date = 04/20/17 
 Pct Recovery = 84%  Analysis Date = 04/18/17 
 Pct Recovery = 85%  Analysis Date = 04/18/17 
 Pct Recovery = 85%  Analysis Date = 04/15/17 
 Pct Recovery = 85%  Analysis Date = 04/15/17 
 Pct Recovery = 85%  Analysis Date = 04/13/17 
 Pct Recovery = 85%  Analysis Date = 04/13/17 
 Pct Recovery = 85%  Analysis Date = 04/11/17 
 Pct Recovery = 86%  Analysis Date = 04/11/17 
 Pct Recovery = 86%  Analysis Date = 04/09/17 
 Pct Recovery = 86%  Analysis Date = 04/09/17 
 Pct Recovery = 86%  Analysis Date = 04/06/17 
 Pct Recovery = 86%  Analysis Date = 04/06/17 
 Pct Recovery = 86%  Analysis Date = 04/04/17 
 Pct Recovery = 87%  Analysis Date = 04/04/17 
 Pct Recovery = 87%  Analysis Date = 04/02/17 
 Pct Recovery = 87%  Analysis Date = 04/02/17 
 Pct Recovery = 87%  Analysis Date = 03/30/17 
 Pct Recovery = 87%  Analysis Date = 03/30/17 
 Pct Recovery = 87%  Analysis Date = 03/28/17 
 Pct Recovery = 88%  Analysis Date = 03/28/17 
 Pct Recovery = 88%  Analysis Date = 03/26/17 
 Pct Recovery = 88%  Analysis Date = 03/26/17 
 Pct Recovery = 88%  Analysis Date = 03/24/17 
 Pct Recovery = 88%  Analysis Date = 03/24/17 
 Pct Recovery = 88%  Analysis Date = 03/21/17 
 Pct Recovery = 89%  Analysis Date = 03/21/17 
 Pct Recovery = 89%  Analysis Date = 03/19/17 
 Pct Recovery = 89%  Analysis Date = 03/19/17 
 Pct Recovery = 89%  Analysis Date = 03/17/17 
 Pct Recovery = 89%  Analysis Date = 03/17/17 
 Pct Recovery = 89%  Analysis Date = 03/14/17 
 Pct Recovery = 90%  Analysis Date = 03/14/17 
 Pct Recovery = 90%  Analysis Date = 03/12/17 
 Pct Recovery = 90%  Analysis Date = 03/12/17 
 Pct Recovery = 90%  Analysis Date = 03/10/17 
 Pct Recovery = 90%  Analysis Date = 03/10/17 
 Pct Recovery = 90%  Analysis Date = 03/08/17 
 Pct Recovery = 91%  Analysis Date = 03/08/17 
 Pct Recovery = 91%  Analysis Date = 03/05/17 
 Pct Recovery = 91%  Analysis Date = 03/05/17 
 Pct Recovery = 91%  Analysis Date = 03/03/17 
 Pct Recovery = 91%  Analysis Date = 03/03/17 
 Pct Recovery = 91%  Analysis Date = 03/01/17 
 Pct Recovery = 92%  Analysis Date = 03/01/17 
 Pct Recovery = 92%  Analysis Date = 02/26/17 
 Pct Recovery = 92%  Analysis Date = 02/26/17 
 Pct Recovery = 92%  Analysis Date = 02/24/17 
 Pct Recovery = 92%  Analysis Date = 02/24/17 
 Pct Recovery = 92%  Analysis Date = 02/22/17 
 Pct Recovery = 93%  Analysis Date = 02/22/17 
 Pct Recovery = 93%  Analysis Date = 02/20/17 
 Pct Recovery = 93%  Analysis Date = 02/20/17 
 Pct Recovery = 93%  Analysis Date = 02/17/17 
 Pct Recovery = 93%  Analysis Date = 02/17/17 
 Pct Recovery = 93%  Analysis Date = 02/15/17 
 Pct Recovery = 93%  Analysis Date = 02/15/17 
 Pct Recovery = 93%  Analysis Date = 02/13/17 
 Pct Recovery = 93%  Analysis Date = 02/13/17 
 Pct Recovery = 93%  Analysis Date = 02/10/17 
 Pct Recovery = 93%  Analysis Date = 02/10/17 
 Pct Recovery = 93%  Analysis Date = 02/08/17 
 Pct Recovery = 93%  Analysis Date = 02/08/17 
 Pct Recovery = 93%  Analysis Date = 02/06/17 
 Pct Recovery = 93%  Analysis Date = 02/06/17 
 Pct Recovery = 93%  Analysis Date = 02/04/17 
 Pct Recovery = 93%  Analysis Date = 02/04/17 
 Pct Recovery = 93%  Analysis Date = 02/01/17 
 Pct Recovery = 93%  Analysis Date = 02/01/17 
 Pct Recovery = 93%  Analysis Date = 01/30/17 
 Pct Recovery = 93%  Analysis Date = 01/30/17 
 Pct Recovery = 93%  Analysis Date = 01/28/17 
 Pct Recovery = 93%  Analysis Date = 01/28/17 
 Pct Recovery = 93%  Analysis Date = 01/25/17 
 Pct Recovery = 93%  Analysis Date = 01/25/17 
 Pct Recovery = 93%  Analysis Date = 01/23/17 
 Pct Recovery = 93%  Analysis Date = 01/23/17 
 Pct Recovery = 93%  Analysis Date = 01/21/17 
 Pct Recovery = 93%  Analysis Date = 01/21/17 
 Pct Recovery = 93%  Analysis Date = 01/19/17 
 Pct Recovery = 93%  Analysis Date = 01/19/17 
 Pct Recovery = 93%  Analysis Date = 01/16/17 
 Pct Recovery = 93%  Analysis Date = 01/16/17 
 Pct Recovery = 93%  Analysis Date = 01/14/17 
 Pct Recovery = 93%  Analysis Date = 01/14/17 
 Pct Recovery = 93%  Analysis Date = 01/12/17 
 Pct Recovery = 93%  Analysis Date = 01/12/17 
 Pct Recovery = 93%  Analysis Date = 01/09/17 
 Pct Recovery = 93%  Analysis Date = 01/09/17 
 Pct Recovery = 93%  Analysis Date = 01/07/17 
 Pct Recovery = 92%  Analysis Date = 01/07/17 
 Pct Recovery = 92%  Analysis Date = 01/05/17 
 Pct Recovery = 92%  Analysis Date = 01/05/17 
 Pct Recovery = 92%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/24/16 
 Pct Recovery = 92%  Analysis Date = 12/24/16 
 Pct Recovery = 92%  Analysis Date = 12/22/16 
 Pct Recovery = 91%  Analysis Date = 12/22/16 
 Pct Recovery = 91%  Analysis Date = 12/20/16 
 Pct Recovery = 91%  Analysis Date = 12/20/16 
 Pct Recovery = 91%  Analysis Date = 12/18/16 
 Pct Recovery = 91%  Analysis Date = 12/18/16 
 Pct Recovery = 91%  Analysis Date = 12/15/16 
 Pct Recovery = 91%  Analysis Date = 12/15/16 
 Pct Recovery = 91%  Analysis Date = 12/13/16 
 Pct Recovery = 91%  Analysis Date = 12/13/16 
 Pct Recovery = 91%  Analysis Date = 12/11/16 
 Pct Recovery = 91%  Analysis Date = 12/11/16 
 Pct Recovery = 91%  Analysis Date = 12/08/16 
 Pct Recovery = 91%  Analysis Date = 12/08/16 
 Pct Recovery = 91%  Analysis Date = 12/06/16 
 Pct Recovery = 91%  Analysis Date = 12/06/16 
 Pct Recovery = 91%  Analysis Date = 12/04/16 
 Pct Recovery = 90%  Analysis Date = 12/04/16 
 Pct Recovery = 90%  Analysis Date = 12/02/16 
 Pct Recovery = 90%  Analysis Date = 12/02/16 
 Pct Recovery = 90%  Analysis Date = 11/29/16 
 Pct Recovery = 90%  Analysis Date = 11/29/16 
 Pct Recovery = 90%  Analysis Date = 11/27/16 
 Pct Recovery = 90%  Analysis Date = 11/27/16 
 Pct Recovery = 90%  Analysis Date = 11/25/16 
 Pct Recovery = 90%  Analysis Date = 11/25/16 
 Pct Recovery = 90%  Analysis Date = 11/22/16 
 Pct Recovery = 90%  Analysis Date = 11/22/16 
 Pct Recovery = 90%  Analysis Date = 11/20/16 
 Pct Recovery = 90%  Analysis Date = 11/20/16 
 Pct Recovery = 90%  Analysis Date = 11/18/16 
 Pct Recovery = 89%  Analysis Date = 11/18/16 
 Pct Recovery = 89%  Analysis Date = 11/16/16 
 Pct Recovery = 89%  Analysis Date = 11/16/16 
 Pct Recovery = 89%  Analysis Date = 11/13/16 
 Pct Recovery = 89%  Analysis Date = 11/13/16 
 Pct Recovery = 89%  Analysis Date = 11/11/16 
 Pct Recovery = 89%  Analysis Date = 11/11/16 
 Pct Recovery = 89%  Analysis Date = 11/09/16 
 Pct Recovery = 89%  Analysis Date = 11/09/16 
 Pct Recovery = 89%  Analysis Date = 11/06/16 
 Pct Recovery = 89%  Analysis Date = 11/06/16 
 Pct Recovery = 89%  Analysis Date = 11/04/16 
 Pct Recovery = 89%  Analysis Date = 11/04/16 
 Pct Recovery = 89%  Analysis Date = 11/02/16 
 Pct Recovery = 89%  Analysis Date = 11/02/16 
 Pct Recovery = 89%  Analysis Date = 10/31/16 
 Pct Recovery = 88%  Analysis Date = 10/31/16 
 Pct Recovery = 88%  Analysis Date = 10/28/16 
 Pct Recovery = 88%  Analysis Date = 10/28/16 
 Pct Recovery = 88%  Analysis Date = 10/26/16 
 Pct Recovery = 88%  Analysis Date = 10/26/16 
 Pct Recovery = 88%  Analysis Date = 10/24/16 
 Pct Recovery = 88%  Analysis Date = 10/24/16 
 Pct Recovery = 88%  Analysis Date = 10/21/16 
 Pct Recovery = 88%  Analysis Date = 10/21/16 
 Pct Recovery = 88%  Analysis Date = 10/19/16 
 Pct Recovery = 88%  Analysis Date = 10/19/16 
 Pct Recovery = 88%  Analysis Date = 10/17/16 
 Pct Recovery = 88%  Analysis Date = 10/17/16 
 Pct Recovery = 88%  Analysis Date = 10/15/16 
 Pct Recovery = 87%  Analysis Date = 10/15/16 
 Pct Recovery = 87%  Analysis Date = 10/12/16 
 Pct Recovery = 87%  Analysis Date = 10/12/16 
 Pct Recovery = 87%  Analysis Date = 10/10/16 
 Pct Recovery = 87%  Analysis Date = 10/10/16 
 Pct Recovery = 87%  Analysis Date = 10/08/16 
 Pct Recovery = 87%  Analysis Date = 10/08/16 
 Pct Recovery = 87%  Analysis Date = 10/05/16 
 Pct Recovery = 87%  Analysis Date = 10/05/16 
 Pct Recovery = 87%  Analysis Date = 10/03/16 
 Pct Recovery = 87%  Analysis Date = 10/03/16 
 Pct Recovery = 87%  Analysis Date = 10/01/16 
 Pct Recovery = 87%  Analysis Date = 10/01/16 
 Pct Recovery = 87%  Analysis Date = 09/29/16 
 Pct Recovery = 86%  Analysis Date = 09/29/16 
 Pct Recovery = 86%  Analysis Date = 09/26/16 
 Pct Recovery = 86%  Analysis Date = 09/26/16 
 Pct Recovery = 86%  Analysis Date = 09/24/16 
 Pct Recovery = 86%  Analysis Date = 09/24/16 
 Pct Recovery = 86%  Analysis Date = 09/22/16 
 Pct Recovery = 86%  Analysis Date = 09/22/16 
 Pct Recovery = 86%  Analysis Date = 09/19/16 
 Pct Recovery = 86%  Analysis Date = 09/19/16 
 Pct Recovery = 86%  Analysis Date = 09/17/16 
 Pct Recovery = 86%  Analysis Date = 09/17/16 
 Pct Recovery = 86%  Analysis Date = 09/15/16 
 Pct Recovery = 86%  Analysis Date = 09/15/16 
 Pct Recovery = 86%  Analysis Date = 09/13/16 
 Pct Recovery = 86%  Analysis Date = 09/13/16 
 Pct Recovery = 86%  Analysis Date = 09/10/16 
 Pct Recovery = 86%  Analysis Date = 09/10/16 
 Pct Recovery = 86%  Analysis Date = 09/08/16 
 Pct Recovery = 85%  Analysis Date = 09/08/16 
 Pct Recovery = 85%  Analysis Date = 09/06/16 
 Pct Recovery = 85%  Analysis Date = 09/06/16 
 Pct Recovery = 85%  Analysis Date = 09/03/16 
 Pct Recovery = 86%  Analysis Date = 09/03/16 
 Pct Recovery = 86%  Analysis Date = 09/01/16 
 Pct Recovery = 86%  Analysis Date = 09/01/16 
 Pct Recovery = 86%  Analysis Date = 08/30/16 
 Pct Recovery = 86%  Analysis Date = 08/30/16 
 Pct Recovery = 86%  Analysis Date = 08/28/16 
 Pct Recovery = 86%  Analysis Date = 08/28/16 
 Pct Recovery = 86%  Analysis Date = 08/25/16 
 Pct Recovery = 86%  Analysis Date = 08/25/16 
 Pct Recovery = 86%  Analysis Date = 08/23/16 
 Pct Recovery = 86%  Analysis Date = 08/23/16 
 Pct Recovery = 86%  Analysis Date = 08/21/16 
 Pct Recovery = 86%  Analysis Date = 08/21/16 
 Pct Recovery = 86%  Analysis Date = 08/18/16 
 Pct Recovery = 86%  Analysis Date = 08/18/16 
 Pct Recovery = 86%  Analysis Date = 08/16/16 
 Pct Recovery = 86%  Analysis Date = 08/16/16 
 Pct Recovery = 86%  Analysis Date = 08/14/16 
 Pct Recovery = 86%  Analysis Date = 08/14/16 
 Pct Recovery = 86%  Analysis Date = 08/12/16 
 Pct Recovery = 86%  Analysis Date = 08/12/16 
 Pct Recovery = 86%  Analysis Date = 08/09/16 
 Pct Recovery = 87%  Analysis Date = 08/09/16 
 Pct Recovery = 87%  Analysis Date = 08/07/16 
 Pct Recovery = 87%  Analysis Date = 08/07/16 
 Pct Recovery = 87%  Analysis Date = 08/05/16 
 Pct Recovery = 87%  Analysis Date = 08/05/16 
 Pct Recovery = 87%  Analysis Date = 08/02/16 
 Pct Recovery = 87%  Analysis Date = 08/02/16 
 Pct Recovery = 87%  Analysis Date = 07/31/16 
 Pct Recovery = 87%  Analysis Date = 07/31/16 
 Pct Recovery = 87%  Analysis Date = 07/29/16 
 Pct Recovery = 87%  Analysis Date = 07/29/16 
 Pct Recovery = 87%  Analysis Date = 07/27/16 
 Pct Recovery = 87%  Analysis Date = 07/27/16 
 Pct Recovery = 87%  Analysis Date = 07/24/16 
 Pct Recovery = 87%  Analysis Date = 07/24/16 
 Pct Recovery = 87%  Analysis Date = 07/22/16 
 Pct Recovery = 87%  Analysis Date = 07/22/16 
 Pct Recovery = 87%  Analysis Date = 07/20/16 
 Pct Recovery = 88%  Analysis Date = 07/20/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/15/16 
 Pct Recovery = 88%  Analysis Date = 07/15/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/11/16 
 Pct Recovery = 88%  Analysis Date = 07/11/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 88%  Analysis Date = 07/06/16 
 Pct Recovery = 88%  Analysis Date = 07/06/16 
 Pct Recovery = 88%  Analysis Date = 07/04/16 
 Pct Recovery = 88%  Analysis Date = 07/04/16 
 Pct Recovery = 88%  Analysis Date = 07/01/16 
 Pct Recovery = 88%  Analysis Date = 07/01/16 
 Pct Recovery = 88%  Analysis Date = 06/29/16 
 Pct Recovery = 88%  Analysis Date = 06/29/16 
 Pct Recovery = 88%  Analysis Date = 06/27/16 
 Pct Recovery = 89%  Analysis Date = 06/27/16 
 Pct Recovery = 89%  Analysis Date = 06/25/16 
 Pct Recovery = 89%  Analysis Date = 06/25/16 
 Pct Recovery = 89%  Analysis Date = 06/22/16 
 Pct Recovery = 89%  Analysis Date = 06/22/16 
 Pct Recovery = 89%  Analysis Date = 06/20/16 
 Pct Recovery = 89%  Analysis Date = 06/20/16 
 Pct Recovery = 89%  Analysis Date = 06/18/16 
 Pct Recovery = 89%  Analysis Date = 06/18/16 
 Pct Recovery = 89%  Analysis Date = 06/15/16 
 Pct Recovery = 89%  Analysis Date = 06/15/16 
 Pct Recovery = 89%  Analysis Date = 06/13/16 
 Pct Recovery = 89%  Analysis Date = 06/13/16 
 Pct Recovery = 89%  Analysis Date = 06/11/16 
 Pct Recovery = 89%  Analysis Date = 06/11/16 
 Pct Recovery = 89%  Analysis Date = 06/09/16 
 Pct Recovery = 89%  Analysis Date = 06/09/16 
 Pct Recovery = 89%  Analysis Date = 06/06/16 
 Pct Recovery = 90%  Analysis Date = 06/06/16 
 Pct Recovery = 90%  Analysis Date = 06/04/16 
 Pct Recovery = 90%  Analysis Date = 06/04/16 
 Pct Recovery = 90%  Analysis Date = 06/02/16 
 Pct Recovery = 90%  Analysis Date = 06/02/16 
 Pct Recovery = 90%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/30/16 
 Pct Recovery = 90%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/24/16 
 Pct Recovery = 90%  Analysis Date = 05/24/16 
 Pct Recovery = 90%  Analysis Date = 05/21/16 
 Pct Recovery = 90%  Analysis Date = 05/21/16 
 Pct Recovery = 90%  Analysis Date = 05/19/16 
 Pct Recovery = 90%  Analysis Date = 05/19/16 
 Pct Recovery = 90%  Analysis Date = 05/17/16 
 Pct Recovery = 90%  Analysis Date = 05/17/16 
 Pct Recovery = 90%  Analysis Date = 05/14/16 
 Pct Recovery = 91%  Analysis Date = 05/14/16 
 Pct Recovery = 91%  Analysis Date = 05/12/16 
 Pct Recovery = 91%  Analysis Date = 05/12/16 
 Pct Recovery = 91%  Analysis Date = 05/10/16 
 Pct Recovery = 91%  Analysis Date = 05/10/16 
 Pct Recovery = 91%  Analysis Date = 05/08/16 
 Pct Recovery = 91%  Analysis Date = 05/08/16 
 Pct Recovery = 91%  Analysis Date = 05/05/16 
 Pct Recovery = 91%  Analysis Date = 05/05/16 
 Pct Recovery = 91%  Analysis Date = 05/03/16 
 Pct Recovery = 91%  Analysis Date = 05/03/16 
 Pct Recovery = 91%  Analysis Date = 05/01/16 
 Pct Recovery = 91%  Analysis Date = 05/01/16 
 Pct Recovery = 91%  Analysis Date = 04/28/16 
 Pct Recovery = 91%  Analysis Date = 04/28/16 
 Pct Recovery = 91%  Analysis Date = 04/26/16 
 Pct Recovery = 91%  Analysis Date = 04/26/16 
 Pct Recovery = 91%  Analysis Date = 04/24/16 
 Pct Recovery = 92%  Analysis Date = 04/24/16 
 Pct Recovery = 92%  Analysis Date = 04/22/16 
 Pct Recovery = 92%  Analysis Date = 04/22/16 
 Pct Recovery = 92%  Analysis Date = 04/19/16 
 Pct Recovery = 92%  Analysis Date = 04/19/16 
 Pct Recovery = 92%  Analysis Date = 04/17/16 
 Pct Recovery = 92%  Analysis Date = 04/17/16 
 Pct Recovery = 92%  Analysis Date = 04/15/16 
 Pct Recovery = 92%  Analysis Date = 04/15/16 
 Pct Recovery = 92%  Analysis Date = 04/12/16 
 Pct Recovery = 92%  Analysis Date = 04/12/16 
 Pct Recovery = 92%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/10/16 
 Pct Recovery = 92%  Analysis Date = 04/08/16 
 Pct Recovery = 92%  Analysis Date = 04/08/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/06/16 
 Pct Recovery = 92%  Analysis Date = 04/03/16 
 Pct Recovery = 92%  Analysis Date = 04/03/16 
 Pct Recovery = 92%  Analysis Date = 04/01/16 
 Pct Recovery = 93%  Analysis Date = 04/01/16 
 Pct Recovery = 93%  Analysis Date = 03/30/16 
 Pct Recovery = 93%  Analysis Date = 03/30/16 
 Pct Recovery = 93%  Analysis Date = 03/27/16 
 Pct Recovery = 93%  Analysis Date = 03/27/16 
 Pct Recovery = 93%  Analysis Date = 03/25/16 
 Pct Recovery = 93%  Analysis Date = 03/25/16 
 Pct Recovery = 93%  Analysis Date = 03/23/16 
 Pct Recovery = 93%  Analysis Date = 03/23/16 
 Pct Recovery = 93%  Analysis Date = 03/21/16 
 Pct Recovery = 93%  Analysis Date = 03/21/16 
 Pct Recovery = 93%  Analysis Date = 03/18/16 
 Pct Recovery = 93%  Analysis Date = 03/18/16 
 Pct Recovery = 93%  Analysis Date = 03/16/16 
 Pct Recovery = 93%  Analysis Date = 03/16/16 
 Pct Recovery = 93%  Analysis Date = 03/14/16 
 Pct Recovery = 93%  Analysis Date = 03/14/16 
 Pct Recovery = 93%  Analysis Date = 03/11/16 
 Pct Recovery = 94%  Analysis Date = 03/11/16 
 Pct Recovery = 94%  Analysis Date = 03/09/16 
 Pct Recovery = 94%  Analysis Date = 03/09/16 
 Pct Recovery = 94%  Analysis Date = 03/07/16 
 Pct Recovery = 94%  Analysis Date = 03/07/16 
 Pct Recovery = 94%  Analysis Date = 03/05/16 
 Pct Recovery = 94%  Analysis Date = 03/05/16 
 Pct Recovery = 94%  Analysis Date = 03/02/16 
 Pct Recovery = 94%  Analysis Date = 03/02/16 
 Pct Recovery = 94%  Analysis Date = 02/29/16 
 Pct Recovery = 94%  Analysis Date = 02/29/16 
 Pct Recovery = 94%  Analysis Date = 02/27/16 
 Pct Recovery = 94%  Analysis Date = 02/27/16 
 Pct Recovery = 94%  Analysis Date = 02/24/16 
 Pct Recovery = 94%  Analysis Date = 02/24/16 
 Pct Recovery = 94%  Analysis Date = 02/22/16 
 Pct Recovery = 94%  Analysis Date = 02/22/16 
 Pct Recovery = 94%  Analysis Date = 02/20/16 
 Pct Recovery = 94%  Analysis Date = 02/20/16 
 Pct Recovery = 94%  Analysis Date = 02/18/16 
 Pct Recovery = 95%  Analysis Date = 02/18/16 
 Pct Recovery = 95%  Analysis Date = 02/15/16 
 Pct Recovery = 95%  Analysis Date = 02/15/16 
 Pct Recovery = 95%  Analysis Date = 02/13/16 
 Pct Recovery = 95%  Analysis Date = 02/13/16 
 Pct Recovery = 95%  Analysis Date = 02/11/16 
 Pct Recovery = 95%  Analysis Date = 02/11/16 
 Pct Recovery = 95%  Analysis Date = 02/09/16 
 Pct Recovery = 95%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,5-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 15 89% 10% 92% 10%
Total 15 89% 10% 92% 10%

Sample Statistics
3,5-DICHLOROANILINE

Characteristic N % % Basis
Plotted 15 83% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 6% Spiked
Spiked 18 .  
False Negatives 2 11% 2 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
4-CHLORO-2-METHYLPHENOL
METHOD: 2033 , TESTIDCODE: 61633GCM39

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 74%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 71%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 60%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 61%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 32%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 39%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 58%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 50%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 57%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 77%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 58%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 59%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 56%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 66%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 69%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 54%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 55%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 46%  Analysis Date = 05/10/17 
 Pct Recovery = 56%  Analysis Date = 05/08/17 
 Pct Recovery = 57%  Analysis Date = 05/08/17 
 Pct Recovery = 57%  Analysis Date = 05/06/17 
 Pct Recovery = 57%  Analysis Date = 05/06/17 
 Pct Recovery = 57%  Analysis Date = 05/04/17 
 Pct Recovery = 57%  Analysis Date = 05/04/17 
 Pct Recovery = 57%  Analysis Date = 05/01/17 
 Pct Recovery = 57%  Analysis Date = 05/01/17 
 Pct Recovery = 57%  Analysis Date = 04/29/17 
 Pct Recovery = 57%  Analysis Date = 04/29/17 
 Pct Recovery = 57%  Analysis Date = 04/27/17 
 Pct Recovery = 57%  Analysis Date = 04/27/17 
 Pct Recovery = 57%  Analysis Date = 04/25/17 
 Pct Recovery = 58%  Analysis Date = 04/25/17 
 Pct Recovery = 58%  Analysis Date = 04/22/17 
 Pct Recovery = 58%  Analysis Date = 04/22/17 
 Pct Recovery = 58%  Analysis Date = 04/20/17 
 Pct Recovery = 58%  Analysis Date = 04/20/17 
 Pct Recovery = 58%  Analysis Date = 04/18/17 
 Pct Recovery = 58%  Analysis Date = 04/18/17 
 Pct Recovery = 58%  Analysis Date = 04/15/17 
 Pct Recovery = 58%  Analysis Date = 04/15/17 
 Pct Recovery = 58%  Analysis Date = 04/13/17 
 Pct Recovery = 59%  Analysis Date = 04/13/17 
 Pct Recovery = 59%  Analysis Date = 04/11/17 
 Pct Recovery = 59%  Analysis Date = 04/11/17 
 Pct Recovery = 59%  Analysis Date = 04/09/17 
 Pct Recovery = 59%  Analysis Date = 04/09/17 
 Pct Recovery = 59%  Analysis Date = 04/06/17 
 Pct Recovery = 59%  Analysis Date = 04/06/17 
 Pct Recovery = 59%  Analysis Date = 04/04/17 
 Pct Recovery = 59%  Analysis Date = 04/04/17 
 Pct Recovery = 59%  Analysis Date = 04/02/17 
 Pct Recovery = 60%  Analysis Date = 04/02/17 
 Pct Recovery = 60%  Analysis Date = 03/30/17 
 Pct Recovery = 60%  Analysis Date = 03/30/17 
 Pct Recovery = 60%  Analysis Date = 03/28/17 
 Pct Recovery = 60%  Analysis Date = 03/28/17 
 Pct Recovery = 60%  Analysis Date = 03/26/17 
 Pct Recovery = 60%  Analysis Date = 03/26/17 
 Pct Recovery = 60%  Analysis Date = 03/24/17 
 Pct Recovery = 60%  Analysis Date = 03/24/17 
 Pct Recovery = 60%  Analysis Date = 03/21/17 
 Pct Recovery = 60%  Analysis Date = 03/21/17 
 Pct Recovery = 60%  Analysis Date = 03/19/17 
 Pct Recovery = 61%  Analysis Date = 03/19/17 
 Pct Recovery = 61%  Analysis Date = 03/17/17 
 Pct Recovery = 61%  Analysis Date = 03/17/17 
 Pct Recovery = 61%  Analysis Date = 03/14/17 
 Pct Recovery = 61%  Analysis Date = 03/14/17 
 Pct Recovery = 61%  Analysis Date = 03/12/17 
 Pct Recovery = 61%  Analysis Date = 03/12/17 
 Pct Recovery = 61%  Analysis Date = 03/10/17 
 Pct Recovery = 61%  Analysis Date = 03/10/17 
 Pct Recovery = 61%  Analysis Date = 03/08/17 
 Pct Recovery = 62%  Analysis Date = 03/08/17 
 Pct Recovery = 62%  Analysis Date = 03/05/17 
 Pct Recovery = 62%  Analysis Date = 03/05/17 
 Pct Recovery = 62%  Analysis Date = 03/03/17 
 Pct Recovery = 62%  Analysis Date = 03/03/17 
 Pct Recovery = 62%  Analysis Date = 03/01/17 
 Pct Recovery = 62%  Analysis Date = 03/01/17 
 Pct Recovery = 62%  Analysis Date = 02/26/17 
 Pct Recovery = 62%  Analysis Date = 02/26/17 
 Pct Recovery = 62%  Analysis Date = 02/24/17 
 Pct Recovery = 62%  Analysis Date = 02/24/17 
 Pct Recovery = 62%  Analysis Date = 02/22/17 
 Pct Recovery = 63%  Analysis Date = 02/22/17 
 Pct Recovery = 63%  Analysis Date = 02/20/17 
 Pct Recovery = 63%  Analysis Date = 02/20/17 
 Pct Recovery = 63%  Analysis Date = 02/17/17 
 Pct Recovery = 63%  Analysis Date = 02/17/17 
 Pct Recovery = 63%  Analysis Date = 02/15/17 
 Pct Recovery = 63%  Analysis Date = 02/15/17 
 Pct Recovery = 63%  Analysis Date = 02/13/17 
 Pct Recovery = 64%  Analysis Date = 02/13/17 
 Pct Recovery = 64%  Analysis Date = 02/10/17 
 Pct Recovery = 64%  Analysis Date = 02/10/17 
 Pct Recovery = 64%  Analysis Date = 02/08/17 
 Pct Recovery = 64%  Analysis Date = 02/08/17 
 Pct Recovery = 64%  Analysis Date = 02/06/17 
 Pct Recovery = 64%  Analysis Date = 02/06/17 
 Pct Recovery = 64%  Analysis Date = 02/04/17 
 Pct Recovery = 64%  Analysis Date = 02/04/17 
 Pct Recovery = 64%  Analysis Date = 02/01/17 
 Pct Recovery = 65%  Analysis Date = 02/01/17 
 Pct Recovery = 65%  Analysis Date = 01/30/17 
 Pct Recovery = 65%  Analysis Date = 01/30/17 
 Pct Recovery = 65%  Analysis Date = 01/28/17 
 Pct Recovery = 65%  Analysis Date = 01/28/17 
 Pct Recovery = 65%  Analysis Date = 01/25/17 
 Pct Recovery = 65%  Analysis Date = 01/25/17 
 Pct Recovery = 65%  Analysis Date = 01/23/17 
 Pct Recovery = 66%  Analysis Date = 01/23/17 
 Pct Recovery = 66%  Analysis Date = 01/21/17 
 Pct Recovery = 66%  Analysis Date = 01/21/17 
 Pct Recovery = 66%  Analysis Date = 01/19/17 
 Pct Recovery = 66%  Analysis Date = 01/19/17 
 Pct Recovery = 66%  Analysis Date = 01/16/17 
 Pct Recovery = 66%  Analysis Date = 01/16/17 
 Pct Recovery = 66%  Analysis Date = 01/14/17 
 Pct Recovery = 66%  Analysis Date = 01/14/17 
 Pct Recovery = 66%  Analysis Date = 01/12/17 
 Pct Recovery = 66%  Analysis Date = 01/12/17 
 Pct Recovery = 66%  Analysis Date = 01/09/17 
 Pct Recovery = 66%  Analysis Date = 01/09/17 
 Pct Recovery = 66%  Analysis Date = 01/07/17 
 Pct Recovery = 65%  Analysis Date = 01/07/17 
 Pct Recovery = 65%  Analysis Date = 01/05/17 
 Pct Recovery = 65%  Analysis Date = 01/05/17 
 Pct Recovery = 65%  Analysis Date = 01/03/17 
 Pct Recovery = 65%  Analysis Date = 01/03/17 
 Pct Recovery = 65%  Analysis Date = 12/31/16 
 Pct Recovery = 65%  Analysis Date = 12/31/16 
 Pct Recovery = 65%  Analysis Date = 12/29/16 
 Pct Recovery = 65%  Analysis Date = 12/29/16 
 Pct Recovery = 65%  Analysis Date = 12/27/16 
 Pct Recovery = 65%  Analysis Date = 12/27/16 
 Pct Recovery = 65%  Analysis Date = 12/24/16 
 Pct Recovery = 64%  Analysis Date = 12/24/16 
 Pct Recovery = 64%  Analysis Date = 12/22/16 
 Pct Recovery = 64%  Analysis Date = 12/22/16 
 Pct Recovery = 64%  Analysis Date = 12/20/16 
 Pct Recovery = 64%  Analysis Date = 12/20/16 
 Pct Recovery = 64%  Analysis Date = 12/18/16 
 Pct Recovery = 64%  Analysis Date = 12/18/16 
 Pct Recovery = 64%  Analysis Date = 12/15/16 
 Pct Recovery = 64%  Analysis Date = 12/15/16 
 Pct Recovery = 64%  Analysis Date = 12/13/16 
 Pct Recovery = 63%  Analysis Date = 12/13/16 
 Pct Recovery = 63%  Analysis Date = 12/11/16 
 Pct Recovery = 63%  Analysis Date = 12/11/16 
 Pct Recovery = 63%  Analysis Date = 12/08/16 
 Pct Recovery = 63%  Analysis Date = 12/08/16 
 Pct Recovery = 63%  Analysis Date = 12/06/16 
 Pct Recovery = 63%  Analysis Date = 12/06/16 
 Pct Recovery = 63%  Analysis Date = 12/04/16 
 Pct Recovery = 63%  Analysis Date = 12/04/16 
 Pct Recovery = 63%  Analysis Date = 12/02/16 
 Pct Recovery = 63%  Analysis Date = 12/02/16 
 Pct Recovery = 63%  Analysis Date = 11/29/16 
 Pct Recovery = 62%  Analysis Date = 11/29/16 
 Pct Recovery = 62%  Analysis Date = 11/27/16 
 Pct Recovery = 62%  Analysis Date = 11/27/16 
 Pct Recovery = 62%  Analysis Date = 11/25/16 
 Pct Recovery = 62%  Analysis Date = 11/25/16 
 Pct Recovery = 62%  Analysis Date = 11/22/16 
 Pct Recovery = 62%  Analysis Date = 11/22/16 
 Pct Recovery = 62%  Analysis Date = 11/20/16 
 Pct Recovery = 62%  Analysis Date = 11/20/16 
 Pct Recovery = 62%  Analysis Date = 11/18/16 
 Pct Recovery = 61%  Analysis Date = 11/18/16 
 Pct Recovery = 61%  Analysis Date = 11/16/16 
 Pct Recovery = 61%  Analysis Date = 11/16/16 
 Pct Recovery = 61%  Analysis Date = 11/13/16 
 Pct Recovery = 61%  Analysis Date = 11/13/16 
 Pct Recovery = 61%  Analysis Date = 11/11/16 
 Pct Recovery = 61%  Analysis Date = 11/11/16 
 Pct Recovery = 61%  Analysis Date = 11/09/16 
 Pct Recovery = 61%  Analysis Date = 11/09/16 
 Pct Recovery = 61%  Analysis Date = 11/06/16 
 Pct Recovery = 61%  Analysis Date = 11/06/16 
 Pct Recovery = 61%  Analysis Date = 11/04/16 
 Pct Recovery = 60%  Analysis Date = 11/04/16 
 Pct Recovery = 60%  Analysis Date = 11/02/16 
 Pct Recovery = 60%  Analysis Date = 11/02/16 
 Pct Recovery = 60%  Analysis Date = 10/31/16 
 Pct Recovery = 60%  Analysis Date = 10/31/16 
 Pct Recovery = 60%  Analysis Date = 10/28/16 
 Pct Recovery = 60%  Analysis Date = 10/28/16 
 Pct Recovery = 60%  Analysis Date = 10/26/16 
 Pct Recovery = 60%  Analysis Date = 10/26/16 
 Pct Recovery = 60%  Analysis Date = 10/24/16 
 Pct Recovery = 59%  Analysis Date = 10/24/16 
 Pct Recovery = 59%  Analysis Date = 10/21/16 
 Pct Recovery = 59%  Analysis Date = 10/21/16 
 Pct Recovery = 59%  Analysis Date = 10/19/16 
 Pct Recovery = 59%  Analysis Date = 10/19/16 
 Pct Recovery = 59%  Analysis Date = 10/17/16 
 Pct Recovery = 59%  Analysis Date = 10/17/16 
 Pct Recovery = 59%  Analysis Date = 10/15/16 
 Pct Recovery = 59%  Analysis Date = 10/15/16 
 Pct Recovery = 59%  Analysis Date = 10/12/16 
 Pct Recovery = 59%  Analysis Date = 10/12/16 
 Pct Recovery = 59%  Analysis Date = 10/10/16 
 Pct Recovery = 58%  Analysis Date = 10/10/16 
 Pct Recovery = 58%  Analysis Date = 10/08/16 
 Pct Recovery = 58%  Analysis Date = 10/08/16 
 Pct Recovery = 58%  Analysis Date = 10/05/16 
 Pct Recovery = 58%  Analysis Date = 10/05/16 
 Pct Recovery = 58%  Analysis Date = 10/03/16 
 Pct Recovery = 58%  Analysis Date = 10/03/16 
 Pct Recovery = 58%  Analysis Date = 10/01/16 
 Pct Recovery = 58%  Analysis Date = 10/01/16 
 Pct Recovery = 58%  Analysis Date = 09/29/16 
 Pct Recovery = 57%  Analysis Date = 09/29/16 
 Pct Recovery = 57%  Analysis Date = 09/26/16 
 Pct Recovery = 57%  Analysis Date = 09/26/16 
 Pct Recovery = 57%  Analysis Date = 09/24/16 
 Pct Recovery = 57%  Analysis Date = 09/24/16 
 Pct Recovery = 57%  Analysis Date = 09/22/16 
 Pct Recovery = 57%  Analysis Date = 09/22/16 
 Pct Recovery = 57%  Analysis Date = 09/19/16 
 Pct Recovery = 57%  Analysis Date = 09/19/16 
 Pct Recovery = 57%  Analysis Date = 09/17/16 
 Pct Recovery = 57%  Analysis Date = 09/17/16 
 Pct Recovery = 57%  Analysis Date = 09/15/16 
 Pct Recovery = 56%  Analysis Date = 09/15/16 
 Pct Recovery = 56%  Analysis Date = 09/13/16 
 Pct Recovery = 56%  Analysis Date = 09/13/16 
 Pct Recovery = 56%  Analysis Date = 09/10/16 
 Pct Recovery = 56%  Analysis Date = 09/10/16 
 Pct Recovery = 56%  Analysis Date = 09/08/16 
 Pct Recovery = 56%  Analysis Date = 09/08/16 
 Pct Recovery = 56%  Analysis Date = 09/06/16 
 Pct Recovery = 56%  Analysis Date = 09/06/16 
 Pct Recovery = 56%  Analysis Date = 09/03/16 
 Pct Recovery = 56%  Analysis Date = 09/03/16 
 Pct Recovery = 56%  Analysis Date = 09/01/16 
 Pct Recovery = 56%  Analysis Date = 09/01/16 
 Pct Recovery = 56%  Analysis Date = 08/30/16 
 Pct Recovery = 56%  Analysis Date = 08/30/16 
 Pct Recovery = 56%  Analysis Date = 08/28/16 
 Pct Recovery = 56%  Analysis Date = 08/28/16 
 Pct Recovery = 56%  Analysis Date = 08/25/16 
 Pct Recovery = 57%  Analysis Date = 08/25/16 
 Pct Recovery = 57%  Analysis Date = 08/23/16 
 Pct Recovery = 57%  Analysis Date = 08/23/16 
 Pct Recovery = 57%  Analysis Date = 08/21/16 
 Pct Recovery = 57%  Analysis Date = 08/21/16 
 Pct Recovery = 57%  Analysis Date = 08/18/16 
 Pct Recovery = 57%  Analysis Date = 08/18/16 
 Pct Recovery = 57%  Analysis Date = 08/16/16 
 Pct Recovery = 57%  Analysis Date = 08/16/16 
 Pct Recovery = 57%  Analysis Date = 08/14/16 
 Pct Recovery = 57%  Analysis Date = 08/14/16 
 Pct Recovery = 57%  Analysis Date = 08/12/16 
 Pct Recovery = 57%  Analysis Date = 08/12/16 
 Pct Recovery = 57%  Analysis Date = 08/09/16 
 Pct Recovery = 57%  Analysis Date = 08/09/16 
 Pct Recovery = 57%  Analysis Date = 08/07/16 
 Pct Recovery = 57%  Analysis Date = 08/07/16 
 Pct Recovery = 57%  Analysis Date = 08/05/16 
 Pct Recovery = 57%  Analysis Date = 08/05/16 
 Pct Recovery = 57%  Analysis Date = 08/02/16 
 Pct Recovery = 57%  Analysis Date = 08/02/16 
 Pct Recovery = 57%  Analysis Date = 07/31/16 
 Pct Recovery = 57%  Analysis Date = 07/31/16 
 Pct Recovery = 57%  Analysis Date = 07/29/16 
 Pct Recovery = 57%  Analysis Date = 07/29/16 
 Pct Recovery = 57%  Analysis Date = 07/27/16 
 Pct Recovery = 57%  Analysis Date = 07/27/16 
 Pct Recovery = 57%  Analysis Date = 07/24/16 
 Pct Recovery = 57%  Analysis Date = 07/24/16 
 Pct Recovery = 57%  Analysis Date = 07/22/16 
 Pct Recovery = 57%  Analysis Date = 07/22/16 
 Pct Recovery = 57%  Analysis Date = 07/20/16 
 Pct Recovery = 57%  Analysis Date = 07/20/16 
 Pct Recovery = 57%  Analysis Date = 07/17/16 
 Pct Recovery = 57%  Analysis Date = 07/17/16 
 Pct Recovery = 57%  Analysis Date = 07/15/16 
 Pct Recovery = 57%  Analysis Date = 07/15/16 
 Pct Recovery = 57%  Analysis Date = 07/13/16 
 Pct Recovery = 57%  Analysis Date = 07/13/16 
 Pct Recovery = 57%  Analysis Date = 07/11/16 
 Pct Recovery = 57%  Analysis Date = 07/11/16 
 Pct Recovery = 57%  Analysis Date = 07/08/16 
 Pct Recovery = 57%  Analysis Date = 07/08/16 
 Pct Recovery = 57%  Analysis Date = 07/06/16 
 Pct Recovery = 57%  Analysis Date = 07/06/16 
 Pct Recovery = 57%  Analysis Date = 07/04/16 
 Pct Recovery = 57%  Analysis Date = 07/04/16 
 Pct Recovery = 57%  Analysis Date = 07/01/16 
 Pct Recovery = 57%  Analysis Date = 07/01/16 
 Pct Recovery = 57%  Analysis Date = 06/29/16 
 Pct Recovery = 57%  Analysis Date = 06/29/16 
 Pct Recovery = 57%  Analysis Date = 06/27/16 
 Pct Recovery = 57%  Analysis Date = 06/27/16 
 Pct Recovery = 57%  Analysis Date = 06/25/16 
 Pct Recovery = 57%  Analysis Date = 06/25/16 
 Pct Recovery = 57%  Analysis Date = 06/22/16 
 Pct Recovery = 57%  Analysis Date = 06/22/16 
 Pct Recovery = 57%  Analysis Date = 06/20/16 
 Pct Recovery = 57%  Analysis Date = 06/20/16 
 Pct Recovery = 57%  Analysis Date = 06/18/16 
 Pct Recovery = 57%  Analysis Date = 06/18/16 
 Pct Recovery = 57%  Analysis Date = 06/15/16 
 Pct Recovery = 57%  Analysis Date = 06/15/16 
 Pct Recovery = 57%  Analysis Date = 06/13/16 
 Pct Recovery = 57%  Analysis Date = 06/13/16 
 Pct Recovery = 57%  Analysis Date = 06/11/16 
 Pct Recovery = 57%  Analysis Date = 06/11/16 
 Pct Recovery = 57%  Analysis Date = 06/09/16 
 Pct Recovery = 57%  Analysis Date = 06/09/16 
 Pct Recovery = 57%  Analysis Date = 06/06/16 
 Pct Recovery = 57%  Analysis Date = 06/06/16 
 Pct Recovery = 57%  Analysis Date = 06/04/16 
 Pct Recovery = 57%  Analysis Date = 06/04/16 
 Pct Recovery = 57%  Analysis Date = 06/02/16 
 Pct Recovery = 57%  Analysis Date = 06/02/16 
 Pct Recovery = 57%  Analysis Date = 05/30/16 
 Pct Recovery = 57%  Analysis Date = 05/30/16 
 Pct Recovery = 57%  Analysis Date = 05/28/16 
 Pct Recovery = 57%  Analysis Date = 05/28/16 
 Pct Recovery = 57%  Analysis Date = 05/26/16 
 Pct Recovery = 57%  Analysis Date = 05/26/16 
 Pct Recovery = 57%  Analysis Date = 05/24/16 
 Pct Recovery = 57%  Analysis Date = 05/24/16 
 Pct Recovery = 57%  Analysis Date = 05/21/16 
 Pct Recovery = 57%  Analysis Date = 05/21/16 
 Pct Recovery = 57%  Analysis Date = 05/19/16 
 Pct Recovery = 57%  Analysis Date = 05/19/16 
 Pct Recovery = 57%  Analysis Date = 05/17/16 
 Pct Recovery = 57%  Analysis Date = 05/17/16 
 Pct Recovery = 57%  Analysis Date = 05/14/16 
 Pct Recovery = 57%  Analysis Date = 05/14/16 
 Pct Recovery = 57%  Analysis Date = 05/12/16 
 Pct Recovery = 57%  Analysis Date = 05/12/16 
 Pct Recovery = 57%  Analysis Date = 05/10/16 
 Pct Recovery = 57%  Analysis Date = 05/10/16 
 Pct Recovery = 57%  Analysis Date = 05/08/16 
 Pct Recovery = 57%  Analysis Date = 05/08/16 
 Pct Recovery = 57%  Analysis Date = 05/05/16 
 Pct Recovery = 57%  Analysis Date = 05/05/16 
 Pct Recovery = 57%  Analysis Date = 05/03/16 
 Pct Recovery = 57%  Analysis Date = 05/03/16 
 Pct Recovery = 57%  Analysis Date = 05/01/16 
 Pct Recovery = 57%  Analysis Date = 05/01/16 
 Pct Recovery = 57%  Analysis Date = 04/28/16 
 Pct Recovery = 57%  Analysis Date = 04/28/16 
 Pct Recovery = 57%  Analysis Date = 04/26/16 
 Pct Recovery = 57%  Analysis Date = 04/26/16 
 Pct Recovery = 57%  Analysis Date = 04/24/16 
 Pct Recovery = 57%  Analysis Date = 04/24/16 
 Pct Recovery = 57%  Analysis Date = 04/22/16 
 Pct Recovery = 57%  Analysis Date = 04/22/16 
 Pct Recovery = 57%  Analysis Date = 04/19/16 
 Pct Recovery = 57%  Analysis Date = 04/19/16 
 Pct Recovery = 57%  Analysis Date = 04/17/16 
 Pct Recovery = 56%  Analysis Date = 04/17/16 
 Pct Recovery = 56%  Analysis Date = 04/15/16 
 Pct Recovery = 56%  Analysis Date = 04/15/16 
 Pct Recovery = 56%  Analysis Date = 04/12/16 
 Pct Recovery = 56%  Analysis Date = 04/12/16 
 Pct Recovery = 56%  Analysis Date = 04/10/16 
 Pct Recovery = 56%  Analysis Date = 04/10/16 
 Pct Recovery = 56%  Analysis Date = 04/08/16 
 Pct Recovery = 56%  Analysis Date = 04/08/16 
 Pct Recovery = 56%  Analysis Date = 04/06/16 
 Pct Recovery = 56%  Analysis Date = 04/06/16 
 Pct Recovery = 56%  Analysis Date = 04/03/16 
 Pct Recovery = 55%  Analysis Date = 04/03/16 
 Pct Recovery = 55%  Analysis Date = 04/01/16 
 Pct Recovery = 55%  Analysis Date = 04/01/16 
 Pct Recovery = 55%  Analysis Date = 03/30/16 
 Pct Recovery = 55%  Analysis Date = 03/30/16 
 Pct Recovery = 55%  Analysis Date = 03/27/16 
 Pct Recovery = 55%  Analysis Date = 03/27/16 
 Pct Recovery = 55%  Analysis Date = 03/25/16 
 Pct Recovery = 54%  Analysis Date = 03/25/16 
 Pct Recovery = 54%  Analysis Date = 03/23/16 
 Pct Recovery = 54%  Analysis Date = 03/23/16 
 Pct Recovery = 54%  Analysis Date = 03/21/16 
 Pct Recovery = 54%  Analysis Date = 03/21/16 
 Pct Recovery = 54%  Analysis Date = 03/18/16 
 Pct Recovery = 54%  Analysis Date = 03/18/16 
 Pct Recovery = 54%  Analysis Date = 03/16/16 
 Pct Recovery = 53%  Analysis Date = 03/16/16 
 Pct Recovery = 53%  Analysis Date = 03/14/16 
 Pct Recovery = 53%  Analysis Date = 03/14/16 
 Pct Recovery = 53%  Analysis Date = 03/11/16 
 Pct Recovery = 53%  Analysis Date = 03/11/16 
 Pct Recovery = 53%  Analysis Date = 03/09/16 
 Pct Recovery = 52%  Analysis Date = 03/09/16 
 Pct Recovery = 52%  Analysis Date = 03/07/16 
 Pct Recovery = 52%  Analysis Date = 03/07/16 
 Pct Recovery = 52%  Analysis Date = 03/05/16 
 Pct Recovery = 52%  Analysis Date = 03/05/16 
 Pct Recovery = 52%  Analysis Date = 03/02/16 
 Pct Recovery = 52%  Analysis Date = 03/02/16 
 Pct Recovery = 52%  Analysis Date = 02/29/16 
 Pct Recovery = 51%  Analysis Date = 02/29/16 
 Pct Recovery = 51%  Analysis Date = 02/27/16 
 Pct Recovery = 51%  Analysis Date = 02/27/16 
 Pct Recovery = 51%  Analysis Date = 02/24/16 
 Pct Recovery = 51%  Analysis Date = 02/24/16 
 Pct Recovery = 51%  Analysis Date = 02/22/16 
 Pct Recovery = 50%  Analysis Date = 02/22/16 
 Pct Recovery = 50%  Analysis Date = 02/20/16 
 Pct Recovery = 50%  Analysis Date = 02/20/16 
 Pct Recovery = 50%  Analysis Date = 02/18/16 
 Pct Recovery = 50%  Analysis Date = 02/18/16 
 Pct Recovery = 50%  Analysis Date = 02/15/16 
 Pct Recovery = 49%  Analysis Date = 02/15/16 
 Pct Recovery = 49%  Analysis Date = 02/13/16 
 Pct Recovery = 49%  Analysis Date = 02/13/16 
 Pct Recovery = 49%  Analysis Date = 02/11/16 
 Pct Recovery = 49%  Analysis Date = 02/11/16 
 Pct Recovery = 49%  Analysis Date = 02/09/16 
 Pct Recovery = 48%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLORO-2-METHYLPHENOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 58% 12% 58% 8%
Total 18 58% 12% 58% 8%

Sample Statistics
4-CHLORO-2-METHYLPHENOL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ACETOCHLOR
METHOD: 2033 , TESTIDCODE: 49260GCM33

 Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 109%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 102%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 96%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 89%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 96%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 110%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 75%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 97%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 83%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 101%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 87%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 85%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 98%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 98%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 98%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 83%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 77%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 85%  Analysis Date = 05/10/17 
 Pct Recovery = 93%  Analysis Date = 05/08/17 
 Pct Recovery = 93%  Analysis Date = 05/08/17 
 Pct Recovery = 93%  Analysis Date = 05/06/17 
 Pct Recovery = 93%  Analysis Date = 05/06/17 
 Pct Recovery = 93%  Analysis Date = 05/04/17 
 Pct Recovery = 93%  Analysis Date = 05/04/17 
 Pct Recovery = 93%  Analysis Date = 05/01/17 
 Pct Recovery = 93%  Analysis Date = 05/01/17 
 Pct Recovery = 93%  Analysis Date = 04/29/17 
 Pct Recovery = 93%  Analysis Date = 04/29/17 
 Pct Recovery = 93%  Analysis Date = 04/27/17 
 Pct Recovery = 93%  Analysis Date = 04/27/17 
 Pct Recovery = 93%  Analysis Date = 04/25/17 
 Pct Recovery = 93%  Analysis Date = 04/25/17 
 Pct Recovery = 93%  Analysis Date = 04/22/17 
 Pct Recovery = 93%  Analysis Date = 04/22/17 
 Pct Recovery = 93%  Analysis Date = 04/20/17 
 Pct Recovery = 93%  Analysis Date = 04/20/17 
 Pct Recovery = 93%  Analysis Date = 04/18/17 
 Pct Recovery = 93%  Analysis Date = 04/18/17 
 Pct Recovery = 93%  Analysis Date = 04/15/17 
 Pct Recovery = 93%  Analysis Date = 04/15/17 
 Pct Recovery = 93%  Analysis Date = 04/13/17 
 Pct Recovery = 93%  Analysis Date = 04/13/17 
 Pct Recovery = 93%  Analysis Date = 04/11/17 
 Pct Recovery = 93%  Analysis Date = 04/11/17 
 Pct Recovery = 93%  Analysis Date = 04/09/17 
 Pct Recovery = 93%  Analysis Date = 04/09/17 
 Pct Recovery = 93%  Analysis Date = 04/06/17 
 Pct Recovery = 93%  Analysis Date = 04/06/17 
 Pct Recovery = 93%  Analysis Date = 04/04/17 
 Pct Recovery = 93%  Analysis Date = 04/04/17 
 Pct Recovery = 93%  Analysis Date = 04/02/17 
 Pct Recovery = 93%  Analysis Date = 04/02/17 
 Pct Recovery = 93%  Analysis Date = 03/30/17 
 Pct Recovery = 93%  Analysis Date = 03/30/17 
 Pct Recovery = 93%  Analysis Date = 03/28/17 
 Pct Recovery = 93%  Analysis Date = 03/28/17 
 Pct Recovery = 93%  Analysis Date = 03/26/17 
 Pct Recovery = 93%  Analysis Date = 03/26/17 
 Pct Recovery = 93%  Analysis Date = 03/24/17 
 Pct Recovery = 94%  Analysis Date = 03/24/17 
 Pct Recovery = 94%  Analysis Date = 03/21/17 
 Pct Recovery = 94%  Analysis Date = 03/21/17 
 Pct Recovery = 94%  Analysis Date = 03/19/17 
 Pct Recovery = 94%  Analysis Date = 03/19/17 
 Pct Recovery = 94%  Analysis Date = 03/17/17 
 Pct Recovery = 94%  Analysis Date = 03/17/17 
 Pct Recovery = 94%  Analysis Date = 03/14/17 
 Pct Recovery = 94%  Analysis Date = 03/14/17 
 Pct Recovery = 94%  Analysis Date = 03/12/17 
 Pct Recovery = 94%  Analysis Date = 03/12/17 
 Pct Recovery = 94%  Analysis Date = 03/10/17 
 Pct Recovery = 94%  Analysis Date = 03/10/17 
 Pct Recovery = 94%  Analysis Date = 03/08/17 
 Pct Recovery = 94%  Analysis Date = 03/08/17 
 Pct Recovery = 94%  Analysis Date = 03/05/17 
 Pct Recovery = 94%  Analysis Date = 03/05/17 
 Pct Recovery = 94%  Analysis Date = 03/03/17 
 Pct Recovery = 94%  Analysis Date = 03/03/17 
 Pct Recovery = 94%  Analysis Date = 03/01/17 
 Pct Recovery = 94%  Analysis Date = 03/01/17 
 Pct Recovery = 94%  Analysis Date = 02/26/17 
 Pct Recovery = 94%  Analysis Date = 02/26/17 
 Pct Recovery = 94%  Analysis Date = 02/24/17 
 Pct Recovery = 94%  Analysis Date = 02/24/17 
 Pct Recovery = 94%  Analysis Date = 02/22/17 
 Pct Recovery = 94%  Analysis Date = 02/22/17 
 Pct Recovery = 94%  Analysis Date = 02/20/17 
 Pct Recovery = 94%  Analysis Date = 02/20/17 
 Pct Recovery = 94%  Analysis Date = 02/17/17 
 Pct Recovery = 94%  Analysis Date = 02/17/17 
 Pct Recovery = 94%  Analysis Date = 02/15/17 
 Pct Recovery = 94%  Analysis Date = 02/15/17 
 Pct Recovery = 94%  Analysis Date = 02/13/17 
 Pct Recovery = 94%  Analysis Date = 02/13/17 
 Pct Recovery = 94%  Analysis Date = 02/10/17 
 Pct Recovery = 94%  Analysis Date = 02/10/17 
 Pct Recovery = 94%  Analysis Date = 02/08/17 
 Pct Recovery = 94%  Analysis Date = 02/08/17 
 Pct Recovery = 94%  Analysis Date = 02/06/17 
 Pct Recovery = 94%  Analysis Date = 02/06/17 
 Pct Recovery = 94%  Analysis Date = 02/04/17 
 Pct Recovery = 94%  Analysis Date = 02/04/17 
 Pct Recovery = 94%  Analysis Date = 02/01/17 
 Pct Recovery = 94%  Analysis Date = 02/01/17 
 Pct Recovery = 94%  Analysis Date = 01/30/17 
 Pct Recovery = 94%  Analysis Date = 01/30/17 
 Pct Recovery = 94%  Analysis Date = 01/28/17 
 Pct Recovery = 94%  Analysis Date = 01/28/17 
 Pct Recovery = 94%  Analysis Date = 01/25/17 
 Pct Recovery = 94%  Analysis Date = 01/25/17 
 Pct Recovery = 94%  Analysis Date = 01/23/17 
 Pct Recovery = 94%  Analysis Date = 01/23/17 
 Pct Recovery = 94%  Analysis Date = 01/21/17 
 Pct Recovery = 94%  Analysis Date = 01/21/17 
 Pct Recovery = 94%  Analysis Date = 01/19/17 
 Pct Recovery = 94%  Analysis Date = 01/19/17 
 Pct Recovery = 94%  Analysis Date = 01/16/17 
 Pct Recovery = 94%  Analysis Date = 01/16/17 
 Pct Recovery = 94%  Analysis Date = 01/14/17 
 Pct Recovery = 95%  Analysis Date = 01/14/17 
 Pct Recovery = 95%  Analysis Date = 01/12/17 
 Pct Recovery = 95%  Analysis Date = 01/12/17 
 Pct Recovery = 95%  Analysis Date = 01/09/17 
 Pct Recovery = 95%  Analysis Date = 01/09/17 
 Pct Recovery = 95%  Analysis Date = 01/07/17 
 Pct Recovery = 95%  Analysis Date = 01/07/17 
 Pct Recovery = 95%  Analysis Date = 01/05/17 
 Pct Recovery = 95%  Analysis Date = 01/05/17 
 Pct Recovery = 95%  Analysis Date = 01/03/17 
 Pct Recovery = 95%  Analysis Date = 01/03/17 
 Pct Recovery = 95%  Analysis Date = 12/31/16 
 Pct Recovery = 95%  Analysis Date = 12/31/16 
 Pct Recovery = 95%  Analysis Date = 12/29/16 
 Pct Recovery = 95%  Analysis Date = 12/29/16 
 Pct Recovery = 95%  Analysis Date = 12/27/16 
 Pct Recovery = 96%  Analysis Date = 12/27/16 
 Pct Recovery = 96%  Analysis Date = 12/24/16 
 Pct Recovery = 96%  Analysis Date = 12/24/16 
 Pct Recovery = 96%  Analysis Date = 12/22/16 
 Pct Recovery = 96%  Analysis Date = 12/22/16 
 Pct Recovery = 96%  Analysis Date = 12/20/16 
 Pct Recovery = 96%  Analysis Date = 12/20/16 
 Pct Recovery = 96%  Analysis Date = 12/18/16 
 Pct Recovery = 96%  Analysis Date = 12/18/16 
 Pct Recovery = 96%  Analysis Date = 12/15/16 
 Pct Recovery = 96%  Analysis Date = 12/15/16 
 Pct Recovery = 96%  Analysis Date = 12/13/16 
 Pct Recovery = 96%  Analysis Date = 12/13/16 
 Pct Recovery = 96%  Analysis Date = 12/11/16 
 Pct Recovery = 96%  Analysis Date = 12/11/16 
 Pct Recovery = 96%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/06/16 
 Pct Recovery = 97%  Analysis Date = 12/06/16 
 Pct Recovery = 97%  Analysis Date = 12/04/16 
 Pct Recovery = 97%  Analysis Date = 12/04/16 
 Pct Recovery = 97%  Analysis Date = 12/02/16 
 Pct Recovery = 97%  Analysis Date = 12/02/16 
 Pct Recovery = 97%  Analysis Date = 11/29/16 
 Pct Recovery = 97%  Analysis Date = 11/29/16 
 Pct Recovery = 97%  Analysis Date = 11/27/16 
 Pct Recovery = 97%  Analysis Date = 11/27/16 
 Pct Recovery = 97%  Analysis Date = 11/25/16 
 Pct Recovery = 97%  Analysis Date = 11/25/16 
 Pct Recovery = 97%  Analysis Date = 11/22/16 
 Pct Recovery = 97%  Analysis Date = 11/22/16 
 Pct Recovery = 97%  Analysis Date = 11/20/16 
 Pct Recovery = 98%  Analysis Date = 11/20/16 
 Pct Recovery = 98%  Analysis Date = 11/18/16 
 Pct Recovery = 98%  Analysis Date = 11/18/16 
 Pct Recovery = 98%  Analysis Date = 11/16/16 
 Pct Recovery = 98%  Analysis Date = 11/16/16 
 Pct Recovery = 98%  Analysis Date = 11/13/16 
 Pct Recovery = 98%  Analysis Date = 11/13/16 
 Pct Recovery = 98%  Analysis Date = 11/11/16 
 Pct Recovery = 98%  Analysis Date = 11/11/16 
 Pct Recovery = 98%  Analysis Date = 11/09/16 
 Pct Recovery = 98%  Analysis Date = 11/09/16 
 Pct Recovery = 98%  Analysis Date = 11/06/16 
 Pct Recovery = 98%  Analysis Date = 11/06/16 
 Pct Recovery = 98%  Analysis Date = 11/04/16 
 Pct Recovery = 99%  Analysis Date = 11/04/16 
 Pct Recovery = 99%  Analysis Date = 11/02/16 
 Pct Recovery = 99%  Analysis Date = 11/02/16 
 Pct Recovery = 99%  Analysis Date = 10/31/16 
 Pct Recovery = 99%  Analysis Date = 10/31/16 
 Pct Recovery = 99%  Analysis Date = 10/28/16 
 Pct Recovery = 99%  Analysis Date = 10/28/16 
 Pct Recovery = 99%  Analysis Date = 10/26/16 
 Pct Recovery = 99%  Analysis Date = 10/26/16 
 Pct Recovery = 99%  Analysis Date = 10/24/16 
 Pct Recovery = 99%  Analysis Date = 10/24/16 
 Pct Recovery = 99%  Analysis Date = 10/21/16 
 Pct Recovery = 99%  Analysis Date = 10/21/16 
 Pct Recovery = 99%  Analysis Date = 10/19/16 
 Pct Recovery = 99%  Analysis Date = 10/19/16 
 Pct Recovery = 99%  Analysis Date = 10/17/16 
 Pct Recovery = 100%  Analysis Date = 10/17/16 
 Pct Recovery = 100%  Analysis Date = 10/15/16 
 Pct Recovery = 100%  Analysis Date = 10/15/16 
 Pct Recovery = 100%  Analysis Date = 10/12/16 
 Pct Recovery = 100%  Analysis Date = 10/12/16 
 Pct Recovery = 100%  Analysis Date = 10/10/16 
 Pct Recovery = 100%  Analysis Date = 10/10/16 
 Pct Recovery = 100%  Analysis Date = 10/08/16 
 Pct Recovery = 100%  Analysis Date = 10/08/16 
 Pct Recovery = 100%  Analysis Date = 10/05/16 
 Pct Recovery = 100%  Analysis Date = 10/05/16 
 Pct Recovery = 100%  Analysis Date = 10/03/16 
 Pct Recovery = 100%  Analysis Date = 10/03/16 
 Pct Recovery = 100%  Analysis Date = 10/01/16 
 Pct Recovery = 100%  Analysis Date = 10/01/16 
 Pct Recovery = 100%  Analysis Date = 09/29/16 
 Pct Recovery = 101%  Analysis Date = 09/29/16 
 Pct Recovery = 101%  Analysis Date = 09/26/16 
 Pct Recovery = 101%  Analysis Date = 09/26/16 
 Pct Recovery = 101%  Analysis Date = 09/24/16 
 Pct Recovery = 101%  Analysis Date = 09/24/16 
 Pct Recovery = 101%  Analysis Date = 09/22/16 
 Pct Recovery = 101%  Analysis Date = 09/22/16 
 Pct Recovery = 101%  Analysis Date = 09/19/16 
 Pct Recovery = 101%  Analysis Date = 09/19/16 
 Pct Recovery = 101%  Analysis Date = 09/17/16 
 Pct Recovery = 101%  Analysis Date = 09/17/16 
 Pct Recovery = 101%  Analysis Date = 09/15/16 
 Pct Recovery = 101%  Analysis Date = 09/15/16 
 Pct Recovery = 101%  Analysis Date = 09/13/16 
 Pct Recovery = 101%  Analysis Date = 09/13/16 
 Pct Recovery = 101%  Analysis Date = 09/10/16 
 Pct Recovery = 102%  Analysis Date = 09/10/16 
 Pct Recovery = 102%  Analysis Date = 09/08/16 
 Pct Recovery = 102%  Analysis Date = 09/08/16 
 Pct Recovery = 102%  Analysis Date = 09/06/16 
 Pct Recovery = 102%  Analysis Date = 09/06/16 
 Pct Recovery = 102%  Analysis Date = 09/03/16 
 Pct Recovery = 101%  Analysis Date = 09/03/16 
 Pct Recovery = 101%  Analysis Date = 09/01/16 
 Pct Recovery = 101%  Analysis Date = 09/01/16 
 Pct Recovery = 101%  Analysis Date = 08/30/16 
 Pct Recovery = 101%  Analysis Date = 08/30/16 
 Pct Recovery = 101%  Analysis Date = 08/28/16 
 Pct Recovery = 101%  Analysis Date = 08/28/16 
 Pct Recovery = 101%  Analysis Date = 08/25/16 
 Pct Recovery = 101%  Analysis Date = 08/25/16 
 Pct Recovery = 101%  Analysis Date = 08/23/16 
 Pct Recovery = 101%  Analysis Date = 08/23/16 
 Pct Recovery = 101%  Analysis Date = 08/21/16 
 Pct Recovery = 101%  Analysis Date = 08/21/16 
 Pct Recovery = 101%  Analysis Date = 08/18/16 
 Pct Recovery = 101%  Analysis Date = 08/18/16 
 Pct Recovery = 101%  Analysis Date = 08/16/16 
 Pct Recovery = 101%  Analysis Date = 08/16/16 
 Pct Recovery = 101%  Analysis Date = 08/14/16 
 Pct Recovery = 100%  Analysis Date = 08/14/16 
 Pct Recovery = 100%  Analysis Date = 08/12/16 
 Pct Recovery = 100%  Analysis Date = 08/12/16 
 Pct Recovery = 100%  Analysis Date = 08/09/16 
 Pct Recovery = 100%  Analysis Date = 08/09/16 
 Pct Recovery = 100%  Analysis Date = 08/07/16 
 Pct Recovery = 100%  Analysis Date = 08/07/16 
 Pct Recovery = 100%  Analysis Date = 08/05/16 
 Pct Recovery = 99%  Analysis Date = 08/05/16 
 Pct Recovery = 99%  Analysis Date = 08/02/16 
 Pct Recovery = 99%  Analysis Date = 08/02/16 
 Pct Recovery = 99%  Analysis Date = 07/31/16 
 Pct Recovery = 99%  Analysis Date = 07/31/16 
 Pct Recovery = 99%  Analysis Date = 07/29/16 
 Pct Recovery = 98%  Analysis Date = 07/29/16 
 Pct Recovery = 98%  Analysis Date = 07/27/16 
 Pct Recovery = 98%  Analysis Date = 07/27/16 
 Pct Recovery = 98%  Analysis Date = 07/24/16 
 Pct Recovery = 98%  Analysis Date = 07/24/16 
 Pct Recovery = 98%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/22/16 
 Pct Recovery = 97%  Analysis Date = 07/20/16 
 Pct Recovery = 97%  Analysis Date = 07/20/16 
 Pct Recovery = 97%  Analysis Date = 07/17/16 
 Pct Recovery = 97%  Analysis Date = 07/17/16 
 Pct Recovery = 97%  Analysis Date = 07/15/16 
 Pct Recovery = 97%  Analysis Date = 07/15/16 
 Pct Recovery = 97%  Analysis Date = 07/13/16 
 Pct Recovery = 96%  Analysis Date = 07/13/16 
 Pct Recovery = 96%  Analysis Date = 07/11/16 
 Pct Recovery = 96%  Analysis Date = 07/11/16 
 Pct Recovery = 96%  Analysis Date = 07/08/16 
 Pct Recovery = 96%  Analysis Date = 07/08/16 
 Pct Recovery = 96%  Analysis Date = 07/06/16 
 Pct Recovery = 95%  Analysis Date = 07/06/16 
 Pct Recovery = 95%  Analysis Date = 07/04/16 
 Pct Recovery = 95%  Analysis Date = 07/04/16 
 Pct Recovery = 95%  Analysis Date = 07/01/16 
 Pct Recovery = 95%  Analysis Date = 07/01/16 
 Pct Recovery = 95%  Analysis Date = 06/29/16 
 Pct Recovery = 94%  Analysis Date = 06/29/16 
 Pct Recovery = 94%  Analysis Date = 06/27/16 
 Pct Recovery = 94%  Analysis Date = 06/27/16 
 Pct Recovery = 94%  Analysis Date = 06/25/16 
 Pct Recovery = 94%  Analysis Date = 06/25/16 
 Pct Recovery = 94%  Analysis Date = 06/22/16 
 Pct Recovery = 94%  Analysis Date = 06/22/16 
 Pct Recovery = 94%  Analysis Date = 06/20/16 
 Pct Recovery = 93%  Analysis Date = 06/20/16 
 Pct Recovery = 93%  Analysis Date = 06/18/16 
 Pct Recovery = 93%  Analysis Date = 06/18/16 
 Pct Recovery = 93%  Analysis Date = 06/15/16 
 Pct Recovery = 93%  Analysis Date = 06/15/16 
 Pct Recovery = 93%  Analysis Date = 06/13/16 
 Pct Recovery = 92%  Analysis Date = 06/13/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/11/16 
 Pct Recovery = 92%  Analysis Date = 06/09/16 
 Pct Recovery = 92%  Analysis Date = 06/09/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/06/16 
 Pct Recovery = 92%  Analysis Date = 06/04/16 
 Pct Recovery = 91%  Analysis Date = 06/04/16 
 Pct Recovery = 91%  Analysis Date = 06/02/16 
 Pct Recovery = 91%  Analysis Date = 06/02/16 
 Pct Recovery = 91%  Analysis Date = 05/30/16 
 Pct Recovery = 91%  Analysis Date = 05/30/16 
 Pct Recovery = 91%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/28/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/26/16 
 Pct Recovery = 90%  Analysis Date = 05/24/16 
 Pct Recovery = 90%  Analysis Date = 05/24/16 
 Pct Recovery = 90%  Analysis Date = 05/21/16 
 Pct Recovery = 89%  Analysis Date = 05/21/16 
 Pct Recovery = 89%  Analysis Date = 05/19/16 
 Pct Recovery = 89%  Analysis Date = 05/19/16 
 Pct Recovery = 89%  Analysis Date = 05/17/16 
 Pct Recovery = 89%  Analysis Date = 05/17/16 
 Pct Recovery = 89%  Analysis Date = 05/14/16 
 Pct Recovery = 88%  Analysis Date = 05/14/16 
 Pct Recovery = 88%  Analysis Date = 05/12/16 
 Pct Recovery = 88%  Analysis Date = 05/12/16 
 Pct Recovery = 88%  Analysis Date = 05/10/16 
 Pct Recovery = 88%  Analysis Date = 05/10/16 
 Pct Recovery = 88%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/05/16 
 Pct Recovery = 87%  Analysis Date = 05/05/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 05/03/16 
 Pct Recovery = 87%  Analysis Date = 05/01/16 
 Pct Recovery = 86%  Analysis Date = 05/01/16 
 Pct Recovery = 86%  Analysis Date = 04/28/16 
 Pct Recovery = 86%  Analysis Date = 04/28/16 
 Pct Recovery = 86%  Analysis Date = 04/26/16 
 Pct Recovery = 86%  Analysis Date = 04/26/16 
 Pct Recovery = 86%  Analysis Date = 04/24/16 
 Pct Recovery = 86%  Analysis Date = 04/24/16 
 Pct Recovery = 86%  Analysis Date = 04/22/16 
 Pct Recovery = 85%  Analysis Date = 04/22/16 
 Pct Recovery = 85%  Analysis Date = 04/19/16 
 Pct Recovery = 85%  Analysis Date = 04/19/16 
 Pct Recovery = 85%  Analysis Date = 04/17/16 
 Pct Recovery = 85%  Analysis Date = 04/17/16 
 Pct Recovery = 85%  Analysis Date = 04/15/16 
 Pct Recovery = 85%  Analysis Date = 04/15/16 
 Pct Recovery = 85%  Analysis Date = 04/12/16 
 Pct Recovery = 85%  Analysis Date = 04/12/16 
 Pct Recovery = 85%  Analysis Date = 04/10/16 
 Pct Recovery = 84%  Analysis Date = 04/10/16 
 Pct Recovery = 84%  Analysis Date = 04/08/16 
 Pct Recovery = 84%  Analysis Date = 04/08/16 
 Pct Recovery = 84%  Analysis Date = 04/06/16 
 Pct Recovery = 84%  Analysis Date = 04/06/16 
 Pct Recovery = 84%  Analysis Date = 04/03/16 
 Pct Recovery = 84%  Analysis Date = 04/03/16 
 Pct Recovery = 84%  Analysis Date = 04/01/16 
 Pct Recovery = 84%  Analysis Date = 04/01/16 
 Pct Recovery = 84%  Analysis Date = 03/30/16 
 Pct Recovery = 83%  Analysis Date = 03/30/16 
 Pct Recovery = 83%  Analysis Date = 03/27/16 
 Pct Recovery = 83%  Analysis Date = 03/27/16 
 Pct Recovery = 83%  Analysis Date = 03/25/16 
 Pct Recovery = 83%  Analysis Date = 03/25/16 
 Pct Recovery = 83%  Analysis Date = 03/23/16 
 Pct Recovery = 83%  Analysis Date = 03/23/16 
 Pct Recovery = 83%  Analysis Date = 03/21/16 
 Pct Recovery = 83%  Analysis Date = 03/21/16 
 Pct Recovery = 83%  Analysis Date = 03/18/16 
 Pct Recovery = 82%  Analysis Date = 03/18/16 
 Pct Recovery = 82%  Analysis Date = 03/16/16 
 Pct Recovery = 82%  Analysis Date = 03/16/16 
 Pct Recovery = 82%  Analysis Date = 03/14/16 
 Pct Recovery = 82%  Analysis Date = 03/14/16 
 Pct Recovery = 82%  Analysis Date = 03/11/16 
 Pct Recovery = 82%  Analysis Date = 03/11/16 
 Pct Recovery = 82%  Analysis Date = 03/09/16 
 Pct Recovery = 82%  Analysis Date = 03/09/16 
 Pct Recovery = 82%  Analysis Date = 03/07/16 
 Pct Recovery = 81%  Analysis Date = 03/07/16 
 Pct Recovery = 81%  Analysis Date = 03/05/16 
 Pct Recovery = 81%  Analysis Date = 03/05/16 
 Pct Recovery = 81%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 03/02/16 
 Pct Recovery = 81%  Analysis Date = 02/29/16 
 Pct Recovery = 81%  Analysis Date = 02/29/16 
 Pct Recovery = 81%  Analysis Date = 02/27/16 
 Pct Recovery = 81%  Analysis Date = 02/27/16 
 Pct Recovery = 81%  Analysis Date = 02/24/16 
 Pct Recovery = 81%  Analysis Date = 02/24/16 
 Pct Recovery = 81%  Analysis Date = 02/22/16 
 Pct Recovery = 80%  Analysis Date = 02/22/16 
 Pct Recovery = 80%  Analysis Date = 02/20/16 
 Pct Recovery = 80%  Analysis Date = 02/20/16 
 Pct Recovery = 80%  Analysis Date = 02/18/16 
 Pct Recovery = 80%  Analysis Date = 02/18/16 
 Pct Recovery = 80%  Analysis Date = 02/15/16 
 Pct Recovery = 80%  Analysis Date = 02/15/16 
 Pct Recovery = 80%  Analysis Date = 02/13/16 
 Pct Recovery = 80%  Analysis Date = 02/13/16 
 Pct Recovery = 80%  Analysis Date = 02/11/16 
 Pct Recovery = 79%  Analysis Date = 02/11/16 
 Pct Recovery = 79%  Analysis Date = 02/09/16 
 Pct Recovery = 79%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 93% 10% 96% 10%
Total 19 93% 10% 96% 10%

Sample Statistics
ACETOCHLOR

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
ALACHLOR
METHOD: 2033 , TESTIDCODE: 46342GCM35

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 114%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 99%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 94%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 96%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 63%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 75%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 96%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 125%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 101%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 101%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 85%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 96%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 84%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 82%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 106%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 90%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 90%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 95%  Analysis Date = 05/02/17 
 Pct Recovery = 101%  Analysis Date = 04/30/17 
 Pct Recovery = 101%  Analysis Date = 04/30/17 
 Pct Recovery = 101%  Analysis Date = 04/28/17 
 Pct Recovery = 102%  Analysis Date = 04/28/17 
 Pct Recovery = 102%  Analysis Date = 04/26/17 
 Pct Recovery = 102%  Analysis Date = 04/26/17 
 Pct Recovery = 102%  Analysis Date = 04/24/17 
 Pct Recovery = 102%  Analysis Date = 04/24/17 
 Pct Recovery = 102%  Analysis Date = 04/21/17 
 Pct Recovery = 102%  Analysis Date = 04/21/17 
 Pct Recovery = 102%  Analysis Date = 04/19/17 
 Pct Recovery = 102%  Analysis Date = 04/19/17 
 Pct Recovery = 102%  Analysis Date = 04/17/17 
 Pct Recovery = 102%  Analysis Date = 04/17/17 
 Pct Recovery = 102%  Analysis Date = 04/15/17 
 Pct Recovery = 102%  Analysis Date = 04/15/17 
 Pct Recovery = 102%  Analysis Date = 04/12/17 
 Pct Recovery = 102%  Analysis Date = 04/12/17 
 Pct Recovery = 102%  Analysis Date = 04/10/17 
 Pct Recovery = 102%  Analysis Date = 04/10/17 
 Pct Recovery = 102%  Analysis Date = 04/08/17 
 Pct Recovery = 102%  Analysis Date = 04/08/17 
 Pct Recovery = 102%  Analysis Date = 04/06/17 
 Pct Recovery = 102%  Analysis Date = 04/06/17 
 Pct Recovery = 102%  Analysis Date = 04/03/17 
 Pct Recovery = 102%  Analysis Date = 04/03/17 
 Pct Recovery = 102%  Analysis Date = 04/01/17 
 Pct Recovery = 102%  Analysis Date = 04/01/17 
 Pct Recovery = 102%  Analysis Date = 03/30/17 
 Pct Recovery = 102%  Analysis Date = 03/30/17 
 Pct Recovery = 102%  Analysis Date = 03/28/17 
 Pct Recovery = 103%  Analysis Date = 03/28/17 
 Pct Recovery = 103%  Analysis Date = 03/25/17 
 Pct Recovery = 103%  Analysis Date = 03/25/17 
 Pct Recovery = 103%  Analysis Date = 03/23/17 
 Pct Recovery = 103%  Analysis Date = 03/23/17 
 Pct Recovery = 103%  Analysis Date = 03/21/17 
 Pct Recovery = 103%  Analysis Date = 03/21/17 
 Pct Recovery = 103%  Analysis Date = 03/19/17 
 Pct Recovery = 103%  Analysis Date = 03/19/17 
 Pct Recovery = 103%  Analysis Date = 03/16/17 
 Pct Recovery = 103%  Analysis Date = 03/16/17 
 Pct Recovery = 103%  Analysis Date = 03/14/17 
 Pct Recovery = 103%  Analysis Date = 03/14/17 
 Pct Recovery = 103%  Analysis Date = 03/12/17 
 Pct Recovery = 103%  Analysis Date = 03/12/17 
 Pct Recovery = 103%  Analysis Date = 03/10/17 
 Pct Recovery = 103%  Analysis Date = 03/10/17 
 Pct Recovery = 103%  Analysis Date = 03/07/17 
 Pct Recovery = 103%  Analysis Date = 03/07/17 
 Pct Recovery = 103%  Analysis Date = 03/05/17 
 Pct Recovery = 103%  Analysis Date = 03/05/17 
 Pct Recovery = 103%  Analysis Date = 03/03/17 
 Pct Recovery = 103%  Analysis Date = 03/03/17 
 Pct Recovery = 103%  Analysis Date = 03/01/17 
 Pct Recovery = 103%  Analysis Date = 03/01/17 
 Pct Recovery = 103%  Analysis Date = 02/26/17 
 Pct Recovery = 103%  Analysis Date = 02/26/17 
 Pct Recovery = 103%  Analysis Date = 02/24/17 
 Pct Recovery = 103%  Analysis Date = 02/24/17 
 Pct Recovery = 103%  Analysis Date = 02/22/17 
 Pct Recovery = 103%  Analysis Date = 02/22/17 
 Pct Recovery = 103%  Analysis Date = 02/20/17 
 Pct Recovery = 103%  Analysis Date = 02/20/17 
 Pct Recovery = 103%  Analysis Date = 02/17/17 
 Pct Recovery = 103%  Analysis Date = 02/17/17 
 Pct Recovery = 103%  Analysis Date = 02/15/17 
 Pct Recovery = 103%  Analysis Date = 02/15/17 
 Pct Recovery = 103%  Analysis Date = 02/13/17 
 Pct Recovery = 103%  Analysis Date = 02/13/17 
 Pct Recovery = 103%  Analysis Date = 02/11/17 
 Pct Recovery = 103%  Analysis Date = 02/11/17 
 Pct Recovery = 103%  Analysis Date = 02/08/17 
 Pct Recovery = 103%  Analysis Date = 02/08/17 
 Pct Recovery = 103%  Analysis Date = 02/06/17 
 Pct Recovery = 103%  Analysis Date = 02/06/17 
 Pct Recovery = 103%  Analysis Date = 02/04/17 
 Pct Recovery = 102%  Analysis Date = 02/04/17 
 Pct Recovery = 102%  Analysis Date = 02/02/17 
 Pct Recovery = 102%  Analysis Date = 02/02/17 
 Pct Recovery = 102%  Analysis Date = 01/30/17 
 Pct Recovery = 102%  Analysis Date = 01/30/17 
 Pct Recovery = 102%  Analysis Date = 01/28/17 
 Pct Recovery = 102%  Analysis Date = 01/28/17 
 Pct Recovery = 102%  Analysis Date = 01/26/17 
 Pct Recovery = 102%  Analysis Date = 01/26/17 
 Pct Recovery = 102%  Analysis Date = 01/24/17 
 Pct Recovery = 102%  Analysis Date = 01/24/17 
 Pct Recovery = 102%  Analysis Date = 01/21/17 
 Pct Recovery = 101%  Analysis Date = 01/21/17 
 Pct Recovery = 101%  Analysis Date = 01/19/17 
 Pct Recovery = 101%  Analysis Date = 01/19/17 
 Pct Recovery = 101%  Analysis Date = 01/17/17 
 Pct Recovery = 101%  Analysis Date = 01/17/17 
 Pct Recovery = 101%  Analysis Date = 01/15/17 
 Pct Recovery = 101%  Analysis Date = 01/15/17 
 Pct Recovery = 101%  Analysis Date = 01/12/17 
 Pct Recovery = 101%  Analysis Date = 01/12/17 
 Pct Recovery = 101%  Analysis Date = 01/10/17 
 Pct Recovery = 101%  Analysis Date = 01/10/17 
 Pct Recovery = 101%  Analysis Date = 01/08/17 
 Pct Recovery = 100%  Analysis Date = 01/08/17 
 Pct Recovery = 100%  Analysis Date = 01/06/17 
 Pct Recovery = 100%  Analysis Date = 01/06/17 
 Pct Recovery = 100%  Analysis Date = 01/04/17 
 Pct Recovery = 100%  Analysis Date = 01/04/17 
 Pct Recovery = 100%  Analysis Date = 01/01/17 
 Pct Recovery = 100%  Analysis Date = 01/01/17 
 Pct Recovery = 100%  Analysis Date = 12/30/16 
 Pct Recovery = 100%  Analysis Date = 12/30/16 
 Pct Recovery = 100%  Analysis Date = 12/28/16 
 Pct Recovery = 100%  Analysis Date = 12/28/16 
 Pct Recovery = 100%  Analysis Date = 12/26/16 
 Pct Recovery = 99%  Analysis Date = 12/26/16 
 Pct Recovery = 99%  Analysis Date = 12/23/16 
 Pct Recovery = 99%  Analysis Date = 12/23/16 
 Pct Recovery = 99%  Analysis Date = 12/21/16 
 Pct Recovery = 99%  Analysis Date = 12/21/16 
 Pct Recovery = 99%  Analysis Date = 12/19/16 
 Pct Recovery = 99%  Analysis Date = 12/19/16 
 Pct Recovery = 99%  Analysis Date = 12/17/16 
 Pct Recovery = 99%  Analysis Date = 12/17/16 
 Pct Recovery = 99%  Analysis Date = 12/14/16 
 Pct Recovery = 98%  Analysis Date = 12/14/16 
 Pct Recovery = 98%  Analysis Date = 12/12/16 
 Pct Recovery = 98%  Analysis Date = 12/12/16 
 Pct Recovery = 98%  Analysis Date = 12/10/16 
 Pct Recovery = 98%  Analysis Date = 12/10/16 
 Pct Recovery = 98%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/08/16 
 Pct Recovery = 97%  Analysis Date = 12/05/16 
 Pct Recovery = 97%  Analysis Date = 12/05/16 
 Pct Recovery = 97%  Analysis Date = 12/03/16 
 Pct Recovery = 97%  Analysis Date = 12/03/16 
 Pct Recovery = 97%  Analysis Date = 12/01/16 
 Pct Recovery = 97%  Analysis Date = 12/01/16 
 Pct Recovery = 97%  Analysis Date = 11/29/16 
 Pct Recovery = 96%  Analysis Date = 11/29/16 
 Pct Recovery = 96%  Analysis Date = 11/26/16 
 Pct Recovery = 96%  Analysis Date = 11/26/16 
 Pct Recovery = 96%  Analysis Date = 11/24/16 
 Pct Recovery = 96%  Analysis Date = 11/24/16 
 Pct Recovery = 96%  Analysis Date = 11/22/16 
 Pct Recovery = 95%  Analysis Date = 11/22/16 
 Pct Recovery = 95%  Analysis Date = 11/20/16 
 Pct Recovery = 95%  Analysis Date = 11/20/16 
 Pct Recovery = 95%  Analysis Date = 11/17/16 
 Pct Recovery = 95%  Analysis Date = 11/17/16 
 Pct Recovery = 95%  Analysis Date = 11/15/16 
 Pct Recovery = 95%  Analysis Date = 11/15/16 
 Pct Recovery = 95%  Analysis Date = 11/13/16 
 Pct Recovery = 94%  Analysis Date = 11/13/16 
 Pct Recovery = 94%  Analysis Date = 11/11/16 
 Pct Recovery = 94%  Analysis Date = 11/11/16 
 Pct Recovery = 94%  Analysis Date = 11/08/16 
 Pct Recovery = 94%  Analysis Date = 11/08/16 
 Pct Recovery = 94%  Analysis Date = 11/06/16 
 Pct Recovery = 93%  Analysis Date = 11/06/16 
 Pct Recovery = 93%  Analysis Date = 11/04/16 
 Pct Recovery = 93%  Analysis Date = 11/04/16 
 Pct Recovery = 93%  Analysis Date = 11/02/16 
 Pct Recovery = 93%  Analysis Date = 11/02/16 
 Pct Recovery = 93%  Analysis Date = 10/30/16 
 Pct Recovery = 93%  Analysis Date = 10/30/16 
 Pct Recovery = 93%  Analysis Date = 10/28/16 
 Pct Recovery = 92%  Analysis Date = 10/28/16 
 Pct Recovery = 92%  Analysis Date = 10/26/16 
 Pct Recovery = 92%  Analysis Date = 10/26/16 
 Pct Recovery = 92%  Analysis Date = 10/24/16 
 Pct Recovery = 92%  Analysis Date = 10/24/16 
 Pct Recovery = 92%  Analysis Date = 10/21/16 
 Pct Recovery = 91%  Analysis Date = 10/21/16 
 Pct Recovery = 91%  Analysis Date = 10/19/16 
 Pct Recovery = 91%  Analysis Date = 10/19/16 
 Pct Recovery = 91%  Analysis Date = 10/17/16 
 Pct Recovery = 91%  Analysis Date = 10/17/16 
 Pct Recovery = 91%  Analysis Date = 10/15/16 
 Pct Recovery = 91%  Analysis Date = 10/15/16 
 Pct Recovery = 91%  Analysis Date = 10/12/16 
 Pct Recovery = 90%  Analysis Date = 10/12/16 
 Pct Recovery = 90%  Analysis Date = 10/10/16 
 Pct Recovery = 90%  Analysis Date = 10/10/16 
 Pct Recovery = 90%  Analysis Date = 10/08/16 
 Pct Recovery = 90%  Analysis Date = 10/08/16 
 Pct Recovery = 90%  Analysis Date = 10/06/16 
 Pct Recovery = 89%  Analysis Date = 10/06/16 
 Pct Recovery = 89%  Analysis Date = 10/03/16 
 Pct Recovery = 89%  Analysis Date = 10/03/16 
 Pct Recovery = 89%  Analysis Date = 10/01/16 
 Pct Recovery = 89%  Analysis Date = 10/01/16 
 Pct Recovery = 89%  Analysis Date = 09/29/16 
 Pct Recovery = 89%  Analysis Date = 09/29/16 
 Pct Recovery = 89%  Analysis Date = 09/27/16 
 Pct Recovery = 88%  Analysis Date = 09/27/16 
 Pct Recovery = 88%  Analysis Date = 09/24/16 
 Pct Recovery = 88%  Analysis Date = 09/24/16 
 Pct Recovery = 88%  Analysis Date = 09/22/16 
 Pct Recovery = 88%  Analysis Date = 09/22/16 
 Pct Recovery = 88%  Analysis Date = 09/20/16 
 Pct Recovery = 87%  Analysis Date = 09/20/16 
 Pct Recovery = 87%  Analysis Date = 09/18/16 
 Pct Recovery = 87%  Analysis Date = 09/18/16 
 Pct Recovery = 87%  Analysis Date = 09/16/16 
 Pct Recovery = 87%  Analysis Date = 09/16/16 
 Pct Recovery = 87%  Analysis Date = 09/13/16 
 Pct Recovery = 86%  Analysis Date = 09/13/16 
 Pct Recovery = 86%  Analysis Date = 09/11/16 
 Pct Recovery = 86%  Analysis Date = 09/11/16 
 Pct Recovery = 86%  Analysis Date = 09/09/16 
 Pct Recovery = 86%  Analysis Date = 09/09/16 
 Pct Recovery = 86%  Analysis Date = 09/07/16 
 Pct Recovery = 86%  Analysis Date = 09/07/16 
 Pct Recovery = 86%  Analysis Date = 09/04/16 
 Pct Recovery = 85%  Analysis Date = 09/04/16 
 Pct Recovery = 85%  Analysis Date = 09/02/16 
 Pct Recovery = 85%  Analysis Date = 09/02/16 
 Pct Recovery = 85%  Analysis Date = 08/31/16 
 Pct Recovery = 85%  Analysis Date = 08/31/16 
 Pct Recovery = 85%  Analysis Date = 08/29/16 
 Pct Recovery = 85%  Analysis Date = 08/29/16 
 Pct Recovery = 85%  Analysis Date = 08/26/16 
 Pct Recovery = 85%  Analysis Date = 08/26/16 
 Pct Recovery = 85%  Analysis Date = 08/24/16 
 Pct Recovery = 85%  Analysis Date = 08/24/16 
 Pct Recovery = 85%  Analysis Date = 08/22/16 
 Pct Recovery = 85%  Analysis Date = 08/22/16 
 Pct Recovery = 85%  Analysis Date = 08/20/16 
 Pct Recovery = 85%  Analysis Date = 08/20/16 
 Pct Recovery = 85%  Analysis Date = 08/17/16 
 Pct Recovery = 85%  Analysis Date = 08/17/16 
 Pct Recovery = 85%  Analysis Date = 08/15/16 
 Pct Recovery = 85%  Analysis Date = 08/15/16 
 Pct Recovery = 85%  Analysis Date = 08/13/16 
 Pct Recovery = 85%  Analysis Date = 08/13/16 
 Pct Recovery = 85%  Analysis Date = 08/11/16 
 Pct Recovery = 85%  Analysis Date = 08/11/16 
 Pct Recovery = 85%  Analysis Date = 08/08/16 
 Pct Recovery = 85%  Analysis Date = 08/08/16 
 Pct Recovery = 85%  Analysis Date = 08/06/16 
 Pct Recovery = 85%  Analysis Date = 08/06/16 
 Pct Recovery = 85%  Analysis Date = 08/04/16 
 Pct Recovery = 85%  Analysis Date = 08/04/16 
 Pct Recovery = 85%  Analysis Date = 08/02/16 
 Pct Recovery = 85%  Analysis Date = 08/02/16 
 Pct Recovery = 85%  Analysis Date = 07/30/16 
 Pct Recovery = 85%  Analysis Date = 07/30/16 
 Pct Recovery = 85%  Analysis Date = 07/28/16 
 Pct Recovery = 85%  Analysis Date = 07/28/16 
 Pct Recovery = 85%  Analysis Date = 07/26/16 
 Pct Recovery = 85%  Analysis Date = 07/26/16 
 Pct Recovery = 85%  Analysis Date = 07/24/16 
 Pct Recovery = 85%  Analysis Date = 07/24/16 
 Pct Recovery = 85%  Analysis Date = 07/21/16 
 Pct Recovery = 85%  Analysis Date = 07/21/16 
 Pct Recovery = 85%  Analysis Date = 07/19/16 
 Pct Recovery = 86%  Analysis Date = 07/19/16 
 Pct Recovery = 86%  Analysis Date = 07/17/16 
 Pct Recovery = 86%  Analysis Date = 07/17/16 
 Pct Recovery = 86%  Analysis Date = 07/15/16 
 Pct Recovery = 86%  Analysis Date = 07/15/16 
 Pct Recovery = 86%  Analysis Date = 07/12/16 
 Pct Recovery = 86%  Analysis Date = 07/12/16 
 Pct Recovery = 86%  Analysis Date = 07/10/16 
 Pct Recovery = 86%  Analysis Date = 07/10/16 
 Pct Recovery = 86%  Analysis Date = 07/08/16 
 Pct Recovery = 86%  Analysis Date = 07/08/16 
 Pct Recovery = 86%  Analysis Date = 07/06/16 
 Pct Recovery = 86%  Analysis Date = 07/06/16 
 Pct Recovery = 86%  Analysis Date = 07/03/16 
 Pct Recovery = 86%  Analysis Date = 07/03/16 
 Pct Recovery = 86%  Analysis Date = 07/01/16 
 Pct Recovery = 86%  Analysis Date = 07/01/16 
 Pct Recovery = 86%  Analysis Date = 06/29/16 
 Pct Recovery = 86%  Analysis Date = 06/29/16 
 Pct Recovery = 86%  Analysis Date = 06/27/16 
 Pct Recovery = 86%  Analysis Date = 06/27/16 
 Pct Recovery = 86%  Analysis Date = 06/24/16 
 Pct Recovery = 86%  Analysis Date = 06/24/16 
 Pct Recovery = 86%  Analysis Date = 06/22/16 
 Pct Recovery = 86%  Analysis Date = 06/22/16 
 Pct Recovery = 86%  Analysis Date = 06/20/16 
 Pct Recovery = 86%  Analysis Date = 06/20/16 
 Pct Recovery = 86%  Analysis Date = 06/18/16 
 Pct Recovery = 86%  Analysis Date = 06/18/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/13/16 
 Pct Recovery = 86%  Analysis Date = 06/13/16 
 Pct Recovery = 86%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/04/16 
 Pct Recovery = 86%  Analysis Date = 06/04/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 06/02/16 
 Pct Recovery = 86%  Analysis Date = 05/31/16 
 Pct Recovery = 86%  Analysis Date = 05/31/16 
 Pct Recovery = 86%  Analysis Date = 05/29/16 
 Pct Recovery = 86%  Analysis Date = 05/29/16 
 Pct Recovery = 86%  Analysis Date = 05/26/16 
 Pct Recovery = 86%  Analysis Date = 05/26/16 
 Pct Recovery = 86%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/22/16 
 Pct Recovery = 87%  Analysis Date = 05/22/16 
 Pct Recovery = 87%  Analysis Date = 05/20/16 
 Pct Recovery = 87%  Analysis Date = 05/20/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/17/16 
 Pct Recovery = 87%  Analysis Date = 05/15/16 
 Pct Recovery = 87%  Analysis Date = 05/15/16 
 Pct Recovery = 87%  Analysis Date = 05/13/16 
 Pct Recovery = 87%  Analysis Date = 05/13/16 
 Pct Recovery = 87%  Analysis Date = 05/11/16 
 Pct Recovery = 87%  Analysis Date = 05/11/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 87%  Analysis Date = 05/06/16 
 Pct Recovery = 87%  Analysis Date = 05/06/16 
 Pct Recovery = 87%  Analysis Date = 05/04/16 
 Pct Recovery = 87%  Analysis Date = 05/04/16 
 Pct Recovery = 87%  Analysis Date = 05/02/16 
 Pct Recovery = 88%  Analysis Date = 05/02/16 
 Pct Recovery = 88%  Analysis Date = 04/29/16 
 Pct Recovery = 88%  Analysis Date = 04/29/16 
 Pct Recovery = 88%  Analysis Date = 04/27/16 
 Pct Recovery = 88%  Analysis Date = 04/27/16 
 Pct Recovery = 88%  Analysis Date = 04/25/16 
 Pct Recovery = 88%  Analysis Date = 04/25/16 
 Pct Recovery = 88%  Analysis Date = 04/23/16 
 Pct Recovery = 88%  Analysis Date = 04/23/16 
 Pct Recovery = 88%  Analysis Date = 04/20/16 
 Pct Recovery = 88%  Analysis Date = 04/20/16 
 Pct Recovery = 88%  Analysis Date = 04/18/16 
 Pct Recovery = 88%  Analysis Date = 04/18/16 
 Pct Recovery = 88%  Analysis Date = 04/16/16 
 Pct Recovery = 88%  Analysis Date = 04/16/16 
 Pct Recovery = 88%  Analysis Date = 04/14/16 
 Pct Recovery = 89%  Analysis Date = 04/14/16 
 Pct Recovery = 89%  Analysis Date = 04/11/16 
 Pct Recovery = 89%  Analysis Date = 04/11/16 
 Pct Recovery = 89%  Analysis Date = 04/09/16 
 Pct Recovery = 89%  Analysis Date = 04/09/16 
 Pct Recovery = 89%  Analysis Date = 04/07/16 
 Pct Recovery = 89%  Analysis Date = 04/07/16 
 Pct Recovery = 89%  Analysis Date = 04/05/16 
 Pct Recovery = 89%  Analysis Date = 04/05/16 
 Pct Recovery = 89%  Analysis Date = 04/02/16 
 Pct Recovery = 89%  Analysis Date = 04/02/16 
 Pct Recovery = 89%  Analysis Date = 03/31/16 
 Pct Recovery = 89%  Analysis Date = 03/31/16 
 Pct Recovery = 89%  Analysis Date = 03/29/16 
 Pct Recovery = 89%  Analysis Date = 03/29/16 
 Pct Recovery = 89%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/24/16 
 Pct Recovery = 90%  Analysis Date = 03/24/16 
 Pct Recovery = 90%  Analysis Date = 03/22/16 
 Pct Recovery = 90%  Analysis Date = 03/22/16 
 Pct Recovery = 90%  Analysis Date = 03/20/16 
 Pct Recovery = 90%  Analysis Date = 03/20/16 
 Pct Recovery = 90%  Analysis Date = 03/18/16 
 Pct Recovery = 90%  Analysis Date = 03/18/16 
 Pct Recovery = 90%  Analysis Date = 03/15/16 
 Pct Recovery = 90%  Analysis Date = 03/15/16 
 Pct Recovery = 90%  Analysis Date = 03/13/16 
 Pct Recovery = 90%  Analysis Date = 03/13/16 
 Pct Recovery = 90%  Analysis Date = 03/11/16 
 Pct Recovery = 90%  Analysis Date = 03/11/16 
 Pct Recovery = 90%  Analysis Date = 03/09/16 
 Pct Recovery = 91%  Analysis Date = 03/09/16 
 Pct Recovery = 91%  Analysis Date = 03/06/16 
 Pct Recovery = 91%  Analysis Date = 03/06/16 
 Pct Recovery = 91%  Analysis Date = 03/04/16 
 Pct Recovery = 91%  Analysis Date = 03/04/16 
 Pct Recovery = 91%  Analysis Date = 03/02/16 
 Pct Recovery = 91%  Analysis Date = 03/02/16 
 Pct Recovery = 91%  Analysis Date = 02/29/16 
 Pct Recovery = 91%  Analysis Date = 02/29/16 
 Pct Recovery = 91%  Analysis Date = 02/26/16 
 Pct Recovery = 91%  Analysis Date = 02/26/16 
 Pct Recovery = 91%  Analysis Date = 02/24/16 
 Pct Recovery = 91%  Analysis Date = 02/24/16 
 Pct Recovery = 91%  Analysis Date = 02/22/16 
 Pct Recovery = 91%  Analysis Date = 02/22/16 
 Pct Recovery = 91%  Analysis Date = 02/20/16 
 Pct Recovery = 91%  Analysis Date = 02/20/16 
 Pct Recovery = 91%  Analysis Date = 02/17/16 
 Pct Recovery = 92%  Analysis Date = 02/17/16 
 Pct Recovery = 92%  Analysis Date = 02/15/16 
 Pct Recovery = 92%  Analysis Date = 02/15/16 
 Pct Recovery = 92%  Analysis Date = 02/13/16 
 Pct Recovery = 92%  Analysis Date = 02/13/16 
 Pct Recovery = 92%  Analysis Date = 02/11/16 
 Pct Recovery = 92%  Analysis Date = 02/11/16 
 Pct Recovery = 92%  Analysis Date = 02/09/16 
 Pct Recovery = 92%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 94% 14% 95% 11%
Total 18 94% 14% 95% 11%

Sample Statistics
ALACHLOR

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ALPHA-ENDOSULFAN (ENDOSULFAN I)
METHOD: 2033 , TESTIDCODE: 34362GCM39

 Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 108%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 109%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 72%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 78%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 85%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 66%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 97%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 79%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 81%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 90%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 99%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 88%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 108%  Analysis Date = 05/19/16 
 SpikeMix = ChemService 3851600: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 87%  Analysis Date = 04/19/16 
 SpikeMix = ERA 0406-15-01: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 79%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 90%  Analysis Date = 04/14/16 
 SpikeMix = ChemService 3851600: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 101%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 94%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 89%  Analysis Date = 05/10/17 
 Pct Recovery = 88%  Analysis Date = 05/08/17 
 Pct Recovery = 88%  Analysis Date = 05/08/17 
 Pct Recovery = 88%  Analysis Date = 05/06/17 
 Pct Recovery = 88%  Analysis Date = 05/06/17 
 Pct Recovery = 88%  Analysis Date = 05/04/17 
 Pct Recovery = 88%  Analysis Date = 05/04/17 
 Pct Recovery = 88%  Analysis Date = 05/01/17 
 Pct Recovery = 88%  Analysis Date = 05/01/17 
 Pct Recovery = 88%  Analysis Date = 04/29/17 
 Pct Recovery = 88%  Analysis Date = 04/29/17 
 Pct Recovery = 88%  Analysis Date = 04/27/17 
 Pct Recovery = 88%  Analysis Date = 04/27/17 
 Pct Recovery = 88%  Analysis Date = 04/25/17 
 Pct Recovery = 88%  Analysis Date = 04/25/17 
 Pct Recovery = 88%  Analysis Date = 04/22/17 
 Pct Recovery = 88%  Analysis Date = 04/22/17 
 Pct Recovery = 88%  Analysis Date = 04/20/17 
 Pct Recovery = 89%  Analysis Date = 04/20/17 
 Pct Recovery = 89%  Analysis Date = 04/18/17 
 Pct Recovery = 89%  Analysis Date = 04/18/17 
 Pct Recovery = 89%  Analysis Date = 04/15/17 
 Pct Recovery = 89%  Analysis Date = 04/15/17 
 Pct Recovery = 89%  Analysis Date = 04/13/17 
 Pct Recovery = 89%  Analysis Date = 04/13/17 
 Pct Recovery = 89%  Analysis Date = 04/11/17 
 Pct Recovery = 89%  Analysis Date = 04/11/17 
 Pct Recovery = 89%  Analysis Date = 04/09/17 
 Pct Recovery = 89%  Analysis Date = 04/09/17 
 Pct Recovery = 89%  Analysis Date = 04/06/17 
 Pct Recovery = 89%  Analysis Date = 04/06/17 
 Pct Recovery = 89%  Analysis Date = 04/04/17 
 Pct Recovery = 89%  Analysis Date = 04/04/17 
 Pct Recovery = 89%  Analysis Date = 04/02/17 
 Pct Recovery = 89%  Analysis Date = 04/02/17 
 Pct Recovery = 89%  Analysis Date = 03/30/17 
 Pct Recovery = 89%  Analysis Date = 03/30/17 
 Pct Recovery = 89%  Analysis Date = 03/28/17 
 Pct Recovery = 89%  Analysis Date = 03/28/17 
 Pct Recovery = 89%  Analysis Date = 03/26/17 
 Pct Recovery = 89%  Analysis Date = 03/26/17 
 Pct Recovery = 89%  Analysis Date = 03/24/17 
 Pct Recovery = 89%  Analysis Date = 03/24/17 
 Pct Recovery = 89%  Analysis Date = 03/21/17 
 Pct Recovery = 89%  Analysis Date = 03/21/17 
 Pct Recovery = 89%  Analysis Date = 03/19/17 
 Pct Recovery = 89%  Analysis Date = 03/19/17 
 Pct Recovery = 89%  Analysis Date = 03/17/17 
 Pct Recovery = 89%  Analysis Date = 03/17/17 
 Pct Recovery = 89%  Analysis Date = 03/14/17 
 Pct Recovery = 90%  Analysis Date = 03/14/17 
 Pct Recovery = 90%  Analysis Date = 03/12/17 
 Pct Recovery = 90%  Analysis Date = 03/12/17 
 Pct Recovery = 90%  Analysis Date = 03/10/17 
 Pct Recovery = 90%  Analysis Date = 03/10/17 
 Pct Recovery = 90%  Analysis Date = 03/08/17 
 Pct Recovery = 90%  Analysis Date = 03/08/17 
 Pct Recovery = 90%  Analysis Date = 03/05/17 
 Pct Recovery = 90%  Analysis Date = 03/05/17 
 Pct Recovery = 90%  Analysis Date = 03/03/17 
 Pct Recovery = 90%  Analysis Date = 03/03/17 
 Pct Recovery = 90%  Analysis Date = 03/01/17 
 Pct Recovery = 90%  Analysis Date = 03/01/17 
 Pct Recovery = 90%  Analysis Date = 02/26/17 
 Pct Recovery = 90%  Analysis Date = 02/26/17 
 Pct Recovery = 90%  Analysis Date = 02/24/17 
 Pct Recovery = 90%  Analysis Date = 02/24/17 
 Pct Recovery = 90%  Analysis Date = 02/22/17 
 Pct Recovery = 90%  Analysis Date = 02/22/17 
 Pct Recovery = 90%  Analysis Date = 02/20/17 
 Pct Recovery = 90%  Analysis Date = 02/20/17 
 Pct Recovery = 90%  Analysis Date = 02/17/17 
 Pct Recovery = 90%  Analysis Date = 02/17/17 
 Pct Recovery = 90%  Analysis Date = 02/15/17 
 Pct Recovery = 90%  Analysis Date = 02/15/17 
 Pct Recovery = 90%  Analysis Date = 02/13/17 
 Pct Recovery = 90%  Analysis Date = 02/13/17 
 Pct Recovery = 90%  Analysis Date = 02/10/17 
 Pct Recovery = 91%  Analysis Date = 02/10/17 
 Pct Recovery = 91%  Analysis Date = 02/08/17 
 Pct Recovery = 91%  Analysis Date = 02/08/17 
 Pct Recovery = 91%  Analysis Date = 02/06/17 
 Pct Recovery = 91%  Analysis Date = 02/06/17 
 Pct Recovery = 91%  Analysis Date = 02/04/17 
 Pct Recovery = 91%  Analysis Date = 02/04/17 
 Pct Recovery = 91%  Analysis Date = 02/01/17 
 Pct Recovery = 91%  Analysis Date = 02/01/17 
 Pct Recovery = 91%  Analysis Date = 01/30/17 
 Pct Recovery = 91%  Analysis Date = 01/30/17 
 Pct Recovery = 91%  Analysis Date = 01/28/17 
 Pct Recovery = 91%  Analysis Date = 01/28/17 
 Pct Recovery = 91%  Analysis Date = 01/25/17 
 Pct Recovery = 91%  Analysis Date = 01/25/17 
 Pct Recovery = 91%  Analysis Date = 01/23/17 
 Pct Recovery = 91%  Analysis Date = 01/23/17 
 Pct Recovery = 91%  Analysis Date = 01/21/17 
 Pct Recovery = 91%  Analysis Date = 01/21/17 
 Pct Recovery = 91%  Analysis Date = 01/19/17 
 Pct Recovery = 92%  Analysis Date = 01/19/17 
 Pct Recovery = 92%  Analysis Date = 01/16/17 
 Pct Recovery = 92%  Analysis Date = 01/16/17 
 Pct Recovery = 92%  Analysis Date = 01/14/17 
 Pct Recovery = 92%  Analysis Date = 01/14/17 
 Pct Recovery = 92%  Analysis Date = 01/12/17 
 Pct Recovery = 92%  Analysis Date = 01/12/17 
 Pct Recovery = 92%  Analysis Date = 01/09/17 
 Pct Recovery = 92%  Analysis Date = 01/09/17 
 Pct Recovery = 92%  Analysis Date = 01/07/17 
 Pct Recovery = 92%  Analysis Date = 01/07/17 
 Pct Recovery = 92%  Analysis Date = 01/05/17 
 Pct Recovery = 92%  Analysis Date = 01/05/17 
 Pct Recovery = 92%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 01/03/17 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/31/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/29/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/27/16 
 Pct Recovery = 92%  Analysis Date = 12/24/16 
 Pct Recovery = 93%  Analysis Date = 12/24/16 
 Pct Recovery = 93%  Analysis Date = 12/22/16 
 Pct Recovery = 93%  Analysis Date = 12/22/16 
 Pct Recovery = 93%  Analysis Date = 12/20/16 
 Pct Recovery = 93%  Analysis Date = 12/20/16 
 Pct Recovery = 93%  Analysis Date = 12/18/16 
 Pct Recovery = 93%  Analysis Date = 12/18/16 
 Pct Recovery = 93%  Analysis Date = 12/15/16 
 Pct Recovery = 93%  Analysis Date = 12/15/16 
 Pct Recovery = 93%  Analysis Date = 12/13/16 
 Pct Recovery = 93%  Analysis Date = 12/13/16 
 Pct Recovery = 93%  Analysis Date = 12/11/16 
 Pct Recovery = 93%  Analysis Date = 12/11/16 
 Pct Recovery = 93%  Analysis Date = 12/08/16 
 Pct Recovery = 93%  Analysis Date = 12/08/16 
 Pct Recovery = 93%  Analysis Date = 12/06/16 
 Pct Recovery = 92%  Analysis Date = 12/06/16 
 Pct Recovery = 92%  Analysis Date = 12/04/16 
 Pct Recovery = 92%  Analysis Date = 12/04/16 
 Pct Recovery = 92%  Analysis Date = 12/02/16 
 Pct Recovery = 92%  Analysis Date = 12/02/16 
 Pct Recovery = 92%  Analysis Date = 11/29/16 
 Pct Recovery = 92%  Analysis Date = 11/29/16 
 Pct Recovery = 92%  Analysis Date = 11/27/16 
 Pct Recovery = 92%  Analysis Date = 11/27/16 
 Pct Recovery = 92%  Analysis Date = 11/25/16 
 Pct Recovery = 92%  Analysis Date = 11/25/16 
 Pct Recovery = 92%  Analysis Date = 11/22/16 
 Pct Recovery = 92%  Analysis Date = 11/22/16 
 Pct Recovery = 92%  Analysis Date = 11/20/16 
 Pct Recovery = 92%  Analysis Date = 11/20/16 
 Pct Recovery = 92%  Analysis Date = 11/18/16 
 Pct Recovery = 92%  Analysis Date = 11/18/16 
 Pct Recovery = 92%  Analysis Date = 11/16/16 
 Pct Recovery = 92%  Analysis Date = 11/16/16 
 Pct Recovery = 92%  Analysis Date = 11/13/16 
 Pct Recovery = 92%  Analysis Date = 11/13/16 
 Pct Recovery = 92%  Analysis Date = 11/11/16 
 Pct Recovery = 92%  Analysis Date = 11/11/16 
 Pct Recovery = 92%  Analysis Date = 11/09/16 
 Pct Recovery = 92%  Analysis Date = 11/09/16 
 Pct Recovery = 92%  Analysis Date = 11/06/16 
 Pct Recovery = 92%  Analysis Date = 11/06/16 
 Pct Recovery = 92%  Analysis Date = 11/04/16 
 Pct Recovery = 92%  Analysis Date = 11/04/16 
 Pct Recovery = 92%  Analysis Date = 11/02/16 
 Pct Recovery = 92%  Analysis Date = 11/02/16 
 Pct Recovery = 92%  Analysis Date = 10/31/16 
 Pct Recovery = 92%  Analysis Date = 10/31/16 
 Pct Recovery = 92%  Analysis Date = 10/28/16 
 Pct Recovery = 92%  Analysis Date = 10/28/16 
 Pct Recovery = 92%  Analysis Date = 10/26/16 
 Pct Recovery = 92%  Analysis Date = 10/26/16 
 Pct Recovery = 92%  Analysis Date = 10/24/16 
 Pct Recovery = 91%  Analysis Date = 10/24/16 
 Pct Recovery = 91%  Analysis Date = 10/21/16 
 Pct Recovery = 91%  Analysis Date = 10/21/16 
 Pct Recovery = 91%  Analysis Date = 10/19/16 
 Pct Recovery = 91%  Analysis Date = 10/19/16 
 Pct Recovery = 91%  Analysis Date = 10/17/16 
 Pct Recovery = 91%  Analysis Date = 10/17/16 
 Pct Recovery = 91%  Analysis Date = 10/15/16 
 Pct Recovery = 91%  Analysis Date = 10/15/16 
 Pct Recovery = 91%  Analysis Date = 10/12/16 
 Pct Recovery = 91%  Analysis Date = 10/12/16 
 Pct Recovery = 91%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/08/16 
 Pct Recovery = 91%  Analysis Date = 10/08/16 
 Pct Recovery = 91%  Analysis Date = 10/05/16 
 Pct Recovery = 91%  Analysis Date = 10/05/16 
 Pct Recovery = 91%  Analysis Date = 10/03/16 
 Pct Recovery = 91%  Analysis Date = 10/03/16 
 Pct Recovery = 91%  Analysis Date = 10/01/16 
 Pct Recovery = 91%  Analysis Date = 10/01/16 
 Pct Recovery = 91%  Analysis Date = 09/29/16 
 Pct Recovery = 91%  Analysis Date = 09/29/16 
 Pct Recovery = 91%  Analysis Date = 09/26/16 
 Pct Recovery = 91%  Analysis Date = 09/26/16 
 Pct Recovery = 91%  Analysis Date = 09/24/16 
 Pct Recovery = 91%  Analysis Date = 09/24/16 
 Pct Recovery = 91%  Analysis Date = 09/22/16 
 Pct Recovery = 91%  Analysis Date = 09/22/16 
 Pct Recovery = 91%  Analysis Date = 09/19/16 
 Pct Recovery = 91%  Analysis Date = 09/19/16 
 Pct Recovery = 91%  Analysis Date = 09/17/16 
 Pct Recovery = 91%  Analysis Date = 09/17/16 
 Pct Recovery = 91%  Analysis Date = 09/15/16 
 Pct Recovery = 91%  Analysis Date = 09/15/16 
 Pct Recovery = 91%  Analysis Date = 09/13/16 
 Pct Recovery = 91%  Analysis Date = 09/13/16 
 Pct Recovery = 91%  Analysis Date = 09/10/16 
 Pct Recovery = 91%  Analysis Date = 09/10/16 
 Pct Recovery = 91%  Analysis Date = 09/08/16 
 Pct Recovery = 91%  Analysis Date = 09/08/16 
 Pct Recovery = 91%  Analysis Date = 09/06/16 
 Pct Recovery = 91%  Analysis Date = 09/06/16 
 Pct Recovery = 91%  Analysis Date = 09/03/16 
 Pct Recovery = 91%  Analysis Date = 09/03/16 
 Pct Recovery = 91%  Analysis Date = 09/01/16 
 Pct Recovery = 91%  Analysis Date = 09/01/16 
 Pct Recovery = 91%  Analysis Date = 08/30/16 
 Pct Recovery = 91%  Analysis Date = 08/30/16 
 Pct Recovery = 91%  Analysis Date = 08/28/16 
 Pct Recovery = 90%  Analysis Date = 08/28/16 
 Pct Recovery = 90%  Analysis Date = 08/25/16 
 Pct Recovery = 90%  Analysis Date = 08/25/16 
 Pct Recovery = 90%  Analysis Date = 08/23/16 
 Pct Recovery = 90%  Analysis Date = 08/23/16 
 Pct Recovery = 90%  Analysis Date = 08/21/16 
 Pct Recovery = 90%  Analysis Date = 08/21/16 
 Pct Recovery = 90%  Analysis Date = 08/18/16 
 Pct Recovery = 90%  Analysis Date = 08/18/16 
 Pct Recovery = 90%  Analysis Date = 08/16/16 
 Pct Recovery = 90%  Analysis Date = 08/16/16 
 Pct Recovery = 90%  Analysis Date = 08/14/16 
 Pct Recovery = 90%  Analysis Date = 08/14/16 
 Pct Recovery = 90%  Analysis Date = 08/12/16 
 Pct Recovery = 89%  Analysis Date = 08/12/16 
 Pct Recovery = 89%  Analysis Date = 08/09/16 
 Pct Recovery = 89%  Analysis Date = 08/09/16 
 Pct Recovery = 89%  Analysis Date = 08/07/16 
 Pct Recovery = 89%  Analysis Date = 08/07/16 
 Pct Recovery = 89%  Analysis Date = 08/05/16 
 Pct Recovery = 89%  Analysis Date = 08/05/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 08/02/16 
 Pct Recovery = 89%  Analysis Date = 07/31/16 
 Pct Recovery = 89%  Analysis Date = 07/31/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/29/16 
 Pct Recovery = 89%  Analysis Date = 07/27/16 
 Pct Recovery = 89%  Analysis Date = 07/27/16 
 Pct Recovery = 89%  Analysis Date = 07/24/16 
 Pct Recovery = 88%  Analysis Date = 07/24/16 
 Pct Recovery = 88%  Analysis Date = 07/22/16 
 Pct Recovery = 88%  Analysis Date = 07/22/16 
 Pct Recovery = 88%  Analysis Date = 07/20/16 
 Pct Recovery = 88%  Analysis Date = 07/20/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/17/16 
 Pct Recovery = 88%  Analysis Date = 07/15/16 
 Pct Recovery = 88%  Analysis Date = 07/15/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/13/16 
 Pct Recovery = 88%  Analysis Date = 07/11/16 
 Pct Recovery = 88%  Analysis Date = 07/11/16 
 Pct Recovery = 88%  Analysis Date = 07/08/16 
 Pct Recovery = 87%  Analysis Date = 07/08/16 
 Pct Recovery = 87%  Analysis Date = 07/06/16 
 Pct Recovery = 87%  Analysis Date = 07/06/16 
 Pct Recovery = 87%  Analysis Date = 07/04/16 
 Pct Recovery = 87%  Analysis Date = 07/04/16 
 Pct Recovery = 87%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 06/29/16 
 Pct Recovery = 87%  Analysis Date = 06/29/16 
 Pct Recovery = 87%  Analysis Date = 06/27/16 
 Pct Recovery = 87%  Analysis Date = 06/27/16 
 Pct Recovery = 87%  Analysis Date = 06/25/16 
 Pct Recovery = 87%  Analysis Date = 06/25/16 
 Pct Recovery = 87%  Analysis Date = 06/22/16 
 Pct Recovery = 87%  Analysis Date = 06/22/16 
 Pct Recovery = 87%  Analysis Date = 06/20/16 
 Pct Recovery = 86%  Analysis Date = 06/20/16 
 Pct Recovery = 86%  Analysis Date = 06/18/16 
 Pct Recovery = 86%  Analysis Date = 06/18/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/15/16 
 Pct Recovery = 86%  Analysis Date = 06/13/16 
 Pct Recovery = 86%  Analysis Date = 06/13/16 
 Pct Recovery = 86%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/11/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/09/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/06/16 
 Pct Recovery = 86%  Analysis Date = 06/04/16 
 Pct Recovery = 85%  Analysis Date = 06/04/16 
 Pct Recovery = 85%  Analysis Date = 06/02/16 
 Pct Recovery = 85%  Analysis Date = 06/02/16 
 Pct Recovery = 85%  Analysis Date = 05/30/16 
 Pct Recovery = 85%  Analysis Date = 05/30/16 
 Pct Recovery = 85%  Analysis Date = 05/28/16 
 Pct Recovery = 85%  Analysis Date = 05/28/16 
 Pct Recovery = 85%  Analysis Date = 05/26/16 
 Pct Recovery = 85%  Analysis Date = 05/26/16 
 Pct Recovery = 85%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/24/16 
 Pct Recovery = 86%  Analysis Date = 05/21/16 
 Pct Recovery = 86%  Analysis Date = 05/21/16 
 Pct Recovery = 86%  Analysis Date = 05/19/16 
 Pct Recovery = 86%  Analysis Date = 05/19/16 
 Pct Recovery = 86%  Analysis Date = 05/17/16 
 Pct Recovery = 86%  Analysis Date = 05/17/16 
 Pct Recovery = 86%  Analysis Date = 05/14/16 
 Pct Recovery = 87%  Analysis Date = 05/14/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/12/16 
 Pct Recovery = 87%  Analysis Date = 05/10/16 
 Pct Recovery = 87%  Analysis Date = 05/10/16 
 Pct Recovery = 87%  Analysis Date = 05/08/16 
 Pct Recovery = 88%  Analysis Date = 05/08/16 
 Pct Recovery = 88%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/05/16 
 Pct Recovery = 88%  Analysis Date = 05/03/16 
 Pct Recovery = 88%  Analysis Date = 05/03/16 
 Pct Recovery = 88%  Analysis Date = 05/01/16 
 Pct Recovery = 88%  Analysis Date = 05/01/16 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 Pct Recovery = 88%  Analysis Date = 04/28/16 
 Pct Recovery = 88%  Analysis Date = 04/26/16 
 Pct Recovery = 89%  Analysis Date = 04/26/16 
 Pct Recovery = 89%  Analysis Date = 04/24/16 
 Pct Recovery = 89%  Analysis Date = 04/24/16 
 Pct Recovery = 89%  Analysis Date = 04/22/16 
 Pct Recovery = 89%  Analysis Date = 04/22/16 
 Pct Recovery = 89%  Analysis Date = 04/19/16 
 Pct Recovery = 89%  Analysis Date = 04/19/16 
 Pct Recovery = 89%  Analysis Date = 04/17/16 
 Pct Recovery = 89%  Analysis Date = 04/17/16 
 Pct Recovery = 89%  Analysis Date = 04/15/16 
 Pct Recovery = 89%  Analysis Date = 04/15/16 
 Pct Recovery = 89%  Analysis Date = 04/12/16 
 Pct Recovery = 90%  Analysis Date = 04/12/16 
 Pct Recovery = 90%  Analysis Date = 04/10/16 
 Pct Recovery = 90%  Analysis Date = 04/10/16 
 Pct Recovery = 90%  Analysis Date = 04/08/16 
 Pct Recovery = 90%  Analysis Date = 04/08/16 
 Pct Recovery = 90%  Analysis Date = 04/06/16 
 Pct Recovery = 90%  Analysis Date = 04/06/16 
 Pct Recovery = 90%  Analysis Date = 04/03/16 
 Pct Recovery = 90%  Analysis Date = 04/03/16 
 Pct Recovery = 90%  Analysis Date = 04/01/16 
 Pct Recovery = 90%  Analysis Date = 04/01/16 
 Pct Recovery = 90%  Analysis Date = 03/30/16 
 Pct Recovery = 90%  Analysis Date = 03/30/16 
 Pct Recovery = 90%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/27/16 
 Pct Recovery = 90%  Analysis Date = 03/25/16 
 Pct Recovery = 91%  Analysis Date = 03/25/16 
 Pct Recovery = 91%  Analysis Date = 03/23/16 
 Pct Recovery = 91%  Analysis Date = 03/23/16 
 Pct Recovery = 91%  Analysis Date = 03/21/16 
 Pct Recovery = 91%  Analysis Date = 03/21/16 
 Pct Recovery = 91%  Analysis Date = 03/18/16 
 Pct Recovery = 91%  Analysis Date = 03/18/16 
 Pct Recovery = 91%  Analysis Date = 03/16/16 
 Pct Recovery = 91%  Analysis Date = 03/16/16 
 Pct Recovery = 91%  Analysis Date = 03/14/16 
 Pct Recovery = 91%  Analysis Date = 03/14/16 
 Pct Recovery = 91%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/11/16 
 Pct Recovery = 91%  Analysis Date = 03/09/16 
 Pct Recovery = 91%  Analysis Date = 03/09/16 
 Pct Recovery = 91%  Analysis Date = 03/07/16 
 Pct Recovery = 92%  Analysis Date = 03/07/16 
 Pct Recovery = 92%  Analysis Date = 03/05/16 
 Pct Recovery = 92%  Analysis Date = 03/05/16 
 Pct Recovery = 92%  Analysis Date = 03/02/16 
 Pct Recovery = 92%  Analysis Date = 03/02/16 
 Pct Recovery = 92%  Analysis Date = 02/29/16 
 Pct Recovery = 92%  Analysis Date = 02/29/16 
 Pct Recovery = 92%  Analysis Date = 02/27/16 
 Pct Recovery = 92%  Analysis Date = 02/27/16 
 Pct Recovery = 92%  Analysis Date = 02/24/16 
 Pct Recovery = 92%  Analysis Date = 02/24/16 
 Pct Recovery = 92%  Analysis Date = 02/22/16 
 Pct Recovery = 92%  Analysis Date = 02/22/16 
 Pct Recovery = 92%  Analysis Date = 02/20/16 
 Pct Recovery = 92%  Analysis Date = 02/20/16 
 Pct Recovery = 92%  Analysis Date = 02/18/16 
 Pct Recovery = 92%  Analysis Date = 02/18/16 
 Pct Recovery = 92%  Analysis Date = 02/15/16 
 Pct Recovery = 93%  Analysis Date = 02/15/16 
 Pct Recovery = 93%  Analysis Date = 02/13/16 
 Pct Recovery = 93%  Analysis Date = 02/13/16 
 Pct Recovery = 93%  Analysis Date = 02/11/16 
 Pct Recovery = 93%  Analysis Date = 02/11/16 
 Pct Recovery = 93%  Analysis Date = 02/09/16 
 Pct Recovery = 93%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 94% 6% 92% 6%
>= Reporting Level 16 88% 13% 87% 14%
Total 20 89% 12% 89% 13%

Sample Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
ATRAZINE
METHOD: 2033 , TESTIDCODE: 39632GCM35

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 118%  Analysis Date = 02/16/17 
 SpikeMix = Abs 060916: 100 Ál & Phenova B20160331: 100 Ál 
 Pct Recovery = 102%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 86%  Analysis Date = 02/28/17 
 SpikeMix = Abs 060916: 80 Ál & Phenova B20160331: 80 Ál 
 Pct Recovery = 107%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 73%  Analysis Date = 04/19/16 
 SpikeMix = ERA 0406-15-01: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 79%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 70%  Analysis Date = 05/19/16 
 SpikeMix = ChemService 3851600: 40 Ál & Spex Organics EN150513008: 40 Ál 
 Pct Recovery = 85%  Analysis Date = 05/03/17 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 92%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 114%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 12/20/16 
 SpikeMix = Abs 060916: 40 Ál & Phenova B20160331: 40 Ál 
 Pct Recovery = 106%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 88%  Analysis Date = 09/01/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 87%  Analysis Date = 05/28/16 
 SpikeMix = Crescent 03FF076: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 76%  Analysis Date = 05/26/16 
 SpikeMix = NSI 041816: 40 Ál & Crescent 03FF076: 40 Ál 
 Pct Recovery = 73%  Analysis Date = 04/14/16 
 SpikeMix = ChemService 3851600: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 108%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 82%  Analysis Date = 05/02/17 
 Pct Recovery = 94%  Analysis Date = 04/30/17 
 Pct Recovery = 94%  Analysis Date = 04/30/17 
 Pct Recovery = 94%  Analysis Date = 04/28/17 
 Pct Recovery = 94%  Analysis Date = 04/28/17 
 Pct Recovery = 94%  Analysis Date = 04/26/17 
 Pct Recovery = 95%  Analysis Date = 04/26/17 
 Pct Recovery = 95%  Analysis Date = 04/24/17 
 Pct Recovery = 95%  Analysis Date = 04/24/17 
 Pct Recovery = 95%  Analysis Date = 04/22/17 
 Pct Recovery = 95%  Analysis Date = 04/22/17 
 Pct Recovery = 95%  Analysis Date = 04/20/17 
 Pct Recovery = 96%  Analysis Date = 04/20/17 
 Pct Recovery = 96%  Analysis Date = 04/18/17 
 Pct Recovery = 96%  Analysis Date = 04/18/17 
 Pct Recovery = 96%  Analysis Date = 04/15/17 
 Pct Recovery = 96%  Analysis Date = 04/15/17 
 Pct Recovery = 96%  Analysis Date = 04/13/17 
 Pct Recovery = 96%  Analysis Date = 04/13/17 
 Pct Recovery = 96%  Analysis Date = 04/11/17 
 Pct Recovery = 97%  Analysis Date = 04/11/17 
 Pct Recovery = 97%  Analysis Date = 04/09/17 
 Pct Recovery = 97%  Analysis Date = 04/09/17 
 Pct Recovery = 97%  Analysis Date = 04/07/17 
 Pct Recovery = 97%  Analysis Date = 04/07/17 
 Pct Recovery = 97%  Analysis Date = 04/05/17 
 Pct Recovery = 98%  Analysis Date = 04/05/17 
 Pct Recovery = 98%  Analysis Date = 04/03/17 
 Pct Recovery = 98%  Analysis Date = 04/03/17 
 Pct Recovery = 98%  Analysis Date = 03/31/17 
 Pct Recovery = 98%  Analysis Date = 03/31/17 
 Pct Recovery = 98%  Analysis Date = 03/29/17 
 Pct Recovery = 98%  Analysis Date = 03/29/17 
 Pct Recovery = 98%  Analysis Date = 03/27/17 
 Pct Recovery = 99%  Analysis Date = 03/27/17 
 Pct Recovery = 99%  Analysis Date = 03/25/17 
 Pct Recovery = 99%  Analysis Date = 03/25/17 
 Pct Recovery = 99%  Analysis Date = 03/23/17 
 Pct Recovery = 99%  Analysis Date = 03/23/17 
 Pct Recovery = 99%  Analysis Date = 03/21/17 
 Pct Recovery = 99%  Analysis Date = 03/21/17 
 Pct Recovery = 99%  Analysis Date = 03/19/17 
 Pct Recovery = 100%  Analysis Date = 03/19/17 
 Pct Recovery = 100%  Analysis Date = 03/17/17 
 Pct Recovery = 100%  Analysis Date = 03/17/17 
 Pct Recovery = 100%  Analysis Date = 03/14/17 
 Pct Recovery = 100%  Analysis Date = 03/14/17 
 Pct Recovery = 100%  Analysis Date = 03/12/17 
 Pct Recovery = 101%  Analysis Date = 03/12/17 
 Pct Recovery = 101%  Analysis Date = 03/10/17 
 Pct Recovery = 101%  Analysis Date = 03/10/17 
 Pct Recovery = 101%  Analysis Date = 03/08/17 
 Pct Recovery = 101%  Analysis Date = 03/08/17 
 Pct Recovery = 101%  Analysis Date = 03/06/17 
 Pct Recovery = 101%  Analysis Date = 03/06/17 
 Pct Recovery = 101%  Analysis Date = 03/04/17 
 Pct Recovery = 102%  Analysis Date = 03/04/17 
 Pct Recovery = 102%  Analysis Date = 03/02/17 
 Pct Recovery = 102%  Analysis Date = 03/02/17 
 Pct Recovery = 102%  Analysis Date = 02/27/17 
 Pct Recovery = 102%  Analysis Date = 02/27/17 
 Pct Recovery = 102%  Analysis Date = 02/25/17 
 Pct Recovery = 102%  Analysis Date = 02/25/17 
 Pct Recovery = 102%  Analysis Date = 02/23/17 
 Pct Recovery = 102%  Analysis Date = 02/23/17 
 Pct Recovery = 102%  Analysis Date = 02/21/17 
 Pct Recovery = 103%  Analysis Date = 02/21/17 
 Pct Recovery = 103%  Analysis Date = 02/19/17 
 Pct Recovery = 103%  Analysis Date = 02/19/17 
 Pct Recovery = 103%  Analysis Date = 02/17/17 
 Pct Recovery = 103%  Analysis Date = 02/17/17 
 Pct Recovery = 103%  Analysis Date = 02/15/17 
 Pct Recovery = 103%  Analysis Date = 02/15/17 
 Pct Recovery = 103%  Analysis Date = 02/13/17 
 Pct Recovery = 103%  Analysis Date = 02/13/17 
 Pct Recovery = 103%  Analysis Date = 02/10/17 
 Pct Recovery = 103%  Analysis Date = 02/10/17 
 Pct Recovery = 103%  Analysis Date = 02/08/17 
 Pct Recovery = 103%  Analysis Date = 02/08/17 
 Pct Recovery = 103%  Analysis Date = 02/06/17 
 Pct Recovery = 103%  Analysis Date = 02/06/17 
 Pct Recovery = 103%  Analysis Date = 02/04/17 
 Pct Recovery = 103%  Analysis Date = 02/04/17 
 Pct Recovery = 103%  Analysis Date = 02/02/17 
 Pct Recovery = 103%  Analysis Date = 02/02/17 
 Pct Recovery = 103%  Analysis Date = 01/31/17 
 Pct Recovery = 103%  Analysis Date = 01/31/17 
 Pct Recovery = 103%  Analysis Date = 01/29/17 
 Pct Recovery = 103%  Analysis Date = 01/29/17 
 Pct Recovery = 103%  Analysis Date = 01/26/17 
 Pct Recovery = 103%  Analysis Date = 01/26/17 
 Pct Recovery = 103%  Analysis Date = 01/24/17 
 Pct Recovery = 104%  Analysis Date = 01/24/17 
 Pct Recovery = 104%  Analysis Date = 01/22/17 
 Pct Recovery = 104%  Analysis Date = 01/22/17 
 Pct Recovery = 104%  Analysis Date = 01/20/17 
 Pct Recovery = 104%  Analysis Date = 01/20/17 
 Pct Recovery = 104%  Analysis Date = 01/18/17 
 Pct Recovery = 104%  Analysis Date = 01/18/17 
 Pct Recovery = 104%  Analysis Date = 01/16/17 
 Pct Recovery = 104%  Analysis Date = 01/16/17 
 Pct Recovery = 104%  Analysis Date = 01/14/17 
 Pct Recovery = 104%  Analysis Date = 01/14/17 
 Pct Recovery = 104%  Analysis Date = 01/11/17 
 Pct Recovery = 104%  Analysis Date = 01/11/17 
 Pct Recovery = 104%  Analysis Date = 01/09/17 
 Pct Recovery = 104%  Analysis Date = 01/09/17 
 Pct Recovery = 104%  Analysis Date = 01/07/17 
 Pct Recovery = 104%  Analysis Date = 01/07/17 
 Pct Recovery = 104%  Analysis Date = 01/05/17 
 Pct Recovery = 104%  Analysis Date = 01/05/17 
 Pct Recovery = 104%  Analysis Date = 01/03/17 
 Pct Recovery = 104%  Analysis Date = 01/03/17 
 Pct Recovery = 104%  Analysis Date = 01/01/17 
 Pct Recovery = 104%  Analysis Date = 01/01/17 
 Pct Recovery = 104%  Analysis Date = 12/30/16 
 Pct Recovery = 104%  Analysis Date = 12/30/16 
 Pct Recovery = 104%  Analysis Date = 12/28/16 
 Pct Recovery = 104%  Analysis Date = 12/28/16 
 Pct Recovery = 104%  Analysis Date = 12/25/16 
 Pct Recovery = 104%  Analysis Date = 12/25/16 
 Pct Recovery = 104%  Analysis Date = 12/23/16 
 Pct Recovery = 104%  Analysis Date = 12/23/16 
 Pct Recovery = 104%  Analysis Date = 12/21/16 
 Pct Recovery = 104%  Analysis Date = 12/21/16 
 Pct Recovery = 104%  Analysis Date = 12/19/16 
 Pct Recovery = 104%  Analysis Date = 12/19/16 
 Pct Recovery = 104%  Analysis Date = 12/17/16 
 Pct Recovery = 103%  Analysis Date = 12/17/16 
 Pct Recovery = 103%  Analysis Date = 12/15/16 
 Pct Recovery = 103%  Analysis Date = 12/15/16 
 Pct Recovery = 103%  Analysis Date = 12/13/16 
 Pct Recovery = 103%  Analysis Date = 12/13/16 
 Pct Recovery = 103%  Analysis Date = 12/10/16 
 Pct Recovery = 102%  Analysis Date = 12/10/16 
 Pct Recovery = 102%  Analysis Date = 12/08/16 
 Pct Recovery = 102%  Analysis Date = 12/08/16 
 Pct Recovery = 102%  Analysis Date = 12/06/16 
 Pct Recovery = 101%  Analysis Date = 12/06/16 
 Pct Recovery = 101%  Analysis Date = 12/04/16 
 Pct Recovery = 101%  Analysis Date = 12/04/16 
 Pct Recovery = 101%  Analysis Date = 12/02/16 
 Pct Recovery = 101%  Analysis Date = 12/02/16 
 Pct Recovery = 101%  Analysis Date = 11/30/16 
 Pct Recovery = 100%  Analysis Date = 11/30/16 
 Pct Recovery = 100%  Analysis Date = 11/28/16 
 Pct Recovery = 100%  Analysis Date = 11/28/16 
 Pct Recovery = 100%  Analysis Date = 11/26/16 
 Pct Recovery = 100%  Analysis Date = 11/26/16 
 Pct Recovery = 100%  Analysis Date = 11/23/16 
 Pct Recovery = 99%  Analysis Date = 11/23/16 
 Pct Recovery = 99%  Analysis Date = 11/21/16 
 Pct Recovery = 99%  Analysis Date = 11/21/16 
 Pct Recovery = 99%  Analysis Date = 11/19/16 
 Pct Recovery = 98%  Analysis Date = 11/19/16 
 Pct Recovery = 98%  Analysis Date = 11/17/16 
 Pct Recovery = 98%  Analysis Date = 11/17/16 
 Pct Recovery = 98%  Analysis Date = 11/15/16 
 Pct Recovery = 98%  Analysis Date = 11/15/16 
 Pct Recovery = 98%  Analysis Date = 11/13/16 
 Pct Recovery = 97%  Analysis Date = 11/13/16 
 Pct Recovery = 97%  Analysis Date = 11/11/16 
 Pct Recovery = 97%  Analysis Date = 11/11/16 
 Pct Recovery = 97%  Analysis Date = 11/08/16 
 Pct Recovery = 96%  Analysis Date = 11/08/16 
 Pct Recovery = 96%  Analysis Date = 11/06/16 
 Pct Recovery = 96%  Analysis Date = 11/06/16 
 Pct Recovery = 96%  Analysis Date = 11/04/16 
 Pct Recovery = 96%  Analysis Date = 11/04/16 
 Pct Recovery = 96%  Analysis Date = 11/02/16 
 Pct Recovery = 95%  Analysis Date = 11/02/16 
 Pct Recovery = 95%  Analysis Date = 10/31/16 
 Pct Recovery = 95%  Analysis Date = 10/31/16 
 Pct Recovery = 95%  Analysis Date = 10/29/16 
 Pct Recovery = 95%  Analysis Date = 10/29/16 
 Pct Recovery = 95%  Analysis Date = 10/27/16 
 Pct Recovery = 94%  Analysis Date = 10/27/16 
 Pct Recovery = 94%  Analysis Date = 10/24/16 
 Pct Recovery = 94%  Analysis Date = 10/24/16 
 Pct Recovery = 94%  Analysis Date = 10/22/16 
 Pct Recovery = 93%  Analysis Date = 10/22/16 
 Pct Recovery = 93%  Analysis Date = 10/20/16 
 Pct Recovery = 93%  Analysis Date = 10/20/16 
 Pct Recovery = 93%  Analysis Date = 10/18/16 
 Pct Recovery = 93%  Analysis Date = 10/18/16 
 Pct Recovery = 93%  Analysis Date = 10/16/16 
 Pct Recovery = 92%  Analysis Date = 10/16/16 
 Pct Recovery = 92%  Analysis Date = 10/14/16 
 Pct Recovery = 92%  Analysis Date = 10/14/16 
 Pct Recovery = 92%  Analysis Date = 10/12/16 
 Pct Recovery = 91%  Analysis Date = 10/12/16 
 Pct Recovery = 91%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/10/16 
 Pct Recovery = 91%  Analysis Date = 10/07/16 
 Pct Recovery = 91%  Analysis Date = 10/07/16 
 Pct Recovery = 91%  Analysis Date = 10/05/16 
 Pct Recovery = 90%  Analysis Date = 10/05/16 
 Pct Recovery = 90%  Analysis Date = 10/03/16 
 Pct Recovery = 90%  Analysis Date = 10/03/16 
 Pct Recovery = 90%  Analysis Date = 10/01/16 
 Pct Recovery = 90%  Analysis Date = 10/01/16 
 Pct Recovery = 90%  Analysis Date = 09/29/16 
 Pct Recovery = 89%  Analysis Date = 09/29/16 
 Pct Recovery = 89%  Analysis Date = 09/27/16 
 Pct Recovery = 89%  Analysis Date = 09/27/16 
 Pct Recovery = 89%  Analysis Date = 09/25/16 
 Pct Recovery = 88%  Analysis Date = 09/25/16 
 Pct Recovery = 88%  Analysis Date = 09/22/16 
 Pct Recovery = 88%  Analysis Date = 09/22/16 
 Pct Recovery = 88%  Analysis Date = 09/20/16 
 Pct Recovery = 88%  Analysis Date = 09/20/16 
 Pct Recovery = 88%  Analysis Date = 09/18/16 
 Pct Recovery = 87%  Analysis Date = 09/18/16 
 Pct Recovery = 87%  Analysis Date = 09/16/16 
 Pct Recovery = 87%  Analysis Date = 09/16/16 
 Pct Recovery = 87%  Analysis Date = 09/14/16 
 Pct Recovery = 87%  Analysis Date = 09/14/16 
 Pct Recovery = 87%  Analysis Date = 09/12/16 
 Pct Recovery = 86%  Analysis Date = 09/12/16 
 Pct Recovery = 86%  Analysis Date = 09/10/16 
 Pct Recovery = 86%  Analysis Date = 09/10/16 
 Pct Recovery = 86%  Analysis Date = 09/08/16 
 Pct Recovery = 85%  Analysis Date = 09/08/16 
 Pct Recovery = 85%  Analysis Date = 09/05/16 
 Pct Recovery = 85%  Analysis Date = 09/05/16 
 Pct Recovery = 85%  Analysis Date = 09/03/16 
 Pct Recovery = 85%  Analysis Date = 09/03/16 
 Pct Recovery = 85%  Analysis Date = 09/01/16 
 Pct Recovery = 84%  Analysis Date = 09/01/16 
 Pct Recovery = 84%  Analysis Date = 08/30/16 
 Pct Recovery = 84%  Analysis Date = 08/30/16 
 Pct Recovery = 84%  Analysis Date = 08/28/16 
 Pct Recovery = 84%  Analysis Date = 08/28/16 
 Pct Recovery = 84%  Analysis Date = 08/26/16 
 Pct Recovery = 84%  Analysis Date = 08/26/16 
 Pct Recovery = 84%  Analysis Date = 08/24/16 
 Pct Recovery = 84%  Analysis Date = 08/24/16 
 Pct Recovery = 84%  Analysis Date = 08/21/16 
 Pct Recovery = 84%  Analysis Date = 08/21/16 
 Pct Recovery = 84%  Analysis Date = 08/19/16 
 Pct Recovery = 83%  Analysis Date = 08/19/16 
 Pct Recovery = 83%  Analysis Date = 08/17/16 
 Pct Recovery = 83%  Analysis Date = 08/17/16 
 Pct Recovery = 83%  Analysis Date = 08/15/16 
 Pct Recovery = 83%  Analysis Date = 08/15/16 
 Pct Recovery = 83%  Analysis Date = 08/13/16 
 Pct Recovery = 83%  Analysis Date = 08/13/16 
 Pct Recovery = 83%  Analysis Date = 08/11/16 
 Pct Recovery = 83%  Analysis Date = 08/11/16 
 Pct Recovery = 83%  Analysis Date = 08/09/16 
 Pct Recovery = 83%  Analysis Date = 08/09/16 
 Pct Recovery = 83%  Analysis Date = 08/06/16 
 Pct Recovery = 83%  Analysis Date = 08/06/16 
 Pct Recovery = 83%  Analysis Date = 08/04/16 
 Pct Recovery = 83%  Analysis Date = 08/04/16 
 Pct Recovery = 83%  Analysis Date = 08/02/16 
 Pct Recovery = 82%  Analysis Date = 08/02/16 
 Pct Recovery = 82%  Analysis Date = 07/31/16 
 Pct Recovery = 82%  Analysis Date = 07/31/16 
 Pct Recovery = 82%  Analysis Date = 07/29/16 
 Pct Recovery = 82%  Analysis Date = 07/29/16 
 Pct Recovery = 82%  Analysis Date = 07/27/16 
 Pct Recovery = 82%  Analysis Date = 07/27/16 
 Pct Recovery = 82%  Analysis Date = 07/25/16 
 Pct Recovery = 82%  Analysis Date = 07/25/16 
 Pct Recovery = 82%  Analysis Date = 07/23/16 
 Pct Recovery = 82%  Analysis Date = 07/23/16 
 Pct Recovery = 82%  Analysis Date = 07/20/16 
 Pct Recovery = 82%  Analysis Date = 07/20/16 
 Pct Recovery = 82%  Analysis Date = 07/18/16 
 Pct Recovery = 82%  Analysis Date = 07/18/16 
 Pct Recovery = 82%  Analysis Date = 07/16/16 
 Pct Recovery = 82%  Analysis Date = 07/16/16 
 Pct Recovery = 82%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/12/16 
 Pct Recovery = 81%  Analysis Date = 07/12/16 
 Pct Recovery = 81%  Analysis Date = 07/10/16 
 Pct Recovery = 81%  Analysis Date = 07/10/16 
 Pct Recovery = 81%  Analysis Date = 07/08/16 
 Pct Recovery = 81%  Analysis Date = 07/08/16 
 Pct Recovery = 81%  Analysis Date = 07/05/16 
 Pct Recovery = 81%  Analysis Date = 07/05/16 
 Pct Recovery = 81%  Analysis Date = 07/03/16 
 Pct Recovery = 81%  Analysis Date = 07/03/16 
 Pct Recovery = 81%  Analysis Date = 07/01/16 
 Pct Recovery = 81%  Analysis Date = 07/01/16 
 Pct Recovery = 81%  Analysis Date = 06/29/16 
 Pct Recovery = 81%  Analysis Date = 06/29/16 
 Pct Recovery = 81%  Analysis Date = 06/27/16 
 Pct Recovery = 80%  Analysis Date = 06/27/16 
 Pct Recovery = 80%  Analysis Date = 06/25/16 
 Pct Recovery = 80%  Analysis Date = 06/25/16 
 Pct Recovery = 80%  Analysis Date = 06/23/16 
 Pct Recovery = 80%  Analysis Date = 06/23/16 
 Pct Recovery = 80%  Analysis Date = 06/21/16 
 Pct Recovery = 80%  Analysis Date = 06/21/16 
 Pct Recovery = 80%  Analysis Date = 06/18/16 
 Pct Recovery = 80%  Analysis Date = 06/18/16 
 Pct Recovery = 80%  Analysis Date = 06/16/16 
 Pct Recovery = 80%  Analysis Date = 06/16/16 
 Pct Recovery = 80%  Analysis Date = 06/14/16 
 Pct Recovery = 80%  Analysis Date = 06/14/16 
 Pct Recovery = 80%  Analysis Date = 06/12/16 
 Pct Recovery = 80%  Analysis Date = 06/12/16 
 Pct Recovery = 80%  Analysis Date = 06/10/16 
 Pct Recovery = 80%  Analysis Date = 06/10/16 
 Pct Recovery = 80%  Analysis Date = 06/08/16 
 Pct Recovery = 79%  Analysis Date = 06/08/16 
 Pct Recovery = 79%  Analysis Date = 06/06/16 
 Pct Recovery = 79%  Analysis Date = 06/06/16 
 Pct Recovery = 79%  Analysis Date = 06/03/16 
 Pct Recovery = 79%  Analysis Date = 06/03/16 
 Pct Recovery = 79%  Analysis Date = 06/01/16 
 Pct Recovery = 79%  Analysis Date = 06/01/16 
 Pct Recovery = 79%  Analysis Date = 05/30/16 
 Pct Recovery = 79%  Analysis Date = 05/30/16 
 Pct Recovery = 79%  Analysis Date = 05/28/16 
 Pct Recovery = 79%  Analysis Date = 05/28/16 
 Pct Recovery = 79%  Analysis Date = 05/26/16 
 Pct Recovery = 79%  Analysis Date = 05/26/16 
 Pct Recovery = 79%  Analysis Date = 05/24/16 
 Pct Recovery = 79%  Analysis Date = 05/24/16 
 Pct Recovery = 79%  Analysis Date = 05/22/16 
 Pct Recovery = 80%  Analysis Date = 05/22/16 
 Pct Recovery = 80%  Analysis Date = 05/19/16 
 Pct Recovery = 80%  Analysis Date = 05/19/16 
 Pct Recovery = 80%  Analysis Date = 05/17/16 
 Pct Recovery = 80%  Analysis Date = 05/17/16 
 Pct Recovery = 80%  Analysis Date = 05/15/16 
 Pct Recovery = 80%  Analysis Date = 05/15/16 
 Pct Recovery = 80%  Analysis Date = 05/13/16 
 Pct Recovery = 80%  Analysis Date = 05/13/16 
 Pct Recovery = 80%  Analysis Date = 05/11/16 
 Pct Recovery = 80%  Analysis Date = 05/11/16 
 Pct Recovery = 80%  Analysis Date = 05/09/16 
 Pct Recovery = 81%  Analysis Date = 05/09/16 
 Pct Recovery = 81%  Analysis Date = 05/07/16 
 Pct Recovery = 81%  Analysis Date = 05/07/16 
 Pct Recovery = 81%  Analysis Date = 05/05/16 
 Pct Recovery = 81%  Analysis Date = 05/05/16 
 Pct Recovery = 81%  Analysis Date = 05/02/16 
 Pct Recovery = 81%  Analysis Date = 05/02/16 
 Pct Recovery = 81%  Analysis Date = 04/30/16 
 Pct Recovery = 81%  Analysis Date = 04/30/16 
 Pct Recovery = 81%  Analysis Date = 04/28/16 
 Pct Recovery = 81%  Analysis Date = 04/28/16 
 Pct Recovery = 81%  Analysis Date = 04/26/16 
 Pct Recovery = 82%  Analysis Date = 04/26/16 
 Pct Recovery = 82%  Analysis Date = 04/24/16 
 Pct Recovery = 82%  Analysis Date = 04/24/16 
 Pct Recovery = 82%  Analysis Date = 04/22/16 
 Pct Recovery = 82%  Analysis Date = 04/22/16 
 Pct Recovery = 82%  Analysis Date = 04/20/16 
 Pct Recovery = 82%  Analysis Date = 04/20/16 
 Pct Recovery = 82%  Analysis Date = 04/17/16 
 Pct Recovery = 82%  Analysis Date = 04/17/16 
 Pct Recovery = 82%  Analysis Date = 04/15/16 
 Pct Recovery = 82%  Analysis Date = 04/15/16 
 Pct Recovery = 82%  Analysis Date = 04/13/16 
 Pct Recovery = 83%  Analysis Date = 04/13/16 
 Pct Recovery = 83%  Analysis Date = 04/11/16 
 Pct Recovery = 83%  Analysis Date = 04/11/16 
 Pct Recovery = 83%  Analysis Date = 04/09/16 
 Pct Recovery = 83%  Analysis Date = 04/09/16 
 Pct Recovery = 83%  Analysis Date = 04/07/16 
 Pct Recovery = 83%  Analysis Date = 04/07/16 
 Pct Recovery = 83%  Analysis Date = 04/05/16 
 Pct Recovery = 83%  Analysis Date = 04/05/16 
 Pct Recovery = 83%  Analysis Date = 04/03/16 
 Pct Recovery = 83%  Analysis Date = 04/03/16 
 Pct Recovery = 83%  Analysis Date = 03/31/16 
 Pct Recovery = 84%  Analysis Date = 03/31/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/29/16 
 Pct Recovery = 84%  Analysis Date = 03/27/16 
 Pct Recovery = 84%  Analysis Date = 03/27/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/25/16 
 Pct Recovery = 84%  Analysis Date = 03/23/16 
 Pct Recovery = 84%  Analysis Date = 03/23/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/21/16 
 Pct Recovery = 84%  Analysis Date = 03/19/16 
 Pct Recovery = 84%  Analysis Date = 03/19/16 
 Pct Recovery = 84%  Analysis Date = 03/16/16 
 Pct Recovery = 84%  Analysis Date = 03/16/16 
 Pct Recovery = 84%  Analysis Date = 03/14/16 
 Pct Recovery = 85%  Analysis Date = 03/14/16 
 Pct Recovery = 85%  Analysis Date = 03/12/16 
 Pct Recovery = 85%  Analysis Date = 03/12/16 
 Pct Recovery = 85%  Analysis Date = 03/10/16 
 Pct Recovery = 85%  Analysis Date = 03/10/16 
 Pct Recovery = 85%  Analysis Date = 03/08/16 
 Pct Recovery = 85%  Analysis Date = 03/08/16 
 Pct Recovery = 85%  Analysis Date = 03/06/16 
 Pct Recovery = 85%  Analysis Date = 03/06/16 
 Pct Recovery = 85%  Analysis Date = 03/04/16 
 Pct Recovery = 85%  Analysis Date = 03/04/16 
 Pct Recovery = 85%  Analysis Date = 03/02/16 
 Pct Recovery = 85%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 91% 15% 88% 20%
Total 18 91% 15% 88% 20%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
AZINPHOS-METHYL
METHOD: 2033 , TESTIDCODE: 82686GCM35

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 64%  Analysis Date = 02/22/17 
 SpikeMix = Phenova B20160331: 100 Ál & Supelco LC20138V: 100 Ál 
 Pct Recovery = 66%  Analysis Date = 09/09/16 
 SpikeMix = Crescent 03FF076: 100 Ál & ChemService 5054800: 100 Ál 
 Pct Recovery = 92%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 68%  Analysis Date = 03/21/17 
 SpikeMix = Supelco LC20138V: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 74%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 61%  Analysis Date = 08/19/16 
 SpikeMix = Supelco LC20138V: 80 Ál & Pheonva B20160331: 80 Ál 
 Pct Recovery = 86%  Analysis Date = 04/07/16 
 SpikeMix = Spex Organics EN150514012: 40 Ál & ERA 0406-15-01: 40 Ál 
 Pct Recovery = 51%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 66%  Analysis Date = 03/16/17 
 SpikeMix = Supelco LC20138V: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 89%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 66%  Analysis Date = 01/18/17 
 SpikeMix = Crescent 03FF076: 40 Ál & Supelco LC20138V: 40 Ál 
 Pct Recovery = 65%  Analysis Date = 09/20/16 
 SpikeMix = Phenova B20160331: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 81%  Analysis Date = 09/14/16 
 SpikeMix = Supelco LC20138V: 40 Ál & NSI 041816: 40 Ál 
 Pct Recovery = 56%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 77%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 61%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 45%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 Ál & Spex Organics EN150514012: 20 Ál 
 Pct Recovery = 63%  Analysis Date = 05/10/17 
 Pct Recovery = 71%  Analysis Date = 05/08/17 
 Pct Recovery = 71%  Analysis Date = 05/08/17 
 Pct Recovery = 71%  Analysis Date = 05/06/17 
 Pct Recovery = 71%  Analysis Date = 05/06/17 
 Pct Recovery = 71%  Analysis Date = 05/04/17 
 Pct Recovery = 71%  Analysis Date = 05/04/17 
 Pct Recovery = 71%  Analysis Date = 05/01/17 
 Pct Recovery = 71%  Analysis Date = 05/01/17 
 Pct Recovery = 71%  Analysis Date = 04/29/17 
 Pct Recovery = 71%  Analysis Date = 04/29/17 
 Pct Recovery = 71%  Analysis Date = 04/27/17 
 Pct Recovery = 71%  Analysis Date = 04/27/17 
 Pct Recovery = 71%  Analysis Date = 04/25/17 
 Pct Recovery = 71%  Analysis Date = 04/25/17 
 Pct Recovery = 71%  Analysis Date = 04/22/17 
 Pct Recovery = 71%  Analysis Date = 04/22/17 
 Pct Recovery = 71%  Analysis Date = 04/20/17 
 Pct Recovery = 71%  Analysis Date = 04/20/17 
 Pct Recovery = 71%  Analysis Date = 04/18/17 
 Pct Recovery = 71%  Analysis Date = 04/18/17 
 Pct Recovery = 71%  Analysis Date = 04/15/17 
 Pct Recovery = 71%  Analysis Date = 04/15/17 
 Pct Recovery = 71%  Analysis Date = 04/13/17 
 Pct Recovery = 71%  Analysis Date = 04/13/17 
 Pct Recovery = 71%  Analysis Date = 04/11/17 
 Pct Recovery = 71%  Analysis Date = 04/11/17 
 Pct Recovery = 71%  Analysis Date = 04/09/17 
 Pct Recovery = 71%  Analysis Date = 04/09/17 
 Pct Recovery = 71%  Analysis Date = 04/06/17 
 Pct Recovery = 70%  Analysis Date = 04/06/17 
 Pct Recovery = 70%  Analysis Date = 04/04/17 
 Pct Recovery = 70%  Analysis Date = 04/04/17 
 Pct Recovery = 70%  Analysis Date = 04/02/17 
 Pct Recovery = 70%  Analysis Date = 04/02/17 
 Pct Recovery = 70%  Analysis Date = 03/30/17 
 Pct Recovery = 70%  Analysis Date = 03/30/17 
 Pct Recovery = 70%  Analysis Date = 03/28/17 
 Pct Recovery = 70%  Analysis Date = 03/28/17 
 Pct Recovery = 70%  Analysis Date = 03/26/17 
 Pct Recovery = 70%  Analysis Date = 03/26/17 
 Pct Recovery = 70%  Analysis Date = 03/24/17 
 Pct Recovery = 70%  Analysis Date = 03/24/17 
 Pct Recovery = 70%  Analysis Date = 03/21/17 
 Pct Recovery = 70%  Analysis Date = 03/21/17 
 Pct Recovery = 70%  Analysis Date = 03/19/17 
 Pct Recovery = 70%  Analysis Date = 03/19/17 
 Pct Recovery = 70%  Analysis Date = 03/17/17 
 Pct Recovery = 70%  Analysis Date = 03/17/17 
 Pct Recovery = 70%  Analysis Date = 03/14/17 
 Pct Recovery = 70%  Analysis Date = 03/14/17 
 Pct Recovery = 70%  Analysis Date = 03/12/17 
 Pct Recovery = 70%  Analysis Date = 03/12/17 
 Pct Recovery = 70%  Analysis Date = 03/10/17 
 Pct Recovery = 70%  Analysis Date = 03/10/17 
 Pct Recovery = 70%  Analysis Date = 03/08/17 
 Pct Recovery = 70%  Analysis Date = 03/08/17 
 Pct Recovery = 70%  Analysis Date = 03/05/17 
 Pct Recovery = 70%  Analysis Date = 03/05/17 
 Pct Recovery = 70%  Analysis Date = 03/03/17 
 Pct Recovery = 70%  Analysis Date = 03/03/17 
 Pct Recovery = 70%  Analysis Date = 03/01/17 
 Pct Recovery = 69%  Analysis Date = 03/01/17 
 Pct Recovery = 69%  Analysis Date = 02/26/17 
 Pct Recovery = 69%  Analysis Date = 02/26/17 
 Pct Recovery = 69%  Analysis Date = 02/24/17 
 Pct Recovery = 69%  Analysis Date = 02/24/17 
 Pct Recovery = 69%  Analysis Date = 02/22/17 
 Pct Recovery = 69%  Analysis Date = 02/22/17 
 Pct Recovery = 69%  Analysis Date = 02/20/17 
 Pct Recovery = 69%  Analysis Date = 02/20/17 
 Pct Recovery = 69%  Analysis Date = 02/17/17 
 Pct Recovery = 68%  Analysis Date = 02/17/17 
 Pct Recovery = 68%  Analysis Date = 02/15/17 
 Pct Recovery = 68%  Analysis Date = 02/15/17 
 Pct Recovery = 68%  Analysis Date = 02/13/17 
 Pct Recovery = 68%  Analysis Date = 02/13/17 
 Pct Recovery = 68%  Analysis Date = 02/10/17 
 Pct Recovery = 67%  Analysis Date = 02/10/17 
 Pct Recovery = 67%  Analysis Date = 02/08/17 
 Pct Recovery = 67%  Analysis Date = 02/08/17 
 Pct Recovery = 67%  Analysis Date = 02/06/17 
 Pct Recovery = 67%  Analysis Date = 02/06/17 
 Pct Recovery = 67%  Analysis Date = 02/04/17 
 Pct Recovery = 66%  Analysis Date = 02/04/17 
 Pct Recovery = 66%  Analysis Date = 02/01/17 
 Pct Recovery = 66%  Analysis Date = 02/01/17 
 Pct Recovery = 66%  Analysis Date = 01/30/17 
 Pct Recovery = 65%  Analysis Date = 01/30/17 
 Pct Recovery = 65%  Analysis Date = 01/28/17 
 Pct Recovery = 65%  Analysis Date = 01/28/17 
 Pct Recovery = 65%  Analysis Date = 01/25/17 
 Pct Recovery = 65%  Analysis Date = 01/25/17 
 Pct Recovery = 65%  Analysis Date = 01/23/17 
 Pct Recovery = 64%  Analysis Date = 01/23/17 
 Pct Recovery = 64%  Analysis Date = 01/21/17 
 Pct Recovery = 64%  Analysis Date = 01/21/17 
 Pct Recovery = 64%  Analysis Date = 01/19/17 
 Pct Recovery = 63%  Analysis Date = 01/19/17 
 Pct Recovery = 63%  Analysis Date = 01/16/17 
 Pct Recovery = 63%  Analysis Date = 01/16/17 
 Pct Recovery = 63%  Analysis Date = 01/14/17 
 Pct Recovery = 64%  Analysis Date = 01/14/17 
 Pct Recovery = 64%  Analysis Date = 01/12/17 
 Pct Recovery = 64%  Analysis Date = 01/12/17 
 Pct Recovery = 64%  Analysis Date = 01/09/17 
 Pct Recovery = 64%  Analysis Date = 01/09/17 
 Pct Recovery = 64%  Analysis Date = 01/07/17 
 Pct Recovery = 64%  Analysis Date = 01/07/17 
 Pct Recovery = 64%  Analysis Date = 01/05/17 
 Pct Recovery = 64%  Analysis Date = 01/05/17 
 Pct Recovery = 64%  Analysis Date = 01/03/17 
 Pct Recovery = 65%  Analysis Date = 01/03/17 
 Pct Recovery = 65%  Analysis Date = 12/31/16 
 Pct Recovery = 65%  Analysis Date = 12/31/16 
 Pct Recovery = 65%  Analysis Date = 12/29/16 
 Pct Recovery = 65%  Analysis Date = 12/29/16 
 Pct Recovery = 65%  Analysis Date = 12/27/16 
 Pct Recovery = 65%  Analysis Date = 12/27/16 
 Pct Recovery = 65%  Analysis Date = 12/24/16 
 Pct Recovery = 65%  Analysis Date = 12/24/16 
 Pct Recovery = 65%  Analysis Date = 12/22/16 
 Pct Recovery = 66%  Analysis Date = 12/22/16 
 Pct Recovery = 66%  Analysis Date = 12/20/16 
 Pct Recovery = 66%  Analysis Date = 12/20/16 
 Pct Recovery = 66%  Analysis Date = 12/18/16 
 Pct Recovery = 66%  Analysis Date = 12/18/16 
 Pct Recovery = 66%  Analysis Date = 12/15/16 
 Pct Recovery = 66%  Analysis Date = 12/15/16 
 Pct Recovery = 66%  Analysis Date = 12/13/16 
 Pct Recovery = 66%  Analysis Date = 12/13/16 
 Pct Recovery = 66%  Analysis Date = 12/11/16 
 Pct Recovery = 67%  Analysis Date = 12/11/16 
 Pct Recovery = 67%  Analysis Date = 12/08/16 
 Pct Recovery = 67%  Analysis Date = 12/08/16 
 Pct Recovery = 67%  Analysis Date = 12/06/16 
 Pct Recovery = 67%  Analysis Date = 12/06/16 
 Pct Recovery = 67%  Analysis Date = 12/04/16 
 Pct Recovery = 67%  Analysis Date = 12/04/16 
 Pct Recovery = 67%  Analysis Date = 12/02/16 
 Pct Recovery = 68%  Analysis Date = 12/02/16 
 Pct Recovery = 68%  Analysis Date = 11/29/16 
 Pct Recovery = 68%  Analysis Date = 11/29/16 
 Pct Recovery = 68%  Analysis Date = 11/27/16 
 Pct Recovery = 68%  Analysis Date = 11/27/16 
 Pct Recovery = 68%  Analysis Date = 11/25/16 
 Pct Recovery = 68%  Analysis Date = 11/25/16 
 Pct Recovery = 68%  Analysis Date = 11/22/16 
 Pct Recovery = 68%  Analysis Date = 11/22/16 
 Pct Recovery = 68%  Analysis Date = 11/20/16 
 Pct Recovery = 69%  Analysis Date = 11/20/16 
 Pct Recovery = 69%  Analysis Date = 11/18/16 
 Pct Recovery = 69%  Analysis Date = 11/18/16 
 Pct Recovery = 69%  Analysis Date = 11/16/16 
 Pct Recovery = 69%  Analysis Date = 11/16/16 
 Pct Recovery = 69%  Analysis Date = 11/13/16 
 Pct Recovery = 69%  Analysis Date = 11/13/16 
 Pct Recovery = 69%  Analysis Date = 11/11/16 
 Pct Recovery = 69%  Analysis Date = 11/11/16 
 Pct Recovery = 69%  Analysis Date = 11/09/16 
 Pct Recovery = 70%  Analysis Date = 11/09/16 
 Pct Recovery = 70%  Analysis Date = 11/06/16 
 Pct Recovery = 70%  Analysis Date = 11/06/16 
 Pct Recovery = 70%  Analysis Date = 11/04/16 
 Pct Recovery = 70%  Analysis Date = 11/04/16 
 Pct Recovery = 70%  Analysis Date = 11/02/16 
 Pct Recovery = 70%  Analysis Date = 11/02/16 
 Pct Recovery = 70%  Analysis Date = 10/31/16 
 Pct Recovery = 70%  Analysis Date = 10/31/16 
 Pct Recovery = 70%  Analysis Date = 10/28/16 
 Pct Recovery = 71%  Analysis Date = 10/28/16 
 Pct Recovery = 71%  Analysis Date = 10/26/16 
 Pct Recovery = 71%  Analysis Date = 10/26/16 
 Pct Recovery = 71%  Analysis Date = 10/24/16 
 Pct Recovery = 71%  Analysis Date = 10/24/16 
 Pct Recovery = 71%  Analysis Date = 10/21/16 
 Pct Recovery = 71%  Analysis Date = 10/21/16 
 Pct Recovery = 71%  Analysis Date = 10/19/16 
 Pct Recovery = 71%  Analysis Date = 10/19/16 
 Pct Recovery = 71%  Analysis Date = 10/17/16 
 Pct Recovery = 72%  Analysis Date = 10/17/16 
 Pct Recovery = 72%  Analysis Date = 10/15/16 
 Pct Recovery = 72%  Analysis Date = 10/15/16 
 Pct Recovery = 72%  Analysis Date = 10/12/16 
 Pct Recovery = 72%  Analysis Date = 10/12/16 
 Pct Recovery = 72%  Analysis Date = 10/10/16 
 Pct Recovery = 72%  Analysis Date = 10/10/16 
 Pct Recovery = 72%  Analysis Date = 10/08/16 
 Pct Recovery = 72%  Analysis Date = 10/08/16 
 Pct Recovery = 72%  Analysis Date = 10/05/16 
 Pct Recovery = 73%  Analysis Date = 10/05/16 
 Pct Recovery = 73%  Analysis Date = 10/03/16 
 Pct Recovery = 73%  Analysis Date = 10/03/16 
 Pct Recovery = 73%  Analysis Date = 10/01/16 
 Pct Recovery = 73%  Analysis Date = 10/01/16 
 Pct Recovery = 73%  Analysis Date = 09/29/16 
 Pct Recovery = 73%  Analysis Date = 09/29/16 
 Pct Recovery = 73%  Analysis Date = 09/26/16 
 Pct Recovery = 73%  Analysis Date = 09/26/16 
 Pct Recovery = 73%  Analysis Date = 09/24/16 
 Pct Recovery = 74%  Analysis Date = 09/24/16 
 Pct Recovery = 74%  Analysis Date = 09/22/16 
 Pct Recovery = 74%  Analysis Date = 09/22/16 
 Pct Recovery = 74%  Analysis Date = 09/19/16 
 Pct Recovery = 74%  Analysis Date = 09/19/16 
 Pct Recovery = 74%  Analysis Date = 09/17/16 
 Pct Recovery = 74%  Analysis Date = 09/17/16 
 Pct Recovery = 74%  Analysis Date = 09/15/16 
 Pct Recovery = 74%  Analysis Date = 09/15/16 
 Pct Recovery = 74%  Analysis Date = 09/13/16 
 Pct Recovery = 75%  Analysis Date = 09/13/16 
 Pct Recovery = 75%  Analysis Date = 09/10/16 
 Pct Recovery = 75%  Analysis Date = 09/10/16 
 Pct Recovery = 75%  Analysis Date = 09/08/16 
 Pct Recovery = 75%  Analysis Date = 09/08/16 
 Pct Recovery = 75%  Analysis Date = 09/06/16 
 Pct Recovery = 75%  Analysis Date = 09/06/16 
 Pct Recovery = 75%  Analysis Date = 09/03/16 
 Pct Recovery = 75%  Analysis Date = 09/03/16 
 Pct Recovery = 75%  Analysis Date = 09/01/16 
 Pct Recovery = 75%  Analysis Date = 09/01/16 
 Pct Recovery = 75%  Analysis Date = 08/30/16 
 Pct Recovery = 75%  Analysis Date = 08/30/16 
 Pct Recovery = 75%  Analysis Date = 08/28/16 
 Pct Recovery = 75%  Analysis Date = 08/28/16 
 Pct Recovery = 75%  Analysis Date = 08/25/16 
 Pct Recovery = 74%  Analysis Date = 08/25/16 
 Pct Recovery = 74%  Analysis Date = 08/23/16 
 Pct Recovery = 74%  Analysis Date = 08/23/16 
 Pct Recovery = 74%  Analysis Date = 08/21/16 
 Pct Recovery = 74%  Analysis Date = 08/21/16 
 Pct Recovery = 74%  Analysis Date = 08/18/16 
 Pct Recovery = 74%  Analysis Date = 08/18/16 
 Pct Recovery = 74%  Analysis Date = 08/16/16 
 Pct Recovery = 74%  Analysis Date = 08/16/16 
 Pct Recovery = 74%  Analysis Date = 08/14/16 
 Pct Recovery = 74%  Analysis Date = 08/14/16 
 Pct Recovery = 74%  Analysis Date = 08/12/16 
 Pct Recovery = 73%  Analysis Date = 08/12/16 
 Pct Recovery = 73%  Analysis Date = 08/09/16 
 Pct Recovery = 73%  Analysis Date = 08/09/16 
 Pct Recovery = 73%  Analysis Date = 08/07/16 
 Pct Recovery = 73%  Analysis Date = 08/07/16 
 Pct Recovery = 73%  Analysis Date = 08/05/16 
 Pct Recovery = 73%  Analysis Date = 08/05/16 
 Pct Recovery = 73%  Analysis Date = 08/02/16 
 Pct Recovery = 73%  Analysis Date = 08/02/16 
 Pct Recovery = 73%  Analysis Date = 07/31/16 
 Pct Recovery = 72%  Analysis Date = 07/31/16 
 Pct Recovery = 72%  Analysis Date = 07/29/16 
 Pct Recovery = 72%  Analysis Date = 07/29/16 
 Pct Recovery = 72%  Analysis Date = 07/27/16 
 Pct Recovery = 72%  Analysis Date = 07/27/16 
 Pct Recovery = 72%  Analysis Date = 07/24/16 
 Pct Recovery = 72%  Analysis Date = 07/24/16 
 Pct Recovery = 72%  Analysis Date = 07/22/16 
 Pct Recovery = 72%  Analysis Date = 07/22/16 
 Pct Recovery = 72%  Analysis Date = 07/20/16 
 Pct Recovery = 72%  Analysis Date = 07/20/16 
 Pct Recovery = 72%  Analysis Date = 07/17/16 
 Pct Recovery = 71%  Analysis Date = 07/17/16 
 Pct Recovery = 71%  Analysis Date = 07/15/16 
 Pct Recovery = 71%  Analysis Date = 07/15/16 
 Pct Recovery = 71%  Analysis Date = 07/13/16 
 Pct Recovery = 71%  Analysis Date = 07/13/16 
 Pct Recovery = 71%  Analysis Date = 07/11/16 
 Pct Recovery = 71%  Analysis Date = 07/11/16 
 Pct Recovery = 71%  Analysis Date = 07/08/16 
 Pct Recovery = 71%  Analysis Date = 07/08/16 
 Pct Recovery = 71%  Analysis Date = 07/06/16 
 Pct Recovery = 70%  Analysis Date = 07/06/16 
 Pct Recovery = 70%  Analysis Date = 07/04/16 
 Pct Recovery = 70%  Analysis Date = 07/04/16 
 Pct Recovery = 70%  Analysis Date = 07/01/16 
 Pct Recovery = 70%  Analysis Date = 07/01/16 
 Pct Recovery = 70%  Analysis Date = 06/29/16 
 Pct Recovery = 70%  Analysis Date = 06/29/16 
 Pct Recovery = 70%  Analysis Date = 06/27/16 
 Pct Recovery = 70%  Analysis Date = 06/27/16 
 Pct Recovery = 70%  Analysis Date = 06/25/16 
 Pct Recovery = 70%  Analysis Date = 06/25/16 
 Pct Recovery = 70%  Analysis Date = 06/22/16 
 Pct Recovery = 69%  Analysis Date = 06/22/16 
 Pct Recovery = 69%  Analysis Date = 06/20/16 
 Pct Recovery = 69%  Analysis Date = 06/20/16 
 Pct Recovery = 69%  Analysis Date = 06/18/16 
 Pct Recovery = 69%  Analysis Date = 06/18/16 
 Pct Recovery = 69%  Analysis Date = 06/15/16 
 Pct Recovery = 69%  Analysis Date = 06/15/16 
 Pct Recovery = 69%  Analysis Date = 06/13/16 
 Pct Recovery = 69%  Analysis Date = 06/13/16 
 Pct Recovery = 69%  Analysis Date = 06/11/16 
 Pct Recovery = 68%  Analysis Date = 06/11/16 
 Pct Recovery = 68%  Analysis Date = 06/09/16 
 Pct Recovery = 68%  Analysis Date = 06/09/16 
 Pct Recovery = 68%  Analysis Date = 06/06/16 
 Pct Recovery = 68%  Analysis Date = 06/06/16 
 Pct Recovery = 68%  Analysis Date = 06/04/16 
 Pct Recovery = 68%  Analysis Date = 06/04/16 
 Pct Recovery = 68%  Analysis Date = 06/02/16 
 Pct Recovery = 68%  Analysis Date = 06/02/16 
 Pct Recovery = 68%  Analysis Date = 05/30/16 
 Pct Recovery = 68%  Analysis Date = 05/30/16 
 Pct Recovery = 68%  Analysis Date = 05/28/16 
 Pct Recovery = 67%  Analysis Date = 05/28/16 
 Pct Recovery = 67%  Analysis Date = 05/26/16 
 Pct Recovery = 67%  Analysis Date = 05/26/16 
 Pct Recovery = 67%  Analysis Date = 05/24/16 
 Pct Recovery = 67%  Analysis Date = 05/24/16 
 Pct Recovery = 67%  Analysis Date = 05/21/16 
 Pct Recovery = 67%  Analysis Date = 05/21/16 
 Pct Recovery = 67%  Analysis Date = 05/19/16 
 Pct Recovery = 67%  Analysis Date = 05/19/16 
 Pct Recovery = 67%  Analysis Date = 05/17/16 
 Pct Recovery = 67%  Analysis Date = 05/17/16 
 Pct Recovery = 67%  Analysis Date = 05/14/16 
 Pct Recovery = 66%  Analysis Date = 05/14/16 
 Pct Recovery = 66%  Analysis Date = 05/12/16 
 Pct Recovery = 66%  Analysis Date = 05/12/16 
 Pct Recovery = 66%  Analysis Date = 05/10/16 
 Pct Recovery = 66%  Analysis Date = 05/10/16 
 Pct Recovery = 66%  Analysis Date = 05/08/16 
 Pct Recovery = 66%  Analysis Date = 05/08/16 
 Pct Recovery = 66%  Analysis Date = 05/05/16 
 Pct Recovery = 66%  Analysis Date = 05/05/16 
 Pct Recovery = 66%  Analysis Date = 05/03/16 
 Pct Recovery = 65%  Analysis Date = 05/03/16 
 Pct Recovery = 65%  Analysis Date = 05/01/16 
 Pct Recovery = 65%  Analysis Date = 05/01/16 
 Pct Recovery = 65%  Analysis Date = 04/28/16 
 Pct Recovery = 65%  Analysis Date = 04/28/16 
 Pct Recovery = 65%  Analysis Date = 04/26/16 
 Pct Recovery = 64%  Analysis Date = 04/26/16 
 Pct Recovery = 64%  Analysis Date = 04/24/16 
 Pct Recovery = 64%  Analysis Date = 04/24/16 
 Pct Recovery = 64%  Analysis Date = 04/22/16 
 Pct Recovery = 64%  Analysis Date = 04/22/16 
 Pct Recovery = 64%  Analysis Date = 04/19/16 
 Pct Recovery = 63%  Analysis Date = 04/19/16 
 Pct Recovery = 63%  Analysis Date = 04/17/16 
 Pct Recovery = 63%  Analysis Date = 04/17/16 
 Pct Recovery = 63%  Analysis Date = 04/15/16 
 Pct Recovery = 63%  Analysis Date = 04/15/16 
 Pct Recovery = 63%  Analysis Date = 04/12/16 
 Pct Recovery = 62%  Analysis Date = 04/12/16 
 Pct Recovery = 62%  Analysis Date = 04/10/16 
 Pct Recovery = 62%  Analysis Date = 04/10/16 
 Pct Recovery = 62%  Analysis Date = 04/08/16 
 Pct Recovery = 62%  Analysis Date = 04/08/16 
 Pct Recovery = 62%  Analysis Date = 04/06/16 
 Pct Recovery = 61%  Analysis Date = 04/06/16 
 Pct Recovery = 61%  Analysis Date = 04/03/16 
 Pct Recovery = 61%  Analysis Date = 04/03/16 
 Pct Recovery = 61%  Analysis Date = 04/01/16 
 Pct Recovery = 61%  Analysis Date = 04/01/16 
 Pct Recovery = 61%  Analysis Date = 03/30/16 
 Pct Recovery = 60%  Analysis Date = 03/30/16 
 Pct Recovery = 60%  Analysis Date = 03/27/16 
 Pct Recovery = 60%  Analysis Date = 03/27/16 
 Pct Recovery = 60%  Analysis Date = 03/25/16 
 Pct Recovery = 60%  Analysis Date = 03/25/16 
 Pct Recovery = 60%  Analysis Date = 03/23/16 
 Pct Recovery = 59%  Analysis Date = 03/23/16 
 Pct Recovery = 59%  Analysis Date = 03/21/16 
 Pct Recovery = 59%  Analysis Date = 03/21/16 
 Pct Recovery = 59%  Analysis Date = 03/18/16 
 Pct Recovery = 59%  Analysis Date = 03/18/16 
 Pct Recovery = 59%  Analysis Date = 03/16/16 
 Pct Recovery = 58%  Analysis Date = 03/16/16 
 Pct Recovery = 58%  Analysis Date = 03/14/16 
 Pct Recovery = 58%  Analysis Date = 03/14/16 
 Pct Recovery = 58%  Analysis Date = 03/11/16 
 Pct Recovery = 58%  Analysis Date = 03/11/16 
 Pct Recovery = 58%  Analysis Date = 03/09/16 
 Pct Recovery = 57%  Analysis Date = 03/09/16 
 Pct Recovery = 57%  Analysis Date = 03/07/16 
 Pct Recovery = 57%  Analysis Date = 03/07/16 
 Pct Recovery = 57%  Analysis Date = 03/05/16 
 Pct Recovery = 57%  Analysis Date = 03/05/16 
 Pct Recovery = 57%  Analysis Date = 03/02/16 
 Pct Recovery = 56%  Analysis Date = 03/02/16 
 Pct Recovery = 56%  Analysis Date = 02/29/16 
 Pct Recovery = 56%  Analysis Date = 02/29/16 
 Pct Recovery = 56%  Analysis Date = 02/27/16 
 Pct Recovery = 55%  Analysis Date = 02/27/16 
 Pct Recovery = 55%  Analysis Date = 02/24/16 
 Pct Recovery = 55%  Analysis Date = 02/24/16 
 Pct Recovery = 55%  Analysis Date = 02/22/16 
 Pct Recovery = 55%  Analysis Date = 02/22/16 
 Pct Recovery = 55%  Analysis Date = 02/20/16 
 Pct Recovery = 54%  Analysis Date = 02/20/16 
 Pct Recovery = 54%  Analysis Date = 02/18/16 
 Pct Recovery = 54%  Analysis Date = 02/18/16 
 Pct Recovery = 54%  Analysis Date = 02/15/16 
 Pct Recovery = 54%  Analysis Date = 02/15/16 
 Pct Recovery = 54%  Analysis Date = 02/13/16 
 Pct Recovery = 53%  Analysis Date = 02/13/16 
 Pct Recovery = 53%  Analysis Date = 02/11/16 
 Pct Recovery = 53%  Analysis Date = 02/11/16 
 Pct Recovery = 53%  Analysis Date = 02/09/16 
 Pct Recovery = 53%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 69% 13% 66% 11%
Total 18 69% 13% 66% 11%

Sample Statistics
AZINPHOS-METHYL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39

 Analysis Date = 02/22/17 
 SpikeMix = ChemService 5054800: 100 Ál & Abs 060916: 100 Ál 
 Pct Recovery = 62%  Analysis Date = 05/11/17 
 SpikeMix = ChemService 5054800: 80 Ál & Crescent 03FF076: 80 Ál 
 Pct Recovery = 69%  Analysis Date = 08/27/16 
 SpikeMix = ChemService 5054800: 80 Ál & NSI 041816: 80 Ál 
 Pct Recovery = 64%  Analysis Date = 04/24/17 
 SpikeMix = Crescent 03FF076: 40 Ál & ChemService 5054800: 40 Ál 
 Pct Recovery = 90%  Analysis Date = 02/27/17 
 SpikeMix = ChemService 5054800: 40 Ál & Abs 060916: 40 Ál 
 Pct Recovery = 69%  Analysis Date = 05/04/16 
 SpikeMix = Abs 041415: 20 Ál & Abs 040615: 20 Ál 
 Pct Recovery = 102%  Analysis Date = 04/06/16 
 SpikeMix = Spex Organics EN150513008: 20 Ál & Abs 041415: 20 Ál 
 Pct Recovery = 113%  Analysis Date = 03/02/16 
 SpikeMix = Abs 041415: 20 Ál & ChemService 3851600: 20 Ál 
 Pct Recovery = 65%  Analysis Date = 05/10/17 
 Pct Recovery = 70%  Analysis Date = 05/08/17 
 Pct Recovery = 73%  Analysis Date = 05/08/17 
 Pct Recovery = 73%  Analysis Date = 05/06/17 
 Pct Recovery = 75%  Analysis Date = 05/06/17 
 Pct Recovery = 75%  Analysis Date = 05/04/17 
 Pct Recovery = 77%  Analysis Date = 05/04/17 
 Pct Recovery = 77%  Analysis Date = 05/02/17 
 Pct Recovery = 79%  Analysis Date = 05/02/17 
 Pct Recovery = 79%  Analysis Date = 04/30/17 
 Pct Recovery = 81%  Analysis Date = 04/30/17 
 Pct Recovery = 81%  Analysis Date = 04/27/17 
 Pct Recovery = 83%  Analysis Date = 04/27/17 
 Pct Recovery = 83%  Analysis Date = 04/25/17 
 Pct Recovery = 85%  Analysis Date = 04/25/17 
 Pct Recovery = 85%  Analysis Date = 04/23/17 
 Pct Recovery = 86%  Analysis Date = 04/23/17 
 Pct Recovery = 86%  Analysis Date = 04/21/17 
 Pct Recovery = 86%  Analysis Date = 04/21/17 
 Pct Recovery = 86%  Analysis Date = 04/19/17 
 Pct Recovery = 85%  Analysis Date = 04/19/17 
 Pct Recovery = 85%  Analysis Date = 04/17/17 
 Pct Recovery = 84%  Analysis Date = 04/17/17 
 Pct Recovery = 84%  Analysis Date = 04/14/17 
 Pct Recovery = 83%  Analysis Date = 04/14/17 
 Pct Recovery = 83%  Analysis Date = 04/12/17 
 Pct Recovery = 83%  Analysis Date = 04/12/17 
 Pct Recovery = 83%  Analysis Date = 04/10/17 
 Pct Recovery = 82%  Analysis Date = 04/10/17 
 Pct Recovery = 82%  Analysis Date = 04/08/17 
 Pct Recovery = 81%  Analysis Date = 04/08/17 
 Pct Recovery = 81%  Analysis Date = 04/06/17 
 Pct Recovery = 80%  Analysis Date = 04/06/17 
 Pct Recovery = 80%  Analysis Date = 04/04/17 
 Pct Recovery = 79%  Analysis Date = 04/04/17 
 Pct Recovery = 79%  Analysis Date = 04/01/17 
 Pct Recovery = 79%  Analysis Date = 04/01/17 
 Pct Recovery = 79%  Analysis Date = 03/30/17 
 Pct Recovery = 78%  Analysis Date = 03/30/17 
 Pct Recovery = 78%  Analysis Date = 03/28/17 
 Pct Recovery = 77%  Analysis Date = 03/28/17 
 Pct Recovery = 77%  Analysis Date = 03/26/17 
 Pct Recovery = 76%  Analysis Date = 03/26/17 
 Pct Recovery = 76%  Analysis Date = 03/24/17 
 Pct Recovery = 75%  Analysis Date = 03/24/17 
 Pct Recovery = 75%  Analysis Date = 03/21/17 
 Pct Recovery = 75%  Analysis Date = 03/21/17 
 Pct Recovery = 75%  Analysis Date = 03/19/17 
 Pct Recovery = 74%  Analysis Date = 03/19/17 
 Pct Recovery = 74%  Analysis Date = 03/17/17 
 Pct Recovery = 73%  Analysis Date = 03/17/17 
 Pct Recovery = 73%  Analysis Date = 03/15/17 
 Pct Recovery = 72%  Analysis Date = 03/15/17 
 Pct Recovery = 72%  Analysis Date = 03/13/17 
 Pct Recovery = 72%  Analysis Date = 03/13/17 
 Pct Recovery = 72%  Analysis Date = 03/11/17 
 Pct Recovery = 71%  Analysis Date = 03/11/17 
 Pct Recovery = 71%  Analysis Date = 03/08/17 
 Pct Recovery = 70%  Analysis Date = 03/08/17 
 Pct Recovery = 70%  Analysis Date = 03/06/17 
 Pct Recovery = 69%  Analysis Date = 03/06/17 
 Pct Recovery = 69%  Analysis Date = 03/04/17 
 Pct Recovery = 68%  Analysis Date = 03/04/17 
 Pct Recovery = 68%  Analysis Date = 03/02/17 
 Pct Recovery = 68%  Analysis Date = 03/02/17 
 Pct Recovery = 68%  Analysis Date = 02/28/17 
 Pct Recovery = 67%  Analysis Date = 02/28/17 
 Pct Recovery = 67%  Analysis Date = 02/26/17 
 Pct Recovery = 66%  Analysis Date = 02/26/17 
 Pct Recovery = 66%  Analysis Date = 02/23/17 
 Pct Recovery = 65%  Analysis Date = 02/23/17 
 Pct Recovery = 65%  Analysis Date = 02/21/17 
 Pct Recovery = 64%  Analysis Date = 02/21/17 
 Pct Recovery = 64%  Analysis Date = 02/19/17 
 Pct Recovery = 64%  Analysis Date = 02/19/17 
 Pct Recovery = 64%  Analysis Date = 02/17/17 
 Pct Recovery = 64%  Analysis Date = 02/17/17 
 Pct Recovery = 64%  Analysis Date = 02/15/17 
 Pct Recovery = 64%  Analysis Date = 02/15/17 
 Pct Recovery = 64%  Analysis Date = 02/12/17 
 Pct Recovery = 64%  Analysis Date = 02/12/17 
 Pct Recovery = 64%  Analysis Date = 02/10/17 
 Pct Recovery = 64%  Analysis Date = 02/10/17 
 Pct Recovery = 64%  Analysis Date = 02/08/17 
 Pct Recovery = 64%  Analysis Date = 02/08/17 
 Pct Recovery = 64%  Analysis Date = 02/06/17 
 Pct Recovery = 64%  Analysis Date = 02/06/17 
 Pct Recovery = 64%  Analysis Date = 02/04/17 
 Pct Recovery = 64%  Analysis Date = 02/04/17 
 Pct Recovery = 64%  Analysis Date = 02/02/17 
 Pct Recovery = 64%  Analysis Date = 02/02/17 
 Pct Recovery = 64%  Analysis Date = 01/30/17 
 Pct Recovery = 64%  Analysis Date = 01/30/17 
 Pct Recovery = 64%  Analysis Date = 01/28/17 
 Pct Recovery = 64%  Analysis Date = 01/28/17 
 Pct Recovery = 64%  Analysis Date = 01/26/17 
 Pct Recovery = 64%  Analysis Date = 01/26/17 
 Pct Recovery = 64%  Analysis Date = 01/24/17 
 Pct Recovery = 64%  Analysis Date = 01/24/17 
 Pct Recovery = 64%  Analysis Date = 01/22/17 
 Pct Recovery = 64%  Analysis Date = 01/22/17 
 Pct Recovery = 64%  Analysis Date = 01/20/17 
 Pct Recovery = 64%  Analysis Date = 01/20/17 
 Pct Recovery = 64%  Analysis Date = 01/17/17 
 Pct Recovery = 64%  Analysis Date = 01/17/17 
 Pct Recovery = 64%  Analysis Date = 01/15/17 
 Pct Recovery = 64%  Analysis Date = 01/15/17 
 Pct Recovery = 64%  Analysis Date = 01/13/17 
 Pct Recovery = 64%  Analysis Date = 01/13/17 
 Pct Recovery = 64%  Analysis Date = 01/11/17 
 Pct Recovery = 64%  Analysis Date = 01/11/17 
 Pct Recovery = 64%  Analysis Date = 01/09/17 
 Pct Recovery = 64%  Analysis Date = 01/09/17 
 Pct Recovery = 64%  Analysis Date = 01/07/17 
 Pct Recovery = 64%  Analysis Date = 01/07/17 
 Pct Recovery = 64%  Analysis Date = 01/04/17 
 Pct Recovery = 64%  Analysis Date = 01/04/17 
 Pct Recovery = 64%  Analysis Date = 01/02/17 
 Pct Recovery = 64%  Analysis Date = 01/02/17 
 Pct Recovery = 64%  Analysis Date = 12/31/16 
 Pct Recovery = 64%  Analysis Date = 12/31/16 
 Pct Recovery = 64%  Analysis Date = 12/29/16 
 Pct Recovery = 64%  Analysis Date = 12/29/16 
 Pct Recovery = 64%  Analysis Date = 12/27/16 
 Pct Recovery = 64%  Analysis Date = 12/27/16 
 Pct Recovery = 64%  Analysis Date = 12/24/16 
 Pct Recovery = 64%  Analysis Date = 12/24/16 
 Pct Recovery = 64%  Analysis Date = 12/22/16 
 Pct Recovery = 64%  Analysis Date = 12/22/16 
 Pct Recovery = 64%  Analysis Date = 12/20/16 
 Pct Recovery = 64%  Analysis Date = 12/20/16 
 Pct Recovery = 64%  Analysis Date = 12/18/16 
 Pct Recovery = 64%  Analysis Date = 12/18/16 
 Pct Recovery = 64%  Analysis Date = 12/16/16 
 Pct Recovery = 64%  Analysis Date = 12/16/16 
 Pct Recovery = 64%  Analysis Date = 12/14/16 
 Pct Recovery = 64%  Analysis Date = 12/14/16 
 Pct Recovery = 64%  Analysis Date = 12/11/16 
 Pct Recovery = 64%  Analysis Date = 12/11/16 
 Pct Recovery = 64%  Analysis Date = 12/09/16 
 Pct Recovery = 64%  Analysis Date = 12/09/16 
 Pct Recovery = 64%  Analysis Date = 12/07/16 
 Pct Recovery = 64%  Analysis Date = 12/07/16 
 Pct Recovery = 64%  Analysis Date = 12/05/16 
 Pct Recovery = 64%  Analysis Date = 12/05/16 
 Pct Recovery = 64%  Analysis Date = 12/03/16 
 Pct Recovery = 64%  Analysis Date = 12/03/16 
 Pct Recovery = 64%  Analysis Date = 12/01/16 
 Pct Recovery = 64%  Analysis Date = 12/01/16 
 Pct Recovery = 64%  Analysis Date = 11/28/16 
 Pct Recovery = 64%  Analysis Date = 11/28/16 
 Pct Recovery = 64%  Analysis Date = 11/26/16 
 Pct Recovery = 64%  Analysis Date = 11/26/16 
 Pct Recovery = 64%  Analysis Date = 11/24/16 
 Pct Recovery = 64%  Analysis Date = 11/24/16 
 Pct Recovery = 64%  Analysis Date = 11/22/16 
 Pct Recovery = 64%  Analysis Date = 11/22/16 
 Pct Recovery = 64%  Analysis Date = 11/20/16 
 Pct Recovery = 64%  Analysis Date = 11/20/16 
 Pct Recovery = 64%  Analysis Date = 11/17/16 
 Pct Recovery = 64%  Analysis Date = 11/17/16 
 Pct Recovery = 64%  Analysis Date = 11/15/16 
 Pct Recovery = 64%  Analysis Date = 11/15/16 
 Pct Recovery = 64%  Analysis Date = 11/13/16 
 Pct Recovery = 64%  Analysis Date = 11/13/16 
 Pct Recovery = 64%  Analysis Date = 11/11/16 
 Pct Recovery = 64%  Analysis Date = 11/11/16 
 Pct Recovery = 64%  Analysis Date = 11/09/16 
 Pct Recovery = 64%  Analysis Date = 11/09/16 
 Pct Recovery = 64%  Analysis Date = 11/07/16 
 Pct Recovery = 64%  Analysis Date = 11/07/16 
 Pct Recovery = 64%  Analysis Date = 11/04/16 
 Pct Recovery = 64%  Analysis Date = 11/04/16 
 Pct Recovery = 64%  Analysis Date = 11/02/16 
 Pct Recovery = 64%  Analysis Date = 11/02/16 
 Pct Recovery = 64%  Analysis Date = 10/31/16 
 Pct Recovery = 64%  Analysis Date = 10/31/16 
 Pct Recovery = 64%  Analysis Date = 10/29/16 
 Pct Recovery = 64%  Analysis Date = 10/29/16 
 Pct Recovery = 64%  Analysis Date = 10/27/16 
 Pct Recovery = 64%  Analysis Date = 10/27/16 
 Pct Recovery = 64%  Analysis Date = 10/25/16 
 Pct Recovery = 64%  Analysis Date = 10/25/16 
 Pct Recovery = 64%  Analysis Date = 10/22/16 
 Pct Recovery = 64%  Analysis Date = 10/22/16 
 Pct Recovery = 64%  Analysis Date = 10/20/16 
 Pct Recovery = 64%  Analysis Date = 10/20/16 
 Pct Recovery = 64%  Analysis Date = 10/18/16 
 Pct Recovery = 64%  Analysis Date = 10/18/16 
 Pct Recovery = 64%  Analysis Date = 10/16/16 
 Pct Recovery = 64%  Analysis Date = 10/16/16 
 Pct Recovery = 64%  Analysis Date = 10/14/16 
 Pct Recovery = 64%  Analysis Date = 10/14/16 
 Pct Recovery = 64%  Analysis Date = 10/12/16 
 Pct Recovery = 64%  Analysis Date = 10/12/16 
 Pct Recovery = 64%  Analysis Date = 10/09/16 
 Pct Recovery = 64%  Analysis Date = 10/09/16 
 Pct Recovery = 64%  Analysis Date = 10/07/16 
 Pct Recovery = 64%  Analysis Date = 10/07/16 
 Pct Recovery = 64%  Analysis Date = 10/05/16 
 Pct Recovery = 64%  Analysis Date = 10/05/16 
 Pct Recovery = 64%  Analysis Date = 10/03/16 
 Pct Recovery = 64%  Analysis Date = 10/03/16 
 Pct Recovery = 64%  Analysis Date = 10/01/16 
 Pct Recovery = 64%  Analysis Date = 10/01/16 
 Pct Recovery = 64%  Analysis Date = 09/28/16 
 Pct Recovery = 64%  Analysis Date = 09/28/16 
 Pct Recovery = 64%  Analysis Date = 09/26/16 
 Pct Recovery = 64%  Analysis Date = 09/26/16 
 Pct Recovery = 64%  Analysis Date = 09/24/16 
 Pct Recovery = 64%  Analysis Date = 09/24/16 
 Pct Recovery = 64%  Analysis Date = 09/22/16 
 Pct Recovery = 64%  Analysis Date = 09/22/16 
 Pct Recovery = 64%  Analysis Date = 09/20/16 
 Pct Recovery = 64%  Analysis Date = 09/20/16 
 Pct Recovery = 64%  Analysis Date = 09/18/16 
 Pct Recovery = 64%  Analysis Date = 09/18/16 
 Pct Recovery = 64%  Analysis Date = 09/15/16 
 Pct Recovery = 64%  Analysis Date = 09/15/16 
 Pct Recovery = 64%  Analysis Date = 09/13/16 
 Pct Recovery = 64%  Analysis Date = 09/13/16 
 Pct Recovery = 64%  Analysis Date = 09/11/16 
 Pct Recovery = 64%  Analysis Date = 09/11/16 
 Pct Recovery = 64%  Analysis Date = 09/09/16 
 Pct Recovery = 64%  Analysis Date = 09/09/16 
 Pct Recovery = 64%  Analysis Date = 09/07/16 
 Pct Recovery = 64%  Analysis Date = 09/07/16 
 Pct Recovery = 64%  Analysis Date = 09/05/16 
 Pct Recovery = 64%  Analysis Date = 09/05/16 
 Pct Recovery = 64%  Analysis Date = 09/02/16 
 Pct Recovery = 64%  Analysis Date = 09/02/16 
 Pct Recovery = 64%  Analysis Date = 08/31/16 
 Pct Recovery = 64%  Analysis Date = 08/31/16 
 Pct Recovery = 64%  Analysis Date = 08/29/16 
 Pct Recovery = 64%  Analysis Date = 08/29/16 
 Pct Recovery = 64%  Analysis Date = 08/27/16 
 Pct Recovery = 64%  Analysis Date = 08/27/16 
 Pct Recovery = 64%  Analysis Date = 08/25/16 
 Pct Recovery = 65%  Analysis Date = 08/25/16 
 Pct Recovery = 65%  Analysis Date = 08/22/16 
 Pct Recovery = 65%  Analysis Date = 08/22/16 
 Pct Recovery = 65%  Analysis Date = 08/20/16 
 Pct Recovery = 66%  Analysis Date = 08/20/16 
 Pct Recovery = 66%  Analysis Date = 08/18/16 
 Pct Recovery = 67%  Analysis Date = 08/18/16 
 Pct Recovery = 67%  Analysis Date = 08/16/16 
 Pct Recovery = 68%  Analysis Date = 08/16/16 
 Pct Recovery = 68%  Analysis Date = 08/14/16 
 Pct Recovery = 69%  Analysis Date = 08/14/16 
 Pct Recovery = 69%  Analysis Date = 08/12/16 
 Pct Recovery = 70%  Analysis Date = 08/12/16 
 Pct Recovery = 70%  Analysis Date = 08/09/16 
 Pct Recovery = 71%  Analysis Date = 08/09/16 
 Pct Recovery = 71%  Analysis Date = 08/07/16 
 Pct Recovery = 72%  Analysis Date = 08/07/16 
 Pct Recovery = 72%  Analysis Date = 08/05/16 
 Pct Recovery = 73%  Analysis Date = 08/05/16 
 Pct Recovery = 73%  Analysis Date = 08/03/16 
 Pct Recovery = 73%  Analysis Date = 08/03/16 
 Pct Recovery = 73%  Analysis Date = 08/01/16 
 Pct Recovery = 74%  Analysis Date = 08/01/16 
 Pct Recovery = 74%  Analysis Date = 07/30/16 
 Pct Recovery = 75%  Analysis Date = 07/30/16 
 Pct Recovery = 75%  Analysis Date = 07/27/16 
 Pct Recovery = 76%  Analysis Date = 07/27/16 
 Pct Recovery = 76%  Analysis Date = 07/25/16 
 Pct Recovery = 77%  Analysis Date = 07/25/16 
 Pct Recovery = 77%  Analysis Date = 07/23/16 
 Pct Recovery = 78%  Analysis Date = 07/23/16 
 Pct Recovery = 78%  Analysis Date = 07/21/16 
 Pct Recovery = 79%  Analysis Date = 07/21/16 
 Pct Recovery = 79%  Analysis Date = 07/19/16 
 Pct Recovery = 80%  Analysis Date = 07/19/16 
 Pct Recovery = 80%  Analysis Date = 07/17/16 
 Pct Recovery = 81%  Analysis Date = 07/17/16 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/14/16 
 Pct Recovery = 81%  Analysis Date = 07/12/16 
 Pct Recovery = 82%  Analysis Date = 07/12/16 
 Pct Recovery = 82%  Analysis Date = 07/10/16 
 Pct Recovery = 83%  Analysis Date = 07/10/16 
 Pct Recovery = 83%  Analysis Date = 07/08/16 
 Pct Recovery = 84%  Analysis Date = 07/08/16 
 Pct Recovery = 84%  Analysis Date = 07/06/16 
 Pct Recovery = 85%  Analysis Date = 07/06/16 
 Pct Recovery = 85%  Analysis Date = 07/03/16 
 Pct Recovery = 86%  Analysis Date = 07/03/16 
 Pct Recovery = 86%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 07/01/16 
 Pct Recovery = 87%  Analysis Date = 06/29/16 
 Pct Recovery = 88%  Analysis Date = 06/29/16 
 Pct Recovery = 88%  Analysis Date = 06/27/16 
 Pct Recovery = 89%  Analysis Date = 06/27/16 
 Pct Recovery = 89%  Analysis Date = 06/25/16 
 Pct Recovery = 89%  Analysis Date = 06/25/16 
 Pct Recovery = 89%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/23/16 
 Pct Recovery = 90%  Analysis Date = 06/20/16 
 Pct Recovery = 91%  Analysis Date = 06/20/16 
 Pct Recovery = 91%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/18/16 
 Pct Recovery = 92%  Analysis Date = 06/16/16 
 Pct Recovery = 93%  Analysis Date = 06/16/16 
 Pct Recovery = 93%  Analysis Date = 06/14/16 
 Pct Recovery = 94%  Analysis Date = 06/14/16 
 Pct Recovery = 94%  Analysis Date = 06/12/16 
 Pct Recovery = 95%  Analysis Date = 06/12/16 
 Pct Recovery = 95%  Analysis Date = 06/10/16 
 Pct Recovery = 96%  Analysis Date = 06/10/16 
 Pct Recovery = 96%  Analysis Date = 06/07/16 
 Pct Recovery = 97%  Analysis Date = 06/07/16 
 Pct Recovery = 97%  Analysis Date = 06/05/16 
 Pct Recovery = 97%  Analysis Date = 06/05/16 
 Pct Recovery = 97%  Analysis Date = 06/03/16 
 Pct Recovery = 98%  Analysis Date = 06/03/16 
 Pct Recovery = 98%  Analysis Date = 06/01/16 
 Pct Recovery = 99%  Analysis Date = 06/01/16 
 Pct Recovery = 99%  Analysis Date = 05/30/16 
 Pct Recovery = 100%  Analysis Date = 05/30/16 
 Pct Recovery = 100%  Analysis Date = 05/27/16 
 Pct Recovery = 101%  Analysis Date = 05/27/16 
 Pct Recovery = 101%  Analysis Date = 05/25/16 
 Pct Recovery = 102%  Analysis Date = 05/25/16 
 Pct Recovery = 102%  Analysis Date = 05/23/16 
 Pct Recovery = 103%  Analysis Date = 05/23/16 
 Pct Recovery = 103%  Analysis Date = 05/21/16 
 Pct Recovery = 104%  Analysis Date = 05/21/16 
 Pct Recovery = 104%  Analysis Date = 05/19/16 
 Pct Recovery = 105%  Analysis Date = 05/19/16 
 Pct Recovery = 105%  Analysis Date = 05/17/16 
 Pct Recovery = 105%  Analysis Date = 05/17/16 
 Pct Recovery = 105%  Analysis Date = 05/14/16 
 Pct Recovery = 106%  Analysis Date = 05/14/16 
 Pct Recovery = 106%  Analysis Date = 05/12/16 
 Pct Recovery = 107%  Analysis Date = 05/12/16 
 Pct Recovery = 107%  Analysis Date = 05/10/16 
 Pct Recovery = 108%  Analysis Date = 05/10/16 
 Pct Recovery = 108%  Analysis Date = 05/08/16 
 Pct Recovery = 109%  Analysis Date = 05/08/16 
 Pct Recovery = 109%  Analysis Date = 05/06/16 
 Pct Recovery = 110%  Analysis Date = 05/06/16 
 Pct Recovery = 110%  Analysis Date = 05/04/16 
 Pct Recovery = 111%  Analysis Date = 05/04/16 
 Pct Recovery = 111%  Analysis Date = 05/01/16 
 Pct Recovery = 110%  Analysis Date = 05/01/16 
 Pct Recovery = 110%  Analysis Date = 04/29/16 
 Pct Recovery = 108%  Analysis Date = 04/29/16 
 Pct Recovery = 108%  Analysis Date = 04/27/16 
 Pct Recovery = 107%  Analysis Date = 04/27/16 
 Pct Recovery = 107%  Analysis Date = 04/25/16 
 Pct Recovery = 106%  Analysis Date = 04/25/16 
 Pct Recovery = 106%  Analysis Date = 04/23/16 
 Pct Recovery = 105%  Analysis Date = 04/23/16 
 Pct Recovery = 105%  Analysis Date = 04/21/16 
 Pct Recovery = 103%  Analysis Date = 04/21/16 
 Pct Recovery = 103%  Analysis Date = 04/18/16 
 Pct Recovery = 102%  Analysis Date = 04/18/16 
 Pct Recovery = 102%  Analysis Date = 04/16/16 
 Pct Recovery = 101%  Analysis Date = 04/16/16 
 Pct Recovery = 101%  Analysis Date = 04/14/16 
 Pct Recovery = 100%  Analysis Date = 04/14/16 
 Pct Recovery = 100%  Analysis Date = 04/12/16 
 Pct Recovery = 98%  Analysis Date = 04/12/16 
 Pct Recovery = 98%