OBSP Determination:
1,7-DIMETHYLXANTHINE (P-XANTHINE)
METHOD: LC9017 , TESTIDCODE: 67446LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 80%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 98%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 93%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 101%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 62%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 96%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 55%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 Pct Recovery = 62%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/11/14 
 Pct Recovery = 63%  Analysis Date = 03/11/14 
 Pct Recovery = 63%  Analysis Date = 03/09/14 
 Pct Recovery = 63%  Analysis Date = 03/09/14 
 Pct Recovery = 63%  Analysis Date = 03/07/14 
 Pct Recovery = 63%  Analysis Date = 03/07/14 
 Pct Recovery = 63%  Analysis Date = 03/04/14 
 Pct Recovery = 63%  Analysis Date = 03/04/14 
 Pct Recovery = 63%  Analysis Date = 03/02/14 
 Pct Recovery = 63%  Analysis Date = 03/02/14 
 Pct Recovery = 63%  Analysis Date = 02/28/14 
 Pct Recovery = 63%  Analysis Date = 02/28/14 
 Pct Recovery = 63%  Analysis Date = 02/25/14 
 Pct Recovery = 63%  Analysis Date = 02/25/14 
 Pct Recovery = 63%  Analysis Date = 02/23/14 
 Pct Recovery = 64%  Analysis Date = 02/23/14 
 Pct Recovery = 64%  Analysis Date = 02/21/14 
 Pct Recovery = 64%  Analysis Date = 02/21/14 
 Pct Recovery = 64%  Analysis Date = 02/18/14 
 Pct Recovery = 64%  Analysis Date = 02/18/14 
 Pct Recovery = 64%  Analysis Date = 02/16/14 
 Pct Recovery = 64%  Analysis Date = 02/16/14 
 Pct Recovery = 64%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 65%  Analysis Date = 02/07/14 
 Pct Recovery = 65%  Analysis Date = 02/05/14 
 Pct Recovery = 65%  Analysis Date = 02/05/14 
 Pct Recovery = 65%  Analysis Date = 02/02/14 
 Pct Recovery = 65%  Analysis Date = 02/02/14 
 Pct Recovery = 65%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/29/14 
 Pct Recovery = 65%  Analysis Date = 01/29/14 
 Pct Recovery = 65%  Analysis Date = 01/26/14 
 Pct Recovery = 65%  Analysis Date = 01/26/14 
 Pct Recovery = 65%  Analysis Date = 01/24/14 
 Pct Recovery = 65%  Analysis Date = 01/24/14 
 Pct Recovery = 65%  Analysis Date = 01/22/14 
 Pct Recovery = 65%  Analysis Date = 01/22/14 
 Pct Recovery = 65%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/23/13 
 Pct Recovery = 67%  Analysis Date = 12/23/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/16/13 
 Pct Recovery = 68%  Analysis Date = 12/16/13 
 Pct Recovery = 68%  Analysis Date = 12/13/13 
 Pct Recovery = 68%  Analysis Date = 12/13/13 
 Pct Recovery = 68%  Analysis Date = 12/11/13 
 Pct Recovery = 68%  Analysis Date = 12/11/13 
 Pct Recovery = 68%  Analysis Date = 12/09/13 
 Pct Recovery = 68%  Analysis Date = 12/09/13 
 Pct Recovery = 68%  Analysis Date = 12/07/13 
 Pct Recovery = 68%  Analysis Date = 12/07/13 
 Pct Recovery = 68%  Analysis Date = 12/04/13 
 Pct Recovery = 69%  Analysis Date = 12/04/13 
 Pct Recovery = 69%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/27/13 
 Pct Recovery = 69%  Analysis Date = 11/27/13 
 Pct Recovery = 69%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/23/13 
 Pct Recovery = 69%  Analysis Date = 11/23/13 
 Pct Recovery = 69%  Analysis Date = 11/20/13 
 Pct Recovery = 69%  Analysis Date = 11/20/13 
 Pct Recovery = 69%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 10/31/13 
 Pct Recovery = 71%  Analysis Date = 10/31/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/26/13 
 Pct Recovery = 71%  Analysis Date = 10/26/13 
 Pct Recovery = 71%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/10/13 
 Pct Recovery = 73%  Analysis Date = 10/10/13 
 Pct Recovery = 73%  Analysis Date = 10/07/13 
 Pct Recovery = 73%  Analysis Date = 10/07/13 
 Pct Recovery = 73%  Analysis Date = 10/05/13 
 Pct Recovery = 73%  Analysis Date = 10/05/13 
 Pct Recovery = 73%  Analysis Date = 10/03/13 
 Pct Recovery = 73%  Analysis Date = 10/03/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 09/28/13 
 Pct Recovery = 74%  Analysis Date = 09/28/13 
 Pct Recovery = 74%  Analysis Date = 09/26/13 
 Pct Recovery = 74%  Analysis Date = 09/26/13 
 Pct Recovery = 74%  Analysis Date = 09/24/13 
 Pct Recovery = 74%  Analysis Date = 09/24/13 
 Pct Recovery = 74%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 75%  Analysis Date = 09/14/13 
 Pct Recovery = 75%  Analysis Date = 09/12/13 
 Pct Recovery = 75%  Analysis Date = 09/12/13 
 Pct Recovery = 75%  Analysis Date = 09/10/13 
 Pct Recovery = 75%  Analysis Date = 09/10/13 
 Pct Recovery = 75%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/03/13 
 Pct Recovery = 76%  Analysis Date = 09/03/13 
 Pct Recovery = 76%  Analysis Date = 09/01/13 
 Pct Recovery = 76%  Analysis Date = 09/01/13 
 Pct Recovery = 76%  Analysis Date = 08/29/13 
 Pct Recovery = 76%  Analysis Date = 08/29/13 
 Pct Recovery = 76%  Analysis Date = 08/27/13 
 Pct Recovery = 76%  Analysis Date = 08/27/13 
 Pct Recovery = 76%  Analysis Date = 08/25/13 
 Pct Recovery = 76%  Analysis Date = 08/25/13 
 Pct Recovery = 76%  Analysis Date = 08/22/13 
 Pct Recovery = 76%  Analysis Date = 08/22/13 
 Pct Recovery = 76%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 78%  Analysis Date = 08/11/13 
 Pct Recovery = 78%  Analysis Date = 08/08/13 
 Pct Recovery = 78%  Analysis Date = 08/08/13 
 Pct Recovery = 78%  Analysis Date = 08/06/13 
 Pct Recovery = 78%  Analysis Date = 08/06/13 
 Pct Recovery = 78%  Analysis Date = 08/04/13 
 Pct Recovery = 78%  Analysis Date = 08/04/13 
 Pct Recovery = 78%  Analysis Date = 08/02/13 
 Pct Recovery = 78%  Analysis Date = 08/02/13 
 Pct Recovery = 78%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/28/13 
 Pct Recovery = 79%  Analysis Date = 07/28/13 
 Pct Recovery = 79%  Analysis Date = 07/26/13 
 Pct Recovery = 79%  Analysis Date = 07/26/13 
 Pct Recovery = 79%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/19/13 
 Pct Recovery = 80%  Analysis Date = 07/19/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/12/13 
 Pct Recovery = 80%  Analysis Date = 07/12/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/07/13 
 Pct Recovery = 81%  Analysis Date = 07/07/13 
 Pct Recovery = 81%  Analysis Date = 07/05/13 
 Pct Recovery = 81%  Analysis Date = 07/05/13 
 Pct Recovery = 81%  Analysis Date = 07/02/13 
 Pct Recovery = 81%  Analysis Date = 07/02/13 
 Pct Recovery = 81%  Analysis Date = 06/30/13 
 Pct Recovery = 81%  Analysis Date = 06/30/13 
 Pct Recovery = 81%  Analysis Date = 06/28/13 
 Pct Recovery = 82%  Analysis Date = 06/28/13 
 Pct Recovery = 82%  Analysis Date = 06/26/13 
 Pct Recovery = 82%  Analysis Date = 06/26/13 
 Pct Recovery = 82%  Analysis Date = 06/23/13 
 Pct Recovery = 82%  Analysis Date = 06/23/13 
 Pct Recovery = 82%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/16/13 
 Pct Recovery = 83%  Analysis Date = 06/16/13 
 Pct Recovery = 83%  Analysis Date = 06/14/13 
 Pct Recovery = 83%  Analysis Date = 06/14/13 
 Pct Recovery = 83%  Analysis Date = 06/12/13 
 Pct Recovery = 83%  Analysis Date = 06/12/13 
 Pct Recovery = 83%  Analysis Date = 06/09/13 
 Pct Recovery = 83%  Analysis Date = 06/09/13 
 Pct Recovery = 83%  Analysis Date = 06/07/13 
 Pct Recovery = 84%  Analysis Date = 06/07/13 
 Pct Recovery = 84%  Analysis Date = 06/05/13 
 Pct Recovery = 84%  Analysis Date = 06/05/13 
 Pct Recovery = 84%  Analysis Date = 06/02/13 
 Pct Recovery = 84%  Analysis Date = 06/02/13 
 Pct Recovery = 84%  Analysis Date = 05/31/13 
 Pct Recovery = 84%  Analysis Date = 05/31/13 
 Pct Recovery = 84%  Analysis Date = 05/29/13 
 Pct Recovery = 84%  Analysis Date = 05/29/13 
 Pct Recovery = 84%  Analysis Date = 05/27/13 
 Pct Recovery = 85%  Analysis Date = 05/27/13 
 Pct Recovery = 85%  Analysis Date = 05/24/13 
 Pct Recovery = 85%  Analysis Date = 05/24/13 
 Pct Recovery = 85%  Analysis Date = 05/22/13 
 Pct Recovery = 85%  Analysis Date = 05/22/13 
 Pct Recovery = 85%  Analysis Date = 05/20/13 
 Pct Recovery = 85%  Analysis Date = 05/20/13 
 Pct Recovery = 85%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/15/13 
 Pct Recovery = 86%  Analysis Date = 05/15/13 
 Pct Recovery = 86%  Analysis Date = 05/13/13 
 Pct Recovery = 86%  Analysis Date = 05/13/13 
 Pct Recovery = 86%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/08/13 
 Pct Recovery = 86%  Analysis Date = 05/08/13 
 Pct Recovery = 86%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/03/13 
 Pct Recovery = 87%  Analysis Date = 05/03/13 
 Pct Recovery = 87%  Analysis Date = 05/01/13 
 Pct Recovery = 87%  Analysis Date = 05/01/13 
 Pct Recovery = 87%  Analysis Date = 04/29/13 
 Pct Recovery = 87%  Analysis Date = 04/29/13 
 Pct Recovery = 87%  Analysis Date = 04/26/13 
 Pct Recovery = 87%  Analysis Date = 04/26/13 
 Pct Recovery = 87%  Analysis Date = 04/24/13 
 Pct Recovery = 88%  Analysis Date = 04/24/13 
 Pct Recovery = 88%  Analysis Date = 04/22/13 
 Pct Recovery = 88%  Analysis Date = 04/22/13 
 Pct Recovery = 88%  Analysis Date = 04/20/13 
 Pct Recovery = 88%  Analysis Date = 04/20/13 
 Pct Recovery = 88%  Analysis Date = 04/17/13 
 Pct Recovery = 88%  Analysis Date = 04/17/13 
 Pct Recovery = 88%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/13/13 
 Pct Recovery = 89%  Analysis Date = 04/13/13 
 Pct Recovery = 89%  Analysis Date = 04/10/13 
 Pct Recovery = 89%  Analysis Date = 04/10/13 
 Pct Recovery = 89%  Analysis Date = 04/08/13 
 Pct Recovery = 90%  Analysis Date = 04/08/13 
 Pct Recovery = 90%  Analysis Date = 04/06/13 
 Pct Recovery = 90%  Analysis Date = 04/06/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/25/13 
 Pct Recovery = 91%  Analysis Date = 03/25/13 
 Pct Recovery = 91%  Analysis Date = 03/23/13 
 Pct Recovery = 91%  Analysis Date = 03/23/13 
 Pct Recovery = 91%  Analysis Date = 03/21/13 
 Pct Recovery = 92%  Analysis Date = 03/21/13 
 Pct Recovery = 92%  Analysis Date = 03/18/13 
 Pct Recovery = 92%  Analysis Date = 03/18/13 
 Pct Recovery = 92%  Analysis Date = 03/16/13 
 Pct Recovery = 92%  Analysis Date = 03/16/13 
 Pct Recovery = 92%  Analysis Date = 03/14/13 
 Pct Recovery = 92%  Analysis Date = 03/14/13 
 Pct Recovery = 92%  Analysis Date = 03/11/13 
 Pct Recovery = 93%  Analysis Date = 03/11/13 
 Pct Recovery = 93%  Analysis Date = 03/09/13 
 Pct Recovery = 93%  Analysis Date = 03/09/13 
 Pct Recovery = 93%  Analysis Date = 03/07/13 
 Pct Recovery = 93%  Analysis Date = 03/07/13 
 Pct Recovery = 93%  Analysis Date = 03/04/13 
 Pct Recovery = 94%  Analysis Date = 03/04/13 
 Pct Recovery = 94%  Analysis Date = 03/02/13 
 Pct Recovery = 94%  Analysis Date = 03/02/13 
 Pct Recovery = 94%  Analysis Date = 02/28/13 
 Pct Recovery = 94%  Analysis Date = 02/28/13 
 Pct Recovery = 94%  Analysis Date = 02/25/13 
 Pct Recovery = 94%  Analysis Date = 02/25/13 
 Pct Recovery = 94%  Analysis Date = 02/23/13 
 Pct Recovery = 95%  Analysis Date = 02/23/13 
 Pct Recovery = 95%  Analysis Date = 02/21/13 
 Pct Recovery = 95%  Analysis Date = 02/21/13 
 Pct Recovery = 95%  Analysis Date = 02/18/13 
 Pct Recovery = 95%  Analysis Date = 02/18/13 
 Pct Recovery = 95%  Analysis Date = 02/16/13 
 Pct Recovery = 95%  Analysis Date = 02/16/13 
 Pct Recovery = 95%  Analysis Date = 02/14/13 
 Pct Recovery = 96%  Analysis Date = 02/14/13 
 Pct Recovery = 96%  Analysis Date = 02/12/13 
 Pct Recovery = 96%  Analysis Date = 02/12/13 
 Pct Recovery = 96%  Analysis Date = 02/09/13 
 Pct Recovery = 96%  Analysis Date = 02/09/13 
 Pct Recovery = 96%  Analysis Date = 02/07/13 
 Pct Recovery = 96%  Analysis Date = 02/07/13 
 Pct Recovery = 96%  Analysis Date = 02/05/13 
 Pct Recovery = 97%  Analysis Date = 02/05/13 
 Pct Recovery = 97%  Analysis Date = 02/02/13 
 Pct Recovery = 97%  Analysis Date = 02/02/13 
 Pct Recovery = 97%  Analysis Date = 01/31/13 
 Pct Recovery = 97%  Analysis Date = 01/31/13 
 Pct Recovery = 97%  Analysis Date = 01/29/13 
 Pct Recovery = 97%  Analysis Date = 01/29/13 
 Pct Recovery = 97%  Analysis Date = 01/26/13 
 Pct Recovery = 98%  Analysis Date = 01/26/13 
 Pct Recovery = 98%  Analysis Date = 01/24/13 
 Pct Recovery = 98%  Analysis Date = 01/24/13 
 Pct Recovery = 98%  Analysis Date = 01/22/13 
 Pct Recovery = 98%  Analysis Date = 01/22/13 
 Pct Recovery = 98%  Analysis Date = 01/19/13 
 Pct Recovery = 98%  Analysis Date = 01/19/13 
 Pct Recovery = 98%  Analysis Date = 01/17/13 
 Pct Recovery = 99%  Analysis Date = 01/17/13 
 Pct Recovery = 99%  Analysis Date = 01/15/13 
 Pct Recovery = 99%  Analysis Date = 01/15/13 
 Pct Recovery = 99%  Analysis Date = 01/13/13 
 Pct Recovery = 99%  Analysis Date = 01/13/13 
 Pct Recovery = 99%  Analysis Date = 01/10/13 
 Pct Recovery = 99%  Analysis Date = 01/10/13 
 Pct Recovery = 99%  Analysis Date = 01/08/13 
 Pct Recovery = 100%  Analysis Date = 01/08/13 
 Pct Recovery = 100%  Analysis Date = 01/06/13 
 Pct Recovery = 100%  Analysis Date = 01/06/13 
 Pct Recovery = 100%  Analysis Date = 01/03/13 
 Pct Recovery = 100%  Analysis Date = 01/03/13 
 Pct Recovery = 100%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 12/30/12 
 Pct Recovery = 101%  Analysis Date = 12/30/12 
 Pct Recovery = 101%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/14/12 
 Pct Recovery = 102%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
1,7-DIMETHYLXANTHINE (P-XANTHINE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 79% 16% 77% 23%
Total 11 79% 16% 77% 23%

Sample Statistics
1,7-DIMETHYLXANTHINE (P-XANTHINE)

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 1 9% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
10-HYDROXY-AMITRIPTYLINE
METHOD: LC9017 , TESTIDCODE: 67995LCM56

The SGPlot Procedure

Sample Statistics
10-HYDROXY-AMITRIPTYLINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
ABACAVIR
METHOD: LC9017 , TESTIDCODE: 68022LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 58%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 58%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 73%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 55%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 57%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 61%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 44%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 72%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/21/14 
 Pct Recovery = 59%  Analysis Date = 02/21/14 
 Pct Recovery = 59%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/16/14 
 Pct Recovery = 60%  Analysis Date = 02/16/14 
 Pct Recovery = 60%  Analysis Date = 02/14/14 
 Pct Recovery = 60%  Analysis Date = 02/14/14 
 Pct Recovery = 60%  Analysis Date = 02/12/14 
 Pct Recovery = 60%  Analysis Date = 02/12/14 
 Pct Recovery = 60%  Analysis Date = 02/09/14 
 Pct Recovery = 60%  Analysis Date = 02/09/14 
 Pct Recovery = 60%  Analysis Date = 02/07/14 
 Pct Recovery = 60%  Analysis Date = 02/07/14 
 Pct Recovery = 60%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/29/14 
 Pct Recovery = 60%  Analysis Date = 01/29/14 
 Pct Recovery = 60%  Analysis Date = 01/26/14 
 Pct Recovery = 60%  Analysis Date = 01/26/14 
 Pct Recovery = 60%  Analysis Date = 01/24/14 
 Pct Recovery = 60%  Analysis Date = 01/24/14 
 Pct Recovery = 60%  Analysis Date = 01/22/14 
 Pct Recovery = 60%  Analysis Date = 01/22/14 
 Pct Recovery = 60%  Analysis Date = 01/19/14 
 Pct Recovery = 60%  Analysis Date = 01/19/14 
 Pct Recovery = 60%  Analysis Date = 01/17/14 
 Pct Recovery = 60%  Analysis Date = 01/17/14 
 Pct Recovery = 60%  Analysis Date = 01/15/14 
 Pct Recovery = 60%  Analysis Date = 01/15/14 
 Pct Recovery = 60%  Analysis Date = 01/13/14 
 Pct Recovery = 60%  Analysis Date = 01/13/14 
 Pct Recovery = 60%  Analysis Date = 01/10/14 
 Pct Recovery = 60%  Analysis Date = 01/10/14 
 Pct Recovery = 60%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/25/13 
 Pct Recovery = 61%  Analysis Date = 12/25/13 
 Pct Recovery = 61%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/20/13 
 Pct Recovery = 61%  Analysis Date = 12/20/13 
 Pct Recovery = 61%  Analysis Date = 12/18/13 
 Pct Recovery = 61%  Analysis Date = 12/18/13 
 Pct Recovery = 61%  Analysis Date = 12/16/13 
 Pct Recovery = 61%  Analysis Date = 12/16/13 
 Pct Recovery = 61%  Analysis Date = 12/13/13 
 Pct Recovery = 61%  Analysis Date = 12/13/13 
 Pct Recovery = 61%  Analysis Date = 12/11/13 
 Pct Recovery = 61%  Analysis Date = 12/11/13 
 Pct Recovery = 61%  Analysis Date = 12/09/13 
 Pct Recovery = 61%  Analysis Date = 12/09/13 
 Pct Recovery = 61%  Analysis Date = 12/07/13 
 Pct Recovery = 61%  Analysis Date = 12/07/13 
 Pct Recovery = 61%  Analysis Date = 12/04/13 
 Pct Recovery = 61%  Analysis Date = 12/04/13 
 Pct Recovery = 61%  Analysis Date = 12/02/13 
 Pct Recovery = 61%  Analysis Date = 12/02/13 
 Pct Recovery = 61%  Analysis Date = 11/30/13 
 Pct Recovery = 61%  Analysis Date = 11/30/13 
 Pct Recovery = 61%  Analysis Date = 11/27/13 
 Pct Recovery = 61%  Analysis Date = 11/27/13 
 Pct Recovery = 61%  Analysis Date = 11/25/13 
 Pct Recovery = 61%  Analysis Date = 11/25/13 
 Pct Recovery = 61%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 60%  Analysis Date = 11/16/13 
 Pct Recovery = 60%  Analysis Date = 11/13/13 
 Pct Recovery = 60%  Analysis Date = 11/13/13 
 Pct Recovery = 60%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/07/13 
 Pct Recovery = 60%  Analysis Date = 11/07/13 
 Pct Recovery = 60%  Analysis Date = 11/04/13 
 Pct Recovery = 60%  Analysis Date = 11/04/13 
 Pct Recovery = 60%  Analysis Date = 11/02/13 
 Pct Recovery = 60%  Analysis Date = 11/02/13 
 Pct Recovery = 60%  Analysis Date = 10/31/13 
 Pct Recovery = 60%  Analysis Date = 10/31/13 
 Pct Recovery = 60%  Analysis Date = 10/28/13 
 Pct Recovery = 60%  Analysis Date = 10/28/13 
 Pct Recovery = 60%  Analysis Date = 10/26/13 
 Pct Recovery = 60%  Analysis Date = 10/26/13 
 Pct Recovery = 60%  Analysis Date = 10/24/13 
 Pct Recovery = 60%  Analysis Date = 10/24/13 
 Pct Recovery = 60%  Analysis Date = 10/21/13 
 Pct Recovery = 60%  Analysis Date = 10/21/13 
 Pct Recovery = 60%  Analysis Date = 10/19/13 
 Pct Recovery = 60%  Analysis Date = 10/19/13 
 Pct Recovery = 60%  Analysis Date = 10/17/13 
 Pct Recovery = 60%  Analysis Date = 10/17/13 
 Pct Recovery = 60%  Analysis Date = 10/14/13 
 Pct Recovery = 60%  Analysis Date = 10/14/13 
 Pct Recovery = 60%  Analysis Date = 10/12/13 
 Pct Recovery = 59%  Analysis Date = 10/12/13 
 Pct Recovery = 59%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 09/28/13 
 Pct Recovery = 59%  Analysis Date = 09/28/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/21/13 
 Pct Recovery = 59%  Analysis Date = 09/21/13 
 Pct Recovery = 59%  Analysis Date = 09/19/13 
 Pct Recovery = 59%  Analysis Date = 09/19/13 
 Pct Recovery = 59%  Analysis Date = 09/17/13 
 Pct Recovery = 59%  Analysis Date = 09/17/13 
 Pct Recovery = 59%  Analysis Date = 09/14/13 
 Pct Recovery = 59%  Analysis Date = 09/14/13 
 Pct Recovery = 59%  Analysis Date = 09/12/13 
 Pct Recovery = 59%  Analysis Date = 09/12/13 
 Pct Recovery = 59%  Analysis Date = 09/10/13 
 Pct Recovery = 59%  Analysis Date = 09/10/13 
 Pct Recovery = 59%  Analysis Date = 09/07/13 
 Pct Recovery = 58%  Analysis Date = 09/07/13 
 Pct Recovery = 58%  Analysis Date = 09/05/13 
 Pct Recovery = 58%  Analysis Date = 09/05/13 
 Pct Recovery = 58%  Analysis Date = 09/03/13 
 Pct Recovery = 58%  Analysis Date = 09/03/13 
 Pct Recovery = 58%  Analysis Date = 09/01/13 
 Pct Recovery = 58%  Analysis Date = 09/01/13 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 Pct Recovery = 58%  Analysis Date = 08/27/13 
 Pct Recovery = 58%  Analysis Date = 08/27/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/22/13 
 Pct Recovery = 58%  Analysis Date = 08/22/13 
 Pct Recovery = 58%  Analysis Date = 08/20/13 
 Pct Recovery = 58%  Analysis Date = 08/20/13 
 Pct Recovery = 58%  Analysis Date = 08/18/13 
 Pct Recovery = 58%  Analysis Date = 08/18/13 
 Pct Recovery = 58%  Analysis Date = 08/15/13 
 Pct Recovery = 58%  Analysis Date = 08/15/13 
 Pct Recovery = 58%  Analysis Date = 08/13/13 
 Pct Recovery = 58%  Analysis Date = 08/13/13 
 Pct Recovery = 58%  Analysis Date = 08/11/13 
 Pct Recovery = 58%  Analysis Date = 08/11/13 
 Pct Recovery = 58%  Analysis Date = 08/08/13 
 Pct Recovery = 58%  Analysis Date = 08/08/13 
 Pct Recovery = 58%  Analysis Date = 08/06/13 
 Pct Recovery = 58%  Analysis Date = 08/06/13 
 Pct Recovery = 58%  Analysis Date = 08/04/13 
 Pct Recovery = 58%  Analysis Date = 08/04/13 
 Pct Recovery = 58%  Analysis Date = 08/02/13 
 Pct Recovery = 58%  Analysis Date = 08/02/13 
 Pct Recovery = 58%  Analysis Date = 07/30/13 
 Pct Recovery = 58%  Analysis Date = 07/30/13 
 Pct Recovery = 58%  Analysis Date = 07/28/13 
 Pct Recovery = 58%  Analysis Date = 07/28/13 
 Pct Recovery = 58%  Analysis Date = 07/26/13 
 Pct Recovery = 58%  Analysis Date = 07/26/13 
 Pct Recovery = 58%  Analysis Date = 07/23/13 
 Pct Recovery = 58%  Analysis Date = 07/23/13 
 Pct Recovery = 58%  Analysis Date = 07/21/13 
 Pct Recovery = 58%  Analysis Date = 07/21/13 
 Pct Recovery = 58%  Analysis Date = 07/19/13 
 Pct Recovery = 58%  Analysis Date = 07/19/13 
 Pct Recovery = 58%  Analysis Date = 07/16/13 
 Pct Recovery = 58%  Analysis Date = 07/16/13 
 Pct Recovery = 58%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/09/13 
 Pct Recovery = 59%  Analysis Date = 07/09/13 
 Pct Recovery = 59%  Analysis Date = 07/07/13 
 Pct Recovery = 59%  Analysis Date = 07/07/13 
 Pct Recovery = 59%  Analysis Date = 07/05/13 
 Pct Recovery = 59%  Analysis Date = 07/05/13 
 Pct Recovery = 59%  Analysis Date = 07/02/13 
 Pct Recovery = 59%  Analysis Date = 07/02/13 
 Pct Recovery = 59%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/26/13 
 Pct Recovery = 59%  Analysis Date = 06/26/13 
 Pct Recovery = 59%  Analysis Date = 06/23/13 
 Pct Recovery = 59%  Analysis Date = 06/23/13 
 Pct Recovery = 59%  Analysis Date = 06/21/13 
 Pct Recovery = 59%  Analysis Date = 06/21/13 
 Pct Recovery = 59%  Analysis Date = 06/19/13 
 Pct Recovery = 59%  Analysis Date = 06/19/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/14/13 
 Pct Recovery = 60%  Analysis Date = 06/14/13 
 Pct Recovery = 60%  Analysis Date = 06/12/13 
 Pct Recovery = 60%  Analysis Date = 06/12/13 
 Pct Recovery = 60%  Analysis Date = 06/09/13 
 Pct Recovery = 60%  Analysis Date = 06/09/13 
 Pct Recovery = 60%  Analysis Date = 06/07/13 
 Pct Recovery = 60%  Analysis Date = 06/07/13 
 Pct Recovery = 60%  Analysis Date = 06/05/13 
 Pct Recovery = 60%  Analysis Date = 06/05/13 
 Pct Recovery = 60%  Analysis Date = 06/02/13 
 Pct Recovery = 60%  Analysis Date = 06/02/13 
 Pct Recovery = 60%  Analysis Date = 05/31/13 
 Pct Recovery = 60%  Analysis Date = 05/31/13 
 Pct Recovery = 60%  Analysis Date = 05/29/13 
 Pct Recovery = 60%  Analysis Date = 05/29/13 
 Pct Recovery = 60%  Analysis Date = 05/27/13 
 Pct Recovery = 60%  Analysis Date = 05/27/13 
 Pct Recovery = 60%  Analysis Date = 05/24/13 
 Pct Recovery = 60%  Analysis Date = 05/24/13 
 Pct Recovery = 60%  Analysis Date = 05/22/13 
 Pct Recovery = 60%  Analysis Date = 05/22/13 
 Pct Recovery = 60%  Analysis Date = 05/20/13 
 Pct Recovery = 60%  Analysis Date = 05/20/13 
 Pct Recovery = 60%  Analysis Date = 05/17/13 
 Pct Recovery = 60%  Analysis Date = 05/17/13 
 Pct Recovery = 60%  Analysis Date = 05/15/13 
 Pct Recovery = 61%  Analysis Date = 05/15/13 
 Pct Recovery = 61%  Analysis Date = 05/13/13 
 Pct Recovery = 61%  Analysis Date = 05/13/13 
 Pct Recovery = 61%  Analysis Date = 05/10/13 
 Pct Recovery = 61%  Analysis Date = 05/10/13 
 Pct Recovery = 61%  Analysis Date = 05/08/13 
 Pct Recovery = 61%  Analysis Date = 05/08/13 
 Pct Recovery = 61%  Analysis Date = 05/06/13 
 Pct Recovery = 61%  Analysis Date = 05/06/13 
 Pct Recovery = 61%  Analysis Date = 05/03/13 
 Pct Recovery = 61%  Analysis Date = 05/03/13 
 Pct Recovery = 61%  Analysis Date = 05/01/13 
 Pct Recovery = 61%  Analysis Date = 05/01/13 
 Pct Recovery = 61%  Analysis Date = 04/29/13 
 Pct Recovery = 61%  Analysis Date = 04/29/13 
 Pct Recovery = 61%  Analysis Date = 04/26/13 
 Pct Recovery = 61%  Analysis Date = 04/26/13 
 Pct Recovery = 61%  Analysis Date = 04/24/13 
 Pct Recovery = 62%  Analysis Date = 04/24/13 
 Pct Recovery = 62%  Analysis Date = 04/22/13 
 Pct Recovery = 62%  Analysis Date = 04/22/13 
 Pct Recovery = 62%  Analysis Date = 04/20/13 
 Pct Recovery = 62%  Analysis Date = 04/20/13 
 Pct Recovery = 62%  Analysis Date = 04/17/13 
 Pct Recovery = 62%  Analysis Date = 04/17/13 
 Pct Recovery = 62%  Analysis Date = 04/15/13 
 Pct Recovery = 62%  Analysis Date = 04/15/13 
 Pct Recovery = 62%  Analysis Date = 04/13/13 
 Pct Recovery = 62%  Analysis Date = 04/13/13 
 Pct Recovery = 62%  Analysis Date = 04/10/13 
 Pct Recovery = 62%  Analysis Date = 04/10/13 
 Pct Recovery = 62%  Analysis Date = 04/08/13 
 Pct Recovery = 63%  Analysis Date = 04/08/13 
 Pct Recovery = 63%  Analysis Date = 04/06/13 
 Pct Recovery = 63%  Analysis Date = 04/06/13 
 Pct Recovery = 63%  Analysis Date = 04/03/13 
 Pct Recovery = 63%  Analysis Date = 04/03/13 
 Pct Recovery = 63%  Analysis Date = 04/01/13 
 Pct Recovery = 63%  Analysis Date = 04/01/13 
 Pct Recovery = 63%  Analysis Date = 03/30/13 
 Pct Recovery = 63%  Analysis Date = 03/30/13 
 Pct Recovery = 63%  Analysis Date = 03/27/13 
 Pct Recovery = 63%  Analysis Date = 03/27/13 
 Pct Recovery = 63%  Analysis Date = 03/25/13 
 Pct Recovery = 64%  Analysis Date = 03/25/13 
 Pct Recovery = 64%  Analysis Date = 03/23/13 
 Pct Recovery = 64%  Analysis Date = 03/23/13 
 Pct Recovery = 64%  Analysis Date = 03/21/13 
 Pct Recovery = 64%  Analysis Date = 03/21/13 
 Pct Recovery = 64%  Analysis Date = 03/18/13 
 Pct Recovery = 64%  Analysis Date = 03/18/13 
 Pct Recovery = 64%  Analysis Date = 03/16/13 
 Pct Recovery = 65%  Analysis Date = 03/16/13 
 Pct Recovery = 65%  Analysis Date = 03/14/13 
 Pct Recovery = 65%  Analysis Date = 03/14/13 
 Pct Recovery = 65%  Analysis Date = 03/11/13 
 Pct Recovery = 65%  Analysis Date = 03/11/13 
 Pct Recovery = 65%  Analysis Date = 03/09/13 
 Pct Recovery = 65%  Analysis Date = 03/09/13 
 Pct Recovery = 65%  Analysis Date = 03/07/13 
 Pct Recovery = 66%  Analysis Date = 03/07/13 
 Pct Recovery = 66%  Analysis Date = 03/04/13 
 Pct Recovery = 66%  Analysis Date = 03/04/13 
 Pct Recovery = 66%  Analysis Date = 03/02/13 
 Pct Recovery = 66%  Analysis Date = 03/02/13 
 Pct Recovery = 66%  Analysis Date = 02/28/13 
 Pct Recovery = 66%  Analysis Date = 02/28/13 
 Pct Recovery = 66%  Analysis Date = 02/25/13 
 Pct Recovery = 66%  Analysis Date = 02/25/13 
 Pct Recovery = 66%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/21/13 
 Pct Recovery = 67%  Analysis Date = 02/21/13 
 Pct Recovery = 67%  Analysis Date = 02/18/13 
 Pct Recovery = 67%  Analysis Date = 02/18/13 
 Pct Recovery = 67%  Analysis Date = 02/16/13 
 Pct Recovery = 67%  Analysis Date = 02/16/13 
 Pct Recovery = 67%  Analysis Date = 02/14/13 
 Pct Recovery = 68%  Analysis Date = 02/14/13 
 Pct Recovery = 68%  Analysis Date = 02/12/13 
 Pct Recovery = 68%  Analysis Date = 02/12/13 
 Pct Recovery = 68%  Analysis Date = 02/09/13 
 Pct Recovery = 68%  Analysis Date = 02/09/13 
 Pct Recovery = 68%  Analysis Date = 02/07/13 
 Pct Recovery = 68%  Analysis Date = 02/07/13 
 Pct Recovery = 68%  Analysis Date = 02/05/13 
 Pct Recovery = 69%  Analysis Date = 02/05/13 
 Pct Recovery = 69%  Analysis Date = 02/02/13 
 Pct Recovery = 69%  Analysis Date = 02/02/13 
 Pct Recovery = 69%  Analysis Date = 01/31/13 
 Pct Recovery = 69%  Analysis Date = 01/31/13 
 Pct Recovery = 69%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/26/13 
 Pct Recovery = 70%  Analysis Date = 01/26/13 
 Pct Recovery = 70%  Analysis Date = 01/24/13 
 Pct Recovery = 70%  Analysis Date = 01/24/13 
 Pct Recovery = 70%  Analysis Date = 01/22/13 
 Pct Recovery = 70%  Analysis Date = 01/22/13 
 Pct Recovery = 70%  Analysis Date = 01/19/13 
 Pct Recovery = 70%  Analysis Date = 01/19/13 
 Pct Recovery = 70%  Analysis Date = 01/17/13 
 Pct Recovery = 71%  Analysis Date = 01/17/13 
 Pct Recovery = 71%  Analysis Date = 01/15/13 
 Pct Recovery = 71%  Analysis Date = 01/15/13 
 Pct Recovery = 71%  Analysis Date = 01/13/13 
 Pct Recovery = 71%  Analysis Date = 01/13/13 
 Pct Recovery = 71%  Analysis Date = 01/10/13 
 Pct Recovery = 71%  Analysis Date = 01/10/13 
 Pct Recovery = 71%  Analysis Date = 01/08/13 
 Pct Recovery = 72%  Analysis Date = 01/08/13 
 Pct Recovery = 72%  Analysis Date = 01/06/13 
 Pct Recovery = 72%  Analysis Date = 01/06/13 
 Pct Recovery = 72%  Analysis Date = 01/03/13 
 Pct Recovery = 72%  Analysis Date = 01/03/13 
 Pct Recovery = 72%  Analysis Date = 01/01/13 
 Pct Recovery = 72%  Analysis Date = 01/01/13 
 Pct Recovery = 72%  Analysis Date = 12/30/12 
 Pct Recovery = 73%  Analysis Date = 12/30/12 
 Pct Recovery = 73%  Analysis Date = 12/27/12 
 Pct Recovery = 73%  Analysis Date = 12/27/12 
 Pct Recovery = 73%  Analysis Date = 12/25/12 
 Pct Recovery = 73%  Analysis Date = 12/25/12 
 Pct Recovery = 73%  Analysis Date = 12/23/12 
 Pct Recovery = 73%  Analysis Date = 12/23/12 
 Pct Recovery = 73%  Analysis Date = 12/20/12 
 Pct Recovery = 74%  Analysis Date = 12/20/12 
 Pct Recovery = 74%  Analysis Date = 12/18/12 
 Pct Recovery = 74%  Analysis Date = 12/18/12 
 Pct Recovery = 74%  Analysis Date = 12/16/12 
 Pct Recovery = 74%  Analysis Date = 12/16/12 
 Pct Recovery = 74%  Analysis Date = 12/14/12 
 Pct Recovery = 74%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ABACAVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 61% 8% 62% 7%
Total 14 61% 8% 62% 7%

Sample Statistics
ABACAVIR

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
ACETAMINOPHEN
METHOD: LC9017 , TESTIDCODE: 67436LCM56

 Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 295%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 82%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 83%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 79%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 119%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 82%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 54%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 72%  Analysis Date = 03/21/14 
 Pct Recovery = 147%  Analysis Date = 03/18/14 
 Pct Recovery = 146%  Analysis Date = 03/18/14 
 Pct Recovery = 146%  Analysis Date = 03/16/14 
 Pct Recovery = 145%  Analysis Date = 03/16/14 
 Pct Recovery = 145%  Analysis Date = 03/14/14 
 Pct Recovery = 144%  Analysis Date = 03/14/14 
 Pct Recovery = 144%  Analysis Date = 03/11/14 
 Pct Recovery = 142%  Analysis Date = 03/11/14 
 Pct Recovery = 142%  Analysis Date = 03/09/14 
 Pct Recovery = 141%  Analysis Date = 03/09/14 
 Pct Recovery = 141%  Analysis Date = 03/07/14 
 Pct Recovery = 140%  Analysis Date = 03/07/14 
 Pct Recovery = 140%  Analysis Date = 03/04/14 
 Pct Recovery = 139%  Analysis Date = 03/04/14 
 Pct Recovery = 139%  Analysis Date = 03/02/14 
 Pct Recovery = 137%  Analysis Date = 03/02/14 
 Pct Recovery = 137%  Analysis Date = 02/28/14 
 Pct Recovery = 136%  Analysis Date = 02/28/14 
 Pct Recovery = 136%  Analysis Date = 02/25/14 
 Pct Recovery = 135%  Analysis Date = 02/25/14 
 Pct Recovery = 135%  Analysis Date = 02/23/14 
 Pct Recovery = 134%  Analysis Date = 02/23/14 
 Pct Recovery = 134%  Analysis Date = 02/21/14 
 Pct Recovery = 132%  Analysis Date = 02/21/14 
 Pct Recovery = 132%  Analysis Date = 02/18/14 
 Pct Recovery = 131%  Analysis Date = 02/18/14 
 Pct Recovery = 131%  Analysis Date = 02/16/14 
 Pct Recovery = 130%  Analysis Date = 02/16/14 
 Pct Recovery = 130%  Analysis Date = 02/14/14 
 Pct Recovery = 129%  Analysis Date = 02/14/14 
 Pct Recovery = 129%  Analysis Date = 02/12/14 
 Pct Recovery = 128%  Analysis Date = 02/12/14 
 Pct Recovery = 128%  Analysis Date = 02/09/14 
 Pct Recovery = 127%  Analysis Date = 02/09/14 
 Pct Recovery = 127%  Analysis Date = 02/07/14 
 Pct Recovery = 126%  Analysis Date = 02/07/14 
 Pct Recovery = 126%  Analysis Date = 02/05/14 
 Pct Recovery = 125%  Analysis Date = 02/05/14 
 Pct Recovery = 125%  Analysis Date = 02/02/14 
 Pct Recovery = 124%  Analysis Date = 02/02/14 
 Pct Recovery = 124%  Analysis Date = 01/31/14 
 Pct Recovery = 123%  Analysis Date = 01/31/14 
 Pct Recovery = 123%  Analysis Date = 01/29/14 
 Pct Recovery = 122%  Analysis Date = 01/29/14 
 Pct Recovery = 122%  Analysis Date = 01/26/14 
 Pct Recovery = 121%  Analysis Date = 01/26/14 
 Pct Recovery = 121%  Analysis Date = 01/24/14 
 Pct Recovery = 120%  Analysis Date = 01/24/14 
 Pct Recovery = 120%  Analysis Date = 01/22/14 
 Pct Recovery = 119%  Analysis Date = 01/22/14 
 Pct Recovery = 119%  Analysis Date = 01/19/14 
 Pct Recovery = 118%  Analysis Date = 01/19/14 
 Pct Recovery = 118%  Analysis Date = 01/17/14 
 Pct Recovery = 117%  Analysis Date = 01/17/14 
 Pct Recovery = 117%  Analysis Date = 01/15/14 
 Pct Recovery = 117%  Analysis Date = 01/15/14 
 Pct Recovery = 117%  Analysis Date = 01/13/14 
 Pct Recovery = 116%  Analysis Date = 01/13/14 
 Pct Recovery = 116%  Analysis Date = 01/10/14 
 Pct Recovery = 116%  Analysis Date = 01/10/14 
 Pct Recovery = 116%  Analysis Date = 01/08/14 
 Pct Recovery = 116%  Analysis Date = 01/08/14 
 Pct Recovery = 116%  Analysis Date = 01/06/14 
 Pct Recovery = 116%  Analysis Date = 01/06/14 
 Pct Recovery = 116%  Analysis Date = 01/03/14 
 Pct Recovery = 116%  Analysis Date = 01/03/14 
 Pct Recovery = 116%  Analysis Date = 01/01/14 
 Pct Recovery = 115%  Analysis Date = 01/01/14 
 Pct Recovery = 115%  Analysis Date = 12/30/13 
 Pct Recovery = 115%  Analysis Date = 12/30/13 
 Pct Recovery = 115%  Analysis Date = 12/27/13 
 Pct Recovery = 115%  Analysis Date = 12/27/13 
 Pct Recovery = 115%  Analysis Date = 12/25/13 
 Pct Recovery = 115%  Analysis Date = 12/25/13 
 Pct Recovery = 115%  Analysis Date = 12/23/13 
 Pct Recovery = 115%  Analysis Date = 12/23/13 
 Pct Recovery = 115%  Analysis Date = 12/20/13 
 Pct Recovery = 115%  Analysis Date = 12/20/13 
 Pct Recovery = 115%  Analysis Date = 12/18/13 
 Pct Recovery = 114%  Analysis Date = 12/18/13 
 Pct Recovery = 114%  Analysis Date = 12/16/13 
 Pct Recovery = 114%  Analysis Date = 12/16/13 
 Pct Recovery = 114%  Analysis Date = 12/13/13 
 Pct Recovery = 114%  Analysis Date = 12/13/13 
 Pct Recovery = 114%  Analysis Date = 12/11/13 
 Pct Recovery = 114%  Analysis Date = 12/11/13 
 Pct Recovery = 114%  Analysis Date = 12/09/13 
 Pct Recovery = 114%  Analysis Date = 12/09/13 
 Pct Recovery = 114%  Analysis Date = 12/07/13 
 Pct Recovery = 114%  Analysis Date = 12/07/13 
 Pct Recovery = 114%  Analysis Date = 12/04/13 
 Pct Recovery = 113%  Analysis Date = 12/04/13 
 Pct Recovery = 113%  Analysis Date = 12/02/13 
 Pct Recovery = 113%  Analysis Date = 12/02/13 
 Pct Recovery = 113%  Analysis Date = 11/30/13 
 Pct Recovery = 113%  Analysis Date = 11/30/13 
 Pct Recovery = 113%  Analysis Date = 11/27/13 
 Pct Recovery = 113%  Analysis Date = 11/27/13 
 Pct Recovery = 113%  Analysis Date = 11/25/13 
 Pct Recovery = 113%  Analysis Date = 11/25/13 
 Pct Recovery = 113%  Analysis Date = 11/23/13 
 Pct Recovery = 113%  Analysis Date = 11/23/13 
 Pct Recovery = 113%  Analysis Date = 11/20/13 
 Pct Recovery = 112%  Analysis Date = 11/20/13 
 Pct Recovery = 112%  Analysis Date = 11/18/13 
 Pct Recovery = 112%  Analysis Date = 11/18/13 
 Pct Recovery = 112%  Analysis Date = 11/16/13 
 Pct Recovery = 112%  Analysis Date = 11/16/13 
 Pct Recovery = 112%  Analysis Date = 11/13/13 
 Pct Recovery = 112%  Analysis Date = 11/13/13 
 Pct Recovery = 112%  Analysis Date = 11/11/13 
 Pct Recovery = 112%  Analysis Date = 11/11/13 
 Pct Recovery = 112%  Analysis Date = 11/09/13 
 Pct Recovery = 112%  Analysis Date = 11/09/13 
 Pct Recovery = 112%  Analysis Date = 11/07/13 
 Pct Recovery = 111%  Analysis Date = 11/07/13 
 Pct Recovery = 111%  Analysis Date = 11/04/13 
 Pct Recovery = 111%  Analysis Date = 11/04/13 
 Pct Recovery = 111%  Analysis Date = 11/02/13 
 Pct Recovery = 111%  Analysis Date = 11/02/13 
 Pct Recovery = 111%  Analysis Date = 10/31/13 
 Pct Recovery = 111%  Analysis Date = 10/31/13 
 Pct Recovery = 111%  Analysis Date = 10/28/13 
 Pct Recovery = 111%  Analysis Date = 10/28/13 
 Pct Recovery = 111%  Analysis Date = 10/26/13 
 Pct Recovery = 110%  Analysis Date = 10/26/13 
 Pct Recovery = 110%  Analysis Date = 10/24/13 
 Pct Recovery = 110%  Analysis Date = 10/24/13 
 Pct Recovery = 110%  Analysis Date = 10/21/13 
 Pct Recovery = 110%  Analysis Date = 10/21/13 
 Pct Recovery = 110%  Analysis Date = 10/19/13 
 Pct Recovery = 110%  Analysis Date = 10/19/13 
 Pct Recovery = 110%  Analysis Date = 10/17/13 
 Pct Recovery = 110%  Analysis Date = 10/17/13 
 Pct Recovery = 110%  Analysis Date = 10/14/13 
 Pct Recovery = 110%  Analysis Date = 10/14/13 
 Pct Recovery = 110%  Analysis Date = 10/12/13 
 Pct Recovery = 109%  Analysis Date = 10/12/13 
 Pct Recovery = 109%  Analysis Date = 10/10/13 
 Pct Recovery = 109%  Analysis Date = 10/10/13 
 Pct Recovery = 109%  Analysis Date = 10/07/13 
 Pct Recovery = 109%  Analysis Date = 10/07/13 
 Pct Recovery = 109%  Analysis Date = 10/05/13 
 Pct Recovery = 109%  Analysis Date = 10/05/13 
 Pct Recovery = 109%  Analysis Date = 10/03/13 
 Pct Recovery = 109%  Analysis Date = 10/03/13 
 Pct Recovery = 109%  Analysis Date = 10/01/13 
 Pct Recovery = 109%  Analysis Date = 10/01/13 
 Pct Recovery = 109%  Analysis Date = 09/28/13 
 Pct Recovery = 108%  Analysis Date = 09/28/13 
 Pct Recovery = 108%  Analysis Date = 09/26/13 
 Pct Recovery = 108%  Analysis Date = 09/26/13 
 Pct Recovery = 108%  Analysis Date = 09/24/13 
 Pct Recovery = 108%  Analysis Date = 09/24/13 
 Pct Recovery = 108%  Analysis Date = 09/21/13 
 Pct Recovery = 108%  Analysis Date = 09/21/13 
 Pct Recovery = 108%  Analysis Date = 09/19/13 
 Pct Recovery = 108%  Analysis Date = 09/19/13 
 Pct Recovery = 108%  Analysis Date = 09/17/13 
 Pct Recovery = 108%  Analysis Date = 09/17/13 
 Pct Recovery = 108%  Analysis Date = 09/14/13 
 Pct Recovery = 107%  Analysis Date = 09/14/13 
 Pct Recovery = 107%  Analysis Date = 09/12/13 
 Pct Recovery = 107%  Analysis Date = 09/12/13 
 Pct Recovery = 107%  Analysis Date = 09/10/13 
 Pct Recovery = 107%  Analysis Date = 09/10/13 
 Pct Recovery = 107%  Analysis Date = 09/07/13 
 Pct Recovery = 107%  Analysis Date = 09/07/13 
 Pct Recovery = 107%  Analysis Date = 09/05/13 
 Pct Recovery = 107%  Analysis Date = 09/05/13 
 Pct Recovery = 107%  Analysis Date = 09/03/13 
 Pct Recovery = 106%  Analysis Date = 09/03/13 
 Pct Recovery = 106%  Analysis Date = 09/01/13 
 Pct Recovery = 106%  Analysis Date = 09/01/13 
 Pct Recovery = 106%  Analysis Date = 08/29/13 
 Pct Recovery = 106%  Analysis Date = 08/29/13 
 Pct Recovery = 106%  Analysis Date = 08/27/13 
 Pct Recovery = 106%  Analysis Date = 08/27/13 
 Pct Recovery = 106%  Analysis Date = 08/25/13 
 Pct Recovery = 105%  Analysis Date = 08/25/13 
 Pct Recovery = 105%  Analysis Date = 08/22/13 
 Pct Recovery = 105%  Analysis Date = 08/22/13 
 Pct Recovery = 105%  Analysis Date = 08/20/13 
 Pct Recovery = 104%  Analysis Date = 08/20/13 
 Pct Recovery = 104%  Analysis Date = 08/18/13 
 Pct Recovery = 104%  Analysis Date = 08/18/13 
 Pct Recovery = 104%  Analysis Date = 08/15/13 
 Pct Recovery = 103%  Analysis Date = 08/15/13 
 Pct Recovery = 103%  Analysis Date = 08/13/13 
 Pct Recovery = 103%  Analysis Date = 08/13/13 
 Pct Recovery = 103%  Analysis Date = 08/11/13 
 Pct Recovery = 103%  Analysis Date = 08/11/13 
 Pct Recovery = 103%  Analysis Date = 08/08/13 
 Pct Recovery = 102%  Analysis Date = 08/08/13 
 Pct Recovery = 102%  Analysis Date = 08/06/13 
 Pct Recovery = 102%  Analysis Date = 08/06/13 
 Pct Recovery = 102%  Analysis Date = 08/04/13 
 Pct Recovery = 101%  Analysis Date = 08/04/13 
 Pct Recovery = 101%  Analysis Date = 08/02/13 
 Pct Recovery = 101%  Analysis Date = 08/02/13 
 Pct Recovery = 101%  Analysis Date = 07/30/13 
 Pct Recovery = 100%  Analysis Date = 07/30/13 
 Pct Recovery = 100%  Analysis Date = 07/28/13 
 Pct Recovery = 100%  Analysis Date = 07/28/13 
 Pct Recovery = 100%  Analysis Date = 07/26/13 
 Pct Recovery = 99%  Analysis Date = 07/26/13 
 Pct Recovery = 99%  Analysis Date = 07/23/13 
 Pct Recovery = 99%  Analysis Date = 07/23/13 
 Pct Recovery = 99%  Analysis Date = 07/21/13 
 Pct Recovery = 98%  Analysis Date = 07/21/13 
 Pct Recovery = 98%  Analysis Date = 07/19/13 
 Pct Recovery = 98%  Analysis Date = 07/19/13 
 Pct Recovery = 98%  Analysis Date = 07/16/13 
 Pct Recovery = 97%  Analysis Date = 07/16/13 
 Pct Recovery = 97%  Analysis Date = 07/14/13 
 Pct Recovery = 97%  Analysis Date = 07/14/13 
 Pct Recovery = 97%  Analysis Date = 07/12/13 
 Pct Recovery = 97%  Analysis Date = 07/12/13 
 Pct Recovery = 97%  Analysis Date = 07/09/13 
 Pct Recovery = 96%  Analysis Date = 07/09/13 
 Pct Recovery = 96%  Analysis Date = 07/07/13 
 Pct Recovery = 96%  Analysis Date = 07/07/13 
 Pct Recovery = 96%  Analysis Date = 07/05/13 
 Pct Recovery = 95%  Analysis Date = 07/05/13 
 Pct Recovery = 95%  Analysis Date = 07/02/13 
 Pct Recovery = 95%  Analysis Date = 07/02/13 
 Pct Recovery = 95%  Analysis Date = 06/30/13 
 Pct Recovery = 94%  Analysis Date = 06/30/13 
 Pct Recovery = 94%  Analysis Date = 06/28/13 
 Pct Recovery = 94%  Analysis Date = 06/28/13 
 Pct Recovery = 94%  Analysis Date = 06/26/13 
 Pct Recovery = 93%  Analysis Date = 06/26/13 
 Pct Recovery = 93%  Analysis Date = 06/23/13 
 Pct Recovery = 93%  Analysis Date = 06/23/13 
 Pct Recovery = 93%  Analysis Date = 06/21/13 
 Pct Recovery = 92%  Analysis Date = 06/21/13 
 Pct Recovery = 92%  Analysis Date = 06/19/13 
 Pct Recovery = 92%  Analysis Date = 06/19/13 
 Pct Recovery = 92%  Analysis Date = 06/16/13 
 Pct Recovery = 91%  Analysis Date = 06/16/13 
 Pct Recovery = 91%  Analysis Date = 06/14/13 
 Pct Recovery = 91%  Analysis Date = 06/14/13 
 Pct Recovery = 91%  Analysis Date = 06/12/13 
 Pct Recovery = 91%  Analysis Date = 06/12/13 
 Pct Recovery = 91%  Analysis Date = 06/09/13 
 Pct Recovery = 90%  Analysis Date = 06/09/13 
 Pct Recovery = 90%  Analysis Date = 06/07/13 
 Pct Recovery = 90%  Analysis Date = 06/07/13 
 Pct Recovery = 90%  Analysis Date = 06/05/13 
 Pct Recovery = 89%  Analysis Date = 06/05/13 
 Pct Recovery = 89%  Analysis Date = 06/02/13 
 Pct Recovery = 89%  Analysis Date = 06/02/13 
 Pct Recovery = 89%  Analysis Date = 05/31/13 
 Pct Recovery = 88%  Analysis Date = 05/31/13 
 Pct Recovery = 88%  Analysis Date = 05/29/13 
 Pct Recovery = 88%  Analysis Date = 05/29/13 
 Pct Recovery = 88%  Analysis Date = 05/27/13 
 Pct Recovery = 87%  Analysis Date = 05/27/13 
 Pct Recovery = 87%  Analysis Date = 05/24/13 
 Pct Recovery = 87%  Analysis Date = 05/24/13 
 Pct Recovery = 87%  Analysis Date = 05/22/13 
 Pct Recovery = 86%  Analysis Date = 05/22/13 
 Pct Recovery = 86%  Analysis Date = 05/20/13 
 Pct Recovery = 86%  Analysis Date = 05/20/13 
 Pct Recovery = 86%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/15/13 
 Pct Recovery = 85%  Analysis Date = 05/15/13 
 Pct Recovery = 85%  Analysis Date = 05/13/13 
 Pct Recovery = 85%  Analysis Date = 05/13/13 
 Pct Recovery = 85%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/08/13 
 Pct Recovery = 84%  Analysis Date = 05/08/13 
 Pct Recovery = 84%  Analysis Date = 05/06/13 
 Pct Recovery = 83%  Analysis Date = 05/06/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/01/13 
 Pct Recovery = 82%  Analysis Date = 05/01/13 
 Pct Recovery = 82%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/24/13 
 Pct Recovery = 82%  Analysis Date = 04/24/13 
 Pct Recovery = 82%  Analysis Date = 04/22/13 
 Pct Recovery = 82%  Analysis Date = 04/22/13 
 Pct Recovery = 82%  Analysis Date = 04/20/13 
 Pct Recovery = 82%  Analysis Date = 04/20/13 
 Pct Recovery = 82%  Analysis Date = 04/17/13 
 Pct Recovery = 82%  Analysis Date = 04/17/13 
 Pct Recovery = 82%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 82%  Analysis Date = 04/10/13 
 Pct Recovery = 82%  Analysis Date = 04/10/13 
 Pct Recovery = 82%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 81%  Analysis Date = 03/30/13 
 Pct Recovery = 81%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/25/13 
 Pct Recovery = 81%  Analysis Date = 03/25/13 
 Pct Recovery = 81%  Analysis Date = 03/23/13 
 Pct Recovery = 81%  Analysis Date = 03/23/13 
 Pct Recovery = 81%  Analysis Date = 03/21/13 
 Pct Recovery = 81%  Analysis Date = 03/21/13 
 Pct Recovery = 81%  Analysis Date = 03/18/13 
 Pct Recovery = 81%  Analysis Date = 03/18/13 
 Pct Recovery = 81%  Analysis Date = 03/16/13 
 Pct Recovery = 81%  Analysis Date = 03/16/13 
 Pct Recovery = 81%  Analysis Date = 03/14/13 
 Pct Recovery = 81%  Analysis Date = 03/14/13 
 Pct Recovery = 81%  Analysis Date = 03/11/13 
 Pct Recovery = 81%  Analysis Date = 03/11/13 
 Pct Recovery = 81%  Analysis Date = 03/09/13 
 Pct Recovery = 81%  Analysis Date = 03/09/13 
 Pct Recovery = 81%  Analysis Date = 03/07/13 
 Pct Recovery = 81%  Analysis Date = 03/07/13 
 Pct Recovery = 81%  Analysis Date = 03/04/13 
 Pct Recovery = 81%  Analysis Date = 03/04/13 
 Pct Recovery = 81%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 Pct Recovery = 81%  Analysis Date = 02/25/13 
 Pct Recovery = 81%  Analysis Date = 02/25/13 
 Pct Recovery = 81%  Analysis Date = 02/23/13 
 Pct Recovery = 81%  Analysis Date = 02/23/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/18/13 
 Pct Recovery = 81%  Analysis Date = 02/18/13 
 Pct Recovery = 81%  Analysis Date = 02/16/13 
 Pct Recovery = 81%  Analysis Date = 02/16/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/05/13 
 Pct Recovery = 81%  Analysis Date = 02/05/13 
 Pct Recovery = 81%  Analysis Date = 02/02/13 
 Pct Recovery = 81%  Analysis Date = 02/02/13 
 Pct Recovery = 81%  Analysis Date = 01/31/13 
 Pct Recovery = 81%  Analysis Date = 01/31/13 
 Pct Recovery = 81%  Analysis Date = 01/29/13 
 Pct Recovery = 81%  Analysis Date = 01/29/13 
 Pct Recovery = 81%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/01/13 
 Pct Recovery = 82%  Analysis Date = 01/01/13 
 Pct Recovery = 82%  Analysis Date = 12/30/12 
 Pct Recovery = 82%  Analysis Date = 12/30/12 
 Pct Recovery = 82%  Analysis Date = 12/27/12 
 Pct Recovery = 82%  Analysis Date = 12/27/12 
 Pct Recovery = 82%  Analysis Date = 12/25/12 
 Pct Recovery = 82%  Analysis Date = 12/25/12 
 Pct Recovery = 82%  Analysis Date = 12/23/12 
 Pct Recovery = 82%  Analysis Date = 12/23/12 
 Pct Recovery = 82%  Analysis Date = 12/20/12 
 Pct Recovery = 82%  Analysis Date = 12/20/12 
 Pct Recovery = 82%  Analysis Date = 12/18/12 
 Pct Recovery = 82%  Analysis Date = 12/18/12 
 Pct Recovery = 82%  Analysis Date = 12/16/12 
 Pct Recovery = 82%  Analysis Date = 12/16/12 
 Pct Recovery = 82%  Analysis Date = 12/14/12 
 Pct Recovery = 82%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETAMINOPHEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 101% 70% 80% 9%
Total 10 101% 70% 80% 9%

Sample Statistics
ACETAMINOPHEN

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
ACYCLOVIR
METHOD: LC9017 , TESTIDCODE: 67484LCM56

The SGPlot Procedure

Sample Statistics
ACYCLOVIR

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 13 42% 13 out of 31

OBSP Determination:
ALBUTEROL (SALBUTAMOL)
METHOD: LC9017 , TESTIDCODE: 67437LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 82%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 64%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 93%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 110%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 88%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 47%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 63%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 106%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 03/21/14 
 Pct Recovery = 106%  Analysis Date = 03/18/14 
 Pct Recovery = 105%  Analysis Date = 03/18/14 
 Pct Recovery = 105%  Analysis Date = 03/16/14 
 Pct Recovery = 104%  Analysis Date = 03/16/14 
 Pct Recovery = 104%  Analysis Date = 03/14/14 
 Pct Recovery = 103%  Analysis Date = 03/14/14 
 Pct Recovery = 103%  Analysis Date = 03/11/14 
 Pct Recovery = 102%  Analysis Date = 03/11/14 
 Pct Recovery = 102%  Analysis Date = 03/09/14 
 Pct Recovery = 101%  Analysis Date = 03/09/14 
 Pct Recovery = 101%  Analysis Date = 03/07/14 
 Pct Recovery = 100%  Analysis Date = 03/07/14 
 Pct Recovery = 100%  Analysis Date = 03/04/14 
 Pct Recovery = 100%  Analysis Date = 03/04/14 
 Pct Recovery = 100%  Analysis Date = 03/02/14 
 Pct Recovery = 99%  Analysis Date = 03/02/14 
 Pct Recovery = 99%  Analysis Date = 02/28/14 
 Pct Recovery = 98%  Analysis Date = 02/28/14 
 Pct Recovery = 98%  Analysis Date = 02/25/14 
 Pct Recovery = 97%  Analysis Date = 02/25/14 
 Pct Recovery = 97%  Analysis Date = 02/23/14 
 Pct Recovery = 96%  Analysis Date = 02/23/14 
 Pct Recovery = 96%  Analysis Date = 02/21/14 
 Pct Recovery = 95%  Analysis Date = 02/21/14 
 Pct Recovery = 95%  Analysis Date = 02/18/14 
 Pct Recovery = 94%  Analysis Date = 02/18/14 
 Pct Recovery = 94%  Analysis Date = 02/16/14 
 Pct Recovery = 94%  Analysis Date = 02/16/14 
 Pct Recovery = 94%  Analysis Date = 02/14/14 
 Pct Recovery = 93%  Analysis Date = 02/14/14 
 Pct Recovery = 93%  Analysis Date = 02/12/14 
 Pct Recovery = 92%  Analysis Date = 02/12/14 
 Pct Recovery = 92%  Analysis Date = 02/09/14 
 Pct Recovery = 91%  Analysis Date = 02/09/14 
 Pct Recovery = 91%  Analysis Date = 02/07/14 
 Pct Recovery = 90%  Analysis Date = 02/07/14 
 Pct Recovery = 90%  Analysis Date = 02/05/14 
 Pct Recovery = 90%  Analysis Date = 02/05/14 
 Pct Recovery = 90%  Analysis Date = 02/02/14 
 Pct Recovery = 89%  Analysis Date = 02/02/14 
 Pct Recovery = 89%  Analysis Date = 01/31/14 
 Pct Recovery = 88%  Analysis Date = 01/31/14 
 Pct Recovery = 88%  Analysis Date = 01/29/14 
 Pct Recovery = 87%  Analysis Date = 01/29/14 
 Pct Recovery = 87%  Analysis Date = 01/26/14 
 Pct Recovery = 86%  Analysis Date = 01/26/14 
 Pct Recovery = 86%  Analysis Date = 01/24/14 
 Pct Recovery = 86%  Analysis Date = 01/24/14 
 Pct Recovery = 86%  Analysis Date = 01/22/14 
 Pct Recovery = 85%  Analysis Date = 01/22/14 
 Pct Recovery = 85%  Analysis Date = 01/19/14 
 Pct Recovery = 84%  Analysis Date = 01/19/14 
 Pct Recovery = 84%  Analysis Date = 01/17/14 
 Pct Recovery = 83%  Analysis Date = 01/17/14 
 Pct Recovery = 83%  Analysis Date = 01/15/14 
 Pct Recovery = 83%  Analysis Date = 01/15/14 
 Pct Recovery = 83%  Analysis Date = 01/13/14 
 Pct Recovery = 82%  Analysis Date = 01/13/14 
 Pct Recovery = 82%  Analysis Date = 01/10/14 
 Pct Recovery = 81%  Analysis Date = 01/10/14 
 Pct Recovery = 81%  Analysis Date = 01/08/14 
 Pct Recovery = 81%  Analysis Date = 01/08/14 
 Pct Recovery = 81%  Analysis Date = 01/06/14 
 Pct Recovery = 80%  Analysis Date = 01/06/14 
 Pct Recovery = 80%  Analysis Date = 01/03/14 
 Pct Recovery = 79%  Analysis Date = 01/03/14 
 Pct Recovery = 79%  Analysis Date = 01/01/14 
 Pct Recovery = 79%  Analysis Date = 01/01/14 
 Pct Recovery = 79%  Analysis Date = 12/30/13 
 Pct Recovery = 78%  Analysis Date = 12/30/13 
 Pct Recovery = 78%  Analysis Date = 12/27/13 
 Pct Recovery = 78%  Analysis Date = 12/27/13 
 Pct Recovery = 78%  Analysis Date = 12/25/13 
 Pct Recovery = 77%  Analysis Date = 12/25/13 
 Pct Recovery = 77%  Analysis Date = 12/23/13 
 Pct Recovery = 76%  Analysis Date = 12/23/13 
 Pct Recovery = 76%  Analysis Date = 12/20/13 
 Pct Recovery = 76%  Analysis Date = 12/20/13 
 Pct Recovery = 76%  Analysis Date = 12/18/13 
 Pct Recovery = 75%  Analysis Date = 12/18/13 
 Pct Recovery = 75%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/13/13 
 Pct Recovery = 74%  Analysis Date = 12/13/13 
 Pct Recovery = 74%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 72%  Analysis Date = 12/07/13 
 Pct Recovery = 72%  Analysis Date = 12/04/13 
 Pct Recovery = 71%  Analysis Date = 12/04/13 
 Pct Recovery = 71%  Analysis Date = 12/02/13 
 Pct Recovery = 71%  Analysis Date = 12/02/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 70%  Analysis Date = 11/27/13 
 Pct Recovery = 70%  Analysis Date = 11/27/13 
 Pct Recovery = 70%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/20/13 
 Pct Recovery = 68%  Analysis Date = 11/20/13 
 Pct Recovery = 68%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/09/13 
 Pct Recovery = 67%  Analysis Date = 11/09/13 
 Pct Recovery = 67%  Analysis Date = 11/07/13 
 Pct Recovery = 66%  Analysis Date = 11/07/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/26/13 
 Pct Recovery = 65%  Analysis Date = 10/26/13 
 Pct Recovery = 65%  Analysis Date = 10/24/13 
 Pct Recovery = 65%  Analysis Date = 10/24/13 
 Pct Recovery = 65%  Analysis Date = 10/21/13 
 Pct Recovery = 65%  Analysis Date = 10/21/13 
 Pct Recovery = 65%  Analysis Date = 10/19/13 
 Pct Recovery = 65%  Analysis Date = 10/19/13 
 Pct Recovery = 65%  Analysis Date = 10/17/13 
 Pct Recovery = 65%  Analysis Date = 10/17/13 
 Pct Recovery = 65%  Analysis Date = 10/14/13 
 Pct Recovery = 64%  Analysis Date = 10/14/13 
 Pct Recovery = 64%  Analysis Date = 10/12/13 
 Pct Recovery = 64%  Analysis Date = 10/12/13 
 Pct Recovery = 64%  Analysis Date = 10/10/13 
 Pct Recovery = 64%  Analysis Date = 10/10/13 
 Pct Recovery = 64%  Analysis Date = 10/07/13 
 Pct Recovery = 64%  Analysis Date = 10/07/13 
 Pct Recovery = 64%  Analysis Date = 10/05/13 
 Pct Recovery = 64%  Analysis Date = 10/05/13 
 Pct Recovery = 64%  Analysis Date = 10/03/13 
 Pct Recovery = 64%  Analysis Date = 10/03/13 
 Pct Recovery = 64%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/19/13 
 Pct Recovery = 62%  Analysis Date = 09/19/13 
 Pct Recovery = 62%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/07/13 
 Pct Recovery = 61%  Analysis Date = 09/07/13 
 Pct Recovery = 61%  Analysis Date = 09/05/13 
 Pct Recovery = 61%  Analysis Date = 09/05/13 
 Pct Recovery = 61%  Analysis Date = 09/03/13 
 Pct Recovery = 61%  Analysis Date = 09/03/13 
 Pct Recovery = 61%  Analysis Date = 09/01/13 
 Pct Recovery = 61%  Analysis Date = 09/01/13 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 Pct Recovery = 61%  Analysis Date = 08/27/13 
 Pct Recovery = 61%  Analysis Date = 08/27/13 
 Pct Recovery = 61%  Analysis Date = 08/25/13 
 Pct Recovery = 61%  Analysis Date = 08/25/13 
 Pct Recovery = 61%  Analysis Date = 08/22/13 
 Pct Recovery = 61%  Analysis Date = 08/22/13 
 Pct Recovery = 61%  Analysis Date = 08/20/13 
 Pct Recovery = 61%  Analysis Date = 08/20/13 
 Pct Recovery = 61%  Analysis Date = 08/18/13 
 Pct Recovery = 61%  Analysis Date = 08/18/13 
 Pct Recovery = 61%  Analysis Date = 08/15/13 
 Pct Recovery = 61%  Analysis Date = 08/15/13 
 Pct Recovery = 61%  Analysis Date = 08/13/13 
 Pct Recovery = 61%  Analysis Date = 08/13/13 
 Pct Recovery = 61%  Analysis Date = 08/11/13 
 Pct Recovery = 61%  Analysis Date = 08/11/13 
 Pct Recovery = 61%  Analysis Date = 08/08/13 
 Pct Recovery = 61%  Analysis Date = 08/08/13 
 Pct Recovery = 61%  Analysis Date = 08/06/13 
 Pct Recovery = 61%  Analysis Date = 08/06/13 
 Pct Recovery = 61%  Analysis Date = 08/04/13 
 Pct Recovery = 62%  Analysis Date = 08/04/13 
 Pct Recovery = 62%  Analysis Date = 08/02/13 
 Pct Recovery = 62%  Analysis Date = 08/02/13 
 Pct Recovery = 62%  Analysis Date = 07/30/13 
 Pct Recovery = 62%  Analysis Date = 07/30/13 
 Pct Recovery = 62%  Analysis Date = 07/28/13 
 Pct Recovery = 62%  Analysis Date = 07/28/13 
 Pct Recovery = 62%  Analysis Date = 07/26/13 
 Pct Recovery = 62%  Analysis Date = 07/26/13 
 Pct Recovery = 62%  Analysis Date = 07/23/13 
 Pct Recovery = 62%  Analysis Date = 07/23/13 
 Pct Recovery = 62%  Analysis Date = 07/21/13 
 Pct Recovery = 62%  Analysis Date = 07/21/13 
 Pct Recovery = 62%  Analysis Date = 07/19/13 
 Pct Recovery = 62%  Analysis Date = 07/19/13 
 Pct Recovery = 62%  Analysis Date = 07/16/13 
 Pct Recovery = 62%  Analysis Date = 07/16/13 
 Pct Recovery = 62%  Analysis Date = 07/14/13 
 Pct Recovery = 62%  Analysis Date = 07/14/13 
 Pct Recovery = 62%  Analysis Date = 07/12/13 
 Pct Recovery = 62%  Analysis Date = 07/12/13 
 Pct Recovery = 62%  Analysis Date = 07/09/13 
 Pct Recovery = 62%  Analysis Date = 07/09/13 
 Pct Recovery = 62%  Analysis Date = 07/07/13 
 Pct Recovery = 63%  Analysis Date = 07/07/13 
 Pct Recovery = 63%  Analysis Date = 07/05/13 
 Pct Recovery = 63%  Analysis Date = 07/05/13 
 Pct Recovery = 63%  Analysis Date = 07/02/13 
 Pct Recovery = 63%  Analysis Date = 07/02/13 
 Pct Recovery = 63%  Analysis Date = 06/30/13 
 Pct Recovery = 63%  Analysis Date = 06/30/13 
 Pct Recovery = 63%  Analysis Date = 06/28/13 
 Pct Recovery = 63%  Analysis Date = 06/28/13 
 Pct Recovery = 63%  Analysis Date = 06/26/13 
 Pct Recovery = 63%  Analysis Date = 06/26/13 
 Pct Recovery = 63%  Analysis Date = 06/23/13 
 Pct Recovery = 63%  Analysis Date = 06/23/13 
 Pct Recovery = 63%  Analysis Date = 06/21/13 
 Pct Recovery = 63%  Analysis Date = 06/21/13 
 Pct Recovery = 63%  Analysis Date = 06/19/13 
 Pct Recovery = 63%  Analysis Date = 06/19/13 
 Pct Recovery = 63%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/12/13 
 Pct Recovery = 64%  Analysis Date = 06/12/13 
 Pct Recovery = 64%  Analysis Date = 06/09/13 
 Pct Recovery = 64%  Analysis Date = 06/09/13 
 Pct Recovery = 64%  Analysis Date = 06/07/13 
 Pct Recovery = 64%  Analysis Date = 06/07/13 
 Pct Recovery = 64%  Analysis Date = 06/05/13 
 Pct Recovery = 64%  Analysis Date = 06/05/13 
 Pct Recovery = 64%  Analysis Date = 06/02/13 
 Pct Recovery = 64%  Analysis Date = 06/02/13 
 Pct Recovery = 64%  Analysis Date = 05/31/13 
 Pct Recovery = 64%  Analysis Date = 05/31/13 
 Pct Recovery = 64%  Analysis Date = 05/29/13 
 Pct Recovery = 64%  Analysis Date = 05/29/13 
 Pct Recovery = 64%  Analysis Date = 05/27/13 
 Pct Recovery = 64%  Analysis Date = 05/27/13 
 Pct Recovery = 64%  Analysis Date = 05/24/13 
 Pct Recovery = 64%  Analysis Date = 05/24/13 
 Pct Recovery = 64%  Analysis Date = 05/22/13 
 Pct Recovery = 64%  Analysis Date = 05/22/13 
 Pct Recovery = 64%  Analysis Date = 05/20/13 
 Pct Recovery = 64%  Analysis Date = 05/20/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 65%  Analysis Date = 05/17/13 
 Pct Recovery = 65%  Analysis Date = 05/15/13 
 Pct Recovery = 65%  Analysis Date = 05/15/13 
 Pct Recovery = 65%  Analysis Date = 05/13/13 
 Pct Recovery = 65%  Analysis Date = 05/13/13 
 Pct Recovery = 65%  Analysis Date = 05/10/13 
 Pct Recovery = 65%  Analysis Date = 05/10/13 
 Pct Recovery = 65%  Analysis Date = 05/08/13 
 Pct Recovery = 65%  Analysis Date = 05/08/13 
 Pct Recovery = 65%  Analysis Date = 05/06/13 
 Pct Recovery = 65%  Analysis Date = 05/06/13 
 Pct Recovery = 65%  Analysis Date = 05/03/13 
 Pct Recovery = 65%  Analysis Date = 05/03/13 
 Pct Recovery = 65%  Analysis Date = 05/01/13 
 Pct Recovery = 65%  Analysis Date = 05/01/13 
 Pct Recovery = 65%  Analysis Date = 04/29/13 
 Pct Recovery = 66%  Analysis Date = 04/29/13 
 Pct Recovery = 66%  Analysis Date = 04/26/13 
 Pct Recovery = 66%  Analysis Date = 04/26/13 
 Pct Recovery = 66%  Analysis Date = 04/24/13 
 Pct Recovery = 66%  Analysis Date = 04/24/13 
 Pct Recovery = 66%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/10/13 
 Pct Recovery = 68%  Analysis Date = 04/10/13 
 Pct Recovery = 68%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/06/13 
 Pct Recovery = 69%  Analysis Date = 04/06/13 
 Pct Recovery = 69%  Analysis Date = 04/03/13 
 Pct Recovery = 69%  Analysis Date = 04/03/13 
 Pct Recovery = 69%  Analysis Date = 04/01/13 
 Pct Recovery = 70%  Analysis Date = 04/01/13 
 Pct Recovery = 70%  Analysis Date = 03/30/13 
 Pct Recovery = 70%  Analysis Date = 03/30/13 
 Pct Recovery = 70%  Analysis Date = 03/27/13 
 Pct Recovery = 70%  Analysis Date = 03/27/13 
 Pct Recovery = 70%  Analysis Date = 03/25/13 
 Pct Recovery = 71%  Analysis Date = 03/25/13 
 Pct Recovery = 71%  Analysis Date = 03/23/13 
 Pct Recovery = 71%  Analysis Date = 03/23/13 
 Pct Recovery = 71%  Analysis Date = 03/21/13 
 Pct Recovery = 71%  Analysis Date = 03/21/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 72%  Analysis Date = 03/18/13 
 Pct Recovery = 72%  Analysis Date = 03/16/13 
 Pct Recovery = 72%  Analysis Date = 03/16/13 
 Pct Recovery = 72%  Analysis Date = 03/14/13 
 Pct Recovery = 72%  Analysis Date = 03/14/13 
 Pct Recovery = 72%  Analysis Date = 03/11/13 
 Pct Recovery = 73%  Analysis Date = 03/11/13 
 Pct Recovery = 73%  Analysis Date = 03/09/13 
 Pct Recovery = 73%  Analysis Date = 03/09/13 
 Pct Recovery = 73%  Analysis Date = 03/07/13 
 Pct Recovery = 73%  Analysis Date = 03/07/13 
 Pct Recovery = 73%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 Pct Recovery = 75%  Analysis Date = 02/28/13 
 Pct Recovery = 75%  Analysis Date = 02/25/13 
 Pct Recovery = 75%  Analysis Date = 02/25/13 
 Pct Recovery = 75%  Analysis Date = 02/23/13 
 Pct Recovery = 75%  Analysis Date = 02/23/13 
 Pct Recovery = 75%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/18/13 
 Pct Recovery = 76%  Analysis Date = 02/18/13 
 Pct Recovery = 76%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 78%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/02/13 
 Pct Recovery = 79%  Analysis Date = 02/02/13 
 Pct Recovery = 79%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 83%  Analysis Date = 01/15/13 
 Pct Recovery = 83%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/10/13 
 Pct Recovery = 84%  Analysis Date = 01/10/13 
 Pct Recovery = 84%  Analysis Date = 01/08/13 
 Pct Recovery = 84%  Analysis Date = 01/08/13 
 Pct Recovery = 84%  Analysis Date = 01/06/13 
 Pct Recovery = 85%  Analysis Date = 01/06/13 
 Pct Recovery = 85%  Analysis Date = 01/03/13 
 Pct Recovery = 85%  Analysis Date = 01/03/13 
 Pct Recovery = 85%  Analysis Date = 01/01/13 
 Pct Recovery = 86%  Analysis Date = 01/01/13 
 Pct Recovery = 86%  Analysis Date = 12/30/12 
 Pct Recovery = 86%  Analysis Date = 12/30/12 
 Pct Recovery = 86%  Analysis Date = 12/27/12 
 Pct Recovery = 86%  Analysis Date = 12/27/12 
 Pct Recovery = 86%  Analysis Date = 12/25/12 
 Pct Recovery = 87%  Analysis Date = 12/25/12 
 Pct Recovery = 87%  Analysis Date = 12/23/12 
 Pct Recovery = 87%  Analysis Date = 12/23/12 
 Pct Recovery = 87%  Analysis Date = 12/20/12 
 Pct Recovery = 88%  Analysis Date = 12/20/12 
 Pct Recovery = 88%  Analysis Date = 12/18/12 
 Pct Recovery = 88%  Analysis Date = 12/18/12 
 Pct Recovery = 88%  Analysis Date = 12/16/12 
 Pct Recovery = 89%  Analysis Date = 12/16/12 
 Pct Recovery = 89%  Analysis Date = 12/14/12 
 Pct Recovery = 89%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALBUTEROL (SALBUTAMOL)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 78% 19% 74% 22%
Total 11 78% 19% 74% 22%

Sample Statistics
ALBUTEROL (SALBUTAMOL)

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 6 55% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
ALPRAZOLAM
METHOD: LC9017 , TESTIDCODE: 68250LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 84%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 75%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 03/20/14 
 Pct Recovery = 75%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/12/14 
 Pct Recovery = 74%  Analysis Date = 03/12/14 
 Pct Recovery = 74%  Analysis Date = 03/10/14 
 Pct Recovery = 73%  Analysis Date = 03/10/14 
 Pct Recovery = 73%  Analysis Date = 03/08/14 
 Pct Recovery = 73%  Analysis Date = 03/08/14 
 Pct Recovery = 73%  Analysis Date = 03/06/14 
 Pct Recovery = 73%  Analysis Date = 03/06/14 
 Pct Recovery = 73%  Analysis Date = 03/04/14 
 Pct Recovery = 73%  Analysis Date = 03/04/14 
 Pct Recovery = 73%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 02/27/14 
 Pct Recovery = 72%  Analysis Date = 02/27/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/21/14 
 Pct Recovery = 71%  Analysis Date = 02/21/14 
 Pct Recovery = 71%  Analysis Date = 02/19/14 
 Pct Recovery = 71%  Analysis Date = 02/19/14 
 Pct Recovery = 71%  Analysis Date = 02/17/14 
 Pct Recovery = 71%  Analysis Date = 02/17/14 
 Pct Recovery = 71%  Analysis Date = 02/15/14 
 Pct Recovery = 70%  Analysis Date = 02/15/14 
 Pct Recovery = 70%  Analysis Date = 02/13/14 
 Pct Recovery = 70%  Analysis Date = 02/13/14 
 Pct Recovery = 70%  Analysis Date = 02/11/14 
 Pct Recovery = 70%  Analysis Date = 02/11/14 
 Pct Recovery = 70%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/04/14 
 Pct Recovery = 69%  Analysis Date = 02/04/14 
 Pct Recovery = 69%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/27/14 
 Pct Recovery = 67%  Analysis Date = 01/27/14 
 Pct Recovery = 67%  Analysis Date = 01/25/14 
 Pct Recovery = 67%  Analysis Date = 01/25/14 
 Pct Recovery = 67%  Analysis Date = 01/23/14 
 Pct Recovery = 67%  Analysis Date = 01/23/14 
 Pct Recovery = 67%  Analysis Date = 01/21/14 
 Pct Recovery = 67%  Analysis Date = 01/21/14 
 Pct Recovery = 67%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 Pct Recovery = 66%  Analysis Date = 01/14/14 
 Pct Recovery = 66%  Analysis Date = 01/14/14 
 Pct Recovery = 66%  Analysis Date = 01/12/14 
 Pct Recovery = 66%  Analysis Date = 01/12/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/04/14 
 Pct Recovery = 66%  Analysis Date = 01/04/14 
 Pct Recovery = 66%  Analysis Date = 01/02/14 
 Pct Recovery = 66%  Analysis Date = 01/02/14 
 Pct Recovery = 66%  Analysis Date = 12/31/13 
 Pct Recovery = 66%  Analysis Date = 12/31/13 
 Pct Recovery = 66%  Analysis Date = 12/28/13 
 Pct Recovery = 66%  Analysis Date = 12/28/13 
 Pct Recovery = 66%  Analysis Date = 12/26/13 
 Pct Recovery = 66%  Analysis Date = 12/26/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/22/13 
 Pct Recovery = 66%  Analysis Date = 12/22/13 
 Pct Recovery = 66%  Analysis Date = 12/20/13 
 Pct Recovery = 66%  Analysis Date = 12/20/13 
 Pct Recovery = 66%  Analysis Date = 12/18/13 
 Pct Recovery = 66%  Analysis Date = 12/18/13 
 Pct Recovery = 66%  Analysis Date = 12/16/13 
 Pct Recovery = 66%  Analysis Date = 12/16/13 
 Pct Recovery = 66%  Analysis Date = 12/14/13 
 Pct Recovery = 66%  Analysis Date = 12/14/13 
 Pct Recovery = 66%  Analysis Date = 12/12/13 
 Pct Recovery = 66%  Analysis Date = 12/12/13 
 Pct Recovery = 66%  Analysis Date = 12/09/13 
 Pct Recovery = 66%  Analysis Date = 12/09/13 
 Pct Recovery = 66%  Analysis Date = 12/07/13 
 Pct Recovery = 66%  Analysis Date = 12/07/13 
 Pct Recovery = 66%  Analysis Date = 12/05/13 
 Pct Recovery = 66%  Analysis Date = 12/05/13 
 Pct Recovery = 66%  Analysis Date = 12/03/13 
 Pct Recovery = 66%  Analysis Date = 12/03/13 
 Pct Recovery = 66%  Analysis Date = 12/01/13 
 Pct Recovery = 66%  Analysis Date = 12/01/13 
 Pct Recovery = 66%  Analysis Date = 11/29/13 
 Pct Recovery = 66%  Analysis Date = 11/29/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/21/13 
 Pct Recovery = 66%  Analysis Date = 11/21/13 
 Pct Recovery = 66%  Analysis Date = 11/18/13 
 Pct Recovery = 66%  Analysis Date = 11/18/13 
 Pct Recovery = 66%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/14/13 
 Pct Recovery = 66%  Analysis Date = 11/14/13 
 Pct Recovery = 66%  Analysis Date = 11/12/13 
 Pct Recovery = 67%  Analysis Date = 11/12/13 
 Pct Recovery = 67%  Analysis Date = 11/10/13 
 Pct Recovery = 67%  Analysis Date = 11/10/13 
 Pct Recovery = 67%  Analysis Date = 11/08/13 
 Pct Recovery = 67%  Analysis Date = 11/08/13 
 Pct Recovery = 67%  Analysis Date = 11/06/13 
 Pct Recovery = 67%  Analysis Date = 11/06/13 
 Pct Recovery = 67%  Analysis Date = 11/04/13 
 Pct Recovery = 67%  Analysis Date = 11/04/13 
 Pct Recovery = 67%  Analysis Date = 11/02/13 
 Pct Recovery = 67%  Analysis Date = 11/02/13 
 Pct Recovery = 67%  Analysis Date = 10/30/13 
 Pct Recovery = 67%  Analysis Date = 10/30/13 
 Pct Recovery = 67%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/26/13 
 Pct Recovery = 67%  Analysis Date = 10/26/13 
 Pct Recovery = 67%  Analysis Date = 10/24/13 
 Pct Recovery = 68%  Analysis Date = 10/24/13 
 Pct Recovery = 68%  Analysis Date = 10/22/13 
 Pct Recovery = 68%  Analysis Date = 10/22/13 
 Pct Recovery = 68%  Analysis Date = 10/20/13 
 Pct Recovery = 68%  Analysis Date = 10/20/13 
 Pct Recovery = 68%  Analysis Date = 10/18/13 
 Pct Recovery = 68%  Analysis Date = 10/18/13 
 Pct Recovery = 68%  Analysis Date = 10/16/13 
 Pct Recovery = 68%  Analysis Date = 10/16/13 
 Pct Recovery = 68%  Analysis Date = 10/14/13 
 Pct Recovery = 68%  Analysis Date = 10/14/13 
 Pct Recovery = 68%  Analysis Date = 10/12/13 
 Pct Recovery = 68%  Analysis Date = 10/12/13 
 Pct Recovery = 68%  Analysis Date = 10/09/13 
 Pct Recovery = 68%  Analysis Date = 10/09/13 
 Pct Recovery = 68%  Analysis Date = 10/07/13 
 Pct Recovery = 69%  Analysis Date = 10/07/13 
 Pct Recovery = 69%  Analysis Date = 10/05/13 
 Pct Recovery = 69%  Analysis Date = 10/05/13 
 Pct Recovery = 69%  Analysis Date = 10/03/13 
 Pct Recovery = 69%  Analysis Date = 10/03/13 
 Pct Recovery = 69%  Analysis Date = 10/01/13 
 Pct Recovery = 69%  Analysis Date = 10/01/13 
 Pct Recovery = 69%  Analysis Date = 09/29/13 
 Pct Recovery = 69%  Analysis Date = 09/29/13 
 Pct Recovery = 69%  Analysis Date = 09/27/13 
 Pct Recovery = 69%  Analysis Date = 09/27/13 
 Pct Recovery = 69%  Analysis Date = 09/25/13 
 Pct Recovery = 69%  Analysis Date = 09/25/13 
 Pct Recovery = 69%  Analysis Date = 09/23/13 
 Pct Recovery = 69%  Analysis Date = 09/23/13 
 Pct Recovery = 69%  Analysis Date = 09/20/13 
 Pct Recovery = 70%  Analysis Date = 09/20/13 
 Pct Recovery = 70%  Analysis Date = 09/18/13 
 Pct Recovery = 70%  Analysis Date = 09/18/13 
 Pct Recovery = 70%  Analysis Date = 09/16/13 
 Pct Recovery = 70%  Analysis Date = 09/16/13 
 Pct Recovery = 70%  Analysis Date = 09/14/13 
 Pct Recovery = 70%  Analysis Date = 09/14/13 
 Pct Recovery = 70%  Analysis Date = 09/12/13 
 Pct Recovery = 70%  Analysis Date = 09/12/13 
 Pct Recovery = 70%  Analysis Date = 09/10/13 
 Pct Recovery = 70%  Analysis Date = 09/10/13 
 Pct Recovery = 70%  Analysis Date = 09/08/13 
 Pct Recovery = 70%  Analysis Date = 09/08/13 
 Pct Recovery = 70%  Analysis Date = 09/06/13 
 Pct Recovery = 70%  Analysis Date = 09/06/13 
 Pct Recovery = 70%  Analysis Date = 09/04/13 
 Pct Recovery = 70%  Analysis Date = 09/04/13 
 Pct Recovery = 70%  Analysis Date = 09/02/13 
 Pct Recovery = 71%  Analysis Date = 09/02/13 
 Pct Recovery = 71%  Analysis Date = 08/30/13 
 Pct Recovery = 71%  Analysis Date = 08/30/13 
 Pct Recovery = 71%  Analysis Date = 08/28/13 
 Pct Recovery = 71%  Analysis Date = 08/28/13 
 Pct Recovery = 71%  Analysis Date = 08/26/13 
 Pct Recovery = 71%  Analysis Date = 08/26/13 
 Pct Recovery = 71%  Analysis Date = 08/24/13 
 Pct Recovery = 71%  Analysis Date = 08/24/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/16/13 
 Pct Recovery = 72%  Analysis Date = 08/16/13 
 Pct Recovery = 72%  Analysis Date = 08/14/13 
 Pct Recovery = 72%  Analysis Date = 08/14/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/09/13 
 Pct Recovery = 72%  Analysis Date = 08/09/13 
 Pct Recovery = 72%  Analysis Date = 08/07/13 
 Pct Recovery = 72%  Analysis Date = 08/07/13 
 Pct Recovery = 72%  Analysis Date = 08/05/13 
 Pct Recovery = 72%  Analysis Date = 08/05/13 
 Pct Recovery = 72%  Analysis Date = 08/03/13 
 Pct Recovery = 72%  Analysis Date = 08/03/13 
 Pct Recovery = 72%  Analysis Date = 08/01/13 
 Pct Recovery = 72%  Analysis Date = 08/01/13 
 Pct Recovery = 72%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/24/13 
 Pct Recovery = 73%  Analysis Date = 07/24/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/17/13 
 Pct Recovery = 73%  Analysis Date = 07/17/13 
 Pct Recovery = 73%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/11/13 
 Pct Recovery = 75%  Analysis Date = 06/11/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 76%  Analysis Date = 06/05/13 
 Pct Recovery = 76%  Analysis Date = 06/03/13 
 Pct Recovery = 76%  Analysis Date = 06/03/13 
 Pct Recovery = 76%  Analysis Date = 06/01/13 
 Pct Recovery = 76%  Analysis Date = 06/01/13 
 Pct Recovery = 76%  Analysis Date = 05/30/13 
 Pct Recovery = 76%  Analysis Date = 05/30/13 
 Pct Recovery = 76%  Analysis Date = 05/28/13 
 Pct Recovery = 76%  Analysis Date = 05/28/13 
 Pct Recovery = 76%  Analysis Date = 05/26/13 
 Pct Recovery = 76%  Analysis Date = 05/26/13 
 Pct Recovery = 76%  Analysis Date = 05/23/13 
 Pct Recovery = 76%  Analysis Date = 05/23/13 
 Pct Recovery = 76%  Analysis Date = 05/21/13 
 Pct Recovery = 76%  Analysis Date = 05/21/13 
 Pct Recovery = 76%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/15/13 
 Pct Recovery = 77%  Analysis Date = 05/15/13 
 Pct Recovery = 77%  Analysis Date = 05/13/13 
 Pct Recovery = 77%  Analysis Date = 05/13/13 
 Pct Recovery = 77%  Analysis Date = 05/11/13 
 Pct Recovery = 77%  Analysis Date = 05/11/13 
 Pct Recovery = 77%  Analysis Date = 05/09/13 
 Pct Recovery = 77%  Analysis Date = 05/09/13 
 Pct Recovery = 77%  Analysis Date = 05/07/13 
 Pct Recovery = 77%  Analysis Date = 05/07/13 
 Pct Recovery = 77%  Analysis Date = 05/05/13 
 Pct Recovery = 77%  Analysis Date = 05/05/13 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 Pct Recovery = 78%  Analysis Date = 05/02/13 
 Pct Recovery = 78%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/28/13 
 Pct Recovery = 78%  Analysis Date = 04/28/13 
 Pct Recovery = 78%  Analysis Date = 04/26/13 
 Pct Recovery = 78%  Analysis Date = 04/26/13 
 Pct Recovery = 78%  Analysis Date = 04/24/13 
 Pct Recovery = 78%  Analysis Date = 04/24/13 
 Pct Recovery = 78%  Analysis Date = 04/22/13 
 Pct Recovery = 78%  Analysis Date = 04/22/13 
 Pct Recovery = 78%  Analysis Date = 04/20/13 
 Pct Recovery = 78%  Analysis Date = 04/20/13 
 Pct Recovery = 78%  Analysis Date = 04/18/13 
 Pct Recovery = 78%  Analysis Date = 04/18/13 
 Pct Recovery = 78%  Analysis Date = 04/16/13 
 Pct Recovery = 79%  Analysis Date = 04/16/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/11/13 
 Pct Recovery = 79%  Analysis Date = 04/11/13 
 Pct Recovery = 79%  Analysis Date = 04/09/13 
 Pct Recovery = 79%  Analysis Date = 04/09/13 
 Pct Recovery = 79%  Analysis Date = 04/07/13 
 Pct Recovery = 79%  Analysis Date = 04/07/13 
 Pct Recovery = 79%  Analysis Date = 04/05/13 
 Pct Recovery = 79%  Analysis Date = 04/05/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/28/13 
 Pct Recovery = 80%  Analysis Date = 03/28/13 
 Pct Recovery = 80%  Analysis Date = 03/26/13 
 Pct Recovery = 80%  Analysis Date = 03/26/13 
 Pct Recovery = 80%  Analysis Date = 03/23/13 
 Pct Recovery = 80%  Analysis Date = 03/23/13 
 Pct Recovery = 80%  Analysis Date = 03/21/13 
 Pct Recovery = 80%  Analysis Date = 03/21/13 
 Pct Recovery = 80%  Analysis Date = 03/19/13 
 Pct Recovery = 80%  Analysis Date = 03/19/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 03/15/13 
 Pct Recovery = 81%  Analysis Date = 03/15/13 
 Pct Recovery = 81%  Analysis Date = 03/13/13 
 Pct Recovery = 81%  Analysis Date = 03/13/13 
 Pct Recovery = 81%  Analysis Date = 03/11/13 
 Pct Recovery = 81%  Analysis Date = 03/11/13 
 Pct Recovery = 81%  Analysis Date = 03/09/13 
 Pct Recovery = 81%  Analysis Date = 03/09/13 
 Pct Recovery = 81%  Analysis Date = 03/07/13 
 Pct Recovery = 81%  Analysis Date = 03/07/13 
 Pct Recovery = 81%  Analysis Date = 03/04/13 
 Pct Recovery = 81%  Analysis Date = 03/04/13 
 Pct Recovery = 81%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 Pct Recovery = 82%  Analysis Date = 02/28/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/24/13 
 Pct Recovery = 82%  Analysis Date = 02/24/13 
 Pct Recovery = 82%  Analysis Date = 02/22/13 
 Pct Recovery = 82%  Analysis Date = 02/22/13 
 Pct Recovery = 82%  Analysis Date = 02/20/13 
 Pct Recovery = 82%  Analysis Date = 02/20/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/14/13 
 Pct Recovery = 83%  Analysis Date = 02/14/13 
 Pct Recovery = 83%  Analysis Date = 02/11/13 
 Pct Recovery = 83%  Analysis Date = 02/11/13 
 Pct Recovery = 83%  Analysis Date = 02/09/13 
 Pct Recovery = 83%  Analysis Date = 02/09/13 
 Pct Recovery = 83%  Analysis Date = 02/07/13 
 Pct Recovery = 83%  Analysis Date = 02/07/13 
 Pct Recovery = 83%  Analysis Date = 02/05/13 
 Pct Recovery = 83%  Analysis Date = 02/05/13 
 Pct Recovery = 83%  Analysis Date = 02/03/13 
 Pct Recovery = 83%  Analysis Date = 02/03/13 
 Pct Recovery = 83%  Analysis Date = 02/01/13 
 Pct Recovery = 83%  Analysis Date = 02/01/13 
 Pct Recovery = 83%  Analysis Date = 01/30/13 
 Pct Recovery = 83%  Analysis Date = 01/30/13 
 Pct Recovery = 83%  Analysis Date = 01/28/13 
 Pct Recovery = 84%  Analysis Date = 01/28/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/24/13 
 Pct Recovery = 84%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPRAZOLAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 73% 7% 73% 8%
Total 6 73% 7% 73% 8%

Sample Statistics
ALPRAZOLAM

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
AMITRIPTYLINE
METHOD: LC9017 , TESTIDCODE: 67522LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 31%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 73%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 49%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 68%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 41%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 6%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 11%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 38%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 66%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 58%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 Pct Recovery = 59%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 57%  Analysis Date = 03/16/14 
 Pct Recovery = 57%  Analysis Date = 03/14/14 
 Pct Recovery = 56%  Analysis Date = 03/14/14 
 Pct Recovery = 56%  Analysis Date = 03/11/14 
 Pct Recovery = 55%  Analysis Date = 03/11/14 
 Pct Recovery = 55%  Analysis Date = 03/09/14 
 Pct Recovery = 54%  Analysis Date = 03/09/14 
 Pct Recovery = 54%  Analysis Date = 03/07/14 
 Pct Recovery = 54%  Analysis Date = 03/07/14 
 Pct Recovery = 54%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 50%  Analysis Date = 02/25/14 
 Pct Recovery = 50%  Analysis Date = 02/23/14 
 Pct Recovery = 50%  Analysis Date = 02/23/14 
 Pct Recovery = 50%  Analysis Date = 02/21/14 
 Pct Recovery = 49%  Analysis Date = 02/21/14 
 Pct Recovery = 49%  Analysis Date = 02/18/14 
 Pct Recovery = 48%  Analysis Date = 02/18/14 
 Pct Recovery = 48%  Analysis Date = 02/16/14 
 Pct Recovery = 47%  Analysis Date = 02/16/14 
 Pct Recovery = 47%  Analysis Date = 02/14/14 
 Pct Recovery = 47%  Analysis Date = 02/14/14 
 Pct Recovery = 47%  Analysis Date = 02/12/14 
 Pct Recovery = 46%  Analysis Date = 02/12/14 
 Pct Recovery = 46%  Analysis Date = 02/09/14 
 Pct Recovery = 46%  Analysis Date = 02/09/14 
 Pct Recovery = 46%  Analysis Date = 02/07/14 
 Pct Recovery = 45%  Analysis Date = 02/07/14 
 Pct Recovery = 45%  Analysis Date = 02/05/14 
 Pct Recovery = 44%  Analysis Date = 02/05/14 
 Pct Recovery = 44%  Analysis Date = 02/02/14 
 Pct Recovery = 44%  Analysis Date = 02/02/14 
 Pct Recovery = 44%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/26/14 
 Pct Recovery = 42%  Analysis Date = 01/26/14 
 Pct Recovery = 42%  Analysis Date = 01/24/14 
 Pct Recovery = 41%  Analysis Date = 01/24/14 
 Pct Recovery = 41%  Analysis Date = 01/22/14 
 Pct Recovery = 41%  Analysis Date = 01/22/14 
 Pct Recovery = 41%  Analysis Date = 01/19/14 
 Pct Recovery = 40%  Analysis Date = 01/19/14 
 Pct Recovery = 40%  Analysis Date = 01/17/14 
 Pct Recovery = 40%  Analysis Date = 01/17/14 
 Pct Recovery = 40%  Analysis Date = 01/15/14 
 Pct Recovery = 39%  Analysis Date = 01/15/14 
 Pct Recovery = 39%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/08/14 
 Pct Recovery = 37%  Analysis Date = 01/08/14 
 Pct Recovery = 37%  Analysis Date = 01/06/14 
 Pct Recovery = 37%  Analysis Date = 01/06/14 
 Pct Recovery = 37%  Analysis Date = 01/03/14 
 Pct Recovery = 36%  Analysis Date = 01/03/14 
 Pct Recovery = 36%  Analysis Date = 01/01/14 
 Pct Recovery = 35%  Analysis Date = 01/01/14 
 Pct Recovery = 35%  Analysis Date = 12/30/13 
 Pct Recovery = 35%  Analysis Date = 12/30/13 
 Pct Recovery = 35%  Analysis Date = 12/27/13 
 Pct Recovery = 34%  Analysis Date = 12/27/13 
 Pct Recovery = 34%  Analysis Date = 12/25/13 
 Pct Recovery = 34%  Analysis Date = 12/25/13 
 Pct Recovery = 34%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/18/13 
 Pct Recovery = 32%  Analysis Date = 12/18/13 
 Pct Recovery = 32%  Analysis Date = 12/16/13 
 Pct Recovery = 31%  Analysis Date = 12/16/13 
 Pct Recovery = 31%  Analysis Date = 12/13/13 
 Pct Recovery = 31%  Analysis Date = 12/13/13 
 Pct Recovery = 31%  Analysis Date = 12/11/13 
 Pct Recovery = 30%  Analysis Date = 12/11/13 
 Pct Recovery = 30%  Analysis Date = 12/09/13 
 Pct Recovery = 29%  Analysis Date = 12/09/13 
 Pct Recovery = 29%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/04/13 
 Pct Recovery = 28%  Analysis Date = 12/04/13 
 Pct Recovery = 28%  Analysis Date = 12/02/13 
 Pct Recovery = 29%  Analysis Date = 12/02/13 
 Pct Recovery = 29%  Analysis Date = 11/30/13 
 Pct Recovery = 29%  Analysis Date = 11/30/13 
 Pct Recovery = 29%  Analysis Date = 11/27/13 
 Pct Recovery = 30%  Analysis Date = 11/27/13 
 Pct Recovery = 30%  Analysis Date = 11/25/13 
 Pct Recovery = 30%  Analysis Date = 11/25/13 
 Pct Recovery = 30%  Analysis Date = 11/23/13 
 Pct Recovery = 31%  Analysis Date = 11/23/13 
 Pct Recovery = 31%  Analysis Date = 11/20/13 
 Pct Recovery = 31%  Analysis Date = 11/20/13 
 Pct Recovery = 31%  Analysis Date = 11/18/13 
 Pct Recovery = 32%  Analysis Date = 11/18/13 
 Pct Recovery = 32%  Analysis Date = 11/16/13 
 Pct Recovery = 32%  Analysis Date = 11/16/13 
 Pct Recovery = 32%  Analysis Date = 11/13/13 
 Pct Recovery = 33%  Analysis Date = 11/13/13 
 Pct Recovery = 33%  Analysis Date = 11/11/13 
 Pct Recovery = 33%  Analysis Date = 11/11/13 
 Pct Recovery = 33%  Analysis Date = 11/09/13 
 Pct Recovery = 34%  Analysis Date = 11/09/13 
 Pct Recovery = 34%  Analysis Date = 11/07/13 
 Pct Recovery = 34%  Analysis Date = 11/07/13 
 Pct Recovery = 34%  Analysis Date = 11/04/13 
 Pct Recovery = 34%  Analysis Date = 11/04/13 
 Pct Recovery = 34%  Analysis Date = 11/02/13 
 Pct Recovery = 35%  Analysis Date = 11/02/13 
 Pct Recovery = 35%  Analysis Date = 10/31/13 
 Pct Recovery = 35%  Analysis Date = 10/31/13 
 Pct Recovery = 35%  Analysis Date = 10/28/13 
 Pct Recovery = 36%  Analysis Date = 10/28/13 
 Pct Recovery = 36%  Analysis Date = 10/26/13 
 Pct Recovery = 36%  Analysis Date = 10/26/13 
 Pct Recovery = 36%  Analysis Date = 10/24/13 
 Pct Recovery = 37%  Analysis Date = 10/24/13 
 Pct Recovery = 37%  Analysis Date = 10/21/13 
 Pct Recovery = 37%  Analysis Date = 10/21/13 
 Pct Recovery = 37%  Analysis Date = 10/19/13 
 Pct Recovery = 38%  Analysis Date = 10/19/13 
 Pct Recovery = 38%  Analysis Date = 10/17/13 
 Pct Recovery = 38%  Analysis Date = 10/17/13 
 Pct Recovery = 38%  Analysis Date = 10/14/13 
 Pct Recovery = 39%  Analysis Date = 10/14/13 
 Pct Recovery = 39%  Analysis Date = 10/12/13 
 Pct Recovery = 39%  Analysis Date = 10/12/13 
 Pct Recovery = 39%  Analysis Date = 10/10/13 
 Pct Recovery = 40%  Analysis Date = 10/10/13 
 Pct Recovery = 40%  Analysis Date = 10/07/13 
 Pct Recovery = 40%  Analysis Date = 10/07/13 
 Pct Recovery = 40%  Analysis Date = 10/05/13 
 Pct Recovery = 41%  Analysis Date = 10/05/13 
 Pct Recovery = 41%  Analysis Date = 10/03/13 
 Pct Recovery = 41%  Analysis Date = 10/03/13 
 Pct Recovery = 41%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 09/28/13 
 Pct Recovery = 42%  Analysis Date = 09/28/13 
 Pct Recovery = 42%  Analysis Date = 09/26/13 
 Pct Recovery = 42%  Analysis Date = 09/26/13 
 Pct Recovery = 42%  Analysis Date = 09/24/13 
 Pct Recovery = 43%  Analysis Date = 09/24/13 
 Pct Recovery = 43%  Analysis Date = 09/21/13 
 Pct Recovery = 43%  Analysis Date = 09/21/13 
 Pct Recovery = 43%  Analysis Date = 09/19/13 
 Pct Recovery = 44%  Analysis Date = 09/19/13 
 Pct Recovery = 44%  Analysis Date = 09/17/13 
 Pct Recovery = 44%  Analysis Date = 09/17/13 
 Pct Recovery = 44%  Analysis Date = 09/14/13 
 Pct Recovery = 45%  Analysis Date = 09/14/13 
 Pct Recovery = 45%  Analysis Date = 09/12/13 
 Pct Recovery = 45%  Analysis Date = 09/12/13 
 Pct Recovery = 45%  Analysis Date = 09/10/13 
 Pct Recovery = 46%  Analysis Date = 09/10/13 
 Pct Recovery = 46%  Analysis Date = 09/07/13 
 Pct Recovery = 46%  Analysis Date = 09/07/13 
 Pct Recovery = 46%  Analysis Date = 09/05/13 
 Pct Recovery = 47%  Analysis Date = 09/05/13 
 Pct Recovery = 47%  Analysis Date = 09/03/13 
 Pct Recovery = 47%  Analysis Date = 09/03/13 
 Pct Recovery = 47%  Analysis Date = 09/01/13 
 Pct Recovery = 48%  Analysis Date = 09/01/13 
 Pct Recovery = 48%  Analysis Date = 08/29/13 
 Pct Recovery = 48%  Analysis Date = 08/29/13 
 Pct Recovery = 48%  Analysis Date = 08/27/13 
 Pct Recovery = 49%  Analysis Date = 08/27/13 
 Pct Recovery = 49%  Analysis Date = 08/25/13 
 Pct Recovery = 50%  Analysis Date = 08/25/13 
 Pct Recovery = 50%  Analysis Date = 08/22/13 
 Pct Recovery = 51%  Analysis Date = 08/22/13 
 Pct Recovery = 51%  Analysis Date = 08/20/13 
 Pct Recovery = 51%  Analysis Date = 08/20/13 
 Pct Recovery = 51%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 53%  Analysis Date = 08/15/13 
 Pct Recovery = 53%  Analysis Date = 08/13/13 
 Pct Recovery = 53%  Analysis Date = 08/13/13 
 Pct Recovery = 53%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 54%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/02/13 
 Pct Recovery = 55%  Analysis Date = 08/02/13 
 Pct Recovery = 55%  Analysis Date = 07/30/13 
 Pct Recovery = 55%  Analysis Date = 07/30/13 
 Pct Recovery = 55%  Analysis Date = 07/28/13 
 Pct Recovery = 54%  Analysis Date = 07/28/13 
 Pct Recovery = 54%  Analysis Date = 07/26/13 
 Pct Recovery = 54%  Analysis Date = 07/26/13 
 Pct Recovery = 54%  Analysis Date = 07/23/13 
 Pct Recovery = 54%  Analysis Date = 07/23/13 
 Pct Recovery = 54%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/16/13 
 Pct Recovery = 52%  Analysis Date = 07/16/13 
 Pct Recovery = 52%  Analysis Date = 07/14/13 
 Pct Recovery = 52%  Analysis Date = 07/14/13 
 Pct Recovery = 52%  Analysis Date = 07/12/13 
 Pct Recovery = 52%  Analysis Date = 07/12/13 
 Pct Recovery = 52%  Analysis Date = 07/09/13 
 Pct Recovery = 51%  Analysis Date = 07/09/13 
 Pct Recovery = 51%  Analysis Date = 07/07/13 
 Pct Recovery = 51%  Analysis Date = 07/07/13 
 Pct Recovery = 51%  Analysis Date = 07/05/13 
 Pct Recovery = 50%  Analysis Date = 07/05/13 
 Pct Recovery = 50%  Analysis Date = 07/02/13 
 Pct Recovery = 50%  Analysis Date = 07/02/13 
 Pct Recovery = 50%  Analysis Date = 06/30/13 
 Pct Recovery = 50%  Analysis Date = 06/30/13 
 Pct Recovery = 50%  Analysis Date = 06/28/13 
 Pct Recovery = 49%  Analysis Date = 06/28/13 
 Pct Recovery = 49%  Analysis Date = 06/26/13 
 Pct Recovery = 49%  Analysis Date = 06/26/13 
 Pct Recovery = 49%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/19/13 
 Pct Recovery = 48%  Analysis Date = 06/19/13 
 Pct Recovery = 48%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/14/13 
 Pct Recovery = 47%  Analysis Date = 06/14/13 
 Pct Recovery = 47%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/07/13 
 Pct Recovery = 46%  Analysis Date = 06/07/13 
 Pct Recovery = 46%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/02/13 
 Pct Recovery = 45%  Analysis Date = 06/02/13 
 Pct Recovery = 45%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/27/13 
 Pct Recovery = 44%  Analysis Date = 05/27/13 
 Pct Recovery = 44%  Analysis Date = 05/24/13 
 Pct Recovery = 43%  Analysis Date = 05/24/13 
 Pct Recovery = 43%  Analysis Date = 05/22/13 
 Pct Recovery = 43%  Analysis Date = 05/22/13 
 Pct Recovery = 43%  Analysis Date = 05/20/13 
 Pct Recovery = 42%  Analysis Date = 05/20/13 
 Pct Recovery = 42%  Analysis Date = 05/17/13 
 Pct Recovery = 42%  Analysis Date = 05/17/13 
 Pct Recovery = 42%  Analysis Date = 05/15/13 
 Pct Recovery = 42%  Analysis Date = 05/15/13 
 Pct Recovery = 42%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/10/13 
 Pct Recovery = 41%  Analysis Date = 05/10/13 
 Pct Recovery = 41%  Analysis Date = 05/08/13 
 Pct Recovery = 40%  Analysis Date = 05/08/13 
 Pct Recovery = 40%  Analysis Date = 05/06/13 
 Pct Recovery = 40%  Analysis Date = 05/06/13 
 Pct Recovery = 40%  Analysis Date = 05/03/13 
 Pct Recovery = 40%  Analysis Date = 05/03/13 
 Pct Recovery = 40%  Analysis Date = 05/01/13 
 Pct Recovery = 39%  Analysis Date = 05/01/13 
 Pct Recovery = 39%  Analysis Date = 04/29/13 
 Pct Recovery = 39%  Analysis Date = 04/29/13 
 Pct Recovery = 39%  Analysis Date = 04/26/13 
 Pct Recovery = 39%  Analysis Date = 04/26/13 
 Pct Recovery = 39%  Analysis Date = 04/24/13 
 Pct Recovery = 39%  Analysis Date = 04/24/13 
 Pct Recovery = 39%  Analysis Date = 04/22/13 
 Pct Recovery = 38%  Analysis Date = 04/22/13 
 Pct Recovery = 38%  Analysis Date = 04/20/13 
 Pct Recovery = 38%  Analysis Date = 04/20/13 
 Pct Recovery = 38%  Analysis Date = 04/17/13 
 Pct Recovery = 38%  Analysis Date = 04/17/13 
 Pct Recovery = 38%  Analysis Date = 04/15/13 
 Pct Recovery = 38%  Analysis Date = 04/15/13 
 Pct Recovery = 38%  Analysis Date = 04/13/13 
 Pct Recovery = 38%  Analysis Date = 04/13/13 
 Pct Recovery = 38%  Analysis Date = 04/10/13 
 Pct Recovery = 38%  Analysis Date = 04/10/13 
 Pct Recovery = 38%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/06/13 
 Pct Recovery = 37%  Analysis Date = 04/06/13 
 Pct Recovery = 37%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 Pct Recovery = 37%  Analysis Date = 03/25/13 
 Pct Recovery = 37%  Analysis Date = 03/25/13 
 Pct Recovery = 37%  Analysis Date = 03/23/13 
 Pct Recovery = 37%  Analysis Date = 03/23/13 
 Pct Recovery = 37%  Analysis Date = 03/21/13 
 Pct Recovery = 38%  Analysis Date = 03/21/13 
 Pct Recovery = 38%  Analysis Date = 03/18/13 
 Pct Recovery = 39%  Analysis Date = 03/18/13 
 Pct Recovery = 39%  Analysis Date = 03/16/13 
 Pct Recovery = 39%  Analysis Date = 03/16/13 
 Pct Recovery = 39%  Analysis Date = 03/14/13 
 Pct Recovery = 40%  Analysis Date = 03/14/13 
 Pct Recovery = 40%  Analysis Date = 03/11/13 
 Pct Recovery = 41%  Analysis Date = 03/11/13 
 Pct Recovery = 41%  Analysis Date = 03/09/13 
 Pct Recovery = 41%  Analysis Date = 03/09/13 
 Pct Recovery = 41%  Analysis Date = 03/07/13 
 Pct Recovery = 42%  Analysis Date = 03/07/13 
 Pct Recovery = 42%  Analysis Date = 03/04/13 
 Pct Recovery = 42%  Analysis Date = 03/04/13 
 Pct Recovery = 42%  Analysis Date = 03/02/13 
 Pct Recovery = 43%  Analysis Date = 03/02/13 
 Pct Recovery = 43%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/25/13 
 Pct Recovery = 44%  Analysis Date = 02/25/13 
 Pct Recovery = 44%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/21/13 
 Pct Recovery = 46%  Analysis Date = 02/21/13 
 Pct Recovery = 46%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/16/13 
 Pct Recovery = 47%  Analysis Date = 02/16/13 
 Pct Recovery = 47%  Analysis Date = 02/14/13 
 Pct Recovery = 48%  Analysis Date = 02/14/13 
 Pct Recovery = 48%  Analysis Date = 02/12/13 
 Pct Recovery = 48%  Analysis Date = 02/12/13 
 Pct Recovery = 48%  Analysis Date = 02/09/13 
 Pct Recovery = 49%  Analysis Date = 02/09/13 
 Pct Recovery = 49%  Analysis Date = 02/07/13 
 Pct Recovery = 50%  Analysis Date = 02/07/13 
 Pct Recovery = 50%  Analysis Date = 02/05/13 
 Pct Recovery = 50%  Analysis Date = 02/05/13 
 Pct Recovery = 50%  Analysis Date = 02/02/13 
 Pct Recovery = 51%  Analysis Date = 02/02/13 
 Pct Recovery = 51%  Analysis Date = 01/31/13 
 Pct Recovery = 52%  Analysis Date = 01/31/13 
 Pct Recovery = 52%  Analysis Date = 01/29/13 
 Pct Recovery = 52%  Analysis Date = 01/29/13 
 Pct Recovery = 52%  Analysis Date = 01/26/13 
 Pct Recovery = 53%  Analysis Date = 01/26/13 
 Pct Recovery = 53%  Analysis Date = 01/24/13 
 Pct Recovery = 54%  Analysis Date = 01/24/13 
 Pct Recovery = 54%  Analysis Date = 01/22/13 
 Pct Recovery = 54%  Analysis Date = 01/22/13 
 Pct Recovery = 54%  Analysis Date = 01/19/13 
 Pct Recovery = 55%  Analysis Date = 01/19/13 
 Pct Recovery = 55%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/13/13 
 Pct Recovery = 57%  Analysis Date = 01/13/13 
 Pct Recovery = 57%  Analysis Date = 01/10/13 
 Pct Recovery = 58%  Analysis Date = 01/10/13 
 Pct Recovery = 58%  Analysis Date = 01/08/13 
 Pct Recovery = 58%  Analysis Date = 01/08/13 
 Pct Recovery = 58%  Analysis Date = 01/06/13 
 Pct Recovery = 59%  Analysis Date = 01/06/13 
 Pct Recovery = 59%  Analysis Date = 01/03/13 
 Pct Recovery = 60%  Analysis Date = 01/03/13 
 Pct Recovery = 60%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 61%  Analysis Date = 12/30/12 
 Pct Recovery = 61%  Analysis Date = 12/27/12 
 Pct Recovery = 62%  Analysis Date = 12/27/12 
 Pct Recovery = 62%  Analysis Date = 12/25/12 
 Pct Recovery = 62%  Analysis Date = 12/25/12 
 Pct Recovery = 62%  Analysis Date = 12/23/12 
 Pct Recovery = 63%  Analysis Date = 12/23/12 
 Pct Recovery = 63%  Analysis Date = 12/20/12 
 Pct Recovery = 64%  Analysis Date = 12/20/12 
 Pct Recovery = 64%  Analysis Date = 12/18/12 
 Pct Recovery = 64%  Analysis Date = 12/18/12 
 Pct Recovery = 64%  Analysis Date = 12/16/12 
 Pct Recovery = 65%  Analysis Date = 12/16/12 
 Pct Recovery = 65%  Analysis Date = 12/14/12 
 Pct Recovery = 66%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
AMITRIPTYLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 46% 20% 48% 17%
Total 14 46% 20% 48% 17%

Sample Statistics
AMITRIPTYLINE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 14 93% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
AMPHETAMINE
METHOD: LC9017 , TESTIDCODE: 67461LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 79%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 82%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 59%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 93%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 84%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 72%  Analysis Date = 02/19/14 
 Pct Recovery = 82%  Analysis Date = 02/18/14 
 Pct Recovery = 84%  Analysis Date = 02/18/14 
 Pct Recovery = 84%  Analysis Date = 02/16/14 
 Pct Recovery = 83%  Analysis Date = 02/16/14 
 Pct Recovery = 83%  Analysis Date = 02/14/14 
 Pct Recovery = 83%  Analysis Date = 02/14/14 
 Pct Recovery = 83%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/11/14 
 Pct Recovery = 81%  Analysis Date = 02/11/14 
 Pct Recovery = 81%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/07/14 
 Pct Recovery = 80%  Analysis Date = 02/07/14 
 Pct Recovery = 80%  Analysis Date = 02/05/14 
 Pct Recovery = 80%  Analysis Date = 02/05/14 
 Pct Recovery = 80%  Analysis Date = 02/03/14 
 Pct Recovery = 79%  Analysis Date = 02/03/14 
 Pct Recovery = 79%  Analysis Date = 02/02/14 
 Pct Recovery = 79%  Analysis Date = 02/02/14 
 Pct Recovery = 79%  Analysis Date = 01/31/14 
 Pct Recovery = 78%  Analysis Date = 01/31/14 
 Pct Recovery = 78%  Analysis Date = 01/29/14 
 Pct Recovery = 77%  Analysis Date = 01/29/14 
 Pct Recovery = 77%  Analysis Date = 01/27/14 
 Pct Recovery = 77%  Analysis Date = 01/27/14 
 Pct Recovery = 77%  Analysis Date = 01/26/14 
 Pct Recovery = 76%  Analysis Date = 01/26/14 
 Pct Recovery = 76%  Analysis Date = 01/24/14 
 Pct Recovery = 76%  Analysis Date = 01/24/14 
 Pct Recovery = 76%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/17/14 
 Pct Recovery = 73%  Analysis Date = 01/17/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/13/14 
 Pct Recovery = 72%  Analysis Date = 01/13/14 
 Pct Recovery = 72%  Analysis Date = 01/11/14 
 Pct Recovery = 72%  Analysis Date = 01/11/14 
 Pct Recovery = 72%  Analysis Date = 01/09/14 
 Pct Recovery = 71%  Analysis Date = 01/09/14 
 Pct Recovery = 71%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/04/14 
 Pct Recovery = 69%  Analysis Date = 01/04/14 
 Pct Recovery = 69%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/28/13 
 Pct Recovery = 67%  Analysis Date = 12/28/13 
 Pct Recovery = 67%  Analysis Date = 12/26/13 
 Pct Recovery = 66%  Analysis Date = 12/26/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/23/13 
 Pct Recovery = 65%  Analysis Date = 12/23/13 
 Pct Recovery = 65%  Analysis Date = 12/21/13 
 Pct Recovery = 65%  Analysis Date = 12/21/13 
 Pct Recovery = 65%  Analysis Date = 12/19/13 
 Pct Recovery = 64%  Analysis Date = 12/19/13 
 Pct Recovery = 64%  Analysis Date = 12/17/13 
 Pct Recovery = 63%  Analysis Date = 12/17/13 
 Pct Recovery = 63%  Analysis Date = 12/15/13 
 Pct Recovery = 63%  Analysis Date = 12/15/13 
 Pct Recovery = 63%  Analysis Date = 12/14/13 
 Pct Recovery = 62%  Analysis Date = 12/14/13 
 Pct Recovery = 62%  Analysis Date = 12/12/13 
 Pct Recovery = 62%  Analysis Date = 12/12/13 
 Pct Recovery = 62%  Analysis Date = 12/10/13 
 Pct Recovery = 61%  Analysis Date = 12/10/13 
 Pct Recovery = 61%  Analysis Date = 12/08/13 
 Pct Recovery = 60%  Analysis Date = 12/08/13 
 Pct Recovery = 60%  Analysis Date = 12/07/13 
 Pct Recovery = 60%  Analysis Date = 12/07/13 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 Pct Recovery = 59%  Analysis Date = 12/05/13 
 Pct Recovery = 59%  Analysis Date = 12/03/13 
 Pct Recovery = 59%  Analysis Date = 12/03/13 
 Pct Recovery = 59%  Analysis Date = 12/01/13 
 Pct Recovery = 60%  Analysis Date = 12/01/13 
 Pct Recovery = 60%  Analysis Date = 11/29/13 
 Pct Recovery = 60%  Analysis Date = 11/29/13 
 Pct Recovery = 60%  Analysis Date = 11/28/13 
 Pct Recovery = 60%  Analysis Date = 11/28/13 
 Pct Recovery = 60%  Analysis Date = 11/26/13 
 Pct Recovery = 60%  Analysis Date = 11/26/13 
 Pct Recovery = 60%  Analysis Date = 11/24/13 
 Pct Recovery = 60%  Analysis Date = 11/24/13 
 Pct Recovery = 60%  Analysis Date = 11/22/13 
 Pct Recovery = 60%  Analysis Date = 11/22/13 
 Pct Recovery = 60%  Analysis Date = 11/20/13 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 Pct Recovery = 61%  Analysis Date = 11/19/13 
 Pct Recovery = 61%  Analysis Date = 11/19/13 
 Pct Recovery = 61%  Analysis Date = 11/17/13 
 Pct Recovery = 61%  Analysis Date = 11/17/13 
 Pct Recovery = 61%  Analysis Date = 11/15/13 
 Pct Recovery = 61%  Analysis Date = 11/15/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/12/13 
 Pct Recovery = 61%  Analysis Date = 11/12/13 
 Pct Recovery = 61%  Analysis Date = 11/10/13 
 Pct Recovery = 62%  Analysis Date = 11/10/13 
 Pct Recovery = 62%  Analysis Date = 11/08/13 
 Pct Recovery = 62%  Analysis Date = 11/08/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/03/13 
 Pct Recovery = 62%  Analysis Date = 11/03/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 10/30/13 
 Pct Recovery = 63%  Analysis Date = 10/30/13 
 Pct Recovery = 63%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/26/13 
 Pct Recovery = 63%  Analysis Date = 10/26/13 
 Pct Recovery = 63%  Analysis Date = 10/25/13 
 Pct Recovery = 63%  Analysis Date = 10/25/13 
 Pct Recovery = 63%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/21/13 
 Pct Recovery = 63%  Analysis Date = 10/21/13 
 Pct Recovery = 63%  Analysis Date = 10/19/13 
 Pct Recovery = 64%  Analysis Date = 10/19/13 
 Pct Recovery = 64%  Analysis Date = 10/18/13 
 Pct Recovery = 64%  Analysis Date = 10/18/13 
 Pct Recovery = 64%  Analysis Date = 10/16/13 
 Pct Recovery = 64%  Analysis Date = 10/16/13 
 Pct Recovery = 64%  Analysis Date = 10/14/13 
 Pct Recovery = 64%  Analysis Date = 10/14/13 
 Pct Recovery = 64%  Analysis Date = 10/12/13 
 Pct Recovery = 64%  Analysis Date = 10/12/13 
 Pct Recovery = 64%  Analysis Date = 10/10/13 
 Pct Recovery = 64%  Analysis Date = 10/10/13 
 Pct Recovery = 64%  Analysis Date = 10/09/13 
 Pct Recovery = 65%  Analysis Date = 10/09/13 
 Pct Recovery = 65%  Analysis Date = 10/07/13 
 Pct Recovery = 65%  Analysis Date = 10/07/13 
 Pct Recovery = 65%  Analysis Date = 10/05/13 
 Pct Recovery = 65%  Analysis Date = 10/05/13 
 Pct Recovery = 65%  Analysis Date = 10/03/13 
 Pct Recovery = 65%  Analysis Date = 10/03/13 
 Pct Recovery = 65%  Analysis Date = 10/01/13 
 Pct Recovery = 65%  Analysis Date = 10/01/13 
 Pct Recovery = 65%  Analysis Date = 09/30/13 
 Pct Recovery = 65%  Analysis Date = 09/30/13 
 Pct Recovery = 65%  Analysis Date = 09/28/13 
 Pct Recovery = 66%  Analysis Date = 09/28/13 
 Pct Recovery = 66%  Analysis Date = 09/26/13 
 Pct Recovery = 66%  Analysis Date = 09/26/13 
 Pct Recovery = 66%  Analysis Date = 09/24/13 
 Pct Recovery = 66%  Analysis Date = 09/24/13 
 Pct Recovery = 66%  Analysis Date = 09/23/13 
 Pct Recovery = 66%  Analysis Date = 09/23/13 
 Pct Recovery = 66%  Analysis Date = 09/21/13 
 Pct Recovery = 66%  Analysis Date = 09/21/13 
 Pct Recovery = 66%  Analysis Date = 09/19/13 
 Pct Recovery = 66%  Analysis Date = 09/19/13 
 Pct Recovery = 66%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/15/13 
 Pct Recovery = 67%  Analysis Date = 09/15/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/06/13 
 Pct Recovery = 68%  Analysis Date = 09/06/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/03/13 
 Pct Recovery = 68%  Analysis Date = 09/03/13 
 Pct Recovery = 68%  Analysis Date = 09/01/13 
 Pct Recovery = 68%  Analysis Date = 09/01/13 
 Pct Recovery = 68%  Analysis Date = 08/30/13 
 Pct Recovery = 68%  Analysis Date = 08/30/13 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 Pct Recovery = 68%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/23/13 
 Pct Recovery = 69%  Analysis Date = 08/23/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/20/13 
 Pct Recovery = 69%  Analysis Date = 08/20/13 
 Pct Recovery = 69%  Analysis Date = 08/18/13 
 Pct Recovery = 69%  Analysis Date = 08/18/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 70%  Analysis Date = 08/16/13 
 Pct Recovery = 70%  Analysis Date = 08/14/13 
 Pct Recovery = 70%  Analysis Date = 08/14/13 
 Pct Recovery = 70%  Analysis Date = 08/13/13 
 Pct Recovery = 70%  Analysis Date = 08/13/13 
 Pct Recovery = 70%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/09/13 
 Pct Recovery = 70%  Analysis Date = 08/09/13 
 Pct Recovery = 70%  Analysis Date = 08/07/13 
 Pct Recovery = 70%  Analysis Date = 08/07/13 
 Pct Recovery = 70%  Analysis Date = 08/05/13 
 Pct Recovery = 71%  Analysis Date = 08/05/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 07/31/13 
 Pct Recovery = 71%  Analysis Date = 07/31/13 
 Pct Recovery = 71%  Analysis Date = 07/29/13 
 Pct Recovery = 71%  Analysis Date = 07/29/13 
 Pct Recovery = 71%  Analysis Date = 07/27/13 
 Pct Recovery = 71%  Analysis Date = 07/27/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/24/13 
 Pct Recovery = 72%  Analysis Date = 07/24/13 
 Pct Recovery = 72%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/20/13 
 Pct Recovery = 72%  Analysis Date = 07/20/13 
 Pct Recovery = 72%  Analysis Date = 07/19/13 
 Pct Recovery = 72%  Analysis Date = 07/19/13 
 Pct Recovery = 72%  Analysis Date = 07/17/13 
 Pct Recovery = 72%  Analysis Date = 07/17/13 
 Pct Recovery = 72%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/10/13 
 Pct Recovery = 73%  Analysis Date = 07/10/13 
 Pct Recovery = 73%  Analysis Date = 07/08/13 
 Pct Recovery = 73%  Analysis Date = 07/08/13 
 Pct Recovery = 73%  Analysis Date = 07/06/13 
 Pct Recovery = 73%  Analysis Date = 07/06/13 
 Pct Recovery = 73%  Analysis Date = 07/04/13 
 Pct Recovery = 74%  Analysis Date = 07/04/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/01/13 
 Pct Recovery = 74%  Analysis Date = 07/01/13 
 Pct Recovery = 74%  Analysis Date = 06/29/13 
 Pct Recovery = 74%  Analysis Date = 06/29/13 
 Pct Recovery = 74%  Analysis Date = 06/27/13 
 Pct Recovery = 74%  Analysis Date = 06/27/13 
 Pct Recovery = 74%  Analysis Date = 06/25/13 
 Pct Recovery = 74%  Analysis Date = 06/25/13 
 Pct Recovery = 74%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/15/13 
 Pct Recovery = 75%  Analysis Date = 06/15/13 
 Pct Recovery = 75%  Analysis Date = 06/13/13 
 Pct Recovery = 76%  Analysis Date = 06/13/13 
 Pct Recovery = 76%  Analysis Date = 06/11/13 
 Pct Recovery = 76%  Analysis Date = 06/11/13 
 Pct Recovery = 76%  Analysis Date = 06/09/13 
 Pct Recovery = 76%  Analysis Date = 06/09/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/06/13 
 Pct Recovery = 76%  Analysis Date = 06/06/13 
 Pct Recovery = 76%  Analysis Date = 06/04/13 
 Pct Recovery = 76%  Analysis Date = 06/04/13 
 Pct Recovery = 76%  Analysis Date = 06/02/13 
 Pct Recovery = 77%  Analysis Date = 06/02/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/21/13 
 Pct Recovery = 78%  Analysis Date = 05/21/13 
 Pct Recovery = 78%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 79%  Analysis Date = 05/12/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 79%  Analysis Date = 05/06/13 
 Pct Recovery = 79%  Analysis Date = 05/06/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/01/13 
 Pct Recovery = 80%  Analysis Date = 05/01/13 
 Pct Recovery = 80%  Analysis Date = 04/29/13 
 Pct Recovery = 81%  Analysis Date = 04/29/13 
 Pct Recovery = 81%  Analysis Date = 04/27/13 
 Pct Recovery = 81%  Analysis Date = 04/27/13 
 Pct Recovery = 81%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/24/13 
 Pct Recovery = 83%  Analysis Date = 04/24/13 
 Pct Recovery = 83%  Analysis Date = 04/22/13 
 Pct Recovery = 83%  Analysis Date = 04/22/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/18/13 
 Pct Recovery = 85%  Analysis Date = 04/18/13 
 Pct Recovery = 85%  Analysis Date = 04/17/13 
 Pct Recovery = 85%  Analysis Date = 04/17/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 86%  Analysis Date = 04/15/13 
 Pct Recovery = 86%  Analysis Date = 04/13/13 
 Pct Recovery = 87%  Analysis Date = 04/13/13 
 Pct Recovery = 87%  Analysis Date = 04/11/13 
 Pct Recovery = 87%  Analysis Date = 04/11/13 
 Pct Recovery = 87%  Analysis Date = 04/10/13 
 Pct Recovery = 88%  Analysis Date = 04/10/13 
 Pct Recovery = 88%  Analysis Date = 04/08/13 
 Pct Recovery = 89%  Analysis Date = 04/08/13 
 Pct Recovery = 89%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/04/13 
 Pct Recovery = 90%  Analysis Date = 04/04/13 
 Pct Recovery = 90%  Analysis Date = 04/02/13 
 Pct Recovery = 91%  Analysis Date = 04/02/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 92%  Analysis Date = 03/30/13 
 Pct Recovery = 92%  Analysis Date = 03/28/13 
 Pct Recovery = 93%  Analysis Date = 03/28/13 
 Pct Recovery = 93%  Analysis Date = 03/26/13 
 Pct Recovery = 93%  Analysis Date = 03/26/13 
 Pct Recovery = 93%  Analysis Date = 03/24/13 
 Pct Recovery = 92%  Analysis Date = 03/24/13 
 Pct Recovery = 92%  Analysis Date = 03/23/13 
 Pct Recovery = 90%  Analysis Date = 03/23/13 
 Pct Recovery = 90%  Analysis Date = 03/21/13 
 Pct Recovery = 89%  Analysis Date = 03/21/13 
 Pct Recovery = 89%  Analysis Date = 03/19/13 
 Pct Recovery = 87%  Analysis Date = 03/19/13 
 Pct Recovery = 87%  Analysis Date = 03/17/13 
 Pct Recovery = 86%  Analysis Date = 03/17/13 
 Pct Recovery = 86%  Analysis Date = 03/16/13 
 Pct Recovery = 85%  Analysis Date = 03/16/13 
 Pct Recovery = 85%  Analysis Date = 03/14/13 
 Pct Recovery = 83%  Analysis Date = 03/14/13 
 Pct Recovery = 83%  Analysis Date = 03/12/13 
 Pct Recovery = 82%  Analysis Date = 03/12/13 
 Pct Recovery = 82%  Analysis Date = 03/10/13 
 Pct Recovery = 80%  Analysis Date = 03/10/13 
 Pct Recovery = 80%  Analysis Date = 03/08/13 
 Pct Recovery = 79%  Analysis Date = 03/08/13 
 Pct Recovery = 79%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/05/13 
 Pct Recovery = 76%  Analysis Date = 03/05/13 
 Pct Recovery = 76%  Analysis Date = 03/03/13 
 Pct Recovery = 75%  Analysis Date = 03/03/13 
 Pct Recovery = 75%  Analysis Date = 03/01/13 
 Pct Recovery = 73%  Analysis Date = 03/01/13 
 Pct Recovery = 73%  Analysis Date = 02/28/13 
 Pct Recovery = 72%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
AMPHETAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 78% 12% 81% 9%
Total 6 78% 12% 81% 9%

Sample Statistics
AMPHETAMINE

Characteristic N % % Basis
Plotted 6 86% Spiked
Estimated Values 3 43% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 1 14% 1 out of 7
Not Spiked 25 .  
False Positives 0 0% 0 out of 24

OBSP Determination:
ANTIPYRINE
METHOD: LC9017 , TESTIDCODE: 67477LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 68%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 75%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 82%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 76%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 76%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 92%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 79%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 63%  Analysis Date = 03/21/14 
 Pct Recovery = 76%  Analysis Date = 03/18/14 
 Pct Recovery = 76%  Analysis Date = 03/18/14 
 Pct Recovery = 76%  Analysis Date = 03/16/14 
 Pct Recovery = 75%  Analysis Date = 03/16/14 
 Pct Recovery = 75%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/11/14 
 Pct Recovery = 75%  Analysis Date = 03/11/14 
 Pct Recovery = 75%  Analysis Date = 03/09/14 
 Pct Recovery = 75%  Analysis Date = 03/09/14 
 Pct Recovery = 75%  Analysis Date = 03/07/14 
 Pct Recovery = 74%  Analysis Date = 03/07/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/25/14 
 Pct Recovery = 73%  Analysis Date = 02/25/14 
 Pct Recovery = 73%  Analysis Date = 02/23/14 
 Pct Recovery = 73%  Analysis Date = 02/23/14 
 Pct Recovery = 73%  Analysis Date = 02/21/14 
 Pct Recovery = 73%  Analysis Date = 02/21/14 
 Pct Recovery = 73%  Analysis Date = 02/18/14 
 Pct Recovery = 73%  Analysis Date = 02/18/14 
 Pct Recovery = 73%  Analysis Date = 02/16/14 
 Pct Recovery = 73%  Analysis Date = 02/16/14 
 Pct Recovery = 73%  Analysis Date = 02/14/14 
 Pct Recovery = 72%  Analysis Date = 02/14/14 
 Pct Recovery = 72%  Analysis Date = 02/12/14 
 Pct Recovery = 72%  Analysis Date = 02/12/14 
 Pct Recovery = 72%  Analysis Date = 02/09/14 
 Pct Recovery = 72%  Analysis Date = 02/09/14 
 Pct Recovery = 72%  Analysis Date = 02/07/14 
 Pct Recovery = 72%  Analysis Date = 02/07/14 
 Pct Recovery = 72%  Analysis Date = 02/05/14 
 Pct Recovery = 71%  Analysis Date = 02/05/14 
 Pct Recovery = 71%  Analysis Date = 02/02/14 
 Pct Recovery = 71%  Analysis Date = 02/02/14 
 Pct Recovery = 71%  Analysis Date = 01/31/14 
 Pct Recovery = 71%  Analysis Date = 01/31/14 
 Pct Recovery = 71%  Analysis Date = 01/29/14 
 Pct Recovery = 71%  Analysis Date = 01/29/14 
 Pct Recovery = 71%  Analysis Date = 01/26/14 
 Pct Recovery = 70%  Analysis Date = 01/26/14 
 Pct Recovery = 70%  Analysis Date = 01/24/14 
 Pct Recovery = 70%  Analysis Date = 01/24/14 
 Pct Recovery = 70%  Analysis Date = 01/22/14 
 Pct Recovery = 70%  Analysis Date = 01/22/14 
 Pct Recovery = 70%  Analysis Date = 01/19/14 
 Pct Recovery = 70%  Analysis Date = 01/19/14 
 Pct Recovery = 70%  Analysis Date = 01/17/14 
 Pct Recovery = 70%  Analysis Date = 01/17/14 
 Pct Recovery = 70%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/13/14 
 Pct Recovery = 70%  Analysis Date = 01/13/14 
 Pct Recovery = 70%  Analysis Date = 01/10/14 
 Pct Recovery = 70%  Analysis Date = 01/10/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/25/13 
 Pct Recovery = 70%  Analysis Date = 12/25/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/18/13 
 Pct Recovery = 71%  Analysis Date = 12/18/13 
 Pct Recovery = 71%  Analysis Date = 12/16/13 
 Pct Recovery = 71%  Analysis Date = 12/16/13 
 Pct Recovery = 71%  Analysis Date = 12/13/13 
 Pct Recovery = 71%  Analysis Date = 12/13/13 
 Pct Recovery = 71%  Analysis Date = 12/11/13 
 Pct Recovery = 71%  Analysis Date = 12/11/13 
 Pct Recovery = 71%  Analysis Date = 12/09/13 
 Pct Recovery = 71%  Analysis Date = 12/09/13 
 Pct Recovery = 71%  Analysis Date = 12/07/13 
 Pct Recovery = 71%  Analysis Date = 12/07/13 
 Pct Recovery = 71%  Analysis Date = 12/04/13 
 Pct Recovery = 71%  Analysis Date = 12/04/13 
 Pct Recovery = 71%  Analysis Date = 12/02/13 
 Pct Recovery = 71%  Analysis Date = 12/02/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/07/13 
 Pct Recovery = 73%  Analysis Date = 11/07/13 
 Pct Recovery = 73%  Analysis Date = 11/04/13 
 Pct Recovery = 73%  Analysis Date = 11/04/13 
 Pct Recovery = 73%  Analysis Date = 11/02/13 
 Pct Recovery = 73%  Analysis Date = 11/02/13 
 Pct Recovery = 73%  Analysis Date = 10/31/13 
 Pct Recovery = 73%  Analysis Date = 10/31/13 
 Pct Recovery = 73%  Analysis Date = 10/28/13 
 Pct Recovery = 73%  Analysis Date = 10/28/13 
 Pct Recovery = 73%  Analysis Date = 10/26/13 
 Pct Recovery = 74%  Analysis Date = 10/26/13 
 Pct Recovery = 74%  Analysis Date = 10/24/13 
 Pct Recovery = 74%  Analysis Date = 10/24/13 
 Pct Recovery = 74%  Analysis Date = 10/21/13 
 Pct Recovery = 74%  Analysis Date = 10/21/13 
 Pct Recovery = 74%  Analysis Date = 10/19/13 
 Pct Recovery = 74%  Analysis Date = 10/19/13 
 Pct Recovery = 74%  Analysis Date = 10/17/13 
 Pct Recovery = 74%  Analysis Date = 10/17/13 
 Pct Recovery = 74%  Analysis Date = 10/14/13 
 Pct Recovery = 74%  Analysis Date = 10/14/13 
 Pct Recovery = 74%  Analysis Date = 10/12/13 
 Pct Recovery = 74%  Analysis Date = 10/12/13 
 Pct Recovery = 74%  Analysis Date = 10/10/13 
 Pct Recovery = 75%  Analysis Date = 10/10/13 
 Pct Recovery = 75%  Analysis Date = 10/07/13 
 Pct Recovery = 75%  Analysis Date = 10/07/13 
 Pct Recovery = 75%  Analysis Date = 10/05/13 
 Pct Recovery = 75%  Analysis Date = 10/05/13 
 Pct Recovery = 75%  Analysis Date = 10/03/13 
 Pct Recovery = 75%  Analysis Date = 10/03/13 
 Pct Recovery = 75%  Analysis Date = 10/01/13 
 Pct Recovery = 75%  Analysis Date = 10/01/13 
 Pct Recovery = 75%  Analysis Date = 09/28/13 
 Pct Recovery = 75%  Analysis Date = 09/28/13 
 Pct Recovery = 75%  Analysis Date = 09/26/13 
 Pct Recovery = 75%  Analysis Date = 09/26/13 
 Pct Recovery = 75%  Analysis Date = 09/24/13 
 Pct Recovery = 76%  Analysis Date = 09/24/13 
 Pct Recovery = 76%  Analysis Date = 09/21/13 
 Pct Recovery = 76%  Analysis Date = 09/21/13 
 Pct Recovery = 76%  Analysis Date = 09/19/13 
 Pct Recovery = 76%  Analysis Date = 09/19/13 
 Pct Recovery = 76%  Analysis Date = 09/17/13 
 Pct Recovery = 76%  Analysis Date = 09/17/13 
 Pct Recovery = 76%  Analysis Date = 09/14/13 
 Pct Recovery = 76%  Analysis Date = 09/14/13 
 Pct Recovery = 76%  Analysis Date = 09/12/13 
 Pct Recovery = 76%  Analysis Date = 09/12/13 
 Pct Recovery = 76%  Analysis Date = 09/10/13 
 Pct Recovery = 77%  Analysis Date = 09/10/13 
 Pct Recovery = 77%  Analysis Date = 09/07/13 
 Pct Recovery = 77%  Analysis Date = 09/07/13 
 Pct Recovery = 77%  Analysis Date = 09/05/13 
 Pct Recovery = 77%  Analysis Date = 09/05/13 
 Pct Recovery = 77%  Analysis Date = 09/03/13 
 Pct Recovery = 77%  Analysis Date = 09/03/13 
 Pct Recovery = 77%  Analysis Date = 09/01/13 
 Pct Recovery = 77%  Analysis Date = 09/01/13 
 Pct Recovery = 77%  Analysis Date = 08/29/13 
 Pct Recovery = 77%  Analysis Date = 08/29/13 
 Pct Recovery = 77%  Analysis Date = 08/27/13 
 Pct Recovery = 77%  Analysis Date = 08/27/13 
 Pct Recovery = 77%  Analysis Date = 08/25/13 
 Pct Recovery = 77%  Analysis Date = 08/25/13 
 Pct Recovery = 77%  Analysis Date = 08/22/13 
 Pct Recovery = 77%  Analysis Date = 08/22/13 
 Pct Recovery = 77%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 77%  Analysis Date = 08/08/13 
 Pct Recovery = 77%  Analysis Date = 08/08/13 
 Pct Recovery = 77%  Analysis Date = 08/06/13 
 Pct Recovery = 77%  Analysis Date = 08/06/13 
 Pct Recovery = 77%  Analysis Date = 08/04/13 
 Pct Recovery = 77%  Analysis Date = 08/04/13 
 Pct Recovery = 77%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/21/13 
 Pct Recovery = 76%  Analysis Date = 07/21/13 
 Pct Recovery = 76%  Analysis Date = 07/19/13 
 Pct Recovery = 76%  Analysis Date = 07/19/13 
 Pct Recovery = 76%  Analysis Date = 07/16/13 
 Pct Recovery = 76%  Analysis Date = 07/16/13 
 Pct Recovery = 76%  Analysis Date = 07/14/13 
 Pct Recovery = 76%  Analysis Date = 07/14/13 
 Pct Recovery = 76%  Analysis Date = 07/12/13 
 Pct Recovery = 76%  Analysis Date = 07/12/13 
 Pct Recovery = 76%  Analysis Date = 07/09/13 
 Pct Recovery = 76%  Analysis Date = 07/09/13 
 Pct Recovery = 76%  Analysis Date = 07/07/13 
 Pct Recovery = 76%  Analysis Date = 07/07/13 
 Pct Recovery = 76%  Analysis Date = 07/05/13 
 Pct Recovery = 76%  Analysis Date = 07/05/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/23/13 
 Pct Recovery = 75%  Analysis Date = 06/23/13 
 Pct Recovery = 75%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 75%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 73%  Analysis Date = 05/01/13 
 Pct Recovery = 73%  Analysis Date = 04/29/13 
 Pct Recovery = 74%  Analysis Date = 04/29/13 
 Pct Recovery = 74%  Analysis Date = 04/26/13 
 Pct Recovery = 74%  Analysis Date = 04/26/13 
 Pct Recovery = 74%  Analysis Date = 04/24/13 
 Pct Recovery = 74%  Analysis Date = 04/24/13 
 Pct Recovery = 74%  Analysis Date = 04/22/13 
 Pct Recovery = 74%  Analysis Date = 04/22/13 
 Pct Recovery = 74%  Analysis Date = 04/20/13 
 Pct Recovery = 74%  Analysis Date = 04/20/13 
 Pct Recovery = 74%  Analysis Date = 04/17/13 
 Pct Recovery = 74%  Analysis Date = 04/17/13 
 Pct Recovery = 74%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/13/13 
 Pct Recovery = 75%  Analysis Date = 04/13/13 
 Pct Recovery = 75%  Analysis Date = 04/10/13 
 Pct Recovery = 75%  Analysis Date = 04/10/13 
 Pct Recovery = 75%  Analysis Date = 04/08/13 
 Pct Recovery = 75%  Analysis Date = 04/08/13 
 Pct Recovery = 75%  Analysis Date = 04/06/13 
 Pct Recovery = 75%  Analysis Date = 04/06/13 
 Pct Recovery = 75%  Analysis Date = 04/03/13 
 Pct Recovery = 75%  Analysis Date = 04/03/13 
 Pct Recovery = 75%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 76%  Analysis Date = 03/23/13 
 Pct Recovery = 76%  Analysis Date = 03/23/13 
 Pct Recovery = 76%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/18/13 
 Pct Recovery = 77%  Analysis Date = 03/18/13 
 Pct Recovery = 77%  Analysis Date = 03/16/13 
 Pct Recovery = 77%  Analysis Date = 03/16/13 
 Pct Recovery = 77%  Analysis Date = 03/14/13 
 Pct Recovery = 77%  Analysis Date = 03/14/13 
 Pct Recovery = 77%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/04/13 
 Pct Recovery = 78%  Analysis Date = 03/04/13 
 Pct Recovery = 78%  Analysis Date = 03/02/13 
 Pct Recovery = 78%  Analysis Date = 03/02/13 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 Pct Recovery = 78%  Analysis Date = 02/25/13 
 Pct Recovery = 78%  Analysis Date = 02/25/13 
 Pct Recovery = 78%  Analysis Date = 02/23/13 
 Pct Recovery = 78%  Analysis Date = 02/23/13 
 Pct Recovery = 78%  Analysis Date = 02/21/13 
 Pct Recovery = 78%  Analysis Date = 02/21/13 
 Pct Recovery = 78%  Analysis Date = 02/18/13 
 Pct Recovery = 79%  Analysis Date = 02/18/13 
 Pct Recovery = 79%  Analysis Date = 02/16/13 
 Pct Recovery = 79%  Analysis Date = 02/16/13 
 Pct Recovery = 79%  Analysis Date = 02/14/13 
 Pct Recovery = 79%  Analysis Date = 02/14/13 
 Pct Recovery = 79%  Analysis Date = 02/12/13 
 Pct Recovery = 79%  Analysis Date = 02/12/13 
 Pct Recovery = 79%  Analysis Date = 02/09/13 
 Pct Recovery = 79%  Analysis Date = 02/09/13 
 Pct Recovery = 79%  Analysis Date = 02/07/13 
 Pct Recovery = 80%  Analysis Date = 02/07/13 
 Pct Recovery = 80%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/19/13 
 Pct Recovery = 81%  Analysis Date = 01/19/13 
 Pct Recovery = 81%  Analysis Date = 01/17/13 
 Pct Recovery = 81%  Analysis Date = 01/17/13 
 Pct Recovery = 81%  Analysis Date = 01/15/13 
 Pct Recovery = 81%  Analysis Date = 01/15/13 
 Pct Recovery = 81%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/01/13 
 Pct Recovery = 83%  Analysis Date = 01/01/13 
 Pct Recovery = 83%  Analysis Date = 12/30/12 
 Pct Recovery = 83%  Analysis Date = 12/30/12 
 Pct Recovery = 83%  Analysis Date = 12/27/12 
 Pct Recovery = 83%  Analysis Date = 12/27/12 
 Pct Recovery = 83%  Analysis Date = 12/25/12 
 Pct Recovery = 83%  Analysis Date = 12/25/12 
 Pct Recovery = 83%  Analysis Date = 12/23/12 
 Pct Recovery = 83%  Analysis Date = 12/23/12 
 Pct Recovery = 83%  Analysis Date = 12/20/12 
 Pct Recovery = 84%  Analysis Date = 12/20/12 
 Pct Recovery = 84%  Analysis Date = 12/18/12 
 Pct Recovery = 84%  Analysis Date = 12/18/12 
 Pct Recovery = 84%  Analysis Date = 12/16/12 
 Pct Recovery = 84%  Analysis Date = 12/16/12 
 Pct Recovery = 84%  Analysis Date = 12/14/12 
 Pct Recovery = 84%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ANTIPYRINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 76% 8% 76% 9%
Total 11 76% 8% 76% 9%

Sample Statistics
ANTIPYRINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
ATENOLOL
METHOD: LC9017 , TESTIDCODE: 67502LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 73%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 87%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 68%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 86%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 60%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 81%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 59%  Analysis Date = 03/18/14 
 Pct Recovery = 59%  Analysis Date = 03/18/14 
 Pct Recovery = 59%  Analysis Date = 03/16/14 
 Pct Recovery = 59%  Analysis Date = 03/16/14 
 Pct Recovery = 59%  Analysis Date = 03/14/14 
 Pct Recovery = 60%  Analysis Date = 03/14/14 
 Pct Recovery = 60%  Analysis Date = 03/11/14 
 Pct Recovery = 60%  Analysis Date = 03/11/14 
 Pct Recovery = 60%  Analysis Date = 03/09/14 
 Pct Recovery = 60%  Analysis Date = 03/09/14 
 Pct Recovery = 60%  Analysis Date = 03/07/14 
 Pct Recovery = 61%  Analysis Date = 03/07/14 
 Pct Recovery = 61%  Analysis Date = 03/04/14 
 Pct Recovery = 61%  Analysis Date = 03/04/14 
 Pct Recovery = 61%  Analysis Date = 03/02/14 
 Pct Recovery = 61%  Analysis Date = 03/02/14 
 Pct Recovery = 61%  Analysis Date = 02/28/14 
 Pct Recovery = 62%  Analysis Date = 02/28/14 
 Pct Recovery = 62%  Analysis Date = 02/25/14 
 Pct Recovery = 62%  Analysis Date = 02/25/14 
 Pct Recovery = 62%  Analysis Date = 02/23/14 
 Pct Recovery = 62%  Analysis Date = 02/23/14 
 Pct Recovery = 62%  Analysis Date = 02/21/14 
 Pct Recovery = 63%  Analysis Date = 02/21/14 
 Pct Recovery = 63%  Analysis Date = 02/18/14 
 Pct Recovery = 63%  Analysis Date = 02/18/14 
 Pct Recovery = 63%  Analysis Date = 02/16/14 
 Pct Recovery = 63%  Analysis Date = 02/16/14 
 Pct Recovery = 63%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 65%  Analysis Date = 02/07/14 
 Pct Recovery = 65%  Analysis Date = 02/05/14 
 Pct Recovery = 65%  Analysis Date = 02/05/14 
 Pct Recovery = 65%  Analysis Date = 02/02/14 
 Pct Recovery = 66%  Analysis Date = 02/02/14 
 Pct Recovery = 66%  Analysis Date = 01/31/14 
 Pct Recovery = 66%  Analysis Date = 01/31/14 
 Pct Recovery = 66%  Analysis Date = 01/29/14 
 Pct Recovery = 66%  Analysis Date = 01/29/14 
 Pct Recovery = 66%  Analysis Date = 01/26/14 
 Pct Recovery = 67%  Analysis Date = 01/26/14 
 Pct Recovery = 67%  Analysis Date = 01/24/14 
 Pct Recovery = 67%  Analysis Date = 01/24/14 
 Pct Recovery = 67%  Analysis Date = 01/22/14 
 Pct Recovery = 67%  Analysis Date = 01/22/14 
 Pct Recovery = 67%  Analysis Date = 01/19/14 
 Pct Recovery = 68%  Analysis Date = 01/19/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 69%  Analysis Date = 01/13/14 
 Pct Recovery = 69%  Analysis Date = 01/10/14 
 Pct Recovery = 69%  Analysis Date = 01/10/14 
 Pct Recovery = 69%  Analysis Date = 01/08/14 
 Pct Recovery = 69%  Analysis Date = 01/08/14 
 Pct Recovery = 69%  Analysis Date = 01/06/14 
 Pct Recovery = 69%  Analysis Date = 01/06/14 
 Pct Recovery = 69%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/23/13 
 Pct Recovery = 71%  Analysis Date = 12/23/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/18/13 
 Pct Recovery = 71%  Analysis Date = 12/18/13 
 Pct Recovery = 71%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/13/13 
 Pct Recovery = 72%  Analysis Date = 12/13/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/09/13 
 Pct Recovery = 72%  Analysis Date = 12/09/13 
 Pct Recovery = 72%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/04/13 
 Pct Recovery = 73%  Analysis Date = 12/04/13 
 Pct Recovery = 73%  Analysis Date = 12/02/13 
 Pct Recovery = 73%  Analysis Date = 12/02/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/27/13 
 Pct Recovery = 74%  Analysis Date = 11/27/13 
 Pct Recovery = 74%  Analysis Date = 11/25/13 
 Pct Recovery = 74%  Analysis Date = 11/25/13 
 Pct Recovery = 74%  Analysis Date = 11/23/13 
 Pct Recovery = 74%  Analysis Date = 11/23/13 
 Pct Recovery = 74%  Analysis Date = 11/20/13 
 Pct Recovery = 74%  Analysis Date = 11/20/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 75%  Analysis Date = 11/18/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/13/13 
 Pct Recovery = 75%  Analysis Date = 11/13/13 
 Pct Recovery = 75%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/09/13 
 Pct Recovery = 76%  Analysis Date = 11/09/13 
 Pct Recovery = 76%  Analysis Date = 11/07/13 
 Pct Recovery = 76%  Analysis Date = 11/07/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/28/13 
 Pct Recovery = 77%  Analysis Date = 10/28/13 
 Pct Recovery = 77%  Analysis Date = 10/26/13 
 Pct Recovery = 77%  Analysis Date = 10/26/13 
 Pct Recovery = 77%  Analysis Date = 10/24/13 
 Pct Recovery = 77%  Analysis Date = 10/24/13 
 Pct Recovery = 77%  Analysis Date = 10/21/13 
 Pct Recovery = 78%  Analysis Date = 10/21/13 
 Pct Recovery = 78%  Analysis Date = 10/19/13 
 Pct Recovery = 78%  Analysis Date = 10/19/13 
 Pct Recovery = 78%  Analysis Date = 10/17/13 
 Pct Recovery = 78%  Analysis Date = 10/17/13 
 Pct Recovery = 78%  Analysis Date = 10/14/13 
 Pct Recovery = 78%  Analysis Date = 10/14/13 
 Pct Recovery = 78%  Analysis Date = 10/12/13 
 Pct Recovery = 79%  Analysis Date = 10/12/13 
 Pct Recovery = 79%  Analysis Date = 10/10/13 
 Pct Recovery = 79%  Analysis Date = 10/10/13 
 Pct Recovery = 79%  Analysis Date = 10/07/13 
 Pct Recovery = 79%  Analysis Date = 10/07/13 
 Pct Recovery = 79%  Analysis Date = 10/05/13 
 Pct Recovery = 79%  Analysis Date = 10/05/13 
 Pct Recovery = 79%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 80%  Analysis Date = 09/28/13 
 Pct Recovery = 80%  Analysis Date = 09/28/13 
 Pct Recovery = 80%  Analysis Date = 09/26/13 
 Pct Recovery = 80%  Analysis Date = 09/26/13 
 Pct Recovery = 80%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/14/13 
 Pct Recovery = 82%  Analysis Date = 09/14/13 
 Pct Recovery = 82%  Analysis Date = 09/12/13 
 Pct Recovery = 82%  Analysis Date = 09/12/13 
 Pct Recovery = 82%  Analysis Date = 09/10/13 
 Pct Recovery = 82%  Analysis Date = 09/10/13 
 Pct Recovery = 82%  Analysis Date = 09/07/13 
 Pct Recovery = 82%  Analysis Date = 09/07/13 
 Pct Recovery = 82%  Analysis Date = 09/05/13 
 Pct Recovery = 83%  Analysis Date = 09/05/13 
 Pct Recovery = 83%  Analysis Date = 09/03/13 
 Pct Recovery = 83%  Analysis Date = 09/03/13 
 Pct Recovery = 83%  Analysis Date = 09/01/13 
 Pct Recovery = 83%  Analysis Date = 09/01/13 
 Pct Recovery = 83%  Analysis Date = 08/29/13 
 Pct Recovery = 83%  Analysis Date = 08/29/13 
 Pct Recovery = 83%  Analysis Date = 08/27/13 
 Pct Recovery = 83%  Analysis Date = 08/27/13 
 Pct Recovery = 83%  Analysis Date = 08/25/13 
 Pct Recovery = 83%  Analysis Date = 08/25/13 
 Pct Recovery = 83%  Analysis Date = 08/22/13 
 Pct Recovery = 83%  Analysis Date = 08/22/13 
 Pct Recovery = 83%  Analysis Date = 08/20/13 
 Pct Recovery = 83%  Analysis Date = 08/20/13 
 Pct Recovery = 83%  Analysis Date = 08/18/13 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 Pct Recovery = 82%  Analysis Date = 08/15/13 
 Pct Recovery = 82%  Analysis Date = 08/15/13 
 Pct Recovery = 82%  Analysis Date = 08/13/13 
 Pct Recovery = 82%  Analysis Date = 08/13/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/08/13 
 Pct Recovery = 81%  Analysis Date = 08/08/13 
 Pct Recovery = 81%  Analysis Date = 08/06/13 
 Pct Recovery = 81%  Analysis Date = 08/06/13 
 Pct Recovery = 81%  Analysis Date = 08/04/13 
 Pct Recovery = 81%  Analysis Date = 08/04/13 
 Pct Recovery = 81%  Analysis Date = 08/02/13 
 Pct Recovery = 81%  Analysis Date = 08/02/13 
 Pct Recovery = 81%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/19/13 
 Pct Recovery = 79%  Analysis Date = 07/19/13 
 Pct Recovery = 79%  Analysis Date = 07/16/13 
 Pct Recovery = 79%  Analysis Date = 07/16/13 
 Pct Recovery = 79%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/12/13 
 Pct Recovery = 78%  Analysis Date = 07/12/13 
 Pct Recovery = 78%  Analysis Date = 07/09/13 
 Pct Recovery = 78%  Analysis Date = 07/09/13 
 Pct Recovery = 78%  Analysis Date = 07/07/13 
 Pct Recovery = 78%  Analysis Date = 07/07/13 
 Pct Recovery = 78%  Analysis Date = 07/05/13 
 Pct Recovery = 77%  Analysis Date = 07/05/13 
 Pct Recovery = 77%  Analysis Date = 07/02/13 
 Pct Recovery = 77%  Analysis Date = 07/02/13 
 Pct Recovery = 77%  Analysis Date = 06/30/13 
 Pct Recovery = 77%  Analysis Date = 06/30/13 
 Pct Recovery = 77%  Analysis Date = 06/28/13 
 Pct Recovery = 77%  Analysis Date = 06/28/13 
 Pct Recovery = 77%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/02/13 
 Pct Recovery = 74%  Analysis Date = 06/02/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/27/13 
 Pct Recovery = 73%  Analysis Date = 05/27/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/22/13 
 Pct Recovery = 73%  Analysis Date = 05/22/13 
 Pct Recovery = 73%  Analysis Date = 05/20/13 
 Pct Recovery = 72%  Analysis Date = 05/20/13 
 Pct Recovery = 72%  Analysis Date = 05/17/13 
 Pct Recovery = 72%  Analysis Date = 05/17/13 
 Pct Recovery = 72%  Analysis Date = 05/15/13 
 Pct Recovery = 72%  Analysis Date = 05/15/13 
 Pct Recovery = 72%  Analysis Date = 05/13/13 
 Pct Recovery = 72%  Analysis Date = 05/13/13 
 Pct Recovery = 72%  Analysis Date = 05/10/13 
 Pct Recovery = 71%  Analysis Date = 05/10/13 
 Pct Recovery = 71%  Analysis Date = 05/08/13 
 Pct Recovery = 71%  Analysis Date = 05/08/13 
 Pct Recovery = 71%  Analysis Date = 05/06/13 
 Pct Recovery = 71%  Analysis Date = 05/06/13 
 Pct Recovery = 71%  Analysis Date = 05/03/13 
 Pct Recovery = 71%  Analysis Date = 05/03/13 
 Pct Recovery = 71%  Analysis Date = 05/01/13 
 Pct Recovery = 71%  Analysis Date = 05/01/13 
 Pct Recovery = 71%  Analysis Date = 04/29/13 
 Pct Recovery = 71%  Analysis Date = 04/29/13 
 Pct Recovery = 71%  Analysis Date = 04/26/13 
 Pct Recovery = 71%  Analysis Date = 04/26/13 
 Pct Recovery = 71%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/20/13 
 Pct Recovery = 73%  Analysis Date = 04/20/13 
 Pct Recovery = 73%  Analysis Date = 04/17/13 
 Pct Recovery = 73%  Analysis Date = 04/17/13 
 Pct Recovery = 73%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 74%  Analysis Date = 04/13/13 
 Pct Recovery = 74%  Analysis Date = 04/10/13 
 Pct Recovery = 74%  Analysis Date = 04/10/13 
 Pct Recovery = 74%  Analysis Date = 04/08/13 
 Pct Recovery = 74%  Analysis Date = 04/08/13 
 Pct Recovery = 74%  Analysis Date = 04/06/13 
 Pct Recovery = 75%  Analysis Date = 04/06/13 
 Pct Recovery = 75%  Analysis Date = 04/03/13 
 Pct Recovery = 75%  Analysis Date = 04/03/13 
 Pct Recovery = 75%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 77%  Analysis Date = 03/25/13 
 Pct Recovery = 77%  Analysis Date = 03/23/13 
 Pct Recovery = 77%  Analysis Date = 03/23/13 
 Pct Recovery = 77%  Analysis Date = 03/21/13 
 Pct Recovery = 78%  Analysis Date = 03/21/13 
 Pct Recovery = 78%  Analysis Date = 03/18/13 
 Pct Recovery = 78%  Analysis Date = 03/18/13 
 Pct Recovery = 78%  Analysis Date = 03/16/13 
 Pct Recovery = 78%  Analysis Date = 03/16/13 
 Pct Recovery = 78%  Analysis Date = 03/14/13 
 Pct Recovery = 79%  Analysis Date = 03/14/13 
 Pct Recovery = 79%  Analysis Date = 03/11/13 
 Pct Recovery = 79%  Analysis Date = 03/11/13 
 Pct Recovery = 79%  Analysis Date = 03/09/13 
 Pct Recovery = 79%  Analysis Date = 03/09/13 
 Pct Recovery = 79%  Analysis Date = 03/07/13 
 Pct Recovery = 80%  Analysis Date = 03/07/13 
 Pct Recovery = 80%  Analysis Date = 03/04/13 
 Pct Recovery = 80%  Analysis Date = 03/04/13 
 Pct Recovery = 80%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 03/02/13 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 Pct Recovery = 81%  Analysis Date = 02/25/13 
 Pct Recovery = 81%  Analysis Date = 02/25/13 
 Pct Recovery = 81%  Analysis Date = 02/23/13 
 Pct Recovery = 82%  Analysis Date = 02/23/13 
 Pct Recovery = 82%  Analysis Date = 02/21/13 
 Pct Recovery = 82%  Analysis Date = 02/21/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/14/13 
 Pct Recovery = 82%  Analysis Date = 02/14/13 
 Pct Recovery = 82%  Analysis Date = 02/12/13 
 Pct Recovery = 83%  Analysis Date = 02/12/13 
 Pct Recovery = 83%  Analysis Date = 02/09/13 
 Pct Recovery = 83%  Analysis Date = 02/09/13 
 Pct Recovery = 83%  Analysis Date = 02/07/13 
 Pct Recovery = 83%  Analysis Date = 02/07/13 
 Pct Recovery = 83%  Analysis Date = 02/05/13 
 Pct Recovery = 83%  Analysis Date = 02/05/13 
 Pct Recovery = 83%  Analysis Date = 02/02/13 
 Pct Recovery = 84%  Analysis Date = 02/02/13 
 Pct Recovery = 84%  Analysis Date = 01/31/13 
 Pct Recovery = 84%  Analysis Date = 01/31/13 
 Pct Recovery = 84%  Analysis Date = 01/29/13 
 Pct Recovery = 84%  Analysis Date = 01/29/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/24/13 
 Pct Recovery = 85%  Analysis Date = 01/24/13 
 Pct Recovery = 85%  Analysis Date = 01/22/13 
 Pct Recovery = 85%  Analysis Date = 01/22/13 
 Pct Recovery = 85%  Analysis Date = 01/19/13 
 Pct Recovery = 85%  Analysis Date = 01/19/13 
 Pct Recovery = 85%  Analysis Date = 01/17/13 
 Pct Recovery = 85%  Analysis Date = 01/17/13 
 Pct Recovery = 85%  Analysis Date = 01/15/13 
 Pct Recovery = 85%  Analysis Date = 01/15/13 
 Pct Recovery = 85%  Analysis Date = 01/13/13 
 Pct Recovery = 85%  Analysis Date = 01/13/13 
 Pct Recovery = 85%  Analysis Date = 01/10/13 
 Pct Recovery = 86%  Analysis Date = 01/10/13 
 Pct Recovery = 86%  Analysis Date = 01/08/13 
 Pct Recovery = 86%  Analysis Date = 01/08/13 
 Pct Recovery = 86%  Analysis Date = 01/06/13 
 Pct Recovery = 86%  Analysis Date = 01/06/13 
 Pct Recovery = 86%  Analysis Date = 01/03/13 
 Pct Recovery = 86%  Analysis Date = 01/03/13 
 Pct Recovery = 86%  Analysis Date = 01/01/13 
 Pct Recovery = 86%  Analysis Date = 01/01/13 
 Pct Recovery = 86%  Analysis Date = 12/30/12 
 Pct Recovery = 86%  Analysis Date = 12/30/12 
 Pct Recovery = 86%  Analysis Date = 12/27/12 
 Pct Recovery = 86%  Analysis Date = 12/27/12 
 Pct Recovery = 86%  Analysis Date = 12/25/12 
 Pct Recovery = 87%  Analysis Date = 12/25/12 
 Pct Recovery = 87%  Analysis Date = 12/23/12 
 Pct Recovery = 87%  Analysis Date = 12/23/12 
 Pct Recovery = 87%  Analysis Date = 12/20/12 
 Pct Recovery = 87%  Analysis Date = 12/20/12 
 Pct Recovery = 87%  Analysis Date = 12/18/12 
 Pct Recovery = 87%  Analysis Date = 12/18/12 
 Pct Recovery = 87%  Analysis Date = 12/16/12 
 Pct Recovery = 87%  Analysis Date = 12/16/12 
 Pct Recovery = 87%  Analysis Date = 12/14/12 
 Pct Recovery = 87%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATENOLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 9 75% 11% 73% 13%
Total 9 75% 11% 73% 13%

Sample Statistics
ATENOLOL

Characteristic N % % Basis
Plotted 9 82% Spiked
Estimated Values 1 9% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 2 18% 2 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
ATRAZINE
METHOD: LC9017 , TESTIDCODE: 65065LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 73%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 75%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 65%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 78%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 72%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 78%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 60%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 03/21/14 
 Pct Recovery = 70%  Analysis Date = 03/18/14 
 Pct Recovery = 70%  Analysis Date = 03/18/14 
 Pct Recovery = 70%  Analysis Date = 03/16/14 
 Pct Recovery = 70%  Analysis Date = 03/16/14 
 Pct Recovery = 70%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/11/14 
 Pct Recovery = 70%  Analysis Date = 03/11/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 69%  Analysis Date = 03/07/14 
 Pct Recovery = 69%  Analysis Date = 03/04/14 
 Pct Recovery = 69%  Analysis Date = 03/04/14 
 Pct Recovery = 69%  Analysis Date = 03/02/14 
 Pct Recovery = 69%  Analysis Date = 03/02/14 
 Pct Recovery = 69%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/16/14 
 Pct Recovery = 69%  Analysis Date = 02/16/14 
 Pct Recovery = 69%  Analysis Date = 02/14/14 
 Pct Recovery = 68%  Analysis Date = 02/14/14 
 Pct Recovery = 68%  Analysis Date = 02/12/14 
 Pct Recovery = 68%  Analysis Date = 02/12/14 
 Pct Recovery = 68%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/07/14 
 Pct Recovery = 68%  Analysis Date = 02/07/14 
 Pct Recovery = 68%  Analysis Date = 02/05/14 
 Pct Recovery = 68%  Analysis Date = 02/05/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/26/14 
 Pct Recovery = 68%  Analysis Date = 01/26/14 
 Pct Recovery = 68%  Analysis Date = 01/24/14 
 Pct Recovery = 68%  Analysis Date = 01/24/14 
 Pct Recovery = 68%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/19/14 
 Pct Recovery = 68%  Analysis Date = 01/19/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/10/14 
 Pct Recovery = 68%  Analysis Date = 01/10/14 
 Pct Recovery = 68%  Analysis Date = 01/08/14 
 Pct Recovery = 68%  Analysis Date = 01/08/14 
 Pct Recovery = 68%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/03/14 
 Pct Recovery = 68%  Analysis Date = 01/03/14 
 Pct Recovery = 68%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 12/30/13 
 Pct Recovery = 68%  Analysis Date = 12/30/13 
 Pct Recovery = 68%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/13/13 
 Pct Recovery = 69%  Analysis Date = 12/13/13 
 Pct Recovery = 69%  Analysis Date = 12/11/13 
 Pct Recovery = 69%  Analysis Date = 12/11/13 
 Pct Recovery = 69%  Analysis Date = 12/09/13 
 Pct Recovery = 69%  Analysis Date = 12/09/13 
 Pct Recovery = 69%  Analysis Date = 12/07/13 
 Pct Recovery = 69%  Analysis Date = 12/07/13 
 Pct Recovery = 69%  Analysis Date = 12/04/13 
 Pct Recovery = 69%  Analysis Date = 12/04/13 
 Pct Recovery = 69%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/27/13 
 Pct Recovery = 69%  Analysis Date = 11/27/13 
 Pct Recovery = 69%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/25/13 
 Pct Recovery = 69%  Analysis Date = 11/23/13 
 Pct Recovery = 69%  Analysis Date = 11/23/13 
 Pct Recovery = 69%  Analysis Date = 11/20/13 
 Pct Recovery = 69%  Analysis Date = 11/20/13 
 Pct Recovery = 69%  Analysis Date = 11/18/13 
 Pct Recovery = 69%  Analysis Date = 11/18/13 
 Pct Recovery = 69%  Analysis Date = 11/16/13 
 Pct Recovery = 69%  Analysis Date = 11/16/13 
 Pct Recovery = 69%  Analysis Date = 11/13/13 
 Pct Recovery = 69%  Analysis Date = 11/13/13 
 Pct Recovery = 69%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 70%  Analysis Date = 11/02/13 
 Pct Recovery = 70%  Analysis Date = 11/02/13 
 Pct Recovery = 70%  Analysis Date = 10/31/13 
 Pct Recovery = 70%  Analysis Date = 10/31/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/24/13 
 Pct Recovery = 70%  Analysis Date = 10/24/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/17/13 
 Pct Recovery = 70%  Analysis Date = 10/17/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 09/28/13 
 Pct Recovery = 70%  Analysis Date = 09/28/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/21/13 
 Pct Recovery = 70%  Analysis Date = 09/21/13 
 Pct Recovery = 70%  Analysis Date = 09/19/13 
 Pct Recovery = 70%  Analysis Date = 09/19/13 
 Pct Recovery = 70%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/15/13 
 Pct Recovery = 71%  Analysis Date = 08/15/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/11/13 
 Pct Recovery = 71%  Analysis Date = 08/11/13 
 Pct Recovery = 71%  Analysis Date = 08/08/13 
 Pct Recovery = 71%  Analysis Date = 08/08/13 
 Pct Recovery = 71%  Analysis Date = 08/06/13 
 Pct Recovery = 71%  Analysis Date = 08/06/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/23/13 
 Pct Recovery = 71%  Analysis Date = 07/23/13 
 Pct Recovery = 71%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/19/13 
 Pct Recovery = 71%  Analysis Date = 07/19/13 
 Pct Recovery = 71%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/12/13 
 Pct Recovery = 71%  Analysis Date = 07/12/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/07/13 
 Pct Recovery = 71%  Analysis Date = 07/07/13 
 Pct Recovery = 71%  Analysis Date = 07/05/13 
 Pct Recovery = 71%  Analysis Date = 07/05/13 
 Pct Recovery = 71%  Analysis Date = 07/02/13 
 Pct Recovery = 71%  Analysis Date = 07/02/13 
 Pct Recovery = 71%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/28/13 
 Pct Recovery = 70%  Analysis Date = 06/28/13 
 Pct Recovery = 70%  Analysis Date = 06/26/13 
 Pct Recovery = 70%  Analysis Date = 06/26/13 
 Pct Recovery = 70%  Analysis Date = 06/23/13 
 Pct Recovery = 70%  Analysis Date = 06/23/13 
 Pct Recovery = 70%  Analysis Date = 06/21/13 
 Pct Recovery = 70%  Analysis Date = 06/21/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 70%  Analysis Date = 06/16/13 
 Pct Recovery = 70%  Analysis Date = 06/16/13 
 Pct Recovery = 70%  Analysis Date = 06/14/13 
 Pct Recovery = 70%  Analysis Date = 06/14/13 
 Pct Recovery = 70%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/27/13 
 Pct Recovery = 70%  Analysis Date = 05/27/13 
 Pct Recovery = 70%  Analysis Date = 05/24/13 
 Pct Recovery = 70%  Analysis Date = 05/24/13 
 Pct Recovery = 70%  Analysis Date = 05/22/13 
 Pct Recovery = 70%  Analysis Date = 05/22/13 
 Pct Recovery = 70%  Analysis Date = 05/20/13 
 Pct Recovery = 70%  Analysis Date = 05/20/13 
 Pct Recovery = 70%  Analysis Date = 05/17/13 
 Pct Recovery = 70%  Analysis Date = 05/17/13 
 Pct Recovery = 70%  Analysis Date = 05/15/13 
 Pct Recovery = 70%  Analysis Date = 05/15/13 
 Pct Recovery = 70%  Analysis Date = 05/13/13 
 Pct Recovery = 70%  Analysis Date = 05/13/13 
 Pct Recovery = 70%  Analysis Date = 05/10/13 
 Pct Recovery = 70%  Analysis Date = 05/10/13 
 Pct Recovery = 70%  Analysis Date = 05/08/13 
 Pct Recovery = 70%  Analysis Date = 05/08/13 
 Pct Recovery = 70%  Analysis Date = 05/06/13 
 Pct Recovery = 70%  Analysis Date = 05/06/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 04/29/13 
 Pct Recovery = 70%  Analysis Date = 04/29/13 
 Pct Recovery = 70%  Analysis Date = 04/26/13 
 Pct Recovery = 70%  Analysis Date = 04/26/13 
 Pct Recovery = 70%  Analysis Date = 04/24/13 
 Pct Recovery = 71%  Analysis Date = 04/24/13 
 Pct Recovery = 71%  Analysis Date = 04/22/13 
 Pct Recovery = 71%  Analysis Date = 04/22/13 
 Pct Recovery = 71%  Analysis Date = 04/20/13 
 Pct Recovery = 71%  Analysis Date = 04/20/13 
 Pct Recovery = 71%  Analysis Date = 04/17/13 
 Pct Recovery = 71%  Analysis Date = 04/17/13 
 Pct Recovery = 71%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/13/13 
 Pct Recovery = 71%  Analysis Date = 04/13/13 
 Pct Recovery = 71%  Analysis Date = 04/10/13 
 Pct Recovery = 71%  Analysis Date = 04/10/13 
 Pct Recovery = 71%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/06/13 
 Pct Recovery = 72%  Analysis Date = 04/06/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 Pct Recovery = 72%  Analysis Date = 03/25/13 
 Pct Recovery = 73%  Analysis Date = 03/25/13 
 Pct Recovery = 73%  Analysis Date = 03/23/13 
 Pct Recovery = 73%  Analysis Date = 03/23/13 
 Pct Recovery = 73%  Analysis Date = 03/21/13 
 Pct Recovery = 73%  Analysis Date = 03/21/13 
 Pct Recovery = 73%  Analysis Date = 03/18/13 
 Pct Recovery = 73%  Analysis Date = 03/18/13 
 Pct Recovery = 73%  Analysis Date = 03/16/13 
 Pct Recovery = 73%  Analysis Date = 03/16/13 
 Pct Recovery = 73%  Analysis Date = 03/14/13 
 Pct Recovery = 73%  Analysis Date = 03/14/13 
 Pct Recovery = 73%  Analysis Date = 03/11/13 
 Pct Recovery = 73%  Analysis Date = 03/11/13 
 Pct Recovery = 73%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/07/13 
 Pct Recovery = 74%  Analysis Date = 03/07/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 Pct Recovery = 74%  Analysis Date = 02/25/13 
 Pct Recovery = 74%  Analysis Date = 02/25/13 
 Pct Recovery = 74%  Analysis Date = 02/23/13 
 Pct Recovery = 74%  Analysis Date = 02/23/13 
 Pct Recovery = 74%  Analysis Date = 02/21/13 
 Pct Recovery = 75%  Analysis Date = 02/21/13 
 Pct Recovery = 75%  Analysis Date = 02/18/13 
 Pct Recovery = 75%  Analysis Date = 02/18/13 
 Pct Recovery = 75%  Analysis Date = 02/16/13 
 Pct Recovery = 75%  Analysis Date = 02/16/13 
 Pct Recovery = 75%  Analysis Date = 02/14/13 
 Pct Recovery = 75%  Analysis Date = 02/14/13 
 Pct Recovery = 75%  Analysis Date = 02/12/13 
 Pct Recovery = 75%  Analysis Date = 02/12/13 
 Pct Recovery = 75%  Analysis Date = 02/09/13 
 Pct Recovery = 75%  Analysis Date = 02/09/13 
 Pct Recovery = 75%  Analysis Date = 02/07/13 
 Pct Recovery = 75%  Analysis Date = 02/07/13 
 Pct Recovery = 75%  Analysis Date = 02/05/13 
 Pct Recovery = 75%  Analysis Date = 02/05/13 
 Pct Recovery = 75%  Analysis Date = 02/02/13 
 Pct Recovery = 76%  Analysis Date = 02/02/13 
 Pct Recovery = 76%  Analysis Date = 01/31/13 
 Pct Recovery = 76%  Analysis Date = 01/31/13 
 Pct Recovery = 76%  Analysis Date = 01/29/13 
 Pct Recovery = 76%  Analysis Date = 01/29/13 
 Pct Recovery = 76%  Analysis Date = 01/26/13 
 Pct Recovery = 76%  Analysis Date = 01/26/13 
 Pct Recovery = 76%  Analysis Date = 01/24/13 
 Pct Recovery = 76%  Analysis Date = 01/24/13 
 Pct Recovery = 76%  Analysis Date = 01/22/13 
 Pct Recovery = 76%  Analysis Date = 01/22/13 
 Pct Recovery = 76%  Analysis Date = 01/19/13 
 Pct Recovery = 76%  Analysis Date = 01/19/13 
 Pct Recovery = 76%  Analysis Date = 01/17/13 
 Pct Recovery = 76%  Analysis Date = 01/17/13 
 Pct Recovery = 76%  Analysis Date = 01/15/13 
 Pct Recovery = 76%  Analysis Date = 01/15/13 
 Pct Recovery = 76%  Analysis Date = 01/13/13 
 Pct Recovery = 77%  Analysis Date = 01/13/13 
 Pct Recovery = 77%  Analysis Date = 01/10/13 
 Pct Recovery = 77%  Analysis Date = 01/10/13 
 Pct Recovery = 77%  Analysis Date = 01/08/13 
 Pct Recovery = 77%  Analysis Date = 01/08/13 
 Pct Recovery = 77%  Analysis Date = 01/06/13 
 Pct Recovery = 77%  Analysis Date = 01/06/13 
 Pct Recovery = 77%  Analysis Date = 01/03/13 
 Pct Recovery = 77%  Analysis Date = 01/03/13 
 Pct Recovery = 77%  Analysis Date = 01/01/13 
 Pct Recovery = 77%  Analysis Date = 01/01/13 
 Pct Recovery = 77%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/20/12 
 Pct Recovery = 78%  Analysis Date = 12/20/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/16/12 
 Pct Recovery = 78%  Analysis Date = 12/16/12 
 Pct Recovery = 78%  Analysis Date = 12/14/12 
 Pct Recovery = 78%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 71% 6% 73% 9%
Total 11 71% 6% 73% 9%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
BENZTROPINE
METHOD: LC9017 , TESTIDCODE: 67997LCM56

The SGPlot Procedure

Sample Statistics
BENZTROPINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
BETAMETHASONE
METHOD: LC9017 , TESTIDCODE: 67485LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 69%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 85%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 96%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 109%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 96%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 107%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 117%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 101%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 78%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 83%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 92%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 79%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 89%  Analysis Date = 03/21/14 
 Pct Recovery = 105%  Analysis Date = 03/18/14 
 Pct Recovery = 105%  Analysis Date = 03/18/14 
 Pct Recovery = 105%  Analysis Date = 03/16/14 
 Pct Recovery = 104%  Analysis Date = 03/16/14 
 Pct Recovery = 104%  Analysis Date = 03/14/14 
 Pct Recovery = 104%  Analysis Date = 03/14/14 
 Pct Recovery = 104%  Analysis Date = 03/11/14 
 Pct Recovery = 104%  Analysis Date = 03/11/14 
 Pct Recovery = 104%  Analysis Date = 03/09/14 
 Pct Recovery = 103%  Analysis Date = 03/09/14 
 Pct Recovery = 103%  Analysis Date = 03/07/14 
 Pct Recovery = 103%  Analysis Date = 03/07/14 
 Pct Recovery = 103%  Analysis Date = 03/04/14 
 Pct Recovery = 103%  Analysis Date = 03/04/14 
 Pct Recovery = 103%  Analysis Date = 03/02/14 
 Pct Recovery = 103%  Analysis Date = 03/02/14 
 Pct Recovery = 103%  Analysis Date = 02/28/14 
 Pct Recovery = 102%  Analysis Date = 02/28/14 
 Pct Recovery = 102%  Analysis Date = 02/25/14 
 Pct Recovery = 102%  Analysis Date = 02/25/14 
 Pct Recovery = 102%  Analysis Date = 02/23/14 
 Pct Recovery = 102%  Analysis Date = 02/23/14 
 Pct Recovery = 102%  Analysis Date = 02/21/14 
 Pct Recovery = 101%  Analysis Date = 02/21/14 
 Pct Recovery = 101%  Analysis Date = 02/18/14 
 Pct Recovery = 101%  Analysis Date = 02/18/14 
 Pct Recovery = 101%  Analysis Date = 02/16/14 
 Pct Recovery = 101%  Analysis Date = 02/16/14 
 Pct Recovery = 101%  Analysis Date = 02/14/14 
 Pct Recovery = 101%  Analysis Date = 02/14/14 
 Pct Recovery = 101%  Analysis Date = 02/12/14 
 Pct Recovery = 100%  Analysis Date = 02/12/14 
 Pct Recovery = 100%  Analysis Date = 02/09/14 
 Pct Recovery = 100%  Analysis Date = 02/09/14 
 Pct Recovery = 100%  Analysis Date = 02/07/14 
 Pct Recovery = 100%  Analysis Date = 02/07/14 
 Pct Recovery = 100%  Analysis Date = 02/05/14 
 Pct Recovery = 100%  Analysis Date = 02/05/14 
 Pct Recovery = 100%  Analysis Date = 02/02/14 
 Pct Recovery = 99%  Analysis Date = 02/02/14 
 Pct Recovery = 99%  Analysis Date = 01/31/14 
 Pct Recovery = 99%  Analysis Date = 01/31/14 
 Pct Recovery = 99%  Analysis Date = 01/29/14 
 Pct Recovery = 99%  Analysis Date = 01/29/14 
 Pct Recovery = 99%  Analysis Date = 01/26/14 
 Pct Recovery = 99%  Analysis Date = 01/26/14 
 Pct Recovery = 99%  Analysis Date = 01/24/14 
 Pct Recovery = 98%  Analysis Date = 01/24/14 
 Pct Recovery = 98%  Analysis Date = 01/22/14 
 Pct Recovery = 98%  Analysis Date = 01/22/14 
 Pct Recovery = 98%  Analysis Date = 01/19/14 
 Pct Recovery = 98%  Analysis Date = 01/19/14 
 Pct Recovery = 98%  Analysis Date = 01/17/14 
 Pct Recovery = 98%  Analysis Date = 01/17/14 
 Pct Recovery = 98%  Analysis Date = 01/15/14 
 Pct Recovery = 97%  Analysis Date = 01/15/14 
 Pct Recovery = 97%  Analysis Date = 01/13/14 
 Pct Recovery = 97%  Analysis Date = 01/13/14 
 Pct Recovery = 97%  Analysis Date = 01/10/14 
 Pct Recovery = 97%  Analysis Date = 01/10/14 
 Pct Recovery = 97%  Analysis Date = 01/08/14 
 Pct Recovery = 97%  Analysis Date = 01/08/14 
 Pct Recovery = 97%  Analysis Date = 01/06/14 
 Pct Recovery = 96%  Analysis Date = 01/06/14 
 Pct Recovery = 96%  Analysis Date = 01/03/14 
 Pct Recovery = 96%  Analysis Date = 01/03/14 
 Pct Recovery = 96%  Analysis Date = 01/01/14 
 Pct Recovery = 96%  Analysis Date = 01/01/14 
 Pct Recovery = 96%  Analysis Date = 12/30/13 
 Pct Recovery = 96%  Analysis Date = 12/30/13 
 Pct Recovery = 96%  Analysis Date = 12/27/13 
 Pct Recovery = 95%  Analysis Date = 12/27/13 
 Pct Recovery = 95%  Analysis Date = 12/25/13 
 Pct Recovery = 95%  Analysis Date = 12/25/13 
 Pct Recovery = 95%  Analysis Date = 12/23/13 
 Pct Recovery = 95%  Analysis Date = 12/23/13 
 Pct Recovery = 95%  Analysis Date = 12/20/13 
 Pct Recovery = 95%  Analysis Date = 12/20/13 
 Pct Recovery = 95%  Analysis Date = 12/18/13 
 Pct Recovery = 94%  Analysis Date = 12/18/13 
 Pct Recovery = 94%  Analysis Date = 12/16/13 
 Pct Recovery = 94%  Analysis Date = 12/16/13 
 Pct Recovery = 94%  Analysis Date = 12/13/13 
 Pct Recovery = 94%  Analysis Date = 12/13/13 
 Pct Recovery = 94%  Analysis Date = 12/11/13 
 Pct Recovery = 94%  Analysis Date = 12/11/13 
 Pct Recovery = 94%  Analysis Date = 12/09/13 
 Pct Recovery = 94%  Analysis Date = 12/09/13 
 Pct Recovery = 94%  Analysis Date = 12/07/13 
 Pct Recovery = 93%  Analysis Date = 12/07/13 
 Pct Recovery = 93%  Analysis Date = 12/04/13 
 Pct Recovery = 93%  Analysis Date = 12/04/13 
 Pct Recovery = 93%  Analysis Date = 12/02/13 
 Pct Recovery = 93%  Analysis Date = 12/02/13 
 Pct Recovery = 93%  Analysis Date = 11/30/13 
 Pct Recovery = 93%  Analysis Date = 11/30/13 
 Pct Recovery = 93%  Analysis Date = 11/27/13 
 Pct Recovery = 92%  Analysis Date = 11/27/13 
 Pct Recovery = 92%  Analysis Date = 11/25/13 
 Pct Recovery = 92%  Analysis Date = 11/25/13 
 Pct Recovery = 92%  Analysis Date = 11/23/13 
 Pct Recovery = 92%  Analysis Date = 11/23/13 
 Pct Recovery = 92%  Analysis Date = 11/20/13 
 Pct Recovery = 92%  Analysis Date = 11/20/13 
 Pct Recovery = 92%  Analysis Date = 11/18/13 
 Pct Recovery = 92%  Analysis Date = 11/18/13 
 Pct Recovery = 92%  Analysis Date = 11/16/13 
 Pct Recovery = 91%  Analysis Date = 11/16/13 
 Pct Recovery = 91%  Analysis Date = 11/13/13 
 Pct Recovery = 91%  Analysis Date = 11/13/13 
 Pct Recovery = 91%  Analysis Date = 11/11/13 
 Pct Recovery = 91%  Analysis Date = 11/11/13 
 Pct Recovery = 91%  Analysis Date = 11/09/13 
 Pct Recovery = 91%  Analysis Date = 11/09/13 
 Pct Recovery = 91%  Analysis Date = 11/07/13 
 Pct Recovery = 91%  Analysis Date = 11/07/13 
 Pct Recovery = 91%  Analysis Date = 11/04/13 
 Pct Recovery = 90%  Analysis Date = 11/04/13 
 Pct Recovery = 90%  Analysis Date = 11/02/13 
 Pct Recovery = 90%  Analysis Date = 11/02/13 
 Pct Recovery = 90%  Analysis Date = 10/31/13 
 Pct Recovery = 90%  Analysis Date = 10/31/13 
 Pct Recovery = 90%  Analysis Date = 10/28/13 
 Pct Recovery = 90%  Analysis Date = 10/28/13 
 Pct Recovery = 90%  Analysis Date = 10/26/13 
 Pct Recovery = 90%  Analysis Date = 10/26/13 
 Pct Recovery = 90%  Analysis Date = 10/24/13 
 Pct Recovery = 89%  Analysis Date = 10/24/13 
 Pct Recovery = 89%  Analysis Date = 10/21/13 
 Pct Recovery = 89%  Analysis Date = 10/21/13 
 Pct Recovery = 89%  Analysis Date = 10/19/13 
 Pct Recovery = 89%  Analysis Date = 10/19/13 
 Pct Recovery = 89%  Analysis Date = 10/17/13 
 Pct Recovery = 89%  Analysis Date = 10/17/13 
 Pct Recovery = 89%  Analysis Date = 10/14/13 
 Pct Recovery = 89%  Analysis Date = 10/14/13 
 Pct Recovery = 89%  Analysis Date = 10/12/13 
 Pct Recovery = 88%  Analysis Date = 10/12/13 
 Pct Recovery = 88%  Analysis Date = 10/10/13 
 Pct Recovery = 88%  Analysis Date = 10/10/13 
 Pct Recovery = 88%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/05/13 
 Pct Recovery = 88%  Analysis Date = 10/05/13 
 Pct Recovery = 88%  Analysis Date = 10/03/13 
 Pct Recovery = 88%  Analysis Date = 10/03/13 
 Pct Recovery = 88%  Analysis Date = 10/01/13 
 Pct Recovery = 88%  Analysis Date = 10/01/13 
 Pct Recovery = 88%  Analysis Date = 09/28/13 
 Pct Recovery = 87%  Analysis Date = 09/28/13 
 Pct Recovery = 87%  Analysis Date = 09/26/13 
 Pct Recovery = 87%  Analysis Date = 09/26/13 
 Pct Recovery = 87%  Analysis Date = 09/24/13 
 Pct Recovery = 87%  Analysis Date = 09/24/13 
 Pct Recovery = 87%  Analysis Date = 09/21/13 
 Pct Recovery = 87%  Analysis Date = 09/21/13 
 Pct Recovery = 87%  Analysis Date = 09/19/13 
 Pct Recovery = 87%  Analysis Date = 09/19/13 
 Pct Recovery = 87%  Analysis Date = 09/17/13 
 Pct Recovery = 86%  Analysis Date = 09/17/13 
 Pct Recovery = 86%  Analysis Date = 09/14/13 
 Pct Recovery = 86%  Analysis Date = 09/14/13 
 Pct Recovery = 86%  Analysis Date = 09/12/13 
 Pct Recovery = 86%  Analysis Date = 09/12/13 
 Pct Recovery = 86%  Analysis Date = 09/10/13 
 Pct Recovery = 86%  Analysis Date = 09/10/13 
 Pct Recovery = 86%  Analysis Date = 09/07/13 
 Pct Recovery = 86%  Analysis Date = 09/07/13 
 Pct Recovery = 86%  Analysis Date = 09/05/13 
 Pct Recovery = 85%  Analysis Date = 09/05/13 
 Pct Recovery = 85%  Analysis Date = 09/03/13 
 Pct Recovery = 85%  Analysis Date = 09/03/13 
 Pct Recovery = 85%  Analysis Date = 09/01/13 
 Pct Recovery = 85%  Analysis Date = 09/01/13 
 Pct Recovery = 85%  Analysis Date = 08/29/13 
 Pct Recovery = 85%  Analysis Date = 08/29/13 
 Pct Recovery = 85%  Analysis Date = 08/27/13 
 Pct Recovery = 85%  Analysis Date = 08/27/13 
 Pct Recovery = 85%  Analysis Date = 08/25/13 
 Pct Recovery = 84%  Analysis Date = 08/25/13 
 Pct Recovery = 84%  Analysis Date = 08/22/13 
 Pct Recovery = 84%  Analysis Date = 08/22/13 
 Pct Recovery = 84%  Analysis Date = 08/20/13 
 Pct Recovery = 84%  Analysis Date = 08/20/13 
 Pct Recovery = 84%  Analysis Date = 08/18/13 
 Pct Recovery = 84%  Analysis Date = 08/18/13 
 Pct Recovery = 84%  Analysis Date = 08/15/13 
 Pct Recovery = 83%  Analysis Date = 08/15/13 
 Pct Recovery = 83%  Analysis Date = 08/13/13 
 Pct Recovery = 83%  Analysis Date = 08/13/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/08/13 
 Pct Recovery = 83%  Analysis Date = 08/08/13 
 Pct Recovery = 83%  Analysis Date = 08/06/13 
 Pct Recovery = 83%  Analysis Date = 08/06/13 
 Pct Recovery = 83%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/19/13 
 Pct Recovery = 82%  Analysis Date = 07/19/13 
 Pct Recovery = 82%  Analysis Date = 07/16/13 
 Pct Recovery = 82%  Analysis Date = 07/16/13 
 Pct Recovery = 82%  Analysis Date = 07/14/13 
 Pct Recovery = 82%  Analysis Date = 07/14/13 
 Pct Recovery = 82%  Analysis Date = 07/12/13 
 Pct Recovery = 82%  Analysis Date = 07/12/13 
 Pct Recovery = 82%  Analysis Date = 07/09/13 
 Pct Recovery = 82%  Analysis Date = 07/09/13 
 Pct Recovery = 82%  Analysis Date = 07/07/13 
 Pct Recovery = 82%  Analysis Date = 07/07/13 
 Pct Recovery = 82%  Analysis Date = 07/05/13 
 Pct Recovery = 82%  Analysis Date = 07/05/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 06/30/13 
 Pct Recovery = 82%  Analysis Date = 06/30/13 
 Pct Recovery = 82%  Analysis Date = 06/28/13 
 Pct Recovery = 82%  Analysis Date = 06/28/13 
 Pct Recovery = 82%  Analysis Date = 06/26/13 
 Pct Recovery = 82%  Analysis Date = 06/26/13 
 Pct Recovery = 82%  Analysis Date = 06/23/13 
 Pct Recovery = 82%  Analysis Date = 06/23/13 
 Pct Recovery = 82%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/16/13 
 Pct Recovery = 82%  Analysis Date = 06/16/13 
 Pct Recovery = 82%  Analysis Date = 06/14/13 
 Pct Recovery = 82%  Analysis Date = 06/14/13 
 Pct Recovery = 82%  Analysis Date = 06/12/13 
 Pct Recovery = 82%  Analysis Date = 06/12/13 
 Pct Recovery = 82%  Analysis Date = 06/09/13 
 Pct Recovery = 82%  Analysis Date = 06/09/13 
 Pct Recovery = 82%  Analysis Date = 06/07/13 
 Pct Recovery = 82%  Analysis Date = 06/07/13 
 Pct Recovery = 82%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/02/13 
 Pct Recovery = 82%  Analysis Date = 06/02/13 
 Pct Recovery = 82%  Analysis Date = 05/31/13 
 Pct Recovery = 82%  Analysis Date = 05/31/13 
 Pct Recovery = 82%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/27/13 
 Pct Recovery = 82%  Analysis Date = 05/27/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/20/13 
 Pct Recovery = 82%  Analysis Date = 05/20/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/15/13 
 Pct Recovery = 82%  Analysis Date = 05/15/13 
 Pct Recovery = 82%  Analysis Date = 05/13/13 
 Pct Recovery = 82%  Analysis Date = 05/13/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/08/13 
 Pct Recovery = 82%  Analysis Date = 05/08/13 
 Pct Recovery = 82%  Analysis Date = 05/06/13 
 Pct Recovery = 82%  Analysis Date = 05/06/13 
 Pct Recovery = 82%  Analysis Date = 05/03/13 
 Pct Recovery = 82%  Analysis Date = 05/03/13 
 Pct Recovery = 82%  Analysis Date = 05/01/13 
 Pct Recovery = 82%  Analysis Date = 05/01/13 
 Pct Recovery = 82%  Analysis Date = 04/29/13 
 Pct Recovery = 83%  Analysis Date = 04/29/13 
 Pct Recovery = 83%  Analysis Date = 04/26/13 
 Pct Recovery = 83%  Analysis Date = 04/26/13 
 Pct Recovery = 83%  Analysis Date = 04/24/13 
 Pct Recovery = 83%  Analysis Date = 04/24/13 
 Pct Recovery = 83%  Analysis Date = 04/22/13 
 Pct Recovery = 84%  Analysis Date = 04/22/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/17/13 
 Pct Recovery = 84%  Analysis Date = 04/17/13 
 Pct Recovery = 84%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/06/13 
 Pct Recovery = 86%  Analysis Date = 04/06/13 
 Pct Recovery = 86%  Analysis Date = 04/03/13 
 Pct Recovery = 87%  Analysis Date = 04/03/13 
 Pct Recovery = 87%  Analysis Date = 04/01/13 
 Pct Recovery = 87%  Analysis Date = 04/01/13 
 Pct Recovery = 87%  Analysis Date = 03/30/13 
 Pct Recovery = 87%  Analysis Date = 03/30/13 
 Pct Recovery = 87%  Analysis Date = 03/27/13 
 Pct Recovery = 88%  Analysis Date = 03/27/13 
 Pct Recovery = 88%  Analysis Date = 03/25/13 
 Pct Recovery = 88%  Analysis Date = 03/25/13 
 Pct Recovery = 88%  Analysis Date = 03/23/13 
 Pct Recovery = 88%  Analysis Date = 03/23/13 
 Pct Recovery = 88%  Analysis Date = 03/21/13 
 Pct Recovery = 88%  Analysis Date = 03/21/13 
 Pct Recovery = 88%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/16/13 
 Pct Recovery = 89%  Analysis Date = 03/16/13 
 Pct Recovery = 89%  Analysis Date = 03/14/13 
 Pct Recovery = 89%  Analysis Date = 03/14/13 
 Pct Recovery = 89%  Analysis Date = 03/11/13 
 Pct Recovery = 89%  Analysis Date = 03/11/13 
 Pct Recovery = 89%  Analysis Date = 03/09/13 
 Pct Recovery = 90%  Analysis Date = 03/09/13 
 Pct Recovery = 90%  Analysis Date = 03/07/13 
 Pct Recovery = 90%  Analysis Date = 03/07/13 
 Pct Recovery = 90%  Analysis Date = 03/04/13 
 Pct Recovery = 90%  Analysis Date = 03/04/13 
 Pct Recovery = 90%  Analysis Date = 03/02/13 
 Pct Recovery = 90%  Analysis Date = 03/02/13 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 Pct Recovery = 91%  Analysis Date = 02/28/13 
 Pct Recovery = 91%  Analysis Date = 02/25/13 
 Pct Recovery = 91%  Analysis Date = 02/25/13 
 Pct Recovery = 91%  Analysis Date = 02/23/13 
 Pct Recovery = 91%  Analysis Date = 02/23/13 
 Pct Recovery = 91%  Analysis Date = 02/21/13 
 Pct Recovery = 91%  Analysis Date = 02/21/13 
 Pct Recovery = 91%  Analysis Date = 02/18/13 
 Pct Recovery = 92%  Analysis Date = 02/18/13 
 Pct Recovery = 92%  Analysis Date = 02/16/13 
 Pct Recovery = 92%  Analysis Date = 02/16/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/12/13 
 Pct Recovery = 92%  Analysis Date = 02/12/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 93%  Analysis Date = 02/07/13 
 Pct Recovery = 93%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 01/31/13 
 Pct Recovery = 93%  Analysis Date = 01/31/13 
 Pct Recovery = 93%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 Pct Recovery = 94%  Analysis Date = 01/22/13 
 Pct Recovery = 94%  Analysis Date = 01/22/13 
 Pct Recovery = 94%  Analysis Date = 01/19/13 
 Pct Recovery = 95%  Analysis Date = 01/19/13 
 Pct Recovery = 95%  Analysis Date = 01/17/13 
 Pct Recovery = 95%  Analysis Date = 01/17/13 
 Pct Recovery = 95%  Analysis Date = 01/15/13 
 Pct Recovery = 95%  Analysis Date = 01/15/13 
 Pct Recovery = 95%  Analysis Date = 01/13/13 
 Pct Recovery = 95%  Analysis Date = 01/13/13 
 Pct Recovery = 95%  Analysis Date = 01/10/13 
 Pct Recovery = 95%  Analysis Date = 01/10/13 
 Pct Recovery = 95%  Analysis Date = 01/08/13 
 Pct Recovery = 96%  Analysis Date = 01/08/13 
 Pct Recovery = 96%  Analysis Date = 01/06/13 
 Pct Recovery = 96%  Analysis Date = 01/06/13 
 Pct Recovery = 96%  Analysis Date = 01/03/13 
 Pct Recovery = 96%  Analysis Date = 01/03/13 
 Pct Recovery = 96%  Analysis Date = 01/01/13 
 Pct Recovery = 96%  Analysis Date = 01/01/13 
 Pct Recovery = 96%  Analysis Date = 12/30/12 
 Pct Recovery = 97%  Analysis Date = 12/30/12 
 Pct Recovery = 97%  Analysis Date = 12/27/12 
 Pct Recovery = 97%  Analysis Date = 12/27/12 
 Pct Recovery = 97%  Analysis Date = 12/25/12 
 Pct Recovery = 97%  Analysis Date = 12/25/12 
 Pct Recovery = 97%  Analysis Date = 12/23/12 
 Pct Recovery = 97%  Analysis Date = 12/23/12 
 Pct Recovery = 97%  Analysis Date = 12/20/12 
 Pct Recovery = 98%  Analysis Date = 12/20/12 
 Pct Recovery = 98%  Analysis Date = 12/18/12 
 Pct Recovery = 98%  Analysis Date = 12/18/12 
 Pct Recovery = 98%  Analysis Date = 12/16/12 
 Pct Recovery = 98%  Analysis Date = 12/16/12 
 Pct Recovery = 98%  Analysis Date = 12/14/12 
 Pct Recovery = 98%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
BETAMETHASONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 92% 14% 91% 14%
Total 14 92% 14% 91% 14%

Sample Statistics
BETAMETHASONE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 6 40% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
BUPROPION
METHOD: LC9017 , TESTIDCODE: 67439LCM56

 Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 48%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 38%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 35%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 30%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 41%  Analysis Date = 03/20/14 
 Pct Recovery = 38%  Analysis Date = 03/18/14 
 Pct Recovery = 38%  Analysis Date = 03/18/14 
 Pct Recovery = 38%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/14/14 
 Pct Recovery = 38%  Analysis Date = 03/14/14 
 Pct Recovery = 38%  Analysis Date = 03/12/14 
 Pct Recovery = 37%  Analysis Date = 03/12/14 
 Pct Recovery = 37%  Analysis Date = 03/10/14 
 Pct Recovery = 37%  Analysis Date = 03/10/14 
 Pct Recovery = 37%  Analysis Date = 03/08/14 
 Pct Recovery = 37%  Analysis Date = 03/08/14 
 Pct Recovery = 37%  Analysis Date = 03/06/14 
 Pct Recovery = 37%  Analysis Date = 03/06/14 
 Pct Recovery = 37%  Analysis Date = 03/04/14 
 Pct Recovery = 37%  Analysis Date = 03/04/14 
 Pct Recovery = 37%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/25/14 
 Pct Recovery = 36%  Analysis Date = 02/25/14 
 Pct Recovery = 36%  Analysis Date = 02/23/14 
 Pct Recovery = 36%  Analysis Date = 02/23/14 
 Pct Recovery = 36%  Analysis Date = 02/21/14 
 Pct Recovery = 36%  Analysis Date = 02/21/14 
 Pct Recovery = 36%  Analysis Date = 02/19/14 
 Pct Recovery = 35%  Analysis Date = 02/19/14 
 Pct Recovery = 35%  Analysis Date = 02/17/14 
 Pct Recovery = 35%  Analysis Date = 02/17/14 
 Pct Recovery = 35%  Analysis Date = 02/15/14 
 Pct Recovery = 35%  Analysis Date = 02/15/14 
 Pct Recovery = 35%  Analysis Date = 02/13/14 
 Pct Recovery = 35%  Analysis Date = 02/13/14 
 Pct Recovery = 35%  Analysis Date = 02/11/14 
 Pct Recovery = 34%  Analysis Date = 02/11/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/06/14 
 Pct Recovery = 34%  Analysis Date = 02/06/14 
 Pct Recovery = 34%  Analysis Date = 02/04/14 
 Pct Recovery = 33%  Analysis Date = 02/04/14 
 Pct Recovery = 33%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 32%  Analysis Date = 01/29/14 
 Pct Recovery = 32%  Analysis Date = 01/27/14 
 Pct Recovery = 32%  Analysis Date = 01/27/14 
 Pct Recovery = 32%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/23/14 
 Pct Recovery = 32%  Analysis Date = 01/23/14 
 Pct Recovery = 32%  Analysis Date = 01/21/14 
 Pct Recovery = 31%  Analysis Date = 01/21/14 
 Pct Recovery = 31%  Analysis Date = 01/18/14 
 Pct Recovery = 31%  Analysis Date = 01/18/14 
 Pct Recovery = 31%  Analysis Date = 01/16/14 
 Pct Recovery = 31%  Analysis Date = 01/16/14 
 Pct Recovery = 31%  Analysis Date = 01/14/14 
 Pct Recovery = 31%  Analysis Date = 01/14/14 
 Pct Recovery = 31%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/10/14 
 Pct Recovery = 31%  Analysis Date = 01/10/14 
 Pct Recovery = 31%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/06/14 
 Pct Recovery = 32%  Analysis Date = 01/06/14 
 Pct Recovery = 32%  Analysis Date = 01/04/14 
 Pct Recovery = 33%  Analysis Date = 01/04/14 
 Pct Recovery = 33%  Analysis Date = 01/02/14 
 Pct Recovery = 33%  Analysis Date = 01/02/14 
 Pct Recovery = 33%  Analysis Date = 12/31/13 
 Pct Recovery = 33%  Analysis Date = 12/31/13 
 Pct Recovery = 33%  Analysis Date = 12/28/13 
 Pct Recovery = 34%  Analysis Date = 12/28/13 
 Pct Recovery = 34%  Analysis Date = 12/26/13 
 Pct Recovery = 34%  Analysis Date = 12/26/13 
 Pct Recovery = 34%  Analysis Date = 12/24/13 
 Pct Recovery = 35%  Analysis Date = 12/24/13 
 Pct Recovery = 35%  Analysis Date = 12/22/13 
 Pct Recovery = 35%  Analysis Date = 12/22/13 
 Pct Recovery = 35%  Analysis Date = 12/20/13 
 Pct Recovery = 35%  Analysis Date = 12/20/13 
 Pct Recovery = 35%  Analysis Date = 12/18/13 
 Pct Recovery = 36%  Analysis Date = 12/18/13 
 Pct Recovery = 36%  Analysis Date = 12/16/13 
 Pct Recovery = 36%  Analysis Date = 12/16/13 
 Pct Recovery = 36%  Analysis Date = 12/14/13 
 Pct Recovery = 36%  Analysis Date = 12/14/13 
 Pct Recovery = 36%  Analysis Date = 12/12/13 
 Pct Recovery = 37%  Analysis Date = 12/12/13 
 Pct Recovery = 37%  Analysis Date = 12/09/13 
 Pct Recovery = 37%  Analysis Date = 12/09/13 
 Pct Recovery = 37%  Analysis Date = 12/07/13 
 Pct Recovery = 38%  Analysis Date = 12/07/13 
 Pct Recovery = 38%  Analysis Date = 12/05/13 
 Pct Recovery = 38%  Analysis Date = 12/05/13 
 Pct Recovery = 38%  Analysis Date = 12/03/13 
 Pct Recovery = 38%  Analysis Date = 12/03/13 
 Pct Recovery = 38%  Analysis Date = 12/01/13 
 Pct Recovery = 39%  Analysis Date = 12/01/13 
 Pct Recovery = 39%  Analysis Date = 11/29/13 
 Pct Recovery = 39%  Analysis Date = 11/29/13 
 Pct Recovery = 39%  Analysis Date = 11/27/13 
 Pct Recovery = 39%  Analysis Date = 11/27/13 
 Pct Recovery = 39%  Analysis Date = 11/25/13 
 Pct Recovery = 40%  Analysis Date = 11/25/13 
 Pct Recovery = 40%  Analysis Date = 11/23/13 
 Pct Recovery = 40%  Analysis Date = 11/23/13 
 Pct Recovery = 40%  Analysis Date = 11/21/13 
 Pct Recovery = 41%  Analysis Date = 11/21/13 
 Pct Recovery = 41%  Analysis Date = 11/18/13 
 Pct Recovery = 41%  Analysis Date = 11/18/13 
 Pct Recovery = 41%  Analysis Date = 11/16/13 
 Pct Recovery = 41%  Analysis Date = 11/16/13 
 Pct Recovery = 41%  Analysis Date = 11/14/13 
 Pct Recovery = 41%  Analysis Date = 11/14/13 
 Pct Recovery = 41%  Analysis Date = 11/12/13 
 Pct Recovery = 41%  Analysis Date = 11/12/13 
 Pct Recovery = 41%  Analysis Date = 11/10/13 
 Pct Recovery = 41%  Analysis Date = 11/10/13 
 Pct Recovery = 41%  Analysis Date = 11/08/13 
 Pct Recovery = 41%  Analysis Date = 11/08/13 
 Pct Recovery = 41%  Analysis Date = 11/06/13 
 Pct Recovery = 41%  Analysis Date = 11/06/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/02/13 
 Pct Recovery = 41%  Analysis Date = 11/02/13 
 Pct Recovery = 41%  Analysis Date = 10/30/13 
 Pct Recovery = 41%  Analysis Date = 10/30/13 
 Pct Recovery = 41%  Analysis Date = 10/28/13 
 Pct Recovery = 41%  Analysis Date = 10/28/13 
 Pct Recovery = 41%  Analysis Date = 10/26/13 
 Pct Recovery = 41%  Analysis Date = 10/26/13 
 Pct Recovery = 41%  Analysis Date = 10/24/13 
 Pct Recovery = 41%  Analysis Date = 10/24/13 
 Pct Recovery = 41%  Analysis Date = 10/22/13 
 Pct Recovery = 41%  Analysis Date = 10/22/13 
 Pct Recovery = 41%  Analysis Date = 10/20/13 
 Pct Recovery = 42%  Analysis Date = 10/20/13 
 Pct Recovery = 42%  Analysis Date = 10/18/13 
 Pct Recovery = 42%  Analysis Date = 10/18/13 
 Pct Recovery = 42%  Analysis Date = 10/16/13 
 Pct Recovery = 42%  Analysis Date = 10/16/13 
 Pct Recovery = 42%  Analysis Date = 10/14/13 
 Pct Recovery = 42%  Analysis Date = 10/14/13 
 Pct Recovery = 42%  Analysis Date = 10/12/13 
 Pct Recovery = 42%  Analysis Date = 10/12/13 
 Pct Recovery = 42%  Analysis Date = 10/09/13 
 Pct Recovery = 42%  Analysis Date = 10/09/13 
 Pct Recovery = 42%  Analysis Date = 10/07/13 
 Pct Recovery = 42%  Analysis Date = 10/07/13 
 Pct Recovery = 42%  Analysis Date = 10/05/13 
 Pct Recovery = 42%  Analysis Date = 10/05/13 
 Pct Recovery = 42%  Analysis Date = 10/03/13 
 Pct Recovery = 42%  Analysis Date = 10/03/13 
 Pct Recovery = 42%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 09/29/13 
 Pct Recovery = 42%  Analysis Date = 09/29/13 
 Pct Recovery = 42%  Analysis Date = 09/27/13 
 Pct Recovery = 42%  Analysis Date = 09/27/13 
 Pct Recovery = 42%  Analysis Date = 09/25/13 
 Pct Recovery = 42%  Analysis Date = 09/25/13 
 Pct Recovery = 42%  Analysis Date = 09/23/13 
 Pct Recovery = 42%  Analysis Date = 09/23/13 
 Pct Recovery = 42%  Analysis Date = 09/20/13 
 Pct Recovery = 42%  Analysis Date = 09/20/13 
 Pct Recovery = 42%  Analysis Date = 09/18/13 
 Pct Recovery = 42%  Analysis Date = 09/18/13 
 Pct Recovery = 42%  Analysis Date = 09/16/13 
 Pct Recovery = 42%  Analysis Date = 09/16/13 
 Pct Recovery = 42%  Analysis Date = 09/14/13 
 Pct Recovery = 42%  Analysis Date = 09/14/13 
 Pct Recovery = 42%  Analysis Date = 09/12/13 
 Pct Recovery = 42%  Analysis Date = 09/12/13 
 Pct Recovery = 42%  Analysis Date = 09/10/13 
 Pct Recovery = 43%  Analysis Date = 09/10/13 
 Pct Recovery = 43%  Analysis Date = 09/08/13 
 Pct Recovery = 43%  Analysis Date = 09/08/13 
 Pct Recovery = 43%  Analysis Date = 09/06/13 
 Pct Recovery = 43%  Analysis Date = 09/06/13 
 Pct Recovery = 43%  Analysis Date = 09/04/13 
 Pct Recovery = 43%  Analysis Date = 09/04/13 
 Pct Recovery = 43%  Analysis Date = 09/02/13 
 Pct Recovery = 43%  Analysis Date = 09/02/13 
 Pct Recovery = 43%  Analysis Date = 08/30/13 
 Pct Recovery = 43%  Analysis Date = 08/30/13 
 Pct Recovery = 43%  Analysis Date = 08/28/13 
 Pct Recovery = 43%  Analysis Date = 08/28/13 
 Pct Recovery = 43%  Analysis Date = 08/26/13 
 Pct Recovery = 43%  Analysis Date = 08/26/13 
 Pct Recovery = 43%  Analysis Date = 08/24/13 
 Pct Recovery = 43%  Analysis Date = 08/24/13 
 Pct Recovery = 43%  Analysis Date = 08/22/13 
 Pct Recovery = 43%  Analysis Date = 08/22/13 
 Pct Recovery = 43%  Analysis Date = 08/20/13 
 Pct Recovery = 43%  Analysis Date = 08/20/13 
 Pct Recovery = 43%  Analysis Date = 08/18/13 
 Pct Recovery = 43%  Analysis Date = 08/18/13 
 Pct Recovery = 43%  Analysis Date = 08/16/13 
 Pct Recovery = 43%  Analysis Date = 08/16/13 
 Pct Recovery = 43%  Analysis Date = 08/14/13 
 Pct Recovery = 43%  Analysis Date = 08/14/13 
 Pct Recovery = 43%  Analysis Date = 08/11/13 
 Pct Recovery = 43%  Analysis Date = 08/11/13 
 Pct Recovery = 43%  Analysis Date = 08/09/13 
 Pct Recovery = 43%  Analysis Date = 08/09/13 
 Pct Recovery = 43%  Analysis Date = 08/07/13 
 Pct Recovery = 43%  Analysis Date = 08/07/13 
 Pct Recovery = 43%  Analysis Date = 08/05/13 
 Pct Recovery = 43%  Analysis Date = 08/05/13 
 Pct Recovery = 43%  Analysis Date = 08/03/13 
 Pct Recovery = 43%  Analysis Date = 08/03/13 
 Pct Recovery = 43%  Analysis Date = 08/01/13 
 Pct Recovery = 44%  Analysis Date = 08/01/13 
 Pct Recovery = 44%  Analysis Date = 07/30/13 
 Pct Recovery = 44%  Analysis Date = 07/30/13 
 Pct Recovery = 44%  Analysis Date = 07/28/13 
 Pct Recovery = 44%  Analysis Date = 07/28/13 
 Pct Recovery = 44%  Analysis Date = 07/26/13 
 Pct Recovery = 44%  Analysis Date = 07/26/13 
 Pct Recovery = 44%  Analysis Date = 07/24/13 
 Pct Recovery = 44%  Analysis Date = 07/24/13 
 Pct Recovery = 44%  Analysis Date = 07/21/13 
 Pct Recovery = 44%  Analysis Date = 07/21/13 
 Pct Recovery = 44%  Analysis Date = 07/19/13 
 Pct Recovery = 44%  Analysis Date = 07/19/13 
 Pct Recovery = 44%  Analysis Date = 07/17/13 
 Pct Recovery = 44%  Analysis Date = 07/17/13 
 Pct Recovery = 44%  Analysis Date = 07/15/13 
 Pct Recovery = 44%  Analysis Date = 07/15/13 
 Pct Recovery = 44%  Analysis Date = 07/13/13 
 Pct Recovery = 44%  Analysis Date = 07/13/13 
 Pct Recovery = 44%  Analysis Date = 07/11/13 
 Pct Recovery = 44%  Analysis Date = 07/11/13 
 Pct Recovery = 44%  Analysis Date = 07/09/13 
 Pct Recovery = 44%  Analysis Date = 07/09/13 
 Pct Recovery = 44%  Analysis Date = 07/07/13 
 Pct Recovery = 44%  Analysis Date = 07/07/13 
 Pct Recovery = 44%  Analysis Date = 07/05/13 
 Pct Recovery = 44%  Analysis Date = 07/05/13 
 Pct Recovery = 44%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 06/30/13 
 Pct Recovery = 44%  Analysis Date = 06/30/13 
 Pct Recovery = 44%  Analysis Date = 06/28/13 
 Pct Recovery = 44%  Analysis Date = 06/28/13 
 Pct Recovery = 44%  Analysis Date = 06/26/13 
 Pct Recovery = 44%  Analysis Date = 06/26/13 
 Pct Recovery = 44%  Analysis Date = 06/24/13 
 Pct Recovery = 44%  Analysis Date = 06/24/13 
 Pct Recovery = 44%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/20/13 
 Pct Recovery = 45%  Analysis Date = 06/20/13 
 Pct Recovery = 45%  Analysis Date = 06/18/13 
 Pct Recovery = 45%  Analysis Date = 06/18/13 
 Pct Recovery = 45%  Analysis Date = 06/16/13 
 Pct Recovery = 45%  Analysis Date = 06/16/13 
 Pct Recovery = 45%  Analysis Date = 06/14/13 
 Pct Recovery = 45%  Analysis Date = 06/14/13 
 Pct Recovery = 45%  Analysis Date = 06/11/13 
 Pct Recovery = 45%  Analysis Date = 06/11/13 
 Pct Recovery = 45%  Analysis Date = 06/09/13 
 Pct Recovery = 45%  Analysis Date = 06/09/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/03/13 
 Pct Recovery = 45%  Analysis Date = 06/03/13 
 Pct Recovery = 45%  Analysis Date = 06/01/13 
 Pct Recovery = 45%  Analysis Date = 06/01/13 
 Pct Recovery = 45%  Analysis Date = 05/30/13 
 Pct Recovery = 45%  Analysis Date = 05/30/13 
 Pct Recovery = 45%  Analysis Date = 05/28/13 
 Pct Recovery = 45%  Analysis Date = 05/28/13 
 Pct Recovery = 45%  Analysis Date = 05/26/13 
 Pct Recovery = 45%  Analysis Date = 05/26/13 
 Pct Recovery = 45%  Analysis Date = 05/23/13 
 Pct Recovery = 45%  Analysis Date = 05/23/13 
 Pct Recovery = 45%  Analysis Date = 05/21/13 
 Pct Recovery = 45%  Analysis Date = 05/21/13 
 Pct Recovery = 45%  Analysis Date = 05/19/13 
 Pct Recovery = 45%  Analysis Date = 05/19/13 
 Pct Recovery = 45%  Analysis Date = 05/17/13 
 Pct Recovery = 45%  Analysis Date = 05/17/13 
 Pct Recovery = 45%  Analysis Date = 05/15/13 
 Pct Recovery = 45%  Analysis Date = 05/15/13 
 Pct Recovery = 45%  Analysis Date = 05/13/13 
 Pct Recovery = 46%  Analysis Date = 05/13/13 
 Pct Recovery = 46%  Analysis Date = 05/11/13 
 Pct Recovery = 46%  Analysis Date = 05/11/13 
 Pct Recovery = 46%  Analysis Date = 05/09/13 
 Pct Recovery = 46%  Analysis Date = 05/09/13 
 Pct Recovery = 46%  Analysis Date = 05/07/13 
 Pct Recovery = 46%  Analysis Date = 05/07/13 
 Pct Recovery = 46%  Analysis Date = 05/05/13 
 Pct Recovery = 46%  Analysis Date = 05/05/13 
 Pct Recovery = 46%  Analysis Date = 05/02/13 
 Pct Recovery = 46%  Analysis Date = 05/02/13 
 Pct Recovery = 46%  Analysis Date = 04/30/13 
 Pct Recovery = 46%  Analysis Date = 04/30/13 
 Pct Recovery = 46%  Analysis Date = 04/28/13 
 Pct Recovery = 46%  Analysis Date = 04/28/13 
 Pct Recovery = 46%  Analysis Date = 04/26/13 
 Pct Recovery = 46%  Analysis Date = 04/26/13 
 Pct Recovery = 46%  Analysis Date = 04/24/13 
 Pct Recovery = 46%  Analysis Date = 04/24/13 
 Pct Recovery = 46%  Analysis Date = 04/22/13 
 Pct Recovery = 46%  Analysis Date = 04/22/13 
 Pct Recovery = 46%  Analysis Date = 04/20/13 
 Pct Recovery = 46%  Analysis Date = 04/20/13 
 Pct Recovery = 46%  Analysis Date = 04/18/13 
 Pct Recovery = 46%  Analysis Date = 04/18/13 
 Pct Recovery = 46%  Analysis Date = 04/16/13 
 Pct Recovery = 46%  Analysis Date = 04/16/13 
 Pct Recovery = 46%  Analysis Date = 04/13/13 
 Pct Recovery = 46%  Analysis Date = 04/13/13 
 Pct Recovery = 46%  Analysis Date = 04/11/13 
 Pct Recovery = 46%  Analysis Date = 04/11/13 
 Pct Recovery = 46%  Analysis Date = 04/09/13 
 Pct Recovery = 46%  Analysis Date = 04/09/13 
 Pct Recovery = 46%  Analysis Date = 04/07/13 
 Pct Recovery = 46%  Analysis Date = 04/07/13 
 Pct Recovery = 46%  Analysis Date = 04/05/13 
 Pct Recovery = 46%  Analysis Date = 04/05/13 
 Pct Recovery = 46%  Analysis Date = 04/03/13 
 Pct Recovery = 47%  Analysis Date = 04/03/13 
 Pct Recovery = 47%  Analysis Date = 04/01/13 
 Pct Recovery = 47%  Analysis Date = 04/01/13 
 Pct Recovery = 47%  Analysis Date = 03/30/13 
 Pct Recovery = 47%  Analysis Date = 03/30/13 
 Pct Recovery = 47%  Analysis Date = 03/28/13 
 Pct Recovery = 47%  Analysis Date = 03/28/13 
 Pct Recovery = 47%  Analysis Date = 03/26/13 
 Pct Recovery = 47%  Analysis Date = 03/26/13 
 Pct Recovery = 47%  Analysis Date = 03/23/13 
 Pct Recovery = 47%  Analysis Date = 03/23/13 
 Pct Recovery = 47%  Analysis Date = 03/21/13 
 Pct Recovery = 47%  Analysis Date = 03/21/13 
 Pct Recovery = 47%  Analysis Date = 03/19/13 
 Pct Recovery = 47%  Analysis Date = 03/19/13 
 Pct Recovery = 47%  Analysis Date = 03/17/13 
 Pct Recovery = 47%  Analysis Date = 03/17/13 
 Pct Recovery = 47%  Analysis Date = 03/15/13 
 Pct Recovery = 47%  Analysis Date = 03/15/13 
 Pct Recovery = 47%  Analysis Date = 03/13/13 
 Pct Recovery = 47%  Analysis Date = 03/13/13 
 Pct Recovery = 47%  Analysis Date = 03/11/13 
 Pct Recovery = 47%  Analysis Date = 03/11/13 
 Pct Recovery = 47%  Analysis Date = 03/09/13 
 Pct Recovery = 47%  Analysis Date = 03/09/13 
 Pct Recovery = 47%  Analysis Date = 03/07/13 
 Pct Recovery = 47%  Analysis Date = 03/07/13 
 Pct Recovery = 47%  Analysis Date = 03/04/13 
 Pct Recovery = 47%  Analysis Date = 03/04/13 
 Pct Recovery = 47%  Analysis Date = 03/02/13 
 Pct Recovery = 47%  Analysis Date = 03/02/13 
 Pct Recovery = 47%  Analysis Date = 02/28/13 
 Pct Recovery = 47%  Analysis Date = 02/28/13 
 Pct Recovery = 47%  Analysis Date = 02/26/13 
 Pct Recovery = 47%  Analysis Date = 02/26/13 
 Pct Recovery = 47%  Analysis Date = 02/24/13 
 Pct Recovery = 48%  Analysis Date = 02/24/13 
 Pct Recovery = 48%  Analysis Date = 02/22/13 
 Pct Recovery = 48%  Analysis Date = 02/22/13 
 Pct Recovery = 48%  Analysis Date = 02/20/13 
 Pct Recovery = 48%  Analysis Date = 02/20/13 
 Pct Recovery = 48%  Analysis Date = 02/18/13 
 Pct Recovery = 48%  Analysis Date = 02/18/13 
 Pct Recovery = 48%  Analysis Date = 02/16/13 
 Pct Recovery = 48%  Analysis Date = 02/16/13 
 Pct Recovery = 48%  Analysis Date = 02/14/13 
 Pct Recovery = 48%  Analysis Date = 02/14/13 
 Pct Recovery = 48%  Analysis Date = 02/11/13 
 Pct Recovery = 48%  Analysis Date = 02/11/13 
 Pct Recovery = 48%  Analysis Date = 02/09/13 
 Pct Recovery = 48%  Analysis Date = 02/09/13 
 Pct Recovery = 48%  Analysis Date = 02/07/13 
 Pct Recovery = 48%  Analysis Date = 02/07/13 
 Pct Recovery = 48%  Analysis Date = 02/05/13 
 Pct Recovery = 48%  Analysis Date = 02/05/13 
 Pct Recovery = 48%  Analysis Date = 02/03/13 
 Pct Recovery = 48%  Analysis Date = 02/03/13 
 Pct Recovery = 48%  Analysis Date = 02/01/13 
 Pct Recovery = 48%  Analysis Date = 02/01/13 
 Pct Recovery = 48%  Analysis Date = 01/30/13 
 Pct Recovery = 48%  Analysis Date = 01/30/13 
 Pct Recovery = 48%  Analysis Date = 01/28/13 
 Pct Recovery = 48%  Analysis Date = 01/28/13 
 Pct Recovery = 48%  Analysis Date = 01/26/13 
 Pct Recovery = 48%  Analysis Date = 01/26/13 
 Pct Recovery = 48%  Analysis Date = 01/24/13 
 Pct Recovery = 48%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
BUPROPION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 5 39% 7% 38% 4%
Total 5 39% 7% 38% 4%

Sample Statistics
BUPROPION

Characteristic N % % Basis
Plotted 5 83% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 1 17% 1 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
CAFFEINE
METHOD: LC9017 , TESTIDCODE: 67440LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 67%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 102%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 73%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 95%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 60%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 92%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 66%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 97%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 56%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 60%  Analysis Date = 03/21/14 
 Pct Recovery = 71%  Analysis Date = 03/18/14 
 Pct Recovery = 71%  Analysis Date = 03/18/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/14/14 
 Pct Recovery = 71%  Analysis Date = 03/14/14 
 Pct Recovery = 71%  Analysis Date = 03/11/14 
 Pct Recovery = 70%  Analysis Date = 03/11/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/16/14 
 Pct Recovery = 68%  Analysis Date = 02/16/14 
 Pct Recovery = 68%  Analysis Date = 02/14/14 
 Pct Recovery = 68%  Analysis Date = 02/14/14 
 Pct Recovery = 68%  Analysis Date = 02/12/14 
 Pct Recovery = 68%  Analysis Date = 02/12/14 
 Pct Recovery = 68%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/07/14 
 Pct Recovery = 67%  Analysis Date = 02/07/14 
 Pct Recovery = 67%  Analysis Date = 02/05/14 
 Pct Recovery = 67%  Analysis Date = 02/05/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/29/14 
 Pct Recovery = 67%  Analysis Date = 01/29/14 
 Pct Recovery = 67%  Analysis Date = 01/26/14 
 Pct Recovery = 66%  Analysis Date = 01/26/14 
 Pct Recovery = 66%  Analysis Date = 01/24/14 
 Pct Recovery = 66%  Analysis Date = 01/24/14 
 Pct Recovery = 66%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 65%  Analysis Date = 01/15/14 
 Pct Recovery = 65%  Analysis Date = 01/13/14 
 Pct Recovery = 65%  Analysis Date = 01/13/14 
 Pct Recovery = 65%  Analysis Date = 01/10/14 
 Pct Recovery = 65%  Analysis Date = 01/10/14 
 Pct Recovery = 65%  Analysis Date = 01/08/14 
 Pct Recovery = 65%  Analysis Date = 01/08/14 
 Pct Recovery = 65%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 12/30/13 
 Pct Recovery = 64%  Analysis Date = 12/30/13 
 Pct Recovery = 64%  Analysis Date = 12/27/13 
 Pct Recovery = 64%  Analysis Date = 12/27/13 
 Pct Recovery = 64%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 63%  Analysis Date = 12/18/13 
 Pct Recovery = 63%  Analysis Date = 12/16/13 
 Pct Recovery = 63%  Analysis Date = 12/16/13 
 Pct Recovery = 63%  Analysis Date = 12/13/13 
 Pct Recovery = 63%  Analysis Date = 12/13/13 
 Pct Recovery = 63%  Analysis Date = 12/11/13 
 Pct Recovery = 63%  Analysis Date = 12/11/13 
 Pct Recovery = 63%  Analysis Date = 12/09/13 
 Pct Recovery = 63%  Analysis Date = 12/09/13 
 Pct Recovery = 63%  Analysis Date = 12/07/13 
 Pct Recovery = 63%  Analysis Date = 12/07/13 
 Pct Recovery = 63%  Analysis Date = 12/04/13 
 Pct Recovery = 63%  Analysis Date = 12/04/13 
 Pct Recovery = 63%  Analysis Date = 12/02/13 
 Pct Recovery = 62%  Analysis Date = 12/02/13 
 Pct Recovery = 62%  Analysis Date = 11/30/13 
 Pct Recovery = 62%  Analysis Date = 11/30/13 
 Pct Recovery = 62%  Analysis Date = 11/27/13 
 Pct Recovery = 62%  Analysis Date = 11/27/13 
 Pct Recovery = 62%  Analysis Date = 11/25/13 
 Pct Recovery = 62%  Analysis Date = 11/25/13 
 Pct Recovery = 62%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/16/13 
 Pct Recovery = 62%  Analysis Date = 11/16/13 
 Pct Recovery = 62%  Analysis Date = 11/13/13 
 Pct Recovery = 62%  Analysis Date = 11/13/13 
 Pct Recovery = 62%  Analysis Date = 11/11/13 
 Pct Recovery = 62%  Analysis Date = 11/11/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/07/13 
 Pct Recovery = 62%  Analysis Date = 11/07/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/02/13 
 Pct Recovery = 62%  Analysis Date = 11/02/13 
 Pct Recovery = 62%  Analysis Date = 10/31/13 
 Pct Recovery = 62%  Analysis Date = 10/31/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/26/13 
 Pct Recovery = 62%  Analysis Date = 10/26/13 
 Pct Recovery = 62%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 63%  Analysis Date = 10/21/13 
 Pct Recovery = 63%  Analysis Date = 10/19/13 
 Pct Recovery = 63%  Analysis Date = 10/19/13 
 Pct Recovery = 63%  Analysis Date = 10/17/13 
 Pct Recovery = 63%  Analysis Date = 10/17/13 
 Pct Recovery = 63%  Analysis Date = 10/14/13 
 Pct Recovery = 63%  Analysis Date = 10/14/13 
 Pct Recovery = 63%  Analysis Date = 10/12/13 
 Pct Recovery = 63%  Analysis Date = 10/12/13 
 Pct Recovery = 63%  Analysis Date = 10/10/13 
 Pct Recovery = 63%  Analysis Date = 10/10/13 
 Pct Recovery = 63%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/17/13 
 Pct Recovery = 64%  Analysis Date = 09/17/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/10/13 
 Pct Recovery = 64%  Analysis Date = 09/10/13 
 Pct Recovery = 64%  Analysis Date = 09/07/13 
 Pct Recovery = 64%  Analysis Date = 09/07/13 
 Pct Recovery = 64%  Analysis Date = 09/05/13 
 Pct Recovery = 64%  Analysis Date = 09/05/13 
 Pct Recovery = 64%  Analysis Date = 09/03/13 
 Pct Recovery = 64%  Analysis Date = 09/03/13 
 Pct Recovery = 64%  Analysis Date = 09/01/13 
 Pct Recovery = 64%  Analysis Date = 09/01/13 
 Pct Recovery = 64%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 65%  Analysis Date = 08/27/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/22/13 
 Pct Recovery = 65%  Analysis Date = 08/22/13 
 Pct Recovery = 65%  Analysis Date = 08/20/13 
 Pct Recovery = 65%  Analysis Date = 08/20/13 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/15/13 
 Pct Recovery = 65%  Analysis Date = 08/15/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 66%  Analysis Date = 08/11/13 
 Pct Recovery = 66%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/02/13 
 Pct Recovery = 66%  Analysis Date = 08/02/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/07/13 
 Pct Recovery = 68%  Analysis Date = 07/07/13 
 Pct Recovery = 68%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 69%  Analysis Date = 06/26/13 
 Pct Recovery = 69%  Analysis Date = 06/23/13 
 Pct Recovery = 69%  Analysis Date = 06/23/13 
 Pct Recovery = 69%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/27/13 
 Pct Recovery = 71%  Analysis Date = 05/27/13 
 Pct Recovery = 71%  Analysis Date = 05/24/13 
 Pct Recovery = 71%  Analysis Date = 05/24/13 
 Pct Recovery = 71%  Analysis Date = 05/22/13 
 Pct Recovery = 71%  Analysis Date = 05/22/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/15/13 
 Pct Recovery = 71%  Analysis Date = 05/15/13 
 Pct Recovery = 71%  Analysis Date = 05/13/13 
 Pct Recovery = 72%  Analysis Date = 05/13/13 
 Pct Recovery = 72%  Analysis Date = 05/10/13 
 Pct Recovery = 72%  Analysis Date = 05/10/13 
 Pct Recovery = 72%  Analysis Date = 05/08/13 
 Pct Recovery = 72%  Analysis Date = 05/08/13 
 Pct Recovery = 72%  Analysis Date = 05/06/13 
 Pct Recovery = 72%  Analysis Date = 05/06/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 04/29/13 
 Pct Recovery = 73%  Analysis Date = 04/29/13 
 Pct Recovery = 73%  Analysis Date = 04/26/13 
 Pct Recovery = 73%  Analysis Date = 04/26/13 
 Pct Recovery = 73%  Analysis Date = 04/24/13 
 Pct Recovery = 74%  Analysis Date = 04/24/13 
 Pct Recovery = 74%  Analysis Date = 04/22/13 
 Pct Recovery = 75%  Analysis Date = 04/22/13 
 Pct Recovery = 75%  Analysis Date = 04/20/13 
 Pct Recovery = 75%  Analysis Date = 04/20/13 
 Pct Recovery = 75%  Analysis Date = 04/17/13 
 Pct Recovery = 76%  Analysis Date = 04/17/13 
 Pct Recovery = 76%  Analysis Date = 04/15/13 
 Pct Recovery = 76%  Analysis Date = 04/15/13 
 Pct Recovery = 76%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 78%  Analysis Date = 04/08/13 
 Pct Recovery = 78%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/25/13 
 Pct Recovery = 81%  Analysis Date = 03/25/13 
 Pct Recovery = 81%  Analysis Date = 03/23/13 
 Pct Recovery = 82%  Analysis Date = 03/23/13 
 Pct Recovery = 82%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/14/13 
 Pct Recovery = 84%  Analysis Date = 03/14/13 
 Pct Recovery = 84%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/07/13 
 Pct Recovery = 86%  Analysis Date = 03/07/13 
 Pct Recovery = 86%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/02/13 
 Pct Recovery = 87%  Analysis Date = 03/02/13 
 Pct Recovery = 87%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 91%  Analysis Date = 02/14/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 01/31/13 
 Pct Recovery = 94%  Analysis Date = 01/31/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 95%  Analysis Date = 01/26/13 
 Pct Recovery = 95%  Analysis Date = 01/24/13 
 Pct Recovery = 95%  Analysis Date = 01/24/13 
 Pct Recovery = 95%  Analysis Date = 01/22/13 
 Pct Recovery = 96%  Analysis Date = 01/22/13 
 Pct Recovery = 96%  Analysis Date = 01/19/13 
 Pct Recovery = 96%  Analysis Date = 01/19/13 
 Pct Recovery = 96%  Analysis Date = 01/17/13 
 Pct Recovery = 96%  Analysis Date = 01/17/13 
 Pct Recovery = 96%  Analysis Date = 01/15/13 
 Pct Recovery = 97%  Analysis Date = 01/15/13 
 Pct Recovery = 97%  Analysis Date = 01/13/13 
 Pct Recovery = 97%  Analysis Date = 01/13/13 
 Pct Recovery = 97%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 12/30/12 
 Pct Recovery = 100%  Analysis Date = 12/30/12 
 Pct Recovery = 100%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 102%  Analysis Date = 12/23/12 
 Pct Recovery = 102%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 103%  Analysis Date = 12/16/12 
 Pct Recovery = 103%  Analysis Date = 12/14/12 
 Pct Recovery = 103%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CAFFEINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 76% 17% 67% 26%
Total 11 76% 17% 67% 26%

Sample Statistics
CAFFEINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 2 10% 2 out of 20

OBSP Determination:
CARBAMAZEPINE
METHOD: LC9017 , TESTIDCODE: 67441LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 83%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 65%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 84%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 56%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 81%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 77%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 54%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 68%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 63%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/21/14 
 Pct Recovery = 59%  Analysis Date = 02/21/14 
 Pct Recovery = 59%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/16/14 
 Pct Recovery = 60%  Analysis Date = 02/16/14 
 Pct Recovery = 60%  Analysis Date = 02/14/14 
 Pct Recovery = 60%  Analysis Date = 02/14/14 
 Pct Recovery = 60%  Analysis Date = 02/12/14 
 Pct Recovery = 60%  Analysis Date = 02/12/14 
 Pct Recovery = 60%  Analysis Date = 02/09/14 
 Pct Recovery = 60%  Analysis Date = 02/09/14 
 Pct Recovery = 60%  Analysis Date = 02/07/14 
 Pct Recovery = 60%  Analysis Date = 02/07/14 
 Pct Recovery = 60%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 61%  Analysis Date = 01/31/14 
 Pct Recovery = 61%  Analysis Date = 01/29/14 
 Pct Recovery = 61%  Analysis Date = 01/29/14 
 Pct Recovery = 61%  Analysis Date = 01/26/14 
 Pct Recovery = 61%  Analysis Date = 01/26/14 
 Pct Recovery = 61%  Analysis Date = 01/24/14 
 Pct Recovery = 61%  Analysis Date = 01/24/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/19/14 
 Pct Recovery = 61%  Analysis Date = 01/19/14 
 Pct Recovery = 61%  Analysis Date = 01/17/14 
 Pct Recovery = 61%  Analysis Date = 01/17/14 
 Pct Recovery = 61%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/10/14 
 Pct Recovery = 62%  Analysis Date = 01/10/14 
 Pct Recovery = 62%  Analysis Date = 01/08/14 
 Pct Recovery = 62%  Analysis Date = 01/08/14 
 Pct Recovery = 62%  Analysis Date = 01/06/14 
 Pct Recovery = 62%  Analysis Date = 01/06/14 
 Pct Recovery = 62%  Analysis Date = 01/03/14 
 Pct Recovery = 63%  Analysis Date = 01/03/14 
 Pct Recovery = 63%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 12/30/13 
 Pct Recovery = 63%  Analysis Date = 12/30/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 64%  Analysis Date = 12/16/13 
 Pct Recovery = 64%  Analysis Date = 12/16/13 
 Pct Recovery = 64%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/02/13 
 Pct Recovery = 66%  Analysis Date = 12/02/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/20/13 
 Pct Recovery = 67%  Analysis Date = 11/20/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/09/13 
 Pct Recovery = 68%  Analysis Date = 11/09/13 
 Pct Recovery = 68%  Analysis Date = 11/07/13 
 Pct Recovery = 68%  Analysis Date = 11/07/13 
 Pct Recovery = 68%  Analysis Date = 11/04/13 
 Pct Recovery = 68%  Analysis Date = 11/04/13 
 Pct Recovery = 68%  Analysis Date = 11/02/13 
 Pct Recovery = 68%  Analysis Date = 11/02/13 
 Pct Recovery = 68%  Analysis Date = 10/31/13 
 Pct Recovery = 68%  Analysis Date = 10/31/13 
 Pct Recovery = 68%  Analysis Date = 10/28/13 
 Pct Recovery = 68%  Analysis Date = 10/28/13 
 Pct Recovery = 68%  Analysis Date = 10/26/13 
 Pct Recovery = 69%  Analysis Date = 10/26/13 
 Pct Recovery = 69%  Analysis Date = 10/24/13 
 Pct Recovery = 69%  Analysis Date = 10/24/13 
 Pct Recovery = 69%  Analysis Date = 10/21/13 
 Pct Recovery = 69%  Analysis Date = 10/21/13 
 Pct Recovery = 69%  Analysis Date = 10/19/13 
 Pct Recovery = 69%  Analysis Date = 10/19/13 
 Pct Recovery = 69%  Analysis Date = 10/17/13 
 Pct Recovery = 69%  Analysis Date = 10/17/13 
 Pct Recovery = 69%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/12/13 
 Pct Recovery = 72%  Analysis Date = 09/12/13 
 Pct Recovery = 72%  Analysis Date = 09/10/13 
 Pct Recovery = 72%  Analysis Date = 09/10/13 
 Pct Recovery = 72%  Analysis Date = 09/07/13 
 Pct Recovery = 72%  Analysis Date = 09/07/13 
 Pct Recovery = 72%  Analysis Date = 09/05/13 
 Pct Recovery = 72%  Analysis Date = 09/05/13 
 Pct Recovery = 72%  Analysis Date = 09/03/13 
 Pct Recovery = 73%  Analysis Date = 09/03/13 
 Pct Recovery = 73%  Analysis Date = 09/01/13 
 Pct Recovery = 73%  Analysis Date = 09/01/13 
 Pct Recovery = 73%  Analysis Date = 08/29/13 
 Pct Recovery = 73%  Analysis Date = 08/29/13 
 Pct Recovery = 73%  Analysis Date = 08/27/13 
 Pct Recovery = 73%  Analysis Date = 08/27/13 
 Pct Recovery = 73%  Analysis Date = 08/25/13 
 Pct Recovery = 73%  Analysis Date = 08/25/13 
 Pct Recovery = 73%  Analysis Date = 08/22/13 
 Pct Recovery = 73%  Analysis Date = 08/22/13 
 Pct Recovery = 73%  Analysis Date = 08/20/13 
 Pct Recovery = 73%  Analysis Date = 08/20/13 
 Pct Recovery = 73%  Analysis Date = 08/18/13 
 Pct Recovery = 73%  Analysis Date = 08/18/13 
 Pct Recovery = 73%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/23/13 
 Pct Recovery = 74%  Analysis Date = 06/23/13 
 Pct Recovery = 74%  Analysis Date = 06/21/13 
 Pct Recovery = 74%  Analysis Date = 06/21/13 
 Pct Recovery = 74%  Analysis Date = 06/19/13 
 Pct Recovery = 74%  Analysis Date = 06/19/13 
 Pct Recovery = 74%  Analysis Date = 06/16/13 
 Pct Recovery = 74%  Analysis Date = 06/16/13 
 Pct Recovery = 74%  Analysis Date = 06/14/13 
 Pct Recovery = 74%  Analysis Date = 06/14/13 
 Pct Recovery = 74%  Analysis Date = 06/12/13 
 Pct Recovery = 74%  Analysis Date = 06/12/13 
 Pct Recovery = 74%  Analysis Date = 06/09/13 
 Pct Recovery = 74%  Analysis Date = 06/09/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/02/13 
 Pct Recovery = 74%  Analysis Date = 06/02/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 Pct Recovery = 75%  Analysis Date = 04/24/13 
 Pct Recovery = 75%  Analysis Date = 04/24/13 
 Pct Recovery = 75%  Analysis Date = 04/22/13 
 Pct Recovery = 75%  Analysis Date = 04/22/13 
 Pct Recovery = 75%  Analysis Date = 04/20/13 
 Pct Recovery = 75%  Analysis Date = 04/20/13 
 Pct Recovery = 75%  Analysis Date = 04/17/13 
 Pct Recovery = 75%  Analysis Date = 04/17/13 
 Pct Recovery = 75%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/13/13 
 Pct Recovery = 75%  Analysis Date = 04/13/13 
 Pct Recovery = 75%  Analysis Date = 04/10/13 
 Pct Recovery = 75%  Analysis Date = 04/10/13 
 Pct Recovery = 75%  Analysis Date = 04/08/13 
 Pct Recovery = 75%  Analysis Date = 04/08/13 
 Pct Recovery = 75%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 76%  Analysis Date = 03/23/13 
 Pct Recovery = 76%  Analysis Date = 03/23/13 
 Pct Recovery = 76%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/18/13 
 Pct Recovery = 76%  Analysis Date = 03/18/13 
 Pct Recovery = 76%  Analysis Date = 03/16/13 
 Pct Recovery = 77%  Analysis Date = 03/16/13 
 Pct Recovery = 77%  Analysis Date = 03/14/13 
 Pct Recovery = 77%  Analysis Date = 03/14/13 
 Pct Recovery = 77%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/07/13 
 Pct Recovery = 77%  Analysis Date = 03/04/13 
 Pct Recovery = 77%  Analysis Date = 03/04/13 
 Pct Recovery = 77%  Analysis Date = 03/02/13 
 Pct Recovery = 77%  Analysis Date = 03/02/13 
 Pct Recovery = 77%  Analysis Date = 02/28/13 
 Pct Recovery = 77%  Analysis Date = 02/28/13 
 Pct Recovery = 77%  Analysis Date = 02/25/13 
 Pct Recovery = 77%  Analysis Date = 02/25/13 
 Pct Recovery = 77%  Analysis Date = 02/23/13 
 Pct Recovery = 77%  Analysis Date = 02/23/13 
 Pct Recovery = 77%  Analysis Date = 02/21/13 
 Pct Recovery = 77%  Analysis Date = 02/21/13 
 Pct Recovery = 77%  Analysis Date = 02/18/13 
 Pct Recovery = 78%  Analysis Date = 02/18/13 
 Pct Recovery = 78%  Analysis Date = 02/16/13 
 Pct Recovery = 78%  Analysis Date = 02/16/13 
 Pct Recovery = 78%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 78%  Analysis Date = 02/05/13 
 Pct Recovery = 78%  Analysis Date = 02/05/13 
 Pct Recovery = 78%  Analysis Date = 02/02/13 
 Pct Recovery = 78%  Analysis Date = 02/02/13 
 Pct Recovery = 78%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/29/13 
 Pct Recovery = 78%  Analysis Date = 01/29/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 Pct Recovery = 79%  Analysis Date = 01/24/13 
 Pct Recovery = 79%  Analysis Date = 01/22/13 
 Pct Recovery = 79%  Analysis Date = 01/22/13 
 Pct Recovery = 79%  Analysis Date = 01/19/13 
 Pct Recovery = 79%  Analysis Date = 01/19/13 
 Pct Recovery = 79%  Analysis Date = 01/17/13 
 Pct Recovery = 79%  Analysis Date = 01/17/13 
 Pct Recovery = 79%  Analysis Date = 01/15/13 
 Pct Recovery = 79%  Analysis Date = 01/15/13 
 Pct Recovery = 79%  Analysis Date = 01/13/13 
 Pct Recovery = 79%  Analysis Date = 01/13/13 
 Pct Recovery = 79%  Analysis Date = 01/10/13 
 Pct Recovery = 79%  Analysis Date = 01/10/13 
 Pct Recovery = 79%  Analysis Date = 01/08/13 
 Pct Recovery = 79%  Analysis Date = 01/08/13 
 Pct Recovery = 79%  Analysis Date = 01/06/13 
 Pct Recovery = 79%  Analysis Date = 01/06/13 
 Pct Recovery = 79%  Analysis Date = 01/03/13 
 Pct Recovery = 79%  Analysis Date = 01/03/13 
 Pct Recovery = 79%  Analysis Date = 01/01/13 
 Pct Recovery = 79%  Analysis Date = 01/01/13 
 Pct Recovery = 79%  Analysis Date = 12/30/12 
 Pct Recovery = 79%  Analysis Date = 12/30/12 
 Pct Recovery = 79%  Analysis Date = 12/27/12 
 Pct Recovery = 80%  Analysis Date = 12/27/12 
 Pct Recovery = 80%  Analysis Date = 12/25/12 
 Pct Recovery = 80%  Analysis Date = 12/25/12 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 12/20/12 
 Pct Recovery = 80%  Analysis Date = 12/20/12 
 Pct Recovery = 80%  Analysis Date = 12/18/12 
 Pct Recovery = 80%  Analysis Date = 12/18/12 
 Pct Recovery = 80%  Analysis Date = 12/16/12 
 Pct Recovery = 80%  Analysis Date = 12/16/12 
 Pct Recovery = 80%  Analysis Date = 12/14/12 
 Pct Recovery = 80%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBAMAZEPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 70% 11% 68% 14%
Total 11 70% 11% 68% 14%

Sample Statistics
CARBAMAZEPINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 2 10% 2 out of 20

OBSP Determination:
CARISOPRODOL
METHOD: LC9017 , TESTIDCODE: 67498LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 67%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 95%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 79%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 101%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 69%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 89%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 75%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 95%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 42%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 75%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/18/14 
 Pct Recovery = 69%  Analysis Date = 03/18/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/11/14 
 Pct Recovery = 69%  Analysis Date = 03/11/14 
 Pct Recovery = 69%  Analysis Date = 03/09/14 
 Pct Recovery = 69%  Analysis Date = 03/09/14 
 Pct Recovery = 69%  Analysis Date = 03/07/14 
 Pct Recovery = 69%  Analysis Date = 03/07/14 
 Pct Recovery = 69%  Analysis Date = 03/04/14 
 Pct Recovery = 69%  Analysis Date = 03/04/14 
 Pct Recovery = 69%  Analysis Date = 03/02/14 
 Pct Recovery = 69%  Analysis Date = 03/02/14 
 Pct Recovery = 69%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/28/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 69%  Analysis Date = 02/16/14 
 Pct Recovery = 69%  Analysis Date = 02/16/14 
 Pct Recovery = 69%  Analysis Date = 02/14/14 
 Pct Recovery = 69%  Analysis Date = 02/14/14 
 Pct Recovery = 69%  Analysis Date = 02/12/14 
 Pct Recovery = 69%  Analysis Date = 02/12/14 
 Pct Recovery = 69%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/07/14 
 Pct Recovery = 69%  Analysis Date = 02/07/14 
 Pct Recovery = 69%  Analysis Date = 02/05/14 
 Pct Recovery = 69%  Analysis Date = 02/05/14 
 Pct Recovery = 69%  Analysis Date = 02/02/14 
 Pct Recovery = 69%  Analysis Date = 02/02/14 
 Pct Recovery = 69%  Analysis Date = 01/31/14 
 Pct Recovery = 69%  Analysis Date = 01/31/14 
 Pct Recovery = 69%  Analysis Date = 01/29/14 
 Pct Recovery = 69%  Analysis Date = 01/29/14 
 Pct Recovery = 69%  Analysis Date = 01/26/14 
 Pct Recovery = 69%  Analysis Date = 01/26/14 
 Pct Recovery = 69%  Analysis Date = 01/24/14 
 Pct Recovery = 69%  Analysis Date = 01/24/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/19/14 
 Pct Recovery = 69%  Analysis Date = 01/19/14 
 Pct Recovery = 69%  Analysis Date = 01/17/14 
 Pct Recovery = 69%  Analysis Date = 01/17/14 
 Pct Recovery = 69%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/13/14 
 Pct Recovery = 69%  Analysis Date = 01/13/14 
 Pct Recovery = 69%  Analysis Date = 01/10/14 
 Pct Recovery = 69%  Analysis Date = 01/10/14 
 Pct Recovery = 69%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/30/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/27/13 
 Pct Recovery = 70%  Analysis Date = 12/25/13 
 Pct Recovery = 70%  Analysis Date = 12/25/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/20/13 
 Pct Recovery = 70%  Analysis Date = 12/20/13 
 Pct Recovery = 70%  Analysis Date = 12/18/13 
 Pct Recovery = 70%  Analysis Date = 12/18/13 
 Pct Recovery = 70%  Analysis Date = 12/16/13 
 Pct Recovery = 70%  Analysis Date = 12/16/13 
 Pct Recovery = 70%  Analysis Date = 12/13/13 
 Pct Recovery = 70%  Analysis Date = 12/13/13 
 Pct Recovery = 70%  Analysis Date = 12/11/13 
 Pct Recovery = 70%  Analysis Date = 12/11/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/02/13 
 Pct Recovery = 70%  Analysis Date = 12/02/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 70%  Analysis Date = 11/27/13 
 Pct Recovery = 70%  Analysis Date = 11/27/13 
 Pct Recovery = 70%  Analysis Date = 11/25/13 
 Pct Recovery = 70%  Analysis Date = 11/25/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/20/13 
 Pct Recovery = 70%  Analysis Date = 11/20/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/07/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 10/31/13 
 Pct Recovery = 71%  Analysis Date = 10/31/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/26/13 
 Pct Recovery = 71%  Analysis Date = 10/26/13 
 Pct Recovery = 71%  Analysis Date = 10/24/13 
 Pct Recovery = 71%  Analysis Date = 10/24/13 
 Pct Recovery = 71%  Analysis Date = 10/21/13 
 Pct Recovery = 71%  Analysis Date = 10/21/13 
 Pct Recovery = 71%  Analysis Date = 10/19/13 
 Pct Recovery = 71%  Analysis Date = 10/19/13 
 Pct Recovery = 71%  Analysis Date = 10/17/13 
 Pct Recovery = 71%  Analysis Date = 10/17/13 
 Pct Recovery = 71%  Analysis Date = 10/14/13 
 Pct Recovery = 71%  Analysis Date = 10/14/13 
 Pct Recovery = 71%  Analysis Date = 10/12/13 
 Pct Recovery = 71%  Analysis Date = 10/12/13 
 Pct Recovery = 71%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/07/13 
 Pct Recovery = 72%  Analysis Date = 10/07/13 
 Pct Recovery = 72%  Analysis Date = 10/05/13 
 Pct Recovery = 72%  Analysis Date = 10/05/13 
 Pct Recovery = 72%  Analysis Date = 10/03/13 
 Pct Recovery = 72%  Analysis Date = 10/03/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 09/28/13 
 Pct Recovery = 72%  Analysis Date = 09/28/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/19/13 
 Pct Recovery = 72%  Analysis Date = 09/19/13 
 Pct Recovery = 72%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/10/13 
 Pct Recovery = 73%  Analysis Date = 09/10/13 
 Pct Recovery = 73%  Analysis Date = 09/07/13 
 Pct Recovery = 73%  Analysis Date = 09/07/13 
 Pct Recovery = 73%  Analysis Date = 09/05/13 
 Pct Recovery = 73%  Analysis Date = 09/05/13 
 Pct Recovery = 73%  Analysis Date = 09/03/13 
 Pct Recovery = 73%  Analysis Date = 09/03/13 
 Pct Recovery = 73%  Analysis Date = 09/01/13 
 Pct Recovery = 73%  Analysis Date = 09/01/13 
 Pct Recovery = 73%  Analysis Date = 08/29/13 
 Pct Recovery = 73%  Analysis Date = 08/29/13 
 Pct Recovery = 73%  Analysis Date = 08/27/13 
 Pct Recovery = 73%  Analysis Date = 08/27/13 
 Pct Recovery = 73%  Analysis Date = 08/25/13 
 Pct Recovery = 73%  Analysis Date = 08/25/13 
 Pct Recovery = 73%  Analysis Date = 08/22/13 
 Pct Recovery = 73%  Analysis Date = 08/22/13 
 Pct Recovery = 73%  Analysis Date = 08/20/13 
 Pct Recovery = 73%  Analysis Date = 08/20/13 
 Pct Recovery = 73%  Analysis Date = 08/18/13 
 Pct Recovery = 73%  Analysis Date = 08/18/13 
 Pct Recovery = 73%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 74%  Analysis Date = 08/08/13 
 Pct Recovery = 74%  Analysis Date = 08/06/13 
 Pct Recovery = 74%  Analysis Date = 08/06/13 
 Pct Recovery = 74%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/26/13 
 Pct Recovery = 74%  Analysis Date = 06/23/13 
 Pct Recovery = 74%  Analysis Date = 06/23/13 
 Pct Recovery = 74%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 75%  Analysis Date = 05/29/13 
 Pct Recovery = 75%  Analysis Date = 05/29/13 
 Pct Recovery = 75%  Analysis Date = 05/27/13 
 Pct Recovery = 75%  Analysis Date = 05/27/13 
 Pct Recovery = 75%  Analysis Date = 05/24/13 
 Pct Recovery = 75%  Analysis Date = 05/24/13 
 Pct Recovery = 75%  Analysis Date = 05/22/13 
 Pct Recovery = 75%  Analysis Date = 05/22/13 
 Pct Recovery = 75%  Analysis Date = 05/20/13 
 Pct Recovery = 75%  Analysis Date = 05/20/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/15/13 
 Pct Recovery = 75%  Analysis Date = 05/15/13 
 Pct Recovery = 75%  Analysis Date = 05/13/13 
 Pct Recovery = 75%  Analysis Date = 05/13/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 76%  Analysis Date = 05/03/13 
 Pct Recovery = 76%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 77%  Analysis Date = 04/24/13 
 Pct Recovery = 77%  Analysis Date = 04/22/13 
 Pct Recovery = 77%  Analysis Date = 04/22/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 78%  Analysis Date = 04/20/13 
 Pct Recovery = 78%  Analysis Date = 04/17/13 
 Pct Recovery = 78%  Analysis Date = 04/17/13 
 Pct Recovery = 78%  Analysis Date = 04/15/13 
 Pct Recovery = 79%  Analysis Date = 04/15/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/10/13 
 Pct Recovery = 80%  Analysis Date = 04/10/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/06/13 
 Pct Recovery = 81%  Analysis Date = 04/06/13 
 Pct Recovery = 81%  Analysis Date = 04/03/13 
 Pct Recovery = 81%  Analysis Date = 04/03/13 
 Pct Recovery = 81%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 82%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 84%  Analysis Date = 03/21/13 
 Pct Recovery = 84%  Analysis Date = 03/18/13 
 Pct Recovery = 84%  Analysis Date = 03/18/13 
 Pct Recovery = 84%  Analysis Date = 03/16/13 
 Pct Recovery = 85%  Analysis Date = 03/16/13 
 Pct Recovery = 85%  Analysis Date = 03/14/13 
 Pct Recovery = 85%  Analysis Date = 03/14/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 86%  Analysis Date = 03/11/13 
 Pct Recovery = 86%  Analysis Date = 03/09/13 
 Pct Recovery = 86%  Analysis Date = 03/09/13 
 Pct Recovery = 86%  Analysis Date = 03/07/13 
 Pct Recovery = 87%  Analysis Date = 03/07/13 
 Pct Recovery = 87%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 89%  Analysis Date = 02/25/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 90%  Analysis Date = 02/21/13 
 Pct Recovery = 90%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 91%  Analysis Date = 02/14/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/05/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 02/02/13 
 Pct Recovery = 93%  Analysis Date = 01/31/13 
 Pct Recovery = 94%  Analysis Date = 01/31/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 95%  Analysis Date = 01/26/13 
 Pct Recovery = 95%  Analysis Date = 01/24/13 
 Pct Recovery = 95%  Analysis Date = 01/24/13 
 Pct Recovery = 95%  Analysis Date = 01/22/13 
 Pct Recovery = 96%  Analysis Date = 01/22/13 
 Pct Recovery = 96%  Analysis Date = 01/19/13 
 Pct Recovery = 96%  Analysis Date = 01/19/13 
 Pct Recovery = 96%  Analysis Date = 01/17/13 
 Pct Recovery = 97%  Analysis Date = 01/17/13 
 Pct Recovery = 97%  Analysis Date = 01/15/13 
 Pct Recovery = 97%  Analysis Date = 01/15/13 
 Pct Recovery = 97%  Analysis Date = 01/13/13 
 Pct Recovery = 97%  Analysis Date = 01/13/13 
 Pct Recovery = 97%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 01/01/13 
 Pct Recovery = 100%  Analysis Date = 12/30/12 
 Pct Recovery = 100%  Analysis Date = 12/30/12 
 Pct Recovery = 100%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/27/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/25/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 102%  Analysis Date = 12/23/12 
 Pct Recovery = 102%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/20/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 103%  Analysis Date = 12/16/12 
 Pct Recovery = 103%  Analysis Date = 12/14/12 
 Pct Recovery = 103%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARISOPRODOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 79% 17% 77% 19%
Total 10 79% 17% 77% 19%

Sample Statistics
CARISOPRODOL

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 1 9% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
CHLORPHENIRAMINE
METHOD: LC9017 , TESTIDCODE: 67497LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 48%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 38%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 63%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 34%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 59%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 28%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 49%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 21%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 99%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 47%  Analysis Date = 03/21/14 
 Pct Recovery = 44%  Analysis Date = 03/18/14 
 Pct Recovery = 44%  Analysis Date = 03/18/14 
 Pct Recovery = 44%  Analysis Date = 03/16/14 
 Pct Recovery = 44%  Analysis Date = 03/16/14 
 Pct Recovery = 44%  Analysis Date = 03/14/14 
 Pct Recovery = 44%  Analysis Date = 03/14/14 
 Pct Recovery = 44%  Analysis Date = 03/11/14 
 Pct Recovery = 45%  Analysis Date = 03/11/14 
 Pct Recovery = 45%  Analysis Date = 03/09/14 
 Pct Recovery = 45%  Analysis Date = 03/09/14 
 Pct Recovery = 45%  Analysis Date = 03/07/14 
 Pct Recovery = 45%  Analysis Date = 03/07/14 
 Pct Recovery = 45%  Analysis Date = 03/04/14 
 Pct Recovery = 45%  Analysis Date = 03/04/14 
 Pct Recovery = 45%  Analysis Date = 03/02/14 
 Pct Recovery = 45%  Analysis Date = 03/02/14 
 Pct Recovery = 45%  Analysis Date = 02/28/14 
 Pct Recovery = 45%  Analysis Date = 02/28/14 
 Pct Recovery = 45%  Analysis Date = 02/25/14 
 Pct Recovery = 46%  Analysis Date = 02/25/14 
 Pct Recovery = 46%  Analysis Date = 02/23/14 
 Pct Recovery = 46%  Analysis Date = 02/23/14 
 Pct Recovery = 46%  Analysis Date = 02/21/14 
 Pct Recovery = 46%  Analysis Date = 02/21/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/16/14 
 Pct Recovery = 46%  Analysis Date = 02/16/14 
 Pct Recovery = 46%  Analysis Date = 02/14/14 
 Pct Recovery = 46%  Analysis Date = 02/14/14 
 Pct Recovery = 46%  Analysis Date = 02/12/14 
 Pct Recovery = 46%  Analysis Date = 02/12/14 
 Pct Recovery = 46%  Analysis Date = 02/09/14 
 Pct Recovery = 47%  Analysis Date = 02/09/14 
 Pct Recovery = 47%  Analysis Date = 02/07/14 
 Pct Recovery = 47%  Analysis Date = 02/07/14 
 Pct Recovery = 47%  Analysis Date = 02/05/14 
 Pct Recovery = 47%  Analysis Date = 02/05/14 
 Pct Recovery = 47%  Analysis Date = 02/02/14 
 Pct Recovery = 47%  Analysis Date = 02/02/14 
 Pct Recovery = 47%  Analysis Date = 01/31/14 
 Pct Recovery = 47%  Analysis Date = 01/31/14 
 Pct Recovery = 47%  Analysis Date = 01/29/14 
 Pct Recovery = 47%  Analysis Date = 01/29/14 
 Pct Recovery = 47%  Analysis Date = 01/26/14 
 Pct Recovery = 48%  Analysis Date = 01/26/14 
 Pct Recovery = 48%  Analysis Date = 01/24/14 
 Pct Recovery = 48%  Analysis Date = 01/24/14 
 Pct Recovery = 48%  Analysis Date = 01/22/14 
 Pct Recovery = 48%  Analysis Date = 01/22/14 
 Pct Recovery = 48%  Analysis Date = 01/19/14 
 Pct Recovery = 48%  Analysis Date = 01/19/14 
 Pct Recovery = 48%  Analysis Date = 01/17/14 
 Pct Recovery = 48%  Analysis Date = 01/17/14 
 Pct Recovery = 48%  Analysis Date = 01/15/14 
 Pct Recovery = 48%  Analysis Date = 01/15/14 
 Pct Recovery = 48%  Analysis Date = 01/13/14 
 Pct Recovery = 48%  Analysis Date = 01/13/14 
 Pct Recovery = 48%  Analysis Date = 01/10/14 
 Pct Recovery = 49%  Analysis Date = 01/10/14 
 Pct Recovery = 49%  Analysis Date = 01/08/14 
 Pct Recovery = 49%  Analysis Date = 01/08/14 
 Pct Recovery = 49%  Analysis Date = 01/06/14 
 Pct Recovery = 49%  Analysis Date = 01/06/14 
 Pct Recovery = 49%  Analysis Date = 01/03/14 
 Pct Recovery = 49%  Analysis Date = 01/03/14 
 Pct Recovery = 49%  Analysis Date = 01/01/14 
 Pct Recovery = 49%  Analysis Date = 01/01/14 
 Pct Recovery = 49%  Analysis Date = 12/30/13 
 Pct Recovery = 49%  Analysis Date = 12/30/13 
 Pct Recovery = 49%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/04/13 
 Pct Recovery = 51%  Analysis Date = 12/04/13 
 Pct Recovery = 51%  Analysis Date = 12/02/13 
 Pct Recovery = 51%  Analysis Date = 12/02/13 
 Pct Recovery = 51%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 Pct Recovery = 52%  Analysis Date = 11/27/13 
 Pct Recovery = 52%  Analysis Date = 11/25/13 
 Pct Recovery = 52%  Analysis Date = 11/25/13 
 Pct Recovery = 52%  Analysis Date = 11/23/13 
 Pct Recovery = 52%  Analysis Date = 11/23/13 
 Pct Recovery = 52%  Analysis Date = 11/20/13 
 Pct Recovery = 52%  Analysis Date = 11/20/13 
 Pct Recovery = 52%  Analysis Date = 11/18/13 
 Pct Recovery = 52%  Analysis Date = 11/18/13 
 Pct Recovery = 52%  Analysis Date = 11/16/13 
 Pct Recovery = 52%  Analysis Date = 11/16/13 
 Pct Recovery = 52%  Analysis Date = 11/13/13 
 Pct Recovery = 52%  Analysis Date = 11/13/13 
 Pct Recovery = 52%  Analysis Date = 11/11/13 
 Pct Recovery = 53%  Analysis Date = 11/11/13 
 Pct Recovery = 53%  Analysis Date = 11/09/13 
 Pct Recovery = 53%  Analysis Date = 11/09/13 
 Pct Recovery = 53%  Analysis Date = 11/07/13 
 Pct Recovery = 53%  Analysis Date = 11/07/13 
 Pct Recovery = 53%  Analysis Date = 11/04/13 
 Pct Recovery = 53%  Analysis Date = 11/04/13 
 Pct Recovery = 53%  Analysis Date = 11/02/13 
 Pct Recovery = 53%  Analysis Date = 11/02/13 
 Pct Recovery = 53%  Analysis Date = 10/31/13 
 Pct Recovery = 53%  Analysis Date = 10/31/13 
 Pct Recovery = 53%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/19/13 
 Pct Recovery = 54%  Analysis Date = 10/19/13 
 Pct Recovery = 54%  Analysis Date = 10/17/13 
 Pct Recovery = 54%  Analysis Date = 10/17/13 
 Pct Recovery = 54%  Analysis Date = 10/14/13 
 Pct Recovery = 54%  Analysis Date = 10/14/13 
 Pct Recovery = 54%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/10/13 
 Pct Recovery = 55%  Analysis Date = 10/10/13 
 Pct Recovery = 55%  Analysis Date = 10/07/13 
 Pct Recovery = 55%  Analysis Date = 10/07/13 
 Pct Recovery = 55%  Analysis Date = 10/05/13 
 Pct Recovery = 55%  Analysis Date = 10/05/13 
 Pct Recovery = 55%  Analysis Date = 10/03/13 
 Pct Recovery = 55%  Analysis Date = 10/03/13 
 Pct Recovery = 55%  Analysis Date = 10/01/13 
 Pct Recovery = 55%  Analysis Date = 10/01/13 
 Pct Recovery = 55%  Analysis Date = 09/28/13 
 Pct Recovery = 56%  Analysis Date = 09/28/13 
 Pct Recovery = 56%  Analysis Date = 09/26/13 
 Pct Recovery = 56%  Analysis Date = 09/26/13 
 Pct Recovery = 56%  Analysis Date = 09/24/13 
 Pct Recovery = 56%  Analysis Date = 09/24/13 
 Pct Recovery = 56%  Analysis Date = 09/21/13 
 Pct Recovery = 56%  Analysis Date = 09/21/13 
 Pct Recovery = 56%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/17/13 
 Pct Recovery = 56%  Analysis Date = 09/17/13 
 Pct Recovery = 56%  Analysis Date = 09/14/13 
 Pct Recovery = 56%  Analysis Date = 09/14/13 
 Pct Recovery = 56%  Analysis Date = 09/12/13 
 Pct Recovery = 57%  Analysis Date = 09/12/13 
 Pct Recovery = 57%  Analysis Date = 09/10/13 
 Pct Recovery = 57%  Analysis Date = 09/10/13 
 Pct Recovery = 57%  Analysis Date = 09/07/13 
 Pct Recovery = 57%  Analysis Date = 09/07/13 
 Pct Recovery = 57%  Analysis Date = 09/05/13 
 Pct Recovery = 57%  Analysis Date = 09/05/13 
 Pct Recovery = 57%  Analysis Date = 09/03/13 
 Pct Recovery = 57%  Analysis Date = 09/03/13 
 Pct Recovery = 57%  Analysis Date = 09/01/13 
 Pct Recovery = 57%  Analysis Date = 09/01/13 
 Pct Recovery = 57%  Analysis Date = 08/29/13 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 Pct Recovery = 58%  Analysis Date = 08/27/13 
 Pct Recovery = 58%  Analysis Date = 08/27/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/22/13 
 Pct Recovery = 58%  Analysis Date = 08/22/13 
 Pct Recovery = 58%  Analysis Date = 08/20/13 
 Pct Recovery = 58%  Analysis Date = 08/20/13 
 Pct Recovery = 58%  Analysis Date = 08/18/13 
 Pct Recovery = 58%  Analysis Date = 08/18/13 
 Pct Recovery = 58%  Analysis Date = 08/15/13 
 Pct Recovery = 59%  Analysis Date = 08/15/13 
 Pct Recovery = 59%  Analysis Date = 08/13/13 
 Pct Recovery = 59%  Analysis Date = 08/13/13 
 Pct Recovery = 59%  Analysis Date = 08/11/13 
 Pct Recovery = 59%  Analysis Date = 08/11/13 
 Pct Recovery = 59%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/06/13 
 Pct Recovery = 59%  Analysis Date = 08/06/13 
 Pct Recovery = 59%  Analysis Date = 08/04/13 
 Pct Recovery = 59%  Analysis Date = 08/04/13 
 Pct Recovery = 59%  Analysis Date = 08/02/13 
 Pct Recovery = 59%  Analysis Date = 08/02/13 
 Pct Recovery = 59%  Analysis Date = 07/30/13 
 Pct Recovery = 59%  Analysis Date = 07/30/13 
 Pct Recovery = 59%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/26/13 
 Pct Recovery = 58%  Analysis Date = 07/26/13 
 Pct Recovery = 58%  Analysis Date = 07/23/13 
 Pct Recovery = 58%  Analysis Date = 07/23/13 
 Pct Recovery = 58%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/19/13 
 Pct Recovery = 57%  Analysis Date = 07/19/13 
 Pct Recovery = 57%  Analysis Date = 07/16/13 
 Pct Recovery = 56%  Analysis Date = 07/16/13 
 Pct Recovery = 56%  Analysis Date = 07/14/13 
 Pct Recovery = 56%  Analysis Date = 07/14/13 
 Pct Recovery = 56%  Analysis Date = 07/12/13 
 Pct Recovery = 55%  Analysis Date = 07/12/13 
 Pct Recovery = 55%  Analysis Date = 07/09/13 
 Pct Recovery = 55%  Analysis Date = 07/09/13 
 Pct Recovery = 55%  Analysis Date = 07/07/13 
 Pct Recovery = 54%  Analysis Date = 07/07/13 
 Pct Recovery = 54%  Analysis Date = 07/05/13 
 Pct Recovery = 54%  Analysis Date = 07/05/13 
 Pct Recovery = 54%  Analysis Date = 07/02/13 
 Pct Recovery = 54%  Analysis Date = 07/02/13 
 Pct Recovery = 54%  Analysis Date = 06/30/13 
 Pct Recovery = 53%  Analysis Date = 06/30/13 
 Pct Recovery = 53%  Analysis Date = 06/28/13 
 Pct Recovery = 53%  Analysis Date = 06/28/13 
 Pct Recovery = 53%  Analysis Date = 06/26/13 
 Pct Recovery = 52%  Analysis Date = 06/26/13 
 Pct Recovery = 52%  Analysis Date = 06/23/13 
 Pct Recovery = 52%  Analysis Date = 06/23/13 
 Pct Recovery = 52%  Analysis Date = 06/21/13 
 Pct Recovery = 51%  Analysis Date = 06/21/13 
 Pct Recovery = 51%  Analysis Date = 06/19/13 
 Pct Recovery = 51%  Analysis Date = 06/19/13 
 Pct Recovery = 51%  Analysis Date = 06/16/13 
 Pct Recovery = 50%  Analysis Date = 06/16/13 
 Pct Recovery = 50%  Analysis Date = 06/14/13 
 Pct Recovery = 50%  Analysis Date = 06/14/13 
 Pct Recovery = 50%  Analysis Date = 06/12/13 
 Pct Recovery = 49%  Analysis Date = 06/12/13 
 Pct Recovery = 49%  Analysis Date = 06/09/13 
 Pct Recovery = 49%  Analysis Date = 06/09/13 
 Pct Recovery = 49%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/05/13 
 Pct Recovery = 48%  Analysis Date = 06/05/13 
 Pct Recovery = 48%  Analysis Date = 06/02/13 
 Pct Recovery = 48%  Analysis Date = 06/02/13 
 Pct Recovery = 48%  Analysis Date = 05/31/13 
 Pct Recovery = 47%  Analysis Date = 05/31/13 
 Pct Recovery = 47%  Analysis Date = 05/29/13 
 Pct Recovery = 47%  Analysis Date = 05/29/13 
 Pct Recovery = 47%  Analysis Date = 05/27/13 
 Pct Recovery = 46%  Analysis Date = 05/27/13 
 Pct Recovery = 46%  Analysis Date = 05/24/13 
 Pct Recovery = 46%  Analysis Date = 05/24/13 
 Pct Recovery = 46%  Analysis Date = 05/22/13 
 Pct Recovery = 45%  Analysis Date = 05/22/13 
 Pct Recovery = 45%  Analysis Date = 05/20/13 
 Pct Recovery = 45%  Analysis Date = 05/20/13 
 Pct Recovery = 45%  Analysis Date = 05/17/13 
 Pct Recovery = 44%  Analysis Date = 05/17/13 
 Pct Recovery = 44%  Analysis Date = 05/15/13 
 Pct Recovery = 44%  Analysis Date = 05/15/13 
 Pct Recovery = 44%  Analysis Date = 05/13/13 
 Pct Recovery = 44%  Analysis Date = 05/13/13 
 Pct Recovery = 44%  Analysis Date = 05/10/13 
 Pct Recovery = 43%  Analysis Date = 05/10/13 
 Pct Recovery = 43%  Analysis Date = 05/08/13 
 Pct Recovery = 43%  Analysis Date = 05/08/13 
 Pct Recovery = 43%  Analysis Date = 05/06/13 
 Pct Recovery = 42%  Analysis Date = 05/06/13 
 Pct Recovery = 42%  Analysis Date = 05/03/13 
 Pct Recovery = 42%  Analysis Date = 05/03/13 
 Pct Recovery = 42%  Analysis Date = 05/01/13 
 Pct Recovery = 41%  Analysis Date = 05/01/13 
 Pct Recovery = 41%  Analysis Date = 04/29/13 
 Pct Recovery = 41%  Analysis Date = 04/29/13 
 Pct Recovery = 41%  Analysis Date = 04/26/13 
 Pct Recovery = 41%  Analysis Date = 04/26/13 
 Pct Recovery = 41%  Analysis Date = 04/24/13 
 Pct Recovery = 41%  Analysis Date = 04/24/13 
 Pct Recovery = 41%  Analysis Date = 04/22/13 
 Pct Recovery = 41%  Analysis Date = 04/22/13 
 Pct Recovery = 41%  Analysis Date = 04/20/13 
 Pct Recovery = 41%  Analysis Date = 04/20/13 
 Pct Recovery = 41%  Analysis Date = 04/17/13 
 Pct Recovery = 41%  Analysis Date = 04/17/13 
 Pct Recovery = 41%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/13/13 
 Pct Recovery = 41%  Analysis Date = 04/13/13 
 Pct Recovery = 41%  Analysis Date = 04/10/13 
 Pct Recovery = 41%  Analysis Date = 04/10/13 
 Pct Recovery = 41%  Analysis Date = 04/08/13 
 Pct Recovery = 41%  Analysis Date = 04/08/13 
 Pct Recovery = 41%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 40%  Analysis Date = 03/27/13 
 Pct Recovery = 40%  Analysis Date = 03/27/13 
 Pct Recovery = 40%  Analysis Date = 03/25/13 
 Pct Recovery = 40%  Analysis Date = 03/25/13 
 Pct Recovery = 40%  Analysis Date = 03/23/13 
 Pct Recovery = 41%  Analysis Date = 03/23/13 
 Pct Recovery = 41%  Analysis Date = 03/21/13 
 Pct Recovery = 41%  Analysis Date = 03/21/13 
 Pct Recovery = 41%  Analysis Date = 03/18/13 
 Pct Recovery = 41%  Analysis Date = 03/18/13 
 Pct Recovery = 41%  Analysis Date = 03/16/13 
 Pct Recovery = 42%  Analysis Date = 03/16/13 
 Pct Recovery = 42%  Analysis Date = 03/14/13 
 Pct Recovery = 42%  Analysis Date = 03/14/13 
 Pct Recovery = 42%  Analysis Date = 03/11/13 
 Pct Recovery = 42%  Analysis Date = 03/11/13 
 Pct Recovery = 42%  Analysis Date = 03/09/13 
 Pct Recovery = 43%  Analysis Date = 03/09/13 
 Pct Recovery = 43%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/04/13 
 Pct Recovery = 43%  Analysis Date = 03/04/13 
 Pct Recovery = 43%  Analysis Date = 03/02/13 
 Pct Recovery = 44%  Analysis Date = 03/02/13 
 Pct Recovery = 44%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/25/13 
 Pct Recovery = 44%  Analysis Date = 02/25/13 
 Pct Recovery = 44%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/21/13 
 Pct Recovery = 46%  Analysis Date = 02/21/13 
 Pct Recovery = 46%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/16/13 
 Pct Recovery = 47%  Analysis Date = 02/16/13 
 Pct Recovery = 47%  Analysis Date = 02/14/13 
 Pct Recovery = 47%  Analysis Date = 02/14/13 
 Pct Recovery = 47%  Analysis Date = 02/12/13 
 Pct Recovery = 48%  Analysis Date = 02/12/13 
 Pct Recovery = 48%  Analysis Date = 02/09/13 
 Pct Recovery = 49%  Analysis Date = 02/09/13 
 Pct Recovery = 49%  Analysis Date = 02/07/13 
 Pct Recovery = 49%  Analysis Date = 02/07/13 
 Pct Recovery = 49%  Analysis Date = 02/05/13 
 Pct Recovery = 50%  Analysis Date = 02/05/13 
 Pct Recovery = 50%  Analysis Date = 02/02/13 
 Pct Recovery = 50%  Analysis Date = 02/02/13 
 Pct Recovery = 50%  Analysis Date = 01/31/13 
 Pct Recovery = 51%  Analysis Date = 01/31/13 
 Pct Recovery = 51%  Analysis Date = 01/29/13 
 Pct Recovery = 52%  Analysis Date = 01/29/13 
 Pct Recovery = 52%  Analysis Date = 01/26/13 
 Pct Recovery = 52%  Analysis Date = 01/26/13 
 Pct Recovery = 52%  Analysis Date = 01/24/13 
 Pct Recovery = 53%  Analysis Date = 01/24/13 
 Pct Recovery = 53%  Analysis Date = 01/22/13 
 Pct Recovery = 53%  Analysis Date = 01/22/13 
 Pct Recovery = 53%  Analysis Date = 01/19/13 
 Pct Recovery = 54%  Analysis Date = 01/19/13 
 Pct Recovery = 54%  Analysis Date = 01/17/13 
 Pct Recovery = 55%  Analysis Date = 01/17/13 
 Pct Recovery = 55%  Analysis Date = 01/15/13 
 Pct Recovery = 55%  Analysis Date = 01/15/13 
 Pct Recovery = 55%  Analysis Date = 01/13/13 
 Pct Recovery = 56%  Analysis Date = 01/13/13 
 Pct Recovery = 56%  Analysis Date = 01/10/13 
 Pct Recovery = 56%  Analysis Date = 01/10/13 
 Pct Recovery = 56%  Analysis Date = 01/08/13 
 Pct Recovery = 57%  Analysis Date = 01/08/13 
 Pct Recovery = 57%  Analysis Date = 01/06/13 
 Pct Recovery = 58%  Analysis Date = 01/06/13 
 Pct Recovery = 58%  Analysis Date = 01/03/13 
 Pct Recovery = 58%  Analysis Date = 01/03/13 
 Pct Recovery = 58%  Analysis Date = 01/01/13 
 Pct Recovery = 59%  Analysis Date = 01/01/13 
 Pct Recovery = 59%  Analysis Date = 12/30/12 
 Pct Recovery = 59%  Analysis Date = 12/30/12 
 Pct Recovery = 59%  Analysis Date = 12/27/12 
 Pct Recovery = 60%  Analysis Date = 12/27/12 
 Pct Recovery = 60%  Analysis Date = 12/25/12 
 Pct Recovery = 61%  Analysis Date = 12/25/12 
 Pct Recovery = 61%  Analysis Date = 12/23/12 
 Pct Recovery = 61%  Analysis Date = 12/23/12 
 Pct Recovery = 61%  Analysis Date = 12/20/12 
 Pct Recovery = 62%  Analysis Date = 12/20/12 
 Pct Recovery = 62%  Analysis Date = 12/18/12 
 Pct Recovery = 62%  Analysis Date = 12/18/12 
 Pct Recovery = 62%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/14/12 
 Pct Recovery = 64%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPHENIRAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 48% 22% 47% 18%
Total 10 48% 22% 47% 18%

Sample Statistics
CHLORPHENIRAMINE

Characteristic N % % Basis
Plotted 10 67% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 5 33% 5 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
CIMETIDINE
METHOD: LC9017 , TESTIDCODE: 67442LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 44%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 73%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 8%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 40%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 28%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 6%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 43%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 33%  Analysis Date = 03/21/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/11/14 
 Pct Recovery = 42%  Analysis Date = 03/11/14 
 Pct Recovery = 42%  Analysis Date = 03/09/14 
 Pct Recovery = 42%  Analysis Date = 03/09/14 
 Pct Recovery = 42%  Analysis Date = 03/07/14 
 Pct Recovery = 41%  Analysis Date = 03/07/14 
 Pct Recovery = 41%  Analysis Date = 03/04/14 
 Pct Recovery = 41%  Analysis Date = 03/04/14 
 Pct Recovery = 41%  Analysis Date = 03/02/14 
 Pct Recovery = 41%  Analysis Date = 03/02/14 
 Pct Recovery = 41%  Analysis Date = 02/28/14 
 Pct Recovery = 41%  Analysis Date = 02/28/14 
 Pct Recovery = 41%  Analysis Date = 02/25/14 
 Pct Recovery = 41%  Analysis Date = 02/25/14 
 Pct Recovery = 41%  Analysis Date = 02/23/14 
 Pct Recovery = 41%  Analysis Date = 02/23/14 
 Pct Recovery = 41%  Analysis Date = 02/21/14 
 Pct Recovery = 41%  Analysis Date = 02/21/14 
 Pct Recovery = 41%  Analysis Date = 02/18/14 
 Pct Recovery = 40%  Analysis Date = 02/18/14 
 Pct Recovery = 40%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/14/14 
 Pct Recovery = 40%  Analysis Date = 02/14/14 
 Pct Recovery = 40%  Analysis Date = 02/12/14 
 Pct Recovery = 40%  Analysis Date = 02/12/14 
 Pct Recovery = 40%  Analysis Date = 02/09/14 
 Pct Recovery = 40%  Analysis Date = 02/09/14 
 Pct Recovery = 40%  Analysis Date = 02/07/14 
 Pct Recovery = 40%  Analysis Date = 02/07/14 
 Pct Recovery = 40%  Analysis Date = 02/05/14 
 Pct Recovery = 39%  Analysis Date = 02/05/14 
 Pct Recovery = 39%  Analysis Date = 02/02/14 
 Pct Recovery = 39%  Analysis Date = 02/02/14 
 Pct Recovery = 39%  Analysis Date = 01/31/14 
 Pct Recovery = 39%  Analysis Date = 01/31/14 
 Pct Recovery = 39%  Analysis Date = 01/29/14 
 Pct Recovery = 39%  Analysis Date = 01/29/14 
 Pct Recovery = 39%  Analysis Date = 01/26/14 
 Pct Recovery = 39%  Analysis Date = 01/26/14 
 Pct Recovery = 39%  Analysis Date = 01/24/14 
 Pct Recovery = 39%  Analysis Date = 01/24/14 
 Pct Recovery = 39%  Analysis Date = 01/22/14 
 Pct Recovery = 39%  Analysis Date = 01/22/14 
 Pct Recovery = 39%  Analysis Date = 01/19/14 
 Pct Recovery = 38%  Analysis Date = 01/19/14 
 Pct Recovery = 38%  Analysis Date = 01/17/14 
 Pct Recovery = 38%  Analysis Date = 01/17/14 
 Pct Recovery = 38%  Analysis Date = 01/15/14 
 Pct Recovery = 38%  Analysis Date = 01/15/14 
 Pct Recovery = 38%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/08/14 
 Pct Recovery = 38%  Analysis Date = 01/08/14 
 Pct Recovery = 38%  Analysis Date = 01/06/14 
 Pct Recovery = 38%  Analysis Date = 01/06/14 
 Pct Recovery = 38%  Analysis Date = 01/03/14 
 Pct Recovery = 37%  Analysis Date = 01/03/14 
 Pct Recovery = 37%  Analysis Date = 01/01/14 
 Pct Recovery = 37%  Analysis Date = 01/01/14 
 Pct Recovery = 37%  Analysis Date = 12/30/13 
 Pct Recovery = 37%  Analysis Date = 12/30/13 
 Pct Recovery = 37%  Analysis Date = 12/27/13 
 Pct Recovery = 37%  Analysis Date = 12/27/13 
 Pct Recovery = 37%  Analysis Date = 12/25/13 
 Pct Recovery = 37%  Analysis Date = 12/25/13 
 Pct Recovery = 37%  Analysis Date = 12/23/13 
 Pct Recovery = 37%  Analysis Date = 12/23/13 
 Pct Recovery = 37%  Analysis Date = 12/20/13 
 Pct Recovery = 36%  Analysis Date = 12/20/13 
 Pct Recovery = 36%  Analysis Date = 12/18/13 
 Pct Recovery = 36%  Analysis Date = 12/18/13 
 Pct Recovery = 36%  Analysis Date = 12/16/13 
 Pct Recovery = 36%  Analysis Date = 12/16/13 
 Pct Recovery = 36%  Analysis Date = 12/13/13 
 Pct Recovery = 36%  Analysis Date = 12/13/13 
 Pct Recovery = 36%  Analysis Date = 12/11/13 
 Pct Recovery = 36%  Analysis Date = 12/11/13 
 Pct Recovery = 36%  Analysis Date = 12/09/13 
 Pct Recovery = 36%  Analysis Date = 12/09/13 
 Pct Recovery = 36%  Analysis Date = 12/07/13 
 Pct Recovery = 36%  Analysis Date = 12/07/13 
 Pct Recovery = 36%  Analysis Date = 12/04/13 
 Pct Recovery = 35%  Analysis Date = 12/04/13 
 Pct Recovery = 35%  Analysis Date = 12/02/13 
 Pct Recovery = 35%  Analysis Date = 12/02/13 
 Pct Recovery = 35%  Analysis Date = 11/30/13 
 Pct Recovery = 35%  Analysis Date = 11/30/13 
 Pct Recovery = 35%  Analysis Date = 11/27/13 
 Pct Recovery = 35%  Analysis Date = 11/27/13 
 Pct Recovery = 35%  Analysis Date = 11/25/13 
 Pct Recovery = 35%  Analysis Date = 11/25/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/18/13 
 Pct Recovery = 34%  Analysis Date = 11/18/13 
 Pct Recovery = 34%  Analysis Date = 11/16/13 
 Pct Recovery = 34%  Analysis Date = 11/16/13 
 Pct Recovery = 34%  Analysis Date = 11/13/13 
 Pct Recovery = 34%  Analysis Date = 11/13/13 
 Pct Recovery = 34%  Analysis Date = 11/11/13 
 Pct Recovery = 34%  Analysis Date = 11/11/13 
 Pct Recovery = 34%  Analysis Date = 11/09/13 
 Pct Recovery = 34%  Analysis Date = 11/09/13 
 Pct Recovery = 34%  Analysis Date = 11/07/13 
 Pct Recovery = 34%  Analysis Date = 11/07/13 
 Pct Recovery = 34%  Analysis Date = 11/04/13 
 Pct Recovery = 34%  Analysis Date = 11/04/13 
 Pct Recovery = 34%  Analysis Date = 11/02/13 
 Pct Recovery = 34%  Analysis Date = 11/02/13 
 Pct Recovery = 34%  Analysis Date = 10/31/13 
 Pct Recovery = 34%  Analysis Date = 10/31/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/26/13 
 Pct Recovery = 34%  Analysis Date = 10/26/13 
 Pct Recovery = 34%  Analysis Date = 10/24/13 
 Pct Recovery = 34%  Analysis Date = 10/24/13 
 Pct Recovery = 34%  Analysis Date = 10/21/13 
 Pct Recovery = 34%  Analysis Date = 10/21/13 
 Pct Recovery = 34%  Analysis Date = 10/19/13 
 Pct Recovery = 34%  Analysis Date = 10/19/13 
 Pct Recovery = 34%  Analysis Date = 10/17/13 
 Pct Recovery = 34%  Analysis Date = 10/17/13 
 Pct Recovery = 34%  Analysis Date = 10/14/13 
 Pct Recovery = 34%  Analysis Date = 10/14/13 
 Pct Recovery = 34%  Analysis Date = 10/12/13 
 Pct Recovery = 34%  Analysis Date = 10/12/13 
 Pct Recovery = 34%  Analysis Date = 10/10/13 
 Pct Recovery = 34%  Analysis Date = 10/10/13 
 Pct Recovery = 34%  Analysis Date = 10/07/13 
 Pct Recovery = 33%  Analysis Date = 10/07/13 
 Pct Recovery = 33%  Analysis Date = 10/05/13 
 Pct Recovery = 33%  Analysis Date = 10/05/13 
 Pct Recovery = 33%  Analysis Date = 10/03/13 
 Pct Recovery = 33%  Analysis Date = 10/03/13 
 Pct Recovery = 33%  Analysis Date = 10/01/13 
 Pct Recovery = 33%  Analysis Date = 10/01/13 
 Pct Recovery = 33%  Analysis Date = 09/28/13 
 Pct Recovery = 33%  Analysis Date = 09/28/13 
 Pct Recovery = 33%  Analysis Date = 09/26/13 
 Pct Recovery = 33%  Analysis Date = 09/26/13 
 Pct Recovery = 33%  Analysis Date = 09/24/13 
 Pct Recovery = 33%  Analysis Date = 09/24/13 
 Pct Recovery = 33%  Analysis Date = 09/21/13 
 Pct Recovery = 33%  Analysis Date = 09/21/13 
 Pct Recovery = 33%  Analysis Date = 09/19/13 
 Pct Recovery = 33%  Analysis Date = 09/19/13 
 Pct Recovery = 33%  Analysis Date = 09/17/13 
 Pct Recovery = 33%  Analysis Date = 09/17/13 
 Pct Recovery = 33%  Analysis Date = 09/14/13 
 Pct Recovery = 33%  Analysis Date = 09/14/13 
 Pct Recovery = 33%  Analysis Date = 09/12/13 
 Pct Recovery = 33%  Analysis Date = 09/12/13 
 Pct Recovery = 33%  Analysis Date = 09/10/13 
 Pct Recovery = 33%  Analysis Date = 09/10/13 
 Pct Recovery = 33%  Analysis Date = 09/07/13 
 Pct Recovery = 33%  Analysis Date = 09/07/13 
 Pct Recovery = 33%  Analysis Date = 09/05/13 
 Pct Recovery = 33%  Analysis Date = 09/05/13 
 Pct Recovery = 33%  Analysis Date = 09/03/13 
 Pct Recovery = 33%  Analysis Date = 09/03/13 
 Pct Recovery = 33%  Analysis Date = 09/01/13 
 Pct Recovery = 33%  Analysis Date = 09/01/13 
 Pct Recovery = 33%  Analysis Date = 08/29/13 
 Pct Recovery = 33%  Analysis Date = 08/29/13 
 Pct Recovery = 33%  Analysis Date = 08/27/13 
 Pct Recovery = 33%  Analysis Date = 08/27/13 
 Pct Recovery = 33%  Analysis Date = 08/25/13 
 Pct Recovery = 33%  Analysis Date = 08/25/13 
 Pct Recovery = 33%  Analysis Date = 08/22/13 
 Pct Recovery = 34%  Analysis Date = 08/22/13 
 Pct Recovery = 34%  Analysis Date = 08/20/13 
 Pct Recovery = 34%  Analysis Date = 08/20/13 
 Pct Recovery = 34%  Analysis Date = 08/18/13 
 Pct Recovery = 35%  Analysis Date = 08/18/13 
 Pct Recovery = 35%  Analysis Date = 08/15/13 
 Pct Recovery = 35%  Analysis Date = 08/15/13 
 Pct Recovery = 35%  Analysis Date = 08/13/13 
 Pct Recovery = 36%  Analysis Date = 08/13/13 
 Pct Recovery = 36%  Analysis Date = 08/11/13 
 Pct Recovery = 36%  Analysis Date = 08/11/13 
 Pct Recovery = 36%  Analysis Date = 08/08/13 
 Pct Recovery = 36%  Analysis Date = 08/08/13 
 Pct Recovery = 36%  Analysis Date = 08/06/13 
 Pct Recovery = 37%  Analysis Date = 08/06/13 
 Pct Recovery = 37%  Analysis Date = 08/04/13 
 Pct Recovery = 37%  Analysis Date = 08/04/13 
 Pct Recovery = 37%  Analysis Date = 08/02/13 
 Pct Recovery = 38%  Analysis Date = 08/02/13 
 Pct Recovery = 38%  Analysis Date = 07/30/13 
 Pct Recovery = 38%  Analysis Date = 07/30/13 
 Pct Recovery = 38%  Analysis Date = 07/28/13 
 Pct Recovery = 39%  Analysis Date = 07/28/13 
 Pct Recovery = 39%  Analysis Date = 07/26/13 
 Pct Recovery = 39%  Analysis Date = 07/26/13 
 Pct Recovery = 39%  Analysis Date = 07/23/13 
 Pct Recovery = 40%  Analysis Date = 07/23/13 
 Pct Recovery = 40%  Analysis Date = 07/21/13 
 Pct Recovery = 40%  Analysis Date = 07/21/13 
 Pct Recovery = 40%  Analysis Date = 07/19/13 
 Pct Recovery = 41%  Analysis Date = 07/19/13 
 Pct Recovery = 41%  Analysis Date = 07/16/13 
 Pct Recovery = 41%  Analysis Date = 07/16/13 
 Pct Recovery = 41%  Analysis Date = 07/14/13 
 Pct Recovery = 41%  Analysis Date = 07/14/13 
 Pct Recovery = 41%  Analysis Date = 07/12/13 
 Pct Recovery = 42%  Analysis Date = 07/12/13 
 Pct Recovery = 42%  Analysis Date = 07/09/13 
 Pct Recovery = 42%  Analysis Date = 07/09/13 
 Pct Recovery = 42%  Analysis Date = 07/07/13 
 Pct Recovery = 43%  Analysis Date = 07/07/13 
 Pct Recovery = 43%  Analysis Date = 07/05/13 
 Pct Recovery = 43%  Analysis Date = 07/05/13 
 Pct Recovery = 43%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 06/30/13 
 Pct Recovery = 44%  Analysis Date = 06/30/13 
 Pct Recovery = 44%  Analysis Date = 06/28/13 
 Pct Recovery = 45%  Analysis Date = 06/28/13 
 Pct Recovery = 45%  Analysis Date = 06/26/13 
 Pct Recovery = 45%  Analysis Date = 06/26/13 
 Pct Recovery = 45%  Analysis Date = 06/23/13 
 Pct Recovery = 45%  Analysis Date = 06/23/13 
 Pct Recovery = 45%  Analysis Date = 06/21/13 
 Pct Recovery = 46%  Analysis Date = 06/21/13 
 Pct Recovery = 46%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/14/13 
 Pct Recovery = 47%  Analysis Date = 06/14/13 
 Pct Recovery = 47%  Analysis Date = 06/12/13 
 Pct Recovery = 48%  Analysis Date = 06/12/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/05/13 
 Pct Recovery = 49%  Analysis Date = 06/05/13 
 Pct Recovery = 49%  Analysis Date = 06/02/13 
 Pct Recovery = 49%  Analysis Date = 06/02/13 
 Pct Recovery = 49%  Analysis Date = 05/31/13 
 Pct Recovery = 50%  Analysis Date = 05/31/13 
 Pct Recovery = 50%  Analysis Date = 05/29/13 
 Pct Recovery = 50%  Analysis Date = 05/29/13 
 Pct Recovery = 50%  Analysis Date = 05/27/13 
 Pct Recovery = 51%  Analysis Date = 05/27/13 
 Pct Recovery = 51%  Analysis Date = 05/24/13 
 Pct Recovery = 51%  Analysis Date = 05/24/13 
 Pct Recovery = 51%  Analysis Date = 05/22/13 
 Pct Recovery = 52%  Analysis Date = 05/22/13 
 Pct Recovery = 52%  Analysis Date = 05/20/13 
 Pct Recovery = 52%  Analysis Date = 05/20/13 
 Pct Recovery = 52%  Analysis Date = 05/17/13 
 Pct Recovery = 53%  Analysis Date = 05/17/13 
 Pct Recovery = 53%  Analysis Date = 05/15/13 
 Pct Recovery = 53%  Analysis Date = 05/15/13 
 Pct Recovery = 53%  Analysis Date = 05/13/13 
 Pct Recovery = 54%  Analysis Date = 05/13/13 
 Pct Recovery = 54%  Analysis Date = 05/10/13 
 Pct Recovery = 54%  Analysis Date = 05/10/13 
 Pct Recovery = 54%  Analysis Date = 05/08/13 
 Pct Recovery = 54%  Analysis Date = 05/08/13 
 Pct Recovery = 54%  Analysis Date = 05/06/13 
 Pct Recovery = 55%  Analysis Date = 05/06/13 
 Pct Recovery = 55%  Analysis Date = 05/03/13 
 Pct Recovery = 55%  Analysis Date = 05/03/13 
 Pct Recovery = 55%  Analysis Date = 05/01/13 
 Pct Recovery = 55%  Analysis Date = 05/01/13 
 Pct Recovery = 55%  Analysis Date = 04/29/13 
 Pct Recovery = 54%  Analysis Date = 04/29/13 
 Pct Recovery = 54%  Analysis Date = 04/26/13 
 Pct Recovery = 53%  Analysis Date = 04/26/13 
 Pct Recovery = 53%  Analysis Date = 04/24/13 
 Pct Recovery = 52%  Analysis Date = 04/24/13 
 Pct Recovery = 52%  Analysis Date = 04/22/13 
 Pct Recovery = 51%  Analysis Date = 04/22/13 
 Pct Recovery = 51%  Analysis Date = 04/20/13 
 Pct Recovery = 50%  Analysis Date = 04/20/13 
 Pct Recovery = 50%  Analysis Date = 04/17/13 
 Pct Recovery = 49%  Analysis Date = 04/17/13 
 Pct Recovery = 49%  Analysis Date = 04/15/13 
 Pct Recovery = 49%  Analysis Date = 04/15/13 
 Pct Recovery = 49%  Analysis Date = 04/13/13 
 Pct Recovery = 48%  Analysis Date = 04/13/13 
 Pct Recovery = 48%  Analysis Date = 04/10/13 
 Pct Recovery = 47%  Analysis Date = 04/10/13 
 Pct Recovery = 47%  Analysis Date = 04/08/13 
 Pct Recovery = 46%  Analysis Date = 04/08/13 
 Pct Recovery = 46%  Analysis Date = 04/06/13 
 Pct Recovery = 45%  Analysis Date = 04/06/13 
 Pct Recovery = 45%  Analysis Date = 04/03/13 
 Pct Recovery = 44%  Analysis Date = 04/03/13 
 Pct Recovery = 44%  Analysis Date = 04/01/13 
 Pct Recovery = 43%  Analysis Date = 04/01/13 
 Pct Recovery = 43%  Analysis Date = 03/30/13 
 Pct Recovery = 42%  Analysis Date = 03/30/13 
 Pct Recovery = 42%  Analysis Date = 03/27/13 
 Pct Recovery = 42%  Analysis Date = 03/27/13 
 Pct Recovery = 42%  Analysis Date = 03/25/13 
 Pct Recovery = 41%  Analysis Date = 03/25/13 
 Pct Recovery = 41%  Analysis Date = 03/23/13 
 Pct Recovery = 40%  Analysis Date = 03/23/13 
 Pct Recovery = 40%  Analysis Date = 03/21/13 
 Pct Recovery = 39%  Analysis Date = 03/21/13 
 Pct Recovery = 39%  Analysis Date = 03/18/13 
 Pct Recovery = 38%  Analysis Date = 03/18/13 
 Pct Recovery = 38%  Analysis Date = 03/16/13 
 Pct Recovery = 37%  Analysis Date = 03/16/13 
 Pct Recovery = 37%  Analysis Date = 03/14/13 
 Pct Recovery = 36%  Analysis Date = 03/14/13 
 Pct Recovery = 36%  Analysis Date = 03/11/13 
 Pct Recovery = 36%  Analysis Date = 03/11/13 
 Pct Recovery = 36%  Analysis Date = 03/09/13 
 Pct Recovery = 35%  Analysis Date = 03/09/13 
 Pct Recovery = 35%  Analysis Date = 03/07/13 
 Pct Recovery = 34%  Analysis Date = 03/07/13 
 Pct Recovery = 34%  Analysis Date = 03/04/13 
 Pct Recovery = 33%  Analysis Date = 03/04/13 
 Pct Recovery = 33%  Analysis Date = 03/02/13 
 Pct Recovery = 32%  Analysis Date = 03/02/13 
 Pct Recovery = 32%  Analysis Date = 02/28/13 
 Pct Recovery = 31%  Analysis Date = 02/28/13 
 Pct Recovery = 31%  Analysis Date = 02/25/13 
 Pct Recovery = 31%  Analysis Date = 02/25/13 
 Pct Recovery = 31%  Analysis Date = 02/23/13 
 Pct Recovery = 31%  Analysis Date = 02/23/13 
 Pct Recovery = 31%  Analysis Date = 02/21/13 
 Pct Recovery = 31%  Analysis Date = 02/21/13 
 Pct Recovery = 31%  Analysis Date = 02/18/13 
 Pct Recovery = 31%  Analysis Date = 02/18/13 
 Pct Recovery = 31%  Analysis Date = 02/16/13 
 Pct Recovery = 31%  Analysis Date = 02/16/13 
 Pct Recovery = 31%  Analysis Date = 02/14/13 
 Pct Recovery = 31%  Analysis Date = 02/14/13 
 Pct Recovery = 31%  Analysis Date = 02/12/13 
 Pct Recovery = 31%  Analysis Date = 02/12/13 
 Pct Recovery = 31%  Analysis Date = 02/09/13 
 Pct Recovery = 31%  Analysis Date = 02/09/13 
 Pct Recovery = 31%  Analysis Date = 02/07/13 
 Pct Recovery = 31%  Analysis Date = 02/07/13 
 Pct Recovery = 31%  Analysis Date = 02/05/13 
 Pct Recovery = 31%  Analysis Date = 02/05/13 
 Pct Recovery = 31%  Analysis Date = 02/02/13 
 Pct Recovery = 31%  Analysis Date = 02/02/13 
 Pct Recovery = 31%  Analysis Date = 01/31/13 
 Pct Recovery = 32%  Analysis Date = 01/31/13 
 Pct Recovery = 32%  Analysis Date = 01/29/13 
 Pct Recovery = 32%  Analysis Date = 01/29/13 
 Pct Recovery = 32%  Analysis Date = 01/26/13 
 Pct Recovery = 32%  Analysis Date = 01/26/13 
 Pct Recovery = 32%  Analysis Date = 01/24/13 
 Pct Recovery = 32%  Analysis Date = 01/24/13 
 Pct Recovery = 32%  Analysis Date = 01/22/13 
 Pct Recovery = 31%  Analysis Date = 01/22/13 
 Pct Recovery = 31%  Analysis Date = 01/19/13 
 Pct Recovery = 31%  Analysis Date = 01/19/13 
 Pct Recovery = 31%  Analysis Date = 01/17/13 
 Pct Recovery = 31%  Analysis Date = 01/17/13 
 Pct Recovery = 31%  Analysis Date = 01/15/13 
 Pct Recovery = 30%  Analysis Date = 01/15/13 
 Pct Recovery = 30%  Analysis Date = 01/13/13 
 Pct Recovery = 30%  Analysis Date = 01/13/13 
 Pct Recovery = 30%  Analysis Date = 01/10/13 
 Pct Recovery = 30%  Analysis Date = 01/10/13 
 Pct Recovery = 30%  Analysis Date = 01/08/13 
 Pct Recovery = 29%  Analysis Date = 01/08/13 
 Pct Recovery = 29%  Analysis Date = 01/06/13 
 Pct Recovery = 29%  Analysis Date = 01/06/13 
 Pct Recovery = 29%  Analysis Date = 01/03/13 
 Pct Recovery = 28%  Analysis Date = 01/03/13 
 Pct Recovery = 28%  Analysis Date = 01/01/13 
 Pct Recovery = 28%  Analysis Date = 01/01/13 
 Pct Recovery = 28%  Analysis Date = 12/30/12 
 Pct Recovery = 28%  Analysis Date = 12/30/12 
 Pct Recovery = 28%  Analysis Date = 12/27/12 
 Pct Recovery = 27%  Analysis Date = 12/27/12 
 Pct Recovery = 27%  Analysis Date = 12/25/12 
 Pct Recovery = 27%  Analysis Date = 12/25/12 
 Pct Recovery = 27%  Analysis Date = 12/23/12 
 Pct Recovery = 27%  Analysis Date = 12/23/12 
 Pct Recovery = 27%  Analysis Date = 12/20/12 
 Pct Recovery = 26%  Analysis Date = 12/20/12 
 Pct Recovery = 26%  Analysis Date = 12/18/12 
 Pct Recovery = 26%  Analysis Date = 12/18/12 
 Pct Recovery = 26%  Analysis Date = 12/16/12 
 Pct Recovery = 25%  Analysis Date = 12/16/12 
 Pct Recovery = 25%  Analysis Date = 12/14/12 
 Pct Recovery = 25%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIMETIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 9 38% 23% 40% 12%
Total 9 38% 23% 40% 12%

Sample Statistics
CIMETIDINE

Characteristic N % % Basis
Plotted 9 82% Spiked
Estimated Values 9 82% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 2 18% 2 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
CITALOPRAM
METHOD: LC9017 , TESTIDCODE: 67505LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 53%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 25%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 67%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 56%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 21%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 44%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 64%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 28%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 49%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 55%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 Pct Recovery = 55%  Analysis Date = 03/18/14 
 Pct Recovery = 54%  Analysis Date = 03/18/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/02/14 
 Pct Recovery = 50%  Analysis Date = 03/02/14 
 Pct Recovery = 50%  Analysis Date = 02/28/14 
 Pct Recovery = 49%  Analysis Date = 02/28/14 
 Pct Recovery = 49%  Analysis Date = 02/25/14 
 Pct Recovery = 49%  Analysis Date = 02/25/14 
 Pct Recovery = 49%  Analysis Date = 02/23/14 
 Pct Recovery = 48%  Analysis Date = 02/23/14 
 Pct Recovery = 48%  Analysis Date = 02/21/14 
 Pct Recovery = 47%  Analysis Date = 02/21/14 
 Pct Recovery = 47%  Analysis Date = 02/18/14 
 Pct Recovery = 47%  Analysis Date = 02/18/14 
 Pct Recovery = 47%  Analysis Date = 02/16/14 
 Pct Recovery = 46%  Analysis Date = 02/16/14 
 Pct Recovery = 46%  Analysis Date = 02/14/14 
 Pct Recovery = 45%  Analysis Date = 02/14/14 
 Pct Recovery = 45%  Analysis Date = 02/12/14 
 Pct Recovery = 45%  Analysis Date = 02/12/14 
 Pct Recovery = 45%  Analysis Date = 02/09/14 
 Pct Recovery = 44%  Analysis Date = 02/09/14 
 Pct Recovery = 44%  Analysis Date = 02/07/14 
 Pct Recovery = 43%  Analysis Date = 02/07/14 
 Pct Recovery = 43%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 01/31/14 
 Pct Recovery = 41%  Analysis Date = 01/31/14 
 Pct Recovery = 41%  Analysis Date = 01/29/14 
 Pct Recovery = 41%  Analysis Date = 01/29/14 
 Pct Recovery = 41%  Analysis Date = 01/26/14 
 Pct Recovery = 40%  Analysis Date = 01/26/14 
 Pct Recovery = 40%  Analysis Date = 01/24/14 
 Pct Recovery = 39%  Analysis Date = 01/24/14 
 Pct Recovery = 39%  Analysis Date = 01/22/14 
 Pct Recovery = 39%  Analysis Date = 01/22/14 
 Pct Recovery = 39%  Analysis Date = 01/19/14 
 Pct Recovery = 38%  Analysis Date = 01/19/14 
 Pct Recovery = 38%  Analysis Date = 01/17/14 
 Pct Recovery = 37%  Analysis Date = 01/17/14 
 Pct Recovery = 37%  Analysis Date = 01/15/14 
 Pct Recovery = 37%  Analysis Date = 01/15/14 
 Pct Recovery = 37%  Analysis Date = 01/13/14 
 Pct Recovery = 36%  Analysis Date = 01/13/14 
 Pct Recovery = 36%  Analysis Date = 01/10/14 
 Pct Recovery = 35%  Analysis Date = 01/10/14 
 Pct Recovery = 35%  Analysis Date = 01/08/14 
 Pct Recovery = 35%  Analysis Date = 01/08/14 
 Pct Recovery = 35%  Analysis Date = 01/06/14 
 Pct Recovery = 34%  Analysis Date = 01/06/14 
 Pct Recovery = 34%  Analysis Date = 01/03/14 
 Pct Recovery = 33%  Analysis Date = 01/03/14 
 Pct Recovery = 33%  Analysis Date = 01/01/14 
 Pct Recovery = 33%  Analysis Date = 01/01/14 
 Pct Recovery = 33%  Analysis Date = 12/30/13 
 Pct Recovery = 32%  Analysis Date = 12/30/13 
 Pct Recovery = 32%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/25/13 
 Pct Recovery = 31%  Analysis Date = 12/25/13 
 Pct Recovery = 31%  Analysis Date = 12/23/13 
 Pct Recovery = 30%  Analysis Date = 12/23/13 
 Pct Recovery = 30%  Analysis Date = 12/20/13 
 Pct Recovery = 29%  Analysis Date = 12/20/13 
 Pct Recovery = 29%  Analysis Date = 12/18/13 
 Pct Recovery = 28%  Analysis Date = 12/18/13 
 Pct Recovery = 28%  Analysis Date = 12/16/13 
 Pct Recovery = 28%  Analysis Date = 12/16/13 
 Pct Recovery = 28%  Analysis Date = 12/13/13 
 Pct Recovery = 27%  Analysis Date = 12/13/13 
 Pct Recovery = 27%  Analysis Date = 12/11/13 
 Pct Recovery = 26%  Analysis Date = 12/11/13 
 Pct Recovery = 26%  Analysis Date = 12/09/13 
 Pct Recovery = 26%  Analysis Date = 12/09/13 
 Pct Recovery = 26%  Analysis Date = 12/07/13 
 Pct Recovery = 25%  Analysis Date = 12/07/13 
 Pct Recovery = 25%  Analysis Date = 12/04/13 
 Pct Recovery = 25%  Analysis Date = 12/04/13 
 Pct Recovery = 25%  Analysis Date = 12/02/13 
 Pct Recovery = 25%  Analysis Date = 12/02/13 
 Pct Recovery = 25%  Analysis Date = 11/30/13 
 Pct Recovery = 26%  Analysis Date = 11/30/13 
 Pct Recovery = 26%  Analysis Date = 11/27/13 
 Pct Recovery = 26%  Analysis Date = 11/27/13 
 Pct Recovery = 26%  Analysis Date = 11/25/13 
 Pct Recovery = 27%  Analysis Date = 11/25/13 
 Pct Recovery = 27%  Analysis Date = 11/23/13 
 Pct Recovery = 28%  Analysis Date = 11/23/13 
 Pct Recovery = 28%  Analysis Date = 11/20/13 
 Pct Recovery = 28%  Analysis Date = 11/20/13 
 Pct Recovery = 28%  Analysis Date = 11/18/13 
 Pct Recovery = 29%  Analysis Date = 11/18/13 
 Pct Recovery = 29%  Analysis Date = 11/16/13 
 Pct Recovery = 29%  Analysis Date = 11/16/13 
 Pct Recovery = 29%  Analysis Date = 11/13/13 
 Pct Recovery = 30%  Analysis Date = 11/13/13 
 Pct Recovery = 30%  Analysis Date = 11/11/13 
 Pct Recovery = 31%  Analysis Date = 11/11/13 
 Pct Recovery = 31%  Analysis Date = 11/09/13 
 Pct Recovery = 31%  Analysis Date = 11/09/13 
 Pct Recovery = 31%  Analysis Date = 11/07/13 
 Pct Recovery = 32%  Analysis Date = 11/07/13 
 Pct Recovery = 32%  Analysis Date = 11/04/13 
 Pct Recovery = 33%  Analysis Date = 11/04/13 
 Pct Recovery = 33%  Analysis Date = 11/02/13 
 Pct Recovery = 33%  Analysis Date = 11/02/13 
 Pct Recovery = 33%  Analysis Date = 10/31/13 
 Pct Recovery = 34%  Analysis Date = 10/31/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/26/13 
 Pct Recovery = 35%  Analysis Date = 10/26/13 
 Pct Recovery = 35%  Analysis Date = 10/24/13 
 Pct Recovery = 36%  Analysis Date = 10/24/13 
 Pct Recovery = 36%  Analysis Date = 10/21/13 
 Pct Recovery = 36%  Analysis Date = 10/21/13 
 Pct Recovery = 36%  Analysis Date = 10/19/13 
 Pct Recovery = 37%  Analysis Date = 10/19/13 
 Pct Recovery = 37%  Analysis Date = 10/17/13 
 Pct Recovery = 38%  Analysis Date = 10/17/13 
 Pct Recovery = 38%  Analysis Date = 10/14/13 
 Pct Recovery = 38%  Analysis Date = 10/14/13 
 Pct Recovery = 38%  Analysis Date = 10/12/13 
 Pct Recovery = 39%  Analysis Date = 10/12/13 
 Pct Recovery = 39%  Analysis Date = 10/10/13 
 Pct Recovery = 39%  Analysis Date = 10/10/13 
 Pct Recovery = 39%  Analysis Date = 10/07/13 
 Pct Recovery = 40%  Analysis Date = 10/07/13 
 Pct Recovery = 40%  Analysis Date = 10/05/13 
 Pct Recovery = 41%  Analysis Date = 10/05/13 
 Pct Recovery = 41%  Analysis Date = 10/03/13 
 Pct Recovery = 41%  Analysis Date = 10/03/13 
 Pct Recovery = 41%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 10/01/13 
 Pct Recovery = 42%  Analysis Date = 09/28/13 
 Pct Recovery = 42%  Analysis Date = 09/28/13 
 Pct Recovery = 42%  Analysis Date = 09/26/13 
 Pct Recovery = 43%  Analysis Date = 09/26/13 
 Pct Recovery = 43%  Analysis Date = 09/24/13 
 Pct Recovery = 44%  Analysis Date = 09/24/13 
 Pct Recovery = 44%  Analysis Date = 09/21/13 
 Pct Recovery = 44%  Analysis Date = 09/21/13 
 Pct Recovery = 44%  Analysis Date = 09/19/13 
 Pct Recovery = 45%  Analysis Date = 09/19/13 
 Pct Recovery = 45%  Analysis Date = 09/17/13 
 Pct Recovery = 46%  Analysis Date = 09/17/13 
 Pct Recovery = 46%  Analysis Date = 09/14/13 
 Pct Recovery = 46%  Analysis Date = 09/14/13 
 Pct Recovery = 46%  Analysis Date = 09/12/13 
 Pct Recovery = 47%  Analysis Date = 09/12/13 
 Pct Recovery = 47%  Analysis Date = 09/10/13 
 Pct Recovery = 47%  Analysis Date = 09/10/13 
 Pct Recovery = 47%  Analysis Date = 09/07/13 
 Pct Recovery = 48%  Analysis Date = 09/07/13 
 Pct Recovery = 48%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/03/13 
 Pct Recovery = 49%  Analysis Date = 09/03/13 
 Pct Recovery = 49%  Analysis Date = 09/01/13 
 Pct Recovery = 50%  Analysis Date = 09/01/13 
 Pct Recovery = 50%  Analysis Date = 08/29/13 
 Pct Recovery = 50%  Analysis Date = 08/29/13 
 Pct Recovery = 50%  Analysis Date = 08/27/13 
 Pct Recovery = 51%  Analysis Date = 08/27/13 
 Pct Recovery = 51%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/20/13 
 Pct Recovery = 53%  Analysis Date = 08/20/13 
 Pct Recovery = 53%  Analysis Date = 08/18/13 
 Pct Recovery = 53%  Analysis Date = 08/18/13 
 Pct Recovery = 53%  Analysis Date = 08/15/13 
 Pct Recovery = 54%  Analysis Date = 08/15/13 
 Pct Recovery = 54%  Analysis Date = 08/13/13 
 Pct Recovery = 54%  Analysis Date = 08/13/13 
 Pct Recovery = 54%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 54%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/02/13 
 Pct Recovery = 55%  Analysis Date = 08/02/13 
 Pct Recovery = 55%  Analysis Date = 07/30/13 
 Pct Recovery = 54%  Analysis Date = 07/30/13 
 Pct Recovery = 54%  Analysis Date = 07/28/13 
 Pct Recovery = 54%  Analysis Date = 07/28/13 
 Pct Recovery = 54%  Analysis Date = 07/26/13 
 Pct Recovery = 54%  Analysis Date = 07/26/13 
 Pct Recovery = 54%  Analysis Date = 07/23/13 
 Pct Recovery = 53%  Analysis Date = 07/23/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 52%  Analysis Date = 07/19/13 
 Pct Recovery = 52%  Analysis Date = 07/16/13 
 Pct Recovery = 52%  Analysis Date = 07/16/13 
 Pct Recovery = 52%  Analysis Date = 07/14/13 
 Pct Recovery = 52%  Analysis Date = 07/14/13 
 Pct Recovery = 52%  Analysis Date = 07/12/13 
 Pct Recovery = 51%  Analysis Date = 07/12/13 
 Pct Recovery = 51%  Analysis Date = 07/09/13 
 Pct Recovery = 51%  Analysis Date = 07/09/13 
 Pct Recovery = 51%  Analysis Date = 07/07/13 
 Pct Recovery = 50%  Analysis Date = 07/07/13 
 Pct Recovery = 50%  Analysis Date = 07/05/13 
 Pct Recovery = 50%  Analysis Date = 07/05/13 
 Pct Recovery = 50%  Analysis Date = 07/02/13 
 Pct Recovery = 50%  Analysis Date = 07/02/13 
 Pct Recovery = 50%  Analysis Date = 06/30/13 
 Pct Recovery = 49%  Analysis Date = 06/30/13 
 Pct Recovery = 49%  Analysis Date = 06/28/13 
 Pct Recovery = 49%  Analysis Date = 06/28/13 
 Pct Recovery = 49%  Analysis Date = 06/26/13 
 Pct Recovery = 48%  Analysis Date = 06/26/13 
 Pct Recovery = 48%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/19/13 
 Pct Recovery = 47%  Analysis Date = 06/19/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/14/13 
 Pct Recovery = 46%  Analysis Date = 06/14/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/02/13 
 Pct Recovery = 44%  Analysis Date = 06/02/13 
 Pct Recovery = 44%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/27/13 
 Pct Recovery = 43%  Analysis Date = 05/27/13 
 Pct Recovery = 43%  Analysis Date = 05/24/13 
 Pct Recovery = 43%  Analysis Date = 05/24/13 
 Pct Recovery = 43%  Analysis Date = 05/22/13 
 Pct Recovery = 42%  Analysis Date = 05/22/13 
 Pct Recovery = 42%  Analysis Date = 05/20/13 
 Pct Recovery = 42%  Analysis Date = 05/20/13 
 Pct Recovery = 42%  Analysis Date = 05/17/13 
 Pct Recovery = 42%  Analysis Date = 05/17/13 
 Pct Recovery = 42%  Analysis Date = 05/15/13 
 Pct Recovery = 41%  Analysis Date = 05/15/13 
 Pct Recovery = 41%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/10/13 
 Pct Recovery = 41%  Analysis Date = 05/10/13 
 Pct Recovery = 41%  Analysis Date = 05/08/13 
 Pct Recovery = 40%  Analysis Date = 05/08/13 
 Pct Recovery = 40%  Analysis Date = 05/06/13 
 Pct Recovery = 40%  Analysis Date = 05/06/13 
 Pct Recovery = 40%  Analysis Date = 05/03/13 
 Pct Recovery = 39%  Analysis Date = 05/03/13 
 Pct Recovery = 39%  Analysis Date = 05/01/13 
 Pct Recovery = 39%  Analysis Date = 05/01/13 
 Pct Recovery = 39%  Analysis Date = 04/29/13 
 Pct Recovery = 39%  Analysis Date = 04/29/13 
 Pct Recovery = 39%  Analysis Date = 04/26/13 
 Pct Recovery = 39%  Analysis Date = 04/26/13 
 Pct Recovery = 39%  Analysis Date = 04/24/13 
 Pct Recovery = 39%  Analysis Date = 04/24/13 
 Pct Recovery = 39%  Analysis Date = 04/22/13 
 Pct Recovery = 39%  Analysis Date = 04/22/13 
 Pct Recovery = 39%  Analysis Date = 04/20/13 
 Pct Recovery = 39%  Analysis Date = 04/20/13 
 Pct Recovery = 39%  Analysis Date = 04/17/13 
 Pct Recovery = 40%  Analysis Date = 04/17/13 
 Pct Recovery = 40%  Analysis Date = 04/15/13 
 Pct Recovery = 40%  Analysis Date = 04/15/13 
 Pct Recovery = 40%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/10/13 
 Pct Recovery = 40%  Analysis Date = 04/10/13 
 Pct Recovery = 40%  Analysis Date = 04/08/13 
 Pct Recovery = 40%  Analysis Date = 04/08/13 
 Pct Recovery = 40%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 40%  Analysis Date = 03/27/13 
 Pct Recovery = 40%  Analysis Date = 03/27/13 
 Pct Recovery = 40%  Analysis Date = 03/25/13 
 Pct Recovery = 41%  Analysis Date = 03/25/13 
 Pct Recovery = 41%  Analysis Date = 03/23/13 
 Pct Recovery = 41%  Analysis Date = 03/23/13 
 Pct Recovery = 41%  Analysis Date = 03/21/13 
 Pct Recovery = 42%  Analysis Date = 03/21/13 
 Pct Recovery = 42%  Analysis Date = 03/18/13 
 Pct Recovery = 42%  Analysis Date = 03/18/13 
 Pct Recovery = 42%  Analysis Date = 03/16/13 
 Pct Recovery = 43%  Analysis Date = 03/16/13 
 Pct Recovery = 43%  Analysis Date = 03/14/13 
 Pct Recovery = 43%  Analysis Date = 03/14/13 
 Pct Recovery = 43%  Analysis Date = 03/11/13 
 Pct Recovery = 44%  Analysis Date = 03/11/13 
 Pct Recovery = 44%  Analysis Date = 03/09/13 
 Pct Recovery = 44%  Analysis Date = 03/09/13 
 Pct Recovery = 44%  Analysis Date = 03/07/13 
 Pct Recovery = 45%  Analysis Date = 03/07/13 
 Pct Recovery = 45%  Analysis Date = 03/04/13 
 Pct Recovery = 45%  Analysis Date = 03/04/13 
 Pct Recovery = 45%  Analysis Date = 03/02/13 
 Pct Recovery = 46%  Analysis Date = 03/02/13 
 Pct Recovery = 46%  Analysis Date = 02/28/13 
 Pct Recovery = 46%  Analysis Date = 02/28/13 
 Pct Recovery = 46%  Analysis Date = 02/25/13 
 Pct Recovery = 47%  Analysis Date = 02/25/13 
 Pct Recovery = 47%  Analysis Date = 02/23/13 
 Pct Recovery = 47%  Analysis Date = 02/23/13 
 Pct Recovery = 47%  Analysis Date = 02/21/13 
 Pct Recovery = 48%  Analysis Date = 02/21/13 
 Pct Recovery = 48%  Analysis Date = 02/18/13 
 Pct Recovery = 48%  Analysis Date = 02/18/13 
 Pct Recovery = 48%  Analysis Date = 02/16/13 
 Pct Recovery = 49%  Analysis Date = 02/16/13 
 Pct Recovery = 49%  Analysis Date = 02/14/13 
 Pct Recovery = 49%  Analysis Date = 02/14/13 
 Pct Recovery = 49%  Analysis Date = 02/12/13 
 Pct Recovery = 50%  Analysis Date = 02/12/13 
 Pct Recovery = 50%  Analysis Date = 02/09/13 
 Pct Recovery = 50%  Analysis Date = 02/09/13 
 Pct Recovery = 50%  Analysis Date = 02/07/13 
 Pct Recovery = 51%  Analysis Date = 02/07/13 
 Pct Recovery = 51%  Analysis Date = 02/05/13 
 Pct Recovery = 52%  Analysis Date = 02/05/13 
 Pct Recovery = 52%  Analysis Date = 02/02/13 
 Pct Recovery = 52%  Analysis Date = 02/02/13 
 Pct Recovery = 52%  Analysis Date = 01/31/13 
 Pct Recovery = 53%  Analysis Date = 01/31/13 
 Pct Recovery = 53%  Analysis Date = 01/29/13 
 Pct Recovery = 53%  Analysis Date = 01/29/13 
 Pct Recovery = 53%  Analysis Date = 01/26/13 
 Pct Recovery = 54%  Analysis Date = 01/26/13 
 Pct Recovery = 54%  Analysis Date = 01/24/13 
 Pct Recovery = 54%  Analysis Date = 01/24/13 
 Pct Recovery = 54%  Analysis Date = 01/22/13 
 Pct Recovery = 55%  Analysis Date = 01/22/13 
 Pct Recovery = 55%  Analysis Date = 01/19/13 
 Pct Recovery = 55%  Analysis Date = 01/19/13 
 Pct Recovery = 55%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/13/13 
 Pct Recovery = 57%  Analysis Date = 01/13/13 
 Pct Recovery = 57%  Analysis Date = 01/10/13 
 Pct Recovery = 57%  Analysis Date = 01/10/13 
 Pct Recovery = 57%  Analysis Date = 01/08/13 
 Pct Recovery = 58%  Analysis Date = 01/08/13 
 Pct Recovery = 58%  Analysis Date = 01/06/13 
 Pct Recovery = 58%  Analysis Date = 01/06/13 
 Pct Recovery = 58%  Analysis Date = 01/03/13 
 Pct Recovery = 59%  Analysis Date = 01/03/13 
 Pct Recovery = 59%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/27/12 
 Pct Recovery = 61%  Analysis Date = 12/27/12 
 Pct Recovery = 61%  Analysis Date = 12/25/12 
 Pct Recovery = 61%  Analysis Date = 12/25/12 
 Pct Recovery = 61%  Analysis Date = 12/23/12 
 Pct Recovery = 62%  Analysis Date = 12/23/12 
 Pct Recovery = 62%  Analysis Date = 12/20/12 
 Pct Recovery = 62%  Analysis Date = 12/20/12 
 Pct Recovery = 62%  Analysis Date = 12/18/12 
 Pct Recovery = 63%  Analysis Date = 12/18/12 
 Pct Recovery = 63%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/14/12 
 Pct Recovery = 64%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CITALOPRAM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 46% . 46% 0%
>= Reporting Level 12 48% 15% 52% 16%
Total 13 48% 15% 52% 9%

Sample Statistics
CITALOPRAM

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
CLONIDINE
METHOD: LC9017 , TESTIDCODE: 67518LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 103%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 80%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 90%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 79%  Analysis Date = 03/20/14 
 Pct Recovery = 80%  Analysis Date = 03/18/14 
 Pct Recovery = 81%  Analysis Date = 03/18/14 
 Pct Recovery = 81%  Analysis Date = 03/16/14 
 Pct Recovery = 81%  Analysis Date = 03/16/14 
 Pct Recovery = 81%  Analysis Date = 03/14/14 
 Pct Recovery = 82%  Analysis Date = 03/14/14 
 Pct Recovery = 82%  Analysis Date = 03/12/14 
 Pct Recovery = 83%  Analysis Date = 03/12/14 
 Pct Recovery = 83%  Analysis Date = 03/10/14 
 Pct Recovery = 83%  Analysis Date = 03/10/14 
 Pct Recovery = 83%  Analysis Date = 03/08/14 
 Pct Recovery = 84%  Analysis Date = 03/08/14 
 Pct Recovery = 84%  Analysis Date = 03/06/14 
 Pct Recovery = 85%  Analysis Date = 03/06/14 
 Pct Recovery = 85%  Analysis Date = 03/04/14 
 Pct Recovery = 85%  Analysis Date = 03/04/14 
 Pct Recovery = 85%  Analysis Date = 03/02/14 
 Pct Recovery = 86%  Analysis Date = 03/02/14 
 Pct Recovery = 86%  Analysis Date = 02/27/14 
 Pct Recovery = 87%  Analysis Date = 02/27/14 
 Pct Recovery = 87%  Analysis Date = 02/25/14 
 Pct Recovery = 87%  Analysis Date = 02/25/14 
 Pct Recovery = 87%  Analysis Date = 02/23/14 
 Pct Recovery = 88%  Analysis Date = 02/23/14 
 Pct Recovery = 88%  Analysis Date = 02/21/14 
 Pct Recovery = 89%  Analysis Date = 02/21/14 
 Pct Recovery = 89%  Analysis Date = 02/19/14 
 Pct Recovery = 89%  Analysis Date = 02/19/14 
 Pct Recovery = 89%  Analysis Date = 02/17/14 
 Pct Recovery = 89%  Analysis Date = 02/17/14 
 Pct Recovery = 89%  Analysis Date = 02/15/14 
 Pct Recovery = 87%  Analysis Date = 02/15/14 
 Pct Recovery = 87%  Analysis Date = 02/13/14 
 Pct Recovery = 86%  Analysis Date = 02/13/14 
 Pct Recovery = 86%  Analysis Date = 02/11/14 
 Pct Recovery = 84%  Analysis Date = 02/11/14 
 Pct Recovery = 84%  Analysis Date = 02/09/14 
 Pct Recovery = 83%  Analysis Date = 02/09/14 
 Pct Recovery = 83%  Analysis Date = 02/06/14 
 Pct Recovery = 81%  Analysis Date = 02/06/14 
 Pct Recovery = 81%  Analysis Date = 02/04/14 
 Pct Recovery = 80%  Analysis Date = 02/04/14 
 Pct Recovery = 80%  Analysis Date = 02/02/14 
 Pct Recovery = 78%  Analysis Date = 02/02/14 
 Pct Recovery = 78%  Analysis Date = 01/31/14 
 Pct Recovery = 77%  Analysis Date = 01/31/14 
 Pct Recovery = 77%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 72%  Analysis Date = 01/25/14 
 Pct Recovery = 72%  Analysis Date = 01/23/14 
 Pct Recovery = 71%  Analysis Date = 01/23/14 
 Pct Recovery = 71%  Analysis Date = 01/21/14 
 Pct Recovery = 69%  Analysis Date = 01/21/14 
 Pct Recovery = 69%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/16/14 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 Pct Recovery = 66%  Analysis Date = 01/14/14 
 Pct Recovery = 66%  Analysis Date = 01/14/14 
 Pct Recovery = 66%  Analysis Date = 01/12/14 
 Pct Recovery = 66%  Analysis Date = 01/12/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/08/14 
 Pct Recovery = 67%  Analysis Date = 01/08/14 
 Pct Recovery = 67%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/04/14 
 Pct Recovery = 68%  Analysis Date = 01/04/14 
 Pct Recovery = 68%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 12/31/13 
 Pct Recovery = 69%  Analysis Date = 12/31/13 
 Pct Recovery = 69%  Analysis Date = 12/28/13 
 Pct Recovery = 70%  Analysis Date = 12/28/13 
 Pct Recovery = 70%  Analysis Date = 12/26/13 
 Pct Recovery = 70%  Analysis Date = 12/26/13 
 Pct Recovery = 70%  Analysis Date = 12/24/13 
 Pct Recovery = 71%  Analysis Date = 12/24/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 72%  Analysis Date = 12/20/13 
 Pct Recovery = 72%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 73%  Analysis Date = 12/16/13 
 Pct Recovery = 73%  Analysis Date = 12/14/13 
 Pct Recovery = 73%  Analysis Date = 12/14/13 
 Pct Recovery = 73%  Analysis Date = 12/12/13 
 Pct Recovery = 74%  Analysis Date = 12/12/13 
 Pct Recovery = 74%  Analysis Date = 12/09/13 
 Pct Recovery = 74%  Analysis Date = 12/09/13 
 Pct Recovery = 74%  Analysis Date = 12/07/13 
 Pct Recovery = 75%  Analysis Date = 12/07/13 
 Pct Recovery = 75%  Analysis Date = 12/05/13 
 Pct Recovery = 75%  Analysis Date = 12/05/13 
 Pct Recovery = 75%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 12/01/13 
 Pct Recovery = 76%  Analysis Date = 12/01/13 
 Pct Recovery = 76%  Analysis Date = 11/29/13 
 Pct Recovery = 77%  Analysis Date = 11/29/13 
 Pct Recovery = 77%  Analysis Date = 11/27/13 
 Pct Recovery = 77%  Analysis Date = 11/27/13 
 Pct Recovery = 77%  Analysis Date = 11/25/13 
 Pct Recovery = 78%  Analysis Date = 11/25/13 
 Pct Recovery = 78%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/21/13 
 Pct Recovery = 79%  Analysis Date = 11/21/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/14/13 
 Pct Recovery = 79%  Analysis Date = 11/14/13 
 Pct Recovery = 79%  Analysis Date = 11/12/13 
 Pct Recovery = 80%  Analysis Date = 11/12/13 
 Pct Recovery = 80%  Analysis Date = 11/10/13 
 Pct Recovery = 80%  Analysis Date = 11/10/13 
 Pct Recovery = 80%  Analysis Date = 11/08/13 
 Pct Recovery = 80%  Analysis Date = 11/08/13 
 Pct Recovery = 80%  Analysis Date = 11/06/13 
 Pct Recovery = 80%  Analysis Date = 11/06/13 
 Pct Recovery = 80%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/02/13 
 Pct Recovery = 80%  Analysis Date = 11/02/13 
 Pct Recovery = 80%  Analysis Date = 10/30/13 
 Pct Recovery = 80%  Analysis Date = 10/30/13 
 Pct Recovery = 80%  Analysis Date = 10/28/13 
 Pct Recovery = 81%  Analysis Date = 10/28/13 
 Pct Recovery = 81%  Analysis Date = 10/26/13 
 Pct Recovery = 81%  Analysis Date = 10/26/13 
 Pct Recovery = 81%  Analysis Date = 10/24/13 
 Pct Recovery = 81%  Analysis Date = 10/24/13 
 Pct Recovery = 81%  Analysis Date = 10/22/13 
 Pct Recovery = 81%  Analysis Date = 10/22/13 
 Pct Recovery = 81%  Analysis Date = 10/20/13 
 Pct Recovery = 81%  Analysis Date = 10/20/13 
 Pct Recovery = 81%  Analysis Date = 10/18/13 
 Pct Recovery = 81%  Analysis Date = 10/18/13 
 Pct Recovery = 81%  Analysis Date = 10/16/13 
 Pct Recovery = 82%  Analysis Date = 10/16/13 
 Pct Recovery = 82%  Analysis Date = 10/14/13 
 Pct Recovery = 82%  Analysis Date = 10/14/13 
 Pct Recovery = 82%  Analysis Date = 10/12/13 
 Pct Recovery = 82%  Analysis Date = 10/12/13 
 Pct Recovery = 82%  Analysis Date = 10/09/13 
 Pct Recovery = 82%  Analysis Date = 10/09/13 
 Pct Recovery = 82%  Analysis Date = 10/07/13 
 Pct Recovery = 82%  Analysis Date = 10/07/13 
 Pct Recovery = 82%  Analysis Date = 10/05/13 
 Pct Recovery = 82%  Analysis Date = 10/05/13 
 Pct Recovery = 82%  Analysis Date = 10/03/13 
 Pct Recovery = 82%  Analysis Date = 10/03/13 
 Pct Recovery = 82%  Analysis Date = 10/01/13 
 Pct Recovery = 83%  Analysis Date = 10/01/13 
 Pct Recovery = 83%  Analysis Date = 09/29/13 
 Pct Recovery = 83%  Analysis Date = 09/29/13 
 Pct Recovery = 83%  Analysis Date = 09/27/13 
 Pct Recovery = 83%  Analysis Date = 09/27/13 
 Pct Recovery = 83%  Analysis Date = 09/25/13 
 Pct Recovery = 83%  Analysis Date = 09/25/13 
 Pct Recovery = 83%  Analysis Date = 09/23/13 
 Pct Recovery = 83%  Analysis Date = 09/23/13 
 Pct Recovery = 83%  Analysis Date = 09/20/13 
 Pct Recovery = 83%  Analysis Date = 09/20/13 
 Pct Recovery = 83%  Analysis Date = 09/18/13 
 Pct Recovery = 84%  Analysis Date = 09/18/13 
 Pct Recovery = 84%  Analysis Date = 09/16/13 
 Pct Recovery = 84%  Analysis Date = 09/16/13 
 Pct Recovery = 84%  Analysis Date = 09/14/13 
 Pct Recovery = 84%  Analysis Date = 09/14/13 
 Pct Recovery = 84%  Analysis Date = 09/12/13 
 Pct Recovery = 84%  Analysis Date = 09/12/13 
 Pct Recovery = 84%  Analysis Date = 09/10/13 
 Pct Recovery = 84%  Analysis Date = 09/10/13 
 Pct Recovery = 84%  Analysis Date = 09/08/13 
 Pct Recovery = 84%  Analysis Date = 09/08/13 
 Pct Recovery = 84%  Analysis Date = 09/06/13 
 Pct Recovery = 84%  Analysis Date = 09/06/13 
 Pct Recovery = 84%  Analysis Date = 09/04/13 
 Pct Recovery = 85%  Analysis Date = 09/04/13 
 Pct Recovery = 85%  Analysis Date = 09/02/13 
 Pct Recovery = 85%  Analysis Date = 09/02/13 
 Pct Recovery = 85%  Analysis Date = 08/30/13 
 Pct Recovery = 85%  Analysis Date = 08/30/13 
 Pct Recovery = 85%  Analysis Date = 08/28/13 
 Pct Recovery = 85%  Analysis Date = 08/28/13 
 Pct Recovery = 85%  Analysis Date = 08/26/13 
 Pct Recovery = 85%  Analysis Date = 08/26/13 
 Pct Recovery = 85%  Analysis Date = 08/24/13 
 Pct Recovery = 85%  Analysis Date = 08/24/13 
 Pct Recovery = 85%  Analysis Date = 08/22/13 
 Pct Recovery = 86%  Analysis Date = 08/22/13 
 Pct Recovery = 86%  Analysis Date = 08/20/13 
 Pct Recovery = 86%  Analysis Date = 08/20/13 
 Pct Recovery = 86%  Analysis Date = 08/18/13 
 Pct Recovery = 86%  Analysis Date = 08/18/13 
 Pct Recovery = 86%  Analysis Date = 08/16/13 
 Pct Recovery = 86%  Analysis Date = 08/16/13 
 Pct Recovery = 86%  Analysis Date = 08/14/13 
 Pct Recovery = 86%  Analysis Date = 08/14/13 
 Pct Recovery = 86%  Analysis Date = 08/11/13 
 Pct Recovery = 86%  Analysis Date = 08/11/13 
 Pct Recovery = 86%  Analysis Date = 08/09/13 
 Pct Recovery = 86%  Analysis Date = 08/09/13 
 Pct Recovery = 86%  Analysis Date = 08/07/13 
 Pct Recovery = 87%  Analysis Date = 08/07/13 
 Pct Recovery = 87%  Analysis Date = 08/05/13 
 Pct Recovery = 87%  Analysis Date = 08/05/13 
 Pct Recovery = 87%  Analysis Date = 08/03/13 
 Pct Recovery = 87%  Analysis Date = 08/03/13 
 Pct Recovery = 87%  Analysis Date = 08/01/13 
 Pct Recovery = 87%  Analysis Date = 08/01/13 
 Pct Recovery = 87%  Analysis Date = 07/30/13 
 Pct Recovery = 87%  Analysis Date = 07/30/13 
 Pct Recovery = 87%  Analysis Date = 07/28/13 
 Pct Recovery = 87%  Analysis Date = 07/28/13 
 Pct Recovery = 87%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/24/13 
 Pct Recovery = 88%  Analysis Date = 07/24/13 
 Pct Recovery = 88%  Analysis Date = 07/21/13 
 Pct Recovery = 88%  Analysis Date = 07/21/13 
 Pct Recovery = 88%  Analysis Date = 07/19/13 
 Pct Recovery = 88%  Analysis Date = 07/19/13 
 Pct Recovery = 88%  Analysis Date = 07/17/13 
 Pct Recovery = 88%  Analysis Date = 07/17/13 
 Pct Recovery = 88%  Analysis Date = 07/15/13 
 Pct Recovery = 88%  Analysis Date = 07/15/13 
 Pct Recovery = 88%  Analysis Date = 07/13/13 
 Pct Recovery = 88%  Analysis Date = 07/13/13 
 Pct Recovery = 88%  Analysis Date = 07/11/13 
 Pct Recovery = 89%  Analysis Date = 07/11/13 
 Pct Recovery = 89%  Analysis Date = 07/09/13 
 Pct Recovery = 89%  Analysis Date = 07/09/13 
 Pct Recovery = 89%  Analysis Date = 07/07/13 
 Pct Recovery = 89%  Analysis Date = 07/07/13 
 Pct Recovery = 89%  Analysis Date = 07/05/13 
 Pct Recovery = 89%  Analysis Date = 07/05/13 
 Pct Recovery = 89%  Analysis Date = 07/02/13 
 Pct Recovery = 89%  Analysis Date = 07/02/13 
 Pct Recovery = 89%  Analysis Date = 06/30/13 
 Pct Recovery = 89%  Analysis Date = 06/30/13 
 Pct Recovery = 89%  Analysis Date = 06/28/13 
 Pct Recovery = 90%  Analysis Date = 06/28/13 
 Pct Recovery = 90%  Analysis Date = 06/26/13 
 Pct Recovery = 90%  Analysis Date = 06/26/13 
 Pct Recovery = 90%  Analysis Date = 06/24/13 
 Pct Recovery = 90%  Analysis Date = 06/24/13 
 Pct Recovery = 90%  Analysis Date = 06/22/13 
 Pct Recovery = 90%  Analysis Date = 06/22/13 
 Pct Recovery = 90%  Analysis Date = 06/20/13 
 Pct Recovery = 90%  Analysis Date = 06/20/13 
 Pct Recovery = 90%  Analysis Date = 06/18/13 
 Pct Recovery = 90%  Analysis Date = 06/18/13 
 Pct Recovery = 90%  Analysis Date = 06/16/13 
 Pct Recovery = 90%  Analysis Date = 06/16/13 
 Pct Recovery = 90%  Analysis Date = 06/14/13 
 Pct Recovery = 91%  Analysis Date = 06/14/13 
 Pct Recovery = 91%  Analysis Date = 06/11/13 
 Pct Recovery = 91%  Analysis Date = 06/11/13 
 Pct Recovery = 91%  Analysis Date = 06/09/13 
 Pct Recovery = 91%  Analysis Date = 06/09/13 
 Pct Recovery = 91%  Analysis Date = 06/07/13 
 Pct Recovery = 91%  Analysis Date = 06/07/13 
 Pct Recovery = 91%  Analysis Date = 06/05/13 
 Pct Recovery = 91%  Analysis Date = 06/05/13 
 Pct Recovery = 91%  Analysis Date = 06/03/13 
 Pct Recovery = 91%  Analysis Date = 06/03/13 
 Pct Recovery = 91%  Analysis Date = 06/01/13 
 Pct Recovery = 92%  Analysis Date = 06/01/13 
 Pct Recovery = 92%  Analysis Date = 05/30/13 
 Pct Recovery = 92%  Analysis Date = 05/30/13 
 Pct Recovery = 92%  Analysis Date = 05/28/13 
 Pct Recovery = 92%  Analysis Date = 05/28/13 
 Pct Recovery = 92%  Analysis Date = 05/26/13 
 Pct Recovery = 92%  Analysis Date = 05/26/13 
 Pct Recovery = 92%  Analysis Date = 05/23/13 
 Pct Recovery = 92%  Analysis Date = 05/23/13 
 Pct Recovery = 92%  Analysis Date = 05/21/13 
 Pct Recovery = 92%  Analysis Date = 05/21/13 
 Pct Recovery = 92%  Analysis Date = 05/19/13 
 Pct Recovery = 92%  Analysis Date = 05/19/13 
 Pct Recovery = 92%  Analysis Date = 05/17/13 
 Pct Recovery = 93%  Analysis Date = 05/17/13 
 Pct Recovery = 93%  Analysis Date = 05/15/13 
 Pct Recovery = 93%  Analysis Date = 05/15/13 
 Pct Recovery = 93%  Analysis Date = 05/13/13 
 Pct Recovery = 93%  Analysis Date = 05/13/13 
 Pct Recovery = 93%  Analysis Date = 05/11/13 
 Pct Recovery = 93%  Analysis Date = 05/11/13 
 Pct Recovery = 93%  Analysis Date = 05/09/13 
 Pct Recovery = 93%  Analysis Date = 05/09/13 
 Pct Recovery = 93%  Analysis Date = 05/07/13 
 Pct Recovery = 93%  Analysis Date = 05/07/13 
 Pct Recovery = 93%  Analysis Date = 05/05/13 
 Pct Recovery = 94%  Analysis Date = 05/05/13 
 Pct Recovery = 94%  Analysis Date = 05/02/13 
 Pct Recovery = 94%  Analysis Date = 05/02/13 
 Pct Recovery = 94%  Analysis Date = 04/30/13 
 Pct Recovery = 94%  Analysis Date = 04/30/13 
 Pct Recovery = 94%  Analysis Date = 04/28/13 
 Pct Recovery = 94%  Analysis Date = 04/28/13 
 Pct Recovery = 94%  Analysis Date = 04/26/13 
 Pct Recovery = 94%  Analysis Date = 04/26/13 
 Pct Recovery = 94%  Analysis Date = 04/24/13 
 Pct Recovery = 94%  Analysis Date = 04/24/13 
 Pct Recovery = 94%  Analysis Date = 04/22/13 
 Pct Recovery = 95%  Analysis Date = 04/22/13 
 Pct Recovery = 95%  Analysis Date = 04/20/13 
 Pct Recovery = 95%  Analysis Date = 04/20/13 
 Pct Recovery = 95%  Analysis Date = 04/18/13 
 Pct Recovery = 95%  Analysis Date = 04/18/13 
 Pct Recovery = 95%  Analysis Date = 04/16/13 
 Pct Recovery = 95%  Analysis Date = 04/16/13 
 Pct Recovery = 95%  Analysis Date = 04/13/13 
 Pct Recovery = 96%  Analysis Date = 04/13/13 
 Pct Recovery = 96%  Analysis Date = 04/11/13 
 Pct Recovery = 96%  Analysis Date = 04/11/13 
 Pct Recovery = 96%  Analysis Date = 04/09/13 
 Pct Recovery = 96%  Analysis Date = 04/09/13 
 Pct Recovery = 96%  Analysis Date = 04/07/13 
 Pct Recovery = 96%  Analysis Date = 04/07/13 
 Pct Recovery = 96%  Analysis Date = 04/05/13 
 Pct Recovery = 96%  Analysis Date = 04/05/13 
 Pct Recovery = 96%  Analysis Date = 04/03/13 
 Pct Recovery = 97%  Analysis Date = 04/03/13 
 Pct Recovery = 97%  Analysis Date = 04/01/13 
 Pct Recovery = 97%  Analysis Date = 04/01/13 
 Pct Recovery = 97%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/28/13 
 Pct Recovery = 97%  Analysis Date = 03/28/13 
 Pct Recovery = 97%  Analysis Date = 03/26/13 
 Pct Recovery = 97%  Analysis Date = 03/26/13 
 Pct Recovery = 97%  Analysis Date = 03/23/13 
 Pct Recovery = 98%  Analysis Date = 03/23/13 
 Pct Recovery = 98%  Analysis Date = 03/21/13 
 Pct Recovery = 98%  Analysis Date = 03/21/13 
 Pct Recovery = 98%  Analysis Date = 03/19/13 
 Pct Recovery = 98%  Analysis Date = 03/19/13 
 Pct Recovery = 98%  Analysis Date = 03/17/13 
 Pct Recovery = 98%  Analysis Date = 03/17/13 
 Pct Recovery = 98%  Analysis Date = 03/15/13 
 Pct Recovery = 98%  Analysis Date = 03/15/13 
 Pct Recovery = 98%  Analysis Date = 03/13/13 
 Pct Recovery = 99%  Analysis Date = 03/13/13 
 Pct Recovery = 99%  Analysis Date = 03/11/13 
 Pct Recovery = 99%  Analysis Date = 03/11/13 
 Pct Recovery = 99%  Analysis Date = 03/09/13 
 Pct Recovery = 99%  Analysis Date = 03/09/13 
 Pct Recovery = 99%  Analysis Date = 03/07/13 
 Pct Recovery = 99%  Analysis Date = 03/07/13 
 Pct Recovery = 99%  Analysis Date = 03/04/13 
 Pct Recovery = 99%  Analysis Date = 03/04/13 
 Pct Recovery = 99%  Analysis Date = 03/02/13 
 Pct Recovery = 100%  Analysis Date = 03/02/13 
 Pct Recovery = 100%  Analysis Date = 02/28/13 
 Pct Recovery = 100%  Analysis Date = 02/28/13 
 Pct Recovery = 100%  Analysis Date = 02/26/13 
 Pct Recovery = 100%  Analysis Date = 02/26/13 
 Pct Recovery = 100%  Analysis Date = 02/24/13 
 Pct Recovery = 100%  Analysis Date = 02/24/13 
 Pct Recovery = 100%  Analysis Date = 02/22/13 
 Pct Recovery = 100%  Analysis Date = 02/22/13 
 Pct Recovery = 100%  Analysis Date = 02/20/13 
 Pct Recovery = 101%  Analysis Date = 02/20/13 
 Pct Recovery = 101%  Analysis Date = 02/18/13 
 Pct Recovery = 101%  Analysis Date = 02/18/13 
 Pct Recovery = 101%  Analysis Date = 02/16/13 
 Pct Recovery = 101%  Analysis Date = 02/16/13 
 Pct Recovery = 101%  Analysis Date = 02/14/13 
 Pct Recovery = 101%  Analysis Date = 02/14/13 
 Pct Recovery = 101%  Analysis Date = 02/11/13 
 Pct Recovery = 101%  Analysis Date = 02/11/13 
 Pct Recovery = 101%  Analysis Date = 02/09/13 
 Pct Recovery = 102%  Analysis Date = 02/09/13 
 Pct Recovery = 102%  Analysis Date = 02/07/13 
 Pct Recovery = 102%  Analysis Date = 02/07/13 
 Pct Recovery = 102%  Analysis Date = 02/05/13 
 Pct Recovery = 102%  Analysis Date = 02/05/13 
 Pct Recovery = 102%  Analysis Date = 02/03/13 
 Pct Recovery = 102%  Analysis Date = 02/03/13 
 Pct Recovery = 102%  Analysis Date = 02/01/13 
 Pct Recovery = 103%  Analysis Date = 02/01/13 
 Pct Recovery = 103%  Analysis Date = 01/30/13 
 Pct Recovery = 103%  Analysis Date = 01/30/13 
 Pct Recovery = 103%  Analysis Date = 01/28/13 
 Pct Recovery = 103%  Analysis Date = 01/28/13 
 Pct Recovery = 103%  Analysis Date = 01/26/13 
 Pct Recovery = 103%  Analysis Date = 01/26/13 
 Pct Recovery = 103%  Analysis Date = 01/24/13 
 Pct Recovery = 103%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CLONIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 85% 13% 85% 11%
Total 6 85% 13% 85% 11%

Sample Statistics
CLONIDINE

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 1 17% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
CODEINE
METHOD: LC9017 , TESTIDCODE: 67443LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 79%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 34%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 56%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 90%  Analysis Date = 02/19/14 
 Pct Recovery = 62%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/16/14 
 Pct Recovery = 56%  Analysis Date = 02/16/14 
 Pct Recovery = 56%  Analysis Date = 02/14/14 
 Pct Recovery = 56%  Analysis Date = 02/14/14 
 Pct Recovery = 56%  Analysis Date = 02/12/14 
 Pct Recovery = 57%  Analysis Date = 02/12/14 
 Pct Recovery = 57%  Analysis Date = 02/11/14 
 Pct Recovery = 57%  Analysis Date = 02/11/14 
 Pct Recovery = 57%  Analysis Date = 02/09/14 
 Pct Recovery = 57%  Analysis Date = 02/09/14 
 Pct Recovery = 57%  Analysis Date = 02/07/14 
 Pct Recovery = 57%  Analysis Date = 02/07/14 
 Pct Recovery = 57%  Analysis Date = 02/05/14 
 Pct Recovery = 57%  Analysis Date = 02/05/14 
 Pct Recovery = 57%  Analysis Date = 02/03/14 
 Pct Recovery = 57%  Analysis Date = 02/03/14 
 Pct Recovery = 57%  Analysis Date = 02/02/14 
 Pct Recovery = 57%  Analysis Date = 02/02/14 
 Pct Recovery = 57%  Analysis Date = 01/31/14 
 Pct Recovery = 57%  Analysis Date = 01/31/14 
 Pct Recovery = 57%  Analysis Date = 01/29/14 
 Pct Recovery = 58%  Analysis Date = 01/29/14 
 Pct Recovery = 58%  Analysis Date = 01/27/14 
 Pct Recovery = 58%  Analysis Date = 01/27/14 
 Pct Recovery = 58%  Analysis Date = 01/26/14 
 Pct Recovery = 58%  Analysis Date = 01/26/14 
 Pct Recovery = 58%  Analysis Date = 01/24/14 
 Pct Recovery = 58%  Analysis Date = 01/24/14 
 Pct Recovery = 58%  Analysis Date = 01/22/14 
 Pct Recovery = 58%  Analysis Date = 01/22/14 
 Pct Recovery = 58%  Analysis Date = 01/20/14 
 Pct Recovery = 58%  Analysis Date = 01/20/14 
 Pct Recovery = 58%  Analysis Date = 01/18/14 
 Pct Recovery = 58%  Analysis Date = 01/18/14 
 Pct Recovery = 58%  Analysis Date = 01/17/14 
 Pct Recovery = 59%  Analysis Date = 01/17/14 
 Pct Recovery = 59%  Analysis Date = 01/15/14 
 Pct Recovery = 59%  Analysis Date = 01/15/14 
 Pct Recovery = 59%  Analysis Date = 01/13/14 
 Pct Recovery = 59%  Analysis Date = 01/13/14 
 Pct Recovery = 59%  Analysis Date = 01/11/14 
 Pct Recovery = 59%  Analysis Date = 01/11/14 
 Pct Recovery = 59%  Analysis Date = 01/09/14 
 Pct Recovery = 59%  Analysis Date = 01/09/14 
 Pct Recovery = 59%  Analysis Date = 01/08/14 
 Pct Recovery = 59%  Analysis Date = 01/08/14 
 Pct Recovery = 59%  Analysis Date = 01/06/14 
 Pct Recovery = 59%  Analysis Date = 01/06/14 
 Pct Recovery = 59%  Analysis Date = 01/04/14 
 Pct Recovery = 60%  Analysis Date = 01/04/14 
 Pct Recovery = 60%  Analysis Date = 01/02/14 
 Pct Recovery = 60%  Analysis Date = 01/02/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/28/13 
 Pct Recovery = 60%  Analysis Date = 12/28/13 
 Pct Recovery = 60%  Analysis Date = 12/26/13 
 Pct Recovery = 60%  Analysis Date = 12/26/13 
 Pct Recovery = 60%  Analysis Date = 12/24/13 
 Pct Recovery = 60%  Analysis Date = 12/24/13 
 Pct Recovery = 60%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/21/13 
 Pct Recovery = 61%  Analysis Date = 12/21/13 
 Pct Recovery = 61%  Analysis Date = 12/19/13 
 Pct Recovery = 61%  Analysis Date = 12/19/13 
 Pct Recovery = 61%  Analysis Date = 12/17/13 
 Pct Recovery = 61%  Analysis Date = 12/17/13 
 Pct Recovery = 61%  Analysis Date = 12/15/13 
 Pct Recovery = 61%  Analysis Date = 12/15/13 
 Pct Recovery = 61%  Analysis Date = 12/14/13 
 Pct Recovery = 61%  Analysis Date = 12/14/13 
 Pct Recovery = 61%  Analysis Date = 12/12/13 
 Pct Recovery = 61%  Analysis Date = 12/12/13 
 Pct Recovery = 61%  Analysis Date = 12/10/13 
 Pct Recovery = 61%  Analysis Date = 12/10/13 
 Pct Recovery = 61%  Analysis Date = 12/08/13 
 Pct Recovery = 62%  Analysis Date = 12/08/13 
 Pct Recovery = 62%  Analysis Date = 12/07/13 
 Pct Recovery = 62%  Analysis Date = 12/07/13 
 Pct Recovery = 62%  Analysis Date = 12/05/13 
 Pct Recovery = 62%  Analysis Date = 12/05/13 
 Pct Recovery = 62%  Analysis Date = 12/03/13 
 Pct Recovery = 62%  Analysis Date = 12/03/13 
 Pct Recovery = 62%  Analysis Date = 12/01/13 
 Pct Recovery = 62%  Analysis Date = 12/01/13 
 Pct Recovery = 62%  Analysis Date = 11/29/13 
 Pct Recovery = 62%  Analysis Date = 11/29/13 
 Pct Recovery = 62%  Analysis Date = 11/28/13 
 Pct Recovery = 62%  Analysis Date = 11/28/13 
 Pct Recovery = 62%  Analysis Date = 11/26/13 
 Pct Recovery = 63%  Analysis Date = 11/26/13 
 Pct Recovery = 63%  Analysis Date = 11/24/13 
 Pct Recovery = 63%  Analysis Date = 11/24/13 
 Pct Recovery = 63%  Analysis Date = 11/22/13 
 Pct Recovery = 63%  Analysis Date = 11/22/13 
 Pct Recovery = 63%  Analysis Date = 11/20/13 
 Pct Recovery = 63%  Analysis Date = 11/20/13 
 Pct Recovery = 63%  Analysis Date = 11/19/13 
 Pct Recovery = 63%  Analysis Date = 11/19/13 
 Pct Recovery = 63%  Analysis Date = 11/17/13 
 Pct Recovery = 63%  Analysis Date = 11/17/13 
 Pct Recovery = 63%  Analysis Date = 11/15/13 
 Pct Recovery = 63%  Analysis Date = 11/15/13 
 Pct Recovery = 63%  Analysis Date = 11/13/13 
 Pct Recovery = 64%  Analysis Date = 11/13/13 
 Pct Recovery = 64%  Analysis Date = 11/12/13 
 Pct Recovery = 64%  Analysis Date = 11/12/13 
 Pct Recovery = 64%  Analysis Date = 11/10/13 
 Pct Recovery = 64%  Analysis Date = 11/10/13 
 Pct Recovery = 64%  Analysis Date = 11/08/13 
 Pct Recovery = 64%  Analysis Date = 11/08/13 
 Pct Recovery = 64%  Analysis Date = 11/06/13 
 Pct Recovery = 64%  Analysis Date = 11/06/13 
 Pct Recovery = 64%  Analysis Date = 11/04/13 
 Pct Recovery = 64%  Analysis Date = 11/04/13 
 Pct Recovery = 64%  Analysis Date = 11/03/13 
 Pct Recovery = 64%  Analysis Date = 11/03/13 
 Pct Recovery = 64%  Analysis Date = 11/01/13 
 Pct Recovery = 65%  Analysis Date = 11/01/13 
 Pct Recovery = 65%  Analysis Date = 10/30/13 
 Pct Recovery = 65%  Analysis Date = 10/30/13 
 Pct Recovery = 65%  Analysis Date = 10/28/13 
 Pct Recovery = 65%  Analysis Date = 10/28/13 
 Pct Recovery = 65%  Analysis Date = 10/26/13 
 Pct Recovery = 65%  Analysis Date = 10/26/13 
 Pct Recovery = 65%  Analysis Date = 10/25/13 
 Pct Recovery = 65%  Analysis Date = 10/25/13 
 Pct Recovery = 65%  Analysis Date = 10/23/13 
 Pct Recovery = 65%  Analysis Date = 10/23/13 
 Pct Recovery = 65%  Analysis Date = 10/21/13 
 Pct Recovery = 65%  Analysis Date = 10/21/13 
 Pct Recovery = 65%  Analysis Date = 10/19/13 
 Pct Recovery = 65%  Analysis Date = 10/19/13 
 Pct Recovery = 65%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/14/13 
 Pct Recovery = 66%  Analysis Date = 10/14/13 
 Pct Recovery = 66%  Analysis Date = 10/12/13 
 Pct Recovery = 66%  Analysis Date = 10/12/13 
 Pct Recovery = 66%  Analysis Date = 10/10/13 
 Pct Recovery = 66%  Analysis Date = 10/10/13 
 Pct Recovery = 66%  Analysis Date = 10/09/13 
 Pct Recovery = 66%  Analysis Date = 10/09/13 
 Pct Recovery = 66%  Analysis Date = 10/07/13 
 Pct Recovery = 66%  Analysis Date = 10/07/13 
 Pct Recovery = 66%  Analysis Date = 10/05/13 
 Pct Recovery = 67%  Analysis Date = 10/05/13 
 Pct Recovery = 67%  Analysis Date = 10/03/13 
 Pct Recovery = 67%  Analysis Date = 10/03/13 
 Pct Recovery = 67%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 09/30/13 
 Pct Recovery = 67%  Analysis Date = 09/30/13 
 Pct Recovery = 67%  Analysis Date = 09/28/13 
 Pct Recovery = 67%  Analysis Date = 09/28/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/23/13 
 Pct Recovery = 68%  Analysis Date = 09/23/13 
 Pct Recovery = 68%  Analysis Date = 09/21/13 
 Pct Recovery = 68%  Analysis Date = 09/21/13 
 Pct Recovery = 68%  Analysis Date = 09/19/13 
 Pct Recovery = 68%  Analysis Date = 09/19/13 
 Pct Recovery = 68%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/15/13 
 Pct Recovery = 68%  Analysis Date = 09/15/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/10/13 
 Pct Recovery = 69%  Analysis Date = 09/10/13 
 Pct Recovery = 69%  Analysis Date = 09/08/13 
 Pct Recovery = 69%  Analysis Date = 09/08/13 
 Pct Recovery = 69%  Analysis Date = 09/06/13 
 Pct Recovery = 69%  Analysis Date = 09/06/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/03/13 
 Pct Recovery = 69%  Analysis Date = 09/03/13 
 Pct Recovery = 69%  Analysis Date = 09/01/13 
 Pct Recovery = 69%  Analysis Date = 09/01/13 
 Pct Recovery = 69%  Analysis Date = 08/30/13 
 Pct Recovery = 69%  Analysis Date = 08/30/13 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 Pct Recovery = 69%  Analysis Date = 08/27/13 
 Pct Recovery = 70%  Analysis Date = 08/27/13 
 Pct Recovery = 70%  Analysis Date = 08/25/13 
 Pct Recovery = 70%  Analysis Date = 08/25/13 
 Pct Recovery = 70%  Analysis Date = 08/23/13 
 Pct Recovery = 70%  Analysis Date = 08/23/13 
 Pct Recovery = 70%  Analysis Date = 08/21/13 
 Pct Recovery = 70%  Analysis Date = 08/21/13 
 Pct Recovery = 70%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/16/13 
 Pct Recovery = 70%  Analysis Date = 08/16/13 
 Pct Recovery = 70%  Analysis Date = 08/14/13 
 Pct Recovery = 71%  Analysis Date = 08/14/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/11/13 
 Pct Recovery = 71%  Analysis Date = 08/11/13 
 Pct Recovery = 71%  Analysis Date = 08/09/13 
 Pct Recovery = 71%  Analysis Date = 08/09/13 
 Pct Recovery = 71%  Analysis Date = 08/07/13 
 Pct Recovery = 71%  Analysis Date = 08/07/13 
 Pct Recovery = 71%  Analysis Date = 08/05/13 
 Pct Recovery = 71%  Analysis Date = 08/05/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 72%  Analysis Date = 08/02/13 
 Pct Recovery = 72%  Analysis Date = 07/31/13 
 Pct Recovery = 72%  Analysis Date = 07/31/13 
 Pct Recovery = 72%  Analysis Date = 07/29/13 
 Pct Recovery = 72%  Analysis Date = 07/29/13 
 Pct Recovery = 72%  Analysis Date = 07/27/13 
 Pct Recovery = 72%  Analysis Date = 07/27/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/24/13 
 Pct Recovery = 72%  Analysis Date = 07/24/13 
 Pct Recovery = 72%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/20/13 
 Pct Recovery = 73%  Analysis Date = 07/20/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/17/13 
 Pct Recovery = 73%  Analysis Date = 07/17/13 
 Pct Recovery = 73%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/15/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/13/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/10/13 
 Pct Recovery = 73%  Analysis Date = 07/10/13 
 Pct Recovery = 73%  Analysis Date = 07/08/13 
 Pct Recovery = 73%  Analysis Date = 07/08/13 
 Pct Recovery = 73%  Analysis Date = 07/06/13 
 Pct Recovery = 74%  Analysis Date = 07/06/13 
 Pct Recovery = 74%  Analysis Date = 07/04/13 
 Pct Recovery = 74%  Analysis Date = 07/04/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/01/13 
 Pct Recovery = 74%  Analysis Date = 07/01/13 
 Pct Recovery = 74%  Analysis Date = 06/29/13 
 Pct Recovery = 74%  Analysis Date = 06/29/13 
 Pct Recovery = 74%  Analysis Date = 06/27/13 
 Pct Recovery = 74%  Analysis Date = 06/27/13 
 Pct Recovery = 74%  Analysis Date = 06/25/13 
 Pct Recovery = 74%  Analysis Date = 06/25/13 
 Pct Recovery = 74%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/20/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/18/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/15/13 
 Pct Recovery = 75%  Analysis Date = 06/15/13 
 Pct Recovery = 75%  Analysis Date = 06/13/13 
 Pct Recovery = 75%  Analysis Date = 06/13/13 
 Pct Recovery = 75%  Analysis Date = 06/11/13 
 Pct Recovery = 76%  Analysis Date = 06/11/13 
 Pct Recovery = 76%  Analysis Date = 06/09/13 
 Pct Recovery = 76%  Analysis Date = 06/09/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/06/13 
 Pct Recovery = 76%  Analysis Date = 06/06/13 
 Pct Recovery = 76%  Analysis Date = 06/04/13 
 Pct Recovery = 76%  Analysis Date = 06/04/13 
 Pct Recovery = 76%  Analysis Date = 06/02/13 
 Pct Recovery = 76%  Analysis Date = 06/02/13 
 Pct Recovery = 76%  Analysis Date = 05/31/13 
 Pct Recovery = 76%  Analysis Date = 05/31/13 
 Pct Recovery = 76%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/21/13 
 Pct Recovery = 77%  Analysis Date = 05/21/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/08/13 
 Pct Recovery = 78%  Analysis Date = 05/08/13 
 Pct Recovery = 78%  Analysis Date = 05/06/13 
 Pct Recovery = 78%  Analysis Date = 05/06/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/01/13 
 Pct Recovery = 77%  Analysis Date = 05/01/13 
 Pct Recovery = 77%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/27/13 
 Pct Recovery = 73%  Analysis Date = 04/27/13 
 Pct Recovery = 73%  Analysis Date = 04/26/13 
 Pct Recovery = 70%  Analysis Date = 04/26/13 
 Pct Recovery = 70%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/22/13 
 Pct Recovery = 66%  Analysis Date = 04/22/13 
 Pct Recovery = 66%  Analysis Date = 04/20/13 
 Pct Recovery = 64%  Analysis Date = 04/20/13 
 Pct Recovery = 64%  Analysis Date = 04/18/13 
 Pct Recovery = 62%  Analysis Date = 04/18/13 
 Pct Recovery = 62%  Analysis Date = 04/17/13 
 Pct Recovery = 60%  Analysis Date = 04/17/13 
 Pct Recovery = 60%  Analysis Date = 04/15/13 
 Pct Recovery = 58%  Analysis Date = 04/15/13 
 Pct Recovery = 58%  Analysis Date = 04/13/13 
 Pct Recovery = 55%  Analysis Date = 04/13/13 
 Pct Recovery = 55%  Analysis Date = 04/11/13 
 Pct Recovery = 53%  Analysis Date = 04/11/13 
 Pct Recovery = 53%  Analysis Date = 04/10/13 
 Pct Recovery = 51%  Analysis Date = 04/10/13 
 Pct Recovery = 51%  Analysis Date = 04/08/13 
 Pct Recovery = 49%  Analysis Date = 04/08/13 
 Pct Recovery = 49%  Analysis Date = 04/06/13 
 Pct Recovery = 47%  Analysis Date = 04/06/13 
 Pct Recovery = 47%  Analysis Date = 04/04/13 
 Pct Recovery = 45%  Analysis Date = 04/04/13 
 Pct Recovery = 45%  Analysis Date = 04/02/13 
 Pct Recovery = 43%  Analysis Date = 04/02/13 
 Pct Recovery = 43%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 38%  Analysis Date = 03/30/13 
 Pct Recovery = 38%  Analysis Date = 03/28/13 
 Pct Recovery = 36%  Analysis Date = 03/28/13 
 Pct Recovery = 36%  Analysis Date = 03/26/13 
 Pct Recovery = 35%  Analysis Date = 03/26/13 
 Pct Recovery = 35%  Analysis Date = 03/24/13 
 Pct Recovery = 39%  Analysis Date = 03/24/13 
 Pct Recovery = 39%  Analysis Date = 03/23/13 
 Pct Recovery = 42%  Analysis Date = 03/23/13 
 Pct Recovery = 42%  Analysis Date = 03/21/13 
 Pct Recovery = 46%  Analysis Date = 03/21/13 
 Pct Recovery = 46%  Analysis Date = 03/19/13 
 Pct Recovery = 50%  Analysis Date = 03/19/13 
 Pct Recovery = 50%  Analysis Date = 03/17/13 
 Pct Recovery = 53%  Analysis Date = 03/17/13 
 Pct Recovery = 53%  Analysis Date = 03/16/13 
 Pct Recovery = 57%  Analysis Date = 03/16/13 
 Pct Recovery = 57%  Analysis Date = 03/14/13 
 Pct Recovery = 61%  Analysis Date = 03/14/13 
 Pct Recovery = 61%  Analysis Date = 03/12/13 
 Pct Recovery = 64%  Analysis Date = 03/12/13 
 Pct Recovery = 64%  Analysis Date = 03/10/13 
 Pct Recovery = 68%  Analysis Date = 03/10/13 
 Pct Recovery = 68%  Analysis Date = 03/08/13 
 Pct Recovery = 72%  Analysis Date = 03/08/13 
 Pct Recovery = 72%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/05/13 
 Pct Recovery = 79%  Analysis Date = 03/05/13 
 Pct Recovery = 79%  Analysis Date = 03/03/13 
 Pct Recovery = 83%  Analysis Date = 03/03/13 
 Pct Recovery = 83%  Analysis Date = 03/01/13 
 Pct Recovery = 87%  Analysis Date = 03/01/13 
 Pct Recovery = 87%  Analysis Date = 02/28/13 
 Pct Recovery = 90%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
CODEINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 5 64% 21% 62% 17%
Total 5 64% 21% 62% 17%

Sample Statistics
CODEINE

Characteristic N % % Basis
Plotted 5 71% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 2 29% 2 out of 7
Not Spiked 25 .  
False Positives 0 0% 0 out of 24

OBSP Determination:
COTININE
METHOD: LC9017 , TESTIDCODE: 67444LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 98%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 110%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 105%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 76%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 107%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 80%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 70%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 77%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 87%  Analysis Date = 03/21/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 75%  Analysis Date = 03/18/14 
 Pct Recovery = 75%  Analysis Date = 03/16/14 
 Pct Recovery = 75%  Analysis Date = 03/16/14 
 Pct Recovery = 75%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/11/14 
 Pct Recovery = 75%  Analysis Date = 03/11/14 
 Pct Recovery = 75%  Analysis Date = 03/09/14 
 Pct Recovery = 75%  Analysis Date = 03/09/14 
 Pct Recovery = 75%  Analysis Date = 03/07/14 
 Pct Recovery = 75%  Analysis Date = 03/07/14 
 Pct Recovery = 75%  Analysis Date = 03/04/14 
 Pct Recovery = 75%  Analysis Date = 03/04/14 
 Pct Recovery = 75%  Analysis Date = 03/02/14 
 Pct Recovery = 76%  Analysis Date = 03/02/14 
 Pct Recovery = 76%  Analysis Date = 02/28/14 
 Pct Recovery = 76%  Analysis Date = 02/28/14 
 Pct Recovery = 76%  Analysis Date = 02/25/14 
 Pct Recovery = 76%  Analysis Date = 02/25/14 
 Pct Recovery = 76%  Analysis Date = 02/23/14 
 Pct Recovery = 76%  Analysis Date = 02/23/14 
 Pct Recovery = 76%  Analysis Date = 02/21/14 
 Pct Recovery = 76%  Analysis Date = 02/21/14 
 Pct Recovery = 76%  Analysis Date = 02/18/14 
 Pct Recovery = 76%  Analysis Date = 02/18/14 
 Pct Recovery = 76%  Analysis Date = 02/16/14 
 Pct Recovery = 76%  Analysis Date = 02/16/14 
 Pct Recovery = 76%  Analysis Date = 02/14/14 
 Pct Recovery = 77%  Analysis Date = 02/14/14 
 Pct Recovery = 77%  Analysis Date = 02/12/14 
 Pct Recovery = 77%  Analysis Date = 02/12/14 
 Pct Recovery = 77%  Analysis Date = 02/09/14 
 Pct Recovery = 77%  Analysis Date = 02/09/14 
 Pct Recovery = 77%  Analysis Date = 02/07/14 
 Pct Recovery = 77%  Analysis Date = 02/07/14 
 Pct Recovery = 77%  Analysis Date = 02/05/14 
 Pct Recovery = 77%  Analysis Date = 02/05/14 
 Pct Recovery = 77%  Analysis Date = 02/02/14 
 Pct Recovery = 77%  Analysis Date = 02/02/14 
 Pct Recovery = 77%  Analysis Date = 01/31/14 
 Pct Recovery = 78%  Analysis Date = 01/31/14 
 Pct Recovery = 78%  Analysis Date = 01/29/14 
 Pct Recovery = 78%  Analysis Date = 01/29/14 
 Pct Recovery = 78%  Analysis Date = 01/26/14 
 Pct Recovery = 78%  Analysis Date = 01/26/14 
 Pct Recovery = 78%  Analysis Date = 01/24/14 
 Pct Recovery = 78%  Analysis Date = 01/24/14 
 Pct Recovery = 78%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/17/14 
 Pct Recovery = 79%  Analysis Date = 01/17/14 
 Pct Recovery = 79%  Analysis Date = 01/15/14 
 Pct Recovery = 79%  Analysis Date = 01/15/14 
 Pct Recovery = 79%  Analysis Date = 01/13/14 
 Pct Recovery = 79%  Analysis Date = 01/13/14 
 Pct Recovery = 79%  Analysis Date = 01/10/14 
 Pct Recovery = 79%  Analysis Date = 01/10/14 
 Pct Recovery = 79%  Analysis Date = 01/08/14 
 Pct Recovery = 79%  Analysis Date = 01/08/14 
 Pct Recovery = 79%  Analysis Date = 01/06/14 
 Pct Recovery = 79%  Analysis Date = 01/06/14 
 Pct Recovery = 79%  Analysis Date = 01/03/14 
 Pct Recovery = 79%  Analysis Date = 01/03/14 
 Pct Recovery = 79%  Analysis Date = 01/01/14 
 Pct Recovery = 79%  Analysis Date = 01/01/14 
 Pct Recovery = 79%  Analysis Date = 12/30/13 
 Pct Recovery = 79%  Analysis Date = 12/30/13 
 Pct Recovery = 79%  Analysis Date = 12/27/13 
 Pct Recovery = 79%  Analysis Date = 12/27/13 
 Pct Recovery = 79%  Analysis Date = 12/25/13 
 Pct Recovery = 79%  Analysis Date = 12/25/13 
 Pct Recovery = 79%  Analysis Date = 12/23/13 
 Pct Recovery = 79%  Analysis Date = 12/23/13 
 Pct Recovery = 79%  Analysis Date = 12/20/13 
 Pct Recovery = 79%  Analysis Date = 12/20/13 
 Pct Recovery = 79%  Analysis Date = 12/18/13 
 Pct Recovery = 79%  Analysis Date = 12/18/13 
 Pct Recovery = 79%  Analysis Date = 12/16/13 
 Pct Recovery = 79%  Analysis Date = 12/16/13 
 Pct Recovery = 79%  Analysis Date = 12/13/13 
 Pct Recovery = 79%  Analysis Date = 12/13/13 
 Pct Recovery = 79%  Analysis Date = 12/11/13 
 Pct Recovery = 79%  Analysis Date = 12/11/13 
 Pct Recovery = 79%  Analysis Date = 12/09/13 
 Pct Recovery = 79%  Analysis Date = 12/09/13 
 Pct Recovery = 79%  Analysis Date = 12/07/13 
 Pct Recovery = 79%  Analysis Date = 12/07/13 
 Pct Recovery = 79%  Analysis Date = 12/04/13 
 Pct Recovery = 79%  Analysis Date = 12/04/13 
 Pct Recovery = 79%  Analysis Date = 12/02/13 
 Pct Recovery = 79%  Analysis Date = 12/02/13 
 Pct Recovery = 79%  Analysis Date = 11/30/13 
 Pct Recovery = 79%  Analysis Date = 11/30/13 
 Pct Recovery = 79%  Analysis Date = 11/27/13 
 Pct Recovery = 79%  Analysis Date = 11/27/13 
 Pct Recovery = 79%  Analysis Date = 11/25/13 
 Pct Recovery = 79%  Analysis Date = 11/25/13 
 Pct Recovery = 79%  Analysis Date = 11/23/13 
 Pct Recovery = 79%  Analysis Date = 11/23/13 
 Pct Recovery = 79%  Analysis Date = 11/20/13 
 Pct Recovery = 79%  Analysis Date = 11/20/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/13/13 
 Pct Recovery = 79%  Analysis Date = 11/13/13 
 Pct Recovery = 79%  Analysis Date = 11/11/13 
 Pct Recovery = 80%  Analysis Date = 11/11/13 
 Pct Recovery = 80%  Analysis Date = 11/09/13 
 Pct Recovery = 80%  Analysis Date = 11/09/13 
 Pct Recovery = 80%  Analysis Date = 11/07/13 
 Pct Recovery = 80%  Analysis Date = 11/07/13 
 Pct Recovery = 80%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/02/13 
 Pct Recovery = 80%  Analysis Date = 11/02/13 
 Pct Recovery = 80%  Analysis Date = 10/31/13 
 Pct Recovery = 80%  Analysis Date = 10/31/13 
 Pct Recovery = 80%  Analysis Date = 10/28/13 
 Pct Recovery = 80%  Analysis Date = 10/28/13 
 Pct Recovery = 80%  Analysis Date = 10/26/13 
 Pct Recovery = 80%  Analysis Date = 10/26/13 
 Pct Recovery = 80%  Analysis Date = 10/24/13 
 Pct Recovery = 80%  Analysis Date = 10/24/13 
 Pct Recovery = 80%  Analysis Date = 10/21/13 
 Pct Recovery = 80%  Analysis Date = 10/21/13 
 Pct Recovery = 80%  Analysis Date = 10/19/13 
 Pct Recovery = 80%  Analysis Date = 10/19/13 
 Pct Recovery = 80%  Analysis Date = 10/17/13 
 Pct Recovery = 80%  Analysis Date = 10/17/13 
 Pct Recovery = 80%  Analysis Date = 10/14/13 
 Pct Recovery = 80%  Analysis Date = 10/14/13 
 Pct Recovery = 80%  Analysis Date = 10/12/13 
 Pct Recovery = 80%  Analysis Date = 10/12/13 
 Pct Recovery = 80%  Analysis Date = 10/10/13 
 Pct Recovery = 80%  Analysis Date = 10/10/13 
 Pct Recovery = 80%  Analysis Date = 10/07/13 
 Pct Recovery = 80%  Analysis Date = 10/07/13 
 Pct Recovery = 80%  Analysis Date = 10/05/13 
 Pct Recovery = 80%  Analysis Date = 10/05/13 
 Pct Recovery = 80%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 81%  Analysis Date = 10/01/13 
 Pct Recovery = 81%  Analysis Date = 09/28/13 
 Pct Recovery = 81%  Analysis Date = 09/28/13 
 Pct Recovery = 81%  Analysis Date = 09/26/13 
 Pct Recovery = 81%  Analysis Date = 09/26/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/14/13 
 Pct Recovery = 81%  Analysis Date = 09/14/13 
 Pct Recovery = 81%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/10/13 
 Pct Recovery = 81%  Analysis Date = 09/10/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/03/13 
 Pct Recovery = 81%  Analysis Date = 09/03/13 
 Pct Recovery = 81%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 08/29/13 
 Pct Recovery = 81%  Analysis Date = 08/29/13 
 Pct Recovery = 81%  Analysis Date = 08/27/13 
 Pct Recovery = 81%  Analysis Date = 08/27/13 
 Pct Recovery = 81%  Analysis Date = 08/25/13 
 Pct Recovery = 82%  Analysis Date = 08/25/13 
 Pct Recovery = 82%  Analysis Date = 08/22/13 
 Pct Recovery = 82%  Analysis Date = 08/22/13 
 Pct Recovery = 82%  Analysis Date = 08/20/13 
 Pct Recovery = 82%  Analysis Date = 08/20/13 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 Pct Recovery = 83%  Analysis Date = 08/18/13 
 Pct Recovery = 83%  Analysis Date = 08/15/13 
 Pct Recovery = 83%  Analysis Date = 08/15/13 
 Pct Recovery = 83%  Analysis Date = 08/13/13 
 Pct Recovery = 83%  Analysis Date = 08/13/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/08/13 
 Pct Recovery = 84%  Analysis Date = 08/08/13 
 Pct Recovery = 84%  Analysis Date = 08/06/13 
 Pct Recovery = 84%  Analysis Date = 08/06/13 
 Pct Recovery = 84%  Analysis Date = 08/04/13 
 Pct Recovery = 84%  Analysis Date = 08/04/13 
 Pct Recovery = 84%  Analysis Date = 08/02/13 
 Pct Recovery = 85%  Analysis Date = 08/02/13 
 Pct Recovery = 85%  Analysis Date = 07/30/13 
 Pct Recovery = 85%  Analysis Date = 07/30/13 
 Pct Recovery = 85%  Analysis Date = 07/28/13 
 Pct Recovery = 85%  Analysis Date = 07/28/13 
 Pct Recovery = 85%  Analysis Date = 07/26/13 
 Pct Recovery = 85%  Analysis Date = 07/26/13 
 Pct Recovery = 85%  Analysis Date = 07/23/13 
 Pct Recovery = 86%  Analysis Date = 07/23/13 
 Pct Recovery = 86%  Analysis Date = 07/21/13 
 Pct Recovery = 86%  Analysis Date = 07/21/13 
 Pct Recovery = 86%  Analysis Date = 07/19/13 
 Pct Recovery = 86%  Analysis Date = 07/19/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 86%  Analysis Date = 07/14/13 
 Pct Recovery = 87%  Analysis Date = 07/14/13 
 Pct Recovery = 87%  Analysis Date = 07/12/13 
 Pct Recovery = 87%  Analysis Date = 07/12/13 
 Pct Recovery = 87%  Analysis Date = 07/09/13 
 Pct Recovery = 87%  Analysis Date = 07/09/13 
 Pct Recovery = 87%  Analysis Date = 07/07/13 
 Pct Recovery = 88%  Analysis Date = 07/07/13 
 Pct Recovery = 88%  Analysis Date = 07/05/13 
 Pct Recovery = 88%  Analysis Date = 07/05/13 
 Pct Recovery = 88%  Analysis Date = 07/02/13 
 Pct Recovery = 88%  Analysis Date = 07/02/13 
 Pct Recovery = 88%  Analysis Date = 06/30/13 
 Pct Recovery = 88%  Analysis Date = 06/30/13 
 Pct Recovery = 88%  Analysis Date = 06/28/13 
 Pct Recovery = 89%  Analysis Date = 06/28/13 
 Pct Recovery = 89%  Analysis Date = 06/26/13 
 Pct Recovery = 89%  Analysis Date = 06/26/13 
 Pct Recovery = 89%  Analysis Date = 06/23/13 
 Pct Recovery = 89%  Analysis Date = 06/23/13 
 Pct Recovery = 89%  Analysis Date = 06/21/13 
 Pct Recovery = 90%  Analysis Date = 06/21/13 
 Pct Recovery = 90%  Analysis Date = 06/19/13 
 Pct Recovery = 90%  Analysis Date = 06/19/13 
 Pct Recovery = 90%  Analysis Date = 06/16/13 
 Pct Recovery = 90%  Analysis Date = 06/16/13 
 Pct Recovery = 90%  Analysis Date = 06/14/13 
 Pct Recovery = 90%  Analysis Date = 06/14/13 
 Pct Recovery = 90%  Analysis Date = 06/12/13 
 Pct Recovery = 91%  Analysis Date = 06/12/13 
 Pct Recovery = 91%  Analysis Date = 06/09/13 
 Pct Recovery = 91%  Analysis Date = 06/09/13 
 Pct Recovery = 91%  Analysis Date = 06/07/13 
 Pct Recovery = 91%  Analysis Date = 06/07/13 
 Pct Recovery = 91%  Analysis Date = 06/05/13 
 Pct Recovery = 91%  Analysis Date = 06/05/13 
 Pct Recovery = 91%  Analysis Date = 06/02/13 
 Pct Recovery = 92%  Analysis Date = 06/02/13 
 Pct Recovery = 92%  Analysis Date = 05/31/13 
 Pct Recovery = 92%  Analysis Date = 05/31/13 
 Pct Recovery = 92%  Analysis Date = 05/29/13 
 Pct Recovery = 92%  Analysis Date = 05/29/13 
 Pct Recovery = 92%  Analysis Date = 05/27/13 
 Pct Recovery = 93%  Analysis Date = 05/27/13 
 Pct Recovery = 93%  Analysis Date = 05/24/13 
 Pct Recovery = 93%  Analysis Date = 05/24/13 
 Pct Recovery = 93%  Analysis Date = 05/22/13 
 Pct Recovery = 93%  Analysis Date = 05/22/13 
 Pct Recovery = 93%  Analysis Date = 05/20/13 
 Pct Recovery = 93%  Analysis Date = 05/20/13 
 Pct Recovery = 93%  Analysis Date = 05/17/13 
 Pct Recovery = 94%  Analysis Date = 05/17/13 
 Pct Recovery = 94%  Analysis Date = 05/15/13 
 Pct Recovery = 94%  Analysis Date = 05/15/13 
 Pct Recovery = 94%  Analysis Date = 05/13/13 
 Pct Recovery = 94%  Analysis Date = 05/13/13 
 Pct Recovery = 94%  Analysis Date = 05/10/13 
 Pct Recovery = 95%  Analysis Date = 05/10/13 
 Pct Recovery = 95%  Analysis Date = 05/08/13 
 Pct Recovery = 95%  Analysis Date = 05/08/13 
 Pct Recovery = 95%  Analysis Date = 05/06/13 
 Pct Recovery = 95%  Analysis Date = 05/06/13 
 Pct Recovery = 95%  Analysis Date = 05/03/13 
 Pct Recovery = 95%  Analysis Date = 05/03/13 
 Pct Recovery = 95%  Analysis Date = 05/01/13 
 Pct Recovery = 96%  Analysis Date = 05/01/13 
 Pct Recovery = 96%  Analysis Date = 04/29/13 
 Pct Recovery = 96%  Analysis Date = 04/29/13 
 Pct Recovery = 96%  Analysis Date = 04/26/13 
 Pct Recovery = 96%  Analysis Date = 04/26/13 
 Pct Recovery = 96%  Analysis Date = 04/24/13 
 Pct Recovery = 97%  Analysis Date = 04/24/13 
 Pct Recovery = 97%  Analysis Date = 04/22/13 
 Pct Recovery = 97%  Analysis Date = 04/22/13 
 Pct Recovery = 97%  Analysis Date = 04/20/13 
 Pct Recovery = 97%  Analysis Date = 04/20/13 
 Pct Recovery = 97%  Analysis Date = 04/17/13 
 Pct Recovery = 97%  Analysis Date = 04/17/13 
 Pct Recovery = 97%  Analysis Date = 04/15/13 
 Pct Recovery = 98%  Analysis Date = 04/15/13 
 Pct Recovery = 98%  Analysis Date = 04/13/13 
 Pct Recovery = 98%  Analysis Date = 04/13/13 
 Pct Recovery = 98%  Analysis Date = 04/10/13 
 Pct Recovery = 98%  Analysis Date = 04/10/13 
 Pct Recovery = 98%  Analysis Date = 04/08/13 
 Pct Recovery = 98%  Analysis Date = 04/08/13 
 Pct Recovery = 98%  Analysis Date = 04/06/13 
 Pct Recovery = 99%  Analysis Date = 04/06/13 
 Pct Recovery = 99%  Analysis Date = 04/03/13 
 Pct Recovery = 99%  Analysis Date = 04/03/13 
 Pct Recovery = 99%  Analysis Date = 04/01/13 
 Pct Recovery = 99%  Analysis Date = 04/01/13 
 Pct Recovery = 99%  Analysis Date = 03/30/13 
 Pct Recovery = 100%  Analysis Date = 03/30/13 
 Pct Recovery = 100%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/25/13 
 Pct Recovery = 100%  Analysis Date = 03/25/13 
 Pct Recovery = 100%  Analysis Date = 03/23/13 
 Pct Recovery = 100%  Analysis Date = 03/23/13 
 Pct Recovery = 100%  Analysis Date = 03/21/13 
 Pct Recovery = 101%  Analysis Date = 03/21/13 
 Pct Recovery = 101%  Analysis Date = 03/18/13 
 Pct Recovery = 101%  Analysis Date = 03/18/13 
 Pct Recovery = 101%  Analysis Date = 03/16/13 
 Pct Recovery = 101%  Analysis Date = 03/16/13 
 Pct Recovery = 101%  Analysis Date = 03/14/13 
 Pct Recovery = 102%  Analysis Date = 03/14/13 
 Pct Recovery = 102%  Analysis Date = 03/11/13 
 Pct Recovery = 102%  Analysis Date = 03/11/13 
 Pct Recovery = 102%  Analysis Date = 03/09/13 
 Pct Recovery = 102%  Analysis Date = 03/09/13 
 Pct Recovery = 102%  Analysis Date = 03/07/13 
 Pct Recovery = 102%  Analysis Date = 03/07/13 
 Pct Recovery = 102%  Analysis Date = 03/04/13 
 Pct Recovery = 103%  Analysis Date = 03/04/13 
 Pct Recovery = 103%  Analysis Date = 03/02/13 
 Pct Recovery = 103%  Analysis Date = 03/02/13 
 Pct Recovery = 103%  Analysis Date = 02/28/13 
 Pct Recovery = 103%  Analysis Date = 02/28/13 
 Pct Recovery = 103%  Analysis Date = 02/25/13 
 Pct Recovery = 103%  Analysis Date = 02/25/13 
 Pct Recovery = 103%  Analysis Date = 02/23/13 
 Pct Recovery = 104%  Analysis Date = 02/23/13 
 Pct Recovery = 104%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/18/13 
 Pct Recovery = 104%  Analysis Date = 02/18/13 
 Pct Recovery = 104%  Analysis Date = 02/16/13 
 Pct Recovery = 104%  Analysis Date = 02/16/13 
 Pct Recovery = 104%  Analysis Date = 02/14/13 
 Pct Recovery = 104%  Analysis Date = 02/14/13 
 Pct Recovery = 104%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 105%  Analysis Date = 02/07/13 
 Pct Recovery = 105%  Analysis Date = 02/07/13 
 Pct Recovery = 105%  Analysis Date = 02/05/13 
 Pct Recovery = 105%  Analysis Date = 02/05/13 
 Pct Recovery = 105%  Analysis Date = 02/02/13 
 Pct Recovery = 106%  Analysis Date = 02/02/13 
 Pct Recovery = 106%  Analysis Date = 01/31/13 
 Pct Recovery = 106%  Analysis Date = 01/31/13 
 Pct Recovery = 106%  Analysis Date = 01/29/13 
 Pct Recovery = 106%  Analysis Date = 01/29/13 
 Pct Recovery = 106%  Analysis Date = 01/26/13 
 Pct Recovery = 106%  Analysis Date = 01/26/13 
 Pct Recovery = 106%  Analysis Date = 01/24/13 
 Pct Recovery = 107%  Analysis Date = 01/24/13 
 Pct Recovery = 107%  Analysis Date = 01/22/13 
 Pct Recovery = 107%  Analysis Date = 01/22/13 
 Pct Recovery = 107%  Analysis Date = 01/19/13 
 Pct Recovery = 107%  Analysis Date = 01/19/13 
 Pct Recovery = 107%  Analysis Date = 01/17/13 
 Pct Recovery = 107%  Analysis Date = 01/17/13 
 Pct Recovery = 107%  Analysis Date = 01/15/13 
 Pct Recovery = 107%  Analysis Date = 01/15/13 
 Pct Recovery = 107%  Analysis Date = 01/13/13 
 Pct Recovery = 108%  Analysis Date = 01/13/13 
 Pct Recovery = 108%  Analysis Date = 01/10/13 
 Pct Recovery = 108%  Analysis Date = 01/10/13 
 Pct Recovery = 108%  Analysis Date = 01/08/13 
 Pct Recovery = 108%  Analysis Date = 01/08/13 
 Pct Recovery = 108%  Analysis Date = 01/06/13 
 Pct Recovery = 108%  Analysis Date = 01/06/13 
 Pct Recovery = 108%  Analysis Date = 01/03/13 
 Pct Recovery = 108%  Analysis Date = 01/03/13 
 Pct Recovery = 108%  Analysis Date = 01/01/13 
 Pct Recovery = 109%  Analysis Date = 01/01/13 
 Pct Recovery = 109%  Analysis Date = 12/30/12 
 Pct Recovery = 109%  Analysis Date = 12/30/12 
 Pct Recovery = 109%  Analysis Date = 12/27/12 
 Pct Recovery = 109%  Analysis Date = 12/27/12 
 Pct Recovery = 109%  Analysis Date = 12/25/12 
 Pct Recovery = 109%  Analysis Date = 12/25/12 
 Pct Recovery = 109%  Analysis Date = 12/23/12 
 Pct Recovery = 110%  Analysis Date = 12/23/12 
 Pct Recovery = 110%  Analysis Date = 12/20/12 
 Pct Recovery = 110%  Analysis Date = 12/20/12 
 Pct Recovery = 110%  Analysis Date = 12/18/12 
 Pct Recovery = 110%  Analysis Date = 12/18/12 
 Pct Recovery = 110%  Analysis Date = 12/16/12 
 Pct Recovery = 110%  Analysis Date = 12/16/12 
 Pct Recovery = 110%  Analysis Date = 12/14/12 
 Pct Recovery = 110%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
COTININE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 88% 15% 87% 22%
Total 11 88% 15% 87% 22%

Sample Statistics
COTININE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 2 10% 2 out of 20

OBSP Determination:
DEHYDRONIFEDIPINE
METHOD: LC9017 , TESTIDCODE: 67445LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 86%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 78%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 89%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 90%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 77%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 72%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 67%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 90%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 52%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 88%  Analysis Date = 03/21/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/11/14 
 Pct Recovery = 74%  Analysis Date = 03/11/14 
 Pct Recovery = 74%  Analysis Date = 03/09/14 
 Pct Recovery = 74%  Analysis Date = 03/09/14 
 Pct Recovery = 74%  Analysis Date = 03/07/14 
 Pct Recovery = 74%  Analysis Date = 03/07/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/25/14 
 Pct Recovery = 74%  Analysis Date = 02/25/14 
 Pct Recovery = 74%  Analysis Date = 02/23/14 
 Pct Recovery = 74%  Analysis Date = 02/23/14 
 Pct Recovery = 74%  Analysis Date = 02/21/14 
 Pct Recovery = 74%  Analysis Date = 02/21/14 
 Pct Recovery = 74%  Analysis Date = 02/18/14 
 Pct Recovery = 74%  Analysis Date = 02/18/14 
 Pct Recovery = 74%  Analysis Date = 02/16/14 
 Pct Recovery = 74%  Analysis Date = 02/16/14 
 Pct Recovery = 74%  Analysis Date = 02/14/14 
 Pct Recovery = 74%  Analysis Date = 02/14/14 
 Pct Recovery = 74%  Analysis Date = 02/12/14 
 Pct Recovery = 74%  Analysis Date = 02/12/14 
 Pct Recovery = 74%  Analysis Date = 02/09/14 
 Pct Recovery = 74%  Analysis Date = 02/09/14 
 Pct Recovery = 74%  Analysis Date = 02/07/14 
 Pct Recovery = 74%  Analysis Date = 02/07/14 
 Pct Recovery = 74%  Analysis Date = 02/05/14 
 Pct Recovery = 74%  Analysis Date = 02/05/14 
 Pct Recovery = 74%  Analysis Date = 02/02/14 
 Pct Recovery = 74%  Analysis Date = 02/02/14 
 Pct Recovery = 74%  Analysis Date = 01/31/14 
 Pct Recovery = 74%  Analysis Date = 01/31/14 
 Pct Recovery = 74%  Analysis Date = 01/29/14 
 Pct Recovery = 74%  Analysis Date = 01/29/14 
 Pct Recovery = 74%  Analysis Date = 01/26/14 
 Pct Recovery = 74%  Analysis Date = 01/26/14 
 Pct Recovery = 74%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/19/14 
 Pct Recovery = 74%  Analysis Date = 01/19/14 
 Pct Recovery = 74%  Analysis Date = 01/17/14 
 Pct Recovery = 74%  Analysis Date = 01/17/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/03/14 
 Pct Recovery = 74%  Analysis Date = 01/03/14 
 Pct Recovery = 74%  Analysis Date = 01/01/14 
 Pct Recovery = 74%  Analysis Date = 01/01/14 
 Pct Recovery = 74%  Analysis Date = 12/30/13 
 Pct Recovery = 74%  Analysis Date = 12/30/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/25/13 
 Pct Recovery = 74%  Analysis Date = 12/25/13 
 Pct Recovery = 74%  Analysis Date = 12/23/13 
 Pct Recovery = 74%  Analysis Date = 12/23/13 
 Pct Recovery = 74%  Analysis Date = 12/20/13 
 Pct Recovery = 74%  Analysis Date = 12/20/13 
 Pct Recovery = 74%  Analysis Date = 12/18/13 
 Pct Recovery = 74%  Analysis Date = 12/18/13 
 Pct Recovery = 74%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/13/13 
 Pct Recovery = 74%  Analysis Date = 12/13/13 
 Pct Recovery = 74%  Analysis Date = 12/11/13 
 Pct Recovery = 74%  Analysis Date = 12/11/13 
 Pct Recovery = 74%  Analysis Date = 12/09/13 
 Pct Recovery = 74%  Analysis Date = 12/09/13 
 Pct Recovery = 74%  Analysis Date = 12/07/13 
 Pct Recovery = 74%  Analysis Date = 12/07/13 
 Pct Recovery = 74%  Analysis Date = 12/04/13 
 Pct Recovery = 74%  Analysis Date = 12/04/13 
 Pct Recovery = 74%  Analysis Date = 12/02/13 
 Pct Recovery = 73%  Analysis Date = 12/02/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/27/13 
 Pct Recovery = 73%  Analysis Date = 11/27/13 
 Pct Recovery = 73%  Analysis Date = 11/25/13 
 Pct Recovery = 73%  Analysis Date = 11/25/13 
 Pct Recovery = 73%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/07/13 
 Pct Recovery = 71%  Analysis Date = 11/07/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 11/02/13 
 Pct Recovery = 71%  Analysis Date = 10/31/13 
 Pct Recovery = 70%  Analysis Date = 10/31/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/24/13 
 Pct Recovery = 70%  Analysis Date = 10/24/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 69%  Analysis Date = 10/19/13 
 Pct Recovery = 69%  Analysis Date = 10/17/13 
 Pct Recovery = 69%  Analysis Date = 10/17/13 
 Pct Recovery = 69%  Analysis Date = 10/14/13 
 Pct Recovery = 69%  Analysis Date = 10/14/13 
 Pct Recovery = 69%  Analysis Date = 10/12/13 
 Pct Recovery = 69%  Analysis Date = 10/12/13 
 Pct Recovery = 69%  Analysis Date = 10/10/13 
 Pct Recovery = 69%  Analysis Date = 10/10/13 
 Pct Recovery = 69%  Analysis Date = 10/07/13 
 Pct Recovery = 68%  Analysis Date = 10/07/13 
 Pct Recovery = 68%  Analysis Date = 10/05/13 
 Pct Recovery = 68%  Analysis Date = 10/05/13 
 Pct Recovery = 68%  Analysis Date = 10/03/13 
 Pct Recovery = 68%  Analysis Date = 10/03/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 09/28/13 
 Pct Recovery = 68%  Analysis Date = 09/28/13 
 Pct Recovery = 68%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 66%  Analysis Date = 09/14/13 
 Pct Recovery = 66%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/10/13 
 Pct Recovery = 66%  Analysis Date = 09/10/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/05/13 
 Pct Recovery = 66%  Analysis Date = 09/05/13 
 Pct Recovery = 66%  Analysis Date = 09/03/13 
 Pct Recovery = 65%  Analysis Date = 09/03/13 
 Pct Recovery = 65%  Analysis Date = 09/01/13 
 Pct Recovery = 65%  Analysis Date = 09/01/13 
 Pct Recovery = 65%  Analysis Date = 08/29/13 
 Pct Recovery = 65%  Analysis Date = 08/29/13 
 Pct Recovery = 65%  Analysis Date = 08/27/13 
 Pct Recovery = 65%  Analysis Date = 08/27/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/11/13 
 Pct Recovery = 64%  Analysis Date = 08/11/13 
 Pct Recovery = 64%  Analysis Date = 08/08/13 
 Pct Recovery = 64%  Analysis Date = 08/08/13 
 Pct Recovery = 64%  Analysis Date = 08/06/13 
 Pct Recovery = 64%  Analysis Date = 08/06/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 07/30/13 
 Pct Recovery = 65%  Analysis Date = 07/30/13 
 Pct Recovery = 65%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 70%  Analysis Date = 07/02/13 
 Pct Recovery = 70%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/28/13 
 Pct Recovery = 71%  Analysis Date = 06/28/13 
 Pct Recovery = 71%  Analysis Date = 06/26/13 
 Pct Recovery = 71%  Analysis Date = 06/26/13 
 Pct Recovery = 71%  Analysis Date = 06/23/13 
 Pct Recovery = 71%  Analysis Date = 06/23/13 
 Pct Recovery = 71%  Analysis Date = 06/21/13 
 Pct Recovery = 72%  Analysis Date = 06/21/13 
 Pct Recovery = 72%  Analysis Date = 06/19/13 
 Pct Recovery = 72%  Analysis Date = 06/19/13 
 Pct Recovery = 72%  Analysis Date = 06/16/13 
 Pct Recovery = 73%  Analysis Date = 06/16/13 
 Pct Recovery = 73%  Analysis Date = 06/14/13 
 Pct Recovery = 73%  Analysis Date = 06/14/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 74%  Analysis Date = 06/12/13 
 Pct Recovery = 74%  Analysis Date = 06/09/13 
 Pct Recovery = 74%  Analysis Date = 06/09/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 76%  Analysis Date = 05/31/13 
 Pct Recovery = 76%  Analysis Date = 05/29/13 
 Pct Recovery = 76%  Analysis Date = 05/29/13 
 Pct Recovery = 76%  Analysis Date = 05/27/13 
 Pct Recovery = 77%  Analysis Date = 05/27/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 78%  Analysis Date = 05/20/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 80%  Analysis Date = 05/10/13 
 Pct Recovery = 80%  Analysis Date = 05/08/13 
 Pct Recovery = 80%  Analysis Date = 05/08/13 
 Pct Recovery = 80%  Analysis Date = 05/06/13 
 Pct Recovery = 80%  Analysis Date = 05/06/13 
 Pct Recovery = 80%  Analysis Date = 05/03/13 
 Pct Recovery = 81%  Analysis Date = 05/03/13 
 Pct Recovery = 81%  Analysis Date = 05/01/13 
 Pct Recovery = 81%  Analysis Date = 05/01/13 
 Pct Recovery = 81%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 82%  Analysis Date = 04/24/13 
 Pct Recovery = 82%  Analysis Date = 04/24/13 
 Pct Recovery = 82%  Analysis Date = 04/22/13 
 Pct Recovery = 83%  Analysis Date = 04/22/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/17/13 
 Pct Recovery = 83%  Analysis Date = 04/17/13 
 Pct Recovery = 83%  Analysis Date = 04/15/13 
 Pct Recovery = 84%  Analysis Date = 04/15/13 
 Pct Recovery = 84%  Analysis Date = 04/13/13 
 Pct Recovery = 84%  Analysis Date = 04/13/13 
 Pct Recovery = 84%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 85%  Analysis Date = 04/06/13 
 Pct Recovery = 85%  Analysis Date = 04/06/13 
 Pct Recovery = 85%  Analysis Date = 04/03/13 
 Pct Recovery = 86%  Analysis Date = 04/03/13 
 Pct Recovery = 86%  Analysis Date = 04/01/13 
 Pct Recovery = 86%  Analysis Date = 04/01/13 
 Pct Recovery = 86%  Analysis Date = 03/30/13 
 Pct Recovery = 86%  Analysis Date = 03/30/13 
 Pct Recovery = 86%  Analysis Date = 03/27/13 
 Pct Recovery = 87%  Analysis Date = 03/27/13 
 Pct Recovery = 87%  Analysis Date = 03/25/13 
 Pct Recovery = 87%  Analysis Date = 03/25/13 
 Pct Recovery = 87%  Analysis Date = 03/23/13 
 Pct Recovery = 87%  Analysis Date = 03/23/13 
 Pct Recovery = 87%  Analysis Date = 03/21/13 
 Pct Recovery = 87%  Analysis Date = 03/21/13 
 Pct Recovery = 87%  Analysis Date = 03/18/13 
 Pct Recovery = 87%  Analysis Date = 03/18/13 
 Pct Recovery = 87%  Analysis Date = 03/16/13 
 Pct Recovery = 87%  Analysis Date = 03/16/13 
 Pct Recovery = 87%  Analysis Date = 03/14/13 
 Pct Recovery = 87%  Analysis Date = 03/14/13 
 Pct Recovery = 87%  Analysis Date = 03/11/13 
 Pct Recovery = 87%  Analysis Date = 03/11/13 
 Pct Recovery = 87%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/07/13 
 Pct Recovery = 88%  Analysis Date = 03/07/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 88%  Analysis Date = 02/21/13 
 Pct Recovery = 88%  Analysis Date = 02/21/13 
 Pct Recovery = 88%  Analysis Date = 02/18/13 
 Pct Recovery = 88%  Analysis Date = 02/18/13 
 Pct Recovery = 88%  Analysis Date = 02/16/13 
 Pct Recovery = 88%  Analysis Date = 02/16/13 
 Pct Recovery = 88%  Analysis Date = 02/14/13 
 Pct Recovery = 89%  Analysis Date = 02/14/13 
 Pct Recovery = 89%  Analysis Date = 02/12/13 
 Pct Recovery = 89%  Analysis Date = 02/12/13 
 Pct Recovery = 89%  Analysis Date = 02/09/13 
 Pct Recovery = 89%  Analysis Date = 02/09/13 
 Pct Recovery = 89%  Analysis Date = 02/07/13 
 Pct Recovery = 89%  Analysis Date = 02/07/13 
 Pct Recovery = 89%  Analysis Date = 02/05/13 
 Pct Recovery = 89%  Analysis Date = 02/05/13 
 Pct Recovery = 89%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 01/31/13 
 Pct Recovery = 89%  Analysis Date = 01/31/13 
 Pct Recovery = 89%  Analysis Date = 01/29/13 
 Pct Recovery = 89%  Analysis Date = 01/29/13 
 Pct Recovery = 89%  Analysis Date = 01/26/13 
 Pct Recovery = 89%  Analysis Date = 01/26/13 
 Pct Recovery = 89%  Analysis Date = 01/24/13 
 Pct Recovery = 89%  Analysis Date = 01/24/13 
 Pct Recovery = 89%  Analysis Date = 01/22/13 
 Pct Recovery = 89%  Analysis Date = 01/22/13 
 Pct Recovery = 89%  Analysis Date = 01/19/13 
 Pct Recovery = 89%  Analysis Date = 01/19/13 
 Pct Recovery = 89%  Analysis Date = 01/17/13 
 Pct Recovery = 90%  Analysis Date = 01/17/13 
 Pct Recovery = 90%  Analysis Date = 01/15/13 
 Pct Recovery = 90%  Analysis Date = 01/15/13 
 Pct Recovery = 90%  Analysis Date = 01/13/13 
 Pct Recovery = 90%  Analysis Date = 01/13/13 
 Pct Recovery = 90%  Analysis Date = 01/10/13 
 Pct Recovery = 90%  Analysis Date = 01/10/13 
 Pct Recovery = 90%  Analysis Date = 01/08/13 
 Pct Recovery = 90%  Analysis Date = 01/08/13 
 Pct Recovery = 90%  Analysis Date = 01/06/13 
 Pct Recovery = 90%  Analysis Date = 01/06/13 
 Pct Recovery = 90%  Analysis Date = 01/03/13 
 Pct Recovery = 90%  Analysis Date = 01/03/13 
 Pct Recovery = 90%  Analysis Date = 01/01/13 
 Pct Recovery = 90%  Analysis Date = 01/01/13 
 Pct Recovery = 90%  Analysis Date = 12/30/12 
 Pct Recovery = 90%  Analysis Date = 12/30/12 
 Pct Recovery = 90%  Analysis Date = 12/27/12 
 Pct Recovery = 90%  Analysis Date = 12/27/12 
 Pct Recovery = 90%  Analysis Date = 12/25/12 
 Pct Recovery = 90%  Analysis Date = 12/25/12 
 Pct Recovery = 90%  Analysis Date = 12/23/12 
 Pct Recovery = 90%  Analysis Date = 12/23/12 
 Pct Recovery = 90%  Analysis Date = 12/20/12 
 Pct Recovery = 91%  Analysis Date = 12/20/12 
 Pct Recovery = 91%  Analysis Date = 12/18/12 
 Pct Recovery = 91%  Analysis Date = 12/18/12 
 Pct Recovery = 91%  Analysis Date = 12/16/12 
 Pct Recovery = 91%  Analysis Date = 12/16/12 
 Pct Recovery = 91%  Analysis Date = 12/14/12 
 Pct Recovery = 91%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEHYDRONIFEDIPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 77% 11% 77% 11%
Total 14 77% 11% 77% 11%

Sample Statistics
DEHYDRONIFEDIPINE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 3 20% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
DESMETHYLDILTIAZEM
METHOD: LC9017 , TESTIDCODE: 67999LCM56

The SGPlot Procedure

Sample Statistics
DESMETHYLDILTIAZEM

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 5 16% 5 out of 31

OBSP Determination:
DESVENLAFAXINE
METHOD: LC9017 , TESTIDCODE: 68251LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 63%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 84%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 66%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 34%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 30%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 66%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 74%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 60%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 47%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 89%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 54%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 88%  Analysis Date = 03/21/14 
 Pct Recovery = 41%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 43%  Analysis Date = 03/14/14 
 Pct Recovery = 43%  Analysis Date = 03/11/14 
 Pct Recovery = 43%  Analysis Date = 03/11/14 
 Pct Recovery = 43%  Analysis Date = 03/09/14 
 Pct Recovery = 43%  Analysis Date = 03/09/14 
 Pct Recovery = 43%  Analysis Date = 03/07/14 
 Pct Recovery = 44%  Analysis Date = 03/07/14 
 Pct Recovery = 44%  Analysis Date = 03/04/14 
 Pct Recovery = 44%  Analysis Date = 03/04/14 
 Pct Recovery = 44%  Analysis Date = 03/02/14 
 Pct Recovery = 44%  Analysis Date = 03/02/14 
 Pct Recovery = 44%  Analysis Date = 02/28/14 
 Pct Recovery = 45%  Analysis Date = 02/28/14 
 Pct Recovery = 45%  Analysis Date = 02/25/14 
 Pct Recovery = 45%  Analysis Date = 02/25/14 
 Pct Recovery = 45%  Analysis Date = 02/23/14 
 Pct Recovery = 46%  Analysis Date = 02/23/14 
 Pct Recovery = 46%  Analysis Date = 02/21/14 
 Pct Recovery = 46%  Analysis Date = 02/21/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/16/14 
 Pct Recovery = 47%  Analysis Date = 02/16/14 
 Pct Recovery = 47%  Analysis Date = 02/14/14 
 Pct Recovery = 47%  Analysis Date = 02/14/14 
 Pct Recovery = 47%  Analysis Date = 02/12/14 
 Pct Recovery = 47%  Analysis Date = 02/12/14 
 Pct Recovery = 47%  Analysis Date = 02/09/14 
 Pct Recovery = 47%  Analysis Date = 02/09/14 
 Pct Recovery = 47%  Analysis Date = 02/07/14 
 Pct Recovery = 47%  Analysis Date = 02/07/14 
 Pct Recovery = 47%  Analysis Date = 02/05/14 
 Pct Recovery = 48%  Analysis Date = 02/05/14 
 Pct Recovery = 48%  Analysis Date = 02/02/14 
 Pct Recovery = 48%  Analysis Date = 02/02/14 
 Pct Recovery = 48%  Analysis Date = 01/31/14 
 Pct Recovery = 48%  Analysis Date = 01/31/14 
 Pct Recovery = 48%  Analysis Date = 01/29/14 
 Pct Recovery = 48%  Analysis Date = 01/29/14 
 Pct Recovery = 48%  Analysis Date = 01/26/14 
 Pct Recovery = 49%  Analysis Date = 01/26/14 
 Pct Recovery = 49%  Analysis Date = 01/24/14 
 Pct Recovery = 49%  Analysis Date = 01/24/14 
 Pct Recovery = 49%  Analysis Date = 01/22/14 
 Pct Recovery = 49%  Analysis Date = 01/22/14 
 Pct Recovery = 49%  Analysis Date = 01/19/14 
 Pct Recovery = 49%  Analysis Date = 01/19/14 
 Pct Recovery = 49%  Analysis Date = 01/17/14 
 Pct Recovery = 50%  Analysis Date = 01/17/14 
 Pct Recovery = 50%  Analysis Date = 01/15/14 
 Pct Recovery = 50%  Analysis Date = 01/15/14 
 Pct Recovery = 50%  Analysis Date = 01/13/14 
 Pct Recovery = 50%  Analysis Date = 01/13/14 
 Pct Recovery = 50%  Analysis Date = 01/10/14 
 Pct Recovery = 50%  Analysis Date = 01/10/14 
 Pct Recovery = 50%  Analysis Date = 01/08/14 
 Pct Recovery = 51%  Analysis Date = 01/08/14 
 Pct Recovery = 51%  Analysis Date = 01/06/14 
 Pct Recovery = 51%  Analysis Date = 01/06/14 
 Pct Recovery = 51%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 12/30/13 
 Pct Recovery = 52%  Analysis Date = 12/30/13 
 Pct Recovery = 52%  Analysis Date = 12/27/13 
 Pct Recovery = 52%  Analysis Date = 12/27/13 
 Pct Recovery = 52%  Analysis Date = 12/25/13 
 Pct Recovery = 52%  Analysis Date = 12/25/13 
 Pct Recovery = 52%  Analysis Date = 12/23/13 
 Pct Recovery = 52%  Analysis Date = 12/23/13 
 Pct Recovery = 52%  Analysis Date = 12/20/13 
 Pct Recovery = 53%  Analysis Date = 12/20/13 
 Pct Recovery = 53%  Analysis Date = 12/18/13 
 Pct Recovery = 53%  Analysis Date = 12/18/13 
 Pct Recovery = 53%  Analysis Date = 12/16/13 
 Pct Recovery = 53%  Analysis Date = 12/16/13 
 Pct Recovery = 53%  Analysis Date = 12/13/13 
 Pct Recovery = 53%  Analysis Date = 12/13/13 
 Pct Recovery = 53%  Analysis Date = 12/11/13 
 Pct Recovery = 54%  Analysis Date = 12/11/13 
 Pct Recovery = 54%  Analysis Date = 12/09/13 
 Pct Recovery = 54%  Analysis Date = 12/09/13 
 Pct Recovery = 54%  Analysis Date = 12/07/13 
 Pct Recovery = 54%  Analysis Date = 12/07/13 
 Pct Recovery = 54%  Analysis Date = 12/04/13 
 Pct Recovery = 54%  Analysis Date = 12/04/13 
 Pct Recovery = 54%  Analysis Date = 12/02/13 
 Pct Recovery = 55%  Analysis Date = 12/02/13 
 Pct Recovery = 55%  Analysis Date = 11/30/13 
 Pct Recovery = 55%  Analysis Date = 11/30/13 
 Pct Recovery = 55%  Analysis Date = 11/27/13 
 Pct Recovery = 55%  Analysis Date = 11/27/13 
 Pct Recovery = 55%  Analysis Date = 11/25/13 
 Pct Recovery = 55%  Analysis Date = 11/25/13 
 Pct Recovery = 55%  Analysis Date = 11/23/13 
 Pct Recovery = 55%  Analysis Date = 11/23/13 
 Pct Recovery = 55%  Analysis Date = 11/20/13 
 Pct Recovery = 56%  Analysis Date = 11/20/13 
 Pct Recovery = 56%  Analysis Date = 11/18/13 
 Pct Recovery = 56%  Analysis Date = 11/18/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 57%  Analysis Date = 11/11/13 
 Pct Recovery = 57%  Analysis Date = 11/09/13 
 Pct Recovery = 57%  Analysis Date = 11/09/13 
 Pct Recovery = 57%  Analysis Date = 11/07/13 
 Pct Recovery = 57%  Analysis Date = 11/07/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 58%  Analysis Date = 11/02/13 
 Pct Recovery = 58%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/26/13 
 Pct Recovery = 58%  Analysis Date = 10/26/13 
 Pct Recovery = 58%  Analysis Date = 10/24/13 
 Pct Recovery = 59%  Analysis Date = 10/24/13 
 Pct Recovery = 59%  Analysis Date = 10/21/13 
 Pct Recovery = 59%  Analysis Date = 10/21/13 
 Pct Recovery = 59%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/05/13 
 Pct Recovery = 60%  Analysis Date = 10/05/13 
 Pct Recovery = 60%  Analysis Date = 10/03/13 
 Pct Recovery = 61%  Analysis Date = 10/03/13 
 Pct Recovery = 61%  Analysis Date = 10/01/13 
 Pct Recovery = 61%  Analysis Date = 10/01/13 
 Pct Recovery = 61%  Analysis Date = 09/28/13 
 Pct Recovery = 61%  Analysis Date = 09/28/13 
 Pct Recovery = 61%  Analysis Date = 09/26/13 
 Pct Recovery = 61%  Analysis Date = 09/26/13 
 Pct Recovery = 61%  Analysis Date = 09/24/13 
 Pct Recovery = 62%  Analysis Date = 09/24/13 
 Pct Recovery = 62%  Analysis Date = 09/21/13 
 Pct Recovery = 62%  Analysis Date = 09/21/13 
 Pct Recovery = 62%  Analysis Date = 09/19/13 
 Pct Recovery = 62%  Analysis Date = 09/19/13 
 Pct Recovery = 62%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/07/13 
 Pct Recovery = 63%  Analysis Date = 09/07/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 64%  Analysis Date = 09/03/13 
 Pct Recovery = 64%  Analysis Date = 09/01/13 
 Pct Recovery = 64%  Analysis Date = 09/01/13 
 Pct Recovery = 64%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/22/13 
 Pct Recovery = 65%  Analysis Date = 08/22/13 
 Pct Recovery = 65%  Analysis Date = 08/20/13 
 Pct Recovery = 65%  Analysis Date = 08/20/13 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 Pct Recovery = 66%  Analysis Date = 08/18/13 
 Pct Recovery = 66%  Analysis Date = 08/15/13 
 Pct Recovery = 66%  Analysis Date = 08/15/13 
 Pct Recovery = 66%  Analysis Date = 08/13/13 
 Pct Recovery = 66%  Analysis Date = 08/13/13 
 Pct Recovery = 66%  Analysis Date = 08/11/13 
 Pct Recovery = 66%  Analysis Date = 08/11/13 
 Pct Recovery = 66%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 67%  Analysis Date = 08/06/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/12/13 
 Pct Recovery = 67%  Analysis Date = 07/12/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/05/13 
 Pct Recovery = 67%  Analysis Date = 07/05/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 06/30/13 
 Pct Recovery = 67%  Analysis Date = 06/30/13 
 Pct Recovery = 67%  Analysis Date = 06/28/13 
 Pct Recovery = 67%  Analysis Date = 06/28/13 
 Pct Recovery = 67%  Analysis Date = 06/26/13 
 Pct Recovery = 67%  Analysis Date = 06/26/13 
 Pct Recovery = 67%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/21/13 
 Pct Recovery = 68%  Analysis Date = 06/21/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/14/13 
 Pct Recovery = 68%  Analysis Date = 06/14/13 
 Pct Recovery = 68%  Analysis Date = 06/12/13 
 Pct Recovery = 68%  Analysis Date = 06/12/13 
 Pct Recovery = 68%  Analysis Date = 06/09/13 
 Pct Recovery = 68%  Analysis Date = 06/09/13 
 Pct Recovery = 68%  Analysis Date = 06/07/13 
 Pct Recovery = 68%  Analysis Date = 06/07/13 
 Pct Recovery = 68%  Analysis Date = 06/05/13 
 Pct Recovery = 68%  Analysis Date = 06/05/13 
 Pct Recovery = 68%  Analysis Date = 06/02/13 
 Pct Recovery = 68%  Analysis Date = 06/02/13 
 Pct Recovery = 68%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/24/13 
 Pct Recovery = 68%  Analysis Date = 05/24/13 
 Pct Recovery = 68%  Analysis Date = 05/22/13 
 Pct Recovery = 68%  Analysis Date = 05/22/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 69%  Analysis Date = 04/26/13 
 Pct Recovery = 69%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/20/13 
 Pct Recovery = 69%  Analysis Date = 04/20/13 
 Pct Recovery = 69%  Analysis Date = 04/17/13 
 Pct Recovery = 70%  Analysis Date = 04/17/13 
 Pct Recovery = 70%  Analysis Date = 04/15/13 
 Pct Recovery = 70%  Analysis Date = 04/15/13 
 Pct Recovery = 70%  Analysis Date = 04/13/13 
 Pct Recovery = 70%  Analysis Date = 04/13/13 
 Pct Recovery = 70%  Analysis Date = 04/10/13 
 Pct Recovery = 70%  Analysis Date = 04/10/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 Pct Recovery = 72%  Analysis Date = 03/25/13 
 Pct Recovery = 72%  Analysis Date = 03/25/13 
 Pct Recovery = 72%  Analysis Date = 03/23/13 
 Pct Recovery = 72%  Analysis Date = 03/23/13 
 Pct Recovery = 72%  Analysis Date = 03/21/13 
 Pct Recovery = 73%  Analysis Date = 03/21/13 
 Pct Recovery = 73%  Analysis Date = 03/18/13 
 Pct Recovery = 73%  Analysis Date = 03/18/13 
 Pct Recovery = 73%  Analysis Date = 03/16/13 
 Pct Recovery = 73%  Analysis Date = 03/16/13 
 Pct Recovery = 73%  Analysis Date = 03/14/13 
 Pct Recovery = 74%  Analysis Date = 03/14/13 
 Pct Recovery = 74%  Analysis Date = 03/11/13 
 Pct Recovery = 74%  Analysis Date = 03/11/13 
 Pct Recovery = 74%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/04/13 
 Pct Recovery = 75%  Analysis Date = 03/04/13 
 Pct Recovery = 75%  Analysis Date = 03/02/13 
 Pct Recovery = 75%  Analysis Date = 03/02/13 
 Pct Recovery = 75%  Analysis Date = 02/28/13 
 Pct Recovery = 76%  Analysis Date = 02/28/13 
 Pct Recovery = 76%  Analysis Date = 02/25/13 
 Pct Recovery = 76%  Analysis Date = 02/25/13 
 Pct Recovery = 76%  Analysis Date = 02/23/13 
 Pct Recovery = 76%  Analysis Date = 02/23/13 
 Pct Recovery = 76%  Analysis Date = 02/21/13 
 Pct Recovery = 77%  Analysis Date = 02/21/13 
 Pct Recovery = 77%  Analysis Date = 02/18/13 
 Pct Recovery = 77%  Analysis Date = 02/18/13 
 Pct Recovery = 77%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 79%  Analysis Date = 02/07/13 
 Pct Recovery = 79%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/29/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/26/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/24/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/22/13 
 Pct Recovery = 81%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/10/13 
 Pct Recovery = 83%  Analysis Date = 01/10/13 
 Pct Recovery = 83%  Analysis Date = 01/08/13 
 Pct Recovery = 83%  Analysis Date = 01/08/13 
 Pct Recovery = 83%  Analysis Date = 01/06/13 
 Pct Recovery = 84%  Analysis Date = 01/06/13 
 Pct Recovery = 84%  Analysis Date = 01/03/13 
 Pct Recovery = 84%  Analysis Date = 01/03/13 
 Pct Recovery = 84%  Analysis Date = 01/01/13 
 Pct Recovery = 85%  Analysis Date = 01/01/13 
 Pct Recovery = 85%  Analysis Date = 12/30/12 
 Pct Recovery = 85%  Analysis Date = 12/30/12 
 Pct Recovery = 85%  Analysis Date = 12/27/12 
 Pct Recovery = 85%  Analysis Date = 12/27/12 
 Pct Recovery = 85%  Analysis Date = 12/25/12 
 Pct Recovery = 86%  Analysis Date = 12/25/12 
 Pct Recovery = 86%  Analysis Date = 12/23/12 
 Pct Recovery = 86%  Analysis Date = 12/23/12 
 Pct Recovery = 86%  Analysis Date = 12/20/12 
 Pct Recovery = 86%  Analysis Date = 12/20/12 
 Pct Recovery = 86%  Analysis Date = 12/18/12 
 Pct Recovery = 87%  Analysis Date = 12/18/12 
 Pct Recovery = 87%  Analysis Date = 12/16/12 
 Pct Recovery = 87%  Analysis Date = 12/16/12 
 Pct Recovery = 87%  Analysis Date = 12/14/12 
 Pct Recovery = 87%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESVENLAFAXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 62% 18% 64% 17%
Total 14 62% 18% 64% 17%

Sample Statistics
DESVENLAFAXINE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
DEXTROMETHORPHAN
METHOD: LC9017 , TESTIDCODE: 67468LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 45%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 82%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 44%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 58%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 48%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 43%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 29%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 70%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 46%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 56%  Analysis Date = 03/21/14 
 Pct Recovery = 53%  Analysis Date = 03/18/14 
 Pct Recovery = 53%  Analysis Date = 03/18/14 
 Pct Recovery = 53%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/14/14 
 Pct Recovery = 52%  Analysis Date = 03/14/14 
 Pct Recovery = 52%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/04/14 
 Pct Recovery = 52%  Analysis Date = 03/04/14 
 Pct Recovery = 52%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 02/28/14 
 Pct Recovery = 52%  Analysis Date = 02/28/14 
 Pct Recovery = 52%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/17/14 
 Pct Recovery = 50%  Analysis Date = 01/17/14 
 Pct Recovery = 50%  Analysis Date = 01/15/14 
 Pct Recovery = 50%  Analysis Date = 01/15/14 
 Pct Recovery = 50%  Analysis Date = 01/13/14 
 Pct Recovery = 50%  Analysis Date = 01/13/14 
 Pct Recovery = 50%  Analysis Date = 01/10/14 
 Pct Recovery = 50%  Analysis Date = 01/10/14 
 Pct Recovery = 50%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/03/14 
 Pct Recovery = 50%  Analysis Date = 01/03/14 
 Pct Recovery = 50%  Analysis Date = 01/01/14 
 Pct Recovery = 50%  Analysis Date = 01/01/14 
 Pct Recovery = 50%  Analysis Date = 12/30/13 
 Pct Recovery = 50%  Analysis Date = 12/30/13 
 Pct Recovery = 50%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/11/13 
 Pct Recovery = 50%  Analysis Date = 12/11/13 
 Pct Recovery = 50%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/07/13 
 Pct Recovery = 50%  Analysis Date = 12/07/13 
 Pct Recovery = 50%  Analysis Date = 12/04/13 
 Pct Recovery = 50%  Analysis Date = 12/04/13 
 Pct Recovery = 50%  Analysis Date = 12/02/13 
 Pct Recovery = 50%  Analysis Date = 12/02/13 
 Pct Recovery = 50%  Analysis Date = 11/30/13 
 Pct Recovery = 50%  Analysis Date = 11/30/13 
 Pct Recovery = 50%  Analysis Date = 11/27/13 
 Pct Recovery = 50%  Analysis Date = 11/27/13 
 Pct Recovery = 50%  Analysis Date = 11/25/13 
 Pct Recovery = 51%  Analysis Date = 11/25/13 
 Pct Recovery = 51%  Analysis Date = 11/23/13 
 Pct Recovery = 51%  Analysis Date = 11/23/13 
 Pct Recovery = 51%  Analysis Date = 11/20/13 
 Pct Recovery = 51%  Analysis Date = 11/20/13 
 Pct Recovery = 51%  Analysis Date = 11/18/13 
 Pct Recovery = 51%  Analysis Date = 11/18/13 
 Pct Recovery = 51%  Analysis Date = 11/16/13 
 Pct Recovery = 52%  Analysis Date = 11/16/13 
 Pct Recovery = 52%  Analysis Date = 11/13/13 
 Pct Recovery = 52%  Analysis Date = 11/13/13 
 Pct Recovery = 52%  Analysis Date = 11/11/13 
 Pct Recovery = 52%  Analysis Date = 11/11/13 
 Pct Recovery = 52%  Analysis Date = 11/09/13 
 Pct Recovery = 52%  Analysis Date = 11/09/13 
 Pct Recovery = 52%  Analysis Date = 11/07/13 
 Pct Recovery = 53%  Analysis Date = 11/07/13 
 Pct Recovery = 53%  Analysis Date = 11/04/13 
 Pct Recovery = 53%  Analysis Date = 11/04/13 
 Pct Recovery = 53%  Analysis Date = 11/02/13 
 Pct Recovery = 53%  Analysis Date = 11/02/13 
 Pct Recovery = 53%  Analysis Date = 10/31/13 
 Pct Recovery = 53%  Analysis Date = 10/31/13 
 Pct Recovery = 53%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/19/13 
 Pct Recovery = 55%  Analysis Date = 10/19/13 
 Pct Recovery = 55%  Analysis Date = 10/17/13 
 Pct Recovery = 55%  Analysis Date = 10/17/13 
 Pct Recovery = 55%  Analysis Date = 10/14/13 
 Pct Recovery = 55%  Analysis Date = 10/14/13 
 Pct Recovery = 55%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/10/13 
 Pct Recovery = 56%  Analysis Date = 10/10/13 
 Pct Recovery = 56%  Analysis Date = 10/07/13 
 Pct Recovery = 56%  Analysis Date = 10/07/13 
 Pct Recovery = 56%  Analysis Date = 10/05/13 
 Pct Recovery = 56%  Analysis Date = 10/05/13 
 Pct Recovery = 56%  Analysis Date = 10/03/13 
 Pct Recovery = 56%  Analysis Date = 10/03/13 
 Pct Recovery = 56%  Analysis Date = 10/01/13 
 Pct Recovery = 57%  Analysis Date = 10/01/13 
 Pct Recovery = 57%  Analysis Date = 09/28/13 
 Pct Recovery = 57%  Analysis Date = 09/28/13 
 Pct Recovery = 57%  Analysis Date = 09/26/13 
 Pct Recovery = 57%  Analysis Date = 09/26/13 
 Pct Recovery = 57%  Analysis Date = 09/24/13 
 Pct Recovery = 57%  Analysis Date = 09/24/13 
 Pct Recovery = 57%  Analysis Date = 09/21/13 
 Pct Recovery = 58%  Analysis Date = 09/21/13 
 Pct Recovery = 58%  Analysis Date = 09/19/13 
 Pct Recovery = 58%  Analysis Date = 09/19/13 
 Pct Recovery = 58%  Analysis Date = 09/17/13 
 Pct Recovery = 58%  Analysis Date = 09/17/13 
 Pct Recovery = 58%  Analysis Date = 09/14/13 
 Pct Recovery = 58%  Analysis Date = 09/14/13 
 Pct Recovery = 58%  Analysis Date = 09/12/13 
 Pct Recovery = 59%  Analysis Date = 09/12/13 
 Pct Recovery = 59%  Analysis Date = 09/10/13 
 Pct Recovery = 59%  Analysis Date = 09/10/13 
 Pct Recovery = 59%  Analysis Date = 09/07/13 
 Pct Recovery = 59%  Analysis Date = 09/07/13 
 Pct Recovery = 59%  Analysis Date = 09/05/13 
 Pct Recovery = 59%  Analysis Date = 09/05/13 
 Pct Recovery = 59%  Analysis Date = 09/03/13 
 Pct Recovery = 60%  Analysis Date = 09/03/13 
 Pct Recovery = 60%  Analysis Date = 09/01/13 
 Pct Recovery = 60%  Analysis Date = 09/01/13 
 Pct Recovery = 60%  Analysis Date = 08/29/13 
 Pct Recovery = 60%  Analysis Date = 08/29/13 
 Pct Recovery = 60%  Analysis Date = 08/27/13 
 Pct Recovery = 60%  Analysis Date = 08/27/13 
 Pct Recovery = 60%  Analysis Date = 08/25/13 
 Pct Recovery = 61%  Analysis Date = 08/25/13 
 Pct Recovery = 61%  Analysis Date = 08/22/13 
 Pct Recovery = 61%  Analysis Date = 08/22/13 
 Pct Recovery = 61%  Analysis Date = 08/20/13 
 Pct Recovery = 61%  Analysis Date = 08/20/13 
 Pct Recovery = 61%  Analysis Date = 08/18/13 
 Pct Recovery = 62%  Analysis Date = 08/18/13 
 Pct Recovery = 62%  Analysis Date = 08/15/13 
 Pct Recovery = 62%  Analysis Date = 08/15/13 
 Pct Recovery = 62%  Analysis Date = 08/13/13 
 Pct Recovery = 62%  Analysis Date = 08/13/13 
 Pct Recovery = 62%  Analysis Date = 08/11/13 
 Pct Recovery = 62%  Analysis Date = 08/11/13 
 Pct Recovery = 62%  Analysis Date = 08/08/13 
 Pct Recovery = 62%  Analysis Date = 08/08/13 
 Pct Recovery = 62%  Analysis Date = 08/06/13 
 Pct Recovery = 62%  Analysis Date = 08/06/13 
 Pct Recovery = 62%  Analysis Date = 08/04/13 
 Pct Recovery = 62%  Analysis Date = 08/04/13 
 Pct Recovery = 62%  Analysis Date = 08/02/13 
 Pct Recovery = 63%  Analysis Date = 08/02/13 
 Pct Recovery = 63%  Analysis Date = 07/30/13 
 Pct Recovery = 62%  Analysis Date = 07/30/13 
 Pct Recovery = 62%  Analysis Date = 07/28/13 
 Pct Recovery = 62%  Analysis Date = 07/28/13 
 Pct Recovery = 62%  Analysis Date = 07/26/13 
 Pct Recovery = 62%  Analysis Date = 07/26/13 
 Pct Recovery = 62%  Analysis Date = 07/23/13 
 Pct Recovery = 61%  Analysis Date = 07/23/13 
 Pct Recovery = 61%  Analysis Date = 07/21/13 
 Pct Recovery = 61%  Analysis Date = 07/21/13 
 Pct Recovery = 61%  Analysis Date = 07/19/13 
 Pct Recovery = 61%  Analysis Date = 07/19/13 
 Pct Recovery = 61%  Analysis Date = 07/16/13 
 Pct Recovery = 60%  Analysis Date = 07/16/13 
 Pct Recovery = 60%  Analysis Date = 07/14/13 
 Pct Recovery = 60%  Analysis Date = 07/14/13 
 Pct Recovery = 60%  Analysis Date = 07/12/13 
 Pct Recovery = 60%  Analysis Date = 07/12/13 
 Pct Recovery = 60%  Analysis Date = 07/09/13 
 Pct Recovery = 59%  Analysis Date = 07/09/13 
 Pct Recovery = 59%  Analysis Date = 07/07/13 
 Pct Recovery = 59%  Analysis Date = 07/07/13 
 Pct Recovery = 59%  Analysis Date = 07/05/13 
 Pct Recovery = 59%  Analysis Date = 07/05/13 
 Pct Recovery = 59%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 06/30/13 
 Pct Recovery = 58%  Analysis Date = 06/30/13 
 Pct Recovery = 58%  Analysis Date = 06/28/13 
 Pct Recovery = 58%  Analysis Date = 06/28/13 
 Pct Recovery = 58%  Analysis Date = 06/26/13 
 Pct Recovery = 58%  Analysis Date = 06/26/13 
 Pct Recovery = 58%  Analysis Date = 06/23/13 
 Pct Recovery = 57%  Analysis Date = 06/23/13 
 Pct Recovery = 57%  Analysis Date = 06/21/13 
 Pct Recovery = 57%  Analysis Date = 06/21/13 
 Pct Recovery = 57%  Analysis Date = 06/19/13 
 Pct Recovery = 57%  Analysis Date = 06/19/13 
 Pct Recovery = 57%  Analysis Date = 06/16/13 
 Pct Recovery = 56%  Analysis Date = 06/16/13 
 Pct Recovery = 56%  Analysis Date = 06/14/13 
 Pct Recovery = 56%  Analysis Date = 06/14/13 
 Pct Recovery = 56%  Analysis Date = 06/12/13 
 Pct Recovery = 56%  Analysis Date = 06/12/13 
 Pct Recovery = 56%  Analysis Date = 06/09/13 
 Pct Recovery = 55%  Analysis Date = 06/09/13 
 Pct Recovery = 55%  Analysis Date = 06/07/13 
 Pct Recovery = 55%  Analysis Date = 06/07/13 
 Pct Recovery = 55%  Analysis Date = 06/05/13 
 Pct Recovery = 55%  Analysis Date = 06/05/13 
 Pct Recovery = 55%  Analysis Date = 06/02/13 
 Pct Recovery = 54%  Analysis Date = 06/02/13 
 Pct Recovery = 54%  Analysis Date = 05/31/13 
 Pct Recovery = 54%  Analysis Date = 05/31/13 
 Pct Recovery = 54%  Analysis Date = 05/29/13 
 Pct Recovery = 54%  Analysis Date = 05/29/13 
 Pct Recovery = 54%  Analysis Date = 05/27/13 
 Pct Recovery = 53%  Analysis Date = 05/27/13 
 Pct Recovery = 53%  Analysis Date = 05/24/13 
 Pct Recovery = 53%  Analysis Date = 05/24/13 
 Pct Recovery = 53%  Analysis Date = 05/22/13 
 Pct Recovery = 53%  Analysis Date = 05/22/13 
 Pct Recovery = 53%  Analysis Date = 05/20/13 
 Pct Recovery = 52%  Analysis Date = 05/20/13 
 Pct Recovery = 52%  Analysis Date = 05/17/13 
 Pct Recovery = 52%  Analysis Date = 05/17/13 
 Pct Recovery = 52%  Analysis Date = 05/15/13 
 Pct Recovery = 52%  Analysis Date = 05/15/13 
 Pct Recovery = 52%  Analysis Date = 05/13/13 
 Pct Recovery = 52%  Analysis Date = 05/13/13 
 Pct Recovery = 52%  Analysis Date = 05/10/13 
 Pct Recovery = 51%  Analysis Date = 05/10/13 
 Pct Recovery = 51%  Analysis Date = 05/08/13 
 Pct Recovery = 51%  Analysis Date = 05/08/13 
 Pct Recovery = 51%  Analysis Date = 05/06/13 
 Pct Recovery = 51%  Analysis Date = 05/06/13 
 Pct Recovery = 51%  Analysis Date = 05/03/13 
 Pct Recovery = 50%  Analysis Date = 05/03/13 
 Pct Recovery = 50%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 04/29/13 
 Pct Recovery = 50%  Analysis Date = 04/29/13 
 Pct Recovery = 50%  Analysis Date = 04/26/13 
 Pct Recovery = 50%  Analysis Date = 04/26/13 
 Pct Recovery = 50%  Analysis Date = 04/24/13 
 Pct Recovery = 50%  Analysis Date = 04/24/13 
 Pct Recovery = 50%  Analysis Date = 04/22/13 
 Pct Recovery = 50%  Analysis Date = 04/22/13 
 Pct Recovery = 50%  Analysis Date = 04/20/13 
 Pct Recovery = 50%  Analysis Date = 04/20/13 
 Pct Recovery = 50%  Analysis Date = 04/17/13 
 Pct Recovery = 50%  Analysis Date = 04/17/13 
 Pct Recovery = 50%  Analysis Date = 04/15/13 
 Pct Recovery = 50%  Analysis Date = 04/15/13 
 Pct Recovery = 50%  Analysis Date = 04/13/13 
 Pct Recovery = 50%  Analysis Date = 04/13/13 
 Pct Recovery = 50%  Analysis Date = 04/10/13 
 Pct Recovery = 50%  Analysis Date = 04/10/13 
 Pct Recovery = 50%  Analysis Date = 04/08/13 
 Pct Recovery = 50%  Analysis Date = 04/08/13 
 Pct Recovery = 50%  Analysis Date = 04/06/13 
 Pct Recovery = 50%  Analysis Date = 04/06/13 
 Pct Recovery = 50%  Analysis Date = 04/03/13 
 Pct Recovery = 49%  Analysis Date = 04/03/13 
 Pct Recovery = 49%  Analysis Date = 04/01/13 
 Pct Recovery = 49%  Analysis Date = 04/01/13 
 Pct Recovery = 49%  Analysis Date = 03/30/13 
 Pct Recovery = 49%  Analysis Date = 03/30/13 
 Pct Recovery = 49%  Analysis Date = 03/27/13 
 Pct Recovery = 49%  Analysis Date = 03/27/13 
 Pct Recovery = 49%  Analysis Date = 03/25/13 
 Pct Recovery = 50%  Analysis Date = 03/25/13 
 Pct Recovery = 50%  Analysis Date = 03/23/13 
 Pct Recovery = 50%  Analysis Date = 03/23/13 
 Pct Recovery = 50%  Analysis Date = 03/21/13 
 Pct Recovery = 51%  Analysis Date = 03/21/13 
 Pct Recovery = 51%  Analysis Date = 03/18/13 
 Pct Recovery = 51%  Analysis Date = 03/18/13 
 Pct Recovery = 51%  Analysis Date = 03/16/13 
 Pct Recovery = 52%  Analysis Date = 03/16/13 
 Pct Recovery = 52%  Analysis Date = 03/14/13 
 Pct Recovery = 53%  Analysis Date = 03/14/13 
 Pct Recovery = 53%  Analysis Date = 03/11/13 
 Pct Recovery = 53%  Analysis Date = 03/11/13 
 Pct Recovery = 53%  Analysis Date = 03/09/13 
 Pct Recovery = 54%  Analysis Date = 03/09/13 
 Pct Recovery = 54%  Analysis Date = 03/07/13 
 Pct Recovery = 54%  Analysis Date = 03/07/13 
 Pct Recovery = 54%  Analysis Date = 03/04/13 
 Pct Recovery = 55%  Analysis Date = 03/04/13 
 Pct Recovery = 55%  Analysis Date = 03/02/13 
 Pct Recovery = 56%  Analysis Date = 03/02/13 
 Pct Recovery = 56%  Analysis Date = 02/28/13 
 Pct Recovery = 56%  Analysis Date = 02/28/13 
 Pct Recovery = 56%  Analysis Date = 02/25/13 
 Pct Recovery = 57%  Analysis Date = 02/25/13 
 Pct Recovery = 57%  Analysis Date = 02/23/13 
 Pct Recovery = 57%  Analysis Date = 02/23/13 
 Pct Recovery = 57%  Analysis Date = 02/21/13 
 Pct Recovery = 58%  Analysis Date = 02/21/13 
 Pct Recovery = 58%  Analysis Date = 02/18/13 
 Pct Recovery = 59%  Analysis Date = 02/18/13 
 Pct Recovery = 59%  Analysis Date = 02/16/13 
 Pct Recovery = 59%  Analysis Date = 02/16/13 
 Pct Recovery = 59%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/12/13 
 Pct Recovery = 61%  Analysis Date = 02/12/13 
 Pct Recovery = 61%  Analysis Date = 02/09/13 
 Pct Recovery = 61%  Analysis Date = 02/09/13 
 Pct Recovery = 61%  Analysis Date = 02/07/13 
 Pct Recovery = 62%  Analysis Date = 02/07/13 
 Pct Recovery = 62%  Analysis Date = 02/05/13 
 Pct Recovery = 62%  Analysis Date = 02/05/13 
 Pct Recovery = 62%  Analysis Date = 02/02/13 
 Pct Recovery = 63%  Analysis Date = 02/02/13 
 Pct Recovery = 63%  Analysis Date = 01/31/13 
 Pct Recovery = 64%  Analysis Date = 01/31/13 
 Pct Recovery = 64%  Analysis Date = 01/29/13 
 Pct Recovery = 64%  Analysis Date = 01/29/13 
 Pct Recovery = 64%  Analysis Date = 01/26/13 
 Pct Recovery = 65%  Analysis Date = 01/26/13 
 Pct Recovery = 65%  Analysis Date = 01/24/13 
 Pct Recovery = 66%  Analysis Date = 01/24/13 
 Pct Recovery = 66%  Analysis Date = 01/22/13 
 Pct Recovery = 66%  Analysis Date = 01/22/13 
 Pct Recovery = 66%  Analysis Date = 01/19/13 
 Pct Recovery = 67%  Analysis Date = 01/19/13 
 Pct Recovery = 67%  Analysis Date = 01/17/13 
 Pct Recovery = 67%  Analysis Date = 01/17/13 
 Pct Recovery = 67%  Analysis Date = 01/15/13 
 Pct Recovery = 68%  Analysis Date = 01/15/13 
 Pct Recovery = 68%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 70%  Analysis Date = 01/08/13 
 Pct Recovery = 70%  Analysis Date = 01/06/13 
 Pct Recovery = 71%  Analysis Date = 01/06/13 
 Pct Recovery = 71%  Analysis Date = 01/03/13 
 Pct Recovery = 71%  Analysis Date = 01/03/13 
 Pct Recovery = 71%  Analysis Date = 01/01/13 
 Pct Recovery = 72%  Analysis Date = 01/01/13 
 Pct Recovery = 72%  Analysis Date = 12/30/12 
 Pct Recovery = 72%  Analysis Date = 12/30/12 
 Pct Recovery = 72%  Analysis Date = 12/27/12 
 Pct Recovery = 73%  Analysis Date = 12/27/12 
 Pct Recovery = 73%  Analysis Date = 12/25/12 
 Pct Recovery = 74%  Analysis Date = 12/25/12 
 Pct Recovery = 74%  Analysis Date = 12/23/12 
 Pct Recovery = 74%  Analysis Date = 12/23/12 
 Pct Recovery = 74%  Analysis Date = 12/20/12 
 Pct Recovery = 75%  Analysis Date = 12/20/12 
 Pct Recovery = 75%  Analysis Date = 12/18/12 
 Pct Recovery = 76%  Analysis Date = 12/18/12 
 Pct Recovery = 76%  Analysis Date = 12/16/12 
 Pct Recovery = 76%  Analysis Date = 12/16/12 
 Pct Recovery = 76%  Analysis Date = 12/14/12 
 Pct Recovery = 77%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEXTROMETHORPHAN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 55% 14% 54% 13%
Total 14 55% 14% 54% 13%

Sample Statistics
DEXTROMETHORPHAN

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
DIAZEPAM (VALIUM)
METHOD: LC9017 , TESTIDCODE: 67499LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 71%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 78%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 26%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 58%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 59%  Analysis Date = 03/20/14 
 Pct Recovery = 26%  Analysis Date = 03/18/14 
 Pct Recovery = 30%  Analysis Date = 03/18/14 
 Pct Recovery = 30%  Analysis Date = 03/16/14 
 Pct Recovery = 33%  Analysis Date = 03/16/14 
 Pct Recovery = 33%  Analysis Date = 03/14/14 
 Pct Recovery = 36%  Analysis Date = 03/14/14 
 Pct Recovery = 36%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/10/14 
 Pct Recovery = 43%  Analysis Date = 03/10/14 
 Pct Recovery = 43%  Analysis Date = 03/08/14 
 Pct Recovery = 46%  Analysis Date = 03/08/14 
 Pct Recovery = 46%  Analysis Date = 03/06/14 
 Pct Recovery = 49%  Analysis Date = 03/06/14 
 Pct Recovery = 49%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/02/14 
 Pct Recovery = 56%  Analysis Date = 03/02/14 
 Pct Recovery = 56%  Analysis Date = 02/27/14 
 Pct Recovery = 59%  Analysis Date = 02/27/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 63%  Analysis Date = 02/25/14 
 Pct Recovery = 63%  Analysis Date = 02/23/14 
 Pct Recovery = 66%  Analysis Date = 02/23/14 
 Pct Recovery = 66%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/21/14 
 Pct Recovery = 69%  Analysis Date = 02/19/14 
 Pct Recovery = 72%  Analysis Date = 02/19/14 
 Pct Recovery = 72%  Analysis Date = 02/17/14 
 Pct Recovery = 73%  Analysis Date = 02/17/14 
 Pct Recovery = 73%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 71%  Analysis Date = 02/13/14 
 Pct Recovery = 71%  Analysis Date = 02/11/14 
 Pct Recovery = 70%  Analysis Date = 02/11/14 
 Pct Recovery = 70%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/09/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/04/14 
 Pct Recovery = 67%  Analysis Date = 02/04/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 66%  Analysis Date = 02/02/14 
 Pct Recovery = 66%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/27/14 
 Pct Recovery = 63%  Analysis Date = 01/27/14 
 Pct Recovery = 63%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/23/14 
 Pct Recovery = 61%  Analysis Date = 01/23/14 
 Pct Recovery = 61%  Analysis Date = 01/21/14 
 Pct Recovery = 60%  Analysis Date = 01/21/14 
 Pct Recovery = 60%  Analysis Date = 01/18/14 
 Pct Recovery = 59%  Analysis Date = 01/18/14 
 Pct Recovery = 59%  Analysis Date = 01/16/14 
 Pct Recovery = 58%  Analysis Date = 01/16/14 
 Pct Recovery = 58%  Analysis Date = 01/14/14 
 Pct Recovery = 58%  Analysis Date = 01/14/14 
 Pct Recovery = 58%  Analysis Date = 01/12/14 
 Pct Recovery = 58%  Analysis Date = 01/12/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/06/14 
 Pct Recovery = 58%  Analysis Date = 01/06/14 
 Pct Recovery = 58%  Analysis Date = 01/04/14 
 Pct Recovery = 58%  Analysis Date = 01/04/14 
 Pct Recovery = 58%  Analysis Date = 01/02/14 
 Pct Recovery = 58%  Analysis Date = 01/02/14 
 Pct Recovery = 58%  Analysis Date = 12/31/13 
 Pct Recovery = 58%  Analysis Date = 12/31/13 
 Pct Recovery = 58%  Analysis Date = 12/28/13 
 Pct Recovery = 58%  Analysis Date = 12/28/13 
 Pct Recovery = 58%  Analysis Date = 12/26/13 
 Pct Recovery = 58%  Analysis Date = 12/26/13 
 Pct Recovery = 58%  Analysis Date = 12/24/13 
 Pct Recovery = 58%  Analysis Date = 12/24/13 
 Pct Recovery = 58%  Analysis Date = 12/22/13 
 Pct Recovery = 58%  Analysis Date = 12/22/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/18/13 
 Pct Recovery = 58%  Analysis Date = 12/18/13 
 Pct Recovery = 58%  Analysis Date = 12/16/13 
 Pct Recovery = 58%  Analysis Date = 12/16/13 
 Pct Recovery = 58%  Analysis Date = 12/14/13 
 Pct Recovery = 58%  Analysis Date = 12/14/13 
 Pct Recovery = 58%  Analysis Date = 12/12/13 
 Pct Recovery = 58%  Analysis Date = 12/12/13 
 Pct Recovery = 58%  Analysis Date = 12/09/13 
 Pct Recovery = 58%  Analysis Date = 12/09/13 
 Pct Recovery = 58%  Analysis Date = 12/07/13 
 Pct Recovery = 59%  Analysis Date = 12/07/13 
 Pct Recovery = 59%  Analysis Date = 12/05/13 
 Pct Recovery = 59%  Analysis Date = 12/05/13 
 Pct Recovery = 59%  Analysis Date = 12/03/13 
 Pct Recovery = 59%  Analysis Date = 12/03/13 
 Pct Recovery = 59%  Analysis Date = 12/01/13 
 Pct Recovery = 59%  Analysis Date = 12/01/13 
 Pct Recovery = 59%  Analysis Date = 11/29/13 
 Pct Recovery = 59%  Analysis Date = 11/29/13 
 Pct Recovery = 59%  Analysis Date = 11/27/13 
 Pct Recovery = 59%  Analysis Date = 11/27/13 
 Pct Recovery = 59%  Analysis Date = 11/25/13 
 Pct Recovery = 59%  Analysis Date = 11/25/13 
 Pct Recovery = 59%  Analysis Date = 11/23/13 
 Pct Recovery = 59%  Analysis Date = 11/23/13 
 Pct Recovery = 59%  Analysis Date = 11/21/13 
 Pct Recovery = 59%  Analysis Date = 11/21/13 
 Pct Recovery = 59%  Analysis Date = 11/18/13 
 Pct Recovery = 59%  Analysis Date = 11/18/13 
 Pct Recovery = 59%  Analysis Date = 11/16/13 
 Pct Recovery = 59%  Analysis Date = 11/16/13 
 Pct Recovery = 59%  Analysis Date = 11/14/13 
 Pct Recovery = 59%  Analysis Date = 11/14/13 
 Pct Recovery = 59%  Analysis Date = 11/12/13 
 Pct Recovery = 59%  Analysis Date = 11/12/13 
 Pct Recovery = 59%  Analysis Date = 11/10/13 
 Pct Recovery = 59%  Analysis Date = 11/10/13 
 Pct Recovery = 59%  Analysis Date = 11/08/13 
 Pct Recovery = 60%  Analysis Date = 11/08/13 
 Pct Recovery = 60%  Analysis Date = 11/06/13 
 Pct Recovery = 60%  Analysis Date = 11/06/13 
 Pct Recovery = 60%  Analysis Date = 11/04/13 
 Pct Recovery = 60%  Analysis Date = 11/04/13 
 Pct Recovery = 60%  Analysis Date = 11/02/13 
 Pct Recovery = 60%  Analysis Date = 11/02/13 
 Pct Recovery = 60%  Analysis Date = 10/30/13 
 Pct Recovery = 60%  Analysis Date = 10/30/13 
 Pct Recovery = 60%  Analysis Date = 10/28/13 
 Pct Recovery = 60%  Analysis Date = 10/28/13 
 Pct Recovery = 60%  Analysis Date = 10/26/13 
 Pct Recovery = 60%  Analysis Date = 10/26/13 
 Pct Recovery = 60%  Analysis Date = 10/24/13 
 Pct Recovery = 60%  Analysis Date = 10/24/13 
 Pct Recovery = 60%  Analysis Date = 10/22/13 
 Pct Recovery = 61%  Analysis Date = 10/22/13 
 Pct Recovery = 61%  Analysis Date = 10/20/13 
 Pct Recovery = 61%  Analysis Date = 10/20/13 
 Pct Recovery = 61%  Analysis Date = 10/18/13 
 Pct Recovery = 61%  Analysis Date = 10/18/13 
 Pct Recovery = 61%  Analysis Date = 10/16/13 
 Pct Recovery = 61%  Analysis Date = 10/16/13 
 Pct Recovery = 61%  Analysis Date = 10/14/13 
 Pct Recovery = 61%  Analysis Date = 10/14/13 
 Pct Recovery = 61%  Analysis Date = 10/12/13 
 Pct Recovery = 61%  Analysis Date = 10/12/13 
 Pct Recovery = 61%  Analysis Date = 10/09/13 
 Pct Recovery = 61%  Analysis Date = 10/09/13 
 Pct Recovery = 61%  Analysis Date = 10/07/13 
 Pct Recovery = 62%  Analysis Date = 10/07/13 
 Pct Recovery = 62%  Analysis Date = 10/05/13 
 Pct Recovery = 62%  Analysis Date = 10/05/13 
 Pct Recovery = 62%  Analysis Date = 10/03/13 
 Pct Recovery = 62%  Analysis Date = 10/03/13 
 Pct Recovery = 62%  Analysis Date = 10/01/13 
 Pct Recovery = 62%  Analysis Date = 10/01/13 
 Pct Recovery = 62%  Analysis Date = 09/29/13 
 Pct Recovery = 62%  Analysis Date = 09/29/13 
 Pct Recovery = 62%  Analysis Date = 09/27/13 
 Pct Recovery = 62%  Analysis Date = 09/27/13 
 Pct Recovery = 62%  Analysis Date = 09/25/13 
 Pct Recovery = 62%  Analysis Date = 09/25/13 
 Pct Recovery = 62%  Analysis Date = 09/23/13 
 Pct Recovery = 62%  Analysis Date = 09/23/13 
 Pct Recovery = 62%  Analysis Date = 09/20/13 
 Pct Recovery = 63%  Analysis Date = 09/20/13 
 Pct Recovery = 63%  Analysis Date = 09/18/13 
 Pct Recovery = 63%  Analysis Date = 09/18/13 
 Pct Recovery = 63%  Analysis Date = 09/16/13 
 Pct Recovery = 63%  Analysis Date = 09/16/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/08/13 
 Pct Recovery = 63%  Analysis Date = 09/08/13 
 Pct Recovery = 63%  Analysis Date = 09/06/13 
 Pct Recovery = 63%  Analysis Date = 09/06/13 
 Pct Recovery = 63%  Analysis Date = 09/04/13 
 Pct Recovery = 64%  Analysis Date = 09/04/13 
 Pct Recovery = 64%  Analysis Date = 09/02/13 
 Pct Recovery = 64%  Analysis Date = 09/02/13 
 Pct Recovery = 64%  Analysis Date = 08/30/13 
 Pct Recovery = 64%  Analysis Date = 08/30/13 
 Pct Recovery = 64%  Analysis Date = 08/28/13 
 Pct Recovery = 64%  Analysis Date = 08/28/13 
 Pct Recovery = 64%  Analysis Date = 08/26/13 
 Pct Recovery = 64%  Analysis Date = 08/26/13 
 Pct Recovery = 64%  Analysis Date = 08/24/13 
 Pct Recovery = 64%  Analysis Date = 08/24/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/16/13 
 Pct Recovery = 65%  Analysis Date = 08/16/13 
 Pct Recovery = 65%  Analysis Date = 08/14/13 
 Pct Recovery = 65%  Analysis Date = 08/14/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/09/13 
 Pct Recovery = 65%  Analysis Date = 08/09/13 
 Pct Recovery = 65%  Analysis Date = 08/07/13 
 Pct Recovery = 65%  Analysis Date = 08/07/13 
 Pct Recovery = 65%  Analysis Date = 08/05/13 
 Pct Recovery = 65%  Analysis Date = 08/05/13 
 Pct Recovery = 65%  Analysis Date = 08/03/13 
 Pct Recovery = 66%  Analysis Date = 08/03/13 
 Pct Recovery = 66%  Analysis Date = 08/01/13 
 Pct Recovery = 66%  Analysis Date = 08/01/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/28/13 
 Pct Recovery = 66%  Analysis Date = 07/28/13 
 Pct Recovery = 66%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/24/13 
 Pct Recovery = 66%  Analysis Date = 07/24/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/19/13 
 Pct Recovery = 66%  Analysis Date = 07/19/13 
 Pct Recovery = 66%  Analysis Date = 07/17/13 
 Pct Recovery = 67%  Analysis Date = 07/17/13 
 Pct Recovery = 67%  Analysis Date = 07/15/13 
 Pct Recovery = 67%  Analysis Date = 07/15/13 
 Pct Recovery = 67%  Analysis Date = 07/13/13 
 Pct Recovery = 67%  Analysis Date = 07/13/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/05/13 
 Pct Recovery = 67%  Analysis Date = 07/05/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/24/13 
 Pct Recovery = 68%  Analysis Date = 06/24/13 
 Pct Recovery = 68%  Analysis Date = 06/22/13 
 Pct Recovery = 68%  Analysis Date = 06/22/13 
 Pct Recovery = 68%  Analysis Date = 06/20/13 
 Pct Recovery = 68%  Analysis Date = 06/20/13 
 Pct Recovery = 68%  Analysis Date = 06/18/13 
 Pct Recovery = 68%  Analysis Date = 06/18/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/11/13 
 Pct Recovery = 69%  Analysis Date = 06/11/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/07/13 
 Pct Recovery = 69%  Analysis Date = 06/07/13 
 Pct Recovery = 69%  Analysis Date = 06/05/13 
 Pct Recovery = 69%  Analysis Date = 06/05/13 
 Pct Recovery = 69%  Analysis Date = 06/03/13 
 Pct Recovery = 69%  Analysis Date = 06/03/13 
 Pct Recovery = 69%  Analysis Date = 06/01/13 
 Pct Recovery = 69%  Analysis Date = 06/01/13 
 Pct Recovery = 69%  Analysis Date = 05/30/13 
 Pct Recovery = 70%  Analysis Date = 05/30/13 
 Pct Recovery = 70%  Analysis Date = 05/28/13 
 Pct Recovery = 70%  Analysis Date = 05/28/13 
 Pct Recovery = 70%  Analysis Date = 05/26/13 
 Pct Recovery = 70%  Analysis Date = 05/26/13 
 Pct Recovery = 70%  Analysis Date = 05/23/13 
 Pct Recovery = 70%  Analysis Date = 05/23/13 
 Pct Recovery = 70%  Analysis Date = 05/21/13 
 Pct Recovery = 70%  Analysis Date = 05/21/13 
 Pct Recovery = 70%  Analysis Date = 05/19/13 
 Pct Recovery = 70%  Analysis Date = 05/19/13 
 Pct Recovery = 70%  Analysis Date = 05/17/13 
 Pct Recovery = 70%  Analysis Date = 05/17/13 
 Pct Recovery = 70%  Analysis Date = 05/15/13 
 Pct Recovery = 70%  Analysis Date = 05/15/13 
 Pct Recovery = 70%  Analysis Date = 05/13/13 
 Pct Recovery = 71%  Analysis Date = 05/13/13 
 Pct Recovery = 71%  Analysis Date = 05/11/13 
 Pct Recovery = 71%  Analysis Date = 05/11/13 
 Pct Recovery = 71%  Analysis Date = 05/09/13 
 Pct Recovery = 71%  Analysis Date = 05/09/13 
 Pct Recovery = 71%  Analysis Date = 05/07/13 
 Pct Recovery = 71%  Analysis Date = 05/07/13 
 Pct Recovery = 71%  Analysis Date = 05/05/13 
 Pct Recovery = 71%  Analysis Date = 05/05/13 
 Pct Recovery = 71%  Analysis Date = 05/02/13 
 Pct Recovery = 71%  Analysis Date = 05/02/13 
 Pct Recovery = 71%  Analysis Date = 04/30/13 
 Pct Recovery = 71%  Analysis Date = 04/30/13 
 Pct Recovery = 71%  Analysis Date = 04/28/13 
 Pct Recovery = 71%  Analysis Date = 04/28/13 
 Pct Recovery = 71%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/20/13 
 Pct Recovery = 72%  Analysis Date = 04/20/13 
 Pct Recovery = 72%  Analysis Date = 04/18/13 
 Pct Recovery = 72%  Analysis Date = 04/18/13 
 Pct Recovery = 72%  Analysis Date = 04/16/13 
 Pct Recovery = 72%  Analysis Date = 04/16/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/05/13 
 Pct Recovery = 73%  Analysis Date = 04/05/13 
 Pct Recovery = 73%  Analysis Date = 04/03/13 
 Pct Recovery = 73%  Analysis Date = 04/03/13 
 Pct Recovery = 73%  Analysis Date = 04/01/13 
 Pct Recovery = 73%  Analysis Date = 04/01/13 
 Pct Recovery = 73%  Analysis Date = 03/30/13 
 Pct Recovery = 74%  Analysis Date = 03/30/13 
 Pct Recovery = 74%  Analysis Date = 03/28/13 
 Pct Recovery = 74%  Analysis Date = 03/28/13 
 Pct Recovery = 74%  Analysis Date = 03/26/13 
 Pct Recovery = 74%  Analysis Date = 03/26/13 
 Pct Recovery = 74%  Analysis Date = 03/23/13 
 Pct Recovery = 74%  Analysis Date = 03/23/13 
 Pct Recovery = 74%  Analysis Date = 03/21/13 
 Pct Recovery = 74%  Analysis Date = 03/21/13 
 Pct Recovery = 74%  Analysis Date = 03/19/13 
 Pct Recovery = 74%  Analysis Date = 03/19/13 
 Pct Recovery = 74%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/11/13 
 Pct Recovery = 75%  Analysis Date = 03/11/13 
 Pct Recovery = 75%  Analysis Date = 03/09/13 
 Pct Recovery = 75%  Analysis Date = 03/09/13 
 Pct Recovery = 75%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/07/13 
 Pct Recovery = 75%  Analysis Date = 03/04/13 
 Pct Recovery = 75%  Analysis Date = 03/04/13 
 Pct Recovery = 75%  Analysis Date = 03/02/13 
 Pct Recovery = 76%  Analysis Date = 03/02/13 
 Pct Recovery = 76%  Analysis Date = 02/28/13 
 Pct Recovery = 76%  Analysis Date = 02/28/13 
 Pct Recovery = 76%  Analysis Date = 02/26/13 
 Pct Recovery = 76%  Analysis Date = 02/26/13 
 Pct Recovery = 76%  Analysis Date = 02/24/13 
 Pct Recovery = 76%  Analysis Date = 02/24/13 
 Pct Recovery = 76%  Analysis Date = 02/22/13 
 Pct Recovery = 76%  Analysis Date = 02/22/13 
 Pct Recovery = 76%  Analysis Date = 02/20/13 
 Pct Recovery = 76%  Analysis Date = 02/20/13 
 Pct Recovery = 76%  Analysis Date = 02/18/13 
 Pct Recovery = 77%  Analysis Date = 02/18/13 
 Pct Recovery = 77%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/16/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/11/13 
 Pct Recovery = 77%  Analysis Date = 02/11/13 
 Pct Recovery = 77%  Analysis Date = 02/09/13 
 Pct Recovery = 77%  Analysis Date = 02/09/13 
 Pct Recovery = 77%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/03/13 
 Pct Recovery = 78%  Analysis Date = 02/03/13 
 Pct Recovery = 78%  Analysis Date = 02/01/13 
 Pct Recovery = 78%  Analysis Date = 02/01/13 
 Pct Recovery = 78%  Analysis Date = 01/30/13 
 Pct Recovery = 78%  Analysis Date = 01/30/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 Pct Recovery = 78%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZEPAM (VALIUM)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 61% 19% 65% 12%
Total 6 61% 19% 65% 12%

Sample Statistics
DIAZEPAM (VALIUM)

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
DILTIAZEM
METHOD: LC9017 , TESTIDCODE: 67519LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 42%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 47%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 30%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 19%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 33%  Analysis Date = 03/20/14 
 Pct Recovery = 47%  Analysis Date = 03/18/14 
 Pct Recovery = 46%  Analysis Date = 03/18/14 
 Pct Recovery = 46%  Analysis Date = 03/16/14 
 Pct Recovery = 45%  Analysis Date = 03/16/14 
 Pct Recovery = 45%  Analysis Date = 03/14/14 
 Pct Recovery = 43%  Analysis Date = 03/14/14 
 Pct Recovery = 43%  Analysis Date = 03/12/14 
 Pct Recovery = 42%  Analysis Date = 03/12/14 
 Pct Recovery = 42%  Analysis Date = 03/10/14 
 Pct Recovery = 41%  Analysis Date = 03/10/14 
 Pct Recovery = 41%  Analysis Date = 03/08/14 
 Pct Recovery = 40%  Analysis Date = 03/08/14 
 Pct Recovery = 40%  Analysis Date = 03/06/14 
 Pct Recovery = 39%  Analysis Date = 03/06/14 
 Pct Recovery = 39%  Analysis Date = 03/04/14 
 Pct Recovery = 37%  Analysis Date = 03/04/14 
 Pct Recovery = 37%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 35%  Analysis Date = 02/27/14 
 Pct Recovery = 35%  Analysis Date = 02/25/14 
 Pct Recovery = 34%  Analysis Date = 02/25/14 
 Pct Recovery = 34%  Analysis Date = 02/23/14 
 Pct Recovery = 33%  Analysis Date = 02/23/14 
 Pct Recovery = 33%  Analysis Date = 02/21/14 
 Pct Recovery = 32%  Analysis Date = 02/21/14 
 Pct Recovery = 32%  Analysis Date = 02/19/14 
 Pct Recovery = 30%  Analysis Date = 02/19/14 
 Pct Recovery = 30%  Analysis Date = 02/17/14 
 Pct Recovery = 30%  Analysis Date = 02/17/14 
 Pct Recovery = 30%  Analysis Date = 02/15/14 
 Pct Recovery = 29%  Analysis Date = 02/15/14 
 Pct Recovery = 29%  Analysis Date = 02/13/14 
 Pct Recovery = 28%  Analysis Date = 02/13/14 
 Pct Recovery = 28%  Analysis Date = 02/11/14 
 Pct Recovery = 28%  Analysis Date = 02/11/14 
 Pct Recovery = 28%  Analysis Date = 02/09/14 
 Pct Recovery = 27%  Analysis Date = 02/09/14 
 Pct Recovery = 27%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/04/14 
 Pct Recovery = 26%  Analysis Date = 02/04/14 
 Pct Recovery = 26%  Analysis Date = 02/02/14 
 Pct Recovery = 25%  Analysis Date = 02/02/14 
 Pct Recovery = 25%  Analysis Date = 01/31/14 
 Pct Recovery = 24%  Analysis Date = 01/31/14 
 Pct Recovery = 24%  Analysis Date = 01/29/14 
 Pct Recovery = 24%  Analysis Date = 01/29/14 
 Pct Recovery = 24%  Analysis Date = 01/27/14 
 Pct Recovery = 23%  Analysis Date = 01/27/14 
 Pct Recovery = 23%  Analysis Date = 01/25/14 
 Pct Recovery = 22%  Analysis Date = 01/25/14 
 Pct Recovery = 22%  Analysis Date = 01/23/14 
 Pct Recovery = 22%  Analysis Date = 01/23/14 
 Pct Recovery = 22%  Analysis Date = 01/21/14 
 Pct Recovery = 21%  Analysis Date = 01/21/14 
 Pct Recovery = 21%  Analysis Date = 01/18/14 
 Pct Recovery = 20%  Analysis Date = 01/18/14 
 Pct Recovery = 20%  Analysis Date = 01/16/14 
 Pct Recovery = 20%  Analysis Date = 01/16/14 
 Pct Recovery = 20%  Analysis Date = 01/14/14 
 Pct Recovery = 20%  Analysis Date = 01/14/14 
 Pct Recovery = 20%  Analysis Date = 01/12/14 
 Pct Recovery = 20%  Analysis Date = 01/12/14 
 Pct Recovery = 20%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/06/14 
 Pct Recovery = 22%  Analysis Date = 01/06/14 
 Pct Recovery = 22%  Analysis Date = 01/04/14 
 Pct Recovery = 22%  Analysis Date = 01/04/14 
 Pct Recovery = 22%  Analysis Date = 01/02/14 
 Pct Recovery = 23%  Analysis Date = 01/02/14 
 Pct Recovery = 23%  Analysis Date = 12/31/13 
 Pct Recovery = 23%  Analysis Date = 12/31/13 
 Pct Recovery = 23%  Analysis Date = 12/28/13 
 Pct Recovery = 24%  Analysis Date = 12/28/13 
 Pct Recovery = 24%  Analysis Date = 12/26/13 
 Pct Recovery = 24%  Analysis Date = 12/26/13 
 Pct Recovery = 24%  Analysis Date = 12/24/13 
 Pct Recovery = 25%  Analysis Date = 12/24/13 
 Pct Recovery = 25%  Analysis Date = 12/22/13 
 Pct Recovery = 25%  Analysis Date = 12/22/13 
 Pct Recovery = 25%  Analysis Date = 12/20/13 
 Pct Recovery = 26%  Analysis Date = 12/20/13 
 Pct Recovery = 26%  Analysis Date = 12/18/13 
 Pct Recovery = 26%  Analysis Date = 12/18/13 
 Pct Recovery = 26%  Analysis Date = 12/16/13 
 Pct Recovery = 27%  Analysis Date = 12/16/13 
 Pct Recovery = 27%  Analysis Date = 12/14/13 
 Pct Recovery = 27%  Analysis Date = 12/14/13 
 Pct Recovery = 27%  Analysis Date = 12/12/13 
 Pct Recovery = 28%  Analysis Date = 12/12/13 
 Pct Recovery = 28%  Analysis Date = 12/09/13 
 Pct Recovery = 28%  Analysis Date = 12/09/13 
 Pct Recovery = 28%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 12/01/13 
 Pct Recovery = 30%  Analysis Date = 12/01/13 
 Pct Recovery = 30%  Analysis Date = 11/29/13 
 Pct Recovery = 30%  Analysis Date = 11/29/13 
 Pct Recovery = 30%  Analysis Date = 11/27/13 
 Pct Recovery = 31%  Analysis Date = 11/27/13 
 Pct Recovery = 31%  Analysis Date = 11/25/13 
 Pct Recovery = 31%  Analysis Date = 11/25/13 
 Pct Recovery = 31%  Analysis Date = 11/23/13 
 Pct Recovery = 32%  Analysis Date = 11/23/13 
 Pct Recovery = 32%  Analysis Date = 11/21/13 
 Pct Recovery = 32%  Analysis Date = 11/21/13 
 Pct Recovery = 32%  Analysis Date = 11/18/13 
 Pct Recovery = 33%  Analysis Date = 11/18/13 
 Pct Recovery = 33%  Analysis Date = 11/16/13 
 Pct Recovery = 33%  Analysis Date = 11/16/13 
 Pct Recovery = 33%  Analysis Date = 11/14/13 
 Pct Recovery = 33%  Analysis Date = 11/14/13 
 Pct Recovery = 33%  Analysis Date = 11/12/13 
 Pct Recovery = 33%  Analysis Date = 11/12/13 
 Pct Recovery = 33%  Analysis Date = 11/10/13 
 Pct Recovery = 33%  Analysis Date = 11/10/13 
 Pct Recovery = 33%  Analysis Date = 11/08/13 
 Pct Recovery = 33%  Analysis Date = 11/08/13 
 Pct Recovery = 33%  Analysis Date = 11/06/13 
 Pct Recovery = 33%  Analysis Date = 11/06/13 
 Pct Recovery = 33%  Analysis Date = 11/04/13 
 Pct Recovery = 33%  Analysis Date = 11/04/13 
 Pct Recovery = 33%  Analysis Date = 11/02/13 
 Pct Recovery = 33%  Analysis Date = 11/02/13 
 Pct Recovery = 33%  Analysis Date = 10/30/13 
 Pct Recovery = 34%  Analysis Date = 10/30/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/28/13 
 Pct Recovery = 34%  Analysis Date = 10/26/13 
 Pct Recovery = 34%  Analysis Date = 10/26/13 
 Pct Recovery = 34%  Analysis Date = 10/24/13 
 Pct Recovery = 34%  Analysis Date = 10/24/13 
 Pct Recovery = 34%  Analysis Date = 10/22/13 
 Pct Recovery = 34%  Analysis Date = 10/22/13 
 Pct Recovery = 34%  Analysis Date = 10/20/13 
 Pct Recovery = 34%  Analysis Date = 10/20/13 
 Pct Recovery = 34%  Analysis Date = 10/18/13 
 Pct Recovery = 34%  Analysis Date = 10/18/13 
 Pct Recovery = 34%  Analysis Date = 10/16/13 
 Pct Recovery = 34%  Analysis Date = 10/16/13 
 Pct Recovery = 34%  Analysis Date = 10/14/13 
 Pct Recovery = 34%  Analysis Date = 10/14/13 
 Pct Recovery = 34%  Analysis Date = 10/12/13 
 Pct Recovery = 34%  Analysis Date = 10/12/13 
 Pct Recovery = 34%  Analysis Date = 10/09/13 
 Pct Recovery = 34%  Analysis Date = 10/09/13 
 Pct Recovery = 34%  Analysis Date = 10/07/13 
 Pct Recovery = 35%  Analysis Date = 10/07/13 
 Pct Recovery = 35%  Analysis Date = 10/05/13 
 Pct Recovery = 35%  Analysis Date = 10/05/13 
 Pct Recovery = 35%  Analysis Date = 10/03/13 
 Pct Recovery = 35%  Analysis Date = 10/03/13 
 Pct Recovery = 35%  Analysis Date = 10/01/13 
 Pct Recovery = 35%  Analysis Date = 10/01/13 
 Pct Recovery = 35%  Analysis Date = 09/29/13 
 Pct Recovery = 35%  Analysis Date = 09/29/13 
 Pct Recovery = 35%  Analysis Date = 09/27/13 
 Pct Recovery = 35%  Analysis Date = 09/27/13 
 Pct Recovery = 35%  Analysis Date = 09/25/13 
 Pct Recovery = 35%  Analysis Date = 09/25/13 
 Pct Recovery = 35%  Analysis Date = 09/23/13 
 Pct Recovery = 35%  Analysis Date = 09/23/13 
 Pct Recovery = 35%  Analysis Date = 09/20/13 
 Pct Recovery = 35%  Analysis Date = 09/20/13 
 Pct Recovery = 35%  Analysis Date = 09/18/13 
 Pct Recovery = 35%  Analysis Date = 09/18/13 
 Pct Recovery = 35%  Analysis Date = 09/16/13 
 Pct Recovery = 36%  Analysis Date = 09/16/13 
 Pct Recovery = 36%  Analysis Date = 09/14/13 
 Pct Recovery = 36%  Analysis Date = 09/14/13 
 Pct Recovery = 36%  Analysis Date = 09/12/13 
 Pct Recovery = 36%  Analysis Date = 09/12/13 
 Pct Recovery = 36%  Analysis Date = 09/10/13 
 Pct Recovery = 36%  Analysis Date = 09/10/13 
 Pct Recovery = 36%  Analysis Date = 09/08/13 
 Pct Recovery = 36%  Analysis Date = 09/08/13 
 Pct Recovery = 36%  Analysis Date = 09/06/13 
 Pct Recovery = 36%  Analysis Date = 09/06/13 
 Pct Recovery = 36%  Analysis Date = 09/04/13 
 Pct Recovery = 36%  Analysis Date = 09/04/13 
 Pct Recovery = 36%  Analysis Date = 09/02/13 
 Pct Recovery = 36%  Analysis Date = 09/02/13 
 Pct Recovery = 36%  Analysis Date = 08/30/13 
 Pct Recovery = 36%  Analysis Date = 08/30/13 
 Pct Recovery = 36%  Analysis Date = 08/28/13 
 Pct Recovery = 36%  Analysis Date = 08/28/13 
 Pct Recovery = 36%  Analysis Date = 08/26/13 
 Pct Recovery = 36%  Analysis Date = 08/26/13 
 Pct Recovery = 36%  Analysis Date = 08/24/13 
 Pct Recovery = 37%  Analysis Date = 08/24/13 
 Pct Recovery = 37%  Analysis Date = 08/22/13 
 Pct Recovery = 37%  Analysis Date = 08/22/13 
 Pct Recovery = 37%  Analysis Date = 08/20/13 
 Pct Recovery = 37%  Analysis Date = 08/20/13 
 Pct Recovery = 37%  Analysis Date = 08/18/13 
 Pct Recovery = 37%  Analysis Date = 08/18/13 
 Pct Recovery = 37%  Analysis Date = 08/16/13 
 Pct Recovery = 37%  Analysis Date = 08/16/13 
 Pct Recovery = 37%  Analysis Date = 08/14/13 
 Pct Recovery = 37%  Analysis Date = 08/14/13 
 Pct Recovery = 37%  Analysis Date = 08/11/13 
 Pct Recovery = 37%  Analysis Date = 08/11/13 
 Pct Recovery = 37%  Analysis Date = 08/09/13 
 Pct Recovery = 37%  Analysis Date = 08/09/13 
 Pct Recovery = 37%  Analysis Date = 08/07/13 
 Pct Recovery = 37%  Analysis Date = 08/07/13 
 Pct Recovery = 37%  Analysis Date = 08/05/13 
 Pct Recovery = 37%  Analysis Date = 08/05/13 
 Pct Recovery = 37%  Analysis Date = 08/03/13 
 Pct Recovery = 38%  Analysis Date = 08/03/13 
 Pct Recovery = 38%  Analysis Date = 08/01/13 
 Pct Recovery = 38%  Analysis Date = 08/01/13 
 Pct Recovery = 38%  Analysis Date = 07/30/13 
 Pct Recovery = 38%  Analysis Date = 07/30/13 
 Pct Recovery = 38%  Analysis Date = 07/28/13 
 Pct Recovery = 38%  Analysis Date = 07/28/13 
 Pct Recovery = 38%  Analysis Date = 07/26/13 
 Pct Recovery = 38%  Analysis Date = 07/26/13 
 Pct Recovery = 38%  Analysis Date = 07/24/13 
 Pct Recovery = 38%  Analysis Date = 07/24/13 
 Pct Recovery = 38%  Analysis Date = 07/21/13 
 Pct Recovery = 38%  Analysis Date = 07/21/13 
 Pct Recovery = 38%  Analysis Date = 07/19/13 
 Pct Recovery = 38%  Analysis Date = 07/19/13 
 Pct Recovery = 38%  Analysis Date = 07/17/13 
 Pct Recovery = 38%  Analysis Date = 07/17/13 
 Pct Recovery = 38%  Analysis Date = 07/15/13 
 Pct Recovery = 38%  Analysis Date = 07/15/13 
 Pct Recovery = 38%  Analysis Date = 07/13/13 
 Pct Recovery = 38%  Analysis Date = 07/13/13 
 Pct Recovery = 38%  Analysis Date = 07/11/13 
 Pct Recovery = 39%  Analysis Date = 07/11/13 
 Pct Recovery = 39%  Analysis Date = 07/09/13 
 Pct Recovery = 39%  Analysis Date = 07/09/13 
 Pct Recovery = 39%  Analysis Date = 07/07/13 
 Pct Recovery = 39%  Analysis Date = 07/07/13 
 Pct Recovery = 39%  Analysis Date = 07/05/13 
 Pct Recovery = 39%  Analysis Date = 07/05/13 
 Pct Recovery = 39%  Analysis Date = 07/02/13 
 Pct Recovery = 39%  Analysis Date = 07/02/13 
 Pct Recovery = 39%  Analysis Date = 06/30/13 
 Pct Recovery = 39%  Analysis Date = 06/30/13 
 Pct Recovery = 39%  Analysis Date = 06/28/13 
 Pct Recovery = 39%  Analysis Date = 06/28/13 
 Pct Recovery = 39%  Analysis Date = 06/26/13 
 Pct Recovery = 39%  Analysis Date = 06/26/13 
 Pct Recovery = 39%  Analysis Date = 06/24/13 
 Pct Recovery = 39%  Analysis Date = 06/24/13 
 Pct Recovery = 39%  Analysis Date = 06/22/13 
 Pct Recovery = 39%  Analysis Date = 06/22/13 
 Pct Recovery = 39%  Analysis Date = 06/20/13 
 Pct Recovery = 39%  Analysis Date = 06/20/13 
 Pct Recovery = 39%  Analysis Date = 06/18/13 
 Pct Recovery = 40%  Analysis Date = 06/18/13 
 Pct Recovery = 40%  Analysis Date = 06/16/13 
 Pct Recovery = 40%  Analysis Date = 06/16/13 
 Pct Recovery = 40%  Analysis Date = 06/14/13 
 Pct Recovery = 40%  Analysis Date = 06/14/13 
 Pct Recovery = 40%  Analysis Date = 06/11/13 
 Pct Recovery = 40%  Analysis Date = 06/11/13 
 Pct Recovery = 40%  Analysis Date = 06/09/13 
 Pct Recovery = 40%  Analysis Date = 06/09/13 
 Pct Recovery = 40%  Analysis Date = 06/07/13 
 Pct Recovery = 40%  Analysis Date = 06/07/13 
 Pct Recovery = 40%  Analysis Date = 06/05/13 
 Pct Recovery = 40%  Analysis Date = 06/05/13 
 Pct Recovery = 40%  Analysis Date = 06/03/13 
 Pct Recovery = 40%  Analysis Date = 06/03/13 
 Pct Recovery = 40%  Analysis Date = 06/01/13 
 Pct Recovery = 40%  Analysis Date = 06/01/13 
 Pct Recovery = 40%  Analysis Date = 05/30/13 
 Pct Recovery = 40%  Analysis Date = 05/30/13 
 Pct Recovery = 40%  Analysis Date = 05/28/13 
 Pct Recovery = 41%  Analysis Date = 05/28/13 
 Pct Recovery = 41%  Analysis Date = 05/26/13 
 Pct Recovery = 41%  Analysis Date = 05/26/13 
 Pct Recovery = 41%  Analysis Date = 05/23/13 
 Pct Recovery = 41%  Analysis Date = 05/23/13 
 Pct Recovery = 41%  Analysis Date = 05/21/13 
 Pct Recovery = 41%  Analysis Date = 05/21/13 
 Pct Recovery = 41%  Analysis Date = 05/19/13 
 Pct Recovery = 41%  Analysis Date = 05/19/13 
 Pct Recovery = 41%  Analysis Date = 05/17/13 
 Pct Recovery = 41%  Analysis Date = 05/17/13 
 Pct Recovery = 41%  Analysis Date = 05/15/13 
 Pct Recovery = 41%  Analysis Date = 05/15/13 
 Pct Recovery = 41%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/13/13 
 Pct Recovery = 41%  Analysis Date = 05/11/13 
 Pct Recovery = 41%  Analysis Date = 05/11/13 
 Pct Recovery = 41%  Analysis Date = 05/09/13 
 Pct Recovery = 41%  Analysis Date = 05/09/13 
 Pct Recovery = 41%  Analysis Date = 05/07/13 
 Pct Recovery = 41%  Analysis Date = 05/07/13 
 Pct Recovery = 41%  Analysis Date = 05/05/13 
 Pct Recovery = 42%  Analysis Date = 05/05/13 
 Pct Recovery = 42%  Analysis Date = 05/02/13 
 Pct Recovery = 42%  Analysis Date = 05/02/13 
 Pct Recovery = 42%  Analysis Date = 04/30/13 
 Pct Recovery = 42%  Analysis Date = 04/30/13 
 Pct Recovery = 42%  Analysis Date = 04/28/13 
 Pct Recovery = 42%  Analysis Date = 04/28/13 
 Pct Recovery = 42%  Analysis Date = 04/26/13 
 Pct Recovery = 42%  Analysis Date = 04/26/13 
 Pct Recovery = 42%  Analysis Date = 04/24/13 
 Pct Recovery = 42%  Analysis Date = 04/24/13 
 Pct Recovery = 42%  Analysis Date = 04/22/13 
 Pct Recovery = 43%  Analysis Date = 04/22/13 
 Pct Recovery = 43%  Analysis Date = 04/20/13 
 Pct Recovery = 43%  Analysis Date = 04/20/13 
 Pct Recovery = 43%  Analysis Date = 04/18/13 
 Pct Recovery = 43%  Analysis Date = 04/18/13 
 Pct Recovery = 43%  Analysis Date = 04/16/13 
 Pct Recovery = 43%  Analysis Date = 04/16/13 
 Pct Recovery = 43%  Analysis Date = 04/13/13 
 Pct Recovery = 44%  Analysis Date = 04/13/13 
 Pct Recovery = 44%  Analysis Date = 04/11/13 
 Pct Recovery = 44%  Analysis Date = 04/11/13 
 Pct Recovery = 44%  Analysis Date = 04/09/13 
 Pct Recovery = 44%  Analysis Date = 04/09/13 
 Pct Recovery = 44%  Analysis Date = 04/07/13 
 Pct Recovery = 44%  Analysis Date = 04/07/13 
 Pct Recovery = 44%  Analysis Date = 04/05/13 
 Pct Recovery = 44%  Analysis Date = 04/05/13 
 Pct Recovery = 44%  Analysis Date = 04/03/13 
 Pct Recovery = 45%  Analysis Date = 04/03/13 
 Pct Recovery = 45%  Analysis Date = 04/01/13 
 Pct Recovery = 45%  Analysis Date = 04/01/13 
 Pct Recovery = 45%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/28/13 
 Pct Recovery = 45%  Analysis Date = 03/28/13 
 Pct Recovery = 45%  Analysis Date = 03/26/13 
 Pct Recovery = 46%  Analysis Date = 03/26/13 
 Pct Recovery = 46%  Analysis Date = 03/23/13 
 Pct Recovery = 46%  Analysis Date = 03/23/13 
 Pct Recovery = 46%  Analysis Date = 03/21/13 
 Pct Recovery = 46%  Analysis Date = 03/21/13 
 Pct Recovery = 46%  Analysis Date = 03/19/13 
 Pct Recovery = 46%  Analysis Date = 03/19/13 
 Pct Recovery = 46%  Analysis Date = 03/17/13 
 Pct Recovery = 46%  Analysis Date = 03/17/13 
 Pct Recovery = 46%  Analysis Date = 03/15/13 
 Pct Recovery = 47%  Analysis Date = 03/15/13 
 Pct Recovery = 47%  Analysis Date = 03/13/13 
 Pct Recovery = 47%  Analysis Date = 03/13/13 
 Pct Recovery = 47%  Analysis Date = 03/11/13 
 Pct Recovery = 47%  Analysis Date = 03/11/13 
 Pct Recovery = 47%  Analysis Date = 03/09/13 
 Pct Recovery = 47%  Analysis Date = 03/09/13 
 Pct Recovery = 47%  Analysis Date = 03/07/13 
 Pct Recovery = 48%  Analysis Date = 03/07/13 
 Pct Recovery = 48%  Analysis Date = 03/04/13 
 Pct Recovery = 48%  Analysis Date = 03/04/13 
 Pct Recovery = 48%  Analysis Date = 03/02/13 
 Pct Recovery = 48%  Analysis Date = 03/02/13 
 Pct Recovery = 48%  Analysis Date = 02/28/13 
 Pct Recovery = 48%  Analysis Date = 02/28/13 
 Pct Recovery = 48%  Analysis Date = 02/26/13 
 Pct Recovery = 48%  Analysis Date = 02/26/13 
 Pct Recovery = 48%  Analysis Date = 02/24/13 
 Pct Recovery = 49%  Analysis Date = 02/24/13 
 Pct Recovery = 49%  Analysis Date = 02/22/13 
 Pct Recovery = 49%  Analysis Date = 02/22/13 
 Pct Recovery = 49%  Analysis Date = 02/20/13 
 Pct Recovery = 49%  Analysis Date = 02/20/13 
 Pct Recovery = 49%  Analysis Date = 02/18/13 
 Pct Recovery = 49%  Analysis Date = 02/18/13 
 Pct Recovery = 49%  Analysis Date = 02/16/13 
 Pct Recovery = 50%  Analysis Date = 02/16/13 
 Pct Recovery = 50%  Analysis Date = 02/14/13 
 Pct Recovery = 50%  Analysis Date = 02/14/13 
 Pct Recovery = 50%  Analysis Date = 02/11/13 
 Pct Recovery = 50%  Analysis Date = 02/11/13 
 Pct Recovery = 50%  Analysis Date = 02/09/13 
 Pct Recovery = 50%  Analysis Date = 02/09/13 
 Pct Recovery = 50%  Analysis Date = 02/07/13 
 Pct Recovery = 50%  Analysis Date = 02/07/13 
 Pct Recovery = 50%  Analysis Date = 02/05/13 
 Pct Recovery = 51%  Analysis Date = 02/05/13 
 Pct Recovery = 51%  Analysis Date = 02/03/13 
 Pct Recovery = 51%  Analysis Date = 02/03/13 
 Pct Recovery = 51%  Analysis Date = 02/01/13 
 Pct Recovery = 51%  Analysis Date = 02/01/13 
 Pct Recovery = 51%  Analysis Date = 01/30/13 
 Pct Recovery = 51%  Analysis Date = 01/30/13 
 Pct Recovery = 51%  Analysis Date = 01/28/13 
 Pct Recovery = 52%  Analysis Date = 01/28/13 
 Pct Recovery = 52%  Analysis Date = 01/26/13 
 Pct Recovery = 52%  Analysis Date = 01/26/13 
 Pct Recovery = 52%  Analysis Date = 01/24/13 
 Pct Recovery = 52%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DILTIAZEM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 37% 12% 37% 13%
Total 6 37% 12% 37% 13%

Sample Statistics
DILTIAZEM

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 1 17% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
DIPHENHYDRAMINE
METHOD: LC9017 , TESTIDCODE: 67447LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 61%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 86%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 80%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 75%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 90%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 80%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 70%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 64%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 67%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 55%  Analysis Date = 03/21/14 
 Pct Recovery = 79%  Analysis Date = 03/18/14 
 Pct Recovery = 78%  Analysis Date = 03/18/14 
 Pct Recovery = 78%  Analysis Date = 03/16/14 
 Pct Recovery = 78%  Analysis Date = 03/16/14 
 Pct Recovery = 78%  Analysis Date = 03/14/14 
 Pct Recovery = 77%  Analysis Date = 03/14/14 
 Pct Recovery = 77%  Analysis Date = 03/11/14 
 Pct Recovery = 77%  Analysis Date = 03/11/14 
 Pct Recovery = 77%  Analysis Date = 03/09/14 
 Pct Recovery = 77%  Analysis Date = 03/09/14 
 Pct Recovery = 77%  Analysis Date = 03/07/14 
 Pct Recovery = 76%  Analysis Date = 03/07/14 
 Pct Recovery = 76%  Analysis Date = 03/04/14 
 Pct Recovery = 76%  Analysis Date = 03/04/14 
 Pct Recovery = 76%  Analysis Date = 03/02/14 
 Pct Recovery = 76%  Analysis Date = 03/02/14 
 Pct Recovery = 76%  Analysis Date = 02/28/14 
 Pct Recovery = 75%  Analysis Date = 02/28/14 
 Pct Recovery = 75%  Analysis Date = 02/25/14 
 Pct Recovery = 75%  Analysis Date = 02/25/14 
 Pct Recovery = 75%  Analysis Date = 02/23/14 
 Pct Recovery = 75%  Analysis Date = 02/23/14 
 Pct Recovery = 75%  Analysis Date = 02/21/14 
 Pct Recovery = 74%  Analysis Date = 02/21/14 
 Pct Recovery = 74%  Analysis Date = 02/18/14 
 Pct Recovery = 74%  Analysis Date = 02/18/14 
 Pct Recovery = 74%  Analysis Date = 02/16/14 
 Pct Recovery = 74%  Analysis Date = 02/16/14 
 Pct Recovery = 74%  Analysis Date = 02/14/14 
 Pct Recovery = 74%  Analysis Date = 02/14/14 
 Pct Recovery = 74%  Analysis Date = 02/12/14 
 Pct Recovery = 74%  Analysis Date = 02/12/14 
 Pct Recovery = 74%  Analysis Date = 02/09/14 
 Pct Recovery = 74%  Analysis Date = 02/09/14 
 Pct Recovery = 74%  Analysis Date = 02/07/14 
 Pct Recovery = 74%  Analysis Date = 02/07/14 
 Pct Recovery = 74%  Analysis Date = 02/05/14 
 Pct Recovery = 74%  Analysis Date = 02/05/14 
 Pct Recovery = 74%  Analysis Date = 02/02/14 
 Pct Recovery = 74%  Analysis Date = 02/02/14 
 Pct Recovery = 74%  Analysis Date = 01/31/14 
 Pct Recovery = 74%  Analysis Date = 01/31/14 
 Pct Recovery = 74%  Analysis Date = 01/29/14 
 Pct Recovery = 74%  Analysis Date = 01/29/14 
 Pct Recovery = 74%  Analysis Date = 01/26/14 
 Pct Recovery = 73%  Analysis Date = 01/26/14 
 Pct Recovery = 73%  Analysis Date = 01/24/14 
 Pct Recovery = 73%  Analysis Date = 01/24/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/19/14 
 Pct Recovery = 73%  Analysis Date = 01/19/14 
 Pct Recovery = 73%  Analysis Date = 01/17/14 
 Pct Recovery = 73%  Analysis Date = 01/17/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/13/14 
 Pct Recovery = 73%  Analysis Date = 01/13/14 
 Pct Recovery = 73%  Analysis Date = 01/10/14 
 Pct Recovery = 73%  Analysis Date = 01/10/14 
 Pct Recovery = 73%  Analysis Date = 01/08/14 
 Pct Recovery = 73%  Analysis Date = 01/08/14 
 Pct Recovery = 73%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 12/30/13 
 Pct Recovery = 73%  Analysis Date = 12/30/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/25/13 
 Pct Recovery = 73%  Analysis Date = 12/25/13 
 Pct Recovery = 73%  Analysis Date = 12/23/13 
 Pct Recovery = 73%  Analysis Date = 12/23/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/18/13 
 Pct Recovery = 73%  Analysis Date = 12/18/13 
 Pct Recovery = 73%  Analysis Date = 12/16/13 
 Pct Recovery = 73%  Analysis Date = 12/16/13 
 Pct Recovery = 73%  Analysis Date = 12/13/13 
 Pct Recovery = 73%  Analysis Date = 12/13/13 
 Pct Recovery = 73%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/04/13 
 Pct Recovery = 72%  Analysis Date = 12/04/13 
 Pct Recovery = 72%  Analysis Date = 12/02/13 
 Pct Recovery = 72%  Analysis Date = 12/02/13 
 Pct Recovery = 72%  Analysis Date = 11/30/13 
 Pct Recovery = 72%  Analysis Date = 11/30/13 
 Pct Recovery = 72%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/07/13 
 Pct Recovery = 72%  Analysis Date = 11/07/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/02/13 
 Pct Recovery = 72%  Analysis Date = 11/02/13 
 Pct Recovery = 72%  Analysis Date = 10/31/13 
 Pct Recovery = 72%  Analysis Date = 10/31/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/26/13 
 Pct Recovery = 72%  Analysis Date = 10/26/13 
 Pct Recovery = 72%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/07/13 
 Pct Recovery = 71%  Analysis Date = 10/07/13 
 Pct Recovery = 71%  Analysis Date = 10/05/13 
 Pct Recovery = 71%  Analysis Date = 10/05/13 
 Pct Recovery = 71%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 70%  Analysis Date = 08/25/13 
 Pct Recovery = 70%  Analysis Date = 08/22/13 
 Pct Recovery = 70%  Analysis Date = 08/22/13 
 Pct Recovery = 70%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/15/13 
 Pct Recovery = 70%  Analysis Date = 08/15/13 
 Pct Recovery = 70%  Analysis Date = 08/13/13 
 Pct Recovery = 70%  Analysis Date = 08/13/13 
 Pct Recovery = 70%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/08/13 
 Pct Recovery = 70%  Analysis Date = 08/08/13 
 Pct Recovery = 70%  Analysis Date = 08/06/13 
 Pct Recovery = 70%  Analysis Date = 08/06/13 
 Pct Recovery = 70%  Analysis Date = 08/04/13 
 Pct Recovery = 70%  Analysis Date = 08/04/13 
 Pct Recovery = 70%  Analysis Date = 08/02/13 
 Pct Recovery = 70%  Analysis Date = 08/02/13 
 Pct Recovery = 70%  Analysis Date = 07/30/13 
 Pct Recovery = 70%  Analysis Date = 07/30/13 
 Pct Recovery = 70%  Analysis Date = 07/28/13 
 Pct Recovery = 70%  Analysis Date = 07/28/13 
 Pct Recovery = 70%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/19/13 
 Pct Recovery = 69%  Analysis Date = 07/19/13 
 Pct Recovery = 69%  Analysis Date = 07/16/13 
 Pct Recovery = 69%  Analysis Date = 07/16/13 
 Pct Recovery = 69%  Analysis Date = 07/14/13 
 Pct Recovery = 69%  Analysis Date = 07/14/13 
 Pct Recovery = 69%  Analysis Date = 07/12/13 
 Pct Recovery = 69%  Analysis Date = 07/12/13 
 Pct Recovery = 69%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 06/30/13 
 Pct Recovery = 69%  Analysis Date = 06/30/13 
 Pct Recovery = 69%  Analysis Date = 06/28/13 
 Pct Recovery = 69%  Analysis Date = 06/28/13 
 Pct Recovery = 69%  Analysis Date = 06/26/13 
 Pct Recovery = 69%  Analysis Date = 06/26/13 
 Pct Recovery = 69%  Analysis Date = 06/23/13 
 Pct Recovery = 69%  Analysis Date = 06/23/13 
 Pct Recovery = 69%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/12/13 
 Pct Recovery = 69%  Analysis Date = 06/12/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/07/13 
 Pct Recovery = 69%  Analysis Date = 06/07/13 
 Pct Recovery = 69%  Analysis Date = 06/05/13 
 Pct Recovery = 69%  Analysis Date = 06/05/13 
 Pct Recovery = 69%  Analysis Date = 06/02/13 
 Pct Recovery = 69%  Analysis Date = 06/02/13 
 Pct Recovery = 69%  Analysis Date = 05/31/13 
 Pct Recovery = 69%  Analysis Date = 05/31/13 
 Pct Recovery = 69%  Analysis Date = 05/29/13 
 Pct Recovery = 69%  Analysis Date = 05/29/13 
 Pct Recovery = 69%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/22/13 
 Pct Recovery = 69%  Analysis Date = 05/22/13 
 Pct Recovery = 69%  Analysis Date = 05/20/13 
 Pct Recovery = 69%  Analysis Date = 05/20/13 
 Pct Recovery = 69%  Analysis Date = 05/17/13 
 Pct Recovery = 69%  Analysis Date = 05/17/13 
 Pct Recovery = 69%  Analysis Date = 05/15/13 
 Pct Recovery = 69%  Analysis Date = 05/15/13 
 Pct Recovery = 69%  Analysis Date = 05/13/13 
 Pct Recovery = 69%  Analysis Date = 05/13/13 
 Pct Recovery = 69%  Analysis Date = 05/10/13 
 Pct Recovery = 69%  Analysis Date = 05/10/13 
 Pct Recovery = 69%  Analysis Date = 05/08/13 
 Pct Recovery = 69%  Analysis Date = 05/08/13 
 Pct Recovery = 69%  Analysis Date = 05/06/13 
 Pct Recovery = 69%  Analysis Date = 05/06/13 
 Pct Recovery = 69%  Analysis Date = 05/03/13 
 Pct Recovery = 69%  Analysis Date = 05/03/13 
 Pct Recovery = 69%  Analysis Date = 05/01/13 
 Pct Recovery = 69%  Analysis Date = 05/01/13 
 Pct Recovery = 69%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 66%  Analysis Date = 04/15/13 
 Pct Recovery = 66%  Analysis Date = 04/13/13 
 Pct Recovery = 66%  Analysis Date = 04/13/13 
 Pct Recovery = 66%  Analysis Date = 04/10/13 
 Pct Recovery = 66%  Analysis Date = 04/10/13 
 Pct Recovery = 66%  Analysis Date = 04/08/13 
 Pct Recovery = 65%  Analysis Date = 04/08/13 
 Pct Recovery = 65%  Analysis Date = 04/06/13 
 Pct Recovery = 65%  Analysis Date = 04/06/13 
 Pct Recovery = 65%  Analysis Date = 04/03/13 
 Pct Recovery = 65%  Analysis Date = 04/03/13 
 Pct Recovery = 65%  Analysis Date = 04/01/13 
 Pct Recovery = 64%  Analysis Date = 04/01/13 
 Pct Recovery = 64%  Analysis Date = 03/30/13 
 Pct Recovery = 64%  Analysis Date = 03/30/13 
 Pct Recovery = 64%  Analysis Date = 03/27/13 
 Pct Recovery = 64%  Analysis Date = 03/27/13 
 Pct Recovery = 64%  Analysis Date = 03/25/13 
 Pct Recovery = 64%  Analysis Date = 03/25/13 
 Pct Recovery = 64%  Analysis Date = 03/23/13 
 Pct Recovery = 64%  Analysis Date = 03/23/13 
 Pct Recovery = 64%  Analysis Date = 03/21/13 
 Pct Recovery = 64%  Analysis Date = 03/21/13 
 Pct Recovery = 64%  Analysis Date = 03/18/13 
 Pct Recovery = 65%  Analysis Date = 03/18/13 
 Pct Recovery = 65%  Analysis Date = 03/16/13 
 Pct Recovery = 65%  Analysis Date = 03/16/13 
 Pct Recovery = 65%  Analysis Date = 03/14/13 
 Pct Recovery = 66%  Analysis Date = 03/14/13 
 Pct Recovery = 66%  Analysis Date = 03/11/13 
 Pct Recovery = 66%  Analysis Date = 03/11/13 
 Pct Recovery = 66%  Analysis Date = 03/09/13 
 Pct Recovery = 66%  Analysis Date = 03/09/13 
 Pct Recovery = 66%  Analysis Date = 03/07/13 
 Pct Recovery = 67%  Analysis Date = 03/07/13 
 Pct Recovery = 67%  Analysis Date = 03/04/13 
 Pct Recovery = 67%  Analysis Date = 03/04/13 
 Pct Recovery = 67%  Analysis Date = 03/02/13 
 Pct Recovery = 67%  Analysis Date = 03/02/13 
 Pct Recovery = 67%  Analysis Date = 02/28/13 
 Pct Recovery = 68%  Analysis Date = 02/28/13 
 Pct Recovery = 68%  Analysis Date = 02/25/13 
 Pct Recovery = 68%  Analysis Date = 02/25/13 
 Pct Recovery = 68%  Analysis Date = 02/23/13 
 Pct Recovery = 68%  Analysis Date = 02/23/13 
 Pct Recovery = 68%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/18/13 
 Pct Recovery = 69%  Analysis Date = 02/18/13 
 Pct Recovery = 69%  Analysis Date = 02/16/13 
 Pct Recovery = 69%  Analysis Date = 02/16/13 
 Pct Recovery = 69%  Analysis Date = 02/14/13 
 Pct Recovery = 70%  Analysis Date = 02/14/13 
 Pct Recovery = 70%  Analysis Date = 02/12/13 
 Pct Recovery = 70%  Analysis Date = 02/12/13 
 Pct Recovery = 70%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/02/13 
 Pct Recovery = 72%  Analysis Date = 02/02/13 
 Pct Recovery = 72%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/29/13 
 Pct Recovery = 72%  Analysis Date = 01/29/13 
 Pct Recovery = 72%  Analysis Date = 01/26/13 
 Pct Recovery = 73%  Analysis Date = 01/26/13 
 Pct Recovery = 73%  Analysis Date = 01/24/13 
 Pct Recovery = 73%  Analysis Date = 01/24/13 
 Pct Recovery = 73%  Analysis Date = 01/22/13 
 Pct Recovery = 73%  Analysis Date = 01/22/13 
 Pct Recovery = 73%  Analysis Date = 01/19/13 
 Pct Recovery = 74%  Analysis Date = 01/19/13 
 Pct Recovery = 74%  Analysis Date = 01/17/13 
 Pct Recovery = 74%  Analysis Date = 01/17/13 
 Pct Recovery = 74%  Analysis Date = 01/15/13 
 Pct Recovery = 74%  Analysis Date = 01/15/13 
 Pct Recovery = 74%  Analysis Date = 01/13/13 
 Pct Recovery = 75%  Analysis Date = 01/13/13 
 Pct Recovery = 75%  Analysis Date = 01/10/13 
 Pct Recovery = 75%  Analysis Date = 01/10/13 
 Pct Recovery = 75%  Analysis Date = 01/08/13 
 Pct Recovery = 75%  Analysis Date = 01/08/13 
 Pct Recovery = 75%  Analysis Date = 01/06/13 
 Pct Recovery = 76%  Analysis Date = 01/06/13 
 Pct Recovery = 76%  Analysis Date = 01/03/13 
 Pct Recovery = 76%  Analysis Date = 01/03/13 
 Pct Recovery = 76%  Analysis Date = 01/01/13 
 Pct Recovery = 76%  Analysis Date = 01/01/13 
 Pct Recovery = 76%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/20/12 
 Pct Recovery = 78%  Analysis Date = 12/20/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/14/12 
 Pct Recovery = 79%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIPHENHYDRAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 55% . 55% 0%
>= Reporting Level 12 72% 11% 70% 12%
Total 13 70% 11% 70% 12%

Sample Statistics
DIPHENHYDRAMINE

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
DULOXETINE
METHOD: LC9017 , TESTIDCODE: 67448LCM56

The SGPlot Procedure

Sample Statistics
DULOXETINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
ERYTHROMYCIN
METHOD: LC9017 , TESTIDCODE: 67449LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 47%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 5%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 16%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 30%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 31%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 15%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 33%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 11%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 7%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 32%  Analysis Date = 02/20/14 
 Pct Recovery = 33%  Analysis Date = 02/17/14 
 Pct Recovery = 33%  Analysis Date = 02/17/14 
 Pct Recovery = 33%  Analysis Date = 02/15/14 
 Pct Recovery = 33%  Analysis Date = 02/15/14 
 Pct Recovery = 33%  Analysis Date = 02/13/14 
 Pct Recovery = 32%  Analysis Date = 02/13/14 
 Pct Recovery = 32%  Analysis Date = 02/11/14 
 Pct Recovery = 32%  Analysis Date = 02/11/14 
 Pct Recovery = 32%  Analysis Date = 02/09/14 
 Pct Recovery = 32%  Analysis Date = 02/09/14 
 Pct Recovery = 32%  Analysis Date = 02/07/14 
 Pct Recovery = 32%  Analysis Date = 02/07/14 
 Pct Recovery = 32%  Analysis Date = 02/04/14 
 Pct Recovery = 31%  Analysis Date = 02/04/14 
 Pct Recovery = 31%  Analysis Date = 02/02/14 
 Pct Recovery = 31%  Analysis Date = 02/02/14 
 Pct Recovery = 31%  Analysis Date = 01/31/14 
 Pct Recovery = 31%  Analysis Date = 01/31/14 
 Pct Recovery = 31%  Analysis Date = 01/29/14 
 Pct Recovery = 31%  Analysis Date = 01/29/14 
 Pct Recovery = 31%  Analysis Date = 01/27/14 
 Pct Recovery = 31%  Analysis Date = 01/27/14 
 Pct Recovery = 31%  Analysis Date = 01/25/14 
 Pct Recovery = 30%  Analysis Date = 01/25/14 
 Pct Recovery = 30%  Analysis Date = 01/22/14 
 Pct Recovery = 30%  Analysis Date = 01/22/14 
 Pct Recovery = 30%  Analysis Date = 01/20/14 
 Pct Recovery = 30%  Analysis Date = 01/20/14 
 Pct Recovery = 30%  Analysis Date = 01/18/14 
 Pct Recovery = 30%  Analysis Date = 01/18/14 
 Pct Recovery = 30%  Analysis Date = 01/16/14 
 Pct Recovery = 29%  Analysis Date = 01/16/14 
 Pct Recovery = 29%  Analysis Date = 01/14/14 
 Pct Recovery = 29%  Analysis Date = 01/14/14 
 Pct Recovery = 29%  Analysis Date = 01/12/14 
 Pct Recovery = 29%  Analysis Date = 01/12/14 
 Pct Recovery = 29%  Analysis Date = 01/09/14 
 Pct Recovery = 29%  Analysis Date = 01/09/14 
 Pct Recovery = 29%  Analysis Date = 01/07/14 
 Pct Recovery = 28%  Analysis Date = 01/07/14 
 Pct Recovery = 28%  Analysis Date = 01/05/14 
 Pct Recovery = 28%  Analysis Date = 01/05/14 
 Pct Recovery = 28%  Analysis Date = 01/03/14 
 Pct Recovery = 28%  Analysis Date = 01/03/14 
 Pct Recovery = 28%  Analysis Date = 01/01/14 
 Pct Recovery = 28%  Analysis Date = 01/01/14 
 Pct Recovery = 28%  Analysis Date = 12/30/13 
 Pct Recovery = 27%  Analysis Date = 12/30/13 
 Pct Recovery = 27%  Analysis Date = 12/27/13 
 Pct Recovery = 27%  Analysis Date = 12/27/13 
 Pct Recovery = 27%  Analysis Date = 12/25/13 
 Pct Recovery = 27%  Analysis Date = 12/25/13 
 Pct Recovery = 27%  Analysis Date = 12/23/13 
 Pct Recovery = 27%  Analysis Date = 12/23/13 
 Pct Recovery = 27%  Analysis Date = 12/21/13 
 Pct Recovery = 26%  Analysis Date = 12/21/13 
 Pct Recovery = 26%  Analysis Date = 12/19/13 
 Pct Recovery = 26%  Analysis Date = 12/19/13 
 Pct Recovery = 26%  Analysis Date = 12/17/13 
 Pct Recovery = 26%  Analysis Date = 12/17/13 
 Pct Recovery = 26%  Analysis Date = 12/14/13 
 Pct Recovery = 26%  Analysis Date = 12/14/13 
 Pct Recovery = 26%  Analysis Date = 12/12/13 
 Pct Recovery = 25%  Analysis Date = 12/12/13 
 Pct Recovery = 25%  Analysis Date = 12/10/13 
 Pct Recovery = 25%  Analysis Date = 12/10/13 
 Pct Recovery = 25%  Analysis Date = 12/08/13 
 Pct Recovery = 25%  Analysis Date = 12/08/13 
 Pct Recovery = 25%  Analysis Date = 12/06/13 
 Pct Recovery = 25%  Analysis Date = 12/06/13 
 Pct Recovery = 25%  Analysis Date = 12/04/13 
 Pct Recovery = 25%  Analysis Date = 12/04/13 
 Pct Recovery = 25%  Analysis Date = 12/01/13 
 Pct Recovery = 24%  Analysis Date = 12/01/13 
 Pct Recovery = 24%  Analysis Date = 11/29/13 
 Pct Recovery = 24%  Analysis Date = 11/29/13 
 Pct Recovery = 24%  Analysis Date = 11/27/13 
 Pct Recovery = 24%  Analysis Date = 11/27/13 
 Pct Recovery = 24%  Analysis Date = 11/25/13 
 Pct Recovery = 24%  Analysis Date = 11/25/13 
 Pct Recovery = 24%  Analysis Date = 11/23/13 
 Pct Recovery = 23%  Analysis Date = 11/23/13 
 Pct Recovery = 23%  Analysis Date = 11/21/13 
 Pct Recovery = 23%  Analysis Date = 11/21/13 
 Pct Recovery = 23%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/16/13 
 Pct Recovery = 23%  Analysis Date = 11/16/13 
 Pct Recovery = 23%  Analysis Date = 11/14/13 
 Pct Recovery = 22%  Analysis Date = 11/14/13 
 Pct Recovery = 22%  Analysis Date = 11/12/13 
 Pct Recovery = 22%  Analysis Date = 11/12/13 
 Pct Recovery = 22%  Analysis Date = 11/10/13 
 Pct Recovery = 22%  Analysis Date = 11/10/13 
 Pct Recovery = 22%  Analysis Date = 11/08/13 
 Pct Recovery = 22%  Analysis Date = 11/08/13 
 Pct Recovery = 22%  Analysis Date = 11/05/13 
 Pct Recovery = 21%  Analysis Date = 11/05/13 
 Pct Recovery = 21%  Analysis Date = 11/03/13 
 Pct Recovery = 21%  Analysis Date = 11/03/13 
 Pct Recovery = 21%  Analysis Date = 11/01/13 
 Pct Recovery = 21%  Analysis Date = 11/01/13 
 Pct Recovery = 21%  Analysis Date = 10/30/13 
 Pct Recovery = 21%  Analysis Date = 10/30/13 
 Pct Recovery = 21%  Analysis Date = 10/28/13 
 Pct Recovery = 21%  Analysis Date = 10/28/13 
 Pct Recovery = 21%  Analysis Date = 10/26/13 
 Pct Recovery = 20%  Analysis Date = 10/26/13 
 Pct Recovery = 20%  Analysis Date = 10/23/13 
 Pct Recovery = 20%  Analysis Date = 10/23/13 
 Pct Recovery = 20%  Analysis Date = 10/21/13 
 Pct Recovery = 20%  Analysis Date = 10/21/13 
 Pct Recovery = 20%  Analysis Date = 10/19/13 
 Pct Recovery = 20%  Analysis Date = 10/19/13 
 Pct Recovery = 20%  Analysis Date = 10/17/13 
 Pct Recovery = 19%  Analysis Date = 10/17/13 
 Pct Recovery = 19%  Analysis Date = 10/15/13 
 Pct Recovery = 19%  Analysis Date = 10/15/13 
 Pct Recovery = 19%  Analysis Date = 10/13/13 
 Pct Recovery = 19%  Analysis Date = 10/13/13 
 Pct Recovery = 19%  Analysis Date = 10/10/13 
 Pct Recovery = 19%  Analysis Date = 10/10/13 
 Pct Recovery = 19%  Analysis Date = 10/08/13 
 Pct Recovery = 18%  Analysis Date = 10/08/13 
 Pct Recovery = 18%  Analysis Date = 10/06/13 
 Pct Recovery = 18%  Analysis Date = 10/06/13 
 Pct Recovery = 18%  Analysis Date = 10/04/13 
 Pct Recovery = 18%  Analysis Date = 10/04/13 
 Pct Recovery = 18%  Analysis Date = 10/02/13 
 Pct Recovery = 18%  Analysis Date = 10/02/13 
 Pct Recovery = 18%  Analysis Date = 09/30/13 
 Pct Recovery = 18%  Analysis Date = 09/30/13 
 Pct Recovery = 18%  Analysis Date = 09/27/13 
 Pct Recovery = 17%  Analysis Date = 09/27/13 
 Pct Recovery = 17%  Analysis Date = 09/25/13 
 Pct Recovery = 17%  Analysis Date = 09/25/13 
 Pct Recovery = 17%  Analysis Date = 09/23/13 
 Pct Recovery = 17%  Analysis Date = 09/23/13 
 Pct Recovery = 17%  Analysis Date = 09/21/13 
 Pct Recovery = 17%  Analysis Date = 09/21/13 
 Pct Recovery = 17%  Analysis Date = 09/19/13 
 Pct Recovery = 16%  Analysis Date = 09/19/13 
 Pct Recovery = 16%  Analysis Date = 09/17/13 
 Pct Recovery = 16%  Analysis Date = 09/17/13 
 Pct Recovery = 16%  Analysis Date = 09/14/13 
 Pct Recovery = 16%  Analysis Date = 09/14/13 
 Pct Recovery = 16%  Analysis Date = 09/12/13 
 Pct Recovery = 16%  Analysis Date = 09/12/13 
 Pct Recovery = 16%  Analysis Date = 09/10/13 
 Pct Recovery = 15%  Analysis Date = 09/10/13 
 Pct Recovery = 15%  Analysis Date = 09/08/13 
 Pct Recovery = 15%  Analysis Date = 09/08/13 
 Pct Recovery = 15%  Analysis Date = 09/06/13 
 Pct Recovery = 15%  Analysis Date = 09/06/13 
 Pct Recovery = 15%  Analysis Date = 09/04/13 
 Pct Recovery = 15%  Analysis Date = 09/04/13 
 Pct Recovery = 15%  Analysis Date = 09/01/13 
 Pct Recovery = 15%  Analysis Date = 09/01/13 
 Pct Recovery = 15%  Analysis Date = 08/30/13 
 Pct Recovery = 14%  Analysis Date = 08/30/13 
 Pct Recovery = 14%  Analysis Date = 08/28/13 
 Pct Recovery = 14%  Analysis Date = 08/28/13 
 Pct Recovery = 14%  Analysis Date = 08/26/13 
 Pct Recovery = 14%  Analysis Date = 08/26/13 
 Pct Recovery = 14%  Analysis Date = 08/24/13 
 Pct Recovery = 14%  Analysis Date = 08/24/13 
 Pct Recovery = 14%  Analysis Date = 08/22/13 
 Pct Recovery = 13%  Analysis Date = 08/22/13 
 Pct Recovery = 13%  Analysis Date = 08/19/13 
 Pct Recovery = 13%  Analysis Date = 08/19/13 
 Pct Recovery = 13%  Analysis Date = 08/17/13 
 Pct Recovery = 13%  Analysis Date = 08/17/13 
 Pct Recovery = 13%  Analysis Date = 08/15/13 
 Pct Recovery = 13%  Analysis Date = 08/15/13 
 Pct Recovery = 13%  Analysis Date = 08/13/13 
 Pct Recovery = 12%  Analysis Date = 08/13/13 
 Pct Recovery = 12%  Analysis Date = 08/11/13 
 Pct Recovery = 12%  Analysis Date = 08/11/13 
 Pct Recovery = 12%  Analysis Date = 08/09/13 
 Pct Recovery = 12%  Analysis Date = 08/09/13 
 Pct Recovery = 12%  Analysis Date = 08/06/13 
 Pct Recovery = 11%  Analysis Date = 08/06/13 
 Pct Recovery = 11%  Analysis Date = 08/04/13 
 Pct Recovery = 11%  Analysis Date = 08/04/13 
 Pct Recovery = 11%  Analysis Date = 08/02/13 
 Pct Recovery = 11%  Analysis Date = 08/02/13 
 Pct Recovery = 11%  Analysis Date = 07/31/13 
 Pct Recovery = 11%  Analysis Date = 07/31/13 
 Pct Recovery = 11%  Analysis Date = 07/29/13 
 Pct Recovery = 11%  Analysis Date = 07/29/13 
 Pct Recovery = 11%  Analysis Date = 07/27/13 
 Pct Recovery = 11%  Analysis Date = 07/27/13 
 Pct Recovery = 11%  Analysis Date = 07/24/13 
 Pct Recovery = 12%  Analysis Date = 07/24/13 
 Pct Recovery = 12%  Analysis Date = 07/22/13 
 Pct Recovery = 12%  Analysis Date = 07/22/13 
 Pct Recovery = 12%  Analysis Date = 07/20/13 
 Pct Recovery = 12%  Analysis Date = 07/20/13 
 Pct Recovery = 12%  Analysis Date = 07/18/13 
 Pct Recovery = 13%  Analysis Date = 07/18/13 
 Pct Recovery = 13%  Analysis Date = 07/16/13 
 Pct Recovery = 13%  Analysis Date = 07/16/13 
 Pct Recovery = 13%  Analysis Date = 07/14/13 
 Pct Recovery = 13%  Analysis Date = 07/14/13 
 Pct Recovery = 13%  Analysis Date = 07/12/13 
 Pct Recovery = 14%  Analysis Date = 07/12/13 
 Pct Recovery = 14%  Analysis Date = 07/09/13 
 Pct Recovery = 14%  Analysis Date = 07/09/13 
 Pct Recovery = 14%  Analysis Date = 07/07/13 
 Pct Recovery = 14%  Analysis Date = 07/07/13 
 Pct Recovery = 14%  Analysis Date = 07/05/13 
 Pct Recovery = 14%  Analysis Date = 07/05/13 
 Pct Recovery = 14%  Analysis Date = 07/03/13 
 Pct Recovery = 15%  Analysis Date = 07/03/13 
 Pct Recovery = 15%  Analysis Date = 07/01/13 
 Pct Recovery = 15%  Analysis Date = 07/01/13 
 Pct Recovery = 15%  Analysis Date = 06/29/13 
 Pct Recovery = 15%  Analysis Date = 06/29/13 
 Pct Recovery = 15%  Analysis Date = 06/26/13 
 Pct Recovery = 16%  Analysis Date = 06/26/13 
 Pct Recovery = 16%  Analysis Date = 06/24/13 
 Pct Recovery = 16%  Analysis Date = 06/24/13 
 Pct Recovery = 16%  Analysis Date = 06/22/13 
 Pct Recovery = 16%  Analysis Date = 06/22/13 
 Pct Recovery = 16%  Analysis Date = 06/20/13 
 Pct Recovery = 17%  Analysis Date = 06/20/13 
 Pct Recovery = 17%  Analysis Date = 06/18/13 
 Pct Recovery = 17%  Analysis Date = 06/18/13 
 Pct Recovery = 17%  Analysis Date = 06/16/13 
 Pct Recovery = 17%  Analysis Date = 06/16/13 
 Pct Recovery = 17%  Analysis Date = 06/13/13 
 Pct Recovery = 18%  Analysis Date = 06/13/13 
 Pct Recovery = 18%  Analysis Date = 06/11/13 
 Pct Recovery = 18%  Analysis Date = 06/11/13 
 Pct Recovery = 18%  Analysis Date = 06/09/13 
 Pct Recovery = 18%  Analysis Date = 06/09/13 
 Pct Recovery = 18%  Analysis Date = 06/07/13 
 Pct Recovery = 18%  Analysis Date = 06/07/13 
 Pct Recovery = 18%  Analysis Date = 06/05/13 
 Pct Recovery = 19%  Analysis Date = 06/05/13 
 Pct Recovery = 19%  Analysis Date = 06/03/13 
 Pct Recovery = 19%  Analysis Date = 06/03/13 
 Pct Recovery = 19%  Analysis Date = 05/31/13 
 Pct Recovery = 19%  Analysis Date = 05/31/13 
 Pct Recovery = 19%  Analysis Date = 05/29/13 
 Pct Recovery = 20%  Analysis Date = 05/29/13 
 Pct Recovery = 20%  Analysis Date = 05/27/13 
 Pct Recovery = 20%  Analysis Date = 05/27/13 
 Pct Recovery = 20%  Analysis Date = 05/25/13 
 Pct Recovery = 20%  Analysis Date = 05/25/13 
 Pct Recovery = 20%  Analysis Date = 05/23/13 
 Pct Recovery = 21%  Analysis Date = 05/23/13 
 Pct Recovery = 21%  Analysis Date = 05/21/13 
 Pct Recovery = 21%  Analysis Date = 05/21/13 
 Pct Recovery = 21%  Analysis Date = 05/18/13 
 Pct Recovery = 21%  Analysis Date = 05/18/13 
 Pct Recovery = 21%  Analysis Date = 05/16/13 
 Pct Recovery = 21%  Analysis Date = 05/16/13 
 Pct Recovery = 21%  Analysis Date = 05/14/13 
 Pct Recovery = 22%  Analysis Date = 05/14/13 
 Pct Recovery = 22%  Analysis Date = 05/12/13 
 Pct Recovery = 22%  Analysis Date = 05/12/13 
 Pct Recovery = 22%  Analysis Date = 05/10/13 
 Pct Recovery = 22%  Analysis Date = 05/10/13 
 Pct Recovery = 22%  Analysis Date = 05/08/13 
 Pct Recovery = 23%  Analysis Date = 05/08/13 
 Pct Recovery = 23%  Analysis Date = 05/05/13 
 Pct Recovery = 23%  Analysis Date = 05/05/13 
 Pct Recovery = 23%  Analysis Date = 05/03/13 
 Pct Recovery = 23%  Analysis Date = 05/03/13 
 Pct Recovery = 23%  Analysis Date = 05/01/13 
 Pct Recovery = 23%  Analysis Date = 05/01/13 
 Pct Recovery = 23%  Analysis Date = 04/29/13 
 Pct Recovery = 24%  Analysis Date = 04/29/13 
 Pct Recovery = 24%  Analysis Date = 04/27/13 
 Pct Recovery = 24%  Analysis Date = 04/27/13 
 Pct Recovery = 24%  Analysis Date = 04/25/13 
 Pct Recovery = 24%  Analysis Date = 04/25/13 
 Pct Recovery = 24%  Analysis Date = 04/22/13 
 Pct Recovery = 24%  Analysis Date = 04/22/13 
 Pct Recovery = 24%  Analysis Date = 04/20/13 
 Pct Recovery = 24%  Analysis Date = 04/20/13 
 Pct Recovery = 24%  Analysis Date = 04/18/13 
 Pct Recovery = 24%  Analysis Date = 04/18/13 
 Pct Recovery = 24%  Analysis Date = 04/16/13 
 Pct Recovery = 24%  Analysis Date = 04/16/13 
 Pct Recovery = 24%  Analysis Date = 04/14/13 
 Pct Recovery = 24%  Analysis Date = 04/14/13 
 Pct Recovery = 24%  Analysis Date = 04/12/13 
 Pct Recovery = 24%  Analysis Date = 04/12/13 
 Pct Recovery = 24%  Analysis Date = 04/09/13 
 Pct Recovery = 24%  Analysis Date = 04/09/13 
 Pct Recovery = 24%  Analysis Date = 04/07/13 
 Pct Recovery = 24%  Analysis Date = 04/07/13 
 Pct Recovery = 24%  Analysis Date = 04/05/13 
 Pct Recovery = 24%  Analysis Date = 04/05/13 
 Pct Recovery = 24%  Analysis Date = 04/03/13 
 Pct Recovery = 24%  Analysis Date = 04/03/13 
 Pct Recovery = 24%  Analysis Date = 04/01/13 
 Pct Recovery = 24%  Analysis Date = 04/01/13 
 Pct Recovery = 24%  Analysis Date = 03/30/13 
 Pct Recovery = 24%  Analysis Date = 03/30/13 
 Pct Recovery = 24%  Analysis Date = 03/27/13 
 Pct Recovery = 24%  Analysis Date = 03/27/13 
 Pct Recovery = 24%  Analysis Date = 03/25/13 
 Pct Recovery = 24%  Analysis Date = 03/25/13 
 Pct Recovery = 24%  Analysis Date = 03/23/13 
 Pct Recovery = 24%  Analysis Date = 03/23/13 
 Pct Recovery = 24%  Analysis Date = 03/21/13 
 Pct Recovery = 24%  Analysis Date = 03/21/13 
 Pct Recovery = 24%  Analysis Date = 03/19/13 
 Pct Recovery = 24%  Analysis Date = 03/19/13 
 Pct Recovery = 24%  Analysis Date = 03/17/13 
 Pct Recovery = 24%  Analysis Date = 03/17/13 
 Pct Recovery = 24%  Analysis Date = 03/14/13 
 Pct Recovery = 24%  Analysis Date = 03/14/13 
 Pct Recovery = 24%  Analysis Date = 03/12/13 
 Pct Recovery = 23%  Analysis Date = 03/12/13 
 Pct Recovery = 23%  Analysis Date = 03/10/13 
 Pct Recovery = 23%  Analysis Date = 03/10/13 
 Pct Recovery = 23%  Analysis Date = 03/08/13 
 Pct Recovery = 23%  Analysis Date = 03/08/13 
 Pct Recovery = 23%  Analysis Date = 03/06/13 
 Pct Recovery = 23%  Analysis Date = 03/06/13 
 Pct Recovery = 23%  Analysis Date = 03/04/13 
 Pct Recovery = 23%  Analysis Date = 03/04/13 
 Pct Recovery = 23%  Analysis Date = 03/01/13 
 Pct Recovery = 23%  Analysis Date = 03/01/13 
 Pct Recovery = 23%  Analysis Date = 02/27/13 
 Pct Recovery = 23%  Analysis Date = 02/27/13 
 Pct Recovery = 23%  Analysis Date = 02/25/13 
 Pct Recovery = 22%  Analysis Date = 02/25/13 
 Pct Recovery = 22%  Analysis Date = 02/23/13 
 Pct Recovery = 22%  Analysis Date = 02/23/13 
 Pct Recovery = 22%  Analysis Date = 02/21/13 
 Pct Recovery = 22%  Analysis Date = 02/21/13 
 Pct Recovery = 22%  Analysis Date = 02/19/13 
 Pct Recovery = 22%  Analysis Date = 02/19/13 
 Pct Recovery = 22%  Analysis Date = 02/16/13 
 Pct Recovery = 22%  Analysis Date = 02/16/13 
 Pct Recovery = 22%  Analysis Date = 02/14/13 
 Pct Recovery = 22%  Analysis Date = 02/14/13 
 Pct Recovery = 22%  Analysis Date = 02/12/13 
 Pct Recovery = 22%  Analysis Date = 02/12/13 
 Pct Recovery = 22%  Analysis Date = 02/10/13 
 Pct Recovery = 22%  Analysis Date = 02/10/13 
 Pct Recovery = 22%  Analysis Date = 02/08/13 
 Pct Recovery = 22%  Analysis Date = 02/08/13 
 Pct Recovery = 22%  Analysis Date = 02/06/13 
 Pct Recovery = 21%  Analysis Date = 02/06/13 
 Pct Recovery = 21%  Analysis Date = 02/03/13 
 Pct Recovery = 21%  Analysis Date = 02/03/13 
 Pct Recovery = 21%  Analysis Date = 02/01/13 
 Pct Recovery = 21%  Analysis Date = 02/01/13 
 Pct Recovery = 21%  Analysis Date = 01/30/13 
 Pct Recovery = 21%  Analysis Date = 01/30/13 
 Pct Recovery = 21%  Analysis Date = 01/28/13 
 Pct Recovery = 21%  Analysis Date = 01/28/13 
 Pct Recovery = 21%  Analysis Date = 01/26/13 
 Pct Recovery = 21%  Analysis Date = 01/26/13 
 Pct Recovery = 21%  Analysis Date = 01/24/13 
 Pct Recovery = 21%  Analysis Date = 01/24/13 
 Pct Recovery = 21%  Analysis Date = 01/21/13 
 Pct Recovery = 21%  Analysis Date = 01/21/13 
 Pct Recovery = 21%  Analysis Date = 01/19/13 
 Pct Recovery = 20%  Analysis Date = 01/19/13 
 Pct Recovery = 20%  Analysis Date = 01/17/13 
 Pct Recovery = 20%  Analysis Date = 01/17/13 
 Pct Recovery = 20%  Analysis Date = 01/15/13 
 Pct Recovery = 20%  Analysis Date = 01/15/13 
 Pct Recovery = 20%  Analysis Date = 01/13/13 
 Pct Recovery = 20%  Analysis Date = 01/13/13 
 Pct Recovery = 20%  Analysis Date = 01/11/13 
 Pct Recovery = 20%  Analysis Date = 01/11/13 
 Pct Recovery = 20%  Analysis Date = 01/08/13 
 Pct Recovery = 20%  Analysis Date = 01/08/13 
 Pct Recovery = 20%  Analysis Date = 01/06/13 
 Pct Recovery = 20%  Analysis Date = 01/06/13 
 Pct Recovery = 20%  Analysis Date = 01/04/13 
 Pct Recovery = 20%  Analysis Date = 01/04/13 
 Pct Recovery = 20%  Analysis Date = 01/02/13 
 Pct Recovery = 20%  Analysis Date = 01/02/13 
 Pct Recovery = 20%  Analysis Date = 12/31/12 
 Pct Recovery = 19%  Analysis Date = 12/31/12 
 Pct Recovery = 19%  Analysis Date = 12/29/12 
 Pct Recovery = 19%  Analysis Date = 12/29/12 
 Pct Recovery = 19%  Analysis Date = 12/26/12 
 Pct Recovery = 19%  Analysis Date = 12/26/12 
 Pct Recovery = 19%  Analysis Date = 12/24/12 
 Pct Recovery = 19%  Analysis Date = 12/24/12 
 Pct Recovery = 19%  Analysis Date = 12/22/12 
 Pct Recovery = 19%  Analysis Date = 12/22/12 
 Pct Recovery = 19%  Analysis Date = 12/20/12 
 Pct Recovery = 19%  Analysis Date = 12/20/12 
 Pct Recovery = 19%  Analysis Date = 12/18/12 
 Pct Recovery = 19%  Analysis Date = 12/18/12 
 Pct Recovery = 19%  Analysis Date = 12/16/12 
 Pct Recovery = 19%  Analysis Date = 12/16/12 
 Pct Recovery = 19%  Analysis Date = 12/14/12 
 Pct Recovery = 18%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ERYTHROMYCIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 23% 14% 23% 16%
Total 10 23% 14% 23% 16%

Sample Statistics
ERYTHROMYCIN

Characteristic N % % Basis
Plotted 10 67% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 5 33% 5 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
EZETIMIBE
METHOD: LC9017 , TESTIDCODE: 67487LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 54%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 45%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 57%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 45%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 44%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 7%  Analysis Date = 02/20/14 
 Pct Recovery = 58%  Analysis Date = 02/17/14 
 Pct Recovery = 55%  Analysis Date = 02/17/14 
 Pct Recovery = 55%  Analysis Date = 02/15/14 
 Pct Recovery = 51%  Analysis Date = 02/15/14 
 Pct Recovery = 51%  Analysis Date = 02/13/14 
 Pct Recovery = 48%  Analysis Date = 02/13/14 
 Pct Recovery = 48%  Analysis Date = 02/11/14 
 Pct Recovery = 45%  Analysis Date = 02/11/14 
 Pct Recovery = 45%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/07/14 
 Pct Recovery = 39%  Analysis Date = 02/07/14 
 Pct Recovery = 39%  Analysis Date = 02/04/14 
 Pct Recovery = 36%  Analysis Date = 02/04/14 
 Pct Recovery = 36%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 30%  Analysis Date = 01/31/14 
 Pct Recovery = 30%  Analysis Date = 01/29/14 
 Pct Recovery = 27%  Analysis Date = 01/29/14 
 Pct Recovery = 27%  Analysis Date = 01/27/14 
 Pct Recovery = 24%  Analysis Date = 01/27/14 
 Pct Recovery = 24%  Analysis Date = 01/25/14 
 Pct Recovery = 21%  Analysis Date = 01/25/14 
 Pct Recovery = 21%  Analysis Date = 01/22/14 
 Pct Recovery = 17%  Analysis Date = 01/22/14 
 Pct Recovery = 17%  Analysis Date = 01/20/14 
 Pct Recovery = 14%  Analysis Date = 01/20/14 
 Pct Recovery = 14%  Analysis Date = 01/18/14 
 Pct Recovery = 11%  Analysis Date = 01/18/14 
 Pct Recovery = 11%  Analysis Date = 01/16/14 
 Pct Recovery = 8%  Analysis Date = 01/16/14 
 Pct Recovery = 8%  Analysis Date = 01/14/14 
 Pct Recovery = 8%  Analysis Date = 01/14/14 
 Pct Recovery = 8%  Analysis Date = 01/12/14 
 Pct Recovery = 9%  Analysis Date = 01/12/14 
 Pct Recovery = 9%  Analysis Date = 01/09/14 
 Pct Recovery = 9%  Analysis Date = 01/09/14 
 Pct Recovery = 9%  Analysis Date = 01/07/14 
 Pct Recovery = 10%  Analysis Date = 01/07/14 
 Pct Recovery = 10%  Analysis Date = 01/05/14 
 Pct Recovery = 10%  Analysis Date = 01/05/14 
 Pct Recovery = 10%  Analysis Date = 01/03/14 
 Pct Recovery = 11%  Analysis Date = 01/03/14 
 Pct Recovery = 11%  Analysis Date = 01/01/14 
 Pct Recovery = 12%  Analysis Date = 01/01/14 
 Pct Recovery = 12%  Analysis Date = 12/30/13 
 Pct Recovery = 12%  Analysis Date = 12/30/13 
 Pct Recovery = 12%  Analysis Date = 12/27/13 
 Pct Recovery = 13%  Analysis Date = 12/27/13 
 Pct Recovery = 13%  Analysis Date = 12/25/13 
 Pct Recovery = 13%  Analysis Date = 12/25/13 
 Pct Recovery = 13%  Analysis Date = 12/23/13 
 Pct Recovery = 14%  Analysis Date = 12/23/13 
 Pct Recovery = 14%  Analysis Date = 12/21/13 
 Pct Recovery = 14%  Analysis Date = 12/21/13 
 Pct Recovery = 14%  Analysis Date = 12/19/13 
 Pct Recovery = 15%  Analysis Date = 12/19/13 
 Pct Recovery = 15%  Analysis Date = 12/17/13 
 Pct Recovery = 16%  Analysis Date = 12/17/13 
 Pct Recovery = 16%  Analysis Date = 12/14/13 
 Pct Recovery = 16%  Analysis Date = 12/14/13 
 Pct Recovery = 16%  Analysis Date = 12/12/13 
 Pct Recovery = 17%  Analysis Date = 12/12/13 
 Pct Recovery = 17%  Analysis Date = 12/10/13 
 Pct Recovery = 17%  Analysis Date = 12/10/13 
 Pct Recovery = 17%  Analysis Date = 12/08/13 
 Pct Recovery = 18%  Analysis Date = 12/08/13 
 Pct Recovery = 18%  Analysis Date = 12/06/13 
 Pct Recovery = 18%  Analysis Date = 12/06/13 
 Pct Recovery = 18%  Analysis Date = 12/04/13 
 Pct Recovery = 19%  Analysis Date = 12/04/13 
 Pct Recovery = 19%  Analysis Date = 12/01/13 
 Pct Recovery = 20%  Analysis Date = 12/01/13 
 Pct Recovery = 20%  Analysis Date = 11/29/13 
 Pct Recovery = 20%  Analysis Date = 11/29/13 
 Pct Recovery = 20%  Analysis Date = 11/27/13 
 Pct Recovery = 21%  Analysis Date = 11/27/13 
 Pct Recovery = 21%  Analysis Date = 11/25/13 
 Pct Recovery = 21%  Analysis Date = 11/25/13 
 Pct Recovery = 21%  Analysis Date = 11/23/13 
 Pct Recovery = 22%  Analysis Date = 11/23/13 
 Pct Recovery = 22%  Analysis Date = 11/21/13 
 Pct Recovery = 22%  Analysis Date = 11/21/13 
 Pct Recovery = 22%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/16/13 
 Pct Recovery = 23%  Analysis Date = 11/16/13 
 Pct Recovery = 23%  Analysis Date = 11/14/13 
 Pct Recovery = 24%  Analysis Date = 11/14/13 
 Pct Recovery = 24%  Analysis Date = 11/12/13 
 Pct Recovery = 25%  Analysis Date = 11/12/13 
 Pct Recovery = 25%  Analysis Date = 11/10/13 
 Pct Recovery = 25%  Analysis Date = 11/10/13 
 Pct Recovery = 25%  Analysis Date = 11/08/13 
 Pct Recovery = 26%  Analysis Date = 11/08/13 
 Pct Recovery = 26%  Analysis Date = 11/05/13 
 Pct Recovery = 26%  Analysis Date = 11/05/13 
 Pct Recovery = 26%  Analysis Date = 11/03/13 
 Pct Recovery = 27%  Analysis Date = 11/03/13 
 Pct Recovery = 27%  Analysis Date = 11/01/13 
 Pct Recovery = 27%  Analysis Date = 11/01/13 
 Pct Recovery = 27%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 29%  Analysis Date = 10/28/13 
 Pct Recovery = 29%  Analysis Date = 10/26/13 
 Pct Recovery = 29%  Analysis Date = 10/26/13 
 Pct Recovery = 29%  Analysis Date = 10/23/13 
 Pct Recovery = 30%  Analysis Date = 10/23/13 
 Pct Recovery = 30%  Analysis Date = 10/21/13 
 Pct Recovery = 30%  Analysis Date = 10/21/13 
 Pct Recovery = 30%  Analysis Date = 10/19/13 
 Pct Recovery = 31%  Analysis Date = 10/19/13 
 Pct Recovery = 31%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/15/13 
 Pct Recovery = 32%  Analysis Date = 10/15/13 
 Pct Recovery = 32%  Analysis Date = 10/13/13 
 Pct Recovery = 33%  Analysis Date = 10/13/13 
 Pct Recovery = 33%  Analysis Date = 10/10/13 
 Pct Recovery = 33%  Analysis Date = 10/10/13 
 Pct Recovery = 33%  Analysis Date = 10/08/13 
 Pct Recovery = 34%  Analysis Date = 10/08/13 
 Pct Recovery = 34%  Analysis Date = 10/06/13 
 Pct Recovery = 34%  Analysis Date = 10/06/13 
 Pct Recovery = 34%  Analysis Date = 10/04/13 
 Pct Recovery = 35%  Analysis Date = 10/04/13 
 Pct Recovery = 35%  Analysis Date = 10/02/13 
 Pct Recovery = 35%  Analysis Date = 10/02/13 
 Pct Recovery = 35%  Analysis Date = 09/30/13 
 Pct Recovery = 36%  Analysis Date = 09/30/13 
 Pct Recovery = 36%  Analysis Date = 09/27/13 
 Pct Recovery = 37%  Analysis Date = 09/27/13 
 Pct Recovery = 37%  Analysis Date = 09/25/13 
 Pct Recovery = 37%  Analysis Date = 09/25/13 
 Pct Recovery = 37%  Analysis Date = 09/23/13 
 Pct Recovery = 38%  Analysis Date = 09/23/13 
 Pct Recovery = 38%  Analysis Date = 09/21/13 
 Pct Recovery = 38%  Analysis Date = 09/21/13 
 Pct Recovery = 38%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/14/13 
 Pct Recovery = 40%  Analysis Date = 09/14/13 
 Pct Recovery = 40%  Analysis Date = 09/12/13 
 Pct Recovery = 41%  Analysis Date = 09/12/13 
 Pct Recovery = 41%  Analysis Date = 09/10/13 
 Pct Recovery = 41%  Analysis Date = 09/10/13 
 Pct Recovery = 41%  Analysis Date = 09/08/13 
 Pct Recovery = 42%  Analysis Date = 09/08/13 
 Pct Recovery = 42%  Analysis Date = 09/06/13 
 Pct Recovery = 42%  Analysis Date = 09/06/13 
 Pct Recovery = 42%  Analysis Date = 09/04/13 
 Pct Recovery = 43%  Analysis Date = 09/04/13 
 Pct Recovery = 43%  Analysis Date = 09/01/13 
 Pct Recovery = 43%  Analysis Date = 09/01/13 
 Pct Recovery = 43%  Analysis Date = 08/30/13 
 Pct Recovery = 44%  Analysis Date = 08/30/13 
 Pct Recovery = 44%  Analysis Date = 08/28/13 
 Pct Recovery = 44%  Analysis Date = 08/28/13 
 Pct Recovery = 44%  Analysis Date = 08/26/13 
 Pct Recovery = 45%  Analysis Date = 08/26/13 
 Pct Recovery = 45%  Analysis Date = 08/24/13 
 Pct Recovery = 45%  Analysis Date = 08/24/13 
 Pct Recovery = 45%  Analysis Date = 08/22/13 
 Pct Recovery = 45%  Analysis Date = 08/22/13 
 Pct Recovery = 45%  Analysis Date = 08/19/13 
 Pct Recovery = 45%  Analysis Date = 08/19/13 
 Pct Recovery = 45%  Analysis Date = 08/17/13 
 Pct Recovery = 45%  Analysis Date = 08/17/13 
 Pct Recovery = 45%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 45%  Analysis Date = 08/09/13 
 Pct Recovery = 45%  Analysis Date = 08/09/13 
 Pct Recovery = 45%  Analysis Date = 08/06/13 
 Pct Recovery = 45%  Analysis Date = 08/06/13 
 Pct Recovery = 45%  Analysis Date = 08/04/13 
 Pct Recovery = 45%  Analysis Date = 08/04/13 
 Pct Recovery = 45%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 07/31/13 
 Pct Recovery = 46%  Analysis Date = 07/31/13 
 Pct Recovery = 46%  Analysis Date = 07/29/13 
 Pct Recovery = 46%  Analysis Date = 07/29/13 
 Pct Recovery = 46%  Analysis Date = 07/27/13 
 Pct Recovery = 46%  Analysis Date = 07/27/13 
 Pct Recovery = 46%  Analysis Date = 07/24/13 
 Pct Recovery = 46%  Analysis Date = 07/24/13 
 Pct Recovery = 46%  Analysis Date = 07/22/13 
 Pct Recovery = 46%  Analysis Date = 07/22/13 
 Pct Recovery = 46%  Analysis Date = 07/20/13 
 Pct Recovery = 46%  Analysis Date = 07/20/13 
 Pct Recovery = 46%  Analysis Date = 07/18/13 
 Pct Recovery = 46%  Analysis Date = 07/18/13 
 Pct Recovery = 46%  Analysis Date = 07/16/13 
 Pct Recovery = 46%  Analysis Date = 07/16/13 
 Pct Recovery = 46%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/12/13 
 Pct Recovery = 46%  Analysis Date = 07/12/13 
 Pct Recovery = 46%  Analysis Date = 07/09/13 
 Pct Recovery = 46%  Analysis Date = 07/09/13 
 Pct Recovery = 46%  Analysis Date = 07/07/13 
 Pct Recovery = 47%  Analysis Date = 07/07/13 
 Pct Recovery = 47%  Analysis Date = 07/05/13 
 Pct Recovery = 47%  Analysis Date = 07/05/13 
 Pct Recovery = 47%  Analysis Date = 07/03/13 
 Pct Recovery = 47%  Analysis Date = 07/03/13 
 Pct Recovery = 47%  Analysis Date = 07/01/13 
 Pct Recovery = 47%  Analysis Date = 07/01/13 
 Pct Recovery = 47%  Analysis Date = 06/29/13 
 Pct Recovery = 47%  Analysis Date = 06/29/13 
 Pct Recovery = 47%  Analysis Date = 06/26/13 
 Pct Recovery = 47%  Analysis Date = 06/26/13 
 Pct Recovery = 47%  Analysis Date = 06/24/13 
 Pct Recovery = 47%  Analysis Date = 06/24/13 
 Pct Recovery = 47%  Analysis Date = 06/22/13 
 Pct Recovery = 47%  Analysis Date = 06/22/13 
 Pct Recovery = 47%  Analysis Date = 06/20/13 
 Pct Recovery = 47%  Analysis Date = 06/20/13 
 Pct Recovery = 47%  Analysis Date = 06/18/13 
 Pct Recovery = 47%  Analysis Date = 06/18/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/16/13 
 Pct Recovery = 47%  Analysis Date = 06/13/13 
 Pct Recovery = 48%  Analysis Date = 06/13/13 
 Pct Recovery = 48%  Analysis Date = 06/11/13 
 Pct Recovery = 48%  Analysis Date = 06/11/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/07/13 
 Pct Recovery = 48%  Analysis Date = 06/07/13 
 Pct Recovery = 48%  Analysis Date = 06/05/13 
 Pct Recovery = 48%  Analysis Date = 06/05/13 
 Pct Recovery = 48%  Analysis Date = 06/03/13 
 Pct Recovery = 48%  Analysis Date = 06/03/13 
 Pct Recovery = 48%  Analysis Date = 05/31/13 
 Pct Recovery = 48%  Analysis Date = 05/31/13 
 Pct Recovery = 48%  Analysis Date = 05/29/13 
 Pct Recovery = 48%  Analysis Date = 05/29/13 
 Pct Recovery = 48%  Analysis Date = 05/27/13 
 Pct Recovery = 48%  Analysis Date = 05/27/13 
 Pct Recovery = 48%  Analysis Date = 05/25/13 
 Pct Recovery = 48%  Analysis Date = 05/25/13 
 Pct Recovery = 48%  Analysis Date = 05/23/13 
 Pct Recovery = 48%  Analysis Date = 05/23/13 
 Pct Recovery = 48%  Analysis Date = 05/21/13 
 Pct Recovery = 48%  Analysis Date = 05/21/13 
 Pct Recovery = 48%  Analysis Date = 05/18/13 
 Pct Recovery = 49%  Analysis Date = 05/18/13 
 Pct Recovery = 49%  Analysis Date = 05/16/13 
 Pct Recovery = 49%  Analysis Date = 05/16/13 
 Pct Recovery = 49%  Analysis Date = 05/14/13 
 Pct Recovery = 49%  Analysis Date = 05/14/13 
 Pct Recovery = 49%  Analysis Date = 05/12/13 
 Pct Recovery = 49%  Analysis Date = 05/12/13 
 Pct Recovery = 49%  Analysis Date = 05/10/13 
 Pct Recovery = 49%  Analysis Date = 05/10/13 
 Pct Recovery = 49%  Analysis Date = 05/08/13 
 Pct Recovery = 49%  Analysis Date = 05/08/13 
 Pct Recovery = 49%  Analysis Date = 05/05/13 
 Pct Recovery = 49%  Analysis Date = 05/05/13 
 Pct Recovery = 49%  Analysis Date = 05/03/13 
 Pct Recovery = 49%  Analysis Date = 05/03/13 
 Pct Recovery = 49%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 04/29/13 
 Pct Recovery = 50%  Analysis Date = 04/29/13 
 Pct Recovery = 50%  Analysis Date = 04/27/13 
 Pct Recovery = 51%  Analysis Date = 04/27/13 
 Pct Recovery = 51%  Analysis Date = 04/25/13 
 Pct Recovery = 51%  Analysis Date = 04/25/13 
 Pct Recovery = 51%  Analysis Date = 04/22/13 
 Pct Recovery = 52%  Analysis Date = 04/22/13 
 Pct Recovery = 52%  Analysis Date = 04/20/13 
 Pct Recovery = 52%  Analysis Date = 04/20/13 
 Pct Recovery = 52%  Analysis Date = 04/18/13 
 Pct Recovery = 53%  Analysis Date = 04/18/13 
 Pct Recovery = 53%  Analysis Date = 04/16/13 
 Pct Recovery = 53%  Analysis Date = 04/16/13 
 Pct Recovery = 53%  Analysis Date = 04/14/13 
 Pct Recovery = 54%  Analysis Date = 04/14/13 
 Pct Recovery = 54%  Analysis Date = 04/12/13 
 Pct Recovery = 54%  Analysis Date = 04/12/13 
 Pct Recovery = 54%  Analysis Date = 04/09/13 
 Pct Recovery = 55%  Analysis Date = 04/09/13 
 Pct Recovery = 55%  Analysis Date = 04/07/13 
 Pct Recovery = 56%  Analysis Date = 04/07/13 
 Pct Recovery = 56%  Analysis Date = 04/05/13 
 Pct Recovery = 56%  Analysis Date = 04/05/13 
 Pct Recovery = 56%  Analysis Date = 04/03/13 
 Pct Recovery = 57%  Analysis Date = 04/03/13 
 Pct Recovery = 57%  Analysis Date = 04/01/13 
 Pct Recovery = 57%  Analysis Date = 04/01/13 
 Pct Recovery = 57%  Analysis Date = 03/30/13 
 Pct Recovery = 58%  Analysis Date = 03/30/13 
 Pct Recovery = 58%  Analysis Date = 03/27/13 
 Pct Recovery = 58%  Analysis Date = 03/27/13 
 Pct Recovery = 58%  Analysis Date = 03/25/13 
 Pct Recovery = 59%  Analysis Date = 03/25/13 
 Pct Recovery = 59%  Analysis Date = 03/23/13 
 Pct Recovery = 59%  Analysis Date = 03/23/13 
 Pct Recovery = 59%  Analysis Date = 03/21/13 
 Pct Recovery = 60%  Analysis Date = 03/21/13 
 Pct Recovery = 60%  Analysis Date = 03/19/13 
 Pct Recovery = 61%  Analysis Date = 03/19/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/14/13 
 Pct Recovery = 62%  Analysis Date = 03/14/13 
 Pct Recovery = 62%  Analysis Date = 03/12/13 
 Pct Recovery = 62%  Analysis Date = 03/12/13 
 Pct Recovery = 62%  Analysis Date = 03/10/13 
 Pct Recovery = 63%  Analysis Date = 03/10/13 
 Pct Recovery = 63%  Analysis Date = 03/08/13 
 Pct Recovery = 63%  Analysis Date = 03/08/13 
 Pct Recovery = 63%  Analysis Date = 03/06/13 
 Pct Recovery = 64%  Analysis Date = 03/06/13 
 Pct Recovery = 64%  Analysis Date = 03/04/13 
 Pct Recovery = 64%  Analysis Date = 03/04/13 
 Pct Recovery = 64%  Analysis Date = 03/01/13 
 Pct Recovery = 65%  Analysis Date = 03/01/13 
 Pct Recovery = 65%  Analysis Date = 02/27/13 
 Pct Recovery = 65%  Analysis Date = 02/27/13 
 Pct Recovery = 65%  Analysis Date = 02/25/13 
 Pct Recovery = 66%  Analysis Date = 02/25/13 
 Pct Recovery = 66%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/21/13 
 Pct Recovery = 67%  Analysis Date = 02/21/13 
 Pct Recovery = 67%  Analysis Date = 02/19/13 
 Pct Recovery = 68%  Analysis Date = 02/19/13 
 Pct Recovery = 68%  Analysis Date = 02/16/13 
 Pct Recovery = 68%  Analysis Date = 02/16/13 
 Pct Recovery = 68%  Analysis Date = 02/14/13 
 Pct Recovery = 69%  Analysis Date = 02/14/13 
 Pct Recovery = 69%  Analysis Date = 02/12/13 
 Pct Recovery = 69%  Analysis Date = 02/12/13 
 Pct Recovery = 69%  Analysis Date = 02/10/13 
 Pct Recovery = 70%  Analysis Date = 02/10/13 
 Pct Recovery = 70%  Analysis Date = 02/08/13 
 Pct Recovery = 70%  Analysis Date = 02/08/13 
 Pct Recovery = 70%  Analysis Date = 02/06/13 
 Pct Recovery = 71%  Analysis Date = 02/06/13 
 Pct Recovery = 71%  Analysis Date = 02/03/13 
 Pct Recovery = 71%  Analysis Date = 02/03/13 
 Pct Recovery = 71%  Analysis Date = 02/01/13 
 Pct Recovery = 72%  Analysis Date = 02/01/13 
 Pct Recovery = 72%  Analysis Date = 01/30/13 
 Pct Recovery = 73%  Analysis Date = 01/30/13 
 Pct Recovery = 73%  Analysis Date = 01/28/13 
 Pct Recovery = 73%  Analysis Date = 01/28/13 
 Pct Recovery = 73%  Analysis Date = 01/26/13 
 Pct Recovery = 74%  Analysis Date = 01/26/13 
 Pct Recovery = 74%  Analysis Date = 01/24/13 
 Pct Recovery = 74%  Analysis Date = 01/24/13 
 Pct Recovery = 74%  Analysis Date = 01/21/13 
 Pct Recovery = 73%  Analysis Date = 01/21/13 
 Pct Recovery = 73%  Analysis Date = 01/19/13 
 Pct Recovery = 72%  Analysis Date = 01/19/13 
 Pct Recovery = 72%  Analysis Date = 01/17/13 
 Pct Recovery = 72%  Analysis Date = 01/17/13 
 Pct Recovery = 72%  Analysis Date = 01/15/13 
 Pct Recovery = 71%  Analysis Date = 01/15/13 
 Pct Recovery = 71%  Analysis Date = 01/13/13 
 Pct Recovery = 70%  Analysis Date = 01/13/13 
 Pct Recovery = 70%  Analysis Date = 01/11/13 
 Pct Recovery = 69%  Analysis Date = 01/11/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 68%  Analysis Date = 01/08/13 
 Pct Recovery = 68%  Analysis Date = 01/06/13 
 Pct Recovery = 67%  Analysis Date = 01/06/13 
 Pct Recovery = 67%  Analysis Date = 01/04/13 
 Pct Recovery = 66%  Analysis Date = 01/04/13 
 Pct Recovery = 66%  Analysis Date = 01/02/13 
 Pct Recovery = 65%  Analysis Date = 01/02/13 
 Pct Recovery = 65%  Analysis Date = 12/31/12 
 Pct Recovery = 64%  Analysis Date = 12/31/12 
 Pct Recovery = 64%  Analysis Date = 12/29/12 
 Pct Recovery = 63%  Analysis Date = 12/29/12 
 Pct Recovery = 63%  Analysis Date = 12/26/12 
 Pct Recovery = 63%  Analysis Date = 12/26/12 
 Pct Recovery = 63%  Analysis Date = 12/24/12 
 Pct Recovery = 62%  Analysis Date = 12/24/12 
 Pct Recovery = 62%  Analysis Date = 12/22/12 
 Pct Recovery = 61%  Analysis Date = 12/22/12 
 Pct Recovery = 61%  Analysis Date = 12/20/12 
 Pct Recovery = 60%  Analysis Date = 12/20/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/14/12 
 Pct Recovery = 57%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
EZETIMIBE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 8 50% 20% 50% 14%
Total 8 50% 20% 50% 14%

Sample Statistics
EZETIMIBE

Characteristic N % % Basis
Plotted 8 73% Spiked
Estimated Values 8 73% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 3 27% 3 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
FADROZOLE
METHOD: LC9017 , TESTIDCODE: 68012LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 51%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 72%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 76%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 53%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 84%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 72%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 75%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 51%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 58%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 77%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 68%  Analysis Date = 03/21/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 68%  Analysis Date = 03/14/14 
 Pct Recovery = 67%  Analysis Date = 03/14/14 
 Pct Recovery = 67%  Analysis Date = 03/11/14 
 Pct Recovery = 67%  Analysis Date = 03/11/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 02/28/14 
 Pct Recovery = 66%  Analysis Date = 02/28/14 
 Pct Recovery = 66%  Analysis Date = 02/25/14 
 Pct Recovery = 65%  Analysis Date = 02/25/14 
 Pct Recovery = 65%  Analysis Date = 02/23/14 
 Pct Recovery = 65%  Analysis Date = 02/23/14 
 Pct Recovery = 65%  Analysis Date = 02/21/14 
 Pct Recovery = 65%  Analysis Date = 02/21/14 
 Pct Recovery = 65%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/16/14 
 Pct Recovery = 64%  Analysis Date = 02/16/14 
 Pct Recovery = 64%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/14/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/12/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/09/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/05/14 
 Pct Recovery = 63%  Analysis Date = 02/05/14 
 Pct Recovery = 63%  Analysis Date = 02/02/14 
 Pct Recovery = 63%  Analysis Date = 02/02/14 
 Pct Recovery = 63%  Analysis Date = 01/31/14 
 Pct Recovery = 63%  Analysis Date = 01/31/14 
 Pct Recovery = 63%  Analysis Date = 01/29/14 
 Pct Recovery = 63%  Analysis Date = 01/29/14 
 Pct Recovery = 63%  Analysis Date = 01/26/14 
 Pct Recovery = 63%  Analysis Date = 01/26/14 
 Pct Recovery = 63%  Analysis Date = 01/24/14 
 Pct Recovery = 62%  Analysis Date = 01/24/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/19/14 
 Pct Recovery = 62%  Analysis Date = 01/19/14 
 Pct Recovery = 62%  Analysis Date = 01/17/14 
 Pct Recovery = 62%  Analysis Date = 01/17/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/10/14 
 Pct Recovery = 61%  Analysis Date = 01/10/14 
 Pct Recovery = 61%  Analysis Date = 01/08/14 
 Pct Recovery = 61%  Analysis Date = 01/08/14 
 Pct Recovery = 61%  Analysis Date = 01/06/14 
 Pct Recovery = 61%  Analysis Date = 01/06/14 
 Pct Recovery = 61%  Analysis Date = 01/03/14 
 Pct Recovery = 61%  Analysis Date = 01/03/14 
 Pct Recovery = 61%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/27/13 
 Pct Recovery = 60%  Analysis Date = 12/27/13 
 Pct Recovery = 60%  Analysis Date = 12/25/13 
 Pct Recovery = 60%  Analysis Date = 12/25/13 
 Pct Recovery = 60%  Analysis Date = 12/23/13 
 Pct Recovery = 60%  Analysis Date = 12/23/13 
 Pct Recovery = 60%  Analysis Date = 12/20/13 
 Pct Recovery = 60%  Analysis Date = 12/20/13 
 Pct Recovery = 60%  Analysis Date = 12/18/13 
 Pct Recovery = 59%  Analysis Date = 12/18/13 
 Pct Recovery = 59%  Analysis Date = 12/16/13 
 Pct Recovery = 59%  Analysis Date = 12/16/13 
 Pct Recovery = 59%  Analysis Date = 12/13/13 
 Pct Recovery = 59%  Analysis Date = 12/13/13 
 Pct Recovery = 59%  Analysis Date = 12/11/13 
 Pct Recovery = 59%  Analysis Date = 12/11/13 
 Pct Recovery = 59%  Analysis Date = 12/09/13 
 Pct Recovery = 59%  Analysis Date = 12/09/13 
 Pct Recovery = 59%  Analysis Date = 12/07/13 
 Pct Recovery = 59%  Analysis Date = 12/07/13 
 Pct Recovery = 59%  Analysis Date = 12/04/13 
 Pct Recovery = 58%  Analysis Date = 12/04/13 
 Pct Recovery = 58%  Analysis Date = 12/02/13 
 Pct Recovery = 59%  Analysis Date = 12/02/13 
 Pct Recovery = 59%  Analysis Date = 11/30/13 
 Pct Recovery = 59%  Analysis Date = 11/30/13 
 Pct Recovery = 59%  Analysis Date = 11/27/13 
 Pct Recovery = 59%  Analysis Date = 11/27/13 
 Pct Recovery = 59%  Analysis Date = 11/25/13 
 Pct Recovery = 59%  Analysis Date = 11/25/13 
 Pct Recovery = 59%  Analysis Date = 11/23/13 
 Pct Recovery = 59%  Analysis Date = 11/23/13 
 Pct Recovery = 59%  Analysis Date = 11/20/13 
 Pct Recovery = 59%  Analysis Date = 11/20/13 
 Pct Recovery = 59%  Analysis Date = 11/18/13 
 Pct Recovery = 60%  Analysis Date = 11/18/13 
 Pct Recovery = 60%  Analysis Date = 11/16/13 
 Pct Recovery = 60%  Analysis Date = 11/16/13 
 Pct Recovery = 60%  Analysis Date = 11/13/13 
 Pct Recovery = 60%  Analysis Date = 11/13/13 
 Pct Recovery = 60%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/07/13 
 Pct Recovery = 60%  Analysis Date = 11/07/13 
 Pct Recovery = 60%  Analysis Date = 11/04/13 
 Pct Recovery = 61%  Analysis Date = 11/04/13 
 Pct Recovery = 61%  Analysis Date = 11/02/13 
 Pct Recovery = 61%  Analysis Date = 11/02/13 
 Pct Recovery = 61%  Analysis Date = 10/31/13 
 Pct Recovery = 61%  Analysis Date = 10/31/13 
 Pct Recovery = 61%  Analysis Date = 10/28/13 
 Pct Recovery = 61%  Analysis Date = 10/28/13 
 Pct Recovery = 61%  Analysis Date = 10/26/13 
 Pct Recovery = 61%  Analysis Date = 10/26/13 
 Pct Recovery = 61%  Analysis Date = 10/24/13 
 Pct Recovery = 61%  Analysis Date = 10/24/13 
 Pct Recovery = 61%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/19/13 
 Pct Recovery = 62%  Analysis Date = 10/19/13 
 Pct Recovery = 62%  Analysis Date = 10/17/13 
 Pct Recovery = 62%  Analysis Date = 10/17/13 
 Pct Recovery = 62%  Analysis Date = 10/14/13 
 Pct Recovery = 62%  Analysis Date = 10/14/13 
 Pct Recovery = 62%  Analysis Date = 10/12/13 
 Pct Recovery = 62%  Analysis Date = 10/12/13 
 Pct Recovery = 62%  Analysis Date = 10/10/13 
 Pct Recovery = 62%  Analysis Date = 10/10/13 
 Pct Recovery = 62%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/17/13 
 Pct Recovery = 64%  Analysis Date = 09/17/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/10/13 
 Pct Recovery = 65%  Analysis Date = 09/10/13 
 Pct Recovery = 65%  Analysis Date = 09/07/13 
 Pct Recovery = 65%  Analysis Date = 09/07/13 
 Pct Recovery = 65%  Analysis Date = 09/05/13 
 Pct Recovery = 65%  Analysis Date = 09/05/13 
 Pct Recovery = 65%  Analysis Date = 09/03/13 
 Pct Recovery = 65%  Analysis Date = 09/03/13 
 Pct Recovery = 65%  Analysis Date = 09/01/13 
 Pct Recovery = 65%  Analysis Date = 09/01/13 
 Pct Recovery = 65%  Analysis Date = 08/29/13 
 Pct Recovery = 66%  Analysis Date = 08/29/13 
 Pct Recovery = 66%  Analysis Date = 08/27/13 
 Pct Recovery = 66%  Analysis Date = 08/27/13 
 Pct Recovery = 66%  Analysis Date = 08/25/13 
 Pct Recovery = 66%  Analysis Date = 08/25/13 
 Pct Recovery = 66%  Analysis Date = 08/22/13 
 Pct Recovery = 66%  Analysis Date = 08/22/13 
 Pct Recovery = 66%  Analysis Date = 08/20/13 
 Pct Recovery = 67%  Analysis Date = 08/20/13 
 Pct Recovery = 67%  Analysis Date = 08/18/13 
 Pct Recovery = 67%  Analysis Date = 08/18/13 
 Pct Recovery = 67%  Analysis Date = 08/15/13 
 Pct Recovery = 67%  Analysis Date = 08/15/13 
 Pct Recovery = 67%  Analysis Date = 08/13/13 
 Pct Recovery = 67%  Analysis Date = 08/13/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/08/13 
 Pct Recovery = 67%  Analysis Date = 08/08/13 
 Pct Recovery = 67%  Analysis Date = 08/06/13 
 Pct Recovery = 67%  Analysis Date = 08/06/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/23/13 
 Pct Recovery = 68%  Analysis Date = 07/23/13 
 Pct Recovery = 68%  Analysis Date = 07/21/13 
 Pct Recovery = 68%  Analysis Date = 07/21/13 
 Pct Recovery = 68%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/16/13 
 Pct Recovery = 68%  Analysis Date = 07/16/13 
 Pct Recovery = 68%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 68%  Analysis Date = 07/07/13 
 Pct Recovery = 68%  Analysis Date = 07/07/13 
 Pct Recovery = 68%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/21/13 
 Pct Recovery = 68%  Analysis Date = 06/21/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/16/13 
 Pct Recovery = 68%  Analysis Date = 06/14/13 
 Pct Recovery = 68%  Analysis Date = 06/14/13 
 Pct Recovery = 68%  Analysis Date = 06/12/13 
 Pct Recovery = 68%  Analysis Date = 06/12/13 
 Pct Recovery = 68%  Analysis Date = 06/09/13 
 Pct Recovery = 68%  Analysis Date = 06/09/13 
 Pct Recovery = 68%  Analysis Date = 06/07/13 
 Pct Recovery = 68%  Analysis Date = 06/07/13 
 Pct Recovery = 68%  Analysis Date = 06/05/13 
 Pct Recovery = 68%  Analysis Date = 06/05/13 
 Pct Recovery = 68%  Analysis Date = 06/02/13 
 Pct Recovery = 68%  Analysis Date = 06/02/13 
 Pct Recovery = 68%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/24/13 
 Pct Recovery = 68%  Analysis Date = 05/24/13 
 Pct Recovery = 68%  Analysis Date = 05/22/13 
 Pct Recovery = 68%  Analysis Date = 05/22/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/20/13 
 Pct Recovery = 69%  Analysis Date = 04/20/13 
 Pct Recovery = 69%  Analysis Date = 04/17/13 
 Pct Recovery = 69%  Analysis Date = 04/17/13 
 Pct Recovery = 69%  Analysis Date = 04/15/13 
 Pct Recovery = 69%  Analysis Date = 04/15/13 
 Pct Recovery = 69%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/10/13 
 Pct Recovery = 70%  Analysis Date = 04/10/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/06/13 
 Pct Recovery = 70%  Analysis Date = 04/06/13 
 Pct Recovery = 70%  Analysis Date = 04/03/13 
 Pct Recovery = 70%  Analysis Date = 04/03/13 
 Pct Recovery = 70%  Analysis Date = 04/01/13 
 Pct Recovery = 70%  Analysis Date = 04/01/13 
 Pct Recovery = 70%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 Pct Recovery = 71%  Analysis Date = 03/25/13 
 Pct Recovery = 71%  Analysis Date = 03/25/13 
 Pct Recovery = 71%  Analysis Date = 03/23/13 
 Pct Recovery = 71%  Analysis Date = 03/23/13 
 Pct Recovery = 71%  Analysis Date = 03/21/13 
 Pct Recovery = 71%  Analysis Date = 03/21/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/16/13 
 Pct Recovery = 72%  Analysis Date = 03/16/13 
 Pct Recovery = 72%  Analysis Date = 03/14/13 
 Pct Recovery = 72%  Analysis Date = 03/14/13 
 Pct Recovery = 72%  Analysis Date = 03/11/13 
 Pct Recovery = 72%  Analysis Date = 03/11/13 
 Pct Recovery = 72%  Analysis Date = 03/09/13 
 Pct Recovery = 72%  Analysis Date = 03/09/13 
 Pct Recovery = 72%  Analysis Date = 03/07/13 
 Pct Recovery = 72%  Analysis Date = 03/07/13 
 Pct Recovery = 72%  Analysis Date = 03/04/13 
 Pct Recovery = 72%  Analysis Date = 03/04/13 
 Pct Recovery = 72%  Analysis Date = 03/02/13 
 Pct Recovery = 73%  Analysis Date = 03/02/13 
 Pct Recovery = 73%  Analysis Date = 02/28/13 
 Pct Recovery = 73%  Analysis Date = 02/28/13 
 Pct Recovery = 73%  Analysis Date = 02/25/13 
 Pct Recovery = 73%  Analysis Date = 02/25/13 
 Pct Recovery = 73%  Analysis Date = 02/23/13 
 Pct Recovery = 73%  Analysis Date = 02/23/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/18/13 
 Pct Recovery = 73%  Analysis Date = 02/18/13 
 Pct Recovery = 73%  Analysis Date = 02/16/13 
 Pct Recovery = 73%  Analysis Date = 02/16/13 
 Pct Recovery = 73%  Analysis Date = 02/14/13 
 Pct Recovery = 74%  Analysis Date = 02/14/13 
 Pct Recovery = 74%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/09/13 
 Pct Recovery = 74%  Analysis Date = 02/09/13 
 Pct Recovery = 74%  Analysis Date = 02/07/13 
 Pct Recovery = 74%  Analysis Date = 02/07/13 
 Pct Recovery = 74%  Analysis Date = 02/05/13 
 Pct Recovery = 74%  Analysis Date = 02/05/13 
 Pct Recovery = 74%  Analysis Date = 02/02/13 
 Pct Recovery = 74%  Analysis Date = 02/02/13 
 Pct Recovery = 74%  Analysis Date = 01/31/13 
 Pct Recovery = 74%  Analysis Date = 01/31/13 
 Pct Recovery = 74%  Analysis Date = 01/29/13 
 Pct Recovery = 75%  Analysis Date = 01/29/13 
 Pct Recovery = 75%  Analysis Date = 01/26/13 
 Pct Recovery = 75%  Analysis Date = 01/26/13 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 Pct Recovery = 75%  Analysis Date = 01/22/13 
 Pct Recovery = 75%  Analysis Date = 01/22/13 
 Pct Recovery = 75%  Analysis Date = 01/19/13 
 Pct Recovery = 75%  Analysis Date = 01/19/13 
 Pct Recovery = 75%  Analysis Date = 01/17/13 
 Pct Recovery = 75%  Analysis Date = 01/17/13 
 Pct Recovery = 75%  Analysis Date = 01/15/13 
 Pct Recovery = 75%  Analysis Date = 01/15/13 
 Pct Recovery = 75%  Analysis Date = 01/13/13 
 Pct Recovery = 76%  Analysis Date = 01/13/13 
 Pct Recovery = 76%  Analysis Date = 01/10/13 
 Pct Recovery = 76%  Analysis Date = 01/10/13 
 Pct Recovery = 76%  Analysis Date = 01/08/13 
 Pct Recovery = 76%  Analysis Date = 01/08/13 
 Pct Recovery = 76%  Analysis Date = 01/06/13 
 Pct Recovery = 76%  Analysis Date = 01/06/13 
 Pct Recovery = 76%  Analysis Date = 01/03/13 
 Pct Recovery = 76%  Analysis Date = 01/03/13 
 Pct Recovery = 76%  Analysis Date = 01/01/13 
 Pct Recovery = 76%  Analysis Date = 01/01/13 
 Pct Recovery = 76%  Analysis Date = 12/30/12 
 Pct Recovery = 76%  Analysis Date = 12/30/12 
 Pct Recovery = 76%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/27/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/25/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 77%  Analysis Date = 12/20/12 
 Pct Recovery = 77%  Analysis Date = 12/20/12 
 Pct Recovery = 77%  Analysis Date = 12/18/12 
 Pct Recovery = 77%  Analysis Date = 12/18/12 
 Pct Recovery = 77%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/14/12 
 Pct Recovery = 77%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FADROZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 68% . 68% 0%
>= Reporting Level 13 68% 11% 72% 13%
Total 14 68% 11% 71% 13%

Sample Statistics
FADROZOLE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
FAMOTIDINE
METHOD: LC9017 , TESTIDCODE: 68000LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 50%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 59%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 94%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 15%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 28%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 29%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 93%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 42%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 49%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 58%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 17%  Analysis Date = 03/21/14 
 Pct Recovery = 22%  Analysis Date = 03/18/14 
 Pct Recovery = 22%  Analysis Date = 03/18/14 
 Pct Recovery = 22%  Analysis Date = 03/16/14 
 Pct Recovery = 23%  Analysis Date = 03/16/14 
 Pct Recovery = 23%  Analysis Date = 03/14/14 
 Pct Recovery = 24%  Analysis Date = 03/14/14 
 Pct Recovery = 24%  Analysis Date = 03/11/14 
 Pct Recovery = 24%  Analysis Date = 03/11/14 
 Pct Recovery = 24%  Analysis Date = 03/09/14 
 Pct Recovery = 25%  Analysis Date = 03/09/14 
 Pct Recovery = 25%  Analysis Date = 03/07/14 
 Pct Recovery = 25%  Analysis Date = 03/07/14 
 Pct Recovery = 25%  Analysis Date = 03/04/14 
 Pct Recovery = 26%  Analysis Date = 03/04/14 
 Pct Recovery = 26%  Analysis Date = 03/02/14 
 Pct Recovery = 26%  Analysis Date = 03/02/14 
 Pct Recovery = 26%  Analysis Date = 02/28/14 
 Pct Recovery = 27%  Analysis Date = 02/28/14 
 Pct Recovery = 27%  Analysis Date = 02/25/14 
 Pct Recovery = 27%  Analysis Date = 02/25/14 
 Pct Recovery = 27%  Analysis Date = 02/23/14 
 Pct Recovery = 28%  Analysis Date = 02/23/14 
 Pct Recovery = 28%  Analysis Date = 02/21/14 
 Pct Recovery = 28%  Analysis Date = 02/21/14 
 Pct Recovery = 28%  Analysis Date = 02/18/14 
 Pct Recovery = 29%  Analysis Date = 02/18/14 
 Pct Recovery = 29%  Analysis Date = 02/16/14 
 Pct Recovery = 29%  Analysis Date = 02/16/14 
 Pct Recovery = 29%  Analysis Date = 02/14/14 
 Pct Recovery = 29%  Analysis Date = 02/14/14 
 Pct Recovery = 29%  Analysis Date = 02/12/14 
 Pct Recovery = 29%  Analysis Date = 02/12/14 
 Pct Recovery = 29%  Analysis Date = 02/09/14 
 Pct Recovery = 30%  Analysis Date = 02/09/14 
 Pct Recovery = 30%  Analysis Date = 02/07/14 
 Pct Recovery = 30%  Analysis Date = 02/07/14 
 Pct Recovery = 30%  Analysis Date = 02/05/14 
 Pct Recovery = 30%  Analysis Date = 02/05/14 
 Pct Recovery = 30%  Analysis Date = 02/02/14 
 Pct Recovery = 30%  Analysis Date = 02/02/14 
 Pct Recovery = 30%  Analysis Date = 01/31/14 
 Pct Recovery = 30%  Analysis Date = 01/31/14 
 Pct Recovery = 30%  Analysis Date = 01/29/14 
 Pct Recovery = 30%  Analysis Date = 01/29/14 
 Pct Recovery = 30%  Analysis Date = 01/26/14 
 Pct Recovery = 30%  Analysis Date = 01/26/14 
 Pct Recovery = 30%  Analysis Date = 01/24/14 
 Pct Recovery = 31%  Analysis Date = 01/24/14 
 Pct Recovery = 31%  Analysis Date = 01/22/14 
 Pct Recovery = 31%  Analysis Date = 01/22/14 
 Pct Recovery = 31%  Analysis Date = 01/19/14 
 Pct Recovery = 31%  Analysis Date = 01/19/14 
 Pct Recovery = 31%  Analysis Date = 01/17/14 
 Pct Recovery = 31%  Analysis Date = 01/17/14 
 Pct Recovery = 31%  Analysis Date = 01/15/14 
 Pct Recovery = 31%  Analysis Date = 01/15/14 
 Pct Recovery = 31%  Analysis Date = 01/13/14 
 Pct Recovery = 31%  Analysis Date = 01/13/14 
 Pct Recovery = 31%  Analysis Date = 01/10/14 
 Pct Recovery = 31%  Analysis Date = 01/10/14 
 Pct Recovery = 31%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/06/14 
 Pct Recovery = 32%  Analysis Date = 01/06/14 
 Pct Recovery = 32%  Analysis Date = 01/03/14 
 Pct Recovery = 32%  Analysis Date = 01/03/14 
 Pct Recovery = 32%  Analysis Date = 01/01/14 
 Pct Recovery = 32%  Analysis Date = 01/01/14 
 Pct Recovery = 32%  Analysis Date = 12/30/13 
 Pct Recovery = 32%  Analysis Date = 12/30/13 
 Pct Recovery = 32%  Analysis Date = 12/27/13 
 Pct Recovery = 32%  Analysis Date = 12/27/13 
 Pct Recovery = 32%  Analysis Date = 12/25/13 
 Pct Recovery = 33%  Analysis Date = 12/25/13 
 Pct Recovery = 33%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/20/13 
 Pct Recovery = 33%  Analysis Date = 12/20/13 
 Pct Recovery = 33%  Analysis Date = 12/18/13 
 Pct Recovery = 33%  Analysis Date = 12/18/13 
 Pct Recovery = 33%  Analysis Date = 12/16/13 
 Pct Recovery = 33%  Analysis Date = 12/16/13 
 Pct Recovery = 33%  Analysis Date = 12/13/13 
 Pct Recovery = 33%  Analysis Date = 12/13/13 
 Pct Recovery = 33%  Analysis Date = 12/11/13 
 Pct Recovery = 33%  Analysis Date = 12/11/13 
 Pct Recovery = 33%  Analysis Date = 12/09/13 
 Pct Recovery = 34%  Analysis Date = 12/09/13 
 Pct Recovery = 34%  Analysis Date = 12/07/13 
 Pct Recovery = 34%  Analysis Date = 12/07/13 
 Pct Recovery = 34%  Analysis Date = 12/04/13 
 Pct Recovery = 34%  Analysis Date = 12/04/13 
 Pct Recovery = 34%  Analysis Date = 12/02/13 
 Pct Recovery = 34%  Analysis Date = 12/02/13 
 Pct Recovery = 34%  Analysis Date = 11/30/13 
 Pct Recovery = 34%  Analysis Date = 11/30/13 
 Pct Recovery = 34%  Analysis Date = 11/27/13 
 Pct Recovery = 34%  Analysis Date = 11/27/13 
 Pct Recovery = 34%  Analysis Date = 11/25/13 
 Pct Recovery = 35%  Analysis Date = 11/25/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/18/13 
 Pct Recovery = 35%  Analysis Date = 11/18/13 
 Pct Recovery = 35%  Analysis Date = 11/16/13 
 Pct Recovery = 35%  Analysis Date = 11/16/13 
 Pct Recovery = 35%  Analysis Date = 11/13/13 
 Pct Recovery = 35%  Analysis Date = 11/13/13 
 Pct Recovery = 35%  Analysis Date = 11/11/13 
 Pct Recovery = 35%  Analysis Date = 11/11/13 
 Pct Recovery = 35%  Analysis Date = 11/09/13 
 Pct Recovery = 36%  Analysis Date = 11/09/13 
 Pct Recovery = 36%  Analysis Date = 11/07/13 
 Pct Recovery = 36%  Analysis Date = 11/07/13 
 Pct Recovery = 36%  Analysis Date = 11/04/13 
 Pct Recovery = 36%  Analysis Date = 11/04/13 
 Pct Recovery = 36%  Analysis Date = 11/02/13 
 Pct Recovery = 36%  Analysis Date = 11/02/13 
 Pct Recovery = 36%  Analysis Date = 10/31/13 
 Pct Recovery = 36%  Analysis Date = 10/31/13 
 Pct Recovery = 36%  Analysis Date = 10/28/13 
 Pct Recovery = 36%  Analysis Date = 10/28/13 
 Pct Recovery = 36%  Analysis Date = 10/26/13 
 Pct Recovery = 36%  Analysis Date = 10/26/13 
 Pct Recovery = 36%  Analysis Date = 10/24/13 
 Pct Recovery = 37%  Analysis Date = 10/24/13 
 Pct Recovery = 37%  Analysis Date = 10/21/13 
 Pct Recovery = 37%  Analysis Date = 10/21/13 
 Pct Recovery = 37%  Analysis Date = 10/19/13 
 Pct Recovery = 37%  Analysis Date = 10/19/13 
 Pct Recovery = 37%  Analysis Date = 10/17/13 
 Pct Recovery = 37%  Analysis Date = 10/17/13 
 Pct Recovery = 37%  Analysis Date = 10/14/13 
 Pct Recovery = 37%  Analysis Date = 10/14/13 
 Pct Recovery = 37%  Analysis Date = 10/12/13 
 Pct Recovery = 37%  Analysis Date = 10/12/13 
 Pct Recovery = 37%  Analysis Date = 10/10/13 
 Pct Recovery = 38%  Analysis Date = 10/10/13 
 Pct Recovery = 38%  Analysis Date = 10/07/13 
 Pct Recovery = 38%  Analysis Date = 10/07/13 
 Pct Recovery = 38%  Analysis Date = 10/05/13 
 Pct Recovery = 38%  Analysis Date = 10/05/13 
 Pct Recovery = 38%  Analysis Date = 10/03/13 
 Pct Recovery = 38%  Analysis Date = 10/03/13 
 Pct Recovery = 38%  Analysis Date = 10/01/13 
 Pct Recovery = 38%  Analysis Date = 10/01/13 
 Pct Recovery = 38%  Analysis Date = 09/28/13 
 Pct Recovery = 38%  Analysis Date = 09/28/13 
 Pct Recovery = 38%  Analysis Date = 09/26/13 
 Pct Recovery = 38%  Analysis Date = 09/26/13 
 Pct Recovery = 38%  Analysis Date = 09/24/13 
 Pct Recovery = 39%  Analysis Date = 09/24/13 
 Pct Recovery = 39%  Analysis Date = 09/21/13 
 Pct Recovery = 39%  Analysis Date = 09/21/13 
 Pct Recovery = 39%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/14/13 
 Pct Recovery = 39%  Analysis Date = 09/14/13 
 Pct Recovery = 39%  Analysis Date = 09/12/13 
 Pct Recovery = 39%  Analysis Date = 09/12/13 
 Pct Recovery = 39%  Analysis Date = 09/10/13 
 Pct Recovery = 40%  Analysis Date = 09/10/13 
 Pct Recovery = 40%  Analysis Date = 09/07/13 
 Pct Recovery = 40%  Analysis Date = 09/07/13 
 Pct Recovery = 40%  Analysis Date = 09/05/13 
 Pct Recovery = 40%  Analysis Date = 09/05/13 
 Pct Recovery = 40%  Analysis Date = 09/03/13 
 Pct Recovery = 40%  Analysis Date = 09/03/13 
 Pct Recovery = 40%  Analysis Date = 09/01/13 
 Pct Recovery = 40%  Analysis Date = 09/01/13 
 Pct Recovery = 40%  Analysis Date = 08/29/13 
 Pct Recovery = 40%  Analysis Date = 08/29/13 
 Pct Recovery = 40%  Analysis Date = 08/27/13 
 Pct Recovery = 41%  Analysis Date = 08/27/13 
 Pct Recovery = 41%  Analysis Date = 08/25/13 
 Pct Recovery = 42%  Analysis Date = 08/25/13 
 Pct Recovery = 42%  Analysis Date = 08/22/13 
 Pct Recovery = 42%  Analysis Date = 08/22/13 
 Pct Recovery = 42%  Analysis Date = 08/20/13 
 Pct Recovery = 43%  Analysis Date = 08/20/13 
 Pct Recovery = 43%  Analysis Date = 08/18/13 
 Pct Recovery = 44%  Analysis Date = 08/18/13 
 Pct Recovery = 44%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/06/13 
 Pct Recovery = 48%  Analysis Date = 08/06/13 
 Pct Recovery = 48%  Analysis Date = 08/04/13 
 Pct Recovery = 48%  Analysis Date = 08/04/13 
 Pct Recovery = 48%  Analysis Date = 08/02/13 
 Pct Recovery = 49%  Analysis Date = 08/02/13 
 Pct Recovery = 49%  Analysis Date = 07/30/13 
 Pct Recovery = 50%  Analysis Date = 07/30/13 
 Pct Recovery = 50%  Analysis Date = 07/28/13 
 Pct Recovery = 51%  Analysis Date = 07/28/13 
 Pct Recovery = 51%  Analysis Date = 07/26/13 
 Pct Recovery = 51%  Analysis Date = 07/26/13 
 Pct Recovery = 51%  Analysis Date = 07/23/13 
 Pct Recovery = 52%  Analysis Date = 07/23/13 
 Pct Recovery = 52%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/16/13 
 Pct Recovery = 54%  Analysis Date = 07/16/13 
 Pct Recovery = 54%  Analysis Date = 07/14/13 
 Pct Recovery = 55%  Analysis Date = 07/14/13 
 Pct Recovery = 55%  Analysis Date = 07/12/13 
 Pct Recovery = 55%  Analysis Date = 07/12/13 
 Pct Recovery = 55%  Analysis Date = 07/09/13 
 Pct Recovery = 56%  Analysis Date = 07/09/13 
 Pct Recovery = 56%  Analysis Date = 07/07/13 
 Pct Recovery = 57%  Analysis Date = 07/07/13 
 Pct Recovery = 57%  Analysis Date = 07/05/13 
 Pct Recovery = 57%  Analysis Date = 07/05/13 
 Pct Recovery = 57%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/26/13 
 Pct Recovery = 60%  Analysis Date = 06/26/13 
 Pct Recovery = 60%  Analysis Date = 06/23/13 
 Pct Recovery = 61%  Analysis Date = 06/23/13 
 Pct Recovery = 61%  Analysis Date = 06/21/13 
 Pct Recovery = 61%  Analysis Date = 06/21/13 
 Pct Recovery = 61%  Analysis Date = 06/19/13 
 Pct Recovery = 62%  Analysis Date = 06/19/13 
 Pct Recovery = 62%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/12/13 
 Pct Recovery = 64%  Analysis Date = 06/12/13 
 Pct Recovery = 64%  Analysis Date = 06/09/13 
 Pct Recovery = 65%  Analysis Date = 06/09/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 66%  Analysis Date = 06/05/13 
 Pct Recovery = 66%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/22/13 
 Pct Recovery = 70%  Analysis Date = 05/22/13 
 Pct Recovery = 70%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/15/13 
 Pct Recovery = 72%  Analysis Date = 05/15/13 
 Pct Recovery = 72%  Analysis Date = 05/13/13 
 Pct Recovery = 73%  Analysis Date = 05/13/13 
 Pct Recovery = 73%  Analysis Date = 05/10/13 
 Pct Recovery = 73%  Analysis Date = 05/10/13 
 Pct Recovery = 73%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/20/13 
 Pct Recovery = 76%  Analysis Date = 04/20/13 
 Pct Recovery = 76%  Analysis Date = 04/17/13 
 Pct Recovery = 76%  Analysis Date = 04/17/13 
 Pct Recovery = 76%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 77%  Analysis Date = 04/06/13 
 Pct Recovery = 77%  Analysis Date = 04/06/13 
 Pct Recovery = 77%  Analysis Date = 04/03/13 
 Pct Recovery = 77%  Analysis Date = 04/03/13 
 Pct Recovery = 77%  Analysis Date = 04/01/13 
 Pct Recovery = 77%  Analysis Date = 04/01/13 
 Pct Recovery = 77%  Analysis Date = 03/30/13 
 Pct Recovery = 77%  Analysis Date = 03/30/13 
 Pct Recovery = 77%  Analysis Date = 03/27/13 
 Pct Recovery = 77%  Analysis Date = 03/27/13 
 Pct Recovery = 77%  Analysis Date = 03/25/13 
 Pct Recovery = 77%  Analysis Date = 03/25/13 
 Pct Recovery = 77%  Analysis Date = 03/23/13 
 Pct Recovery = 77%  Analysis Date = 03/23/13 
 Pct Recovery = 77%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/21/13 
 Pct Recovery = 76%  Analysis Date = 03/18/13 
 Pct Recovery = 76%  Analysis Date = 03/18/13 
 Pct Recovery = 76%  Analysis Date = 03/16/13 
 Pct Recovery = 76%  Analysis Date = 03/16/13 
 Pct Recovery = 76%  Analysis Date = 03/14/13 
 Pct Recovery = 75%  Analysis Date = 03/14/13 
 Pct Recovery = 75%  Analysis Date = 03/11/13 
 Pct Recovery = 75%  Analysis Date = 03/11/13 
 Pct Recovery = 75%  Analysis Date = 03/09/13 
 Pct Recovery = 75%  Analysis Date = 03/09/13 
 Pct Recovery = 75%  Analysis Date = 03/07/13 
 Pct Recovery = 74%  Analysis Date = 03/07/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 Pct Recovery = 74%  Analysis Date = 02/25/13 
 Pct Recovery = 73%  Analysis Date = 02/25/13 
 Pct Recovery = 73%  Analysis Date = 02/23/13 
 Pct Recovery = 73%  Analysis Date = 02/23/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/18/13 
 Pct Recovery = 72%  Analysis Date = 02/18/13 
 Pct Recovery = 72%  Analysis Date = 02/16/13 
 Pct Recovery = 72%  Analysis Date = 02/16/13 
 Pct Recovery = 72%  Analysis Date = 02/14/13 
 Pct Recovery = 72%  Analysis Date = 02/14/13 
 Pct Recovery = 72%  Analysis Date = 02/12/13 
 Pct Recovery = 71%  Analysis Date = 02/12/13 
 Pct Recovery = 71%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 70%  Analysis Date = 02/05/13 
 Pct Recovery = 70%  Analysis Date = 02/02/13 
 Pct Recovery = 70%  Analysis Date = 02/02/13 
 Pct Recovery = 70%  Analysis Date = 01/31/13 
 Pct Recovery = 70%  Analysis Date = 01/31/13 
 Pct Recovery = 70%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/26/13 
 Pct Recovery = 69%  Analysis Date = 01/26/13 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 Pct Recovery = 69%  Analysis Date = 01/22/13 
 Pct Recovery = 68%  Analysis Date = 01/22/13 
 Pct Recovery = 68%  Analysis Date = 01/19/13 
 Pct Recovery = 68%  Analysis Date = 01/19/13 
 Pct Recovery = 68%  Analysis Date = 01/17/13 
 Pct Recovery = 68%  Analysis Date = 01/17/13 
 Pct Recovery = 68%  Analysis Date = 01/15/13 
 Pct Recovery = 67%  Analysis Date = 01/15/13 
 Pct Recovery = 67%  Analysis Date = 01/13/13 
 Pct Recovery = 67%  Analysis Date = 01/13/13 
 Pct Recovery = 67%  Analysis Date = 01/10/13 
 Pct Recovery = 67%  Analysis Date = 01/10/13 
 Pct Recovery = 67%  Analysis Date = 01/08/13 
 Pct Recovery = 66%  Analysis Date = 01/08/13 
 Pct Recovery = 66%  Analysis Date = 01/06/13 
 Pct Recovery = 66%  Analysis Date = 01/06/13 
 Pct Recovery = 66%  Analysis Date = 01/03/13 
 Pct Recovery = 66%  Analysis Date = 01/03/13 
 Pct Recovery = 66%  Analysis Date = 01/01/13 
 Pct Recovery = 65%  Analysis Date = 01/01/13 
 Pct Recovery = 65%  Analysis Date = 12/30/12 
 Pct Recovery = 65%  Analysis Date = 12/30/12 
 Pct Recovery = 65%  Analysis Date = 12/27/12 
 Pct Recovery = 65%  Analysis Date = 12/27/12 
 Pct Recovery = 65%  Analysis Date = 12/25/12 
 Pct Recovery = 64%  Analysis Date = 12/25/12 
 Pct Recovery = 64%  Analysis Date = 12/23/12 
 Pct Recovery = 64%  Analysis Date = 12/23/12 
 Pct Recovery = 64%  Analysis Date = 12/20/12 
 Pct Recovery = 64%  Analysis Date = 12/20/12 
 Pct Recovery = 64%  Analysis Date = 12/18/12 
 Pct Recovery = 63%  Analysis Date = 12/18/12 
 Pct Recovery = 63%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/16/12 
 Pct Recovery = 63%  Analysis Date = 12/14/12 
 Pct Recovery = 63%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FAMOTIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 49% 27% 49% 24%
Total 11 49% 27% 49% 24%

Sample Statistics
FAMOTIDINE

Characteristic N % % Basis
Plotted 11 73% Spiked
Estimated Values 11 73% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 4 27% 4 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
FENOFIBRATE
METHOD: LC9017 , TESTIDCODE: 67489LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 49%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 61%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 24%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 64%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 42%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 24%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 48%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 31%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 34%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 14%  Analysis Date = 02/20/14 
 Pct Recovery = 35%  Analysis Date = 02/17/14 
 Pct Recovery = 35%  Analysis Date = 02/17/14 
 Pct Recovery = 35%  Analysis Date = 02/15/14 
 Pct Recovery = 35%  Analysis Date = 02/15/14 
 Pct Recovery = 35%  Analysis Date = 02/13/14 
 Pct Recovery = 35%  Analysis Date = 02/13/14 
 Pct Recovery = 35%  Analysis Date = 02/11/14 
 Pct Recovery = 34%  Analysis Date = 02/11/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/04/14 
 Pct Recovery = 34%  Analysis Date = 02/04/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/27/14 
 Pct Recovery = 33%  Analysis Date = 01/27/14 
 Pct Recovery = 33%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/20/14 
 Pct Recovery = 32%  Analysis Date = 01/20/14 
 Pct Recovery = 32%  Analysis Date = 01/18/14 
 Pct Recovery = 32%  Analysis Date = 01/18/14 
 Pct Recovery = 32%  Analysis Date = 01/16/14 
 Pct Recovery = 31%  Analysis Date = 01/16/14 
 Pct Recovery = 31%  Analysis Date = 01/14/14 
 Pct Recovery = 31%  Analysis Date = 01/14/14 
 Pct Recovery = 31%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/09/14 
 Pct Recovery = 31%  Analysis Date = 01/09/14 
 Pct Recovery = 31%  Analysis Date = 01/07/14 
 Pct Recovery = 30%  Analysis Date = 01/07/14 
 Pct Recovery = 30%  Analysis Date = 01/05/14 
 Pct Recovery = 30%  Analysis Date = 01/05/14 
 Pct Recovery = 30%  Analysis Date = 01/03/14 
 Pct Recovery = 30%  Analysis Date = 01/03/14 
 Pct Recovery = 30%  Analysis Date = 01/01/14 
 Pct Recovery = 30%  Analysis Date = 01/01/14 
 Pct Recovery = 30%  Analysis Date = 12/30/13 
 Pct Recovery = 30%  Analysis Date = 12/30/13 
 Pct Recovery = 30%  Analysis Date = 12/27/13 
 Pct Recovery = 29%  Analysis Date = 12/27/13 
 Pct Recovery = 29%  Analysis Date = 12/25/13 
 Pct Recovery = 29%  Analysis Date = 12/25/13 
 Pct Recovery = 29%  Analysis Date = 12/23/13 
 Pct Recovery = 29%  Analysis Date = 12/23/13 
 Pct Recovery = 29%  Analysis Date = 12/21/13 
 Pct Recovery = 29%  Analysis Date = 12/21/13 
 Pct Recovery = 29%  Analysis Date = 12/19/13 
 Pct Recovery = 28%  Analysis Date = 12/19/13 
 Pct Recovery = 28%  Analysis Date = 12/17/13 
 Pct Recovery = 28%  Analysis Date = 12/17/13 
 Pct Recovery = 28%  Analysis Date = 12/14/13 
 Pct Recovery = 28%  Analysis Date = 12/14/13 
 Pct Recovery = 28%  Analysis Date = 12/12/13 
 Pct Recovery = 28%  Analysis Date = 12/12/13 
 Pct Recovery = 28%  Analysis Date = 12/10/13 
 Pct Recovery = 27%  Analysis Date = 12/10/13 
 Pct Recovery = 27%  Analysis Date = 12/08/13 
 Pct Recovery = 27%  Analysis Date = 12/08/13 
 Pct Recovery = 27%  Analysis Date = 12/06/13 
 Pct Recovery = 27%  Analysis Date = 12/06/13 
 Pct Recovery = 27%  Analysis Date = 12/04/13 
 Pct Recovery = 27%  Analysis Date = 12/04/13 
 Pct Recovery = 27%  Analysis Date = 12/01/13 
 Pct Recovery = 27%  Analysis Date = 12/01/13 
 Pct Recovery = 27%  Analysis Date = 11/29/13 
 Pct Recovery = 26%  Analysis Date = 11/29/13 
 Pct Recovery = 26%  Analysis Date = 11/27/13 
 Pct Recovery = 26%  Analysis Date = 11/27/13 
 Pct Recovery = 26%  Analysis Date = 11/25/13 
 Pct Recovery = 26%  Analysis Date = 11/25/13 
 Pct Recovery = 26%  Analysis Date = 11/23/13 
 Pct Recovery = 26%  Analysis Date = 11/23/13 
 Pct Recovery = 26%  Analysis Date = 11/21/13 
 Pct Recovery = 25%  Analysis Date = 11/21/13 
 Pct Recovery = 25%  Analysis Date = 11/18/13 
 Pct Recovery = 25%  Analysis Date = 11/18/13 
 Pct Recovery = 25%  Analysis Date = 11/16/13 
 Pct Recovery = 25%  Analysis Date = 11/16/13 
 Pct Recovery = 25%  Analysis Date = 11/14/13 
 Pct Recovery = 25%  Analysis Date = 11/14/13 
 Pct Recovery = 25%  Analysis Date = 11/12/13 
 Pct Recovery = 25%  Analysis Date = 11/12/13 
 Pct Recovery = 25%  Analysis Date = 11/10/13 
 Pct Recovery = 25%  Analysis Date = 11/10/13 
 Pct Recovery = 25%  Analysis Date = 11/08/13 
 Pct Recovery = 25%  Analysis Date = 11/08/13 
 Pct Recovery = 25%  Analysis Date = 11/05/13 
 Pct Recovery = 25%  Analysis Date = 11/05/13 
 Pct Recovery = 25%  Analysis Date = 11/03/13 
 Pct Recovery = 25%  Analysis Date = 11/03/13 
 Pct Recovery = 25%  Analysis Date = 11/01/13 
 Pct Recovery = 25%  Analysis Date = 11/01/13 
 Pct Recovery = 25%  Analysis Date = 10/30/13 
 Pct Recovery = 25%  Analysis Date = 10/30/13 
 Pct Recovery = 25%  Analysis Date = 10/28/13 
 Pct Recovery = 25%  Analysis Date = 10/28/13 
 Pct Recovery = 25%  Analysis Date = 10/26/13 
 Pct Recovery = 25%  Analysis Date = 10/26/13 
 Pct Recovery = 25%  Analysis Date = 10/23/13 
 Pct Recovery = 25%  Analysis Date = 10/23/13 
 Pct Recovery = 25%  Analysis Date = 10/21/13 
 Pct Recovery = 25%  Analysis Date = 10/21/13 
 Pct Recovery = 25%  Analysis Date = 10/19/13 
 Pct Recovery = 25%  Analysis Date = 10/19/13 
 Pct Recovery = 25%  Analysis Date = 10/17/13 
 Pct Recovery = 25%  Analysis Date = 10/17/13 
 Pct Recovery = 25%  Analysis Date = 10/15/13 
 Pct Recovery = 25%  Analysis Date = 10/15/13 
 Pct Recovery = 25%  Analysis Date = 10/13/13 
 Pct Recovery = 25%  Analysis Date = 10/13/13 
 Pct Recovery = 25%  Analysis Date = 10/10/13 
 Pct Recovery = 25%  Analysis Date = 10/10/13 
 Pct Recovery = 25%  Analysis Date = 10/08/13 
 Pct Recovery = 25%  Analysis Date = 10/08/13 
 Pct Recovery = 25%  Analysis Date = 10/06/13 
 Pct Recovery = 25%  Analysis Date = 10/06/13 
 Pct Recovery = 25%  Analysis Date = 10/04/13 
 Pct Recovery = 25%  Analysis Date = 10/04/13 
 Pct Recovery = 25%  Analysis Date = 10/02/13 
 Pct Recovery = 25%  Analysis Date = 10/02/13 
 Pct Recovery = 25%  Analysis Date = 09/30/13 
 Pct Recovery = 25%  Analysis Date = 09/30/13 
 Pct Recovery = 25%  Analysis Date = 09/27/13 
 Pct Recovery = 25%  Analysis Date = 09/27/13 
 Pct Recovery = 25%  Analysis Date = 09/25/13 
 Pct Recovery = 25%  Analysis Date = 09/25/13 
 Pct Recovery = 25%  Analysis Date = 09/23/13 
 Pct Recovery = 25%  Analysis Date = 09/23/13 
 Pct Recovery = 25%  Analysis Date = 09/21/13 
 Pct Recovery = 25%  Analysis Date = 09/21/13 
 Pct Recovery = 25%  Analysis Date = 09/19/13 
 Pct Recovery = 25%  Analysis Date = 09/19/13 
 Pct Recovery = 25%  Analysis Date = 09/17/13 
 Pct Recovery = 25%  Analysis Date = 09/17/13 
 Pct Recovery = 25%  Analysis Date = 09/14/13 
 Pct Recovery = 25%  Analysis Date = 09/14/13 
 Pct Recovery = 25%  Analysis Date = 09/12/13 
 Pct Recovery = 25%  Analysis Date = 09/12/13 
 Pct Recovery = 25%  Analysis Date = 09/10/13 
 Pct Recovery = 25%  Analysis Date = 09/10/13 
 Pct Recovery = 25%  Analysis Date = 09/08/13 
 Pct Recovery = 25%  Analysis Date = 09/08/13 
 Pct Recovery = 25%  Analysis Date = 09/06/13 
 Pct Recovery = 25%  Analysis Date = 09/06/13 
 Pct Recovery = 25%  Analysis Date = 09/04/13 
 Pct Recovery = 25%  Analysis Date = 09/04/13 
 Pct Recovery = 25%  Analysis Date = 09/01/13 
 Pct Recovery = 25%  Analysis Date = 09/01/13 
 Pct Recovery = 25%  Analysis Date = 08/30/13 
 Pct Recovery = 25%  Analysis Date = 08/30/13 
 Pct Recovery = 25%  Analysis Date = 08/28/13 
 Pct Recovery = 25%  Analysis Date = 08/28/13 
 Pct Recovery = 25%  Analysis Date = 08/26/13 
 Pct Recovery = 25%  Analysis Date = 08/26/13 
 Pct Recovery = 25%  Analysis Date = 08/24/13 
 Pct Recovery = 25%  Analysis Date = 08/24/13 
 Pct Recovery = 25%  Analysis Date = 08/22/13 
 Pct Recovery = 25%  Analysis Date = 08/22/13 
 Pct Recovery = 25%  Analysis Date = 08/19/13 
 Pct Recovery = 26%  Analysis Date = 08/19/13 
 Pct Recovery = 26%  Analysis Date = 08/17/13 
 Pct Recovery = 26%  Analysis Date = 08/17/13 
 Pct Recovery = 26%  Analysis Date = 08/15/13 
 Pct Recovery = 26%  Analysis Date = 08/15/13 
 Pct Recovery = 26%  Analysis Date = 08/13/13 
 Pct Recovery = 26%  Analysis Date = 08/13/13 
 Pct Recovery = 26%  Analysis Date = 08/11/13 
 Pct Recovery = 27%  Analysis Date = 08/11/13 
 Pct Recovery = 27%  Analysis Date = 08/09/13 
 Pct Recovery = 27%  Analysis Date = 08/09/13 
 Pct Recovery = 27%  Analysis Date = 08/06/13 
 Pct Recovery = 27%  Analysis Date = 08/06/13 
 Pct Recovery = 27%  Analysis Date = 08/04/13 
 Pct Recovery = 27%  Analysis Date = 08/04/13 
 Pct Recovery = 27%  Analysis Date = 08/02/13 
 Pct Recovery = 27%  Analysis Date = 08/02/13 
 Pct Recovery = 27%  Analysis Date = 07/31/13 
 Pct Recovery = 28%  Analysis Date = 07/31/13 
 Pct Recovery = 28%  Analysis Date = 07/29/13 
 Pct Recovery = 28%  Analysis Date = 07/29/13 
 Pct Recovery = 28%  Analysis Date = 07/27/13 
 Pct Recovery = 28%  Analysis Date = 07/27/13 
 Pct Recovery = 28%  Analysis Date = 07/24/13 
 Pct Recovery = 28%  Analysis Date = 07/24/13 
 Pct Recovery = 28%  Analysis Date = 07/22/13 
 Pct Recovery = 29%  Analysis Date = 07/22/13 
 Pct Recovery = 29%  Analysis Date = 07/20/13 
 Pct Recovery = 29%  Analysis Date = 07/20/13 
 Pct Recovery = 29%  Analysis Date = 07/18/13 
 Pct Recovery = 29%  Analysis Date = 07/18/13 
 Pct Recovery = 29%  Analysis Date = 07/16/13 
 Pct Recovery = 29%  Analysis Date = 07/16/13 
 Pct Recovery = 29%  Analysis Date = 07/14/13 
 Pct Recovery = 29%  Analysis Date = 07/14/13 
 Pct Recovery = 29%  Analysis Date = 07/12/13 
 Pct Recovery = 30%  Analysis Date = 07/12/13 
 Pct Recovery = 30%  Analysis Date = 07/09/13 
 Pct Recovery = 30%  Analysis Date = 07/09/13 
 Pct Recovery = 30%  Analysis Date = 07/07/13 
 Pct Recovery = 30%  Analysis Date = 07/07/13 
 Pct Recovery = 30%  Analysis Date = 07/05/13 
 Pct Recovery = 30%  Analysis Date = 07/05/13 
 Pct Recovery = 30%  Analysis Date = 07/03/13 
 Pct Recovery = 31%  Analysis Date = 07/03/13 
 Pct Recovery = 31%  Analysis Date = 07/01/13 
 Pct Recovery = 31%  Analysis Date = 07/01/13 
 Pct Recovery = 31%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/26/13 
 Pct Recovery = 31%  Analysis Date = 06/26/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/22/13 
 Pct Recovery = 32%  Analysis Date = 06/22/13 
 Pct Recovery = 32%  Analysis Date = 06/20/13 
 Pct Recovery = 32%  Analysis Date = 06/20/13 
 Pct Recovery = 32%  Analysis Date = 06/18/13 
 Pct Recovery = 32%  Analysis Date = 06/18/13 
 Pct Recovery = 32%  Analysis Date = 06/16/13 
 Pct Recovery = 32%  Analysis Date = 06/16/13 
 Pct Recovery = 32%  Analysis Date = 06/13/13 
 Pct Recovery = 33%  Analysis Date = 06/13/13 
 Pct Recovery = 33%  Analysis Date = 06/11/13 
 Pct Recovery = 33%  Analysis Date = 06/11/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/03/13 
 Pct Recovery = 34%  Analysis Date = 06/03/13 
 Pct Recovery = 34%  Analysis Date = 05/31/13 
 Pct Recovery = 34%  Analysis Date = 05/31/13 
 Pct Recovery = 34%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/25/13 
 Pct Recovery = 35%  Analysis Date = 05/25/13 
 Pct Recovery = 35%  Analysis Date = 05/23/13 
 Pct Recovery = 35%  Analysis Date = 05/23/13 
 Pct Recovery = 35%  Analysis Date = 05/21/13 
 Pct Recovery = 35%  Analysis Date = 05/21/13 
 Pct Recovery = 35%  Analysis Date = 05/18/13 
 Pct Recovery = 35%  Analysis Date = 05/18/13 
 Pct Recovery = 35%  Analysis Date = 05/16/13 
 Pct Recovery = 35%  Analysis Date = 05/16/13 
 Pct Recovery = 35%  Analysis Date = 05/14/13 
 Pct Recovery = 36%  Analysis Date = 05/14/13 
 Pct Recovery = 36%  Analysis Date = 05/12/13 
 Pct Recovery = 36%  Analysis Date = 05/12/13 
 Pct Recovery = 36%  Analysis Date = 05/10/13 
 Pct Recovery = 36%  Analysis Date = 05/10/13 
 Pct Recovery = 36%  Analysis Date = 05/08/13 
 Pct Recovery = 36%  Analysis Date = 05/08/13 
 Pct Recovery = 36%  Analysis Date = 05/05/13 
 Pct Recovery = 37%  Analysis Date = 05/05/13 
 Pct Recovery = 37%  Analysis Date = 05/03/13 
 Pct Recovery = 37%  Analysis Date = 05/03/13 
 Pct Recovery = 37%  Analysis Date = 05/01/13 
 Pct Recovery = 37%  Analysis Date = 05/01/13 
 Pct Recovery = 37%  Analysis Date = 04/29/13 
 Pct Recovery = 37%  Analysis Date = 04/29/13 
 Pct Recovery = 37%  Analysis Date = 04/27/13 
 Pct Recovery = 38%  Analysis Date = 04/27/13 
 Pct Recovery = 38%  Analysis Date = 04/25/13 
 Pct Recovery = 38%  Analysis Date = 04/25/13 
 Pct Recovery = 38%  Analysis Date = 04/22/13 
 Pct Recovery = 39%  Analysis Date = 04/22/13 
 Pct Recovery = 39%  Analysis Date = 04/20/13 
 Pct Recovery = 39%  Analysis Date = 04/20/13 
 Pct Recovery = 39%  Analysis Date = 04/18/13 
 Pct Recovery = 40%  Analysis Date = 04/18/13 
 Pct Recovery = 40%  Analysis Date = 04/16/13 
 Pct Recovery = 40%  Analysis Date = 04/16/13 
 Pct Recovery = 40%  Analysis Date = 04/14/13 
 Pct Recovery = 40%  Analysis Date = 04/14/13 
 Pct Recovery = 40%  Analysis Date = 04/12/13 
 Pct Recovery = 41%  Analysis Date = 04/12/13 
 Pct Recovery = 41%  Analysis Date = 04/09/13 
 Pct Recovery = 41%  Analysis Date = 04/09/13 
 Pct Recovery = 41%  Analysis Date = 04/07/13 
 Pct Recovery = 42%  Analysis Date = 04/07/13 
 Pct Recovery = 42%  Analysis Date = 04/05/13 
 Pct Recovery = 42%  Analysis Date = 04/05/13 
 Pct Recovery = 42%  Analysis Date = 04/03/13 
 Pct Recovery = 43%  Analysis Date = 04/03/13 
 Pct Recovery = 43%  Analysis Date = 04/01/13 
 Pct Recovery = 43%  Analysis Date = 04/01/13 
 Pct Recovery = 43%  Analysis Date = 03/30/13 
 Pct Recovery = 44%  Analysis Date = 03/30/13 
 Pct Recovery = 44%  Analysis Date = 03/27/13 
 Pct Recovery = 44%  Analysis Date = 03/27/13 
 Pct Recovery = 44%  Analysis Date = 03/25/13 
 Pct Recovery = 44%  Analysis Date = 03/25/13 
 Pct Recovery = 44%  Analysis Date = 03/23/13 
 Pct Recovery = 45%  Analysis Date = 03/23/13 
 Pct Recovery = 45%  Analysis Date = 03/21/13 
 Pct Recovery = 45%  Analysis Date = 03/21/13 
 Pct Recovery = 45%  Analysis Date = 03/19/13 
 Pct Recovery = 46%  Analysis Date = 03/19/13 
 Pct Recovery = 46%  Analysis Date = 03/17/13 
 Pct Recovery = 46%  Analysis Date = 03/17/13 
 Pct Recovery = 46%  Analysis Date = 03/14/13 
 Pct Recovery = 47%  Analysis Date = 03/14/13 
 Pct Recovery = 47%  Analysis Date = 03/12/13 
 Pct Recovery = 47%  Analysis Date = 03/12/13 
 Pct Recovery = 47%  Analysis Date = 03/10/13 
 Pct Recovery = 48%  Analysis Date = 03/10/13 
 Pct Recovery = 48%  Analysis Date = 03/08/13 
 Pct Recovery = 48%  Analysis Date = 03/08/13 
 Pct Recovery = 48%  Analysis Date = 03/06/13 
 Pct Recovery = 48%  Analysis Date = 03/06/13 
 Pct Recovery = 48%  Analysis Date = 03/04/13 
 Pct Recovery = 49%  Analysis Date = 03/04/13 
 Pct Recovery = 49%  Analysis Date = 03/01/13 
 Pct Recovery = 49%  Analysis Date = 03/01/13 
 Pct Recovery = 49%  Analysis Date = 02/27/13 
 Pct Recovery = 50%  Analysis Date = 02/27/13 
 Pct Recovery = 50%  Analysis Date = 02/25/13 
 Pct Recovery = 50%  Analysis Date = 02/25/13 
 Pct Recovery = 50%  Analysis Date = 02/23/13 
 Pct Recovery = 51%  Analysis Date = 02/23/13 
 Pct Recovery = 51%  Analysis Date = 02/21/13 
 Pct Recovery = 51%  Analysis Date = 02/21/13 
 Pct Recovery = 51%  Analysis Date = 02/19/13 
 Pct Recovery = 51%  Analysis Date = 02/19/13 
 Pct Recovery = 51%  Analysis Date = 02/16/13 
 Pct Recovery = 52%  Analysis Date = 02/16/13 
 Pct Recovery = 52%  Analysis Date = 02/14/13 
 Pct Recovery = 52%  Analysis Date = 02/14/13 
 Pct Recovery = 52%  Analysis Date = 02/12/13 
 Pct Recovery = 53%  Analysis Date = 02/12/13 
 Pct Recovery = 53%  Analysis Date = 02/10/13 
 Pct Recovery = 53%  Analysis Date = 02/10/13 
 Pct Recovery = 53%  Analysis Date = 02/08/13 
 Pct Recovery = 54%  Analysis Date = 02/08/13 
 Pct Recovery = 54%  Analysis Date = 02/06/13 
 Pct Recovery = 54%  Analysis Date = 02/06/13 
 Pct Recovery = 54%  Analysis Date = 02/03/13 
 Pct Recovery = 54%  Analysis Date = 02/03/13 
 Pct Recovery = 54%  Analysis Date = 02/01/13 
 Pct Recovery = 55%  Analysis Date = 02/01/13 
 Pct Recovery = 55%  Analysis Date = 01/30/13 
 Pct Recovery = 55%  Analysis Date = 01/30/13 
 Pct Recovery = 55%  Analysis Date = 01/28/13 
 Pct Recovery = 56%  Analysis Date = 01/28/13 
 Pct Recovery = 56%  Analysis Date = 01/26/13 
 Pct Recovery = 56%  Analysis Date = 01/26/13 
 Pct Recovery = 56%  Analysis Date = 01/24/13 
 Pct Recovery = 57%  Analysis Date = 01/24/13 
 Pct Recovery = 57%  Analysis Date = 01/21/13 
 Pct Recovery = 57%  Analysis Date = 01/21/13 
 Pct Recovery = 57%  Analysis Date = 01/19/13 
 Pct Recovery = 57%  Analysis Date = 01/19/13 
 Pct Recovery = 57%  Analysis Date = 01/17/13 
 Pct Recovery = 58%  Analysis Date = 01/17/13 
 Pct Recovery = 58%  Analysis Date = 01/15/13 
 Pct Recovery = 58%  Analysis Date = 01/15/13 
 Pct Recovery = 58%  Analysis Date = 01/13/13 
 Pct Recovery = 59%  Analysis Date = 01/13/13 
 Pct Recovery = 59%  Analysis Date = 01/11/13 
 Pct Recovery = 59%  Analysis Date = 01/11/13 
 Pct Recovery = 59%  Analysis Date = 01/08/13 
 Pct Recovery = 59%  Analysis Date = 01/08/13 
 Pct Recovery = 59%  Analysis Date = 01/06/13 
 Pct Recovery = 60%  Analysis Date = 01/06/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/02/13 
 Pct Recovery = 61%  Analysis Date = 01/02/13 
 Pct Recovery = 61%  Analysis Date = 12/31/12 
 Pct Recovery = 61%  Analysis Date = 12/31/12 
 Pct Recovery = 61%  Analysis Date = 12/29/12 
 Pct Recovery = 62%  Analysis Date = 12/29/12 
 Pct Recovery = 62%  Analysis Date = 12/26/12 
 Pct Recovery = 62%  Analysis Date = 12/26/12 
 Pct Recovery = 62%  Analysis Date = 12/24/12 
 Pct Recovery = 62%  Analysis Date = 12/24/12 
 Pct Recovery = 62%  Analysis Date = 12/22/12 
 Pct Recovery = 63%  Analysis Date = 12/22/12 
 Pct Recovery = 63%  Analysis Date = 12/20/12 
 Pct Recovery = 63%  Analysis Date = 12/20/12 
 Pct Recovery = 63%  Analysis Date = 12/18/12 
 Pct Recovery = 64%  Analysis Date = 12/18/12 
 Pct Recovery = 64%  Analysis Date = 12/16/12 
 Pct Recovery = 64%  Analysis Date = 12/16/12 
 Pct Recovery = 64%  Analysis Date = 12/14/12 
 Pct Recovery = 65%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENOFIBRATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 39% 16% 38% 19%
Total 10 39% 16% 38% 19%

Sample Statistics
FENOFIBRATE

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 2 18% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
FEXOFENADINE
METHOD: LC9017 , TESTIDCODE: 67510LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 60%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 75%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 52%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 58%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 53%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 49%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 72%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 49%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 51%  Analysis Date = 03/21/14 
 Pct Recovery = 51%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/11/14 
 Pct Recovery = 51%  Analysis Date = 03/11/14 
 Pct Recovery = 51%  Analysis Date = 03/09/14 
 Pct Recovery = 51%  Analysis Date = 03/09/14 
 Pct Recovery = 51%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/02/14 
 Pct Recovery = 51%  Analysis Date = 03/02/14 
 Pct Recovery = 51%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/17/14 
 Pct Recovery = 51%  Analysis Date = 01/17/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/10/14 
 Pct Recovery = 51%  Analysis Date = 01/10/14 
 Pct Recovery = 51%  Analysis Date = 01/08/14 
 Pct Recovery = 51%  Analysis Date = 01/08/14 
 Pct Recovery = 51%  Analysis Date = 01/06/14 
 Pct Recovery = 51%  Analysis Date = 01/06/14 
 Pct Recovery = 51%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 12/30/13 
 Pct Recovery = 51%  Analysis Date = 12/30/13 
 Pct Recovery = 51%  Analysis Date = 12/27/13 
 Pct Recovery = 51%  Analysis Date = 12/27/13 
 Pct Recovery = 51%  Analysis Date = 12/25/13 
 Pct Recovery = 51%  Analysis Date = 12/25/13 
 Pct Recovery = 51%  Analysis Date = 12/23/13 
 Pct Recovery = 51%  Analysis Date = 12/23/13 
 Pct Recovery = 51%  Analysis Date = 12/20/13 
 Pct Recovery = 51%  Analysis Date = 12/20/13 
 Pct Recovery = 51%  Analysis Date = 12/18/13 
 Pct Recovery = 51%  Analysis Date = 12/18/13 
 Pct Recovery = 51%  Analysis Date = 12/16/13 
 Pct Recovery = 51%  Analysis Date = 12/16/13 
 Pct Recovery = 51%  Analysis Date = 12/13/13 
 Pct Recovery = 51%  Analysis Date = 12/13/13 
 Pct Recovery = 51%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/04/13 
 Pct Recovery = 51%  Analysis Date = 12/04/13 
 Pct Recovery = 51%  Analysis Date = 12/02/13 
 Pct Recovery = 51%  Analysis Date = 12/02/13 
 Pct Recovery = 51%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 Pct Recovery = 51%  Analysis Date = 11/25/13 
 Pct Recovery = 51%  Analysis Date = 11/25/13 
 Pct Recovery = 51%  Analysis Date = 11/23/13 
 Pct Recovery = 51%  Analysis Date = 11/23/13 
 Pct Recovery = 51%  Analysis Date = 11/20/13 
 Pct Recovery = 51%  Analysis Date = 11/20/13 
 Pct Recovery = 51%  Analysis Date = 11/18/13 
 Pct Recovery = 51%  Analysis Date = 11/18/13 
 Pct Recovery = 51%  Analysis Date = 11/16/13 
 Pct Recovery = 51%  Analysis Date = 11/16/13 
 Pct Recovery = 51%  Analysis Date = 11/13/13 
 Pct Recovery = 51%  Analysis Date = 11/13/13 
 Pct Recovery = 51%  Analysis Date = 11/11/13 
 Pct Recovery = 51%  Analysis Date = 11/11/13 
 Pct Recovery = 51%  Analysis Date = 11/09/13 
 Pct Recovery = 51%  Analysis Date = 11/09/13 
 Pct Recovery = 51%  Analysis Date = 11/07/13 
 Pct Recovery = 51%  Analysis Date = 11/07/13 
 Pct Recovery = 51%  Analysis Date = 11/04/13 
 Pct Recovery = 51%  Analysis Date = 11/04/13 
 Pct Recovery = 51%  Analysis Date = 11/02/13 
 Pct Recovery = 51%  Analysis Date = 11/02/13 
 Pct Recovery = 51%  Analysis Date = 10/31/13 
 Pct Recovery = 51%  Analysis Date = 10/31/13 
 Pct Recovery = 51%  Analysis Date = 10/28/13 
 Pct Recovery = 51%  Analysis Date = 10/28/13 
 Pct Recovery = 51%  Analysis Date = 10/26/13 
 Pct Recovery = 51%  Analysis Date = 10/26/13 
 Pct Recovery = 51%  Analysis Date = 10/24/13 
 Pct Recovery = 51%  Analysis Date = 10/24/13 
 Pct Recovery = 51%  Analysis Date = 10/21/13 
 Pct Recovery = 51%  Analysis Date = 10/21/13 
 Pct Recovery = 51%  Analysis Date = 10/19/13 
 Pct Recovery = 51%  Analysis Date = 10/19/13 
 Pct Recovery = 51%  Analysis Date = 10/17/13 
 Pct Recovery = 51%  Analysis Date = 10/17/13 
 Pct Recovery = 51%  Analysis Date = 10/14/13 
 Pct Recovery = 51%  Analysis Date = 10/14/13 
 Pct Recovery = 51%  Analysis Date = 10/12/13 
 Pct Recovery = 51%  Analysis Date = 10/12/13 
 Pct Recovery = 51%  Analysis Date = 10/10/13 
 Pct Recovery = 51%  Analysis Date = 10/10/13 
 Pct Recovery = 51%  Analysis Date = 10/07/13 
 Pct Recovery = 51%  Analysis Date = 10/07/13 
 Pct Recovery = 51%  Analysis Date = 10/05/13 
 Pct Recovery = 51%  Analysis Date = 10/05/13 
 Pct Recovery = 51%  Analysis Date = 10/03/13 
 Pct Recovery = 51%  Analysis Date = 10/03/13 
 Pct Recovery = 51%  Analysis Date = 10/01/13 
 Pct Recovery = 51%  Analysis Date = 10/01/13 
 Pct Recovery = 51%  Analysis Date = 09/28/13 
 Pct Recovery = 51%  Analysis Date = 09/28/13 
 Pct Recovery = 51%  Analysis Date = 09/26/13 
 Pct Recovery = 51%  Analysis Date = 09/26/13 
 Pct Recovery = 51%  Analysis Date = 09/24/13 
 Pct Recovery = 51%  Analysis Date = 09/24/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/17/13 
 Pct Recovery = 51%  Analysis Date = 09/17/13 
 Pct Recovery = 51%  Analysis Date = 09/14/13 
 Pct Recovery = 51%  Analysis Date = 09/14/13 
 Pct Recovery = 51%  Analysis Date = 09/12/13 
 Pct Recovery = 51%  Analysis Date = 09/12/13 
 Pct Recovery = 51%  Analysis Date = 09/10/13 
 Pct Recovery = 51%  Analysis Date = 09/10/13 
 Pct Recovery = 51%  Analysis Date = 09/07/13 
 Pct Recovery = 51%  Analysis Date = 09/07/13 
 Pct Recovery = 51%  Analysis Date = 09/05/13 
 Pct Recovery = 51%  Analysis Date = 09/05/13 
 Pct Recovery = 51%  Analysis Date = 09/03/13 
 Pct Recovery = 51%  Analysis Date = 09/03/13 
 Pct Recovery = 51%  Analysis Date = 09/01/13 
 Pct Recovery = 51%  Analysis Date = 09/01/13 
 Pct Recovery = 51%  Analysis Date = 08/29/13 
 Pct Recovery = 51%  Analysis Date = 08/29/13 
 Pct Recovery = 51%  Analysis Date = 08/27/13 
 Pct Recovery = 52%  Analysis Date = 08/27/13 
 Pct Recovery = 52%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/20/13 
 Pct Recovery = 52%  Analysis Date = 08/20/13 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/13/13 
 Pct Recovery = 52%  Analysis Date = 08/13/13 
 Pct Recovery = 52%  Analysis Date = 08/11/13 
 Pct Recovery = 52%  Analysis Date = 08/11/13 
 Pct Recovery = 52%  Analysis Date = 08/08/13 
 Pct Recovery = 52%  Analysis Date = 08/08/13 
 Pct Recovery = 52%  Analysis Date = 08/06/13 
 Pct Recovery = 53%  Analysis Date = 08/06/13 
 Pct Recovery = 53%  Analysis Date = 08/04/13 
 Pct Recovery = 53%  Analysis Date = 08/04/13 
 Pct Recovery = 53%  Analysis Date = 08/02/13 
 Pct Recovery = 53%  Analysis Date = 08/02/13 
 Pct Recovery = 53%  Analysis Date = 07/30/13 
 Pct Recovery = 53%  Analysis Date = 07/30/13 
 Pct Recovery = 53%  Analysis Date = 07/28/13 
 Pct Recovery = 53%  Analysis Date = 07/28/13 
 Pct Recovery = 53%  Analysis Date = 07/26/13 
 Pct Recovery = 53%  Analysis Date = 07/26/13 
 Pct Recovery = 53%  Analysis Date = 07/23/13 
 Pct Recovery = 53%  Analysis Date = 07/23/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/21/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/19/13 
 Pct Recovery = 53%  Analysis Date = 07/16/13 
 Pct Recovery = 54%  Analysis Date = 07/16/13 
 Pct Recovery = 54%  Analysis Date = 07/14/13 
 Pct Recovery = 54%  Analysis Date = 07/14/13 
 Pct Recovery = 54%  Analysis Date = 07/12/13 
 Pct Recovery = 54%  Analysis Date = 07/12/13 
 Pct Recovery = 54%  Analysis Date = 07/09/13 
 Pct Recovery = 54%  Analysis Date = 07/09/13 
 Pct Recovery = 54%  Analysis Date = 07/07/13 
 Pct Recovery = 54%  Analysis Date = 07/07/13 
 Pct Recovery = 54%  Analysis Date = 07/05/13 
 Pct Recovery = 54%  Analysis Date = 07/05/13 
 Pct Recovery = 54%  Analysis Date = 07/02/13 
 Pct Recovery = 54%  Analysis Date = 07/02/13 
 Pct Recovery = 54%  Analysis Date = 06/30/13 
 Pct Recovery = 54%  Analysis Date = 06/30/13 
 Pct Recovery = 54%  Analysis Date = 06/28/13 
 Pct Recovery = 55%  Analysis Date = 06/28/13 
 Pct Recovery = 55%  Analysis Date = 06/26/13 
 Pct Recovery = 55%  Analysis Date = 06/26/13 
 Pct Recovery = 55%  Analysis Date = 06/23/13 
 Pct Recovery = 55%  Analysis Date = 06/23/13 
 Pct Recovery = 55%  Analysis Date = 06/21/13 
 Pct Recovery = 55%  Analysis Date = 06/21/13 
 Pct Recovery = 55%  Analysis Date = 06/19/13 
 Pct Recovery = 55%  Analysis Date = 06/19/13 
 Pct Recovery = 55%  Analysis Date = 06/16/13 
 Pct Recovery = 55%  Analysis Date = 06/16/13 
 Pct Recovery = 55%  Analysis Date = 06/14/13 
 Pct Recovery = 55%  Analysis Date = 06/14/13 
 Pct Recovery = 55%  Analysis Date = 06/12/13 
 Pct Recovery = 55%  Analysis Date = 06/12/13 
 Pct Recovery = 55%  Analysis Date = 06/09/13 
 Pct Recovery = 55%  Analysis Date = 06/09/13 
 Pct Recovery = 55%  Analysis Date = 06/07/13 
 Pct Recovery = 56%  Analysis Date = 06/07/13 
 Pct Recovery = 56%  Analysis Date = 06/05/13 
 Pct Recovery = 56%  Analysis Date = 06/05/13 
 Pct Recovery = 56%  Analysis Date = 06/02/13 
 Pct Recovery = 56%  Analysis Date = 06/02/13 
 Pct Recovery = 56%  Analysis Date = 05/31/13 
 Pct Recovery = 56%  Analysis Date = 05/31/13 
 Pct Recovery = 56%  Analysis Date = 05/29/13 
 Pct Recovery = 56%  Analysis Date = 05/29/13 
 Pct Recovery = 56%  Analysis Date = 05/27/13 
 Pct Recovery = 56%  Analysis Date = 05/27/13 
 Pct Recovery = 56%  Analysis Date = 05/24/13 
 Pct Recovery = 56%  Analysis Date = 05/24/13 
 Pct Recovery = 56%  Analysis Date = 05/22/13 
 Pct Recovery = 56%  Analysis Date = 05/22/13 
 Pct Recovery = 56%  Analysis Date = 05/20/13 
 Pct Recovery = 57%  Analysis Date = 05/20/13 
 Pct Recovery = 57%  Analysis Date = 05/17/13 
 Pct Recovery = 57%  Analysis Date = 05/17/13 
 Pct Recovery = 57%  Analysis Date = 05/15/13 
 Pct Recovery = 57%  Analysis Date = 05/15/13 
 Pct Recovery = 57%  Analysis Date = 05/13/13 
 Pct Recovery = 57%  Analysis Date = 05/13/13 
 Pct Recovery = 57%  Analysis Date = 05/10/13 
 Pct Recovery = 57%  Analysis Date = 05/10/13 
 Pct Recovery = 57%  Analysis Date = 05/08/13 
 Pct Recovery = 57%  Analysis Date = 05/08/13 
 Pct Recovery = 57%  Analysis Date = 05/06/13 
 Pct Recovery = 57%  Analysis Date = 05/06/13 
 Pct Recovery = 57%  Analysis Date = 05/03/13 
 Pct Recovery = 57%  Analysis Date = 05/03/13 
 Pct Recovery = 57%  Analysis Date = 05/01/13 
 Pct Recovery = 57%  Analysis Date = 05/01/13 
 Pct Recovery = 57%  Analysis Date = 04/29/13 
 Pct Recovery = 58%  Analysis Date = 04/29/13 
 Pct Recovery = 58%  Analysis Date = 04/26/13 
 Pct Recovery = 58%  Analysis Date = 04/26/13 
 Pct Recovery = 58%  Analysis Date = 04/24/13 
 Pct Recovery = 58%  Analysis Date = 04/24/13 
 Pct Recovery = 58%  Analysis Date = 04/22/13 
 Pct Recovery = 58%  Analysis Date = 04/22/13 
 Pct Recovery = 58%  Analysis Date = 04/20/13 
 Pct Recovery = 59%  Analysis Date = 04/20/13 
 Pct Recovery = 59%  Analysis Date = 04/17/13 
 Pct Recovery = 59%  Analysis Date = 04/17/13 
 Pct Recovery = 59%  Analysis Date = 04/15/13 
 Pct Recovery = 59%  Analysis Date = 04/15/13 
 Pct Recovery = 59%  Analysis Date = 04/13/13 
 Pct Recovery = 59%  Analysis Date = 04/13/13 
 Pct Recovery = 59%  Analysis Date = 04/10/13 
 Pct Recovery = 60%  Analysis Date = 04/10/13 
 Pct Recovery = 60%  Analysis Date = 04/08/13 
 Pct Recovery = 60%  Analysis Date = 04/08/13 
 Pct Recovery = 60%  Analysis Date = 04/06/13 
 Pct Recovery = 60%  Analysis Date = 04/06/13 
 Pct Recovery = 60%  Analysis Date = 04/03/13 
 Pct Recovery = 60%  Analysis Date = 04/03/13 
 Pct Recovery = 60%  Analysis Date = 04/01/13 
 Pct Recovery = 61%  Analysis Date = 04/01/13 
 Pct Recovery = 61%  Analysis Date = 03/30/13 
 Pct Recovery = 61%  Analysis Date = 03/30/13 
 Pct Recovery = 61%  Analysis Date = 03/27/13 
 Pct Recovery = 61%  Analysis Date = 03/27/13 
 Pct Recovery = 61%  Analysis Date = 03/25/13 
 Pct Recovery = 61%  Analysis Date = 03/25/13 
 Pct Recovery = 61%  Analysis Date = 03/23/13 
 Pct Recovery = 61%  Analysis Date = 03/23/13 
 Pct Recovery = 61%  Analysis Date = 03/21/13 
 Pct Recovery = 62%  Analysis Date = 03/21/13 
 Pct Recovery = 62%  Analysis Date = 03/18/13 
 Pct Recovery = 62%  Analysis Date = 03/18/13 
 Pct Recovery = 62%  Analysis Date = 03/16/13 
 Pct Recovery = 62%  Analysis Date = 03/16/13 
 Pct Recovery = 62%  Analysis Date = 03/14/13 
 Pct Recovery = 62%  Analysis Date = 03/14/13 
 Pct Recovery = 62%  Analysis Date = 03/11/13 
 Pct Recovery = 63%  Analysis Date = 03/11/13 
 Pct Recovery = 63%  Analysis Date = 03/09/13 
 Pct Recovery = 63%  Analysis Date = 03/09/13 
 Pct Recovery = 63%  Analysis Date = 03/07/13 
 Pct Recovery = 63%  Analysis Date = 03/07/13 
 Pct Recovery = 63%  Analysis Date = 03/04/13 
 Pct Recovery = 63%  Analysis Date = 03/04/13 
 Pct Recovery = 63%  Analysis Date = 03/02/13 
 Pct Recovery = 64%  Analysis Date = 03/02/13 
 Pct Recovery = 64%  Analysis Date = 02/28/13 
 Pct Recovery = 64%  Analysis Date = 02/28/13 
 Pct Recovery = 64%  Analysis Date = 02/25/13 
 Pct Recovery = 64%  Analysis Date = 02/25/13 
 Pct Recovery = 64%  Analysis Date = 02/23/13 
 Pct Recovery = 64%  Analysis Date = 02/23/13 
 Pct Recovery = 64%  Analysis Date = 02/21/13 
 Pct Recovery = 65%  Analysis Date = 02/21/13 
 Pct Recovery = 65%  Analysis Date = 02/18/13 
 Pct Recovery = 65%  Analysis Date = 02/18/13 
 Pct Recovery = 65%  Analysis Date = 02/16/13 
 Pct Recovery = 65%  Analysis Date = 02/16/13 
 Pct Recovery = 65%  Analysis Date = 02/14/13 
 Pct Recovery = 65%  Analysis Date = 02/14/13 
 Pct Recovery = 65%  Analysis Date = 02/12/13 
 Pct Recovery = 66%  Analysis Date = 02/12/13 
 Pct Recovery = 66%  Analysis Date = 02/09/13 
 Pct Recovery = 66%  Analysis Date = 02/09/13 
 Pct Recovery = 66%  Analysis Date = 02/07/13 
 Pct Recovery = 66%  Analysis Date = 02/07/13 
 Pct Recovery = 66%  Analysis Date = 02/05/13 
 Pct Recovery = 66%  Analysis Date = 02/05/13 
 Pct Recovery = 66%  Analysis Date = 02/02/13 
 Pct Recovery = 67%  Analysis Date = 02/02/13 
 Pct Recovery = 67%  Analysis Date = 01/31/13 
 Pct Recovery = 67%  Analysis Date = 01/31/13 
 Pct Recovery = 67%  Analysis Date = 01/29/13 
 Pct Recovery = 67%  Analysis Date = 01/29/13 
 Pct Recovery = 67%  Analysis Date = 01/26/13 
 Pct Recovery = 67%  Analysis Date = 01/26/13 
 Pct Recovery = 67%  Analysis Date = 01/24/13 
 Pct Recovery = 68%  Analysis Date = 01/24/13 
 Pct Recovery = 68%  Analysis Date = 01/22/13 
 Pct Recovery = 68%  Analysis Date = 01/22/13 
 Pct Recovery = 68%  Analysis Date = 01/19/13 
 Pct Recovery = 68%  Analysis Date = 01/19/13 
 Pct Recovery = 68%  Analysis Date = 01/17/13 
 Pct Recovery = 68%  Analysis Date = 01/17/13 
 Pct Recovery = 68%  Analysis Date = 01/15/13 
 Pct Recovery = 69%  Analysis Date = 01/15/13 
 Pct Recovery = 69%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 69%  Analysis Date = 01/06/13 
 Pct Recovery = 70%  Analysis Date = 01/06/13 
 Pct Recovery = 70%  Analysis Date = 01/03/13 
 Pct Recovery = 70%  Analysis Date = 01/03/13 
 Pct Recovery = 70%  Analysis Date = 01/01/13 
 Pct Recovery = 70%  Analysis Date = 01/01/13 
 Pct Recovery = 70%  Analysis Date = 12/30/12 
 Pct Recovery = 70%  Analysis Date = 12/30/12 
 Pct Recovery = 70%  Analysis Date = 12/27/12 
 Pct Recovery = 71%  Analysis Date = 12/27/12 
 Pct Recovery = 71%  Analysis Date = 12/25/12 
 Pct Recovery = 71%  Analysis Date = 12/25/12 
 Pct Recovery = 71%  Analysis Date = 12/23/12 
 Pct Recovery = 71%  Analysis Date = 12/23/12 
 Pct Recovery = 71%  Analysis Date = 12/20/12 
 Pct Recovery = 71%  Analysis Date = 12/20/12 
 Pct Recovery = 71%  Analysis Date = 12/18/12 
 Pct Recovery = 72%  Analysis Date = 12/18/12 
 Pct Recovery = 72%  Analysis Date = 12/16/12 
 Pct Recovery = 72%  Analysis Date = 12/16/12 
 Pct Recovery = 72%  Analysis Date = 12/14/12 
 Pct Recovery = 72%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FEXOFENADINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 57% 10% 53% 7%
Total 10 57% 10% 53% 7%

Sample Statistics
FEXOFENADINE

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 2 18% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
FLUCONAZOLE
METHOD: LC9017 , TESTIDCODE: 67478LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 82%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 95%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 93%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 90%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 80%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 102%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 80%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 64%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 84%  Analysis Date = 03/21/14 
 Pct Recovery = 85%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/14/14 
 Pct Recovery = 84%  Analysis Date = 03/14/14 
 Pct Recovery = 84%  Analysis Date = 03/11/14 
 Pct Recovery = 84%  Analysis Date = 03/11/14 
 Pct Recovery = 84%  Analysis Date = 03/09/14 
 Pct Recovery = 84%  Analysis Date = 03/09/14 
 Pct Recovery = 84%  Analysis Date = 03/07/14 
 Pct Recovery = 84%  Analysis Date = 03/07/14 
 Pct Recovery = 84%  Analysis Date = 03/04/14 
 Pct Recovery = 83%  Analysis Date = 03/04/14 
 Pct Recovery = 83%  Analysis Date = 03/02/14 
 Pct Recovery = 83%  Analysis Date = 03/02/14 
 Pct Recovery = 83%  Analysis Date = 02/28/14 
 Pct Recovery = 83%  Analysis Date = 02/28/14 
 Pct Recovery = 83%  Analysis Date = 02/25/14 
 Pct Recovery = 83%  Analysis Date = 02/25/14 
 Pct Recovery = 83%  Analysis Date = 02/23/14 
 Pct Recovery = 82%  Analysis Date = 02/23/14 
 Pct Recovery = 82%  Analysis Date = 02/21/14 
 Pct Recovery = 82%  Analysis Date = 02/21/14 
 Pct Recovery = 82%  Analysis Date = 02/18/14 
 Pct Recovery = 82%  Analysis Date = 02/18/14 
 Pct Recovery = 82%  Analysis Date = 02/16/14 
 Pct Recovery = 82%  Analysis Date = 02/16/14 
 Pct Recovery = 82%  Analysis Date = 02/14/14 
 Pct Recovery = 81%  Analysis Date = 02/14/14 
 Pct Recovery = 81%  Analysis Date = 02/12/14 
 Pct Recovery = 81%  Analysis Date = 02/12/14 
 Pct Recovery = 81%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/07/14 
 Pct Recovery = 81%  Analysis Date = 02/07/14 
 Pct Recovery = 81%  Analysis Date = 02/05/14 
 Pct Recovery = 80%  Analysis Date = 02/05/14 
 Pct Recovery = 80%  Analysis Date = 02/02/14 
 Pct Recovery = 80%  Analysis Date = 02/02/14 
 Pct Recovery = 80%  Analysis Date = 01/31/14 
 Pct Recovery = 80%  Analysis Date = 01/31/14 
 Pct Recovery = 80%  Analysis Date = 01/29/14 
 Pct Recovery = 79%  Analysis Date = 01/29/14 
 Pct Recovery = 79%  Analysis Date = 01/26/14 
 Pct Recovery = 79%  Analysis Date = 01/26/14 
 Pct Recovery = 79%  Analysis Date = 01/24/14 
 Pct Recovery = 79%  Analysis Date = 01/24/14 
 Pct Recovery = 79%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/17/14 
 Pct Recovery = 78%  Analysis Date = 01/17/14 
 Pct Recovery = 78%  Analysis Date = 01/15/14 
 Pct Recovery = 78%  Analysis Date = 01/15/14 
 Pct Recovery = 78%  Analysis Date = 01/13/14 
 Pct Recovery = 77%  Analysis Date = 01/13/14 
 Pct Recovery = 77%  Analysis Date = 01/10/14 
 Pct Recovery = 77%  Analysis Date = 01/10/14 
 Pct Recovery = 77%  Analysis Date = 01/08/14 
 Pct Recovery = 77%  Analysis Date = 01/08/14 
 Pct Recovery = 77%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 12/30/13 
 Pct Recovery = 76%  Analysis Date = 12/30/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 75%  Analysis Date = 12/27/13 
 Pct Recovery = 75%  Analysis Date = 12/25/13 
 Pct Recovery = 75%  Analysis Date = 12/25/13 
 Pct Recovery = 75%  Analysis Date = 12/23/13 
 Pct Recovery = 75%  Analysis Date = 12/23/13 
 Pct Recovery = 75%  Analysis Date = 12/20/13 
 Pct Recovery = 74%  Analysis Date = 12/20/13 
 Pct Recovery = 74%  Analysis Date = 12/18/13 
 Pct Recovery = 74%  Analysis Date = 12/18/13 
 Pct Recovery = 74%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/16/13 
 Pct Recovery = 74%  Analysis Date = 12/13/13 
 Pct Recovery = 73%  Analysis Date = 12/13/13 
 Pct Recovery = 73%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/11/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/04/13 
 Pct Recovery = 72%  Analysis Date = 12/04/13 
 Pct Recovery = 72%  Analysis Date = 12/02/13 
 Pct Recovery = 72%  Analysis Date = 12/02/13 
 Pct Recovery = 72%  Analysis Date = 11/30/13 
 Pct Recovery = 72%  Analysis Date = 11/30/13 
 Pct Recovery = 72%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/27/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/25/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/07/13 
 Pct Recovery = 72%  Analysis Date = 11/07/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/02/13 
 Pct Recovery = 72%  Analysis Date = 11/02/13 
 Pct Recovery = 72%  Analysis Date = 10/31/13 
 Pct Recovery = 72%  Analysis Date = 10/31/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/26/13 
 Pct Recovery = 72%  Analysis Date = 10/26/13 
 Pct Recovery = 72%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/24/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/21/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/19/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/17/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/14/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/12/13 
 Pct Recovery = 72%  Analysis Date = 10/10/13 
 Pct Recovery = 72%  Analysis Date = 10/10/13 
 Pct Recovery = 72%  Analysis Date = 10/07/13 
 Pct Recovery = 72%  Analysis Date = 10/07/13 
 Pct Recovery = 72%  Analysis Date = 10/05/13 
 Pct Recovery = 72%  Analysis Date = 10/05/13 
 Pct Recovery = 72%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/26/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/24/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/21/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/19/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/17/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/14/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/12/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/10/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/07/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/05/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/03/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 09/01/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/29/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 72%  Analysis Date = 08/22/13 
 Pct Recovery = 72%  Analysis Date = 08/20/13 
 Pct Recovery = 72%  Analysis Date = 08/20/13 
 Pct Recovery = 72%  Analysis Date = 08/18/13 
 Pct Recovery = 72%  Analysis Date = 08/18/13 
 Pct Recovery = 72%  Analysis Date = 08/15/13 
 Pct Recovery = 72%  Analysis Date = 08/15/13 
 Pct Recovery = 72%  Analysis Date = 08/13/13 
 Pct Recovery = 72%  Analysis Date = 08/13/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/16/13 
 Pct Recovery = 76%  Analysis Date = 06/16/13 
 Pct Recovery = 76%  Analysis Date = 06/14/13 
 Pct Recovery = 76%  Analysis Date = 06/14/13 
 Pct Recovery = 76%  Analysis Date = 06/12/13 
 Pct Recovery = 76%  Analysis Date = 06/12/13 
 Pct Recovery = 76%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/02/13 
 Pct Recovery = 77%  Analysis Date = 06/02/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/27/13 
 Pct Recovery = 78%  Analysis Date = 05/27/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/20/13 
 Pct Recovery = 78%  Analysis Date = 05/20/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/15/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/13/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 79%  Analysis Date = 05/06/13 
 Pct Recovery = 79%  Analysis Date = 05/06/13 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 Pct Recovery = 79%  Analysis Date = 05/01/13 
 Pct Recovery = 79%  Analysis Date = 05/01/13 
 Pct Recovery = 79%  Analysis Date = 04/29/13 
 Pct Recovery = 79%  Analysis Date = 04/29/13 
 Pct Recovery = 79%  Analysis Date = 04/26/13 
 Pct Recovery = 80%  Analysis Date = 04/26/13 
 Pct Recovery = 80%  Analysis Date = 04/24/13 
 Pct Recovery = 80%  Analysis Date = 04/24/13 
 Pct Recovery = 80%  Analysis Date = 04/22/13 
 Pct Recovery = 80%  Analysis Date = 04/22/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/17/13 
 Pct Recovery = 81%  Analysis Date = 04/17/13 
 Pct Recovery = 81%  Analysis Date = 04/15/13 
 Pct Recovery = 81%  Analysis Date = 04/15/13 
 Pct Recovery = 81%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/10/13 
 Pct Recovery = 81%  Analysis Date = 04/10/13 
 Pct Recovery = 81%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 84%  Analysis Date = 03/21/13 
 Pct Recovery = 84%  Analysis Date = 03/18/13 
 Pct Recovery = 84%  Analysis Date = 03/18/13 
 Pct Recovery = 84%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/14/13 
 Pct Recovery = 85%  Analysis Date = 03/14/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/07/13 
 Pct Recovery = 85%  Analysis Date = 03/07/13 
 Pct Recovery = 85%  Analysis Date = 03/04/13 
 Pct Recovery = 86%  Analysis Date = 03/04/13 
 Pct Recovery = 86%  Analysis Date = 03/02/13 
 Pct Recovery = 86%  Analysis Date = 03/02/13 
 Pct Recovery = 86%  Analysis Date = 02/28/13 
 Pct Recovery = 86%  Analysis Date = 02/28/13 
 Pct Recovery = 86%  Analysis Date = 02/25/13 
 Pct Recovery = 86%  Analysis Date = 02/25/13 
 Pct Recovery = 86%  Analysis Date = 02/23/13 
 Pct Recovery = 87%  Analysis Date = 02/23/13 
 Pct Recovery = 87%  Analysis Date = 02/21/13 
 Pct Recovery = 87%  Analysis Date = 02/21/13 
 Pct Recovery = 87%  Analysis Date = 02/18/13 
 Pct Recovery = 87%  Analysis Date = 02/18/13 
 Pct Recovery = 87%  Analysis Date = 02/16/13 
 Pct Recovery = 87%  Analysis Date = 02/16/13 
 Pct Recovery = 87%  Analysis Date = 02/14/13 
 Pct Recovery = 88%  Analysis Date = 02/14/13 
 Pct Recovery = 88%  Analysis Date = 02/12/13 
 Pct Recovery = 88%  Analysis Date = 02/12/13 
 Pct Recovery = 88%  Analysis Date = 02/09/13 
 Pct Recovery = 88%  Analysis Date = 02/09/13 
 Pct Recovery = 88%  Analysis Date = 02/07/13 
 Pct Recovery = 88%  Analysis Date = 02/07/13 
 Pct Recovery = 88%  Analysis Date = 02/05/13 
 Pct Recovery = 89%  Analysis Date = 02/05/13 
 Pct Recovery = 89%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 01/31/13 
 Pct Recovery = 89%  Analysis Date = 01/31/13 
 Pct Recovery = 89%  Analysis Date = 01/29/13 
 Pct Recovery = 89%  Analysis Date = 01/29/13 
 Pct Recovery = 89%  Analysis Date = 01/26/13 
 Pct Recovery = 90%  Analysis Date = 01/26/13 
 Pct Recovery = 90%  Analysis Date = 01/24/13 
 Pct Recovery = 90%  Analysis Date = 01/24/13 
 Pct Recovery = 90%  Analysis Date = 01/22/13 
 Pct Recovery = 90%  Analysis Date = 01/22/13 
 Pct Recovery = 90%  Analysis Date = 01/19/13 
 Pct Recovery = 90%  Analysis Date = 01/19/13 
 Pct Recovery = 90%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/15/13 
 Pct Recovery = 91%  Analysis Date = 01/15/13 
 Pct Recovery = 91%  Analysis Date = 01/13/13 
 Pct Recovery = 91%  Analysis Date = 01/13/13 
 Pct Recovery = 91%  Analysis Date = 01/10/13 
 Pct Recovery = 92%  Analysis Date = 01/10/13 
 Pct Recovery = 92%  Analysis Date = 01/08/13 
 Pct Recovery = 92%  Analysis Date = 01/08/13 
 Pct Recovery = 92%  Analysis Date = 01/06/13 
 Pct Recovery = 92%  Analysis Date = 01/06/13 
 Pct Recovery = 92%  Analysis Date = 01/03/13 
 Pct Recovery = 92%  Analysis Date = 01/03/13 
 Pct Recovery = 92%  Analysis Date = 01/01/13 
 Pct Recovery = 93%  Analysis Date = 01/01/13 
 Pct Recovery = 93%  Analysis Date = 12/30/12 
 Pct Recovery = 93%  Analysis Date = 12/30/12 
 Pct Recovery = 93%  Analysis Date = 12/27/12 
 Pct Recovery = 93%  Analysis Date = 12/27/12 
 Pct Recovery = 93%  Analysis Date = 12/25/12 
 Pct Recovery = 93%  Analysis Date = 12/25/12 
 Pct Recovery = 93%  Analysis Date = 12/23/12 
 Pct Recovery = 94%  Analysis Date = 12/23/12 
 Pct Recovery = 94%  Analysis Date = 12/20/12 
 Pct Recovery = 94%  Analysis Date = 12/20/12 
 Pct Recovery = 94%  Analysis Date = 12/18/12 
 Pct Recovery = 94%  Analysis Date = 12/18/12 
 Pct Recovery = 94%  Analysis Date = 12/16/12 
 Pct Recovery = 94%  Analysis Date = 12/16/12 
 Pct Recovery = 94%  Analysis Date = 12/14/12 
 Pct Recovery = 95%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 81% 12% 80% 13%
Total 14 81% 12% 80% 13%

Sample Statistics
FLUCONAZOLE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
FLUOXETINE
METHOD: LC9017 , TESTIDCODE: 67450LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 64%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 74%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 81%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 52%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 57%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 65%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 37%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 51%  Analysis Date = 03/21/14 
 Pct Recovery = 52%  Analysis Date = 03/18/14 
 Pct Recovery = 52%  Analysis Date = 03/18/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/14/14 
 Pct Recovery = 52%  Analysis Date = 03/14/14 
 Pct Recovery = 52%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/11/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/04/14 
 Pct Recovery = 52%  Analysis Date = 03/04/14 
 Pct Recovery = 52%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 03/02/14 
 Pct Recovery = 52%  Analysis Date = 02/28/14 
 Pct Recovery = 52%  Analysis Date = 02/28/14 
 Pct Recovery = 52%  Analysis Date = 02/25/14 
 Pct Recovery = 52%  Analysis Date = 02/25/14 
 Pct Recovery = 52%  Analysis Date = 02/23/14 
 Pct Recovery = 52%  Analysis Date = 02/23/14 
 Pct Recovery = 52%  Analysis Date = 02/21/14 
 Pct Recovery = 52%  Analysis Date = 02/21/14 
 Pct Recovery = 52%  Analysis Date = 02/18/14 
 Pct Recovery = 52%  Analysis Date = 02/18/14 
 Pct Recovery = 52%  Analysis Date = 02/16/14 
 Pct Recovery = 52%  Analysis Date = 02/16/14 
 Pct Recovery = 52%  Analysis Date = 02/14/14 
 Pct Recovery = 53%  Analysis Date = 02/14/14 
 Pct Recovery = 53%  Analysis Date = 02/12/14 
 Pct Recovery = 53%  Analysis Date = 02/12/14 
 Pct Recovery = 53%  Analysis Date = 02/09/14 
 Pct Recovery = 53%  Analysis Date = 02/09/14 
 Pct Recovery = 53%  Analysis Date = 02/07/14 
 Pct Recovery = 53%  Analysis Date = 02/07/14 
 Pct Recovery = 53%  Analysis Date = 02/05/14 
 Pct Recovery = 53%  Analysis Date = 02/05/14 
 Pct Recovery = 53%  Analysis Date = 02/02/14 
 Pct Recovery = 53%  Analysis Date = 02/02/14 
 Pct Recovery = 53%  Analysis Date = 01/31/14 
 Pct Recovery = 53%  Analysis Date = 01/31/14 
 Pct Recovery = 53%  Analysis Date = 01/29/14 
 Pct Recovery = 53%  Analysis Date = 01/29/14 
 Pct Recovery = 53%  Analysis Date = 01/26/14 
 Pct Recovery = 53%  Analysis Date = 01/26/14 
 Pct Recovery = 53%  Analysis Date = 01/24/14 
 Pct Recovery = 53%  Analysis Date = 01/24/14 
 Pct Recovery = 53%  Analysis Date = 01/22/14 
 Pct Recovery = 53%  Analysis Date = 01/22/14 
 Pct Recovery = 53%  Analysis Date = 01/19/14 
 Pct Recovery = 53%  Analysis Date = 01/19/14 
 Pct Recovery = 53%  Analysis Date = 01/17/14 
 Pct Recovery = 53%  Analysis Date = 01/17/14 
 Pct Recovery = 53%  Analysis Date = 01/15/14 
 Pct Recovery = 53%  Analysis Date = 01/15/14 
 Pct Recovery = 53%  Analysis Date = 01/13/14 
 Pct Recovery = 53%  Analysis Date = 01/13/14 
 Pct Recovery = 53%  Analysis Date = 01/10/14 
 Pct Recovery = 54%  Analysis Date = 01/10/14 
 Pct Recovery = 54%  Analysis Date = 01/08/14 
 Pct Recovery = 54%  Analysis Date = 01/08/14 
 Pct Recovery = 54%  Analysis Date = 01/06/14 
 Pct Recovery = 54%  Analysis Date = 01/06/14 
 Pct Recovery = 54%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 55%  Analysis Date = 12/18/13 
 Pct Recovery = 55%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/13/13 
 Pct Recovery = 55%  Analysis Date = 12/13/13 
 Pct Recovery = 55%  Analysis Date = 12/11/13 
 Pct Recovery = 55%  Analysis Date = 12/11/13 
 Pct Recovery = 55%  Analysis Date = 12/09/13 
 Pct Recovery = 55%  Analysis Date = 12/09/13 
 Pct Recovery = 55%  Analysis Date = 12/07/13 
 Pct Recovery = 55%  Analysis Date = 12/07/13 
 Pct Recovery = 55%  Analysis Date = 12/04/13 
 Pct Recovery = 55%  Analysis Date = 12/04/13 
 Pct Recovery = 55%  Analysis Date = 12/02/13 
 Pct Recovery = 55%  Analysis Date = 12/02/13 
 Pct Recovery = 55%  Analysis Date = 11/30/13 
 Pct Recovery = 55%  Analysis Date = 11/30/13 
 Pct Recovery = 55%  Analysis Date = 11/27/13 
 Pct Recovery = 56%  Analysis Date = 11/27/13 
 Pct Recovery = 56%  Analysis Date = 11/25/13 
 Pct Recovery = 56%  Analysis Date = 11/25/13 
 Pct Recovery = 56%  Analysis Date = 11/23/13 
 Pct Recovery = 56%  Analysis Date = 11/23/13 
 Pct Recovery = 56%  Analysis Date = 11/20/13 
 Pct Recovery = 56%  Analysis Date = 11/20/13 
 Pct Recovery = 56%  Analysis Date = 11/18/13 
 Pct Recovery = 56%  Analysis Date = 11/18/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 57%  Analysis Date = 11/11/13 
 Pct Recovery = 57%  Analysis Date = 11/09/13 
 Pct Recovery = 57%  Analysis Date = 11/09/13 
 Pct Recovery = 57%  Analysis Date = 11/07/13 
 Pct Recovery = 57%  Analysis Date = 11/07/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/26/13 
 Pct Recovery = 58%  Analysis Date = 10/26/13 
 Pct Recovery = 58%  Analysis Date = 10/24/13 
 Pct Recovery = 58%  Analysis Date = 10/24/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/12/13 
 Pct Recovery = 59%  Analysis Date = 10/12/13 
 Pct Recovery = 59%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/05/13 
 Pct Recovery = 60%  Analysis Date = 10/05/13 
 Pct Recovery = 60%  Analysis Date = 10/03/13 
 Pct Recovery = 60%  Analysis Date = 10/03/13 
 Pct Recovery = 60%  Analysis Date = 10/01/13 
 Pct Recovery = 60%  Analysis Date = 10/01/13 
 Pct Recovery = 60%  Analysis Date = 09/28/13 
 Pct Recovery = 60%  Analysis Date = 09/28/13 
 Pct Recovery = 60%  Analysis Date = 09/26/13 
 Pct Recovery = 61%  Analysis Date = 09/26/13 
 Pct Recovery = 61%  Analysis Date = 09/24/13 
 Pct Recovery = 61%  Analysis Date = 09/24/13 
 Pct Recovery = 61%  Analysis Date = 09/21/13 
 Pct Recovery = 61%  Analysis Date = 09/21/13 
 Pct Recovery = 61%  Analysis Date = 09/19/13 
 Pct Recovery = 61%  Analysis Date = 09/19/13 
 Pct Recovery = 61%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/17/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/07/13 
 Pct Recovery = 62%  Analysis Date = 09/07/13 
 Pct Recovery = 62%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 08/29/13 
 Pct Recovery = 63%  Analysis Date = 08/29/13 
 Pct Recovery = 63%  Analysis Date = 08/27/13 
 Pct Recovery = 63%  Analysis Date = 08/27/13 
 Pct Recovery = 63%  Analysis Date = 08/25/13 
 Pct Recovery = 63%  Analysis Date = 08/25/13 
 Pct Recovery = 63%  Analysis Date = 08/22/13 
 Pct Recovery = 63%  Analysis Date = 08/22/13 
 Pct Recovery = 63%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/11/13 
 Pct Recovery = 64%  Analysis Date = 08/11/13 
 Pct Recovery = 64%  Analysis Date = 08/08/13 
 Pct Recovery = 64%  Analysis Date = 08/08/13 
 Pct Recovery = 64%  Analysis Date = 08/06/13 
 Pct Recovery = 64%  Analysis Date = 08/06/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 07/30/13 
 Pct Recovery = 64%  Analysis Date = 07/30/13 
 Pct Recovery = 64%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/26/13 
 Pct Recovery = 65%  Analysis Date = 07/26/13 
 Pct Recovery = 65%  Analysis Date = 07/23/13 
 Pct Recovery = 65%  Analysis Date = 07/23/13 
 Pct Recovery = 65%  Analysis Date = 07/21/13 
 Pct Recovery = 65%  Analysis Date = 07/21/13 
 Pct Recovery = 65%  Analysis Date = 07/19/13 
 Pct Recovery = 65%  Analysis Date = 07/19/13 
 Pct Recovery = 65%  Analysis Date = 07/16/13 
 Pct Recovery = 65%  Analysis Date = 07/16/13 
 Pct Recovery = 65%  Analysis Date = 07/14/13 
 Pct Recovery = 65%  Analysis Date = 07/14/13 
 Pct Recovery = 65%  Analysis Date = 07/12/13 
 Pct Recovery = 65%  Analysis Date = 07/12/13 
 Pct Recovery = 65%  Analysis Date = 07/09/13 
 Pct Recovery = 65%  Analysis Date = 07/09/13 
 Pct Recovery = 65%  Analysis Date = 07/07/13 
 Pct Recovery = 65%  Analysis Date = 07/07/13 
 Pct Recovery = 65%  Analysis Date = 07/05/13 
 Pct Recovery = 65%  Analysis Date = 07/05/13 
 Pct Recovery = 65%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 06/30/13 
 Pct Recovery = 66%  Analysis Date = 06/30/13 
 Pct Recovery = 66%  Analysis Date = 06/28/13 
 Pct Recovery = 66%  Analysis Date = 06/28/13 
 Pct Recovery = 66%  Analysis Date = 06/26/13 
 Pct Recovery = 66%  Analysis Date = 06/26/13 
 Pct Recovery = 66%  Analysis Date = 06/23/13 
 Pct Recovery = 66%  Analysis Date = 06/23/13 
 Pct Recovery = 66%  Analysis Date = 06/21/13 
 Pct Recovery = 66%  Analysis Date = 06/21/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/16/13 
 Pct Recovery = 66%  Analysis Date = 06/16/13 
 Pct Recovery = 66%  Analysis Date = 06/14/13 
 Pct Recovery = 66%  Analysis Date = 06/14/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/05/13 
 Pct Recovery = 67%  Analysis Date = 06/05/13 
 Pct Recovery = 67%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/29/13 
 Pct Recovery = 67%  Analysis Date = 05/29/13 
 Pct Recovery = 67%  Analysis Date = 05/27/13 
 Pct Recovery = 67%  Analysis Date = 05/27/13 
 Pct Recovery = 67%  Analysis Date = 05/24/13 
 Pct Recovery = 67%  Analysis Date = 05/24/13 
 Pct Recovery = 67%  Analysis Date = 05/22/13 
 Pct Recovery = 67%  Analysis Date = 05/22/13 
 Pct Recovery = 67%  Analysis Date = 05/20/13 
 Pct Recovery = 67%  Analysis Date = 05/20/13 
 Pct Recovery = 67%  Analysis Date = 05/17/13 
 Pct Recovery = 67%  Analysis Date = 05/17/13 
 Pct Recovery = 67%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/03/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 05/01/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/29/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/26/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/24/13 
 Pct Recovery = 68%  Analysis Date = 04/22/13 
 Pct Recovery = 68%  Analysis Date = 04/22/13 
 Pct Recovery = 68%  Analysis Date = 04/20/13 
 Pct Recovery = 68%  Analysis Date = 04/20/13 
 Pct Recovery = 68%  Analysis Date = 04/17/13 
 Pct Recovery = 69%  Analysis Date = 04/17/13 
 Pct Recovery = 69%  Analysis Date = 04/15/13 
 Pct Recovery = 69%  Analysis Date = 04/15/13 
 Pct Recovery = 69%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/10/13 
 Pct Recovery = 69%  Analysis Date = 04/10/13 
 Pct Recovery = 69%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/06/13 
 Pct Recovery = 69%  Analysis Date = 04/06/13 
 Pct Recovery = 69%  Analysis Date = 04/03/13 
 Pct Recovery = 69%  Analysis Date = 04/03/13 
 Pct Recovery = 69%  Analysis Date = 04/01/13 
 Pct Recovery = 69%  Analysis Date = 04/01/13 
 Pct Recovery = 69%  Analysis Date = 03/30/13 
 Pct Recovery = 69%  Analysis Date = 03/30/13 
 Pct Recovery = 69%  Analysis Date = 03/27/13 
 Pct Recovery = 69%  Analysis Date = 03/27/13 
 Pct Recovery = 69%  Analysis Date = 03/25/13 
 Pct Recovery = 69%  Analysis Date = 03/25/13 
 Pct Recovery = 69%  Analysis Date = 03/23/13 
 Pct Recovery = 69%  Analysis Date = 03/23/13 
 Pct Recovery = 69%  Analysis Date = 03/21/13 
 Pct Recovery = 69%  Analysis Date = 03/21/13 
 Pct Recovery = 69%  Analysis Date = 03/18/13 
 Pct Recovery = 70%  Analysis Date = 03/18/13 
 Pct Recovery = 70%  Analysis Date = 03/16/13 
 Pct Recovery = 70%  Analysis Date = 03/16/13 
 Pct Recovery = 70%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/11/13 
 Pct Recovery = 70%  Analysis Date = 03/11/13 
 Pct Recovery = 70%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/07/13 
 Pct Recovery = 70%  Analysis Date = 03/07/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 02/28/13 
 Pct Recovery = 70%  Analysis Date = 02/28/13 
 Pct Recovery = 70%  Analysis Date = 02/25/13 
 Pct Recovery = 70%  Analysis Date = 02/25/13 
 Pct Recovery = 70%  Analysis Date = 02/23/13 
 Pct Recovery = 70%  Analysis Date = 02/23/13 
 Pct Recovery = 70%  Analysis Date = 02/21/13 
 Pct Recovery = 70%  Analysis Date = 02/21/13 
 Pct Recovery = 70%  Analysis Date = 02/18/13 
 Pct Recovery = 71%  Analysis Date = 02/18/13 
 Pct Recovery = 71%  Analysis Date = 02/16/13 
 Pct Recovery = 71%  Analysis Date = 02/16/13 
 Pct Recovery = 71%  Analysis Date = 02/14/13 
 Pct Recovery = 71%  Analysis Date = 02/14/13 
 Pct Recovery = 71%  Analysis Date = 02/12/13 
 Pct Recovery = 71%  Analysis Date = 02/12/13 
 Pct Recovery = 71%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/09/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/07/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/02/13 
 Pct Recovery = 71%  Analysis Date = 02/02/13 
 Pct Recovery = 71%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/29/13 
 Pct Recovery = 72%  Analysis Date = 01/29/13 
 Pct Recovery = 72%  Analysis Date = 01/26/13 
 Pct Recovery = 72%  Analysis Date = 01/26/13 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 Pct Recovery = 72%  Analysis Date = 01/22/13 
 Pct Recovery = 72%  Analysis Date = 01/22/13 
 Pct Recovery = 72%  Analysis Date = 01/19/13 
 Pct Recovery = 72%  Analysis Date = 01/19/13 
 Pct Recovery = 72%  Analysis Date = 01/17/13 
 Pct Recovery = 72%  Analysis Date = 01/17/13 
 Pct Recovery = 72%  Analysis Date = 01/15/13 
 Pct Recovery = 73%  Analysis Date = 01/15/13 
 Pct Recovery = 73%  Analysis Date = 01/13/13 
 Pct Recovery = 73%  Analysis Date = 01/13/13 
 Pct Recovery = 73%  Analysis Date = 01/10/13 
 Pct Recovery = 73%  Analysis Date = 01/10/13 
 Pct Recovery = 73%  Analysis Date = 01/08/13 
 Pct Recovery = 73%  Analysis Date = 01/08/13 
 Pct Recovery = 73%  Analysis Date = 01/06/13 
 Pct Recovery = 73%  Analysis Date = 01/06/13 
 Pct Recovery = 73%  Analysis Date = 01/03/13 
 Pct Recovery = 73%  Analysis Date = 01/03/13 
 Pct Recovery = 73%  Analysis Date = 01/01/13 
 Pct Recovery = 73%  Analysis Date = 01/01/13 
 Pct Recovery = 73%  Analysis Date = 12/30/12 
 Pct Recovery = 74%  Analysis Date = 12/30/12 
 Pct Recovery = 74%  Analysis Date = 12/27/12 
 Pct Recovery = 74%  Analysis Date = 12/27/12 
 Pct Recovery = 74%  Analysis Date = 12/25/12 
 Pct Recovery = 74%  Analysis Date = 12/25/12 
 Pct Recovery = 74%  Analysis Date = 12/23/12 
 Pct Recovery = 74%  Analysis Date = 12/23/12 
 Pct Recovery = 74%  Analysis Date = 12/20/12 
 Pct Recovery = 74%  Analysis Date = 12/20/12 
 Pct Recovery = 74%  Analysis Date = 12/18/12 
 Pct Recovery = 74%  Analysis Date = 12/18/12 
 Pct Recovery = 74%  Analysis Date = 12/16/12 
 Pct Recovery = 74%  Analysis Date = 12/16/12 
 Pct Recovery = 74%  Analysis Date = 12/14/12 
 Pct Recovery = 75%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUOXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 63% 14% 64% 16%
Total 10 63% 14% 64% 16%

Sample Statistics
FLUOXETINE

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 10 91% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
FLUTICASONE PROPIONATE
METHOD: LC9017 , TESTIDCODE: 67529LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 58%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 42%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 61%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 65%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 43%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 11%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 44%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 43%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 72%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 40%  Analysis Date = 03/21/14 
 Pct Recovery = 39%  Analysis Date = 03/18/14 
 Pct Recovery = 40%  Analysis Date = 03/18/14 
 Pct Recovery = 40%  Analysis Date = 03/16/14 
 Pct Recovery = 41%  Analysis Date = 03/16/14 
 Pct Recovery = 41%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/11/14 
 Pct Recovery = 43%  Analysis Date = 03/11/14 
 Pct Recovery = 43%  Analysis Date = 03/09/14 
 Pct Recovery = 44%  Analysis Date = 03/09/14 
 Pct Recovery = 44%  Analysis Date = 03/07/14 
 Pct Recovery = 44%  Analysis Date = 03/07/14 
 Pct Recovery = 44%  Analysis Date = 03/04/14 
 Pct Recovery = 45%  Analysis Date = 03/04/14 
 Pct Recovery = 45%  Analysis Date = 03/02/14 
 Pct Recovery = 46%  Analysis Date = 03/02/14 
 Pct Recovery = 46%  Analysis Date = 02/28/14 
 Pct Recovery = 47%  Analysis Date = 02/28/14 
 Pct Recovery = 47%  Analysis Date = 02/25/14 
 Pct Recovery = 48%  Analysis Date = 02/25/14 
 Pct Recovery = 48%  Analysis Date = 02/23/14 
 Pct Recovery = 49%  Analysis Date = 02/23/14 
 Pct Recovery = 49%  Analysis Date = 02/21/14 
 Pct Recovery = 49%  Analysis Date = 02/21/14 
 Pct Recovery = 49%  Analysis Date = 02/18/14 
 Pct Recovery = 50%  Analysis Date = 02/18/14 
 Pct Recovery = 50%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 52%  Analysis Date = 02/12/14 
 Pct Recovery = 52%  Analysis Date = 02/09/14 
 Pct Recovery = 52%  Analysis Date = 02/09/14 
 Pct Recovery = 52%  Analysis Date = 02/07/14 
 Pct Recovery = 52%  Analysis Date = 02/07/14 
 Pct Recovery = 52%  Analysis Date = 02/05/14 
 Pct Recovery = 53%  Analysis Date = 02/05/14 
 Pct Recovery = 53%  Analysis Date = 02/02/14 
 Pct Recovery = 53%  Analysis Date = 02/02/14 
 Pct Recovery = 53%  Analysis Date = 01/31/14 
 Pct Recovery = 54%  Analysis Date = 01/31/14 
 Pct Recovery = 54%  Analysis Date = 01/29/14 
 Pct Recovery = 54%  Analysis Date = 01/29/14 
 Pct Recovery = 54%  Analysis Date = 01/26/14 
 Pct Recovery = 55%  Analysis Date = 01/26/14 
 Pct Recovery = 55%  Analysis Date = 01/24/14 
 Pct Recovery = 55%  Analysis Date = 01/24/14 
 Pct Recovery = 55%  Analysis Date = 01/22/14 
 Pct Recovery = 55%  Analysis Date = 01/22/14 
 Pct Recovery = 55%  Analysis Date = 01/19/14 
 Pct Recovery = 56%  Analysis Date = 01/19/14 
 Pct Recovery = 56%  Analysis Date = 01/17/14 
 Pct Recovery = 56%  Analysis Date = 01/17/14 
 Pct Recovery = 56%  Analysis Date = 01/15/14 
 Pct Recovery = 57%  Analysis Date = 01/15/14 
 Pct Recovery = 57%  Analysis Date = 01/13/14 
 Pct Recovery = 57%  Analysis Date = 01/13/14 
 Pct Recovery = 57%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/06/14 
 Pct Recovery = 59%  Analysis Date = 01/06/14 
 Pct Recovery = 59%  Analysis Date = 01/03/14 
 Pct Recovery = 59%  Analysis Date = 01/03/14 
 Pct Recovery = 59%  Analysis Date = 01/01/14 
 Pct Recovery = 59%  Analysis Date = 01/01/14 
 Pct Recovery = 59%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 60%  Analysis Date = 12/27/13 
 Pct Recovery = 60%  Analysis Date = 12/27/13 
 Pct Recovery = 60%  Analysis Date = 12/25/13 
 Pct Recovery = 61%  Analysis Date = 12/25/13 
 Pct Recovery = 61%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/23/13 
 Pct Recovery = 61%  Analysis Date = 12/20/13 
 Pct Recovery = 62%  Analysis Date = 12/20/13 
 Pct Recovery = 62%  Analysis Date = 12/18/13 
 Pct Recovery = 62%  Analysis Date = 12/18/13 
 Pct Recovery = 62%  Analysis Date = 12/16/13 
 Pct Recovery = 62%  Analysis Date = 12/16/13 
 Pct Recovery = 62%  Analysis Date = 12/13/13 
 Pct Recovery = 63%  Analysis Date = 12/13/13 
 Pct Recovery = 63%  Analysis Date = 12/11/13 
 Pct Recovery = 63%  Analysis Date = 12/11/13 
 Pct Recovery = 63%  Analysis Date = 12/09/13 
 Pct Recovery = 64%  Analysis Date = 12/09/13 
 Pct Recovery = 64%  Analysis Date = 12/07/13 
 Pct Recovery = 64%  Analysis Date = 12/07/13 
 Pct Recovery = 64%  Analysis Date = 12/04/13 
 Pct Recovery = 64%  Analysis Date = 12/04/13 
 Pct Recovery = 64%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/27/13 
 Pct Recovery = 63%  Analysis Date = 11/27/13 
 Pct Recovery = 63%  Analysis Date = 11/25/13 
 Pct Recovery = 63%  Analysis Date = 11/25/13 
 Pct Recovery = 63%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/11/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/09/13 
 Pct Recovery = 60%  Analysis Date = 11/07/13 
 Pct Recovery = 59%  Analysis Date = 11/07/13 
 Pct Recovery = 59%  Analysis Date = 11/04/13 
 Pct Recovery = 59%  Analysis Date = 11/04/13 
 Pct Recovery = 59%  Analysis Date = 11/02/13 
 Pct Recovery = 59%  Analysis Date = 11/02/13 
 Pct Recovery = 59%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/28/13 
 Pct Recovery = 58%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/19/13 
 Pct Recovery = 56%  Analysis Date = 10/19/13 
 Pct Recovery = 56%  Analysis Date = 10/17/13 
 Pct Recovery = 56%  Analysis Date = 10/17/13 
 Pct Recovery = 56%  Analysis Date = 10/14/13 
 Pct Recovery = 55%  Analysis Date = 10/14/13 
 Pct Recovery = 55%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/12/13 
 Pct Recovery = 55%  Analysis Date = 10/10/13 
 Pct Recovery = 54%  Analysis Date = 10/10/13 
 Pct Recovery = 54%  Analysis Date = 10/07/13 
 Pct Recovery = 54%  Analysis Date = 10/07/13 
 Pct Recovery = 54%  Analysis Date = 10/05/13 
 Pct Recovery = 54%  Analysis Date = 10/05/13 
 Pct Recovery = 54%  Analysis Date = 10/03/13 
 Pct Recovery = 53%  Analysis Date = 10/03/13 
 Pct Recovery = 53%  Analysis Date = 10/01/13 
 Pct Recovery = 53%  Analysis Date = 10/01/13 
 Pct Recovery = 53%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/26/13 
 Pct Recovery = 52%  Analysis Date = 09/26/13 
 Pct Recovery = 52%  Analysis Date = 09/24/13 
 Pct Recovery = 52%  Analysis Date = 09/24/13 
 Pct Recovery = 52%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/17/13 
 Pct Recovery = 50%  Analysis Date = 09/17/13 
 Pct Recovery = 50%  Analysis Date = 09/14/13 
 Pct Recovery = 50%  Analysis Date = 09/14/13 
 Pct Recovery = 50%  Analysis Date = 09/12/13 
 Pct Recovery = 49%  Analysis Date = 09/12/13 
 Pct Recovery = 49%  Analysis Date = 09/10/13 
 Pct Recovery = 49%  Analysis Date = 09/10/13 
 Pct Recovery = 49%  Analysis Date = 09/07/13 
 Pct Recovery = 49%  Analysis Date = 09/07/13 
 Pct Recovery = 49%  Analysis Date = 09/05/13 
 Pct Recovery = 48%  Analysis Date = 09/05/13 
 Pct Recovery = 48%  Analysis Date = 09/03/13 
 Pct Recovery = 48%  Analysis Date = 09/03/13 
 Pct Recovery = 48%  Analysis Date = 09/01/13 
 Pct Recovery = 47%  Analysis Date = 09/01/13 
 Pct Recovery = 47%  Analysis Date = 08/29/13 
 Pct Recovery = 47%  Analysis Date = 08/29/13 
 Pct Recovery = 47%  Analysis Date = 08/27/13 
 Pct Recovery = 47%  Analysis Date = 08/27/13 
 Pct Recovery = 47%  Analysis Date = 08/25/13 
 Pct Recovery = 46%  Analysis Date = 08/25/13 
 Pct Recovery = 46%  Analysis Date = 08/22/13 
 Pct Recovery = 46%  Analysis Date = 08/22/13 
 Pct Recovery = 46%  Analysis Date = 08/20/13 
 Pct Recovery = 45%  Analysis Date = 08/20/13 
 Pct Recovery = 45%  Analysis Date = 08/18/13 
 Pct Recovery = 45%  Analysis Date = 08/18/13 
 Pct Recovery = 45%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/15/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/13/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 45%  Analysis Date = 08/08/13 
 Pct Recovery = 45%  Analysis Date = 08/08/13 
 Pct Recovery = 45%  Analysis Date = 08/06/13 
 Pct Recovery = 46%  Analysis Date = 08/06/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/28/13 
 Pct Recovery = 46%  Analysis Date = 07/28/13 
 Pct Recovery = 46%  Analysis Date = 07/26/13 
 Pct Recovery = 46%  Analysis Date = 07/26/13 
 Pct Recovery = 46%  Analysis Date = 07/23/13 
 Pct Recovery = 46%  Analysis Date = 07/23/13 
 Pct Recovery = 46%  Analysis Date = 07/21/13 
 Pct Recovery = 46%  Analysis Date = 07/21/13 
 Pct Recovery = 46%  Analysis Date = 07/19/13 
 Pct Recovery = 46%  Analysis Date = 07/19/13 
 Pct Recovery = 46%  Analysis Date = 07/16/13 
 Pct Recovery = 47%  Analysis Date = 07/16/13 
 Pct Recovery = 47%  Analysis Date = 07/14/13 
 Pct Recovery = 47%  Analysis Date = 07/14/13 
 Pct Recovery = 47%  Analysis Date = 07/12/13 
 Pct Recovery = 47%  Analysis Date = 07/12/13 
 Pct Recovery = 47%  Analysis Date = 07/09/13 
 Pct Recovery = 47%  Analysis Date = 07/09/13 
 Pct Recovery = 47%  Analysis Date = 07/07/13 
 Pct Recovery = 47%  Analysis Date = 07/07/13 
 Pct Recovery = 47%  Analysis Date = 07/05/13 
 Pct Recovery = 47%  Analysis Date = 07/05/13 
 Pct Recovery = 47%  Analysis Date = 07/02/13 
 Pct Recovery = 47%  Analysis Date = 07/02/13 
 Pct Recovery = 47%  Analysis Date = 06/30/13 
 Pct Recovery = 47%  Analysis Date = 06/30/13 
 Pct Recovery = 47%  Analysis Date = 06/28/13 
 Pct Recovery = 48%  Analysis Date = 06/28/13 
 Pct Recovery = 48%  Analysis Date = 06/26/13 
 Pct Recovery = 48%  Analysis Date = 06/26/13 
 Pct Recovery = 48%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/23/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/21/13 
 Pct Recovery = 48%  Analysis Date = 06/19/13 
 Pct Recovery = 48%  Analysis Date = 06/19/13 
 Pct Recovery = 48%  Analysis Date = 06/16/13 
 Pct Recovery = 48%  Analysis Date = 06/16/13 
 Pct Recovery = 48%  Analysis Date = 06/14/13 
 Pct Recovery = 48%  Analysis Date = 06/14/13 
 Pct Recovery = 48%  Analysis Date = 06/12/13 
 Pct Recovery = 48%  Analysis Date = 06/12/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/09/13 
 Pct Recovery = 48%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/07/13 
 Pct Recovery = 49%  Analysis Date = 06/05/13 
 Pct Recovery = 49%  Analysis Date = 06/05/13 
 Pct Recovery = 49%  Analysis Date = 06/02/13 
 Pct Recovery = 49%  Analysis Date = 06/02/13 
 Pct Recovery = 49%  Analysis Date = 05/31/13 
 Pct Recovery = 49%  Analysis Date = 05/31/13 
 Pct Recovery = 49%  Analysis Date = 05/29/13 
 Pct Recovery = 49%  Analysis Date = 05/29/13 
 Pct Recovery = 49%  Analysis Date = 05/27/13 
 Pct Recovery = 49%  Analysis Date = 05/27/13 
 Pct Recovery = 49%  Analysis Date = 05/24/13 
 Pct Recovery = 49%  Analysis Date = 05/24/13 
 Pct Recovery = 49%  Analysis Date = 05/22/13 
 Pct Recovery = 49%  Analysis Date = 05/22/13 
 Pct Recovery = 49%  Analysis Date = 05/20/13 
 Pct Recovery = 50%  Analysis Date = 05/20/13 
 Pct Recovery = 50%  Analysis Date = 05/17/13 
 Pct Recovery = 50%  Analysis Date = 05/17/13 
 Pct Recovery = 50%  Analysis Date = 05/15/13 
 Pct Recovery = 50%  Analysis Date = 05/15/13 
 Pct Recovery = 50%  Analysis Date = 05/13/13 
 Pct Recovery = 50%  Analysis Date = 05/13/13 
 Pct Recovery = 50%  Analysis Date = 05/10/13 
 Pct Recovery = 50%  Analysis Date = 05/10/13 
 Pct Recovery = 50%  Analysis Date = 05/08/13 
 Pct Recovery = 50%  Analysis Date = 05/08/13 
 Pct Recovery = 50%  Analysis Date = 05/06/13 
 Pct Recovery = 50%  Analysis Date = 05/06/13 
 Pct Recovery = 50%  Analysis Date = 05/03/13 
 Pct Recovery = 50%  Analysis Date = 05/03/13 
 Pct Recovery = 50%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 05/01/13 
 Pct Recovery = 50%  Analysis Date = 04/29/13 
 Pct Recovery = 51%  Analysis Date = 04/29/13 
 Pct Recovery = 51%  Analysis Date = 04/26/13 
 Pct Recovery = 51%  Analysis Date = 04/26/13 
 Pct Recovery = 51%  Analysis Date = 04/24/13 
 Pct Recovery = 51%  Analysis Date = 04/24/13 
 Pct Recovery = 51%  Analysis Date = 04/22/13 
 Pct Recovery = 51%  Analysis Date = 04/22/13 
 Pct Recovery = 51%  Analysis Date = 04/20/13 
 Pct Recovery = 51%  Analysis Date = 04/20/13 
 Pct Recovery = 51%  Analysis Date = 04/17/13 
 Pct Recovery = 52%  Analysis Date = 04/17/13 
 Pct Recovery = 52%  Analysis Date = 04/15/13 
 Pct Recovery = 52%  Analysis Date = 04/15/13 
 Pct Recovery = 52%  Analysis Date = 04/13/13 
 Pct Recovery = 52%  Analysis Date = 04/13/13 
 Pct Recovery = 52%  Analysis Date = 04/10/13 
 Pct Recovery = 52%  Analysis Date = 04/10/13 
 Pct Recovery = 52%  Analysis Date = 04/08/13 
 Pct Recovery = 52%  Analysis Date = 04/08/13 
 Pct Recovery = 52%  Analysis Date = 04/06/13 
 Pct Recovery = 53%  Analysis Date = 04/06/13 
 Pct Recovery = 53%  Analysis Date = 04/03/13 
 Pct Recovery = 53%  Analysis Date = 04/03/13 
 Pct Recovery = 53%  Analysis Date = 04/01/13 
 Pct Recovery = 53%  Analysis Date = 04/01/13 
 Pct Recovery = 53%  Analysis Date = 03/30/13 
 Pct Recovery = 53%  Analysis Date = 03/30/13 
 Pct Recovery = 53%  Analysis Date = 03/27/13 
 Pct Recovery = 53%  Analysis Date = 03/27/13 
 Pct Recovery = 53%  Analysis Date = 03/25/13 
 Pct Recovery = 53%  Analysis Date = 03/25/13 
 Pct Recovery = 53%  Analysis Date = 03/23/13 
 Pct Recovery = 54%  Analysis Date = 03/23/13 
 Pct Recovery = 54%  Analysis Date = 03/21/13 
 Pct Recovery = 54%  Analysis Date = 03/21/13 
 Pct Recovery = 54%  Analysis Date = 03/18/13 
 Pct Recovery = 54%  Analysis Date = 03/18/13 
 Pct Recovery = 54%  Analysis Date = 03/16/13 
 Pct Recovery = 54%  Analysis Date = 03/16/13 
 Pct Recovery = 54%  Analysis Date = 03/14/13 
 Pct Recovery = 54%  Analysis Date = 03/14/13 
 Pct Recovery = 54%  Analysis Date = 03/11/13 
 Pct Recovery = 54%  Analysis Date = 03/11/13 
 Pct Recovery = 54%  Analysis Date = 03/09/13 
 Pct Recovery = 55%  Analysis Date = 03/09/13 
 Pct Recovery = 55%  Analysis Date = 03/07/13 
 Pct Recovery = 55%  Analysis Date = 03/07/13 
 Pct Recovery = 55%  Analysis Date = 03/04/13 
 Pct Recovery = 55%  Analysis Date = 03/04/13 
 Pct Recovery = 55%  Analysis Date = 03/02/13 
 Pct Recovery = 55%  Analysis Date = 03/02/13 
 Pct Recovery = 55%  Analysis Date = 02/28/13 
 Pct Recovery = 55%  Analysis Date = 02/28/13 
 Pct Recovery = 55%  Analysis Date = 02/25/13 
 Pct Recovery = 55%  Analysis Date = 02/25/13 
 Pct Recovery = 55%  Analysis Date = 02/23/13 
 Pct Recovery = 56%  Analysis Date = 02/23/13 
 Pct Recovery = 56%  Analysis Date = 02/21/13 
 Pct Recovery = 56%  Analysis Date = 02/21/13 
 Pct Recovery = 56%  Analysis Date = 02/18/13 
 Pct Recovery = 56%  Analysis Date = 02/18/13 
 Pct Recovery = 56%  Analysis Date = 02/16/13 
 Pct Recovery = 56%  Analysis Date = 02/16/13 
 Pct Recovery = 56%  Analysis Date = 02/14/13 
 Pct Recovery = 56%  Analysis Date = 02/14/13 
 Pct Recovery = 56%  Analysis Date = 02/12/13 
 Pct Recovery = 57%  Analysis Date = 02/12/13 
 Pct Recovery = 57%  Analysis Date = 02/09/13 
 Pct Recovery = 57%  Analysis Date = 02/09/13 
 Pct Recovery = 57%  Analysis Date = 02/07/13 
 Pct Recovery = 57%  Analysis Date = 02/07/13 
 Pct Recovery = 57%  Analysis Date = 02/05/13 
 Pct Recovery = 57%  Analysis Date = 02/05/13 
 Pct Recovery = 57%  Analysis Date = 02/02/13 
 Pct Recovery = 57%  Analysis Date = 02/02/13 
 Pct Recovery = 57%  Analysis Date = 01/31/13 
 Pct Recovery = 57%  Analysis Date = 01/31/13 
 Pct Recovery = 57%  Analysis Date = 01/29/13 
 Pct Recovery = 58%  Analysis Date = 01/29/13 
 Pct Recovery = 58%  Analysis Date = 01/26/13 
 Pct Recovery = 58%  Analysis Date = 01/26/13 
 Pct Recovery = 58%  Analysis Date = 01/24/13 
 Pct Recovery = 58%  Analysis Date = 01/24/13 
 Pct Recovery = 58%  Analysis Date = 01/22/13 
 Pct Recovery = 58%  Analysis Date = 01/22/13 
 Pct Recovery = 58%  Analysis Date = 01/19/13 
 Pct Recovery = 58%  Analysis Date = 01/19/13 
 Pct Recovery = 58%  Analysis Date = 01/17/13 
 Pct Recovery = 58%  Analysis Date = 01/17/13 
 Pct Recovery = 58%  Analysis Date = 01/15/13 
 Pct Recovery = 59%  Analysis Date = 01/15/13 
 Pct Recovery = 59%  Analysis Date = 01/13/13 
 Pct Recovery = 59%  Analysis Date = 01/13/13 
 Pct Recovery = 59%  Analysis Date = 01/10/13 
 Pct Recovery = 59%  Analysis Date = 01/10/13 
 Pct Recovery = 59%  Analysis Date = 01/08/13 
 Pct Recovery = 59%  Analysis Date = 01/08/13 
 Pct Recovery = 59%  Analysis Date = 01/06/13 
 Pct Recovery = 59%  Analysis Date = 01/06/13 
 Pct Recovery = 59%  Analysis Date = 01/03/13 
 Pct Recovery = 59%  Analysis Date = 01/03/13 
 Pct Recovery = 59%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 01/01/13 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/27/12 
 Pct Recovery = 60%  Analysis Date = 12/27/12 
 Pct Recovery = 60%  Analysis Date = 12/25/12 
 Pct Recovery = 60%  Analysis Date = 12/25/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/20/12 
 Pct Recovery = 60%  Analysis Date = 12/20/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 61%  Analysis Date = 12/18/12 
 Pct Recovery = 61%  Analysis Date = 12/16/12 
 Pct Recovery = 61%  Analysis Date = 12/16/12 
 Pct Recovery = 61%  Analysis Date = 12/14/12 
 Pct Recovery = 61%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUTICASONE PROPIONATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 12 51% 17% 51% 16%
Total 12 51% 17% 51% 16%

Sample Statistics
FLUTICASONE PROPIONATE

Characteristic N % % Basis
Plotted 12 80% Spiked
Estimated Values 4 27% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
FLUVOXAMINE
METHOD: LC9017 , TESTIDCODE: 67521LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 41%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 42%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 38%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 49%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 16%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 10%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 25%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 14%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 36%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 14%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 11%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 42%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 18%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 25%  Analysis Date = 04/09/14 
 Pct Recovery = 16%  Analysis Date = 04/07/14 
 Pct Recovery = 16%  Analysis Date = 04/07/14 
 Pct Recovery = 16%  Analysis Date = 04/05/14 
 Pct Recovery = 17%  Analysis Date = 04/05/14 
 Pct Recovery = 17%  Analysis Date = 04/02/14 
 Pct Recovery = 17%  Analysis Date = 04/02/14 
 Pct Recovery = 17%  Analysis Date = 03/31/14 
 Pct Recovery = 17%  Analysis Date = 03/31/14 
 Pct Recovery = 17%  Analysis Date = 03/28/14 
 Pct Recovery = 17%  Analysis Date = 03/28/14 
 Pct Recovery = 17%  Analysis Date = 03/26/14 
 Pct Recovery = 17%  Analysis Date = 03/26/14 
 Pct Recovery = 17%  Analysis Date = 03/24/14 
 Pct Recovery = 17%  Analysis Date = 03/24/14 
 Pct Recovery = 17%  Analysis Date = 03/21/14 
 Pct Recovery = 17%  Analysis Date = 03/21/14 
 Pct Recovery = 17%  Analysis Date = 03/19/14 
 Pct Recovery = 18%  Analysis Date = 03/19/14 
 Pct Recovery = 18%  Analysis Date = 03/16/14 
 Pct Recovery = 18%  Analysis Date = 03/16/14 
 Pct Recovery = 18%  Analysis Date = 03/14/14 
 Pct Recovery = 18%  Analysis Date = 03/14/14 
 Pct Recovery = 18%  Analysis Date = 03/12/14 
 Pct Recovery = 18%  Analysis Date = 03/12/14 
 Pct Recovery = 18%  Analysis Date = 03/09/14 
 Pct Recovery = 18%  Analysis Date = 03/09/14 
 Pct Recovery = 18%  Analysis Date = 03/07/14 
 Pct Recovery = 18%  Analysis Date = 03/07/14 
 Pct Recovery = 18%  Analysis Date = 03/04/14 
 Pct Recovery = 18%  Analysis Date = 03/04/14 
 Pct Recovery = 18%  Analysis Date = 03/02/14 
 Pct Recovery = 18%  Analysis Date = 03/02/14 
 Pct Recovery = 18%  Analysis Date = 02/28/14 
 Pct Recovery = 19%  Analysis Date = 02/28/14 
 Pct Recovery = 19%  Analysis Date = 02/25/14 
 Pct Recovery = 19%  Analysis Date = 02/25/14 
 Pct Recovery = 19%  Analysis Date = 02/23/14 
 Pct Recovery = 19%  Analysis Date = 02/23/14 
 Pct Recovery = 19%  Analysis Date = 02/20/14 
 Pct Recovery = 19%  Analysis Date = 02/20/14 
 Pct Recovery = 19%  Analysis Date = 02/18/14 
 Pct Recovery = 19%  Analysis Date = 02/18/14 
 Pct Recovery = 19%  Analysis Date = 02/15/14 
 Pct Recovery = 19%  Analysis Date = 02/15/14 
 Pct Recovery = 19%  Analysis Date = 02/13/14 
 Pct Recovery = 19%  Analysis Date = 02/13/14 
 Pct Recovery = 19%  Analysis Date = 02/11/14 
 Pct Recovery = 19%  Analysis Date = 02/11/14 
 Pct Recovery = 19%  Analysis Date = 02/08/14 
 Pct Recovery = 20%  Analysis Date = 02/08/14 
 Pct Recovery = 20%  Analysis Date = 02/06/14 
 Pct Recovery = 20%  Analysis Date = 02/06/14 
 Pct Recovery = 20%  Analysis Date = 02/03/14 
 Pct Recovery = 20%  Analysis Date = 02/03/14 
 Pct Recovery = 20%  Analysis Date = 02/01/14 
 Pct Recovery = 20%  Analysis Date = 02/01/14 
 Pct Recovery = 20%  Analysis Date = 01/30/14 
 Pct Recovery = 20%  Analysis Date = 01/30/14 
 Pct Recovery = 20%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/22/14 
 Pct Recovery = 21%  Analysis Date = 01/22/14 
 Pct Recovery = 21%  Analysis Date = 01/20/14 
 Pct Recovery = 21%  Analysis Date = 01/20/14 
 Pct Recovery = 21%  Analysis Date = 01/18/14 
 Pct Recovery = 21%  Analysis Date = 01/18/14 
 Pct Recovery = 21%  Analysis Date = 01/15/14 
 Pct Recovery = 21%  Analysis Date = 01/15/14 
 Pct Recovery = 21%  Analysis Date = 01/13/14 
 Pct Recovery = 21%  Analysis Date = 01/13/14 
 Pct Recovery = 21%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/06/14 
 Pct Recovery = 21%  Analysis Date = 01/06/14 
 Pct Recovery = 21%  Analysis Date = 01/03/14 
 Pct Recovery = 21%  Analysis Date = 01/03/14 
 Pct Recovery = 21%  Analysis Date = 01/01/14 
 Pct Recovery = 22%  Analysis Date = 01/01/14 
 Pct Recovery = 22%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/27/13 
 Pct Recovery = 22%  Analysis Date = 12/27/13 
 Pct Recovery = 22%  Analysis Date = 12/24/13 
 Pct Recovery = 22%  Analysis Date = 12/24/13 
 Pct Recovery = 22%  Analysis Date = 12/22/13 
 Pct Recovery = 22%  Analysis Date = 12/22/13 
 Pct Recovery = 22%  Analysis Date = 12/20/13 
 Pct Recovery = 22%  Analysis Date = 12/20/13 
 Pct Recovery = 22%  Analysis Date = 12/17/13 
 Pct Recovery = 22%  Analysis Date = 12/17/13 
 Pct Recovery = 22%  Analysis Date = 12/15/13 
 Pct Recovery = 22%  Analysis Date = 12/15/13 
 Pct Recovery = 22%  Analysis Date = 12/12/13 
 Pct Recovery = 22%  Analysis Date = 12/12/13 
 Pct Recovery = 22%  Analysis Date = 12/10/13 
 Pct Recovery = 22%  Analysis Date = 12/10/13 
 Pct Recovery = 22%  Analysis Date = 12/08/13 
 Pct Recovery = 23%  Analysis Date = 12/08/13 
 Pct Recovery = 23%  Analysis Date = 12/05/13 
 Pct Recovery = 23%  Analysis Date = 12/05/13 
 Pct Recovery = 23%  Analysis Date = 12/03/13 
 Pct Recovery = 23%  Analysis Date = 12/03/13 
 Pct Recovery = 23%  Analysis Date = 11/30/13 
 Pct Recovery = 23%  Analysis Date = 11/30/13 
 Pct Recovery = 23%  Analysis Date = 11/28/13 
 Pct Recovery = 23%  Analysis Date = 11/28/13 
 Pct Recovery = 23%  Analysis Date = 11/26/13 
 Pct Recovery = 23%  Analysis Date = 11/26/13 
 Pct Recovery = 23%  Analysis Date = 11/23/13 
 Pct Recovery = 23%  Analysis Date = 11/23/13 
 Pct Recovery = 23%  Analysis Date = 11/21/13 
 Pct Recovery = 23%  Analysis Date = 11/21/13 
 Pct Recovery = 23%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/18/13 
 Pct Recovery = 23%  Analysis Date = 11/16/13 
 Pct Recovery = 24%  Analysis Date = 11/16/13 
 Pct Recovery = 24%  Analysis Date = 11/13/13 
 Pct Recovery = 24%  Analysis Date = 11/13/13 
 Pct Recovery = 24%  Analysis Date = 11/11/13 
 Pct Recovery = 24%  Analysis Date = 11/11/13 
 Pct Recovery = 24%  Analysis Date = 11/09/13 
 Pct Recovery = 24%  Analysis Date = 11/09/13 
 Pct Recovery = 24%  Analysis Date = 11/06/13 
 Pct Recovery = 24%  Analysis Date = 11/06/13 
 Pct Recovery = 24%  Analysis Date = 11/04/13 
 Pct Recovery = 24%  Analysis Date = 11/04/13 
 Pct Recovery = 24%  Analysis Date = 11/01/13 
 Pct Recovery = 24%  Analysis Date = 11/01/13 
 Pct Recovery = 24%  Analysis Date = 10/30/13 
 Pct Recovery = 24%  Analysis Date = 10/30/13 
 Pct Recovery = 24%  Analysis Date = 10/28/13 
 Pct Recovery = 24%  Analysis Date = 10/28/13 
 Pct Recovery = 24%  Analysis Date = 10/25/13 
 Pct Recovery = 25%  Analysis Date = 10/25/13 
 Pct Recovery = 25%  Analysis Date = 10/23/13 
 Pct Recovery = 25%  Analysis Date = 10/23/13 
 Pct Recovery = 25%  Analysis Date = 10/20/13 
 Pct Recovery = 25%  Analysis Date = 10/20/13 
 Pct Recovery = 25%  Analysis Date = 10/18/13 
 Pct Recovery = 25%  Analysis Date = 10/18/13 
 Pct Recovery = 25%  Analysis Date = 10/16/13 
 Pct Recovery = 26%  Analysis Date = 10/16/13 
 Pct Recovery = 26%  Analysis Date = 10/13/13 
 Pct Recovery = 26%  Analysis Date = 10/13/13 
 Pct Recovery = 26%  Analysis Date = 10/11/13 
 Pct Recovery = 26%  Analysis Date = 10/11/13 
 Pct Recovery = 26%  Analysis Date = 10/08/13 
 Pct Recovery = 26%  Analysis Date = 10/08/13 
 Pct Recovery = 26%  Analysis Date = 10/06/13 
 Pct Recovery = 26%  Analysis Date = 10/06/13 
 Pct Recovery = 26%  Analysis Date = 10/04/13 
 Pct Recovery = 27%  Analysis Date = 10/04/13 
 Pct Recovery = 27%  Analysis Date = 10/01/13 
 Pct Recovery = 27%  Analysis Date = 10/01/13 
 Pct Recovery = 27%  Analysis Date = 09/29/13 
 Pct Recovery = 27%  Analysis Date = 09/29/13 
 Pct Recovery = 27%  Analysis Date = 09/26/13 
 Pct Recovery = 27%  Analysis Date = 09/26/13 
 Pct Recovery = 27%  Analysis Date = 09/24/13 
 Pct Recovery = 28%  Analysis Date = 09/24/13 
 Pct Recovery = 28%  Analysis Date = 09/21/13 
 Pct Recovery = 28%  Analysis Date = 09/21/13 
 Pct Recovery = 28%  Analysis Date = 09/19/13 
 Pct Recovery = 28%  Analysis Date = 09/19/13 
 Pct Recovery = 28%  Analysis Date = 09/17/13 
 Pct Recovery = 28%  Analysis Date = 09/17/13 
 Pct Recovery = 28%  Analysis Date = 09/14/13 
 Pct Recovery = 29%  Analysis Date = 09/14/13 
 Pct Recovery = 29%  Analysis Date = 09/12/13 
 Pct Recovery = 29%  Analysis Date = 09/12/13 
 Pct Recovery = 29%  Analysis Date = 09/09/13 
 Pct Recovery = 29%  Analysis Date = 09/09/13 
 Pct Recovery = 29%  Analysis Date = 09/07/13 
 Pct Recovery = 29%  Analysis Date = 09/07/13 
 Pct Recovery = 29%  Analysis Date = 09/05/13 
 Pct Recovery = 29%  Analysis Date = 09/05/13 
 Pct Recovery = 29%  Analysis Date = 09/02/13 
 Pct Recovery = 30%  Analysis Date = 09/02/13 
 Pct Recovery = 30%  Analysis Date = 08/31/13 
 Pct Recovery = 30%  Analysis Date = 08/31/13 
 Pct Recovery = 30%  Analysis Date = 08/28/13 
 Pct Recovery = 30%  Analysis Date = 08/28/13 
 Pct Recovery = 30%  Analysis Date = 08/26/13 
 Pct Recovery = 30%  Analysis Date = 08/26/13 
 Pct Recovery = 30%  Analysis Date = 08/24/13 
 Pct Recovery = 31%  Analysis Date = 08/24/13 
 Pct Recovery = 31%  Analysis Date = 08/21/13 
 Pct Recovery = 31%  Analysis Date = 08/21/13 
 Pct Recovery = 31%  Analysis Date = 08/19/13 
 Pct Recovery = 31%  Analysis Date = 08/19/13 
 Pct Recovery = 31%  Analysis Date = 08/16/13 
 Pct Recovery = 31%  Analysis Date = 08/16/13 
 Pct Recovery = 31%  Analysis Date = 08/14/13 
 Pct Recovery = 31%  Analysis Date = 08/14/13 
 Pct Recovery = 31%  Analysis Date = 08/11/13 
 Pct Recovery = 32%  Analysis Date = 08/11/13 
 Pct Recovery = 32%  Analysis Date = 08/09/13 
 Pct Recovery = 32%  Analysis Date = 08/09/13 
 Pct Recovery = 32%  Analysis Date = 08/07/13 
 Pct Recovery = 32%  Analysis Date = 08/07/13 
 Pct Recovery = 32%  Analysis Date = 08/04/13 
 Pct Recovery = 32%  Analysis Date = 08/04/13 
 Pct Recovery = 32%  Analysis Date = 08/02/13 
 Pct Recovery = 32%  Analysis Date = 08/02/13 
 Pct Recovery = 32%  Analysis Date = 07/30/13 
 Pct Recovery = 32%  Analysis Date = 07/30/13 
 Pct Recovery = 32%  Analysis Date = 07/28/13 
 Pct Recovery = 32%  Analysis Date = 07/28/13 
 Pct Recovery = 32%  Analysis Date = 07/26/13 
 Pct Recovery = 33%  Analysis Date = 07/26/13 
 Pct Recovery = 33%  Analysis Date = 07/23/13 
 Pct Recovery = 33%  Analysis Date = 07/23/13 
 Pct Recovery = 33%  Analysis Date = 07/21/13 
 Pct Recovery = 33%  Analysis Date = 07/21/13 
 Pct Recovery = 33%  Analysis Date = 07/18/13 
 Pct Recovery = 33%  Analysis Date = 07/18/13 
 Pct Recovery = 33%  Analysis Date = 07/16/13 
 Pct Recovery = 33%  Analysis Date = 07/16/13 
 Pct Recovery = 33%  Analysis Date = 07/14/13 
 Pct Recovery = 33%  Analysis Date = 07/14/13 
 Pct Recovery = 33%  Analysis Date = 07/11/13 
 Pct Recovery = 34%  Analysis Date = 07/11/13 
 Pct Recovery = 34%  Analysis Date = 07/09/13 
 Pct Recovery = 34%  Analysis Date = 07/09/13 
 Pct Recovery = 34%  Analysis Date = 07/06/13 
 Pct Recovery = 34%  Analysis Date = 07/06/13 
 Pct Recovery = 34%  Analysis Date = 07/04/13 
 Pct Recovery = 34%  Analysis Date = 07/04/13 
 Pct Recovery = 34%  Analysis Date = 07/02/13 
 Pct Recovery = 34%  Analysis Date = 07/02/13 
 Pct Recovery = 34%  Analysis Date = 06/29/13 
 Pct Recovery = 34%  Analysis Date = 06/29/13 
 Pct Recovery = 34%  Analysis Date = 06/27/13 
 Pct Recovery = 35%  Analysis Date = 06/27/13 
 Pct Recovery = 35%  Analysis Date = 06/24/13 
 Pct Recovery = 35%  Analysis Date = 06/24/13 
 Pct Recovery = 35%  Analysis Date = 06/22/13 
 Pct Recovery = 35%  Analysis Date = 06/22/13 
 Pct Recovery = 35%  Analysis Date = 06/19/13 
 Pct Recovery = 35%  Analysis Date = 06/19/13 
 Pct Recovery = 35%  Analysis Date = 06/17/13 
 Pct Recovery = 35%  Analysis Date = 06/17/13 
 Pct Recovery = 35%  Analysis Date = 06/15/13 
 Pct Recovery = 35%  Analysis Date = 06/15/13 
 Pct Recovery = 35%  Analysis Date = 06/12/13 
 Pct Recovery = 36%  Analysis Date = 06/12/13 
 Pct Recovery = 36%  Analysis Date = 06/10/13 
 Pct Recovery = 36%  Analysis Date = 06/10/13 
 Pct Recovery = 36%  Analysis Date = 06/07/13 
 Pct Recovery = 36%  Analysis Date = 06/07/13 
 Pct Recovery = 36%  Analysis Date = 06/05/13 
 Pct Recovery = 36%  Analysis Date = 06/05/13 
 Pct Recovery = 36%  Analysis Date = 06/03/13 
 Pct Recovery = 36%  Analysis Date = 06/03/13 
 Pct Recovery = 36%  Analysis Date = 05/31/13 
 Pct Recovery = 36%  Analysis Date = 05/31/13 
 Pct Recovery = 36%  Analysis Date = 05/29/13 
 Pct Recovery = 36%  Analysis Date = 05/29/13 
 Pct Recovery = 36%  Analysis Date = 05/26/13 
 Pct Recovery = 37%  Analysis Date = 05/26/13 
 Pct Recovery = 37%  Analysis Date = 05/24/13 
 Pct Recovery = 37%  Analysis Date = 05/24/13 
 Pct Recovery = 37%  Analysis Date = 05/22/13 
 Pct Recovery = 37%  Analysis Date = 05/22/13 
 Pct Recovery = 37%  Analysis Date = 05/19/13 
 Pct Recovery = 37%  Analysis Date = 05/19/13 
 Pct Recovery = 37%  Analysis Date = 05/17/13 
 Pct Recovery = 37%  Analysis Date = 05/17/13 
 Pct Recovery = 37%  Analysis Date = 05/14/13 
 Pct Recovery = 37%  Analysis Date = 05/14/13 
 Pct Recovery = 37%  Analysis Date = 05/12/13 
 Pct Recovery = 38%  Analysis Date = 05/12/13 
 Pct Recovery = 38%  Analysis Date = 05/10/13 
 Pct Recovery = 38%  Analysis Date = 05/10/13 
 Pct Recovery = 38%  Analysis Date = 05/07/13 
 Pct Recovery = 38%  Analysis Date = 05/07/13 
 Pct Recovery = 38%  Analysis Date = 05/05/13 
 Pct Recovery = 38%  Analysis Date = 05/05/13 
 Pct Recovery = 38%  Analysis Date = 05/02/13 
 Pct Recovery = 38%  Analysis Date = 05/02/13 
 Pct Recovery = 38%  Analysis Date = 04/30/13 
 Pct Recovery = 37%  Analysis Date = 04/30/13 
 Pct Recovery = 37%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/25/13 
 Pct Recovery = 32%  Analysis Date = 04/25/13 
 Pct Recovery = 32%  Analysis Date = 04/23/13 
 Pct Recovery = 32%  Analysis Date = 04/23/13 
 Pct Recovery = 32%  Analysis Date = 04/20/13 
 Pct Recovery = 32%  Analysis Date = 04/20/13 
 Pct Recovery = 32%  Analysis Date = 04/18/13 
 Pct Recovery = 32%  Analysis Date = 04/18/13 
 Pct Recovery = 32%  Analysis Date = 04/15/13 
 Pct Recovery = 32%  Analysis Date = 04/15/13 
 Pct Recovery = 32%  Analysis Date = 04/13/13 
 Pct Recovery = 32%  Analysis Date = 04/13/13 
 Pct Recovery = 32%  Analysis Date = 04/11/13 
 Pct Recovery = 31%  Analysis Date = 04/11/13 
 Pct Recovery = 31%  Analysis Date = 04/08/13 
 Pct Recovery = 31%  Analysis Date = 04/08/13 
 Pct Recovery = 31%  Analysis Date = 04/06/13 
 Pct Recovery = 31%  Analysis Date = 04/06/13 
 Pct Recovery = 31%  Analysis Date = 04/03/13 
 Pct Recovery = 31%  Analysis Date = 04/03/13 
 Pct Recovery = 31%  Analysis Date = 04/01/13 
 Pct Recovery = 31%  Analysis Date = 04/01/13 
 Pct Recovery = 31%  Analysis Date = 03/30/13 
 Pct Recovery = 31%  Analysis Date = 03/30/13 
 Pct Recovery = 31%  Analysis Date = 03/27/13 
 Pct Recovery = 31%  Analysis Date = 03/27/13 
 Pct Recovery = 31%  Analysis Date = 03/25/13 
 Pct Recovery = 31%  Analysis Date = 03/25/13 
 Pct Recovery = 31%  Analysis Date = 03/22/13 
 Pct Recovery = 31%  Analysis Date = 03/22/13 
 Pct Recovery = 31%  Analysis Date = 03/20/13 
 Pct Recovery = 31%  Analysis Date = 03/20/13 
 Pct Recovery = 31%  Analysis Date = 03/17/13 
 Pct Recovery = 31%  Analysis Date = 03/17/13 
 Pct Recovery = 31%  Analysis Date = 03/15/13 
 Pct Recovery = 31%  Analysis Date = 03/15/13 
 Pct Recovery = 31%  Analysis Date = 03/13/13 
 Pct Recovery = 31%  Analysis Date = 03/13/13 
 Pct Recovery = 31%  Analysis Date = 03/10/13 
 Pct Recovery = 32%  Analysis Date = 03/10/13 
 Pct Recovery = 32%  Analysis Date = 03/08/13 
 Pct Recovery = 32%  Analysis Date = 03/08/13 
 Pct Recovery = 32%  Analysis Date = 03/05/13 
 Pct Recovery = 32%  Analysis Date = 03/05/13 
 Pct Recovery = 32%  Analysis Date = 03/03/13 
 Pct Recovery = 32%  Analysis Date = 03/03/13 
 Pct Recovery = 32%  Analysis Date = 03/01/13 
 Pct Recovery = 32%  Analysis Date = 03/01/13 
 Pct Recovery = 32%  Analysis Date = 02/26/13 
 Pct Recovery = 32%  Analysis Date = 02/26/13 
 Pct Recovery = 32%  Analysis Date = 02/24/13 
 Pct Recovery = 32%  Analysis Date = 02/24/13 
 Pct Recovery = 32%  Analysis Date = 02/21/13 
 Pct Recovery = 33%  Analysis Date = 02/21/13 
 Pct Recovery = 33%  Analysis Date = 02/19/13 
 Pct Recovery = 33%  Analysis Date = 02/19/13 
 Pct Recovery = 33%  Analysis Date = 02/17/13 
 Pct Recovery = 33%  Analysis Date = 02/17/13 
 Pct Recovery = 33%  Analysis Date = 02/14/13 
 Pct Recovery = 33%  Analysis Date = 02/14/13 
 Pct Recovery = 33%  Analysis Date = 02/12/13 
 Pct Recovery = 33%  Analysis Date = 02/12/13 
 Pct Recovery = 33%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/07/13 
 Pct Recovery = 34%  Analysis Date = 02/07/13 
 Pct Recovery = 34%  Analysis Date = 02/05/13 
 Pct Recovery = 34%  Analysis Date = 02/05/13 
 Pct Recovery = 34%  Analysis Date = 02/02/13 
 Pct Recovery = 34%  Analysis Date = 02/02/13 
 Pct Recovery = 34%  Analysis Date = 01/31/13 
 Pct Recovery = 34%  Analysis Date = 01/31/13 
 Pct Recovery = 34%  Analysis Date = 01/28/13 
 Pct Recovery = 34%  Analysis Date = 01/28/13 
 Pct Recovery = 34%  Analysis Date = 01/26/13 
 Pct Recovery = 34%  Analysis Date = 01/26/13 
 Pct Recovery = 34%  Analysis Date = 01/23/13 
 Pct Recovery = 34%  Analysis Date = 01/23/13 
 Pct Recovery = 34%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/19/13 
 Pct Recovery = 35%  Analysis Date = 01/19/13 
 Pct Recovery = 35%  Analysis Date = 01/16/13 
 Pct Recovery = 35%  Analysis Date = 01/16/13 
 Pct Recovery = 35%  Analysis Date = 01/14/13 
 Pct Recovery = 35%  Analysis Date = 01/14/13 
 Pct Recovery = 35%  Analysis Date = 01/11/13 
 Pct Recovery = 35%  Analysis Date = 01/11/13 
 Pct Recovery = 35%  Analysis Date = 01/09/13 
 Pct Recovery = 35%  Analysis Date = 01/09/13 
 Pct Recovery = 35%  Analysis Date = 01/07/13 
 Pct Recovery = 35%  Analysis Date = 01/07/13 
 Pct Recovery = 35%  Analysis Date = 01/04/13 
 Pct Recovery = 36%  Analysis Date = 01/04/13 
 Pct Recovery = 36%  Analysis Date = 01/02/13 
 Pct Recovery = 36%  Analysis Date = 01/02/13 
 Pct Recovery = 36%  Analysis Date = 12/30/12 
 Pct Recovery = 36%  Analysis Date = 12/30/12 
 Pct Recovery = 36%  Analysis Date = 12/28/12 
 Pct Recovery = 36%  Analysis Date = 12/28/12 
 Pct Recovery = 36%  Analysis Date = 12/26/12 
 Pct Recovery = 36%  Analysis Date = 12/26/12 
 Pct Recovery = 36%  Analysis Date = 12/23/12 
 Pct Recovery = 36%  Analysis Date = 12/23/12 
 Pct Recovery = 36%  Analysis Date = 12/21/12 
 Pct Recovery = 36%  Analysis Date = 12/21/12 
 Pct Recovery = 36%  Analysis Date = 12/18/12 
 Pct Recovery = 37%  Analysis Date = 12/18/12 
 Pct Recovery = 37%  Analysis Date = 12/16/12 
 Pct Recovery = 37%  Analysis Date = 12/16/12 
 Pct Recovery = 37%  Analysis Date = 12/14/12 
 Pct Recovery = 37%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUVOXAMINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 25% . 25% 0%
>= Reporting Level 13 28% 14% 25% 20%
Total 14 27% 14% 25% 20%

Sample Statistics
FLUVOXAMINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 14 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
GLIPIZIDE
METHOD: LC9017 , TESTIDCODE: 68001LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 157%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 157%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 182%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 66%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 113%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 162%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 171%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 83%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 52%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 170%  Analysis Date = 03/21/14 
 Pct Recovery = 73%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/14/14 
 Pct Recovery = 75%  Analysis Date = 03/11/14 
 Pct Recovery = 76%  Analysis Date = 03/11/14 
 Pct Recovery = 76%  Analysis Date = 03/09/14 
 Pct Recovery = 77%  Analysis Date = 03/09/14 
 Pct Recovery = 77%  Analysis Date = 03/07/14 
 Pct Recovery = 78%  Analysis Date = 03/07/14 
 Pct Recovery = 78%  Analysis Date = 03/04/14 
 Pct Recovery = 78%  Analysis Date = 03/04/14 
 Pct Recovery = 78%  Analysis Date = 03/02/14 
 Pct Recovery = 79%  Analysis Date = 03/02/14 
 Pct Recovery = 79%  Analysis Date = 02/28/14 
 Pct Recovery = 80%  Analysis Date = 02/28/14 
 Pct Recovery = 80%  Analysis Date = 02/25/14 
 Pct Recovery = 81%  Analysis Date = 02/25/14 
 Pct Recovery = 81%  Analysis Date = 02/23/14 
 Pct Recovery = 82%  Analysis Date = 02/23/14 
 Pct Recovery = 82%  Analysis Date = 02/21/14 
 Pct Recovery = 82%  Analysis Date = 02/21/14 
 Pct Recovery = 82%  Analysis Date = 02/18/14 
 Pct Recovery = 83%  Analysis Date = 02/18/14 
 Pct Recovery = 83%  Analysis Date = 02/16/14 
 Pct Recovery = 83%  Analysis Date = 02/16/14 
 Pct Recovery = 83%  Analysis Date = 02/14/14 
 Pct Recovery = 82%  Analysis Date = 02/14/14 
 Pct Recovery = 82%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/09/14 
 Pct Recovery = 82%  Analysis Date = 02/09/14 
 Pct Recovery = 82%  Analysis Date = 02/07/14 
 Pct Recovery = 81%  Analysis Date = 02/07/14 
 Pct Recovery = 81%  Analysis Date = 02/05/14 
 Pct Recovery = 81%  Analysis Date = 02/05/14 
 Pct Recovery = 81%  Analysis Date = 02/02/14 
 Pct Recovery = 80%  Analysis Date = 02/02/14 
 Pct Recovery = 80%  Analysis Date = 01/31/14 
 Pct Recovery = 80%  Analysis Date = 01/31/14 
 Pct Recovery = 80%  Analysis Date = 01/29/14 
 Pct Recovery = 79%  Analysis Date = 01/29/14 
 Pct Recovery = 79%  Analysis Date = 01/26/14 
 Pct Recovery = 79%  Analysis Date = 01/26/14 
 Pct Recovery = 79%  Analysis Date = 01/24/14 
 Pct Recovery = 79%  Analysis Date = 01/24/14 
 Pct Recovery = 79%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/22/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/19/14 
 Pct Recovery = 78%  Analysis Date = 01/17/14 
 Pct Recovery = 77%  Analysis Date = 01/17/14 
 Pct Recovery = 77%  Analysis Date = 01/15/14 
 Pct Recovery = 77%  Analysis Date = 01/15/14 
 Pct Recovery = 77%  Analysis Date = 01/13/14 
 Pct Recovery = 77%  Analysis Date = 01/13/14 
 Pct Recovery = 77%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/01/14 
 Pct Recovery = 75%  Analysis Date = 01/01/14 
 Pct Recovery = 75%  Analysis Date = 12/30/13 
 Pct Recovery = 74%  Analysis Date = 12/30/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/25/13 
 Pct Recovery = 73%  Analysis Date = 12/25/13 
 Pct Recovery = 73%  Analysis Date = 12/23/13 
 Pct Recovery = 73%  Analysis Date = 12/23/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/13/13 
 Pct Recovery = 71%  Analysis Date = 12/13/13 
 Pct Recovery = 71%  Analysis Date = 12/11/13 
 Pct Recovery = 71%  Analysis Date = 12/11/13 
 Pct Recovery = 71%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 12/02/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/27/13 
 Pct Recovery = 68%  Analysis Date = 11/27/13 
 Pct Recovery = 68%  Analysis Date = 11/25/13 
 Pct Recovery = 68%  Analysis Date = 11/25/13 
 Pct Recovery = 68%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/20/13 
 Pct Recovery = 67%  Analysis Date = 11/20/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/07/13 
 Pct Recovery = 65%  Analysis Date = 11/07/13 
 Pct Recovery = 65%  Analysis Date = 11/04/13 
 Pct Recovery = 64%  Analysis Date = 11/04/13 
 Pct Recovery = 64%  Analysis Date = 11/02/13 
 Pct Recovery = 64%  Analysis Date = 11/02/13 
 Pct Recovery = 64%  Analysis Date = 10/31/13 
 Pct Recovery = 63%  Analysis Date = 10/31/13 
 Pct Recovery = 63%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/26/13 
 Pct Recovery = 63%  Analysis Date = 10/26/13 
 Pct Recovery = 63%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/19/13 
 Pct Recovery = 61%  Analysis Date = 10/19/13 
 Pct Recovery = 61%  Analysis Date = 10/17/13 
 Pct Recovery = 61%  Analysis Date = 10/17/13 
 Pct Recovery = 61%  Analysis Date = 10/14/13 
 Pct Recovery = 61%  Analysis Date = 10/14/13 
 Pct Recovery = 61%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 58%  Analysis Date = 10/01/13 
 Pct Recovery = 58%  Analysis Date = 09/28/13 
 Pct Recovery = 58%  Analysis Date = 09/28/13 
 Pct Recovery = 58%  Analysis Date = 09/26/13 
 Pct Recovery = 57%  Analysis Date = 09/26/13 
 Pct Recovery = 57%  Analysis Date = 09/24/13 
 Pct Recovery = 57%  Analysis Date = 09/24/13 
 Pct Recovery = 57%  Analysis Date = 09/21/13 
 Pct Recovery = 57%  Analysis Date = 09/21/13 
 Pct Recovery = 57%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/17/13 
 Pct Recovery = 56%  Analysis Date = 09/17/13 
 Pct Recovery = 56%  Analysis Date = 09/14/13 
 Pct Recovery = 55%  Analysis Date = 09/14/13 
 Pct Recovery = 55%  Analysis Date = 09/12/13 
 Pct Recovery = 55%  Analysis Date = 09/12/13 
 Pct Recovery = 55%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/07/13 
 Pct Recovery = 54%  Analysis Date = 09/07/13 
 Pct Recovery = 54%  Analysis Date = 09/05/13 
 Pct Recovery = 54%  Analysis Date = 09/05/13 
 Pct Recovery = 54%  Analysis Date = 09/03/13 
 Pct Recovery = 53%  Analysis Date = 09/03/13 
 Pct Recovery = 53%  Analysis Date = 09/01/13 
 Pct Recovery = 53%  Analysis Date = 09/01/13 
 Pct Recovery = 53%  Analysis Date = 08/29/13 
 Pct Recovery = 52%  Analysis Date = 08/29/13 
 Pct Recovery = 52%  Analysis Date = 08/27/13 
 Pct Recovery = 54%  Analysis Date = 08/27/13 
 Pct Recovery = 54%  Analysis Date = 08/25/13 
 Pct Recovery = 55%  Analysis Date = 08/25/13 
 Pct Recovery = 55%  Analysis Date = 08/22/13 
 Pct Recovery = 57%  Analysis Date = 08/22/13 
 Pct Recovery = 57%  Analysis Date = 08/20/13 
 Pct Recovery = 59%  Analysis Date = 08/20/13 
 Pct Recovery = 59%  Analysis Date = 08/18/13 
 Pct Recovery = 61%  Analysis Date = 08/18/13 
 Pct Recovery = 61%  Analysis Date = 08/15/13 
 Pct Recovery = 63%  Analysis Date = 08/15/13 
 Pct Recovery = 63%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/08/13 
 Pct Recovery = 69%  Analysis Date = 08/08/13 
 Pct Recovery = 69%  Analysis Date = 08/06/13 
 Pct Recovery = 71%  Analysis Date = 08/06/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 78%  Analysis Date = 07/28/13 
 Pct Recovery = 78%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 84%  Analysis Date = 07/21/13 
 Pct Recovery = 84%  Analysis Date = 07/19/13 
 Pct Recovery = 86%  Analysis Date = 07/19/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 88%  Analysis Date = 07/16/13 
 Pct Recovery = 88%  Analysis Date = 07/14/13 
 Pct Recovery = 90%  Analysis Date = 07/14/13 
 Pct Recovery = 90%  Analysis Date = 07/12/13 
 Pct Recovery = 92%  Analysis Date = 07/12/13 
 Pct Recovery = 92%  Analysis Date = 07/09/13 
 Pct Recovery = 94%  Analysis Date = 07/09/13 
 Pct Recovery = 94%  Analysis Date = 07/07/13 
 Pct Recovery = 96%  Analysis Date = 07/07/13 
 Pct Recovery = 96%  Analysis Date = 07/05/13 
 Pct Recovery = 98%  Analysis Date = 07/05/13 
 Pct Recovery = 98%  Analysis Date = 07/02/13 
 Pct Recovery = 100%  Analysis Date = 07/02/13 
 Pct Recovery = 100%  Analysis Date = 06/30/13 
 Pct Recovery = 102%  Analysis Date = 06/30/13 
 Pct Recovery = 102%  Analysis Date = 06/28/13 
 Pct Recovery = 104%  Analysis Date = 06/28/13 
 Pct Recovery = 104%  Analysis Date = 06/26/13 
 Pct Recovery = 106%  Analysis Date = 06/26/13 
 Pct Recovery = 106%  Analysis Date = 06/23/13 
 Pct Recovery = 108%  Analysis Date = 06/23/13 
 Pct Recovery = 108%  Analysis Date = 06/21/13 
 Pct Recovery = 110%  Analysis Date = 06/21/13 
 Pct Recovery = 110%  Analysis Date = 06/19/13 
 Pct Recovery = 112%  Analysis Date = 06/19/13 
 Pct Recovery = 112%  Analysis Date = 06/16/13 
 Pct Recovery = 114%  Analysis Date = 06/16/13 
 Pct Recovery = 114%  Analysis Date = 06/14/13 
 Pct Recovery = 116%  Analysis Date = 06/14/13 
 Pct Recovery = 116%  Analysis Date = 06/12/13 
 Pct Recovery = 118%  Analysis Date = 06/12/13 
 Pct Recovery = 118%  Analysis Date = 06/09/13 
 Pct Recovery = 120%  Analysis Date = 06/09/13 
 Pct Recovery = 120%  Analysis Date = 06/07/13 
 Pct Recovery = 122%  Analysis Date = 06/07/13 
 Pct Recovery = 122%  Analysis Date = 06/05/13 
 Pct Recovery = 124%  Analysis Date = 06/05/13 
 Pct Recovery = 124%  Analysis Date = 06/02/13 
 Pct Recovery = 126%  Analysis Date = 06/02/13 
 Pct Recovery = 126%  Analysis Date = 05/31/13 
 Pct Recovery = 128%  Analysis Date = 05/31/13 
 Pct Recovery = 128%  Analysis Date = 05/29/13 
 Pct Recovery = 130%  Analysis Date = 05/29/13 
 Pct Recovery = 130%  Analysis Date = 05/27/13 
 Pct Recovery = 132%  Analysis Date = 05/27/13 
 Pct Recovery = 132%  Analysis Date = 05/24/13 
 Pct Recovery = 134%  Analysis Date = 05/24/13 
 Pct Recovery = 134%  Analysis Date = 05/22/13 
 Pct Recovery = 136%  Analysis Date = 05/22/13 
 Pct Recovery = 136%  Analysis Date = 05/20/13 
 Pct Recovery = 138%  Analysis Date = 05/20/13 
 Pct Recovery = 138%  Analysis Date = 05/17/13 
 Pct Recovery = 140%  Analysis Date = 05/17/13 
 Pct Recovery = 140%  Analysis Date = 05/15/13 
 Pct Recovery = 142%  Analysis Date = 05/15/13 
 Pct Recovery = 142%  Analysis Date = 05/13/13 
 Pct Recovery = 144%  Analysis Date = 05/13/13 
 Pct Recovery = 144%  Analysis Date = 05/10/13 
 Pct Recovery = 146%  Analysis Date = 05/10/13 
 Pct Recovery = 146%  Analysis Date = 05/08/13 
 Pct Recovery = 148%  Analysis Date = 05/08/13 
 Pct Recovery = 148%  Analysis Date = 05/06/13 
 Pct Recovery = 150%  Analysis Date = 05/06/13 
 Pct Recovery = 150%  Analysis Date = 05/03/13 
 Pct Recovery = 152%  Analysis Date = 05/03/13 
 Pct Recovery = 152%  Analysis Date = 05/01/13 
 Pct Recovery = 153%  Analysis Date = 05/01/13 
 Pct Recovery = 153%  Analysis Date = 04/29/13 
 Pct Recovery = 154%  Analysis Date = 04/29/13 
 Pct Recovery = 154%  Analysis Date = 04/26/13 
 Pct Recovery = 155%  Analysis Date = 04/26/13 
 Pct Recovery = 155%  Analysis Date = 04/24/13 
 Pct Recovery = 155%  Analysis Date = 04/24/13 
 Pct Recovery = 155%  Analysis Date = 04/22/13 
 Pct Recovery = 156%  Analysis Date = 04/22/13 
 Pct Recovery = 156%  Analysis Date = 04/20/13 
 Pct Recovery = 157%  Analysis Date = 04/20/13 
 Pct Recovery = 157%  Analysis Date = 04/17/13 
 Pct Recovery = 158%  Analysis Date = 04/17/13 
 Pct Recovery = 158%  Analysis Date = 04/15/13 
 Pct Recovery = 159%  Analysis Date = 04/15/13 
 Pct Recovery = 159%  Analysis Date = 04/13/13 
 Pct Recovery = 159%  Analysis Date = 04/13/13 
 Pct Recovery = 159%  Analysis Date = 04/10/13 
 Pct Recovery = 160%  Analysis Date = 04/10/13 
 Pct Recovery = 160%  Analysis Date = 04/08/13 
 Pct Recovery = 161%  Analysis Date = 04/08/13 
 Pct Recovery = 161%  Analysis Date = 04/06/13 
 Pct Recovery = 162%  Analysis Date = 04/06/13 
 Pct Recovery = 162%  Analysis Date = 04/03/13 
 Pct Recovery = 163%  Analysis Date = 04/03/13 
 Pct Recovery = 163%  Analysis Date = 04/01/13 
 Pct Recovery = 163%  Analysis Date = 04/01/13 
 Pct Recovery = 163%  Analysis Date = 03/30/13 
 Pct Recovery = 164%  Analysis Date = 03/30/13 
 Pct Recovery = 164%  Analysis Date = 03/27/13 
 Pct Recovery = 165%  Analysis Date = 03/27/13 
 Pct Recovery = 165%  Analysis Date = 03/25/13 
 Pct Recovery = 165%  Analysis Date = 03/25/13 
 Pct Recovery = 165%  Analysis Date = 03/23/13 
 Pct Recovery = 166%  Analysis Date = 03/23/13 
 Pct Recovery = 166%  Analysis Date = 03/21/13 
 Pct Recovery = 166%  Analysis Date = 03/21/13 
 Pct Recovery = 166%  Analysis Date = 03/18/13 
 Pct Recovery = 167%  Analysis Date = 03/18/13 
 Pct Recovery = 167%  Analysis Date = 03/16/13 
 Pct Recovery = 167%  Analysis Date = 03/16/13 
 Pct Recovery = 167%  Analysis Date = 03/14/13 
 Pct Recovery = 167%  Analysis Date = 03/14/13 
 Pct Recovery = 167%  Analysis Date = 03/11/13 
 Pct Recovery = 168%  Analysis Date = 03/11/13 
 Pct Recovery = 168%  Analysis Date = 03/09/13 
 Pct Recovery = 168%  Analysis Date = 03/09/13 
 Pct Recovery = 168%  Analysis Date = 03/07/13 
 Pct Recovery = 169%  Analysis Date = 03/07/13 
 Pct Recovery = 169%  Analysis Date = 03/04/13 
 Pct Recovery = 169%  Analysis Date = 03/04/13 
 Pct Recovery = 169%  Analysis Date = 03/02/13 
 Pct Recovery = 169%  Analysis Date = 03/02/13 
 Pct Recovery = 169%  Analysis Date = 02/28/13 
 Pct Recovery = 170%  Analysis Date = 02/28/13 
 Pct Recovery = 170%  Analysis Date = 02/25/13 
 Pct Recovery = 170%  Analysis Date = 02/25/13 
 Pct Recovery = 170%  Analysis Date = 02/23/13 
 Pct Recovery = 170%  Analysis Date = 02/23/13 
 Pct Recovery = 170%  Analysis Date = 02/21/13 
 Pct Recovery = 171%  Analysis Date = 02/21/13 
 Pct Recovery = 171%  Analysis Date = 02/18/13 
 Pct Recovery = 171%  Analysis Date = 02/18/13 
 Pct Recovery = 171%  Analysis Date = 02/16/13 
 Pct Recovery = 172%  Analysis Date = 02/16/13 
 Pct Recovery = 172%  Analysis Date = 02/14/13 
 Pct Recovery = 172%  Analysis Date = 02/14/13 
 Pct Recovery = 172%  Analysis Date = 02/12/13 
 Pct Recovery = 172%  Analysis Date = 02/12/13 
 Pct Recovery = 172%  Analysis Date = 02/09/13 
 Pct Recovery = 173%  Analysis Date = 02/09/13 
 Pct Recovery = 173%  Analysis Date = 02/07/13 
 Pct Recovery = 173%  Analysis Date = 02/07/13 
 Pct Recovery = 173%  Analysis Date = 02/05/13 
 Pct Recovery = 174%  Analysis Date = 02/05/13 
 Pct Recovery = 174%  Analysis Date = 02/02/13 
 Pct Recovery = 174%  Analysis Date = 02/02/13 
 Pct Recovery = 174%  Analysis Date = 01/31/13 
 Pct Recovery = 174%  Analysis Date = 01/31/13 
 Pct Recovery = 174%  Analysis Date = 01/29/13 
 Pct Recovery = 175%  Analysis Date = 01/29/13 
 Pct Recovery = 175%  Analysis Date = 01/26/13 
 Pct Recovery = 175%  Analysis Date = 01/26/13 
 Pct Recovery = 175%  Analysis Date = 01/24/13 
 Pct Recovery = 175%  Analysis Date = 01/24/13 
 Pct Recovery = 175%  Analysis Date = 01/22/13 
 Pct Recovery = 176%  Analysis Date = 01/22/13 
 Pct Recovery = 176%  Analysis Date = 01/19/13 
 Pct Recovery = 176%  Analysis Date = 01/19/13 
 Pct Recovery = 176%  Analysis Date = 01/17/13 
 Pct Recovery = 177%  Analysis Date = 01/17/13 
 Pct Recovery = 177%  Analysis Date = 01/15/13 
 Pct Recovery = 177%  Analysis Date = 01/15/13 
 Pct Recovery = 177%  Analysis Date = 01/13/13 
 Pct Recovery = 177%  Analysis Date = 01/13/13 
 Pct Recovery = 177%  Analysis Date = 01/10/13 
 Pct Recovery = 178%  Analysis Date = 01/10/13 
 Pct Recovery = 178%  Analysis Date = 01/08/13 
 Pct Recovery = 178%  Analysis Date = 01/08/13 
 Pct Recovery = 178%  Analysis Date = 01/06/13 
 Pct Recovery = 179%  Analysis Date = 01/06/13 
 Pct Recovery = 179%  Analysis Date = 01/03/13 
 Pct Recovery = 179%  Analysis Date = 01/03/13 
 Pct Recovery = 179%  Analysis Date = 01/01/13 
 Pct Recovery = 179%  Analysis Date = 01/01/13 
 Pct Recovery = 179%  Analysis Date = 12/30/12 
 Pct Recovery = 180%  Analysis Date = 12/30/12 
 Pct Recovery = 180%  Analysis Date = 12/27/12 
 Pct Recovery = 180%  Analysis Date = 12/27/12 
 Pct Recovery = 180%  Analysis Date = 12/25/12 
 Pct Recovery = 181%  Analysis Date = 12/25/12 
 Pct Recovery = 181%  Analysis Date = 12/23/12 
 Pct Recovery = 181%  Analysis Date = 12/23/12 
 Pct Recovery = 181%  Analysis Date = 12/20/12 
 Pct Recovery = 181%  Analysis Date = 12/20/12 
 Pct Recovery = 181%  Analysis Date = 12/18/12 
 Pct Recovery = 182%  Analysis Date = 12/18/12 
 Pct Recovery = 182%  Analysis Date = 12/16/12 
 Pct Recovery = 182%  Analysis Date = 12/16/12 
 Pct Recovery = 182%  Analysis Date = 12/14/12 
 Pct Recovery = 182%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLIPIZIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 170% . 170% 0%
>= Reporting Level 12 111% 52% 98% 73%
Total 13 116% 52% 113% 72%

Sample Statistics
GLIPIZIDE

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 7 47% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
GLYBURIDE
METHOD: LC9017 , TESTIDCODE: 68002LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 112%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 101%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 70%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 81%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 72%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 45%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 89%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 60%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 59%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 57%  Analysis Date = 03/21/14 
 Pct Recovery = 65%  Analysis Date = 03/18/14 
 Pct Recovery = 65%  Analysis Date = 03/18/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/11/14 
 Pct Recovery = 64%  Analysis Date = 03/11/14 
 Pct Recovery = 64%  Analysis Date = 03/09/14 
 Pct Recovery = 64%  Analysis Date = 03/09/14 
 Pct Recovery = 64%  Analysis Date = 03/07/14 
 Pct Recovery = 64%  Analysis Date = 03/07/14 
 Pct Recovery = 64%  Analysis Date = 03/04/14 
 Pct Recovery = 64%  Analysis Date = 03/04/14 
 Pct Recovery = 64%  Analysis Date = 03/02/14 
 Pct Recovery = 64%  Analysis Date = 03/02/14 
 Pct Recovery = 64%  Analysis Date = 02/28/14 
 Pct Recovery = 64%  Analysis Date = 02/28/14 
 Pct Recovery = 64%  Analysis Date = 02/25/14 
 Pct Recovery = 64%  Analysis Date = 02/25/14 
 Pct Recovery = 64%  Analysis Date = 02/23/14 
 Pct Recovery = 63%  Analysis Date = 02/23/14 
 Pct Recovery = 63%  Analysis Date = 02/21/14 
 Pct Recovery = 63%  Analysis Date = 02/21/14 
 Pct Recovery = 63%  Analysis Date = 02/18/14 
 Pct Recovery = 63%  Analysis Date = 02/18/14 
 Pct Recovery = 63%  Analysis Date = 02/16/14 
 Pct Recovery = 63%  Analysis Date = 02/16/14 
 Pct Recovery = 63%  Analysis Date = 02/14/14 
 Pct Recovery = 63%  Analysis Date = 02/14/14 
 Pct Recovery = 63%  Analysis Date = 02/12/14 
 Pct Recovery = 63%  Analysis Date = 02/12/14 
 Pct Recovery = 63%  Analysis Date = 02/09/14 
 Pct Recovery = 63%  Analysis Date = 02/09/14 
 Pct Recovery = 63%  Analysis Date = 02/07/14 
 Pct Recovery = 63%  Analysis Date = 02/07/14 
 Pct Recovery = 63%  Analysis Date = 02/05/14 
 Pct Recovery = 62%  Analysis Date = 02/05/14 
 Pct Recovery = 62%  Analysis Date = 02/02/14 
 Pct Recovery = 62%  Analysis Date = 02/02/14 
 Pct Recovery = 62%  Analysis Date = 01/31/14 
 Pct Recovery = 62%  Analysis Date = 01/31/14 
 Pct Recovery = 62%  Analysis Date = 01/29/14 
 Pct Recovery = 62%  Analysis Date = 01/29/14 
 Pct Recovery = 62%  Analysis Date = 01/26/14 
 Pct Recovery = 62%  Analysis Date = 01/26/14 
 Pct Recovery = 62%  Analysis Date = 01/24/14 
 Pct Recovery = 62%  Analysis Date = 01/24/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/19/14 
 Pct Recovery = 61%  Analysis Date = 01/19/14 
 Pct Recovery = 61%  Analysis Date = 01/17/14 
 Pct Recovery = 61%  Analysis Date = 01/17/14 
 Pct Recovery = 61%  Analysis Date = 01/15/14 
 Pct Recovery = 61%  Analysis Date = 01/15/14 
 Pct Recovery = 61%  Analysis Date = 01/13/14 
 Pct Recovery = 61%  Analysis Date = 01/13/14 
 Pct Recovery = 61%  Analysis Date = 01/10/14 
 Pct Recovery = 61%  Analysis Date = 01/10/14 
 Pct Recovery = 61%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 60%  Analysis Date = 12/30/13 
 Pct Recovery = 59%  Analysis Date = 12/30/13 
 Pct Recovery = 59%  Analysis Date = 12/27/13 
 Pct Recovery = 59%  Analysis Date = 12/27/13 
 Pct Recovery = 59%  Analysis Date = 12/25/13 
 Pct Recovery = 59%  Analysis Date = 12/25/13 
 Pct Recovery = 59%  Analysis Date = 12/23/13 
 Pct Recovery = 59%  Analysis Date = 12/23/13 
 Pct Recovery = 59%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/18/13 
 Pct Recovery = 58%  Analysis Date = 12/18/13 
 Pct Recovery = 58%  Analysis Date = 12/16/13 
 Pct Recovery = 58%  Analysis Date = 12/16/13 
 Pct Recovery = 58%  Analysis Date = 12/13/13 
 Pct Recovery = 58%  Analysis Date = 12/13/13 
 Pct Recovery = 58%  Analysis Date = 12/11/13 
 Pct Recovery = 58%  Analysis Date = 12/11/13 
 Pct Recovery = 58%  Analysis Date = 12/09/13 
 Pct Recovery = 57%  Analysis Date = 12/09/13 
 Pct Recovery = 57%  Analysis Date = 12/07/13 
 Pct Recovery = 57%  Analysis Date = 12/07/13 
 Pct Recovery = 57%  Analysis Date = 12/04/13 
 Pct Recovery = 57%  Analysis Date = 12/04/13 
 Pct Recovery = 57%  Analysis Date = 12/02/13 
 Pct Recovery = 57%  Analysis Date = 12/02/13 
 Pct Recovery = 57%  Analysis Date = 11/30/13 
 Pct Recovery = 56%  Analysis Date = 11/30/13 
 Pct Recovery = 56%  Analysis Date = 11/27/13 
 Pct Recovery = 56%  Analysis Date = 11/27/13 
 Pct Recovery = 56%  Analysis Date = 11/25/13 
 Pct Recovery = 56%  Analysis Date = 11/25/13 
 Pct Recovery = 56%  Analysis Date = 11/23/13 
 Pct Recovery = 56%  Analysis Date = 11/23/13 
 Pct Recovery = 56%  Analysis Date = 11/20/13 
 Pct Recovery = 55%  Analysis Date = 11/20/13 
 Pct Recovery = 55%  Analysis Date = 11/18/13 
 Pct Recovery = 55%  Analysis Date = 11/18/13 
 Pct Recovery = 55%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/07/13 
 Pct Recovery = 56%  Analysis Date = 11/07/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 10/31/13 
 Pct Recovery = 57%  Analysis Date = 10/31/13 
 Pct Recovery = 57%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/19/13 
 Pct Recovery = 57%  Analysis Date = 10/19/13 
 Pct Recovery = 57%  Analysis Date = 10/17/13 
 Pct Recovery = 58%  Analysis Date = 10/17/13 
 Pct Recovery = 58%  Analysis Date = 10/14/13 
 Pct Recovery = 58%  Analysis Date = 10/14/13 
 Pct Recovery = 58%  Analysis Date = 10/12/13 
 Pct Recovery = 58%  Analysis Date = 10/12/13 
 Pct Recovery = 58%  Analysis Date = 10/10/13 
 Pct Recovery = 58%  Analysis Date = 10/10/13 
 Pct Recovery = 58%  Analysis Date = 10/07/13 
 Pct Recovery = 58%  Analysis Date = 10/07/13 
 Pct Recovery = 58%  Analysis Date = 10/05/13 
 Pct Recovery = 58%  Analysis Date = 10/05/13 
 Pct Recovery = 58%  Analysis Date = 10/03/13 
 Pct Recovery = 58%  Analysis Date = 10/03/13 
 Pct Recovery = 58%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 09/28/13 
 Pct Recovery = 59%  Analysis Date = 09/28/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/21/13 
 Pct Recovery = 59%  Analysis Date = 09/21/13 
 Pct Recovery = 59%  Analysis Date = 09/19/13 
 Pct Recovery = 59%  Analysis Date = 09/19/13 
 Pct Recovery = 59%  Analysis Date = 09/17/13 
 Pct Recovery = 60%  Analysis Date = 09/17/13 
 Pct Recovery = 60%  Analysis Date = 09/14/13 
 Pct Recovery = 60%  Analysis Date = 09/14/13 
 Pct Recovery = 60%  Analysis Date = 09/12/13 
 Pct Recovery = 60%  Analysis Date = 09/12/13 
 Pct Recovery = 60%  Analysis Date = 09/10/13 
 Pct Recovery = 60%  Analysis Date = 09/10/13 
 Pct Recovery = 60%  Analysis Date = 09/07/13 
 Pct Recovery = 60%  Analysis Date = 09/07/13 
 Pct Recovery = 60%  Analysis Date = 09/05/13 
 Pct Recovery = 60%  Analysis Date = 09/05/13 
 Pct Recovery = 60%  Analysis Date = 09/03/13 
 Pct Recovery = 60%  Analysis Date = 09/03/13 
 Pct Recovery = 60%  Analysis Date = 09/01/13 
 Pct Recovery = 61%  Analysis Date = 09/01/13 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 Pct Recovery = 61%  Analysis Date = 08/27/13 
 Pct Recovery = 61%  Analysis Date = 08/27/13 
 Pct Recovery = 61%  Analysis Date = 08/25/13 
 Pct Recovery = 62%  Analysis Date = 08/25/13 
 Pct Recovery = 62%  Analysis Date = 08/22/13 
 Pct Recovery = 62%  Analysis Date = 08/22/13 
 Pct Recovery = 62%  Analysis Date = 08/20/13 
 Pct Recovery = 63%  Analysis Date = 08/20/13 
 Pct Recovery = 63%  Analysis Date = 08/18/13 
 Pct Recovery = 63%  Analysis Date = 08/18/13 
 Pct Recovery = 63%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 64%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/08/13 
 Pct Recovery = 65%  Analysis Date = 08/08/13 
 Pct Recovery = 65%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 69%  Analysis Date = 07/26/13 
 Pct Recovery = 69%  Analysis Date = 07/23/13 
 Pct Recovery = 69%  Analysis Date = 07/23/13 
 Pct Recovery = 69%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/19/13 
 Pct Recovery = 70%  Analysis Date = 07/19/13 
 Pct Recovery = 70%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/12/13 
 Pct Recovery = 72%  Analysis Date = 07/12/13 
 Pct Recovery = 72%  Analysis Date = 07/09/13 
 Pct Recovery = 72%  Analysis Date = 07/09/13 
 Pct Recovery = 72%  Analysis Date = 07/07/13 
 Pct Recovery = 73%  Analysis Date = 07/07/13 
 Pct Recovery = 73%  Analysis Date = 07/05/13 
 Pct Recovery = 73%  Analysis Date = 07/05/13 
 Pct Recovery = 73%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 07/02/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 77%  Analysis Date = 06/19/13 
 Pct Recovery = 77%  Analysis Date = 06/16/13 
 Pct Recovery = 78%  Analysis Date = 06/16/13 
 Pct Recovery = 78%  Analysis Date = 06/14/13 
 Pct Recovery = 78%  Analysis Date = 06/14/13 
 Pct Recovery = 78%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/09/13 
 Pct Recovery = 79%  Analysis Date = 06/09/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/02/13 
 Pct Recovery = 81%  Analysis Date = 06/02/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/27/13 
 Pct Recovery = 82%  Analysis Date = 05/27/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 83%  Analysis Date = 05/24/13 
 Pct Recovery = 83%  Analysis Date = 05/22/13 
 Pct Recovery = 83%  Analysis Date = 05/22/13 
 Pct Recovery = 83%  Analysis Date = 05/20/13 
 Pct Recovery = 84%  Analysis Date = 05/20/13 
 Pct Recovery = 84%  Analysis Date = 05/17/13 
 Pct Recovery = 84%  Analysis Date = 05/17/13 
 Pct Recovery = 84%  Analysis Date = 05/15/13 
 Pct Recovery = 85%  Analysis Date = 05/15/13 
 Pct Recovery = 85%  Analysis Date = 05/13/13 
 Pct Recovery = 85%  Analysis Date = 05/13/13 
 Pct Recovery = 85%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/08/13 
 Pct Recovery = 87%  Analysis Date = 05/08/13 
 Pct Recovery = 87%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/03/13 
 Pct Recovery = 88%  Analysis Date = 05/03/13 
 Pct Recovery = 88%  Analysis Date = 05/01/13 
 Pct Recovery = 88%  Analysis Date = 05/01/13 
 Pct Recovery = 88%  Analysis Date = 04/29/13 
 Pct Recovery = 88%  Analysis Date = 04/29/13 
 Pct Recovery = 88%  Analysis Date = 04/26/13 
 Pct Recovery = 88%  Analysis Date = 04/26/13 
 Pct Recovery = 88%  Analysis Date = 04/24/13 
 Pct Recovery = 88%  Analysis Date = 04/24/13 
 Pct Recovery = 88%  Analysis Date = 04/22/13 
 Pct Recovery = 89%  Analysis Date = 04/22/13 
 Pct Recovery = 89%  Analysis Date = 04/20/13 
 Pct Recovery = 89%  Analysis Date = 04/20/13 
 Pct Recovery = 89%  Analysis Date = 04/17/13 
 Pct Recovery = 89%  Analysis Date = 04/17/13 
 Pct Recovery = 89%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/13/13 
 Pct Recovery = 89%  Analysis Date = 04/13/13 
 Pct Recovery = 89%  Analysis Date = 04/10/13 
 Pct Recovery = 89%  Analysis Date = 04/10/13 
 Pct Recovery = 89%  Analysis Date = 04/08/13 
 Pct Recovery = 89%  Analysis Date = 04/08/13 
 Pct Recovery = 89%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/03/13 
 Pct Recovery = 89%  Analysis Date = 04/03/13 
 Pct Recovery = 89%  Analysis Date = 04/01/13 
 Pct Recovery = 89%  Analysis Date = 04/01/13 
 Pct Recovery = 89%  Analysis Date = 03/30/13 
 Pct Recovery = 89%  Analysis Date = 03/30/13 
 Pct Recovery = 89%  Analysis Date = 03/27/13 
 Pct Recovery = 89%  Analysis Date = 03/27/13 
 Pct Recovery = 89%  Analysis Date = 03/25/13 
 Pct Recovery = 89%  Analysis Date = 03/25/13 
 Pct Recovery = 89%  Analysis Date = 03/23/13 
 Pct Recovery = 89%  Analysis Date = 03/23/13 
 Pct Recovery = 89%  Analysis Date = 03/21/13 
 Pct Recovery = 89%  Analysis Date = 03/21/13 
 Pct Recovery = 89%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/16/13 
 Pct Recovery = 90%  Analysis Date = 03/16/13 
 Pct Recovery = 90%  Analysis Date = 03/14/13 
 Pct Recovery = 90%  Analysis Date = 03/14/13 
 Pct Recovery = 90%  Analysis Date = 03/11/13 
 Pct Recovery = 90%  Analysis Date = 03/11/13 
 Pct Recovery = 90%  Analysis Date = 03/09/13 
 Pct Recovery = 90%  Analysis Date = 03/09/13 
 Pct Recovery = 90%  Analysis Date = 03/07/13 
 Pct Recovery = 90%  Analysis Date = 03/07/13 
 Pct Recovery = 90%  Analysis Date = 03/04/13 
 Pct Recovery = 90%  Analysis Date = 03/04/13 
 Pct Recovery = 90%  Analysis Date = 03/02/13 
 Pct Recovery = 90%  Analysis Date = 03/02/13 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 Pct Recovery = 90%  Analysis Date = 02/25/13 
 Pct Recovery = 90%  Analysis Date = 02/25/13 
 Pct Recovery = 90%  Analysis Date = 02/23/13 
 Pct Recovery = 90%  Analysis Date = 02/23/13 
 Pct Recovery = 90%  Analysis Date = 02/21/13 
 Pct Recovery = 90%  Analysis Date = 02/21/13 
 Pct Recovery = 90%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/18/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/09/13 
 Pct Recovery = 91%  Analysis Date = 02/09/13 
 Pct Recovery = 91%  Analysis Date = 02/07/13 
 Pct Recovery = 91%  Analysis Date = 02/07/13 
 Pct Recovery = 91%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/29/13 
 Pct Recovery = 91%  Analysis Date = 01/29/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/24/13 
 Pct Recovery = 91%  Analysis Date = 01/24/13 
 Pct Recovery = 91%  Analysis Date = 01/22/13 
 Pct Recovery = 91%  Analysis Date = 01/22/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/15/13 
 Pct Recovery = 92%  Analysis Date = 01/15/13 
 Pct Recovery = 92%  Analysis Date = 01/13/13 
 Pct Recovery = 92%  Analysis Date = 01/13/13 
 Pct Recovery = 92%  Analysis Date = 01/10/13 
 Pct Recovery = 92%  Analysis Date = 01/10/13 
 Pct Recovery = 92%  Analysis Date = 01/08/13 
 Pct Recovery = 92%  Analysis Date = 01/08/13 
 Pct Recovery = 92%  Analysis Date = 01/06/13 
 Pct Recovery = 92%  Analysis Date = 01/06/13 
 Pct Recovery = 92%  Analysis Date = 01/03/13 
 Pct Recovery = 92%  Analysis Date = 01/03/13 
 Pct Recovery = 92%  Analysis Date = 01/01/13 
 Pct Recovery = 92%  Analysis Date = 01/01/13 
 Pct Recovery = 92%  Analysis Date = 12/30/12 
 Pct Recovery = 92%  Analysis Date = 12/30/12 
 Pct Recovery = 92%  Analysis Date = 12/27/12 
 Pct Recovery = 92%  Analysis Date = 12/27/12 
 Pct Recovery = 92%  Analysis Date = 12/25/12 
 Pct Recovery = 92%  Analysis Date = 12/25/12 
 Pct Recovery = 92%  Analysis Date = 12/23/12 
 Pct Recovery = 92%  Analysis Date = 12/23/12 
 Pct Recovery = 92%  Analysis Date = 12/20/12 
 Pct Recovery = 93%  Analysis Date = 12/20/12 
 Pct Recovery = 93%  Analysis Date = 12/18/12 
 Pct Recovery = 93%  Analysis Date = 12/18/12 
 Pct Recovery = 93%  Analysis Date = 12/16/12 
 Pct Recovery = 93%  Analysis Date = 12/16/12 
 Pct Recovery = 93%  Analysis Date = 12/14/12 
 Pct Recovery = 93%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLYBURIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 73% 20% 70% 23%
Total 11 73% 20% 70% 23%

Sample Statistics
GLYBURIDE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
HYDROCODONE
METHOD: LC9017 , TESTIDCODE: 67506LCM56

The SGPlot Procedure

Sample Statistics
HYDROCODONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
HYDROCORTISONE
METHOD: LC9017 , TESTIDCODE: 67459LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 70%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 99%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 92%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 95%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 84%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 93%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 76%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 93%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 91%  Analysis Date = 03/21/14 
 Pct Recovery = 90%  Analysis Date = 03/18/14 
 Pct Recovery = 90%  Analysis Date = 03/18/14 
 Pct Recovery = 90%  Analysis Date = 03/16/14 
 Pct Recovery = 90%  Analysis Date = 03/16/14 
 Pct Recovery = 90%  Analysis Date = 03/14/14 
 Pct Recovery = 90%  Analysis Date = 03/14/14 
 Pct Recovery = 90%  Analysis Date = 03/11/14 
 Pct Recovery = 90%  Analysis Date = 03/11/14 
 Pct Recovery = 90%  Analysis Date = 03/09/14 
 Pct Recovery = 90%  Analysis Date = 03/09/14 
 Pct Recovery = 90%  Analysis Date = 03/07/14 
 Pct Recovery = 89%  Analysis Date = 03/07/14 
 Pct Recovery = 89%  Analysis Date = 03/04/14 
 Pct Recovery = 89%  Analysis Date = 03/04/14 
 Pct Recovery = 89%  Analysis Date = 03/02/14 
 Pct Recovery = 89%  Analysis Date = 03/02/14 
 Pct Recovery = 89%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/25/14 
 Pct Recovery = 89%  Analysis Date = 02/25/14 
 Pct Recovery = 89%  Analysis Date = 02/23/14 
 Pct Recovery = 88%  Analysis Date = 02/23/14 
 Pct Recovery = 88%  Analysis Date = 02/21/14 
 Pct Recovery = 88%  Analysis Date = 02/21/14 
 Pct Recovery = 88%  Analysis Date = 02/18/14 
 Pct Recovery = 88%  Analysis Date = 02/18/14 
 Pct Recovery = 88%  Analysis Date = 02/16/14 
 Pct Recovery = 88%  Analysis Date = 02/16/14 
 Pct Recovery = 88%  Analysis Date = 02/14/14 
 Pct Recovery = 88%  Analysis Date = 02/14/14 
 Pct Recovery = 88%  Analysis Date = 02/12/14 
 Pct Recovery = 88%  Analysis Date = 02/12/14 
 Pct Recovery = 88%  Analysis Date = 02/09/14 
 Pct Recovery = 88%  Analysis Date = 02/09/14 
 Pct Recovery = 88%  Analysis Date = 02/07/14 
 Pct Recovery = 87%  Analysis Date = 02/07/14 
 Pct Recovery = 87%  Analysis Date = 02/05/14 
 Pct Recovery = 87%  Analysis Date = 02/05/14 
 Pct Recovery = 87%  Analysis Date = 02/02/14 
 Pct Recovery = 87%  Analysis Date = 02/02/14 
 Pct Recovery = 87%  Analysis Date = 01/31/14 
 Pct Recovery = 87%  Analysis Date = 01/31/14 
 Pct Recovery = 87%  Analysis Date = 01/29/14 
 Pct Recovery = 87%  Analysis Date = 01/29/14 
 Pct Recovery = 87%  Analysis Date = 01/26/14 
 Pct Recovery = 87%  Analysis Date = 01/26/14 
 Pct Recovery = 87%  Analysis Date = 01/24/14 
 Pct Recovery = 87%  Analysis Date = 01/24/14 
 Pct Recovery = 87%  Analysis Date = 01/22/14 
 Pct Recovery = 86%  Analysis Date = 01/22/14 
 Pct Recovery = 86%  Analysis Date = 01/19/14 
 Pct Recovery = 86%  Analysis Date = 01/19/14 
 Pct Recovery = 86%  Analysis Date = 01/17/14 
 Pct Recovery = 86%  Analysis Date = 01/17/14 
 Pct Recovery = 86%  Analysis Date = 01/15/14 
 Pct Recovery = 86%  Analysis Date = 01/15/14 
 Pct Recovery = 86%  Analysis Date = 01/13/14 
 Pct Recovery = 86%  Analysis Date = 01/13/14 
 Pct Recovery = 86%  Analysis Date = 01/10/14 
 Pct Recovery = 86%  Analysis Date = 01/10/14 
 Pct Recovery = 86%  Analysis Date = 01/08/14 
 Pct Recovery = 86%  Analysis Date = 01/08/14 
 Pct Recovery = 86%  Analysis Date = 01/06/14 
 Pct Recovery = 85%  Analysis Date = 01/06/14 
 Pct Recovery = 85%  Analysis Date = 01/03/14 
 Pct Recovery = 85%  Analysis Date = 01/03/14 
 Pct Recovery = 85%  Analysis Date = 01/01/14 
 Pct Recovery = 85%  Analysis Date = 01/01/14 
 Pct Recovery = 85%  Analysis Date = 12/30/13 
 Pct Recovery = 85%  Analysis Date = 12/30/13 
 Pct Recovery = 85%  Analysis Date = 12/27/13 
 Pct Recovery = 85%  Analysis Date = 12/27/13 
 Pct Recovery = 85%  Analysis Date = 12/25/13 
 Pct Recovery = 85%  Analysis Date = 12/25/13 
 Pct Recovery = 85%  Analysis Date = 12/23/13 
 Pct Recovery = 85%  Analysis Date = 12/23/13 
 Pct Recovery = 85%  Analysis Date = 12/20/13 
 Pct Recovery = 85%  Analysis Date = 12/20/13 
 Pct Recovery = 85%  Analysis Date = 12/18/13 
 Pct Recovery = 84%  Analysis Date = 12/18/13 
 Pct Recovery = 84%  Analysis Date = 12/16/13 
 Pct Recovery = 84%  Analysis Date = 12/16/13 
 Pct Recovery = 84%  Analysis Date = 12/13/13 
 Pct Recovery = 84%  Analysis Date = 12/13/13 
 Pct Recovery = 84%  Analysis Date = 12/11/13 
 Pct Recovery = 84%  Analysis Date = 12/11/13 
 Pct Recovery = 84%  Analysis Date = 12/09/13 
 Pct Recovery = 84%  Analysis Date = 12/09/13 
 Pct Recovery = 84%  Analysis Date = 12/07/13 
 Pct Recovery = 84%  Analysis Date = 12/07/13 
 Pct Recovery = 84%  Analysis Date = 12/04/13 
 Pct Recovery = 84%  Analysis Date = 12/04/13 
 Pct Recovery = 84%  Analysis Date = 12/02/13 
 Pct Recovery = 83%  Analysis Date = 12/02/13 
 Pct Recovery = 83%  Analysis Date = 11/30/13 
 Pct Recovery = 83%  Analysis Date = 11/30/13 
 Pct Recovery = 83%  Analysis Date = 11/27/13 
 Pct Recovery = 83%  Analysis Date = 11/27/13 
 Pct Recovery = 83%  Analysis Date = 11/25/13 
 Pct Recovery = 83%  Analysis Date = 11/25/13 
 Pct Recovery = 83%  Analysis Date = 11/23/13 
 Pct Recovery = 83%  Analysis Date = 11/23/13 
 Pct Recovery = 83%  Analysis Date = 11/20/13 
 Pct Recovery = 83%  Analysis Date = 11/20/13 
 Pct Recovery = 83%  Analysis Date = 11/18/13 
 Pct Recovery = 83%  Analysis Date = 11/18/13 
 Pct Recovery = 83%  Analysis Date = 11/16/13 
 Pct Recovery = 82%  Analysis Date = 11/16/13 
 Pct Recovery = 82%  Analysis Date = 11/13/13 
 Pct Recovery = 82%  Analysis Date = 11/13/13 
 Pct Recovery = 82%  Analysis Date = 11/11/13 
 Pct Recovery = 82%  Analysis Date = 11/11/13 
 Pct Recovery = 82%  Analysis Date = 11/09/13 
 Pct Recovery = 82%  Analysis Date = 11/09/13 
 Pct Recovery = 82%  Analysis Date = 11/07/13 
 Pct Recovery = 82%  Analysis Date = 11/07/13 
 Pct Recovery = 82%  Analysis Date = 11/04/13 
 Pct Recovery = 82%  Analysis Date = 11/04/13 
 Pct Recovery = 82%  Analysis Date = 11/02/13 
 Pct Recovery = 82%  Analysis Date = 11/02/13 
 Pct Recovery = 82%  Analysis Date = 10/31/13 
 Pct Recovery = 81%  Analysis Date = 10/31/13 
 Pct Recovery = 81%  Analysis Date = 10/28/13 
 Pct Recovery = 81%  Analysis Date = 10/28/13 
 Pct Recovery = 81%  Analysis Date = 10/26/13 
 Pct Recovery = 81%  Analysis Date = 10/26/13 
 Pct Recovery = 81%  Analysis Date = 10/24/13 
 Pct Recovery = 81%  Analysis Date = 10/24/13 
 Pct Recovery = 81%  Analysis Date = 10/21/13 
 Pct Recovery = 81%  Analysis Date = 10/21/13 
 Pct Recovery = 81%  Analysis Date = 10/19/13 
 Pct Recovery = 81%  Analysis Date = 10/19/13 
 Pct Recovery = 81%  Analysis Date = 10/17/13 
 Pct Recovery = 81%  Analysis Date = 10/17/13 
 Pct Recovery = 81%  Analysis Date = 10/14/13 
 Pct Recovery = 81%  Analysis Date = 10/14/13 
 Pct Recovery = 81%  Analysis Date = 10/12/13 
 Pct Recovery = 80%  Analysis Date = 10/12/13 
 Pct Recovery = 80%  Analysis Date = 10/10/13 
 Pct Recovery = 80%  Analysis Date = 10/10/13 
 Pct Recovery = 80%  Analysis Date = 10/07/13 
 Pct Recovery = 80%  Analysis Date = 10/07/13 
 Pct Recovery = 80%  Analysis Date = 10/05/13 
 Pct Recovery = 80%  Analysis Date = 10/05/13 
 Pct Recovery = 80%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/03/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 80%  Analysis Date = 09/28/13 
 Pct Recovery = 80%  Analysis Date = 09/28/13 
 Pct Recovery = 80%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/10/13 
 Pct Recovery = 78%  Analysis Date = 09/10/13 
 Pct Recovery = 78%  Analysis Date = 09/07/13 
 Pct Recovery = 78%  Analysis Date = 09/07/13 
 Pct Recovery = 78%  Analysis Date = 09/05/13 
 Pct Recovery = 78%  Analysis Date = 09/05/13 
 Pct Recovery = 78%  Analysis Date = 09/03/13 
 Pct Recovery = 78%  Analysis Date = 09/03/13 
 Pct Recovery = 78%  Analysis Date = 09/01/13 
 Pct Recovery = 78%  Analysis Date = 09/01/13 
 Pct Recovery = 78%  Analysis Date = 08/29/13 
 Pct Recovery = 78%  Analysis Date = 08/29/13 
 Pct Recovery = 78%  Analysis Date = 08/27/13 
 Pct Recovery = 78%  Analysis Date = 08/27/13 
 Pct Recovery = 78%  Analysis Date = 08/25/13 
 Pct Recovery = 77%  Analysis Date = 08/25/13 
 Pct Recovery = 77%  Analysis Date = 08/22/13 
 Pct Recovery = 77%  Analysis Date = 08/22/13 
 Pct Recovery = 77%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/20/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/18/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/15/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/13/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/08/13 
 Pct Recovery = 76%  Analysis Date = 08/08/13 
 Pct Recovery = 76%  Analysis Date = 08/06/13 
 Pct Recovery = 76%  Analysis Date = 08/06/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/21/13 
 Pct Recovery = 75%  Analysis Date = 07/21/13 
 Pct Recovery = 75%  Analysis Date = 07/19/13 
 Pct Recovery = 75%  Analysis Date = 07/19/13 
 Pct Recovery = 75%  Analysis Date = 07/16/13 
 Pct Recovery = 75%  Analysis Date = 07/16/13 
 Pct Recovery = 75%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/12/13 
 Pct Recovery = 75%  Analysis Date = 07/12/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/26/13 
 Pct Recovery = 75%  Analysis Date = 06/23/13 
 Pct Recovery = 75%  Analysis Date = 06/23/13 
 Pct Recovery = 75%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/21/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/19/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/16/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/14/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/12/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/09/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 06/02/13 
 Pct Recovery = 75%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/27/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/06/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 Pct Recovery = 75%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/17/13 
 Pct Recovery = 77%  Analysis Date = 04/17/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 78%  Analysis Date = 04/15/13 
 Pct Recovery = 78%  Analysis Date = 04/13/13 
 Pct Recovery = 78%  Analysis Date = 04/13/13 
 Pct Recovery = 78%  Analysis Date = 04/10/13 
 Pct Recovery = 79%  Analysis Date = 04/10/13 
 Pct Recovery = 79%  Analysis Date = 04/08/13 
 Pct Recovery = 79%  Analysis Date = 04/08/13 
 Pct Recovery = 79%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 80%  Analysis Date = 04/03/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 81%  Analysis Date = 03/30/13 
 Pct Recovery = 81%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/27/13 
 Pct Recovery = 81%  Analysis Date = 03/25/13 
 Pct Recovery = 82%  Analysis Date = 03/25/13 
 Pct Recovery = 82%  Analysis Date = 03/23/13 
 Pct Recovery = 82%  Analysis Date = 03/23/13 
 Pct Recovery = 82%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/16/13 
 Pct Recovery = 84%  Analysis Date = 03/14/13 
 Pct Recovery = 84%  Analysis Date = 03/14/13 
 Pct Recovery = 84%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/09/13 
 Pct Recovery = 85%  Analysis Date = 03/07/13 
 Pct Recovery = 86%  Analysis Date = 03/07/13 
 Pct Recovery = 86%  Analysis Date = 03/04/13 
 Pct Recovery = 86%  Analysis Date = 03/04/13 
 Pct Recovery = 86%  Analysis Date = 03/02/13 
 Pct Recovery = 87%  Analysis Date = 03/02/13 
 Pct Recovery = 87%  Analysis Date = 02/28/13 
 Pct Recovery = 87%  Analysis Date = 02/28/13 
 Pct Recovery = 87%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 88%  Analysis Date = 02/21/13 
 Pct Recovery = 88%  Analysis Date = 02/21/13 
 Pct Recovery = 88%  Analysis Date = 02/18/13 
 Pct Recovery = 89%  Analysis Date = 02/18/13 
 Pct Recovery = 89%  Analysis Date = 02/16/13 
 Pct Recovery = 89%  Analysis Date = 02/16/13 
 Pct Recovery = 89%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/12/13 
 Pct Recovery = 90%  Analysis Date = 02/12/13 
 Pct Recovery = 90%  Analysis Date = 02/09/13 
 Pct Recovery = 91%  Analysis Date = 02/09/13 
 Pct Recovery = 91%  Analysis Date = 02/07/13 
 Pct Recovery = 91%  Analysis Date = 02/07/13 
 Pct Recovery = 91%  Analysis Date = 02/05/13 
 Pct Recovery = 92%  Analysis Date = 02/05/13 
 Pct Recovery = 92%  Analysis Date = 02/02/13 
 Pct Recovery = 92%  Analysis Date = 02/02/13 
 Pct Recovery = 92%  Analysis Date = 01/31/13 
 Pct Recovery = 93%  Analysis Date = 01/31/13 
 Pct Recovery = 93%  Analysis Date = 01/29/13 
 Pct Recovery = 93%  Analysis Date = 01/29/13 
 Pct Recovery = 93%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 Pct Recovery = 94%  Analysis Date = 01/22/13 
 Pct Recovery = 95%  Analysis Date = 01/22/13 
 Pct Recovery = 95%  Analysis Date = 01/19/13 
 Pct Recovery = 95%  Analysis Date = 01/19/13 
 Pct Recovery = 95%  Analysis Date = 01/17/13 
 Pct Recovery = 95%  Analysis Date = 01/17/13 
 Pct Recovery = 95%  Analysis Date = 01/15/13 
 Pct Recovery = 96%  Analysis Date = 01/15/13 
 Pct Recovery = 96%  Analysis Date = 01/13/13 
 Pct Recovery = 96%  Analysis Date = 01/13/13 
 Pct Recovery = 96%  Analysis Date = 01/10/13 
 Pct Recovery = 97%  Analysis Date = 01/10/13 
 Pct Recovery = 97%  Analysis Date = 01/08/13 
 Pct Recovery = 97%  Analysis Date = 01/08/13 
 Pct Recovery = 97%  Analysis Date = 01/06/13 
 Pct Recovery = 98%  Analysis Date = 01/06/13 
 Pct Recovery = 98%  Analysis Date = 01/03/13 
 Pct Recovery = 98%  Analysis Date = 01/03/13 
 Pct Recovery = 98%  Analysis Date = 01/01/13 
 Pct Recovery = 99%  Analysis Date = 01/01/13 
 Pct Recovery = 99%  Analysis Date = 12/30/12 
 Pct Recovery = 99%  Analysis Date = 12/30/12 
 Pct Recovery = 99%  Analysis Date = 12/27/12 
 Pct Recovery = 100%  Analysis Date = 12/27/12 
 Pct Recovery = 100%  Analysis Date = 12/25/12 
 Pct Recovery = 100%  Analysis Date = 12/25/12 
 Pct Recovery = 100%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/20/12 
 Pct Recovery = 101%  Analysis Date = 12/20/12 
 Pct Recovery = 101%  Analysis Date = 12/18/12 
 Pct Recovery = 101%  Analysis Date = 12/18/12 
 Pct Recovery = 101%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/14/12 
 Pct Recovery = 102%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROCORTISONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 83% 11% 84% 13%
Total 14 83% 11% 84% 13%

Sample Statistics
HYDROCORTISONE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 5 33% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
HYDROXYZINE
METHOD: LC9017 , TESTIDCODE: 68005LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 76%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 71%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 63%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 63%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 56%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 59%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 Pct Recovery = 60%  Analysis Date = 03/18/14 
 Pct Recovery = 60%  Analysis Date = 03/18/14 
 Pct Recovery = 60%  Analysis Date = 03/16/14 
 Pct Recovery = 60%  Analysis Date = 03/16/14 
 Pct Recovery = 60%  Analysis Date = 03/14/14 
 Pct Recovery = 60%  Analysis Date = 03/14/14 
 Pct Recovery = 60%  Analysis Date = 03/11/14 
 Pct Recovery = 59%  Analysis Date = 03/11/14 
 Pct Recovery = 59%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 58%  Analysis Date = 03/02/14 
 Pct Recovery = 58%  Analysis Date = 02/28/14 
 Pct Recovery = 58%  Analysis Date = 02/28/14 
 Pct Recovery = 58%  Analysis Date = 02/25/14 
 Pct Recovery = 58%  Analysis Date = 02/25/14 
 Pct Recovery = 58%  Analysis Date = 02/23/14 
 Pct Recovery = 58%  Analysis Date = 02/23/14 
 Pct Recovery = 58%  Analysis Date = 02/21/14 
 Pct Recovery = 57%  Analysis Date = 02/21/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/14/14 
 Pct Recovery = 57%  Analysis Date = 02/14/14 
 Pct Recovery = 57%  Analysis Date = 02/12/14 
 Pct Recovery = 56%  Analysis Date = 02/12/14 
 Pct Recovery = 56%  Analysis Date = 02/09/14 
 Pct Recovery = 56%  Analysis Date = 02/09/14 
 Pct Recovery = 56%  Analysis Date = 02/07/14 
 Pct Recovery = 56%  Analysis Date = 02/07/14 
 Pct Recovery = 56%  Analysis Date = 02/05/14 
 Pct Recovery = 56%  Analysis Date = 02/05/14 
 Pct Recovery = 56%  Analysis Date = 02/02/14 
 Pct Recovery = 55%  Analysis Date = 02/02/14 
 Pct Recovery = 55%  Analysis Date = 01/31/14 
 Pct Recovery = 55%  Analysis Date = 01/31/14 
 Pct Recovery = 55%  Analysis Date = 01/29/14 
 Pct Recovery = 55%  Analysis Date = 01/29/14 
 Pct Recovery = 55%  Analysis Date = 01/26/14 
 Pct Recovery = 55%  Analysis Date = 01/26/14 
 Pct Recovery = 55%  Analysis Date = 01/24/14 
 Pct Recovery = 54%  Analysis Date = 01/24/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/19/14 
 Pct Recovery = 54%  Analysis Date = 01/19/14 
 Pct Recovery = 54%  Analysis Date = 01/17/14 
 Pct Recovery = 54%  Analysis Date = 01/17/14 
 Pct Recovery = 54%  Analysis Date = 01/15/14 
 Pct Recovery = 53%  Analysis Date = 01/15/14 
 Pct Recovery = 53%  Analysis Date = 01/13/14 
 Pct Recovery = 54%  Analysis Date = 01/13/14 
 Pct Recovery = 54%  Analysis Date = 01/10/14 
 Pct Recovery = 54%  Analysis Date = 01/10/14 
 Pct Recovery = 54%  Analysis Date = 01/08/14 
 Pct Recovery = 54%  Analysis Date = 01/08/14 
 Pct Recovery = 54%  Analysis Date = 01/06/14 
 Pct Recovery = 54%  Analysis Date = 01/06/14 
 Pct Recovery = 54%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 54%  Analysis Date = 12/16/13 
 Pct Recovery = 54%  Analysis Date = 12/16/13 
 Pct Recovery = 54%  Analysis Date = 12/13/13 
 Pct Recovery = 54%  Analysis Date = 12/13/13 
 Pct Recovery = 54%  Analysis Date = 12/11/13 
 Pct Recovery = 54%  Analysis Date = 12/11/13 
 Pct Recovery = 54%  Analysis Date = 12/09/13 
 Pct Recovery = 54%  Analysis Date = 12/09/13 
 Pct Recovery = 54%  Analysis Date = 12/07/13 
 Pct Recovery = 54%  Analysis Date = 12/07/13 
 Pct Recovery = 54%  Analysis Date = 12/04/13 
 Pct Recovery = 54%  Analysis Date = 12/04/13 
 Pct Recovery = 54%  Analysis Date = 12/02/13 
 Pct Recovery = 54%  Analysis Date = 12/02/13 
 Pct Recovery = 54%  Analysis Date = 11/30/13 
 Pct Recovery = 54%  Analysis Date = 11/30/13 
 Pct Recovery = 54%  Analysis Date = 11/27/13 
 Pct Recovery = 54%  Analysis Date = 11/27/13 
 Pct Recovery = 54%  Analysis Date = 11/25/13 
 Pct Recovery = 54%  Analysis Date = 11/25/13 
 Pct Recovery = 54%  Analysis Date = 11/23/13 
 Pct Recovery = 54%  Analysis Date = 11/23/13 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/16/13 
 Pct Recovery = 54%  Analysis Date = 11/16/13 
 Pct Recovery = 54%  Analysis Date = 11/13/13 
 Pct Recovery = 55%  Analysis Date = 11/13/13 
 Pct Recovery = 55%  Analysis Date = 11/11/13 
 Pct Recovery = 55%  Analysis Date = 11/11/13 
 Pct Recovery = 55%  Analysis Date = 11/09/13 
 Pct Recovery = 55%  Analysis Date = 11/09/13 
 Pct Recovery = 55%  Analysis Date = 11/07/13 
 Pct Recovery = 56%  Analysis Date = 11/07/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 10/31/13 
 Pct Recovery = 56%  Analysis Date = 10/31/13 
 Pct Recovery = 56%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/21/13 
 Pct Recovery = 57%  Analysis Date = 10/19/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 58%  Analysis Date = 10/17/13 
 Pct Recovery = 58%  Analysis Date = 10/17/13 
 Pct Recovery = 58%  Analysis Date = 10/14/13 
 Pct Recovery = 58%  Analysis Date = 10/14/13 
 Pct Recovery = 58%  Analysis Date = 10/12/13 
 Pct Recovery = 58%  Analysis Date = 10/12/13 
 Pct Recovery = 58%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/10/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/07/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/05/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/03/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 60%  Analysis Date = 10/01/13 
 Pct Recovery = 60%  Analysis Date = 09/28/13 
 Pct Recovery = 60%  Analysis Date = 09/28/13 
 Pct Recovery = 60%  Analysis Date = 09/26/13 
 Pct Recovery = 60%  Analysis Date = 09/26/13 
 Pct Recovery = 60%  Analysis Date = 09/24/13 
 Pct Recovery = 60%  Analysis Date = 09/24/13 
 Pct Recovery = 60%  Analysis Date = 09/21/13 
 Pct Recovery = 61%  Analysis Date = 09/21/13 
 Pct Recovery = 61%  Analysis Date = 09/19/13 
 Pct Recovery = 61%  Analysis Date = 09/19/13 
 Pct Recovery = 61%  Analysis Date = 09/17/13 
 Pct Recovery = 61%  Analysis Date = 09/17/13 
 Pct Recovery = 61%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/14/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/12/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/10/13 
 Pct Recovery = 62%  Analysis Date = 09/07/13 
 Pct Recovery = 62%  Analysis Date = 09/07/13 
 Pct Recovery = 62%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 08/29/13 
 Pct Recovery = 63%  Analysis Date = 08/29/13 
 Pct Recovery = 63%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/25/13 
 Pct Recovery = 64%  Analysis Date = 08/25/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/15/13 
 Pct Recovery = 64%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/08/13 
 Pct Recovery = 65%  Analysis Date = 08/08/13 
 Pct Recovery = 65%  Analysis Date = 08/06/13 
 Pct Recovery = 65%  Analysis Date = 08/06/13 
 Pct Recovery = 65%  Analysis Date = 08/04/13 
 Pct Recovery = 65%  Analysis Date = 08/04/13 
 Pct Recovery = 65%  Analysis Date = 08/02/13 
 Pct Recovery = 65%  Analysis Date = 08/02/13 
 Pct Recovery = 65%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 66%  Analysis Date = 07/28/13 
 Pct Recovery = 66%  Analysis Date = 07/28/13 
 Pct Recovery = 66%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/26/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/19/13 
 Pct Recovery = 66%  Analysis Date = 07/19/13 
 Pct Recovery = 66%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/12/13 
 Pct Recovery = 67%  Analysis Date = 07/12/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/07/13 
 Pct Recovery = 67%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/05/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/30/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/28/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/26/13 
 Pct Recovery = 68%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/23/13 
 Pct Recovery = 68%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/21/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/19/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/16/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/14/13 
 Pct Recovery = 69%  Analysis Date = 06/12/13 
 Pct Recovery = 69%  Analysis Date = 06/12/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/09/13 
 Pct Recovery = 69%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/29/13 
 Pct Recovery = 70%  Analysis Date = 05/27/13 
 Pct Recovery = 70%  Analysis Date = 05/27/13 
 Pct Recovery = 70%  Analysis Date = 05/24/13 
 Pct Recovery = 71%  Analysis Date = 05/24/13 
 Pct Recovery = 71%  Analysis Date = 05/22/13 
 Pct Recovery = 71%  Analysis Date = 05/22/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/17/13 
 Pct Recovery = 71%  Analysis Date = 05/15/13 
 Pct Recovery = 71%  Analysis Date = 05/15/13 
 Pct Recovery = 71%  Analysis Date = 05/13/13 
 Pct Recovery = 71%  Analysis Date = 05/13/13 
 Pct Recovery = 71%  Analysis Date = 05/10/13 
 Pct Recovery = 72%  Analysis Date = 05/10/13 
 Pct Recovery = 72%  Analysis Date = 05/08/13 
 Pct Recovery = 72%  Analysis Date = 05/08/13 
 Pct Recovery = 72%  Analysis Date = 05/06/13 
 Pct Recovery = 72%  Analysis Date = 05/06/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 04/29/13 
 Pct Recovery = 72%  Analysis Date = 04/29/13 
 Pct Recovery = 72%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/20/13 
 Pct Recovery = 72%  Analysis Date = 04/20/13 
 Pct Recovery = 72%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/13/13 
 Pct Recovery = 71%  Analysis Date = 04/13/13 
 Pct Recovery = 71%  Analysis Date = 04/10/13 
 Pct Recovery = 71%  Analysis Date = 04/10/13 
 Pct Recovery = 71%  Analysis Date = 04/08/13 
 Pct Recovery = 71%  Analysis Date = 04/08/13 
 Pct Recovery = 71%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 Pct Recovery = 71%  Analysis Date = 03/25/13 
 Pct Recovery = 70%  Analysis Date = 03/25/13 
 Pct Recovery = 70%  Analysis Date = 03/23/13 
 Pct Recovery = 70%  Analysis Date = 03/23/13 
 Pct Recovery = 70%  Analysis Date = 03/21/13 
 Pct Recovery = 70%  Analysis Date = 03/21/13 
 Pct Recovery = 70%  Analysis Date = 03/18/13 
 Pct Recovery = 70%  Analysis Date = 03/18/13 
 Pct Recovery = 70%  Analysis Date = 03/16/13 
 Pct Recovery = 70%  Analysis Date = 03/16/13 
 Pct Recovery = 70%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/11/13 
 Pct Recovery = 70%  Analysis Date = 03/11/13 
 Pct Recovery = 70%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/07/13 
 Pct Recovery = 69%  Analysis Date = 03/07/13 
 Pct Recovery = 69%  Analysis Date = 03/04/13 
 Pct Recovery = 69%  Analysis Date = 03/04/13 
 Pct Recovery = 69%  Analysis Date = 03/02/13 
 Pct Recovery = 69%  Analysis Date = 03/02/13 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 Pct Recovery = 69%  Analysis Date = 02/25/13 
 Pct Recovery = 69%  Analysis Date = 02/25/13 
 Pct Recovery = 69%  Analysis Date = 02/23/13 
 Pct Recovery = 69%  Analysis Date = 02/23/13 
 Pct Recovery = 69%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/18/13 
 Pct Recovery = 69%  Analysis Date = 02/18/13 
 Pct Recovery = 69%  Analysis Date = 02/16/13 
 Pct Recovery = 69%  Analysis Date = 02/16/13 
 Pct Recovery = 69%  Analysis Date = 02/14/13 
 Pct Recovery = 69%  Analysis Date = 02/14/13 
 Pct Recovery = 69%  Analysis Date = 02/12/13 
 Pct Recovery = 69%  Analysis Date = 02/12/13 
 Pct Recovery = 69%  Analysis Date = 02/09/13 
 Pct Recovery = 69%  Analysis Date = 02/09/13 
 Pct Recovery = 69%  Analysis Date = 02/07/13 
 Pct Recovery = 69%  Analysis Date = 02/07/13 
 Pct Recovery = 69%  Analysis Date = 02/05/13 
 Pct Recovery = 69%  Analysis Date = 02/05/13 
 Pct Recovery = 69%  Analysis Date = 02/02/13 
 Pct Recovery = 69%  Analysis Date = 02/02/13 
 Pct Recovery = 69%  Analysis Date = 01/31/13 
 Pct Recovery = 69%  Analysis Date = 01/31/13 
 Pct Recovery = 69%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/29/13 
 Pct Recovery = 69%  Analysis Date = 01/26/13 
 Pct Recovery = 69%  Analysis Date = 01/26/13 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 Pct Recovery = 69%  Analysis Date = 01/22/13 
 Pct Recovery = 69%  Analysis Date = 01/22/13 
 Pct Recovery = 69%  Analysis Date = 01/19/13 
 Pct Recovery = 69%  Analysis Date = 01/19/13 
 Pct Recovery = 69%  Analysis Date = 01/17/13 
 Pct Recovery = 69%  Analysis Date = 01/17/13 
 Pct Recovery = 69%  Analysis Date = 01/15/13 
 Pct Recovery = 69%  Analysis Date = 01/15/13 
 Pct Recovery = 69%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/13/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/10/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 69%  Analysis Date = 01/08/13 
 Pct Recovery = 69%  Analysis Date = 01/06/13 
 Pct Recovery = 69%  Analysis Date = 01/06/13 
 Pct Recovery = 69%  Analysis Date = 01/03/13 
 Pct Recovery = 69%  Analysis Date = 01/03/13 
 Pct Recovery = 69%  Analysis Date = 01/01/13 
 Pct Recovery = 69%  Analysis Date = 01/01/13 
 Pct Recovery = 69%  Analysis Date = 12/30/12 
 Pct Recovery = 69%  Analysis Date = 12/30/12 
 Pct Recovery = 69%  Analysis Date = 12/27/12 
 Pct Recovery = 69%  Analysis Date = 12/27/12 
 Pct Recovery = 69%  Analysis Date = 12/25/12 
 Pct Recovery = 69%  Analysis Date = 12/25/12 
 Pct Recovery = 69%  Analysis Date = 12/23/12 
 Pct Recovery = 69%  Analysis Date = 12/23/12 
 Pct Recovery = 69%  Analysis Date = 12/20/12 
 Pct Recovery = 69%  Analysis Date = 12/20/12 
 Pct Recovery = 69%  Analysis Date = 12/18/12 
 Pct Recovery = 69%  Analysis Date = 12/18/12 
 Pct Recovery = 69%  Analysis Date = 12/16/12 
 Pct Recovery = 69%  Analysis Date = 12/16/12 
 Pct Recovery = 69%  Analysis Date = 12/14/12 
 Pct Recovery = 69%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROXYZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 63% 10% 63% 11%
Total 11 63% 10% 63% 11%

Sample Statistics
HYDROXYZINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
IMINOSTILBENE
METHOD: LC9017 , TESTIDCODE: 67481LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 69%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 58%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 50%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 101%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 41%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 72%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 87%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 87%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 102%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 77%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 54%  Analysis Date = 03/21/14 
 Pct Recovery = 98%  Analysis Date = 03/18/14 
 Pct Recovery = 97%  Analysis Date = 03/18/14 
 Pct Recovery = 97%  Analysis Date = 03/16/14 
 Pct Recovery = 96%  Analysis Date = 03/16/14 
 Pct Recovery = 96%  Analysis Date = 03/14/14 
 Pct Recovery = 95%  Analysis Date = 03/14/14 
 Pct Recovery = 95%  Analysis Date = 03/11/14 
 Pct Recovery = 94%  Analysis Date = 03/11/14 
 Pct Recovery = 94%  Analysis Date = 03/09/14 
 Pct Recovery = 93%  Analysis Date = 03/09/14 
 Pct Recovery = 93%  Analysis Date = 03/07/14 
 Pct Recovery = 92%  Analysis Date = 03/07/14 
 Pct Recovery = 92%  Analysis Date = 03/04/14 
 Pct Recovery = 91%  Analysis Date = 03/04/14 
 Pct Recovery = 91%  Analysis Date = 03/02/14 
 Pct Recovery = 90%  Analysis Date = 03/02/14 
 Pct Recovery = 90%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/25/14 
 Pct Recovery = 88%  Analysis Date = 02/25/14 
 Pct Recovery = 88%  Analysis Date = 02/23/14 
 Pct Recovery = 87%  Analysis Date = 02/23/14 
 Pct Recovery = 87%  Analysis Date = 02/21/14 
 Pct Recovery = 86%  Analysis Date = 02/21/14 
 Pct Recovery = 86%  Analysis Date = 02/18/14 
 Pct Recovery = 85%  Analysis Date = 02/18/14 
 Pct Recovery = 85%  Analysis Date = 02/16/14 
 Pct Recovery = 84%  Analysis Date = 02/16/14 
 Pct Recovery = 84%  Analysis Date = 02/14/14 
 Pct Recovery = 83%  Analysis Date = 02/14/14 
 Pct Recovery = 83%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/12/14 
 Pct Recovery = 82%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/09/14 
 Pct Recovery = 81%  Analysis Date = 02/07/14 
 Pct Recovery = 80%  Analysis Date = 02/07/14 
 Pct Recovery = 80%  Analysis Date = 02/05/14 
 Pct Recovery = 79%  Analysis Date = 02/05/14 
 Pct Recovery = 79%  Analysis Date = 02/02/14 
 Pct Recovery = 78%  Analysis Date = 02/02/14 
 Pct Recovery = 78%  Analysis Date = 01/31/14 
 Pct Recovery = 77%  Analysis Date = 01/31/14 
 Pct Recovery = 77%  Analysis Date = 01/29/14 
 Pct Recovery = 76%  Analysis Date = 01/29/14 
 Pct Recovery = 76%  Analysis Date = 01/26/14 
 Pct Recovery = 75%  Analysis Date = 01/26/14 
 Pct Recovery = 75%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 72%  Analysis Date = 01/22/14 
 Pct Recovery = 72%  Analysis Date = 01/19/14 
 Pct Recovery = 71%  Analysis Date = 01/19/14 
 Pct Recovery = 71%  Analysis Date = 01/17/14 
 Pct Recovery = 70%  Analysis Date = 01/17/14 
 Pct Recovery = 70%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/15/14 
 Pct Recovery = 69%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 12/30/13 
 Pct Recovery = 62%  Analysis Date = 12/30/13 
 Pct Recovery = 62%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/25/13 
 Pct Recovery = 59%  Analysis Date = 12/25/13 
 Pct Recovery = 59%  Analysis Date = 12/23/13 
 Pct Recovery = 58%  Analysis Date = 12/23/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 57%  Analysis Date = 12/20/13 
 Pct Recovery = 57%  Analysis Date = 12/18/13 
 Pct Recovery = 56%  Analysis Date = 12/18/13 
 Pct Recovery = 56%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/13/13 
 Pct Recovery = 54%  Analysis Date = 12/13/13 
 Pct Recovery = 54%  Analysis Date = 12/11/13 
 Pct Recovery = 53%  Analysis Date = 12/11/13 
 Pct Recovery = 53%  Analysis Date = 12/09/13 
 Pct Recovery = 52%  Analysis Date = 12/09/13 
 Pct Recovery = 52%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 51%  Analysis Date = 12/04/13 
 Pct Recovery = 50%  Analysis Date = 12/04/13 
 Pct Recovery = 50%  Analysis Date = 12/02/13 
 Pct Recovery = 50%  Analysis Date = 12/02/13 
 Pct Recovery = 50%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/30/13 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 Pct Recovery = 51%  Analysis Date = 11/27/13 
 Pct Recovery = 51%  Analysis Date = 11/25/13 
 Pct Recovery = 52%  Analysis Date = 11/25/13 
 Pct Recovery = 52%  Analysis Date = 11/23/13 
 Pct Recovery = 52%  Analysis Date = 11/23/13 
 Pct Recovery = 52%  Analysis Date = 11/20/13 
 Pct Recovery = 53%  Analysis Date = 11/20/13 
 Pct Recovery = 53%  Analysis Date = 11/18/13 
 Pct Recovery = 53%  Analysis Date = 11/18/13 
 Pct Recovery = 53%  Analysis Date = 11/16/13 
 Pct Recovery = 53%  Analysis Date = 11/16/13 
 Pct Recovery = 53%  Analysis Date = 11/13/13 
 Pct Recovery = 54%  Analysis Date = 11/13/13 
 Pct Recovery = 54%  Analysis Date = 11/11/13 
 Pct Recovery = 54%  Analysis Date = 11/11/13 
 Pct Recovery = 54%  Analysis Date = 11/09/13 
 Pct Recovery = 55%  Analysis Date = 11/09/13 
 Pct Recovery = 55%  Analysis Date = 11/07/13 
 Pct Recovery = 55%  Analysis Date = 11/07/13 
 Pct Recovery = 55%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 56%  Analysis Date = 10/31/13 
 Pct Recovery = 56%  Analysis Date = 10/31/13 
 Pct Recovery = 56%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/26/13 
 Pct Recovery = 57%  Analysis Date = 10/24/13 
 Pct Recovery = 58%  Analysis Date = 10/24/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/14/13 
 Pct Recovery = 59%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/12/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/10/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 61%  Analysis Date = 10/07/13 
 Pct Recovery = 61%  Analysis Date = 10/05/13 
 Pct Recovery = 61%  Analysis Date = 10/05/13 
 Pct Recovery = 61%  Analysis Date = 10/03/13 
 Pct Recovery = 62%  Analysis Date = 10/03/13 
 Pct Recovery = 62%  Analysis Date = 10/01/13 
 Pct Recovery = 62%  Analysis Date = 10/01/13 
 Pct Recovery = 62%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/14/13 
 Pct Recovery = 65%  Analysis Date = 09/14/13 
 Pct Recovery = 65%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/10/13 
 Pct Recovery = 66%  Analysis Date = 09/10/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/03/13 
 Pct Recovery = 67%  Analysis Date = 09/03/13 
 Pct Recovery = 67%  Analysis Date = 09/01/13 
 Pct Recovery = 68%  Analysis Date = 09/01/13 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 Pct Recovery = 68%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/22/13 
 Pct Recovery = 69%  Analysis Date = 08/22/13 
 Pct Recovery = 69%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/20/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/18/13 
 Pct Recovery = 70%  Analysis Date = 08/15/13 
 Pct Recovery = 71%  Analysis Date = 08/15/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/13/13 
 Pct Recovery = 71%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/06/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 73%  Analysis Date = 07/16/13 
 Pct Recovery = 73%  Analysis Date = 07/16/13 
 Pct Recovery = 73%  Analysis Date = 07/14/13 
 Pct Recovery = 73%  Analysis Date = 07/14/13 
 Pct Recovery = 73%  Analysis Date = 07/12/13 
 Pct Recovery = 73%  Analysis Date = 07/12/13 
 Pct Recovery = 73%  Analysis Date = 07/09/13 
 Pct Recovery = 73%  Analysis Date = 07/09/13 
 Pct Recovery = 73%  Analysis Date = 07/07/13 
 Pct Recovery = 72%  Analysis Date = 07/07/13 
 Pct Recovery = 72%  Analysis Date = 07/05/13 
 Pct Recovery = 72%  Analysis Date = 07/05/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 06/30/13 
 Pct Recovery = 72%  Analysis Date = 06/30/13 
 Pct Recovery = 72%  Analysis Date = 06/28/13 
 Pct Recovery = 72%  Analysis Date = 06/28/13 
 Pct Recovery = 72%  Analysis Date = 06/26/13 
 Pct Recovery = 71%  Analysis Date = 06/26/13 
 Pct Recovery = 71%  Analysis Date = 06/23/13 
 Pct Recovery = 71%  Analysis Date = 06/23/13 
 Pct Recovery = 71%  Analysis Date = 06/21/13 
 Pct Recovery = 71%  Analysis Date = 06/21/13 
 Pct Recovery = 71%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/16/13 
 Pct Recovery = 71%  Analysis Date = 06/16/13 
 Pct Recovery = 71%  Analysis Date = 06/14/13 
 Pct Recovery = 71%  Analysis Date = 06/14/13 
 Pct Recovery = 71%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/12/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 06/02/13 
 Pct Recovery = 70%  Analysis Date = 05/31/13 
 Pct Recovery = 69%  Analysis Date = 05/31/13 
 Pct Recovery = 69%  Analysis Date = 05/29/13 
 Pct Recovery = 69%  Analysis Date = 05/29/13 
 Pct Recovery = 69%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/27/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/24/13 
 Pct Recovery = 69%  Analysis Date = 05/22/13 
 Pct Recovery = 69%  Analysis Date = 05/22/13 
 Pct Recovery = 69%  Analysis Date = 05/20/13 
 Pct Recovery = 69%  Analysis Date = 05/20/13 
 Pct Recovery = 69%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/17/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/15/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/13/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/10/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/08/13 
 Pct Recovery = 68%  Analysis Date = 05/06/13 
 Pct Recovery = 67%  Analysis Date = 05/06/13 
 Pct Recovery = 67%  Analysis Date = 05/03/13 
 Pct Recovery = 67%  Analysis Date = 05/03/13 
 Pct Recovery = 67%  Analysis Date = 05/01/13 
 Pct Recovery = 67%  Analysis Date = 05/01/13 
 Pct Recovery = 67%  Analysis Date = 04/29/13 
 Pct Recovery = 67%  Analysis Date = 04/29/13 
 Pct Recovery = 67%  Analysis Date = 04/26/13 
 Pct Recovery = 67%  Analysis Date = 04/26/13 
 Pct Recovery = 67%  Analysis Date = 04/24/13 
 Pct Recovery = 67%  Analysis Date = 04/24/13 
 Pct Recovery = 67%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/22/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/20/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 66%  Analysis Date = 04/15/13 
 Pct Recovery = 66%  Analysis Date = 04/13/13 
 Pct Recovery = 66%  Analysis Date = 04/13/13 
 Pct Recovery = 66%  Analysis Date = 04/10/13 
 Pct Recovery = 66%  Analysis Date = 04/10/13 
 Pct Recovery = 66%  Analysis Date = 04/08/13 
 Pct Recovery = 66%  Analysis Date = 04/08/13 
 Pct Recovery = 66%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/03/13 
 Pct Recovery = 66%  Analysis Date = 04/03/13 
 Pct Recovery = 66%  Analysis Date = 04/01/13 
 Pct Recovery = 66%  Analysis Date = 04/01/13 
 Pct Recovery = 66%  Analysis Date = 03/30/13 
 Pct Recovery = 66%  Analysis Date = 03/30/13 
 Pct Recovery = 66%  Analysis Date = 03/27/13 
 Pct Recovery = 65%  Analysis Date = 03/27/13 
 Pct Recovery = 65%  Analysis Date = 03/25/13 
 Pct Recovery = 65%  Analysis Date = 03/25/13 
 Pct Recovery = 65%  Analysis Date = 03/23/13 
 Pct Recovery = 65%  Analysis Date = 03/23/13 
 Pct Recovery = 65%  Analysis Date = 03/21/13 
 Pct Recovery = 65%  Analysis Date = 03/21/13 
 Pct Recovery = 65%  Analysis Date = 03/18/13 
 Pct Recovery = 64%  Analysis Date = 03/18/13 
 Pct Recovery = 64%  Analysis Date = 03/16/13 
 Pct Recovery = 64%  Analysis Date = 03/16/13 
 Pct Recovery = 64%  Analysis Date = 03/14/13 
 Pct Recovery = 64%  Analysis Date = 03/14/13 
 Pct Recovery = 64%  Analysis Date = 03/11/13 
 Pct Recovery = 63%  Analysis Date = 03/11/13 
 Pct Recovery = 63%  Analysis Date = 03/09/13 
 Pct Recovery = 63%  Analysis Date = 03/09/13 
 Pct Recovery = 63%  Analysis Date = 03/07/13 
 Pct Recovery = 63%  Analysis Date = 03/07/13 
 Pct Recovery = 63%  Analysis Date = 03/04/13 
 Pct Recovery = 62%  Analysis Date = 03/04/13 
 Pct Recovery = 62%  Analysis Date = 03/02/13 
 Pct Recovery = 62%  Analysis Date = 03/02/13 
 Pct Recovery = 62%  Analysis Date = 02/28/13 
 Pct Recovery = 62%  Analysis Date = 02/28/13 
 Pct Recovery = 62%  Analysis Date = 02/25/13 
 Pct Recovery = 61%  Analysis Date = 02/25/13 
 Pct Recovery = 61%  Analysis Date = 02/23/13 
 Pct Recovery = 61%  Analysis Date = 02/23/13 
 Pct Recovery = 61%  Analysis Date = 02/21/13 
 Pct Recovery = 61%  Analysis Date = 02/21/13 
 Pct Recovery = 61%  Analysis Date = 02/18/13 
 Pct Recovery = 60%  Analysis Date = 02/18/13 
 Pct Recovery = 60%  Analysis Date = 02/16/13 
 Pct Recovery = 60%  Analysis Date = 02/16/13 
 Pct Recovery = 60%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/12/13 
 Pct Recovery = 59%  Analysis Date = 02/12/13 
 Pct Recovery = 59%  Analysis Date = 02/09/13 
 Pct Recovery = 59%  Analysis Date = 02/09/13 
 Pct Recovery = 59%  Analysis Date = 02/07/13 
 Pct Recovery = 59%  Analysis Date = 02/07/13 
 Pct Recovery = 59%  Analysis Date = 02/05/13 
 Pct Recovery = 58%  Analysis Date = 02/05/13 
 Pct Recovery = 58%  Analysis Date = 02/02/13 
 Pct Recovery = 58%  Analysis Date = 02/02/13 
 Pct Recovery = 58%  Analysis Date = 01/31/13 
 Pct Recovery = 58%  Analysis Date = 01/31/13 
 Pct Recovery = 58%  Analysis Date = 01/29/13 
 Pct Recovery = 57%  Analysis Date = 01/29/13 
 Pct Recovery = 57%  Analysis Date = 01/26/13 
 Pct Recovery = 57%  Analysis Date = 01/26/13 
 Pct Recovery = 57%  Analysis Date = 01/24/13 
 Pct Recovery = 57%  Analysis Date = 01/24/13 
 Pct Recovery = 57%  Analysis Date = 01/22/13 
 Pct Recovery = 56%  Analysis Date = 01/22/13 
 Pct Recovery = 56%  Analysis Date = 01/19/13 
 Pct Recovery = 56%  Analysis Date = 01/19/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 55%  Analysis Date = 01/15/13 
 Pct Recovery = 55%  Analysis Date = 01/13/13 
 Pct Recovery = 55%  Analysis Date = 01/13/13 
 Pct Recovery = 55%  Analysis Date = 01/10/13 
 Pct Recovery = 55%  Analysis Date = 01/10/13 
 Pct Recovery = 55%  Analysis Date = 01/08/13 
 Pct Recovery = 54%  Analysis Date = 01/08/13 
 Pct Recovery = 54%  Analysis Date = 01/06/13 
 Pct Recovery = 54%  Analysis Date = 01/06/13 
 Pct Recovery = 54%  Analysis Date = 01/03/13 
 Pct Recovery = 54%  Analysis Date = 01/03/13 
 Pct Recovery = 54%  Analysis Date = 01/01/13 
 Pct Recovery = 53%  Analysis Date = 01/01/13 
 Pct Recovery = 53%  Analysis Date = 12/30/12 
 Pct Recovery = 53%  Analysis Date = 12/30/12 
 Pct Recovery = 53%  Analysis Date = 12/27/12 
 Pct Recovery = 53%  Analysis Date = 12/27/12 
 Pct Recovery = 53%  Analysis Date = 12/25/12 
 Pct Recovery = 52%  Analysis Date = 12/25/12 
 Pct Recovery = 52%  Analysis Date = 12/23/12 
 Pct Recovery = 52%  Analysis Date = 12/23/12 
 Pct Recovery = 52%  Analysis Date = 12/20/12 
 Pct Recovery = 52%  Analysis Date = 12/20/12 
 Pct Recovery = 52%  Analysis Date = 12/18/12 
 Pct Recovery = 51%  Analysis Date = 12/18/12 
 Pct Recovery = 51%  Analysis Date = 12/16/12 
 Pct Recovery = 51%  Analysis Date = 12/16/12 
 Pct Recovery = 51%  Analysis Date = 12/14/12 
 Pct Recovery = 51%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
IMINOSTILBENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 73% 19% 74% 21%
Total 13 73% 19% 74% 21%

Sample Statistics
IMINOSTILBENE

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
KETOCONAZOLE
METHOD: LC9017 , TESTIDCODE: 68014LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 20%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 25%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 53%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 37%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 48%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 49%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 41%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 39%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 12%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 40%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 43%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 59%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/14/14 
 Pct Recovery = 42%  Analysis Date = 03/11/14 
 Pct Recovery = 42%  Analysis Date = 03/11/14 
 Pct Recovery = 42%  Analysis Date = 03/09/14 
 Pct Recovery = 42%  Analysis Date = 03/09/14 
 Pct Recovery = 42%  Analysis Date = 03/07/14 
 Pct Recovery = 42%  Analysis Date = 03/07/14 
 Pct Recovery = 42%  Analysis Date = 03/04/14 
 Pct Recovery = 43%  Analysis Date = 03/04/14 
 Pct Recovery = 43%  Analysis Date = 03/02/14 
 Pct Recovery = 43%  Analysis Date = 03/02/14 
 Pct Recovery = 43%  Analysis Date = 02/28/14 
 Pct Recovery = 43%  Analysis Date = 02/28/14 
 Pct Recovery = 43%  Analysis Date = 02/25/14 
 Pct Recovery = 43%  Analysis Date = 02/25/14 
 Pct Recovery = 43%  Analysis Date = 02/23/14 
 Pct Recovery = 43%  Analysis Date = 02/23/14 
 Pct Recovery = 43%  Analysis Date = 02/21/14 
 Pct Recovery = 43%  Analysis Date = 02/21/14 
 Pct Recovery = 43%  Analysis Date = 02/18/14 
 Pct Recovery = 43%  Analysis Date = 02/18/14 
 Pct Recovery = 43%  Analysis Date = 02/16/14 
 Pct Recovery = 43%  Analysis Date = 02/16/14 
 Pct Recovery = 43%  Analysis Date = 02/14/14 
 Pct Recovery = 43%  Analysis Date = 02/14/14 
 Pct Recovery = 43%  Analysis Date = 02/12/14 
 Pct Recovery = 43%  Analysis Date = 02/12/14 
 Pct Recovery = 43%  Analysis Date = 02/09/14 
 Pct Recovery = 43%  Analysis Date = 02/09/14 
 Pct Recovery = 43%  Analysis Date = 02/07/14 
 Pct Recovery = 43%  Analysis Date = 02/07/14 
 Pct Recovery = 43%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/26/14 
 Pct Recovery = 43%  Analysis Date = 01/26/14 
 Pct Recovery = 43%  Analysis Date = 01/24/14 
 Pct Recovery = 43%  Analysis Date = 01/24/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/19/14 
 Pct Recovery = 42%  Analysis Date = 01/19/14 
 Pct Recovery = 42%  Analysis Date = 01/17/14 
 Pct Recovery = 42%  Analysis Date = 01/17/14 
 Pct Recovery = 42%  Analysis Date = 01/15/14 
 Pct Recovery = 42%  Analysis Date = 01/15/14 
 Pct Recovery = 42%  Analysis Date = 01/13/14 
 Pct Recovery = 42%  Analysis Date = 01/13/14 
 Pct Recovery = 42%  Analysis Date = 01/10/14 
 Pct Recovery = 42%  Analysis Date = 01/10/14 
 Pct Recovery = 42%  Analysis Date = 01/08/14 
 Pct Recovery = 42%  Analysis Date = 01/08/14 
 Pct Recovery = 42%  Analysis Date = 01/06/14 
 Pct Recovery = 42%  Analysis Date = 01/06/14 
 Pct Recovery = 42%  Analysis Date = 01/03/14 
 Pct Recovery = 42%  Analysis Date = 01/03/14 
 Pct Recovery = 42%  Analysis Date = 01/01/14 
 Pct Recovery = 42%  Analysis Date = 01/01/14 
 Pct Recovery = 42%  Analysis Date = 12/30/13 
 Pct Recovery = 42%  Analysis Date = 12/30/13 
 Pct Recovery = 42%  Analysis Date = 12/27/13 
 Pct Recovery = 42%  Analysis Date = 12/27/13 
 Pct Recovery = 42%  Analysis Date = 12/25/13 
 Pct Recovery = 42%  Analysis Date = 12/25/13 
 Pct Recovery = 42%  Analysis Date = 12/23/13 
 Pct Recovery = 42%  Analysis Date = 12/23/13 
 Pct Recovery = 42%  Analysis Date = 12/20/13 
 Pct Recovery = 42%  Analysis Date = 12/20/13 
 Pct Recovery = 42%  Analysis Date = 12/18/13 
 Pct Recovery = 42%  Analysis Date = 12/18/13 
 Pct Recovery = 42%  Analysis Date = 12/16/13 
 Pct Recovery = 42%  Analysis Date = 12/16/13 
 Pct Recovery = 42%  Analysis Date = 12/13/13 
 Pct Recovery = 42%  Analysis Date = 12/13/13 
 Pct Recovery = 42%  Analysis Date = 12/11/13 
 Pct Recovery = 42%  Analysis Date = 12/11/13 
 Pct Recovery = 42%  Analysis Date = 12/09/13 
 Pct Recovery = 42%  Analysis Date = 12/09/13 
 Pct Recovery = 42%  Analysis Date = 12/07/13 
 Pct Recovery = 42%  Analysis Date = 12/07/13 
 Pct Recovery = 42%  Analysis Date = 12/04/13 
 Pct Recovery = 42%  Analysis Date = 12/04/13 
 Pct Recovery = 42%  Analysis Date = 12/02/13 
 Pct Recovery = 42%  Analysis Date = 12/02/13 
 Pct Recovery = 42%  Analysis Date = 11/30/13 
 Pct Recovery = 41%  Analysis Date = 11/30/13 
 Pct Recovery = 41%  Analysis Date = 11/27/13 
 Pct Recovery = 41%  Analysis Date = 11/27/13 
 Pct Recovery = 41%  Analysis Date = 11/25/13 
 Pct Recovery = 41%  Analysis Date = 11/25/13 
 Pct Recovery = 41%  Analysis Date = 11/23/13 
 Pct Recovery = 41%  Analysis Date = 11/23/13 
 Pct Recovery = 41%  Analysis Date = 11/20/13 
 Pct Recovery = 41%  Analysis Date = 11/20/13 
 Pct Recovery = 41%  Analysis Date = 11/18/13 
 Pct Recovery = 41%  Analysis Date = 11/18/13 
 Pct Recovery = 41%  Analysis Date = 11/16/13 
 Pct Recovery = 41%  Analysis Date = 11/16/13 
 Pct Recovery = 41%  Analysis Date = 11/13/13 
 Pct Recovery = 41%  Analysis Date = 11/13/13 
 Pct Recovery = 41%  Analysis Date = 11/11/13 
 Pct Recovery = 41%  Analysis Date = 11/11/13 
 Pct Recovery = 41%  Analysis Date = 11/09/13 
 Pct Recovery = 41%  Analysis Date = 11/09/13 
 Pct Recovery = 41%  Analysis Date = 11/07/13 
 Pct Recovery = 41%  Analysis Date = 11/07/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/02/13 
 Pct Recovery = 40%  Analysis Date = 11/02/13 
 Pct Recovery = 40%  Analysis Date = 10/31/13 
 Pct Recovery = 40%  Analysis Date = 10/31/13 
 Pct Recovery = 40%  Analysis Date = 10/28/13 
 Pct Recovery = 40%  Analysis Date = 10/28/13 
 Pct Recovery = 40%  Analysis Date = 10/26/13 
 Pct Recovery = 40%  Analysis Date = 10/26/13 
 Pct Recovery = 40%  Analysis Date = 10/24/13 
 Pct Recovery = 40%  Analysis Date = 10/24/13 
 Pct Recovery = 40%  Analysis Date = 10/21/13 
 Pct Recovery = 40%  Analysis Date = 10/21/13 
 Pct Recovery = 40%  Analysis Date = 10/19/13 
 Pct Recovery = 40%  Analysis Date = 10/19/13 
 Pct Recovery = 40%  Analysis Date = 10/17/13 
 Pct Recovery = 40%  Analysis Date = 10/17/13 
 Pct Recovery = 40%  Analysis Date = 10/14/13 
 Pct Recovery = 40%  Analysis Date = 10/14/13 
 Pct Recovery = 40%  Analysis Date = 10/12/13 
 Pct Recovery = 40%  Analysis Date = 10/12/13 
 Pct Recovery = 40%  Analysis Date = 10/10/13 
 Pct Recovery = 40%  Analysis Date = 10/10/13 
 Pct Recovery = 40%  Analysis Date = 10/07/13 
 Pct Recovery = 39%  Analysis Date = 10/07/13 
 Pct Recovery = 39%  Analysis Date = 10/05/13 
 Pct Recovery = 39%  Analysis Date = 10/05/13 
 Pct Recovery = 39%  Analysis Date = 10/03/13 
 Pct Recovery = 39%  Analysis Date = 10/03/13 
 Pct Recovery = 39%  Analysis Date = 10/01/13 
 Pct Recovery = 39%  Analysis Date = 10/01/13 
 Pct Recovery = 39%  Analysis Date = 09/28/13 
 Pct Recovery = 39%  Analysis Date = 09/28/13 
 Pct Recovery = 39%  Analysis Date = 09/26/13 
 Pct Recovery = 39%  Analysis Date = 09/26/13 
 Pct Recovery = 39%  Analysis Date = 09/24/13 
 Pct Recovery = 39%  Analysis Date = 09/24/13 
 Pct Recovery = 39%  Analysis Date = 09/21/13 
 Pct Recovery = 39%  Analysis Date = 09/21/13 
 Pct Recovery = 39%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/19/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/17/13 
 Pct Recovery = 39%  Analysis Date = 09/14/13 
 Pct Recovery = 39%  Analysis Date = 09/14/13 
 Pct Recovery = 39%  Analysis Date = 09/12/13 
 Pct Recovery = 39%  Analysis Date = 09/12/13 
 Pct Recovery = 39%  Analysis Date = 09/10/13 
 Pct Recovery = 38%  Analysis Date = 09/10/13 
 Pct Recovery = 38%  Analysis Date = 09/07/13 
 Pct Recovery = 38%  Analysis Date = 09/07/13 
 Pct Recovery = 38%  Analysis Date = 09/05/13 
 Pct Recovery = 38%  Analysis Date = 09/05/13 
 Pct Recovery = 38%  Analysis Date = 09/03/13 
 Pct Recovery = 38%  Analysis Date = 09/03/13 
 Pct Recovery = 38%  Analysis Date = 09/01/13 
 Pct Recovery = 38%  Analysis Date = 09/01/13 
 Pct Recovery = 38%  Analysis Date = 08/29/13 
 Pct Recovery = 38%  Analysis Date = 08/29/13 
 Pct Recovery = 38%  Analysis Date = 08/27/13 
 Pct Recovery = 38%  Analysis Date = 08/27/13 
 Pct Recovery = 38%  Analysis Date = 08/25/13 
 Pct Recovery = 38%  Analysis Date = 08/25/13 
 Pct Recovery = 38%  Analysis Date = 08/22/13 
 Pct Recovery = 37%  Analysis Date = 08/22/13 
 Pct Recovery = 37%  Analysis Date = 08/20/13 
 Pct Recovery = 37%  Analysis Date = 08/20/13 
 Pct Recovery = 37%  Analysis Date = 08/18/13 
 Pct Recovery = 37%  Analysis Date = 08/18/13 
 Pct Recovery = 37%  Analysis Date = 08/15/13 
 Pct Recovery = 37%  Analysis Date = 08/15/13 
 Pct Recovery = 37%  Analysis Date = 08/13/13 
 Pct Recovery = 37%  Analysis Date = 08/13/13 
 Pct Recovery = 37%  Analysis Date = 08/11/13 
 Pct Recovery = 36%  Analysis Date = 08/11/13 
 Pct Recovery = 36%  Analysis Date = 08/08/13 
 Pct Recovery = 36%  Analysis Date = 08/08/13 
 Pct Recovery = 36%  Analysis Date = 08/06/13 
 Pct Recovery = 36%  Analysis Date = 08/06/13 
 Pct Recovery = 36%  Analysis Date = 08/04/13 
 Pct Recovery = 36%  Analysis Date = 08/04/13 
 Pct Recovery = 36%  Analysis Date = 08/02/13 
 Pct Recovery = 36%  Analysis Date = 08/02/13 
 Pct Recovery = 36%  Analysis Date = 07/30/13 
 Pct Recovery = 36%  Analysis Date = 07/30/13 
 Pct Recovery = 36%  Analysis Date = 07/28/13 
 Pct Recovery = 36%  Analysis Date = 07/28/13 
 Pct Recovery = 36%  Analysis Date = 07/26/13 
 Pct Recovery = 36%  Analysis Date = 07/26/13 
 Pct Recovery = 36%  Analysis Date = 07/23/13 
 Pct Recovery = 36%  Analysis Date = 07/23/13 
 Pct Recovery = 36%  Analysis Date = 07/21/13 
 Pct Recovery = 36%  Analysis Date = 07/21/13 
 Pct Recovery = 36%  Analysis Date = 07/19/13 
 Pct Recovery = 36%  Analysis Date = 07/19/13 
 Pct Recovery = 36%  Analysis Date = 07/16/13 
 Pct Recovery = 35%  Analysis Date = 07/16/13 
 Pct Recovery = 35%  Analysis Date = 07/14/13 
 Pct Recovery = 35%  Analysis Date = 07/14/13 
 Pct Recovery = 35%  Analysis Date = 07/12/13 
 Pct Recovery = 35%  Analysis Date = 07/12/13 
 Pct Recovery = 35%  Analysis Date = 07/09/13 
 Pct Recovery = 35%  Analysis Date = 07/09/13 
 Pct Recovery = 35%  Analysis Date = 07/07/13 
 Pct Recovery = 35%  Analysis Date = 07/07/13 
 Pct Recovery = 35%  Analysis Date = 07/05/13 
 Pct Recovery = 35%  Analysis Date = 07/05/13 
 Pct Recovery = 35%  Analysis Date = 07/02/13 
 Pct Recovery = 35%  Analysis Date = 07/02/13 
 Pct Recovery = 35%  Analysis Date = 06/30/13 
 Pct Recovery = 35%  Analysis Date = 06/30/13 
 Pct Recovery = 35%  Analysis Date = 06/28/13 
 Pct Recovery = 35%  Analysis Date = 06/28/13 
 Pct Recovery = 35%  Analysis Date = 06/26/13 
 Pct Recovery = 35%  Analysis Date = 06/26/13 
 Pct Recovery = 35%  Analysis Date = 06/23/13 
 Pct Recovery = 35%  Analysis Date = 06/23/13 
 Pct Recovery = 35%  Analysis Date = 06/21/13 
 Pct Recovery = 35%  Analysis Date = 06/21/13 
 Pct Recovery = 35%  Analysis Date = 06/19/13 
 Pct Recovery = 35%  Analysis Date = 06/19/13 
 Pct Recovery = 35%  Analysis Date = 06/16/13 
 Pct Recovery = 35%  Analysis Date = 06/16/13 
 Pct Recovery = 35%  Analysis Date = 06/14/13 
 Pct Recovery = 34%  Analysis Date = 06/14/13 
 Pct Recovery = 34%  Analysis Date = 06/12/13 
 Pct Recovery = 34%  Analysis Date = 06/12/13 
 Pct Recovery = 34%  Analysis Date = 06/09/13 
 Pct Recovery = 34%  Analysis Date = 06/09/13 
 Pct Recovery = 34%  Analysis Date = 06/07/13 
 Pct Recovery = 34%  Analysis Date = 06/07/13 
 Pct Recovery = 34%  Analysis Date = 06/05/13 
 Pct Recovery = 34%  Analysis Date = 06/05/13 
 Pct Recovery = 34%  Analysis Date = 06/02/13 
 Pct Recovery = 34%  Analysis Date = 06/02/13 
 Pct Recovery = 34%  Analysis Date = 05/31/13 
 Pct Recovery = 34%  Analysis Date = 05/31/13 
 Pct Recovery = 34%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/24/13 
 Pct Recovery = 34%  Analysis Date = 05/24/13 
 Pct Recovery = 34%  Analysis Date = 05/22/13 
 Pct Recovery = 34%  Analysis Date = 05/22/13 
 Pct Recovery = 34%  Analysis Date = 05/20/13 
 Pct Recovery = 34%  Analysis Date = 05/20/13 
 Pct Recovery = 34%  Analysis Date = 05/17/13 
 Pct Recovery = 34%  Analysis Date = 05/17/13 
 Pct Recovery = 34%  Analysis Date = 05/15/13 
 Pct Recovery = 34%  Analysis Date = 05/15/13 
 Pct Recovery = 34%  Analysis Date = 05/13/13 
 Pct Recovery = 34%  Analysis Date = 05/13/13 
 Pct Recovery = 34%  Analysis Date = 05/10/13 
 Pct Recovery = 33%  Analysis Date = 05/10/13 
 Pct Recovery = 33%  Analysis Date = 05/08/13 
 Pct Recovery = 33%  Analysis Date = 05/08/13 
 Pct Recovery = 33%  Analysis Date = 05/06/13 
 Pct Recovery = 33%  Analysis Date = 05/06/13 
 Pct Recovery = 33%  Analysis Date = 05/03/13 
 Pct Recovery = 33%  Analysis Date = 05/03/13 
 Pct Recovery = 33%  Analysis Date = 05/01/13 
 Pct Recovery = 33%  Analysis Date = 05/01/13 
 Pct Recovery = 33%  Analysis Date = 04/29/13 
 Pct Recovery = 34%  Analysis Date = 04/29/13 
 Pct Recovery = 34%  Analysis Date = 04/26/13 
 Pct Recovery = 34%  Analysis Date = 04/26/13 
 Pct Recovery = 34%  Analysis Date = 04/24/13 
 Pct Recovery = 35%  Analysis Date = 04/24/13 
 Pct Recovery = 35%  Analysis Date = 04/22/13 
 Pct Recovery = 35%  Analysis Date = 04/22/13 
 Pct Recovery = 35%  Analysis Date = 04/20/13 
 Pct Recovery = 35%  Analysis Date = 04/20/13 
 Pct Recovery = 35%  Analysis Date = 04/17/13 
 Pct Recovery = 36%  Analysis Date = 04/17/13 
 Pct Recovery = 36%  Analysis Date = 04/15/13 
 Pct Recovery = 36%  Analysis Date = 04/15/13 
 Pct Recovery = 36%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/10/13 
 Pct Recovery = 37%  Analysis Date = 04/10/13 
 Pct Recovery = 37%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/06/13 
 Pct Recovery = 38%  Analysis Date = 04/06/13 
 Pct Recovery = 38%  Analysis Date = 04/03/13 
 Pct Recovery = 38%  Analysis Date = 04/03/13 
 Pct Recovery = 38%  Analysis Date = 04/01/13 
 Pct Recovery = 38%  Analysis Date = 04/01/13 
 Pct Recovery = 38%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/23/13 
 Pct Recovery = 40%  Analysis Date = 03/23/13 
 Pct Recovery = 40%  Analysis Date = 03/21/13 
 Pct Recovery = 40%  Analysis Date = 03/21/13 
 Pct Recovery = 40%  Analysis Date = 03/18/13 
 Pct Recovery = 41%  Analysis Date = 03/18/13 
 Pct Recovery = 41%  Analysis Date = 03/16/13 
 Pct Recovery = 41%  Analysis Date = 03/16/13 
 Pct Recovery = 41%  Analysis Date = 03/14/13 
 Pct Recovery = 42%  Analysis Date = 03/14/13 
 Pct Recovery = 42%  Analysis Date = 03/11/13 
 Pct Recovery = 42%  Analysis Date = 03/11/13 
 Pct Recovery = 42%  Analysis Date = 03/09/13 
 Pct Recovery = 42%  Analysis Date = 03/09/13 
 Pct Recovery = 42%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/04/13 
 Pct Recovery = 43%  Analysis Date = 03/04/13 
 Pct Recovery = 43%  Analysis Date = 03/02/13 
 Pct Recovery = 44%  Analysis Date = 03/02/13 
 Pct Recovery = 44%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/28/13 
 Pct Recovery = 44%  Analysis Date = 02/25/13 
 Pct Recovery = 45%  Analysis Date = 02/25/13 
 Pct Recovery = 45%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/23/13 
 Pct Recovery = 45%  Analysis Date = 02/21/13 
 Pct Recovery = 45%  Analysis Date = 02/21/13 
 Pct Recovery = 45%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/18/13 
 Pct Recovery = 46%  Analysis Date = 02/16/13 
 Pct Recovery = 46%  Analysis Date = 02/16/13 
 Pct Recovery = 46%  Analysis Date = 02/14/13 
 Pct Recovery = 47%  Analysis Date = 02/14/13 
 Pct Recovery = 47%  Analysis Date = 02/12/13 
 Pct Recovery = 47%  Analysis Date = 02/12/13 
 Pct Recovery = 47%  Analysis Date = 02/09/13 
 Pct Recovery = 48%  Analysis Date = 02/09/13 
 Pct Recovery = 48%  Analysis Date = 02/07/13 
 Pct Recovery = 48%  Analysis Date = 02/07/13 
 Pct Recovery = 48%  Analysis Date = 02/05/13 
 Pct Recovery = 48%  Analysis Date = 02/05/13 
 Pct Recovery = 48%  Analysis Date = 02/02/13 
 Pct Recovery = 49%  Analysis Date = 02/02/13 
 Pct Recovery = 49%  Analysis Date = 01/31/13 
 Pct Recovery = 49%  Analysis Date = 01/31/13 
 Pct Recovery = 49%  Analysis Date = 01/29/13 
 Pct Recovery = 50%  Analysis Date = 01/29/13 
 Pct Recovery = 50%  Analysis Date = 01/26/13 
 Pct Recovery = 50%  Analysis Date = 01/26/13 
 Pct Recovery = 50%  Analysis Date = 01/24/13 
 Pct Recovery = 50%  Analysis Date = 01/24/13 
 Pct Recovery = 50%  Analysis Date = 01/22/13 
 Pct Recovery = 51%  Analysis Date = 01/22/13 
 Pct Recovery = 51%  Analysis Date = 01/19/13 
 Pct Recovery = 51%  Analysis Date = 01/19/13 
 Pct Recovery = 51%  Analysis Date = 01/17/13 
 Pct Recovery = 52%  Analysis Date = 01/17/13 
 Pct Recovery = 52%  Analysis Date = 01/15/13 
 Pct Recovery = 52%  Analysis Date = 01/15/13 
 Pct Recovery = 52%  Analysis Date = 01/13/13 
 Pct Recovery = 53%  Analysis Date = 01/13/13 
 Pct Recovery = 53%  Analysis Date = 01/10/13 
 Pct Recovery = 53%  Analysis Date = 01/10/13 
 Pct Recovery = 53%  Analysis Date = 01/08/13 
 Pct Recovery = 53%  Analysis Date = 01/08/13 
 Pct Recovery = 53%  Analysis Date = 01/06/13 
 Pct Recovery = 54%  Analysis Date = 01/06/13 
 Pct Recovery = 54%  Analysis Date = 01/03/13 
 Pct Recovery = 54%  Analysis Date = 01/03/13 
 Pct Recovery = 54%  Analysis Date = 01/01/13 
 Pct Recovery = 55%  Analysis Date = 01/01/13 
 Pct Recovery = 55%  Analysis Date = 12/30/12 
 Pct Recovery = 55%  Analysis Date = 12/30/12 
 Pct Recovery = 55%  Analysis Date = 12/27/12 
 Pct Recovery = 55%  Analysis Date = 12/27/12 
 Pct Recovery = 55%  Analysis Date = 12/25/12 
 Pct Recovery = 56%  Analysis Date = 12/25/12 
 Pct Recovery = 56%  Analysis Date = 12/23/12 
 Pct Recovery = 56%  Analysis Date = 12/23/12 
 Pct Recovery = 56%  Analysis Date = 12/20/12 
 Pct Recovery = 57%  Analysis Date = 12/20/12 
 Pct Recovery = 57%  Analysis Date = 12/18/12 
 Pct Recovery = 57%  Analysis Date = 12/18/12 
 Pct Recovery = 57%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/14/12 
 Pct Recovery = 58%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
KETOCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 41% 13% 42% 10%
Total 14 41% 13% 42% 10%

Sample Statistics
KETOCONAZOLE

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 4 27% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
LAMIVUDINE
METHOD: LC9017 , TESTIDCODE: 68018LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 76%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 78%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 70%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 59%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 70%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 80%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 96%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 54%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 108%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 84%  Analysis Date = 03/21/14 
 Pct Recovery = 62%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/11/14 
 Pct Recovery = 62%  Analysis Date = 03/11/14 
 Pct Recovery = 62%  Analysis Date = 03/09/14 
 Pct Recovery = 62%  Analysis Date = 03/09/14 
 Pct Recovery = 62%  Analysis Date = 03/07/14 
 Pct Recovery = 61%  Analysis Date = 03/07/14 
 Pct Recovery = 61%  Analysis Date = 03/04/14 
 Pct Recovery = 61%  Analysis Date = 03/04/14 
 Pct Recovery = 61%  Analysis Date = 03/02/14 
 Pct Recovery = 61%  Analysis Date = 03/02/14 
 Pct Recovery = 61%  Analysis Date = 02/28/14 
 Pct Recovery = 61%  Analysis Date = 02/28/14 
 Pct Recovery = 61%  Analysis Date = 02/25/14 
 Pct Recovery = 61%  Analysis Date = 02/25/14 
 Pct Recovery = 61%  Analysis Date = 02/23/14 
 Pct Recovery = 61%  Analysis Date = 02/23/14 
 Pct Recovery = 61%  Analysis Date = 02/21/14 
 Pct Recovery = 61%  Analysis Date = 02/21/14 
 Pct Recovery = 61%  Analysis Date = 02/18/14 
 Pct Recovery = 61%  Analysis Date = 02/18/14 
 Pct Recovery = 61%  Analysis Date = 02/16/14 
 Pct Recovery = 61%  Analysis Date = 02/16/14 
 Pct Recovery = 61%  Analysis Date = 02/14/14 
 Pct Recovery = 62%  Analysis Date = 02/14/14 
 Pct Recovery = 62%  Analysis Date = 02/12/14 
 Pct Recovery = 62%  Analysis Date = 02/12/14 
 Pct Recovery = 62%  Analysis Date = 02/09/14 
 Pct Recovery = 62%  Analysis Date = 02/09/14 
 Pct Recovery = 62%  Analysis Date = 02/07/14 
 Pct Recovery = 63%  Analysis Date = 02/07/14 
 Pct Recovery = 63%  Analysis Date = 02/05/14 
 Pct Recovery = 63%  Analysis Date = 02/05/14 
 Pct Recovery = 63%  Analysis Date = 02/02/14 
 Pct Recovery = 63%  Analysis Date = 02/02/14 
 Pct Recovery = 63%  Analysis Date = 01/31/14 
 Pct Recovery = 63%  Analysis Date = 01/31/14 
 Pct Recovery = 63%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/26/14 
 Pct Recovery = 64%  Analysis Date = 01/26/14 
 Pct Recovery = 64%  Analysis Date = 01/24/14 
 Pct Recovery = 64%  Analysis Date = 01/24/14 
 Pct Recovery = 64%  Analysis Date = 01/22/14 
 Pct Recovery = 64%  Analysis Date = 01/22/14 
 Pct Recovery = 64%  Analysis Date = 01/19/14 
 Pct Recovery = 65%  Analysis Date = 01/19/14 
 Pct Recovery = 65%  Analysis Date = 01/17/14 
 Pct Recovery = 65%  Analysis Date = 01/17/14 
 Pct Recovery = 65%  Analysis Date = 01/15/14 
 Pct Recovery = 65%  Analysis Date = 01/15/14 
 Pct Recovery = 65%  Analysis Date = 01/13/14 
 Pct Recovery = 65%  Analysis Date = 01/13/14 
 Pct Recovery = 65%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/30/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 68%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/13/13 
 Pct Recovery = 69%  Analysis Date = 12/13/13 
 Pct Recovery = 69%  Analysis Date = 12/11/13 
 Pct Recovery = 69%  Analysis Date = 12/11/13 
 Pct Recovery = 69%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/04/13 
 Pct Recovery = 70%  Analysis Date = 12/02/13 
 Pct Recovery = 70%  Analysis Date = 12/02/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/27/13 
 Pct Recovery = 71%  Analysis Date = 11/27/13 
 Pct Recovery = 71%  Analysis Date = 11/25/13 
 Pct Recovery = 71%  Analysis Date = 11/25/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/20/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/07/13 
 Pct Recovery = 73%  Analysis Date = 11/07/13 
 Pct Recovery = 73%  Analysis Date = 11/04/13 
 Pct Recovery = 74%  Analysis Date = 11/04/13 
 Pct Recovery = 74%  Analysis Date = 11/02/13 
 Pct Recovery = 74%  Analysis Date = 11/02/13 
 Pct Recovery = 74%  Analysis Date = 10/31/13 
 Pct Recovery = 74%  Analysis Date = 10/31/13 
 Pct Recovery = 74%  Analysis Date = 10/28/13 
 Pct Recovery = 74%  Analysis Date = 10/28/13 
 Pct Recovery = 74%  Analysis Date = 10/26/13 
 Pct Recovery = 75%  Analysis Date = 10/26/13 
 Pct Recovery = 75%  Analysis Date = 10/24/13 
 Pct Recovery = 75%  Analysis Date = 10/24/13 
 Pct Recovery = 75%  Analysis Date = 10/21/13 
 Pct Recovery = 75%  Analysis Date = 10/21/13 
 Pct Recovery = 75%  Analysis Date = 10/19/13 
 Pct Recovery = 76%  Analysis Date = 10/19/13 
 Pct Recovery = 76%  Analysis Date = 10/17/13 
 Pct Recovery = 76%  Analysis Date = 10/17/13 
 Pct Recovery = 76%  Analysis Date = 10/14/13 
 Pct Recovery = 76%  Analysis Date = 10/14/13 
 Pct Recovery = 76%  Analysis Date = 10/12/13 
 Pct Recovery = 76%  Analysis Date = 10/12/13 
 Pct Recovery = 76%  Analysis Date = 10/10/13 
 Pct Recovery = 77%  Analysis Date = 10/10/13 
 Pct Recovery = 77%  Analysis Date = 10/07/13 
 Pct Recovery = 77%  Analysis Date = 10/07/13 
 Pct Recovery = 77%  Analysis Date = 10/05/13 
 Pct Recovery = 77%  Analysis Date = 10/05/13 
 Pct Recovery = 77%  Analysis Date = 10/03/13 
 Pct Recovery = 77%  Analysis Date = 10/03/13 
 Pct Recovery = 77%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 09/28/13 
 Pct Recovery = 78%  Analysis Date = 09/28/13 
 Pct Recovery = 78%  Analysis Date = 09/26/13 
 Pct Recovery = 78%  Analysis Date = 09/26/13 
 Pct Recovery = 78%  Analysis Date = 09/24/13 
 Pct Recovery = 78%  Analysis Date = 09/24/13 
 Pct Recovery = 78%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/10/13 
 Pct Recovery = 80%  Analysis Date = 09/10/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/03/13 
 Pct Recovery = 81%  Analysis Date = 09/03/13 
 Pct Recovery = 81%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 08/29/13 
 Pct Recovery = 81%  Analysis Date = 08/29/13 
 Pct Recovery = 81%  Analysis Date = 08/27/13 
 Pct Recovery = 82%  Analysis Date = 08/27/13 
 Pct Recovery = 82%  Analysis Date = 08/25/13 
 Pct Recovery = 82%  Analysis Date = 08/25/13 
 Pct Recovery = 82%  Analysis Date = 08/22/13 
 Pct Recovery = 82%  Analysis Date = 08/22/13 
 Pct Recovery = 82%  Analysis Date = 08/20/13 
 Pct Recovery = 82%  Analysis Date = 08/20/13 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 Pct Recovery = 82%  Analysis Date = 08/15/13 
 Pct Recovery = 82%  Analysis Date = 08/15/13 
 Pct Recovery = 82%  Analysis Date = 08/13/13 
 Pct Recovery = 82%  Analysis Date = 08/13/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/08/13 
 Pct Recovery = 82%  Analysis Date = 08/08/13 
 Pct Recovery = 82%  Analysis Date = 08/06/13 
 Pct Recovery = 82%  Analysis Date = 08/06/13 
 Pct Recovery = 82%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 81%  Analysis Date = 07/21/13 
 Pct Recovery = 81%  Analysis Date = 07/19/13 
 Pct Recovery = 81%  Analysis Date = 07/19/13 
 Pct Recovery = 81%  Analysis Date = 07/16/13 
 Pct Recovery = 81%  Analysis Date = 07/16/13 
 Pct Recovery = 81%  Analysis Date = 07/14/13 
 Pct Recovery = 81%  Analysis Date = 07/14/13 
 Pct Recovery = 81%  Analysis Date = 07/12/13 
 Pct Recovery = 81%  Analysis Date = 07/12/13 
 Pct Recovery = 81%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/07/13 
 Pct Recovery = 81%  Analysis Date = 07/07/13 
 Pct Recovery = 81%  Analysis Date = 07/05/13 
 Pct Recovery = 81%  Analysis Date = 07/05/13 
 Pct Recovery = 81%  Analysis Date = 07/02/13 
 Pct Recovery = 81%  Analysis Date = 07/02/13 
 Pct Recovery = 81%  Analysis Date = 06/30/13 
 Pct Recovery = 81%  Analysis Date = 06/30/13 
 Pct Recovery = 81%  Analysis Date = 06/28/13 
 Pct Recovery = 80%  Analysis Date = 06/28/13 
 Pct Recovery = 80%  Analysis Date = 06/26/13 
 Pct Recovery = 80%  Analysis Date = 06/26/13 
 Pct Recovery = 80%  Analysis Date = 06/23/13 
 Pct Recovery = 80%  Analysis Date = 06/23/13 
 Pct Recovery = 80%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/02/13 
 Pct Recovery = 79%  Analysis Date = 06/02/13 
 Pct Recovery = 79%  Analysis Date = 05/31/13 
 Pct Recovery = 79%  Analysis Date = 05/31/13 
 Pct Recovery = 79%  Analysis Date = 05/29/13 
 Pct Recovery = 79%  Analysis Date = 05/29/13 
 Pct Recovery = 79%  Analysis Date = 05/27/13 
 Pct Recovery = 79%  Analysis Date = 05/27/13 
 Pct Recovery = 79%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/20/13 
 Pct Recovery = 79%  Analysis Date = 05/20/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 78%  Analysis Date = 05/08/13 
 Pct Recovery = 78%  Analysis Date = 05/06/13 
 Pct Recovery = 78%  Analysis Date = 05/06/13 
 Pct Recovery = 78%  Analysis Date = 05/03/13 
 Pct Recovery = 78%  Analysis Date = 05/03/13 
 Pct Recovery = 78%  Analysis Date = 05/01/13 
 Pct Recovery = 78%  Analysis Date = 05/01/13 
 Pct Recovery = 78%  Analysis Date = 04/29/13 
 Pct Recovery = 79%  Analysis Date = 04/29/13 
 Pct Recovery = 79%  Analysis Date = 04/26/13 
 Pct Recovery = 79%  Analysis Date = 04/26/13 
 Pct Recovery = 79%  Analysis Date = 04/24/13 
 Pct Recovery = 79%  Analysis Date = 04/24/13 
 Pct Recovery = 79%  Analysis Date = 04/22/13 
 Pct Recovery = 80%  Analysis Date = 04/22/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/17/13 
 Pct Recovery = 80%  Analysis Date = 04/17/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/10/13 
 Pct Recovery = 81%  Analysis Date = 04/10/13 
 Pct Recovery = 81%  Analysis Date = 04/08/13 
 Pct Recovery = 81%  Analysis Date = 04/08/13 
 Pct Recovery = 81%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 82%  Analysis Date = 03/30/13 
 Pct Recovery = 82%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/25/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/23/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/21/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/18/13 
 Pct Recovery = 83%  Analysis Date = 03/16/13 
 Pct Recovery = 83%  Analysis Date = 03/16/13 
 Pct Recovery = 83%  Analysis Date = 03/14/13 
 Pct Recovery = 83%  Analysis Date = 03/14/13 
 Pct Recovery = 83%  Analysis Date = 03/11/13 
 Pct Recovery = 82%  Analysis Date = 03/11/13 
 Pct Recovery = 82%  Analysis Date = 03/09/13 
 Pct Recovery = 82%  Analysis Date = 03/09/13 
 Pct Recovery = 82%  Analysis Date = 03/07/13 
 Pct Recovery = 82%  Analysis Date = 03/07/13 
 Pct Recovery = 82%  Analysis Date = 03/04/13 
 Pct Recovery = 82%  Analysis Date = 03/04/13 
 Pct Recovery = 82%  Analysis Date = 03/02/13 
 Pct Recovery = 82%  Analysis Date = 03/02/13 
 Pct Recovery = 82%  Analysis Date = 02/28/13 
 Pct Recovery = 82%  Analysis Date = 02/28/13 
 Pct Recovery = 82%  Analysis Date = 02/25/13 
 Pct Recovery = 82%  Analysis Date = 02/25/13 
 Pct Recovery = 82%  Analysis Date = 02/23/13 
 Pct Recovery = 82%  Analysis Date = 02/23/13 
 Pct Recovery = 82%  Analysis Date = 02/21/13 
 Pct Recovery = 82%  Analysis Date = 02/21/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/18/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/16/13 
 Pct Recovery = 82%  Analysis Date = 02/14/13 
 Pct Recovery = 82%  Analysis Date = 02/14/13 
 Pct Recovery = 82%  Analysis Date = 02/12/13 
 Pct Recovery = 82%  Analysis Date = 02/12/13 
 Pct Recovery = 82%  Analysis Date = 02/09/13 
 Pct Recovery = 82%  Analysis Date = 02/09/13 
 Pct Recovery = 82%  Analysis Date = 02/07/13 
 Pct Recovery = 82%  Analysis Date = 02/07/13 
 Pct Recovery = 82%  Analysis Date = 02/05/13 
 Pct Recovery = 82%  Analysis Date = 02/05/13 
 Pct Recovery = 82%  Analysis Date = 02/02/13 
 Pct Recovery = 82%  Analysis Date = 02/02/13 
 Pct Recovery = 82%  Analysis Date = 01/31/13 
 Pct Recovery = 82%  Analysis Date = 01/31/13 
 Pct Recovery = 82%  Analysis Date = 01/29/13 
 Pct Recovery = 82%  Analysis Date = 01/29/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/24/13 
 Pct Recovery = 82%  Analysis Date = 01/24/13 
 Pct Recovery = 82%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/13/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/10/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/08/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/06/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/03/13 
 Pct Recovery = 82%  Analysis Date = 01/01/13 
 Pct Recovery = 82%  Analysis Date = 01/01/13 
 Pct Recovery = 82%  Analysis Date = 12/30/12 
 Pct Recovery = 82%  Analysis Date = 12/30/12 
 Pct Recovery = 82%  Analysis Date = 12/27/12 
 Pct Recovery = 82%  Analysis Date = 12/27/12 
 Pct Recovery = 82%  Analysis Date = 12/25/12 
 Pct Recovery = 81%  Analysis Date = 12/25/12 
 Pct Recovery = 81%  Analysis Date = 12/23/12 
 Pct Recovery = 81%  Analysis Date = 12/23/12 
 Pct Recovery = 81%  Analysis Date = 12/20/12 
 Pct Recovery = 81%  Analysis Date = 12/20/12 
 Pct Recovery = 81%  Analysis Date = 12/18/12 
 Pct Recovery = 81%  Analysis Date = 12/18/12 
 Pct Recovery = 81%  Analysis Date = 12/16/12 
 Pct Recovery = 81%  Analysis Date = 12/16/12 
 Pct Recovery = 81%  Analysis Date = 12/14/12 
 Pct Recovery = 81%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
LAMIVUDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 84% . 84% 0%
>= Reporting Level 10 75% 17% 73% 13%
Total 11 76% 16% 76% 17%

Sample Statistics
LAMIVUDINE

Characteristic N % % Basis
Plotted 11 73% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 4 27% 4 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
LIDOCAINE
METHOD: LC9017 , TESTIDCODE: 67462LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 77%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 92%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 88%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 96%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 77%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 68%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 79%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 88%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 49%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 63%  Analysis Date = 03/21/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 67%  Analysis Date = 03/16/14 
 Pct Recovery = 67%  Analysis Date = 03/14/14 
 Pct Recovery = 67%  Analysis Date = 03/14/14 
 Pct Recovery = 67%  Analysis Date = 03/11/14 
 Pct Recovery = 67%  Analysis Date = 03/11/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/07/14 
 Pct Recovery = 67%  Analysis Date = 03/07/14 
 Pct Recovery = 67%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 02/28/14 
 Pct Recovery = 66%  Analysis Date = 02/28/14 
 Pct Recovery = 66%  Analysis Date = 02/25/14 
 Pct Recovery = 66%  Analysis Date = 02/25/14 
 Pct Recovery = 66%  Analysis Date = 02/23/14 
 Pct Recovery = 66%  Analysis Date = 02/23/14 
 Pct Recovery = 66%  Analysis Date = 02/21/14 
 Pct Recovery = 65%  Analysis Date = 02/21/14 
 Pct Recovery = 65%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/16/14 
 Pct Recovery = 65%  Analysis Date = 02/16/14 
 Pct Recovery = 65%  Analysis Date = 02/14/14 
 Pct Recovery = 65%  Analysis Date = 02/14/14 
 Pct Recovery = 65%  Analysis Date = 02/12/14 
 Pct Recovery = 65%  Analysis Date = 02/12/14 
 Pct Recovery = 65%  Analysis Date = 02/09/14 
 Pct Recovery = 65%  Analysis Date = 02/09/14 
 Pct Recovery = 65%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/05/14 
 Pct Recovery = 64%  Analysis Date = 02/05/14 
 Pct Recovery = 64%  Analysis Date = 02/02/14 
 Pct Recovery = 64%  Analysis Date = 02/02/14 
 Pct Recovery = 64%  Analysis Date = 01/31/14 
 Pct Recovery = 64%  Analysis Date = 01/31/14 
 Pct Recovery = 64%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/29/14 
 Pct Recovery = 64%  Analysis Date = 01/26/14 
 Pct Recovery = 64%  Analysis Date = 01/26/14 
 Pct Recovery = 64%  Analysis Date = 01/24/14 
 Pct Recovery = 63%  Analysis Date = 01/24/14 
 Pct Recovery = 63%  Analysis Date = 01/22/14 
 Pct Recovery = 63%  Analysis Date = 01/22/14 
 Pct Recovery = 63%  Analysis Date = 01/19/14 
 Pct Recovery = 63%  Analysis Date = 01/19/14 
 Pct Recovery = 63%  Analysis Date = 01/17/14 
 Pct Recovery = 63%  Analysis Date = 01/17/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/08/14 
 Pct Recovery = 63%  Analysis Date = 01/08/14 
 Pct Recovery = 63%  Analysis Date = 01/06/14 
 Pct Recovery = 63%  Analysis Date = 01/06/14 
 Pct Recovery = 63%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 12/30/13 
 Pct Recovery = 64%  Analysis Date = 12/30/13 
 Pct Recovery = 64%  Analysis Date = 12/27/13 
 Pct Recovery = 64%  Analysis Date = 12/27/13 
 Pct Recovery = 64%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/25/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/23/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 65%  Analysis Date = 12/18/13 
 Pct Recovery = 65%  Analysis Date = 12/16/13 
 Pct Recovery = 65%  Analysis Date = 12/16/13 
 Pct Recovery = 65%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/02/13 
 Pct Recovery = 66%  Analysis Date = 12/02/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/27/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/25/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/20/13 
 Pct Recovery = 66%  Analysis Date = 11/20/13 
 Pct Recovery = 66%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/18/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/16/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/13/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/11/13 
 Pct Recovery = 67%  Analysis Date = 11/09/13 
 Pct Recovery = 68%  Analysis Date = 11/09/13 
 Pct Recovery = 68%  Analysis Date = 11/07/13 
 Pct Recovery = 68%  Analysis Date = 11/07/13 
 Pct Recovery = 68%  Analysis Date = 11/04/13 
 Pct Recovery = 68%  Analysis Date = 11/04/13 
 Pct Recovery = 68%  Analysis Date = 11/02/13 
 Pct Recovery = 68%  Analysis Date = 11/02/13 
 Pct Recovery = 68%  Analysis Date = 10/31/13 
 Pct Recovery = 68%  Analysis Date = 10/31/13 
 Pct Recovery = 68%  Analysis Date = 10/28/13 
 Pct Recovery = 69%  Analysis Date = 10/28/13 
 Pct Recovery = 69%  Analysis Date = 10/26/13 
 Pct Recovery = 69%  Analysis Date = 10/26/13 
 Pct Recovery = 69%  Analysis Date = 10/24/13 
 Pct Recovery = 69%  Analysis Date = 10/24/13 
 Pct Recovery = 69%  Analysis Date = 10/21/13 
 Pct Recovery = 69%  Analysis Date = 10/21/13 
 Pct Recovery = 69%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/17/13 
 Pct Recovery = 70%  Analysis Date = 10/17/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/10/13 
 Pct Recovery = 71%  Analysis Date = 10/07/13 
 Pct Recovery = 71%  Analysis Date = 10/07/13 
 Pct Recovery = 71%  Analysis Date = 10/05/13 
 Pct Recovery = 71%  Analysis Date = 10/05/13 
 Pct Recovery = 71%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/03/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 10/01/13 
 Pct Recovery = 71%  Analysis Date = 09/28/13 
 Pct Recovery = 72%  Analysis Date = 09/28/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/10/13 
 Pct Recovery = 74%  Analysis Date = 09/10/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/03/13 
 Pct Recovery = 74%  Analysis Date = 09/03/13 
 Pct Recovery = 74%  Analysis Date = 09/01/13 
 Pct Recovery = 74%  Analysis Date = 09/01/13 
 Pct Recovery = 74%  Analysis Date = 08/29/13 
 Pct Recovery = 75%  Analysis Date = 08/29/13 
 Pct Recovery = 75%  Analysis Date = 08/27/13 
 Pct Recovery = 75%  Analysis Date = 08/27/13 
 Pct Recovery = 75%  Analysis Date = 08/25/13 
 Pct Recovery = 75%  Analysis Date = 08/25/13 
 Pct Recovery = 75%  Analysis Date = 08/22/13 
 Pct Recovery = 75%  Analysis Date = 08/22/13 
 Pct Recovery = 75%  Analysis Date = 08/20/13 
 Pct Recovery = 75%  Analysis Date = 08/20/13 
 Pct Recovery = 75%  Analysis Date = 08/18/13 
 Pct Recovery = 75%  Analysis Date = 08/18/13 
 Pct Recovery = 75%  Analysis Date = 08/15/13 
 Pct Recovery = 76%  Analysis Date = 08/15/13 
 Pct Recovery = 76%  Analysis Date = 08/13/13 
 Pct Recovery = 76%  Analysis Date = 08/13/13 
 Pct Recovery = 76%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/08/13 
 Pct Recovery = 76%  Analysis Date = 08/08/13 
 Pct Recovery = 76%  Analysis Date = 08/06/13 
 Pct Recovery = 76%  Analysis Date = 08/06/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 77%  Analysis Date = 08/02/13 
 Pct Recovery = 77%  Analysis Date = 07/30/13 
 Pct Recovery = 77%  Analysis Date = 07/30/13 
 Pct Recovery = 77%  Analysis Date = 07/28/13 
 Pct Recovery = 77%  Analysis Date = 07/28/13 
 Pct Recovery = 77%  Analysis Date = 07/26/13 
 Pct Recovery = 77%  Analysis Date = 07/26/13 
 Pct Recovery = 77%  Analysis Date = 07/23/13 
 Pct Recovery = 77%  Analysis Date = 07/23/13 
 Pct Recovery = 77%  Analysis Date = 07/21/13 
 Pct Recovery = 77%  Analysis Date = 07/21/13 
 Pct Recovery = 77%  Analysis Date = 07/19/13 
 Pct Recovery = 78%  Analysis Date = 07/19/13 
 Pct Recovery = 78%  Analysis Date = 07/16/13 
 Pct Recovery = 78%  Analysis Date = 07/16/13 
 Pct Recovery = 78%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/12/13 
 Pct Recovery = 78%  Analysis Date = 07/12/13 
 Pct Recovery = 78%  Analysis Date = 07/09/13 
 Pct Recovery = 78%  Analysis Date = 07/09/13 
 Pct Recovery = 78%  Analysis Date = 07/07/13 
 Pct Recovery = 78%  Analysis Date = 07/07/13 
 Pct Recovery = 78%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 06/30/13 
 Pct Recovery = 79%  Analysis Date = 06/30/13 
 Pct Recovery = 79%  Analysis Date = 06/28/13 
 Pct Recovery = 79%  Analysis Date = 06/28/13 
 Pct Recovery = 79%  Analysis Date = 06/26/13 
 Pct Recovery = 79%  Analysis Date = 06/26/13 
 Pct Recovery = 79%  Analysis Date = 06/23/13 
 Pct Recovery = 79%  Analysis Date = 06/23/13 
 Pct Recovery = 79%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/02/13 
 Pct Recovery = 81%  Analysis Date = 06/02/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/27/13 
 Pct Recovery = 81%  Analysis Date = 05/27/13 
 Pct Recovery = 81%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/20/13 
 Pct Recovery = 82%  Analysis Date = 05/20/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/15/13 
 Pct Recovery = 82%  Analysis Date = 05/15/13 
 Pct Recovery = 82%  Analysis Date = 05/13/13 
 Pct Recovery = 82%  Analysis Date = 05/13/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 83%  Analysis Date = 05/10/13 
 Pct Recovery = 83%  Analysis Date = 05/08/13 
 Pct Recovery = 83%  Analysis Date = 05/08/13 
 Pct Recovery = 83%  Analysis Date = 05/06/13 
 Pct Recovery = 83%  Analysis Date = 05/06/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/01/13 
 Pct Recovery = 83%  Analysis Date = 05/01/13 
 Pct Recovery = 83%  Analysis Date = 04/29/13 
 Pct Recovery = 83%  Analysis Date = 04/29/13 
 Pct Recovery = 83%  Analysis Date = 04/26/13 
 Pct Recovery = 84%  Analysis Date = 04/26/13 
 Pct Recovery = 84%  Analysis Date = 04/24/13 
 Pct Recovery = 84%  Analysis Date = 04/24/13 
 Pct Recovery = 84%  Analysis Date = 04/22/13 
 Pct Recovery = 84%  Analysis Date = 04/22/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/17/13 
 Pct Recovery = 84%  Analysis Date = 04/17/13 
 Pct Recovery = 84%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 85%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/10/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 85%  Analysis Date = 04/06/13 
 Pct Recovery = 85%  Analysis Date = 04/06/13 
 Pct Recovery = 85%  Analysis Date = 04/03/13 
 Pct Recovery = 86%  Analysis Date = 04/03/13 
 Pct Recovery = 86%  Analysis Date = 04/01/13 
 Pct Recovery = 86%  Analysis Date = 04/01/13 
 Pct Recovery = 86%  Analysis Date = 03/30/13 
 Pct Recovery = 86%  Analysis Date = 03/30/13 
 Pct Recovery = 86%  Analysis Date = 03/27/13 
 Pct Recovery = 86%  Analysis Date = 03/27/13 
 Pct Recovery = 86%  Analysis Date = 03/25/13 
 Pct Recovery = 86%  Analysis Date = 03/25/13 
 Pct Recovery = 86%  Analysis Date = 03/23/13 
 Pct Recovery = 87%  Analysis Date = 03/23/13 
 Pct Recovery = 87%  Analysis Date = 03/21/13 
 Pct Recovery = 87%  Analysis Date = 03/21/13 
 Pct Recovery = 87%  Analysis Date = 03/18/13 
 Pct Recovery = 87%  Analysis Date = 03/18/13 
 Pct Recovery = 87%  Analysis Date = 03/16/13 
 Pct Recovery = 87%  Analysis Date = 03/16/13 
 Pct Recovery = 87%  Analysis Date = 03/14/13 
 Pct Recovery = 87%  Analysis Date = 03/14/13 
 Pct Recovery = 87%  Analysis Date = 03/11/13 
 Pct Recovery = 88%  Analysis Date = 03/11/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/07/13 
 Pct Recovery = 88%  Analysis Date = 03/07/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/25/13 
 Pct Recovery = 89%  Analysis Date = 02/25/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/18/13 
 Pct Recovery = 89%  Analysis Date = 02/18/13 
 Pct Recovery = 89%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/16/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/14/13 
 Pct Recovery = 90%  Analysis Date = 02/12/13 
 Pct Recovery = 90%  Analysis Date = 02/12/13 
 Pct Recovery = 90%  Analysis Date = 02/09/13 
 Pct Recovery = 90%  Analysis Date = 02/09/13 
 Pct Recovery = 90%  Analysis Date = 02/07/13 
 Pct Recovery = 90%  Analysis Date = 02/07/13 
 Pct Recovery = 90%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/29/13 
 Pct Recovery = 91%  Analysis Date = 01/29/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 92%  Analysis Date = 01/26/13 
 Pct Recovery = 92%  Analysis Date = 01/24/13 
 Pct Recovery = 92%  Analysis Date = 01/24/13 
 Pct Recovery = 92%  Analysis Date = 01/22/13 
 Pct Recovery = 92%  Analysis Date = 01/22/13 
 Pct Recovery = 92%  Analysis Date = 01/19/13 
 Pct Recovery = 92%  Analysis Date = 01/19/13 
 Pct Recovery = 92%  Analysis Date = 01/17/13 
 Pct Recovery = 92%  Analysis Date = 01/17/13 
 Pct Recovery = 92%  Analysis Date = 01/15/13 
 Pct Recovery = 93%  Analysis Date = 01/15/13 
 Pct Recovery = 93%  Analysis Date = 01/13/13 
 Pct Recovery = 93%  Analysis Date = 01/13/13 
 Pct Recovery = 93%  Analysis Date = 01/10/13 
 Pct Recovery = 93%  Analysis Date = 01/10/13 
 Pct Recovery = 93%  Analysis Date = 01/08/13 
 Pct Recovery = 93%  Analysis Date = 01/08/13 
 Pct Recovery = 93%  Analysis Date = 01/06/13 
 Pct Recovery = 93%  Analysis Date = 01/06/13 
 Pct Recovery = 93%  Analysis Date = 01/03/13 
 Pct Recovery = 94%  Analysis Date = 01/03/13 
 Pct Recovery = 94%  Analysis Date = 01/01/13 
 Pct Recovery = 94%  Analysis Date = 01/01/13 
 Pct Recovery = 94%  Analysis Date = 12/30/12 
 Pct Recovery = 94%  Analysis Date = 12/30/12 
 Pct Recovery = 94%  Analysis Date = 12/27/12 
 Pct Recovery = 94%  Analysis Date = 12/27/12 
 Pct Recovery = 94%  Analysis Date = 12/25/12 
 Pct Recovery = 95%  Analysis Date = 12/25/12 
 Pct Recovery = 95%  Analysis Date = 12/23/12 
 Pct Recovery = 95%  Analysis Date = 12/23/12 
 Pct Recovery = 95%  Analysis Date = 12/20/12 
 Pct Recovery = 95%  Analysis Date = 12/20/12 
 Pct Recovery = 95%  Analysis Date = 12/18/12 
 Pct Recovery = 95%  Analysis Date = 12/18/12 
 Pct Recovery = 95%  Analysis Date = 12/16/12 
 Pct Recovery = 95%  Analysis Date = 12/16/12 
 Pct Recovery = 95%  Analysis Date = 12/14/12 
 Pct Recovery = 96%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
LIDOCAINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 76% 14% 77% 18%
Total 11 76% 14% 77% 18%

Sample Statistics
LIDOCAINE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 1 9% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
LOPERAMIDE
METHOD: LC9017 , TESTIDCODE: 67515LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 48%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 43%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 34%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 13%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 30%  Analysis Date = 03/20/14 
 Pct Recovery = 43%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/18/14 
 Pct Recovery = 42%  Analysis Date = 03/16/14 
 Pct Recovery = 41%  Analysis Date = 03/16/14 
 Pct Recovery = 41%  Analysis Date = 03/14/14 
 Pct Recovery = 41%  Analysis Date = 03/14/14 
 Pct Recovery = 41%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/10/14 
 Pct Recovery = 40%  Analysis Date = 03/10/14 
 Pct Recovery = 40%  Analysis Date = 03/08/14 
 Pct Recovery = 39%  Analysis Date = 03/08/14 
 Pct Recovery = 39%  Analysis Date = 03/06/14 
 Pct Recovery = 38%  Analysis Date = 03/06/14 
 Pct Recovery = 38%  Analysis Date = 03/04/14 
 Pct Recovery = 38%  Analysis Date = 03/04/14 
 Pct Recovery = 38%  Analysis Date = 03/02/14 
 Pct Recovery = 37%  Analysis Date = 03/02/14 
 Pct Recovery = 37%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/25/14 
 Pct Recovery = 36%  Analysis Date = 02/25/14 
 Pct Recovery = 36%  Analysis Date = 02/23/14 
 Pct Recovery = 35%  Analysis Date = 02/23/14 
 Pct Recovery = 35%  Analysis Date = 02/21/14 
 Pct Recovery = 35%  Analysis Date = 02/21/14 
 Pct Recovery = 35%  Analysis Date = 02/19/14 
 Pct Recovery = 34%  Analysis Date = 02/19/14 
 Pct Recovery = 34%  Analysis Date = 02/17/14 
 Pct Recovery = 33%  Analysis Date = 02/17/14 
 Pct Recovery = 33%  Analysis Date = 02/15/14 
 Pct Recovery = 31%  Analysis Date = 02/15/14 
 Pct Recovery = 31%  Analysis Date = 02/13/14 
 Pct Recovery = 30%  Analysis Date = 02/13/14 
 Pct Recovery = 30%  Analysis Date = 02/11/14 
 Pct Recovery = 29%  Analysis Date = 02/11/14 
 Pct Recovery = 29%  Analysis Date = 02/09/14 
 Pct Recovery = 28%  Analysis Date = 02/09/14 
 Pct Recovery = 28%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/04/14 
 Pct Recovery = 25%  Analysis Date = 02/04/14 
 Pct Recovery = 25%  Analysis Date = 02/02/14 
 Pct Recovery = 24%  Analysis Date = 02/02/14 
 Pct Recovery = 24%  Analysis Date = 01/31/14 
 Pct Recovery = 22%  Analysis Date = 01/31/14 
 Pct Recovery = 22%  Analysis Date = 01/29/14 
 Pct Recovery = 21%  Analysis Date = 01/29/14 
 Pct Recovery = 21%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 18%  Analysis Date = 01/25/14 
 Pct Recovery = 18%  Analysis Date = 01/23/14 
 Pct Recovery = 17%  Analysis Date = 01/23/14 
 Pct Recovery = 17%  Analysis Date = 01/21/14 
 Pct Recovery = 16%  Analysis Date = 01/21/14 
 Pct Recovery = 16%  Analysis Date = 01/18/14 
 Pct Recovery = 15%  Analysis Date = 01/18/14 
 Pct Recovery = 15%  Analysis Date = 01/16/14 
 Pct Recovery = 13%  Analysis Date = 01/16/14 
 Pct Recovery = 13%  Analysis Date = 01/14/14 
 Pct Recovery = 13%  Analysis Date = 01/14/14 
 Pct Recovery = 13%  Analysis Date = 01/12/14 
 Pct Recovery = 14%  Analysis Date = 01/12/14 
 Pct Recovery = 14%  Analysis Date = 01/10/14 
 Pct Recovery = 14%  Analysis Date = 01/10/14 
 Pct Recovery = 14%  Analysis Date = 01/08/14 
 Pct Recovery = 15%  Analysis Date = 01/08/14 
 Pct Recovery = 15%  Analysis Date = 01/06/14 
 Pct Recovery = 16%  Analysis Date = 01/06/14 
 Pct Recovery = 16%  Analysis Date = 01/04/14 
 Pct Recovery = 16%  Analysis Date = 01/04/14 
 Pct Recovery = 16%  Analysis Date = 01/02/14 
 Pct Recovery = 17%  Analysis Date = 01/02/14 
 Pct Recovery = 17%  Analysis Date = 12/31/13 
 Pct Recovery = 17%  Analysis Date = 12/31/13 
 Pct Recovery = 17%  Analysis Date = 12/28/13 
 Pct Recovery = 18%  Analysis Date = 12/28/13 
 Pct Recovery = 18%  Analysis Date = 12/26/13 
 Pct Recovery = 19%  Analysis Date = 12/26/13 
 Pct Recovery = 19%  Analysis Date = 12/24/13 
 Pct Recovery = 19%  Analysis Date = 12/24/13 
 Pct Recovery = 19%  Analysis Date = 12/22/13 
 Pct Recovery = 20%  Analysis Date = 12/22/13 
 Pct Recovery = 20%  Analysis Date = 12/20/13 
 Pct Recovery = 21%  Analysis Date = 12/20/13 
 Pct Recovery = 21%  Analysis Date = 12/18/13 
 Pct Recovery = 21%  Analysis Date = 12/18/13 
 Pct Recovery = 21%  Analysis Date = 12/16/13 
 Pct Recovery = 22%  Analysis Date = 12/16/13 
 Pct Recovery = 22%  Analysis Date = 12/14/13 
 Pct Recovery = 22%  Analysis Date = 12/14/13 
 Pct Recovery = 22%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/09/13 
 Pct Recovery = 24%  Analysis Date = 12/09/13 
 Pct Recovery = 24%  Analysis Date = 12/07/13 
 Pct Recovery = 24%  Analysis Date = 12/07/13 
 Pct Recovery = 24%  Analysis Date = 12/05/13 
 Pct Recovery = 25%  Analysis Date = 12/05/13 
 Pct Recovery = 25%  Analysis Date = 12/03/13 
 Pct Recovery = 26%  Analysis Date = 12/03/13 
 Pct Recovery = 26%  Analysis Date = 12/01/13 
 Pct Recovery = 26%  Analysis Date = 12/01/13 
 Pct Recovery = 26%  Analysis Date = 11/29/13 
 Pct Recovery = 27%  Analysis Date = 11/29/13 
 Pct Recovery = 27%  Analysis Date = 11/27/13 
 Pct Recovery = 28%  Analysis Date = 11/27/13 
 Pct Recovery = 28%  Analysis Date = 11/25/13 
 Pct Recovery = 28%  Analysis Date = 11/25/13 
 Pct Recovery = 28%  Analysis Date = 11/23/13 
 Pct Recovery = 29%  Analysis Date = 11/23/13 
 Pct Recovery = 29%  Analysis Date = 11/21/13 
 Pct Recovery = 29%  Analysis Date = 11/21/13 
 Pct Recovery = 29%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/14/13 
 Pct Recovery = 30%  Analysis Date = 11/14/13 
 Pct Recovery = 30%  Analysis Date = 11/12/13 
 Pct Recovery = 30%  Analysis Date = 11/12/13 
 Pct Recovery = 30%  Analysis Date = 11/10/13 
 Pct Recovery = 31%  Analysis Date = 11/10/13 
 Pct Recovery = 31%  Analysis Date = 11/08/13 
 Pct Recovery = 31%  Analysis Date = 11/08/13 
 Pct Recovery = 31%  Analysis Date = 11/06/13 
 Pct Recovery = 31%  Analysis Date = 11/06/13 
 Pct Recovery = 31%  Analysis Date = 11/04/13 
 Pct Recovery = 31%  Analysis Date = 11/04/13 
 Pct Recovery = 31%  Analysis Date = 11/02/13 
 Pct Recovery = 31%  Analysis Date = 11/02/13 
 Pct Recovery = 31%  Analysis Date = 10/30/13 
 Pct Recovery = 32%  Analysis Date = 10/30/13 
 Pct Recovery = 32%  Analysis Date = 10/28/13 
 Pct Recovery = 32%  Analysis Date = 10/28/13 
 Pct Recovery = 32%  Analysis Date = 10/26/13 
 Pct Recovery = 32%  Analysis Date = 10/26/13 
 Pct Recovery = 32%  Analysis Date = 10/24/13 
 Pct Recovery = 32%  Analysis Date = 10/24/13 
 Pct Recovery = 32%  Analysis Date = 10/22/13 
 Pct Recovery = 32%  Analysis Date = 10/22/13 
 Pct Recovery = 32%  Analysis Date = 10/20/13 
 Pct Recovery = 33%  Analysis Date = 10/20/13 
 Pct Recovery = 33%  Analysis Date = 10/18/13 
 Pct Recovery = 33%  Analysis Date = 10/18/13 
 Pct Recovery = 33%  Analysis Date = 10/16/13 
 Pct Recovery = 33%  Analysis Date = 10/16/13 
 Pct Recovery = 33%  Analysis Date = 10/14/13 
 Pct Recovery = 33%  Analysis Date = 10/14/13 
 Pct Recovery = 33%  Analysis Date = 10/12/13 
 Pct Recovery = 33%  Analysis Date = 10/12/13 
 Pct Recovery = 33%  Analysis Date = 10/09/13 
 Pct Recovery = 33%  Analysis Date = 10/09/13 
 Pct Recovery = 33%  Analysis Date = 10/07/13 
 Pct Recovery = 34%  Analysis Date = 10/07/13 
 Pct Recovery = 34%  Analysis Date = 10/05/13 
 Pct Recovery = 34%  Analysis Date = 10/05/13 
 Pct Recovery = 34%  Analysis Date = 10/03/13 
 Pct Recovery = 34%  Analysis Date = 10/03/13 
 Pct Recovery = 34%  Analysis Date = 10/01/13 
 Pct Recovery = 34%  Analysis Date = 10/01/13 
 Pct Recovery = 34%  Analysis Date = 09/29/13 
 Pct Recovery = 34%  Analysis Date = 09/29/13 
 Pct Recovery = 34%  Analysis Date = 09/27/13 
 Pct Recovery = 35%  Analysis Date = 09/27/13 
 Pct Recovery = 35%  Analysis Date = 09/25/13 
 Pct Recovery = 35%  Analysis Date = 09/25/13 
 Pct Recovery = 35%  Analysis Date = 09/23/13 
 Pct Recovery = 35%  Analysis Date = 09/23/13 
 Pct Recovery = 35%  Analysis Date = 09/20/13 
 Pct Recovery = 35%  Analysis Date = 09/20/13 
 Pct Recovery = 35%  Analysis Date = 09/18/13 
 Pct Recovery = 35%  Analysis Date = 09/18/13 
 Pct Recovery = 35%  Analysis Date = 09/16/13 
 Pct Recovery = 36%  Analysis Date = 09/16/13 
 Pct Recovery = 36%  Analysis Date = 09/14/13 
 Pct Recovery = 36%  Analysis Date = 09/14/13 
 Pct Recovery = 36%  Analysis Date = 09/12/13 
 Pct Recovery = 36%  Analysis Date = 09/12/13 
 Pct Recovery = 36%  Analysis Date = 09/10/13 
 Pct Recovery = 36%  Analysis Date = 09/10/13 
 Pct Recovery = 36%  Analysis Date = 09/08/13 
 Pct Recovery = 36%  Analysis Date = 09/08/13 
 Pct Recovery = 36%  Analysis Date = 09/06/13 
 Pct Recovery = 37%  Analysis Date = 09/06/13 
 Pct Recovery = 37%  Analysis Date = 09/04/13 
 Pct Recovery = 37%  Analysis Date = 09/04/13 
 Pct Recovery = 37%  Analysis Date = 09/02/13 
 Pct Recovery = 37%  Analysis Date = 09/02/13 
 Pct Recovery = 37%  Analysis Date = 08/30/13 
 Pct Recovery = 37%  Analysis Date = 08/30/13 
 Pct Recovery = 37%  Analysis Date = 08/28/13 
 Pct Recovery = 37%  Analysis Date = 08/28/13 
 Pct Recovery = 37%  Analysis Date = 08/26/13 
 Pct Recovery = 38%  Analysis Date = 08/26/13 
 Pct Recovery = 38%  Analysis Date = 08/24/13 
 Pct Recovery = 38%  Analysis Date = 08/24/13 
 Pct Recovery = 38%  Analysis Date = 08/22/13 
 Pct Recovery = 38%  Analysis Date = 08/22/13 
 Pct Recovery = 38%  Analysis Date = 08/20/13 
 Pct Recovery = 38%  Analysis Date = 08/20/13 
 Pct Recovery = 38%  Analysis Date = 08/18/13 
 Pct Recovery = 38%  Analysis Date = 08/18/13 
 Pct Recovery = 38%  Analysis Date = 08/16/13 
 Pct Recovery = 39%  Analysis Date = 08/16/13 
 Pct Recovery = 39%  Analysis Date = 08/14/13 
 Pct Recovery = 39%  Analysis Date = 08/14/13 
 Pct Recovery = 39%  Analysis Date = 08/11/13 
 Pct Recovery = 39%  Analysis Date = 08/11/13 
 Pct Recovery = 39%  Analysis Date = 08/09/13 
 Pct Recovery = 39%  Analysis Date = 08/09/13 
 Pct Recovery = 39%  Analysis Date = 08/07/13 
 Pct Recovery = 39%  Analysis Date = 08/07/13 
 Pct Recovery = 39%  Analysis Date = 08/05/13 
 Pct Recovery = 39%  Analysis Date = 08/05/13 
 Pct Recovery = 39%  Analysis Date = 08/03/13 
 Pct Recovery = 40%  Analysis Date = 08/03/13 
 Pct Recovery = 40%  Analysis Date = 08/01/13 
 Pct Recovery = 40%  Analysis Date = 08/01/13 
 Pct Recovery = 40%  Analysis Date = 07/30/13 
 Pct Recovery = 40%  Analysis Date = 07/30/13 
 Pct Recovery = 40%  Analysis Date = 07/28/13 
 Pct Recovery = 40%  Analysis Date = 07/28/13 
 Pct Recovery = 40%  Analysis Date = 07/26/13 
 Pct Recovery = 40%  Analysis Date = 07/26/13 
 Pct Recovery = 40%  Analysis Date = 07/24/13 
 Pct Recovery = 41%  Analysis Date = 07/24/13 
 Pct Recovery = 41%  Analysis Date = 07/21/13 
 Pct Recovery = 41%  Analysis Date = 07/21/13 
 Pct Recovery = 41%  Analysis Date = 07/19/13 
 Pct Recovery = 41%  Analysis Date = 07/19/13 
 Pct Recovery = 41%  Analysis Date = 07/17/13 
 Pct Recovery = 41%  Analysis Date = 07/17/13 
 Pct Recovery = 41%  Analysis Date = 07/15/13 
 Pct Recovery = 41%  Analysis Date = 07/15/13 
 Pct Recovery = 41%  Analysis Date = 07/13/13 
 Pct Recovery = 42%  Analysis Date = 07/13/13 
 Pct Recovery = 42%  Analysis Date = 07/11/13 
 Pct Recovery = 42%  Analysis Date = 07/11/13 
 Pct Recovery = 42%  Analysis Date = 07/09/13 
 Pct Recovery = 42%  Analysis Date = 07/09/13 
 Pct Recovery = 42%  Analysis Date = 07/07/13 
 Pct Recovery = 42%  Analysis Date = 07/07/13 
 Pct Recovery = 42%  Analysis Date = 07/05/13 
 Pct Recovery = 42%  Analysis Date = 07/05/13 
 Pct Recovery = 42%  Analysis Date = 07/02/13 
 Pct Recovery = 43%  Analysis Date = 07/02/13 
 Pct Recovery = 43%  Analysis Date = 06/30/13 
 Pct Recovery = 43%  Analysis Date = 06/30/13 
 Pct Recovery = 43%  Analysis Date = 06/28/13 
 Pct Recovery = 43%  Analysis Date = 06/28/13 
 Pct Recovery = 43%  Analysis Date = 06/26/13 
 Pct Recovery = 43%  Analysis Date = 06/26/13 
 Pct Recovery = 43%  Analysis Date = 06/24/13 
 Pct Recovery = 43%  Analysis Date = 06/24/13 
 Pct Recovery = 43%  Analysis Date = 06/22/13 
 Pct Recovery = 44%  Analysis Date = 06/22/13 
 Pct Recovery = 44%  Analysis Date = 06/20/13 
 Pct Recovery = 44%  Analysis Date = 06/20/13 
 Pct Recovery = 44%  Analysis Date = 06/18/13 
 Pct Recovery = 44%  Analysis Date = 06/18/13 
 Pct Recovery = 44%  Analysis Date = 06/16/13 
 Pct Recovery = 44%  Analysis Date = 06/16/13 
 Pct Recovery = 44%  Analysis Date = 06/14/13 
 Pct Recovery = 44%  Analysis Date = 06/14/13 
 Pct Recovery = 44%  Analysis Date = 06/11/13 
 Pct Recovery = 45%  Analysis Date = 06/11/13 
 Pct Recovery = 45%  Analysis Date = 06/09/13 
 Pct Recovery = 45%  Analysis Date = 06/09/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 45%  Analysis Date = 06/03/13 
 Pct Recovery = 45%  Analysis Date = 06/03/13 
 Pct Recovery = 45%  Analysis Date = 06/01/13 
 Pct Recovery = 45%  Analysis Date = 06/01/13 
 Pct Recovery = 45%  Analysis Date = 05/30/13 
 Pct Recovery = 46%  Analysis Date = 05/30/13 
 Pct Recovery = 46%  Analysis Date = 05/28/13 
 Pct Recovery = 46%  Analysis Date = 05/28/13 
 Pct Recovery = 46%  Analysis Date = 05/26/13 
 Pct Recovery = 46%  Analysis Date = 05/26/13 
 Pct Recovery = 46%  Analysis Date = 05/23/13 
 Pct Recovery = 46%  Analysis Date = 05/23/13 
 Pct Recovery = 46%  Analysis Date = 05/21/13 
 Pct Recovery = 46%  Analysis Date = 05/21/13 
 Pct Recovery = 46%  Analysis Date = 05/19/13 
 Pct Recovery = 47%  Analysis Date = 05/19/13 
 Pct Recovery = 47%  Analysis Date = 05/17/13 
 Pct Recovery = 47%  Analysis Date = 05/17/13 
 Pct Recovery = 47%  Analysis Date = 05/15/13 
 Pct Recovery = 47%  Analysis Date = 05/15/13 
 Pct Recovery = 47%  Analysis Date = 05/13/13 
 Pct Recovery = 47%  Analysis Date = 05/13/13 
 Pct Recovery = 47%  Analysis Date = 05/11/13 
 Pct Recovery = 47%  Analysis Date = 05/11/13 
 Pct Recovery = 47%  Analysis Date = 05/09/13 
 Pct Recovery = 48%  Analysis Date = 05/09/13 
 Pct Recovery = 48%  Analysis Date = 05/07/13 
 Pct Recovery = 48%  Analysis Date = 05/07/13 
 Pct Recovery = 48%  Analysis Date = 05/05/13 
 Pct Recovery = 48%  Analysis Date = 05/05/13 
 Pct Recovery = 48%  Analysis Date = 05/02/13 
 Pct Recovery = 48%  Analysis Date = 05/02/13 
 Pct Recovery = 48%  Analysis Date = 04/30/13 
 Pct Recovery = 48%  Analysis Date = 04/30/13 
 Pct Recovery = 48%  Analysis Date = 04/28/13 
 Pct Recovery = 48%  Analysis Date = 04/28/13 
 Pct Recovery = 48%  Analysis Date = 04/26/13 
 Pct Recovery = 48%  Analysis Date = 04/26/13 
 Pct Recovery = 48%  Analysis Date = 04/24/13 
 Pct Recovery = 48%  Analysis Date = 04/24/13 
 Pct Recovery = 48%  Analysis Date = 04/22/13 
 Pct Recovery = 47%  Analysis Date = 04/22/13 
 Pct Recovery = 47%  Analysis Date = 04/20/13 
 Pct Recovery = 47%  Analysis Date = 04/20/13 
 Pct Recovery = 47%  Analysis Date = 04/18/13 
 Pct Recovery = 47%  Analysis Date = 04/18/13 
 Pct Recovery = 47%  Analysis Date = 04/16/13 
 Pct Recovery = 47%  Analysis Date = 04/16/13 
 Pct Recovery = 47%  Analysis Date = 04/13/13 
 Pct Recovery = 46%  Analysis Date = 04/13/13 
 Pct Recovery = 46%  Analysis Date = 04/11/13 
 Pct Recovery = 46%  Analysis Date = 04/11/13 
 Pct Recovery = 46%  Analysis Date = 04/09/13 
 Pct Recovery = 46%  Analysis Date = 04/09/13 
 Pct Recovery = 46%  Analysis Date = 04/07/13 
 Pct Recovery = 46%  Analysis Date = 04/07/13 
 Pct Recovery = 46%  Analysis Date = 04/05/13 
 Pct Recovery = 46%  Analysis Date = 04/05/13 
 Pct Recovery = 46%  Analysis Date = 04/03/13 
 Pct Recovery = 45%  Analysis Date = 04/03/13 
 Pct Recovery = 45%  Analysis Date = 04/01/13 
 Pct Recovery = 45%  Analysis Date = 04/01/13 
 Pct Recovery = 45%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/28/13 
 Pct Recovery = 45%  Analysis Date = 03/28/13 
 Pct Recovery = 45%  Analysis Date = 03/26/13 
 Pct Recovery = 45%  Analysis Date = 03/26/13 
 Pct Recovery = 45%  Analysis Date = 03/23/13 
 Pct Recovery = 44%  Analysis Date = 03/23/13 
 Pct Recovery = 44%  Analysis Date = 03/21/13 
 Pct Recovery = 44%  Analysis Date = 03/21/13 
 Pct Recovery = 44%  Analysis Date = 03/19/13 
 Pct Recovery = 44%  Analysis Date = 03/19/13 
 Pct Recovery = 44%  Analysis Date = 03/17/13 
 Pct Recovery = 44%  Analysis Date = 03/17/13 
 Pct Recovery = 44%  Analysis Date = 03/15/13 
 Pct Recovery = 44%  Analysis Date = 03/15/13 
 Pct Recovery = 44%  Analysis Date = 03/13/13 
 Pct Recovery = 43%  Analysis Date = 03/13/13 
 Pct Recovery = 43%  Analysis Date = 03/11/13 
 Pct Recovery = 43%  Analysis Date = 03/11/13 
 Pct Recovery = 43%  Analysis Date = 03/09/13 
 Pct Recovery = 43%  Analysis Date = 03/09/13 
 Pct Recovery = 43%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/07/13 
 Pct Recovery = 43%  Analysis Date = 03/04/13 
 Pct Recovery = 42%  Analysis Date = 03/04/13 
 Pct Recovery = 42%  Analysis Date = 03/02/13 
 Pct Recovery = 42%  Analysis Date = 03/02/13 
 Pct Recovery = 42%  Analysis Date = 02/28/13 
 Pct Recovery = 42%  Analysis Date = 02/28/13 
 Pct Recovery = 42%  Analysis Date = 02/26/13 
 Pct Recovery = 42%  Analysis Date = 02/26/13 
 Pct Recovery = 42%  Analysis Date = 02/24/13 
 Pct Recovery = 42%  Analysis Date = 02/24/13 
 Pct Recovery = 42%  Analysis Date = 02/22/13 
 Pct Recovery = 41%  Analysis Date = 02/22/13 
 Pct Recovery = 41%  Analysis Date = 02/20/13 
 Pct Recovery = 41%  Analysis Date = 02/20/13 
 Pct Recovery = 41%  Analysis Date = 02/18/13 
 Pct Recovery = 41%  Analysis Date = 02/18/13 
 Pct Recovery = 41%  Analysis Date = 02/16/13 
 Pct Recovery = 41%  Analysis Date = 02/16/13 
 Pct Recovery = 41%  Analysis Date = 02/14/13 
 Pct Recovery = 41%  Analysis Date = 02/14/13 
 Pct Recovery = 41%  Analysis Date = 02/11/13 
 Pct Recovery = 40%  Analysis Date = 02/11/13 
 Pct Recovery = 40%  Analysis Date = 02/09/13 
 Pct Recovery = 40%  Analysis Date = 02/09/13 
 Pct Recovery = 40%  Analysis Date = 02/07/13 
 Pct Recovery = 40%  Analysis Date = 02/07/13 
 Pct Recovery = 40%  Analysis Date = 02/05/13 
 Pct Recovery = 40%  Analysis Date = 02/05/13 
 Pct Recovery = 40%  Analysis Date = 02/03/13 
 Pct Recovery = 39%  Analysis Date = 02/03/13 
 Pct Recovery = 39%  Analysis Date = 02/01/13 
 Pct Recovery = 39%  Analysis Date = 02/01/13 
 Pct Recovery = 39%  Analysis Date = 01/30/13 
 Pct Recovery = 39%  Analysis Date = 01/30/13 
 Pct Recovery = 39%  Analysis Date = 01/28/13 
 Pct Recovery = 39%  Analysis Date = 01/28/13 
 Pct Recovery = 39%  Analysis Date = 01/26/13 
 Pct Recovery = 39%  Analysis Date = 01/26/13 
 Pct Recovery = 39%  Analysis Date = 01/24/13 
 Pct Recovery = 38%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
LOPERAMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 34% 12% 36% 10%
Total 6 34% 12% 36% 10%

Sample Statistics
LOPERAMIDE

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 6 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
LORATADINE
METHOD: LC9017 , TESTIDCODE: 67488LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 38%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 57%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 51%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 37%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 21%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 59%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 47%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 42%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 59%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 48%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 30%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 42%  Analysis Date = 03/21/14 
 Pct Recovery = 31%  Analysis Date = 03/18/14 
 Pct Recovery = 32%  Analysis Date = 03/18/14 
 Pct Recovery = 32%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/14/14 
 Pct Recovery = 33%  Analysis Date = 03/14/14 
 Pct Recovery = 33%  Analysis Date = 03/11/14 
 Pct Recovery = 34%  Analysis Date = 03/11/14 
 Pct Recovery = 34%  Analysis Date = 03/09/14 
 Pct Recovery = 34%  Analysis Date = 03/09/14 
 Pct Recovery = 34%  Analysis Date = 03/07/14 
 Pct Recovery = 35%  Analysis Date = 03/07/14 
 Pct Recovery = 35%  Analysis Date = 03/04/14 
 Pct Recovery = 36%  Analysis Date = 03/04/14 
 Pct Recovery = 36%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 03/02/14 
 Pct Recovery = 36%  Analysis Date = 02/28/14 
 Pct Recovery = 37%  Analysis Date = 02/28/14 
 Pct Recovery = 37%  Analysis Date = 02/25/14 
 Pct Recovery = 37%  Analysis Date = 02/25/14 
 Pct Recovery = 37%  Analysis Date = 02/23/14 
 Pct Recovery = 38%  Analysis Date = 02/23/14 
 Pct Recovery = 38%  Analysis Date = 02/21/14 
 Pct Recovery = 39%  Analysis Date = 02/21/14 
 Pct Recovery = 39%  Analysis Date = 02/18/14 
 Pct Recovery = 39%  Analysis Date = 02/18/14 
 Pct Recovery = 39%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/14/14 
 Pct Recovery = 41%  Analysis Date = 02/14/14 
 Pct Recovery = 41%  Analysis Date = 02/12/14 
 Pct Recovery = 41%  Analysis Date = 02/12/14 
 Pct Recovery = 41%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/07/14 
 Pct Recovery = 42%  Analysis Date = 02/07/14 
 Pct Recovery = 42%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/05/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 01/31/14 
 Pct Recovery = 44%  Analysis Date = 01/31/14 
 Pct Recovery = 44%  Analysis Date = 01/29/14 
 Pct Recovery = 45%  Analysis Date = 01/29/14 
 Pct Recovery = 45%  Analysis Date = 01/26/14 
 Pct Recovery = 45%  Analysis Date = 01/26/14 
 Pct Recovery = 45%  Analysis Date = 01/24/14 
 Pct Recovery = 46%  Analysis Date = 01/24/14 
 Pct Recovery = 46%  Analysis Date = 01/22/14 
 Pct Recovery = 46%  Analysis Date = 01/22/14 
 Pct Recovery = 46%  Analysis Date = 01/19/14 
 Pct Recovery = 47%  Analysis Date = 01/19/14 
 Pct Recovery = 47%  Analysis Date = 01/17/14 
 Pct Recovery = 47%  Analysis Date = 01/17/14 
 Pct Recovery = 47%  Analysis Date = 01/15/14 
 Pct Recovery = 48%  Analysis Date = 01/15/14 
 Pct Recovery = 48%  Analysis Date = 01/13/14 
 Pct Recovery = 49%  Analysis Date = 01/13/14 
 Pct Recovery = 49%  Analysis Date = 01/10/14 
 Pct Recovery = 49%  Analysis Date = 01/10/14 
 Pct Recovery = 49%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/03/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 01/01/14 
 Pct Recovery = 51%  Analysis Date = 12/30/13 
 Pct Recovery = 52%  Analysis Date = 12/30/13 
 Pct Recovery = 52%  Analysis Date = 12/27/13 
 Pct Recovery = 53%  Analysis Date = 12/27/13 
 Pct Recovery = 53%  Analysis Date = 12/25/13 
 Pct Recovery = 53%  Analysis Date = 12/25/13 
 Pct Recovery = 53%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 55%  Analysis Date = 12/18/13 
 Pct Recovery = 55%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/16/13 
 Pct Recovery = 55%  Analysis Date = 12/13/13 
 Pct Recovery = 56%  Analysis Date = 12/13/13 
 Pct Recovery = 56%  Analysis Date = 12/11/13 
 Pct Recovery = 57%  Analysis Date = 12/11/13 
 Pct Recovery = 57%  Analysis Date = 12/09/13 
 Pct Recovery = 57%  Analysis Date = 12/09/13 
 Pct Recovery = 57%  Analysis Date = 12/07/13 
 Pct Recovery = 58%  Analysis Date = 12/07/13 
 Pct Recovery = 58%  Analysis Date = 12/04/13 
 Pct Recovery = 58%  Analysis Date = 12/04/13 
 Pct Recovery = 58%  Analysis Date = 12/02/13 
 Pct Recovery = 58%  Analysis Date = 12/02/13 
 Pct Recovery = 58%  Analysis Date = 11/30/13 
 Pct Recovery = 58%  Analysis Date = 11/30/13 
 Pct Recovery = 58%  Analysis Date = 11/27/13 
 Pct Recovery = 58%  Analysis Date = 11/27/13 
 Pct Recovery = 58%  Analysis Date = 11/25/13 
 Pct Recovery = 57%  Analysis Date = 11/25/13 
 Pct Recovery = 57%  Analysis Date = 11/23/13 
 Pct Recovery = 57%  Analysis Date = 11/23/13 
 Pct Recovery = 57%  Analysis Date = 11/20/13 
 Pct Recovery = 57%  Analysis Date = 11/20/13 
 Pct Recovery = 57%  Analysis Date = 11/18/13 
 Pct Recovery = 57%  Analysis Date = 11/18/13 
 Pct Recovery = 57%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/16/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/07/13 
 Pct Recovery = 55%  Analysis Date = 11/07/13 
 Pct Recovery = 55%  Analysis Date = 11/04/13 
 Pct Recovery = 55%  Analysis Date = 11/04/13 
 Pct Recovery = 55%  Analysis Date = 11/02/13 
 Pct Recovery = 55%  Analysis Date = 11/02/13 
 Pct Recovery = 55%  Analysis Date = 10/31/13 
 Pct Recovery = 55%  Analysis Date = 10/31/13 
 Pct Recovery = 55%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/28/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/26/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/24/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/21/13 
 Pct Recovery = 54%  Analysis Date = 10/19/13 
 Pct Recovery = 53%  Analysis Date = 10/19/13 
 Pct Recovery = 53%  Analysis Date = 10/17/13 
 Pct Recovery = 53%  Analysis Date = 10/17/13 
 Pct Recovery = 53%  Analysis Date = 10/14/13 
 Pct Recovery = 53%  Analysis Date = 10/14/13 
 Pct Recovery = 53%  Analysis Date = 10/12/13 
 Pct Recovery = 53%  Analysis Date = 10/12/13 
 Pct Recovery = 53%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 51%  Analysis Date = 09/28/13 
 Pct Recovery = 51%  Analysis Date = 09/26/13 
 Pct Recovery = 51%  Analysis Date = 09/26/13 
 Pct Recovery = 51%  Analysis Date = 09/24/13 
 Pct Recovery = 51%  Analysis Date = 09/24/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 50%  Analysis Date = 09/19/13 
 Pct Recovery = 50%  Analysis Date = 09/17/13 
 Pct Recovery = 50%  Analysis Date = 09/17/13 
 Pct Recovery = 50%  Analysis Date = 09/14/13 
 Pct Recovery = 50%  Analysis Date = 09/14/13 
 Pct Recovery = 50%  Analysis Date = 09/12/13 
 Pct Recovery = 50%  Analysis Date = 09/12/13 
 Pct Recovery = 50%  Analysis Date = 09/10/13 
 Pct Recovery = 49%  Analysis Date = 09/10/13 
 Pct Recovery = 49%  Analysis Date = 09/07/13 
 Pct Recovery = 49%  Analysis Date = 09/07/13 
 Pct Recovery = 49%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/03/13 
 Pct Recovery = 49%  Analysis Date = 09/03/13 
 Pct Recovery = 49%  Analysis Date = 09/01/13 
 Pct Recovery = 48%  Analysis Date = 09/01/13 
 Pct Recovery = 48%  Analysis Date = 08/29/13 
 Pct Recovery = 48%  Analysis Date = 08/29/13 
 Pct Recovery = 48%  Analysis Date = 08/27/13 
 Pct Recovery = 48%  Analysis Date = 08/27/13 
 Pct Recovery = 48%  Analysis Date = 08/25/13 
 Pct Recovery = 48%  Analysis Date = 08/25/13 
 Pct Recovery = 48%  Analysis Date = 08/22/13 
 Pct Recovery = 47%  Analysis Date = 08/22/13 
 Pct Recovery = 47%  Analysis Date = 08/20/13 
 Pct Recovery = 47%  Analysis Date = 08/20/13 
 Pct Recovery = 47%  Analysis Date = 08/18/13 
 Pct Recovery = 47%  Analysis Date = 08/18/13 
 Pct Recovery = 47%  Analysis Date = 08/15/13 
 Pct Recovery = 47%  Analysis Date = 08/15/13 
 Pct Recovery = 47%  Analysis Date = 08/13/13 
 Pct Recovery = 46%  Analysis Date = 08/13/13 
 Pct Recovery = 46%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/08/13 
 Pct Recovery = 46%  Analysis Date = 08/08/13 
 Pct Recovery = 46%  Analysis Date = 08/06/13 
 Pct Recovery = 46%  Analysis Date = 08/06/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 45%  Analysis Date = 08/02/13 
 Pct Recovery = 45%  Analysis Date = 07/30/13 
 Pct Recovery = 45%  Analysis Date = 07/30/13 
 Pct Recovery = 45%  Analysis Date = 07/28/13 
 Pct Recovery = 45%  Analysis Date = 07/28/13 
 Pct Recovery = 45%  Analysis Date = 07/26/13 
 Pct Recovery = 45%  Analysis Date = 07/26/13 
 Pct Recovery = 45%  Analysis Date = 07/23/13 
 Pct Recovery = 45%  Analysis Date = 07/23/13 
 Pct Recovery = 45%  Analysis Date = 07/21/13 
 Pct Recovery = 45%  Analysis Date = 07/21/13 
 Pct Recovery = 45%  Analysis Date = 07/19/13 
 Pct Recovery = 45%  Analysis Date = 07/19/13 
 Pct Recovery = 45%  Analysis Date = 07/16/13 
 Pct Recovery = 45%  Analysis Date = 07/16/13 
 Pct Recovery = 45%  Analysis Date = 07/14/13 
 Pct Recovery = 45%  Analysis Date = 07/14/13 
 Pct Recovery = 45%  Analysis Date = 07/12/13 
 Pct Recovery = 45%  Analysis Date = 07/12/13 
 Pct Recovery = 45%  Analysis Date = 07/09/13 
 Pct Recovery = 45%  Analysis Date = 07/09/13 
 Pct Recovery = 45%  Analysis Date = 07/07/13 
 Pct Recovery = 45%  Analysis Date = 07/07/13 
 Pct Recovery = 45%  Analysis Date = 07/05/13 
 Pct Recovery = 45%  Analysis Date = 07/05/13 
 Pct Recovery = 45%  Analysis Date = 07/02/13 
 Pct Recovery = 46%  Analysis Date = 07/02/13 
 Pct Recovery = 46%  Analysis Date = 06/30/13 
 Pct Recovery = 46%  Analysis Date = 06/30/13 
 Pct Recovery = 46%  Analysis Date = 06/28/13 
 Pct Recovery = 46%  Analysis Date = 06/28/13 
 Pct Recovery = 46%  Analysis Date = 06/26/13 
 Pct Recovery = 46%  Analysis Date = 06/26/13 
 Pct Recovery = 46%  Analysis Date = 06/23/13 
 Pct Recovery = 46%  Analysis Date = 06/23/13 
 Pct Recovery = 46%  Analysis Date = 06/21/13 
 Pct Recovery = 46%  Analysis Date = 06/21/13 
 Pct Recovery = 46%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/16/13 
 Pct Recovery = 46%  Analysis Date = 06/16/13 
 Pct Recovery = 46%  Analysis Date = 06/14/13 
 Pct Recovery = 46%  Analysis Date = 06/14/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/09/13 
 Pct Recovery = 46%  Analysis Date = 06/07/13 
 Pct Recovery = 46%  Analysis Date = 06/07/13 
 Pct Recovery = 46%  Analysis Date = 06/05/13 
 Pct Recovery = 46%  Analysis Date = 06/05/13 
 Pct Recovery = 46%  Analysis Date = 06/02/13 
 Pct Recovery = 46%  Analysis Date = 06/02/13 
 Pct Recovery = 46%  Analysis Date = 05/31/13 
 Pct Recovery = 46%  Analysis Date = 05/31/13 
 Pct Recovery = 46%  Analysis Date = 05/29/13 
 Pct Recovery = 46%  Analysis Date = 05/29/13 
 Pct Recovery = 46%  Analysis Date = 05/27/13 
 Pct Recovery = 46%  Analysis Date = 05/27/13 
 Pct Recovery = 46%  Analysis Date = 05/24/13 
 Pct Recovery = 46%  Analysis Date = 05/24/13 
 Pct Recovery = 46%  Analysis Date = 05/22/13 
 Pct Recovery = 46%  Analysis Date = 05/22/13 
 Pct Recovery = 46%  Analysis Date = 05/20/13 
 Pct Recovery = 46%  Analysis Date = 05/20/13 
 Pct Recovery = 46%  Analysis Date = 05/17/13 
 Pct Recovery = 46%  Analysis Date = 05/17/13 
 Pct Recovery = 46%  Analysis Date = 05/15/13 
 Pct Recovery = 46%  Analysis Date = 05/15/13 
 Pct Recovery = 46%  Analysis Date = 05/13/13 
 Pct Recovery = 46%  Analysis Date = 05/13/13 
 Pct Recovery = 46%  Analysis Date = 05/10/13 
 Pct Recovery = 46%  Analysis Date = 05/10/13 
 Pct Recovery = 46%  Analysis Date = 05/08/13 
 Pct Recovery = 46%  Analysis Date = 05/08/13 
 Pct Recovery = 46%  Analysis Date = 05/06/13 
 Pct Recovery = 46%  Analysis Date = 05/06/13 
 Pct Recovery = 46%  Analysis Date = 05/03/13 
 Pct Recovery = 46%  Analysis Date = 05/03/13 
 Pct Recovery = 46%  Analysis Date = 05/01/13 
 Pct Recovery = 46%  Analysis Date = 05/01/13 
 Pct Recovery = 46%  Analysis Date = 04/29/13 
 Pct Recovery = 46%  Analysis Date = 04/29/13 
 Pct Recovery = 46%  Analysis Date = 04/26/13 
 Pct Recovery = 47%  Analysis Date = 04/26/13 
 Pct Recovery = 47%  Analysis Date = 04/24/13 
 Pct Recovery = 47%  Analysis Date = 04/24/13 
 Pct Recovery = 47%  Analysis Date = 04/22/13 
 Pct Recovery = 47%  Analysis Date = 04/22/13 
 Pct Recovery = 47%  Analysis Date = 04/20/13 
 Pct Recovery = 48%  Analysis Date = 04/20/13 
 Pct Recovery = 48%  Analysis Date = 04/17/13 
 Pct Recovery = 48%  Analysis Date = 04/17/13 
 Pct Recovery = 48%  Analysis Date = 04/15/13 
 Pct Recovery = 48%  Analysis Date = 04/15/13 
 Pct Recovery = 48%  Analysis Date = 04/13/13 
 Pct Recovery = 49%  Analysis Date = 04/13/13 
 Pct Recovery = 49%  Analysis Date = 04/10/13 
 Pct Recovery = 49%  Analysis Date = 04/10/13 
 Pct Recovery = 49%  Analysis Date = 04/08/13 
 Pct Recovery = 49%  Analysis Date = 04/08/13 
 Pct Recovery = 49%  Analysis Date = 04/06/13 
 Pct Recovery = 50%  Analysis Date = 04/06/13 
 Pct Recovery = 50%  Analysis Date = 04/03/13 
 Pct Recovery = 50%  Analysis Date = 04/03/13 
 Pct Recovery = 50%  Analysis Date = 04/01/13 
 Pct Recovery = 50%  Analysis Date = 04/01/13 
 Pct Recovery = 50%  Analysis Date = 03/30/13 
 Pct Recovery = 51%  Analysis Date = 03/30/13 
 Pct Recovery = 51%  Analysis Date = 03/27/13 
 Pct Recovery = 51%  Analysis Date = 03/27/13 
 Pct Recovery = 51%  Analysis Date = 03/25/13 
 Pct Recovery = 51%  Analysis Date = 03/25/13 
 Pct Recovery = 51%  Analysis Date = 03/23/13 
 Pct Recovery = 51%  Analysis Date = 03/23/13 
 Pct Recovery = 51%  Analysis Date = 03/21/13 
 Pct Recovery = 52%  Analysis Date = 03/21/13 
 Pct Recovery = 52%  Analysis Date = 03/18/13 
 Pct Recovery = 52%  Analysis Date = 03/18/13 
 Pct Recovery = 52%  Analysis Date = 03/16/13 
 Pct Recovery = 52%  Analysis Date = 03/16/13 
 Pct Recovery = 52%  Analysis Date = 03/14/13 
 Pct Recovery = 52%  Analysis Date = 03/14/13 
 Pct Recovery = 52%  Analysis Date = 03/11/13 
 Pct Recovery = 52%  Analysis Date = 03/11/13 
 Pct Recovery = 52%  Analysis Date = 03/09/13 
 Pct Recovery = 52%  Analysis Date = 03/09/13 
 Pct Recovery = 52%  Analysis Date = 03/07/13 
 Pct Recovery = 53%  Analysis Date = 03/07/13 
 Pct Recovery = 53%  Analysis Date = 03/04/13 
 Pct Recovery = 53%  Analysis Date = 03/04/13 
 Pct Recovery = 53%  Analysis Date = 03/02/13 
 Pct Recovery = 53%  Analysis Date = 03/02/13 
 Pct Recovery = 53%  Analysis Date = 02/28/13 
 Pct Recovery = 53%  Analysis Date = 02/28/13 
 Pct Recovery = 53%  Analysis Date = 02/25/13 
 Pct Recovery = 53%  Analysis Date = 02/25/13 
 Pct Recovery = 53%  Analysis Date = 02/23/13 
 Pct Recovery = 53%  Analysis Date = 02/23/13 
 Pct Recovery = 53%  Analysis Date = 02/21/13 
 Pct Recovery = 53%  Analysis Date = 02/21/13 
 Pct Recovery = 53%  Analysis Date = 02/18/13 
 Pct Recovery = 54%  Analysis Date = 02/18/13 
 Pct Recovery = 54%  Analysis Date = 02/16/13 
 Pct Recovery = 54%  Analysis Date = 02/16/13 
 Pct Recovery = 54%  Analysis Date = 02/14/13 
 Pct Recovery = 54%  Analysis Date = 02/14/13 
 Pct Recovery = 54%  Analysis Date = 02/12/13 
 Pct Recovery = 54%  Analysis Date = 02/12/13 
 Pct Recovery = 54%  Analysis Date = 02/09/13 
 Pct Recovery = 54%  Analysis Date = 02/09/13 
 Pct Recovery = 54%  Analysis Date = 02/07/13 
 Pct Recovery = 54%  Analysis Date = 02/07/13 
 Pct Recovery = 54%  Analysis Date = 02/05/13 
 Pct Recovery = 55%  Analysis Date = 02/05/13 
 Pct Recovery = 55%  Analysis Date = 02/02/13 
 Pct Recovery = 55%  Analysis Date = 02/02/13 
 Pct Recovery = 55%  Analysis Date = 01/31/13 
 Pct Recovery = 55%  Analysis Date = 01/31/13 
 Pct Recovery = 55%  Analysis Date = 01/29/13 
 Pct Recovery = 55%  Analysis Date = 01/29/13 
 Pct Recovery = 55%  Analysis Date = 01/26/13 
 Pct Recovery = 55%  Analysis Date = 01/26/13 
 Pct Recovery = 55%  Analysis Date = 01/24/13 
 Pct Recovery = 55%  Analysis Date = 01/24/13 
 Pct Recovery = 55%  Analysis Date = 01/22/13 
 Pct Recovery = 56%  Analysis Date = 01/22/13 
 Pct Recovery = 56%  Analysis Date = 01/19/13 
 Pct Recovery = 56%  Analysis Date = 01/19/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/17/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/15/13 
 Pct Recovery = 56%  Analysis Date = 01/13/13 
 Pct Recovery = 56%  Analysis Date = 01/13/13 
 Pct Recovery = 56%  Analysis Date = 01/10/13 
 Pct Recovery = 56%  Analysis Date = 01/10/13 
 Pct Recovery = 56%  Analysis Date = 01/08/13 
 Pct Recovery = 57%  Analysis Date = 01/08/13 
 Pct Recovery = 57%  Analysis Date = 01/06/13 
 Pct Recovery = 57%  Analysis Date = 01/06/13 
 Pct Recovery = 57%  Analysis Date = 01/03/13 
 Pct Recovery = 57%  Analysis Date = 01/03/13 
 Pct Recovery = 57%  Analysis Date = 01/01/13 
 Pct Recovery = 57%  Analysis Date = 01/01/13 
 Pct Recovery = 57%  Analysis Date = 12/30/12 
 Pct Recovery = 57%  Analysis Date = 12/30/12 
 Pct Recovery = 57%  Analysis Date = 12/27/12 
 Pct Recovery = 57%  Analysis Date = 12/27/12 
 Pct Recovery = 57%  Analysis Date = 12/25/12 
 Pct Recovery = 57%  Analysis Date = 12/25/12 
 Pct Recovery = 57%  Analysis Date = 12/23/12 
 Pct Recovery = 58%  Analysis Date = 12/23/12 
 Pct Recovery = 58%  Analysis Date = 12/20/12 
 Pct Recovery = 58%  Analysis Date = 12/20/12 
 Pct Recovery = 58%  Analysis Date = 12/18/12 
 Pct Recovery = 58%  Analysis Date = 12/18/12 
 Pct Recovery = 58%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/16/12 
 Pct Recovery = 58%  Analysis Date = 12/14/12 
 Pct Recovery = 58%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
LORATADINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 46% 12% 47% 14%
Total 13 46% 12% 47% 14%

Sample Statistics
LORATADINE

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
LORAZEPAM
METHOD: LC9017 , TESTIDCODE: 67470LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 94%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 89%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 101%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 95%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 118%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 82%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 91%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 77%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 92%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 85%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 50%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 72%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 97%  Analysis Date = 03/21/14 
 Pct Recovery = 84%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/14/14 
 Pct Recovery = 86%  Analysis Date = 03/14/14 
 Pct Recovery = 86%  Analysis Date = 03/11/14 
 Pct Recovery = 87%  Analysis Date = 03/11/14 
 Pct Recovery = 87%  Analysis Date = 03/09/14 
 Pct Recovery = 87%  Analysis Date = 03/09/14 
 Pct Recovery = 87%  Analysis Date = 03/07/14 
 Pct Recovery = 88%  Analysis Date = 03/07/14 
 Pct Recovery = 88%  Analysis Date = 03/04/14 
 Pct Recovery = 88%  Analysis Date = 03/04/14 
 Pct Recovery = 88%  Analysis Date = 03/02/14 
 Pct Recovery = 89%  Analysis Date = 03/02/14 
 Pct Recovery = 89%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/28/14 
 Pct Recovery = 89%  Analysis Date = 02/25/14 
 Pct Recovery = 90%  Analysis Date = 02/25/14 
 Pct Recovery = 90%  Analysis Date = 02/23/14 
 Pct Recovery = 91%  Analysis Date = 02/23/14 
 Pct Recovery = 91%  Analysis Date = 02/21/14 
 Pct Recovery = 91%  Analysis Date = 02/21/14 
 Pct Recovery = 91%  Analysis Date = 02/18/14 
 Pct Recovery = 92%  Analysis Date = 02/18/14 
 Pct Recovery = 92%  Analysis Date = 02/16/14 
 Pct Recovery = 92%  Analysis Date = 02/16/14 
 Pct Recovery = 92%  Analysis Date = 02/14/14 
 Pct Recovery = 92%  Analysis Date = 02/14/14 
 Pct Recovery = 92%  Analysis Date = 02/12/14 
 Pct Recovery = 93%  Analysis Date = 02/12/14 
 Pct Recovery = 93%  Analysis Date = 02/09/14 
 Pct Recovery = 93%  Analysis Date = 02/09/14 
 Pct Recovery = 93%  Analysis Date = 02/07/14 
 Pct Recovery = 94%  Analysis Date = 02/07/14 
 Pct Recovery = 94%  Analysis Date = 02/05/14 
 Pct Recovery = 94%  Analysis Date = 02/05/14 
 Pct Recovery = 94%  Analysis Date = 02/02/14 
 Pct Recovery = 94%  Analysis Date = 02/02/14 
 Pct Recovery = 94%  Analysis Date = 01/31/14 
 Pct Recovery = 95%  Analysis Date = 01/31/14 
 Pct Recovery = 95%  Analysis Date = 01/29/14 
 Pct Recovery = 95%  Analysis Date = 01/29/14 
 Pct Recovery = 95%  Analysis Date = 01/26/14 
 Pct Recovery = 95%  Analysis Date = 01/26/14 
 Pct Recovery = 95%  Analysis Date = 01/24/14 
 Pct Recovery = 96%  Analysis Date = 01/24/14 
 Pct Recovery = 96%  Analysis Date = 01/22/14 
 Pct Recovery = 96%  Analysis Date = 01/22/14 
 Pct Recovery = 96%  Analysis Date = 01/19/14 
 Pct Recovery = 96%  Analysis Date = 01/19/14 
 Pct Recovery = 96%  Analysis Date = 01/17/14 
 Pct Recovery = 97%  Analysis Date = 01/17/14 
 Pct Recovery = 97%  Analysis Date = 01/15/14 
 Pct Recovery = 97%  Analysis Date = 01/15/14 
 Pct Recovery = 97%  Analysis Date = 01/13/14 
 Pct Recovery = 98%  Analysis Date = 01/13/14 
 Pct Recovery = 98%  Analysis Date = 01/10/14 
 Pct Recovery = 98%  Analysis Date = 01/10/14 
 Pct Recovery = 98%  Analysis Date = 01/08/14 
 Pct Recovery = 98%  Analysis Date = 01/08/14 
 Pct Recovery = 98%  Analysis Date = 01/06/14 
 Pct Recovery = 99%  Analysis Date = 01/06/14 
 Pct Recovery = 99%  Analysis Date = 01/03/14 
 Pct Recovery = 99%  Analysis Date = 01/03/14 
 Pct Recovery = 99%  Analysis Date = 01/01/14 
 Pct Recovery = 99%  Analysis Date = 01/01/14 
 Pct Recovery = 99%  Analysis Date = 12/30/13 
 Pct Recovery = 100%  Analysis Date = 12/30/13 
 Pct Recovery = 100%  Analysis Date = 12/27/13 
 Pct Recovery = 100%  Analysis Date = 12/27/13 
 Pct Recovery = 100%  Analysis Date = 12/25/13 
 Pct Recovery = 100%  Analysis Date = 12/25/13 
 Pct Recovery = 100%  Analysis Date = 12/23/13 
 Pct Recovery = 101%  Analysis Date = 12/23/13 
 Pct Recovery = 101%  Analysis Date = 12/20/13 
 Pct Recovery = 101%  Analysis Date = 12/20/13 
 Pct Recovery = 101%  Analysis Date = 12/18/13 
 Pct Recovery = 101%  Analysis Date = 12/18/13 
 Pct Recovery = 101%  Analysis Date = 12/16/13 
 Pct Recovery = 102%  Analysis Date = 12/16/13 
 Pct Recovery = 102%  Analysis Date = 12/13/13 
 Pct Recovery = 102%  Analysis Date = 12/13/13 
 Pct Recovery = 102%  Analysis Date = 12/11/13 
 Pct Recovery = 103%  Analysis Date = 12/11/13 
 Pct Recovery = 103%  Analysis Date = 12/09/13 
 Pct Recovery = 103%  Analysis Date = 12/09/13 
 Pct Recovery = 103%  Analysis Date = 12/07/13 
 Pct Recovery = 103%  Analysis Date = 12/07/13 
 Pct Recovery = 103%  Analysis Date = 12/04/13 
 Pct Recovery = 104%  Analysis Date = 12/04/13 
 Pct Recovery = 104%  Analysis Date = 12/02/13 
 Pct Recovery = 103%  Analysis Date = 12/02/13 
 Pct Recovery = 103%  Analysis Date = 11/30/13 
 Pct Recovery = 102%  Analysis Date = 11/30/13 
 Pct Recovery = 102%  Analysis Date = 11/27/13 
 Pct Recovery = 102%  Analysis Date = 11/27/13 
 Pct Recovery = 102%  Analysis Date = 11/25/13 
 Pct Recovery = 101%  Analysis Date = 11/25/13 
 Pct Recovery = 101%  Analysis Date = 11/23/13 
 Pct Recovery = 100%  Analysis Date = 11/23/13 
 Pct Recovery = 100%  Analysis Date = 11/20/13 
 Pct Recovery = 100%  Analysis Date = 11/20/13 
 Pct Recovery = 100%  Analysis Date = 11/18/13 
 Pct Recovery = 99%  Analysis Date = 11/18/13 
 Pct Recovery = 99%  Analysis Date = 11/16/13 
 Pct Recovery = 99%  Analysis Date = 11/16/13 
 Pct Recovery = 99%  Analysis Date = 11/13/13 
 Pct Recovery = 98%  Analysis Date = 11/13/13 
 Pct Recovery = 98%  Analysis Date = 11/11/13 
 Pct Recovery = 97%  Analysis Date = 11/11/13 
 Pct Recovery = 97%  Analysis Date = 11/09/13 
 Pct Recovery = 97%  Analysis Date = 11/09/13 
 Pct Recovery = 97%  Analysis Date = 11/07/13 
 Pct Recovery = 96%  Analysis Date = 11/07/13 
 Pct Recovery = 96%  Analysis Date = 11/04/13 
 Pct Recovery = 96%  Analysis Date = 11/04/13 
 Pct Recovery = 96%  Analysis Date = 11/02/13 
 Pct Recovery = 95%  Analysis Date = 11/02/13 
 Pct Recovery = 95%  Analysis Date = 10/31/13 
 Pct Recovery = 94%  Analysis Date = 10/31/13 
 Pct Recovery = 94%  Analysis Date = 10/28/13 
 Pct Recovery = 94%  Analysis Date = 10/28/13 
 Pct Recovery = 94%  Analysis Date = 10/26/13 
 Pct Recovery = 93%  Analysis Date = 10/26/13 
 Pct Recovery = 93%  Analysis Date = 10/24/13 
 Pct Recovery = 92%  Analysis Date = 10/24/13 
 Pct Recovery = 92%  Analysis Date = 10/21/13 
 Pct Recovery = 92%  Analysis Date = 10/21/13 
 Pct Recovery = 92%  Analysis Date = 10/19/13 
 Pct Recovery = 91%  Analysis Date = 10/19/13 
 Pct Recovery = 91%  Analysis Date = 10/17/13 
 Pct Recovery = 91%  Analysis Date = 10/17/13 
 Pct Recovery = 91%  Analysis Date = 10/14/13 
 Pct Recovery = 90%  Analysis Date = 10/14/13 
 Pct Recovery = 90%  Analysis Date = 10/12/13 
 Pct Recovery = 89%  Analysis Date = 10/12/13 
 Pct Recovery = 89%  Analysis Date = 10/10/13 
 Pct Recovery = 89%  Analysis Date = 10/10/13 
 Pct Recovery = 89%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/05/13 
 Pct Recovery = 87%  Analysis Date = 10/05/13 
 Pct Recovery = 87%  Analysis Date = 10/03/13 
 Pct Recovery = 87%  Analysis Date = 10/03/13 
 Pct Recovery = 87%  Analysis Date = 10/01/13 
 Pct Recovery = 86%  Analysis Date = 10/01/13 
 Pct Recovery = 86%  Analysis Date = 09/28/13 
 Pct Recovery = 86%  Analysis Date = 09/28/13 
 Pct Recovery = 86%  Analysis Date = 09/26/13 
 Pct Recovery = 85%  Analysis Date = 09/26/13 
 Pct Recovery = 85%  Analysis Date = 09/24/13 
 Pct Recovery = 84%  Analysis Date = 09/24/13 
 Pct Recovery = 84%  Analysis Date = 09/21/13 
 Pct Recovery = 84%  Analysis Date = 09/21/13 
 Pct Recovery = 84%  Analysis Date = 09/19/13 
 Pct Recovery = 83%  Analysis Date = 09/19/13 
 Pct Recovery = 83%  Analysis Date = 09/17/13 
 Pct Recovery = 83%  Analysis Date = 09/17/13 
 Pct Recovery = 83%  Analysis Date = 09/14/13 
 Pct Recovery = 82%  Analysis Date = 09/14/13 
 Pct Recovery = 82%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/10/13 
 Pct Recovery = 81%  Analysis Date = 09/10/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/03/13 
 Pct Recovery = 79%  Analysis Date = 09/03/13 
 Pct Recovery = 79%  Analysis Date = 09/01/13 
 Pct Recovery = 78%  Analysis Date = 09/01/13 
 Pct Recovery = 78%  Analysis Date = 08/29/13 
 Pct Recovery = 78%  Analysis Date = 08/29/13 
 Pct Recovery = 78%  Analysis Date = 08/27/13 
 Pct Recovery = 77%  Analysis Date = 08/27/13 
 Pct Recovery = 77%  Analysis Date = 08/25/13 
 Pct Recovery = 76%  Analysis Date = 08/25/13 
 Pct Recovery = 76%  Analysis Date = 08/22/13 
 Pct Recovery = 75%  Analysis Date = 08/22/13 
 Pct Recovery = 75%  Analysis Date = 08/20/13 
 Pct Recovery = 74%  Analysis Date = 08/20/13 
 Pct Recovery = 74%  Analysis Date = 08/18/13 
 Pct Recovery = 74%  Analysis Date = 08/18/13 
 Pct Recovery = 74%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/15/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/13/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/08/13 
 Pct Recovery = 72%  Analysis Date = 08/08/13 
 Pct Recovery = 72%  Analysis Date = 08/06/13 
 Pct Recovery = 72%  Analysis Date = 08/06/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/28/13 
 Pct Recovery = 72%  Analysis Date = 07/28/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/12/13 
 Pct Recovery = 75%  Analysis Date = 07/12/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 76%  Analysis Date = 07/07/13 
 Pct Recovery = 76%  Analysis Date = 07/05/13 
 Pct Recovery = 76%  Analysis Date = 07/05/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 77%  Analysis Date = 07/02/13 
 Pct Recovery = 77%  Analysis Date = 06/30/13 
 Pct Recovery = 77%  Analysis Date = 06/30/13 
 Pct Recovery = 77%  Analysis Date = 06/28/13 
 Pct Recovery = 78%  Analysis Date = 06/28/13 
 Pct Recovery = 78%  Analysis Date = 06/26/13 
 Pct Recovery = 78%  Analysis Date = 06/26/13 
 Pct Recovery = 78%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/21/13 
 Pct Recovery = 79%  Analysis Date = 06/21/13 
 Pct Recovery = 79%  Analysis Date = 06/19/13 
 Pct Recovery = 79%  Analysis Date = 06/19/13 
 Pct Recovery = 79%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/16/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/14/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 81%  Analysis Date = 06/12/13 
 Pct Recovery = 81%  Analysis Date = 06/09/13 
 Pct Recovery = 81%  Analysis Date = 06/09/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/02/13 
 Pct Recovery = 82%  Analysis Date = 06/02/13 
 Pct Recovery = 82%  Analysis Date = 05/31/13 
 Pct Recovery = 83%  Analysis Date = 05/31/13 
 Pct Recovery = 83%  Analysis Date = 05/29/13 
 Pct Recovery = 83%  Analysis Date = 05/29/13 
 Pct Recovery = 83%  Analysis Date = 05/27/13 
 Pct Recovery = 83%  Analysis Date = 05/27/13 
 Pct Recovery = 83%  Analysis Date = 05/24/13 
 Pct Recovery = 84%  Analysis Date = 05/24/13 
 Pct Recovery = 84%  Analysis Date = 05/22/13 
 Pct Recovery = 84%  Analysis Date = 05/22/13 
 Pct Recovery = 84%  Analysis Date = 05/20/13 
 Pct Recovery = 85%  Analysis Date = 05/20/13 
 Pct Recovery = 85%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/17/13 
 Pct Recovery = 85%  Analysis Date = 05/15/13 
 Pct Recovery = 86%  Analysis Date = 05/15/13 
 Pct Recovery = 86%  Analysis Date = 05/13/13 
 Pct Recovery = 86%  Analysis Date = 05/13/13 
 Pct Recovery = 86%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/10/13 
 Pct Recovery = 86%  Analysis Date = 05/08/13 
 Pct Recovery = 87%  Analysis Date = 05/08/13 
 Pct Recovery = 87%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/06/13 
 Pct Recovery = 87%  Analysis Date = 05/03/13 
 Pct Recovery = 88%  Analysis Date = 05/03/13 
 Pct Recovery = 88%  Analysis Date = 05/01/13 
 Pct Recovery = 88%  Analysis Date = 05/01/13 
 Pct Recovery = 88%  Analysis Date = 04/29/13 
 Pct Recovery = 88%  Analysis Date = 04/29/13 
 Pct Recovery = 88%  Analysis Date = 04/26/13 
 Pct Recovery = 88%  Analysis Date = 04/26/13 
 Pct Recovery = 88%  Analysis Date = 04/24/13 
 Pct Recovery = 89%  Analysis Date = 04/24/13 
 Pct Recovery = 89%  Analysis Date = 04/22/13 
 Pct Recovery = 89%  Analysis Date = 04/22/13 
 Pct Recovery = 89%  Analysis Date = 04/20/13 
 Pct Recovery = 89%  Analysis Date = 04/20/13 
 Pct Recovery = 89%  Analysis Date = 04/17/13 
 Pct Recovery = 89%  Analysis Date = 04/17/13 
 Pct Recovery = 89%  Analysis Date = 04/15/13 
 Pct Recovery = 90%  Analysis Date = 04/15/13 
 Pct Recovery = 90%  Analysis Date = 04/13/13 
 Pct Recovery = 90%  Analysis Date = 04/13/13 
 Pct Recovery = 90%  Analysis Date = 04/10/13 
 Pct Recovery = 90%  Analysis Date = 04/10/13 
 Pct Recovery = 90%  Analysis Date = 04/08/13 
 Pct Recovery = 90%  Analysis Date = 04/08/13 
 Pct Recovery = 90%  Analysis Date = 04/06/13 
 Pct Recovery = 90%  Analysis Date = 04/06/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 91%  Analysis Date = 04/03/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/25/13 
 Pct Recovery = 92%  Analysis Date = 03/25/13 
 Pct Recovery = 92%  Analysis Date = 03/23/13 
 Pct Recovery = 92%  Analysis Date = 03/23/13 
 Pct Recovery = 92%  Analysis Date = 03/21/13 
 Pct Recovery = 92%  Analysis Date = 03/21/13 
 Pct Recovery = 92%  Analysis Date = 03/18/13 
 Pct Recovery = 92%  Analysis Date = 03/18/13 
 Pct Recovery = 92%  Analysis Date = 03/16/13 
 Pct Recovery = 92%  Analysis Date = 03/16/13 
 Pct Recovery = 92%  Analysis Date = 03/14/13 
 Pct Recovery = 93%  Analysis Date = 03/14/13 
 Pct Recovery = 93%  Analysis Date = 03/11/13 
 Pct Recovery = 93%  Analysis Date = 03/11/13 
 Pct Recovery = 93%  Analysis Date = 03/09/13 
 Pct Recovery = 93%  Analysis Date = 03/09/13 
 Pct Recovery = 93%  Analysis Date = 03/07/13 
 Pct Recovery = 93%  Analysis Date = 03/07/13 
 Pct Recovery = 93%  Analysis Date = 03/04/13 
 Pct Recovery = 93%  Analysis Date = 03/04/13 
 Pct Recovery = 93%  Analysis Date = 03/02/13 
 Pct Recovery = 94%  Analysis Date = 03/02/13 
 Pct Recovery = 94%  Analysis Date = 02/28/13 
 Pct Recovery = 94%  Analysis Date = 02/28/13 
 Pct Recovery = 94%  Analysis Date = 02/25/13 
 Pct Recovery = 94%  Analysis Date = 02/25/13 
 Pct Recovery = 94%  Analysis Date = 02/23/13 
 Pct Recovery = 94%  Analysis Date = 02/23/13 
 Pct Recovery = 94%  Analysis Date = 02/21/13 
 Pct Recovery = 94%  Analysis Date = 02/21/13 
 Pct Recovery = 94%  Analysis Date = 02/18/13 
 Pct Recovery = 95%  Analysis Date = 02/18/13 
 Pct Recovery = 95%  Analysis Date = 02/16/13 
 Pct Recovery = 95%  Analysis Date = 02/16/13 
 Pct Recovery = 95%  Analysis Date = 02/14/13 
 Pct Recovery = 95%  Analysis Date = 02/14/13 
 Pct Recovery = 95%  Analysis Date = 02/12/13 
 Pct Recovery = 95%  Analysis Date = 02/12/13 
 Pct Recovery = 95%  Analysis Date = 02/09/13 
 Pct Recovery = 95%  Analysis Date = 02/09/13 
 Pct Recovery = 95%  Analysis Date = 02/07/13 
 Pct Recovery = 96%  Analysis Date = 02/07/13 
 Pct Recovery = 96%  Analysis Date = 02/05/13 
 Pct Recovery = 96%  Analysis Date = 02/05/13 
 Pct Recovery = 96%  Analysis Date = 02/02/13 
 Pct Recovery = 96%  Analysis Date = 02/02/13 
 Pct Recovery = 96%  Analysis Date = 01/31/13 
 Pct Recovery = 96%  Analysis Date = 01/31/13 
 Pct Recovery = 96%  Analysis Date = 01/29/13 
 Pct Recovery = 96%  Analysis Date = 01/29/13 
 Pct Recovery = 96%  Analysis Date = 01/26/13 
 Pct Recovery = 97%  Analysis Date = 01/26/13 
 Pct Recovery = 97%  Analysis Date = 01/24/13 
 Pct Recovery = 97%  Analysis Date = 01/24/13 
 Pct Recovery = 97%  Analysis Date = 01/22/13 
 Pct Recovery = 97%  Analysis Date = 01/22/13 
 Pct Recovery = 97%  Analysis Date = 01/19/13 
 Pct Recovery = 97%  Analysis Date = 01/19/13 
 Pct Recovery = 97%  Analysis Date = 01/17/13 
 Pct Recovery = 97%  Analysis Date = 01/17/13 
 Pct Recovery = 97%  Analysis Date = 01/15/13 
 Pct Recovery = 98%  Analysis Date = 01/15/13 
 Pct Recovery = 98%  Analysis Date = 01/13/13 
 Pct Recovery = 98%  Analysis Date = 01/13/13 
 Pct Recovery = 98%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/10/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/08/13 
 Pct Recovery = 98%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/06/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/03/13 
 Pct Recovery = 99%  Analysis Date = 01/01/13 
 Pct Recovery = 99%  Analysis Date = 01/01/13 
 Pct Recovery = 99%  Analysis Date = 12/30/12 
 Pct Recovery = 99%  Analysis Date = 12/30/12 
 Pct Recovery = 99%  Analysis Date = 12/27/12 
 Pct Recovery = 99%  Analysis Date = 12/27/12 
 Pct Recovery = 99%  Analysis Date = 12/25/12 
 Pct Recovery = 100%  Analysis Date = 12/25/12 
 Pct Recovery = 100%  Analysis Date = 12/23/12 
 Pct Recovery = 100%  Analysis Date = 12/23/12 
 Pct Recovery = 100%  Analysis Date = 12/20/12 
 Pct Recovery = 100%  Analysis Date = 12/20/12 
 Pct Recovery = 100%  Analysis Date = 12/18/12 
 Pct Recovery = 100%  Analysis Date = 12/18/12 
 Pct Recovery = 100%  Analysis Date = 12/16/12 
 Pct Recovery = 100%  Analysis Date = 12/16/12 
 Pct Recovery = 100%  Analysis Date = 12/14/12 
 Pct Recovery = 101%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
LORAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 88% 16% 90% 10%
Total 14 88% 16% 90% 10%

Sample Statistics
LORAZEPAM

Characteristic N % % Basis
Plotted 14 93% Spiked
Estimated Values 3 20% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
MEPROBAMATE
METHOD: LC9017 , TESTIDCODE: 67464LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 79%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 96%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 75%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 78%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 77%  Analysis Date = 03/20/14 
 Pct Recovery = 75%  Analysis Date = 03/18/14 
 Pct Recovery = 75%  Analysis Date = 03/18/14 
 Pct Recovery = 75%  Analysis Date = 03/16/14 
 Pct Recovery = 76%  Analysis Date = 03/16/14 
 Pct Recovery = 76%  Analysis Date = 03/14/14 
 Pct Recovery = 76%  Analysis Date = 03/14/14 
 Pct Recovery = 76%  Analysis Date = 03/12/14 
 Pct Recovery = 76%  Analysis Date = 03/12/14 
 Pct Recovery = 76%  Analysis Date = 03/10/14 
 Pct Recovery = 76%  Analysis Date = 03/10/14 
 Pct Recovery = 76%  Analysis Date = 03/08/14 
 Pct Recovery = 76%  Analysis Date = 03/08/14 
 Pct Recovery = 76%  Analysis Date = 03/06/14 
 Pct Recovery = 76%  Analysis Date = 03/06/14 
 Pct Recovery = 76%  Analysis Date = 03/04/14 
 Pct Recovery = 77%  Analysis Date = 03/04/14 
 Pct Recovery = 77%  Analysis Date = 03/02/14 
 Pct Recovery = 77%  Analysis Date = 03/02/14 
 Pct Recovery = 77%  Analysis Date = 02/27/14 
 Pct Recovery = 77%  Analysis Date = 02/27/14 
 Pct Recovery = 77%  Analysis Date = 02/25/14 
 Pct Recovery = 77%  Analysis Date = 02/25/14 
 Pct Recovery = 77%  Analysis Date = 02/23/14 
 Pct Recovery = 77%  Analysis Date = 02/23/14 
 Pct Recovery = 77%  Analysis Date = 02/21/14 
 Pct Recovery = 78%  Analysis Date = 02/21/14 
 Pct Recovery = 78%  Analysis Date = 02/19/14 
 Pct Recovery = 78%  Analysis Date = 02/19/14 
 Pct Recovery = 78%  Analysis Date = 02/17/14 
 Pct Recovery = 78%  Analysis Date = 02/17/14 
 Pct Recovery = 78%  Analysis Date = 02/15/14 
 Pct Recovery = 77%  Analysis Date = 02/15/14 
 Pct Recovery = 77%  Analysis Date = 02/13/14 
 Pct Recovery = 77%  Analysis Date = 02/13/14 
 Pct Recovery = 77%  Analysis Date = 02/11/14 
 Pct Recovery = 77%  Analysis Date = 02/11/14 
 Pct Recovery = 77%  Analysis Date = 02/09/14 
 Pct Recovery = 76%  Analysis Date = 02/09/14 
 Pct Recovery = 76%  Analysis Date = 02/06/14 
 Pct Recovery = 76%  Analysis Date = 02/06/14 
 Pct Recovery = 76%  Analysis Date = 02/04/14 
 Pct Recovery = 76%  Analysis Date = 02/04/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 01/31/14 
 Pct Recovery = 75%  Analysis Date = 01/31/14 
 Pct Recovery = 75%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/27/14 
 Pct Recovery = 75%  Analysis Date = 01/27/14 
 Pct Recovery = 75%  Analysis Date = 01/25/14 
 Pct Recovery = 75%  Analysis Date = 01/25/14 
 Pct Recovery = 75%  Analysis Date = 01/23/14 
 Pct Recovery = 74%  Analysis Date = 01/23/14 
 Pct Recovery = 74%  Analysis Date = 01/21/14 
 Pct Recovery = 74%  Analysis Date = 01/21/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/16/14 
 Pct Recovery = 74%  Analysis Date = 01/16/14 
 Pct Recovery = 74%  Analysis Date = 01/14/14 
 Pct Recovery = 74%  Analysis Date = 01/14/14 
 Pct Recovery = 74%  Analysis Date = 01/12/14 
 Pct Recovery = 74%  Analysis Date = 01/12/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/04/14 
 Pct Recovery = 74%  Analysis Date = 01/04/14 
 Pct Recovery = 74%  Analysis Date = 01/02/14 
 Pct Recovery = 74%  Analysis Date = 01/02/14 
 Pct Recovery = 74%  Analysis Date = 12/31/13 
 Pct Recovery = 75%  Analysis Date = 12/31/13 
 Pct Recovery = 75%  Analysis Date = 12/28/13 
 Pct Recovery = 75%  Analysis Date = 12/28/13 
 Pct Recovery = 75%  Analysis Date = 12/26/13 
 Pct Recovery = 75%  Analysis Date = 12/26/13 
 Pct Recovery = 75%  Analysis Date = 12/24/13 
 Pct Recovery = 75%  Analysis Date = 12/24/13 
 Pct Recovery = 75%  Analysis Date = 12/22/13 
 Pct Recovery = 75%  Analysis Date = 12/22/13 
 Pct Recovery = 75%  Analysis Date = 12/20/13 
 Pct Recovery = 75%  Analysis Date = 12/20/13 
 Pct Recovery = 75%  Analysis Date = 12/18/13 
 Pct Recovery = 75%  Analysis Date = 12/18/13 
 Pct Recovery = 75%  Analysis Date = 12/16/13 
 Pct Recovery = 76%  Analysis Date = 12/16/13 
 Pct Recovery = 76%  Analysis Date = 12/14/13 
 Pct Recovery = 76%  Analysis Date = 12/14/13 
 Pct Recovery = 76%  Analysis Date = 12/12/13 
 Pct Recovery = 76%  Analysis Date = 12/12/13 
 Pct Recovery = 76%  Analysis Date = 12/09/13 
 Pct Recovery = 76%  Analysis Date = 12/09/13 
 Pct Recovery = 76%  Analysis Date = 12/07/13 
 Pct Recovery = 76%  Analysis Date = 12/07/13 
 Pct Recovery = 76%  Analysis Date = 12/05/13 
 Pct Recovery = 76%  Analysis Date = 12/05/13 
 Pct Recovery = 76%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 12/01/13 
 Pct Recovery = 77%  Analysis Date = 12/01/13 
 Pct Recovery = 77%  Analysis Date = 11/29/13 
 Pct Recovery = 77%  Analysis Date = 11/29/13 
 Pct Recovery = 77%  Analysis Date = 11/27/13 
 Pct Recovery = 77%  Analysis Date = 11/27/13 
 Pct Recovery = 77%  Analysis Date = 11/25/13 
 Pct Recovery = 77%  Analysis Date = 11/25/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/14/13 
 Pct Recovery = 77%  Analysis Date = 11/14/13 
 Pct Recovery = 77%  Analysis Date = 11/12/13 
 Pct Recovery = 77%  Analysis Date = 11/12/13 
 Pct Recovery = 77%  Analysis Date = 11/10/13 
 Pct Recovery = 77%  Analysis Date = 11/10/13 
 Pct Recovery = 77%  Analysis Date = 11/08/13 
 Pct Recovery = 77%  Analysis Date = 11/08/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/02/13 
 Pct Recovery = 78%  Analysis Date = 11/02/13 
 Pct Recovery = 78%  Analysis Date = 10/30/13 
 Pct Recovery = 78%  Analysis Date = 10/30/13 
 Pct Recovery = 78%  Analysis Date = 10/28/13 
 Pct Recovery = 78%  Analysis Date = 10/28/13 
 Pct Recovery = 78%  Analysis Date = 10/26/13 
 Pct Recovery = 78%  Analysis Date = 10/26/13 
 Pct Recovery = 78%  Analysis Date = 10/24/13 
 Pct Recovery = 78%  Analysis Date = 10/24/13 
 Pct Recovery = 78%  Analysis Date = 10/22/13 
 Pct Recovery = 78%  Analysis Date = 10/22/13 
 Pct Recovery = 78%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/18/13 
 Pct Recovery = 78%  Analysis Date = 10/18/13 
 Pct Recovery = 78%  Analysis Date = 10/16/13 
 Pct Recovery = 78%  Analysis Date = 10/16/13 
 Pct Recovery = 78%  Analysis Date = 10/14/13 
 Pct Recovery = 78%  Analysis Date = 10/14/13 
 Pct Recovery = 78%  Analysis Date = 10/12/13 
 Pct Recovery = 78%  Analysis Date = 10/12/13 
 Pct Recovery = 78%  Analysis Date = 10/09/13 
 Pct Recovery = 78%  Analysis Date = 10/09/13 
 Pct Recovery = 78%  Analysis Date = 10/07/13 
 Pct Recovery = 78%  Analysis Date = 10/07/13 
 Pct Recovery = 78%  Analysis Date = 10/05/13 
 Pct Recovery = 78%  Analysis Date = 10/05/13 
 Pct Recovery = 78%  Analysis Date = 10/03/13 
 Pct Recovery = 78%  Analysis Date = 10/03/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 78%  Analysis Date = 09/27/13 
 Pct Recovery = 78%  Analysis Date = 09/27/13 
 Pct Recovery = 78%  Analysis Date = 09/25/13 
 Pct Recovery = 78%  Analysis Date = 09/25/13 
 Pct Recovery = 78%  Analysis Date = 09/23/13 
 Pct Recovery = 78%  Analysis Date = 09/23/13 
 Pct Recovery = 78%  Analysis Date = 09/20/13 
 Pct Recovery = 78%  Analysis Date = 09/20/13 
 Pct Recovery = 78%  Analysis Date = 09/18/13 
 Pct Recovery = 78%  Analysis Date = 09/18/13 
 Pct Recovery = 78%  Analysis Date = 09/16/13 
 Pct Recovery = 78%  Analysis Date = 09/16/13 
 Pct Recovery = 78%  Analysis Date = 09/14/13 
 Pct Recovery = 78%  Analysis Date = 09/14/13 
 Pct Recovery = 78%  Analysis Date = 09/12/13 
 Pct Recovery = 78%  Analysis Date = 09/12/13 
 Pct Recovery = 78%  Analysis Date = 09/10/13 
 Pct Recovery = 78%  Analysis Date = 09/10/13 
 Pct Recovery = 78%  Analysis Date = 09/08/13 
 Pct Recovery = 78%  Analysis Date = 09/08/13 
 Pct Recovery = 78%  Analysis Date = 09/06/13 
 Pct Recovery = 78%  Analysis Date = 09/06/13 
 Pct Recovery = 78%  Analysis Date = 09/04/13 
 Pct Recovery = 78%  Analysis Date = 09/04/13 
 Pct Recovery = 78%  Analysis Date = 09/02/13 
 Pct Recovery = 78%  Analysis Date = 09/02/13 
 Pct Recovery = 78%  Analysis Date = 08/30/13 
 Pct Recovery = 78%  Analysis Date = 08/30/13 
 Pct Recovery = 78%  Analysis Date = 08/28/13 
 Pct Recovery = 78%  Analysis Date = 08/28/13 
 Pct Recovery = 78%  Analysis Date = 08/26/13 
 Pct Recovery = 78%  Analysis Date = 08/26/13 
 Pct Recovery = 78%  Analysis Date = 08/24/13 
 Pct Recovery = 78%  Analysis Date = 08/24/13 
 Pct Recovery = 78%  Analysis Date = 08/22/13 
 Pct Recovery = 78%  Analysis Date = 08/22/13 
 Pct Recovery = 78%  Analysis Date = 08/20/13 
 Pct Recovery = 78%  Analysis Date = 08/20/13 
 Pct Recovery = 78%  Analysis Date = 08/18/13 
 Pct Recovery = 78%  Analysis Date = 08/18/13 
 Pct Recovery = 78%  Analysis Date = 08/16/13 
 Pct Recovery = 78%  Analysis Date = 08/16/13 
 Pct Recovery = 78%  Analysis Date = 08/14/13 
 Pct Recovery = 78%  Analysis Date = 08/14/13 
 Pct Recovery = 78%  Analysis Date = 08/11/13 
 Pct Recovery = 78%  Analysis Date = 08/11/13 
 Pct Recovery = 78%  Analysis Date = 08/09/13 
 Pct Recovery = 78%  Analysis Date = 08/09/13 
 Pct Recovery = 78%  Analysis Date = 08/07/13 
 Pct Recovery = 78%  Analysis Date = 08/07/13 
 Pct Recovery = 78%  Analysis Date = 08/05/13 
 Pct Recovery = 78%  Analysis Date = 08/05/13 
 Pct Recovery = 78%  Analysis Date = 08/03/13 
 Pct Recovery = 78%  Analysis Date = 08/03/13 
 Pct Recovery = 78%  Analysis Date = 08/01/13 
 Pct Recovery = 78%  Analysis Date = 08/01/13 
 Pct Recovery = 78%  Analysis Date = 07/30/13 
 Pct Recovery = 78%  Analysis Date = 07/30/13 
 Pct Recovery = 78%  Analysis Date = 07/28/13 
 Pct Recovery = 78%  Analysis Date = 07/28/13 
 Pct Recovery = 78%  Analysis Date = 07/26/13 
 Pct Recovery = 78%  Analysis Date = 07/26/13 
 Pct Recovery = 78%  Analysis Date = 07/24/13 
 Pct Recovery = 79%  Analysis Date = 07/24/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 79%  Analysis Date = 07/19/13 
 Pct Recovery = 79%  Analysis Date = 07/19/13 
 Pct Recovery = 79%  Analysis Date = 07/17/13 
 Pct Recovery = 79%  Analysis Date = 07/17/13 
 Pct Recovery = 79%  Analysis Date = 07/15/13 
 Pct Recovery = 79%  Analysis Date = 07/15/13 
 Pct Recovery = 79%  Analysis Date = 07/13/13 
 Pct Recovery = 79%  Analysis Date = 07/13/13 
 Pct Recovery = 79%  Analysis Date = 07/11/13 
 Pct Recovery = 79%  Analysis Date = 07/11/13 
 Pct Recovery = 79%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/07/13 
 Pct Recovery = 79%  Analysis Date = 07/07/13 
 Pct Recovery = 79%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 06/30/13 
 Pct Recovery = 79%  Analysis Date = 06/30/13 
 Pct Recovery = 79%  Analysis Date = 06/28/13 
 Pct Recovery = 79%  Analysis Date = 06/28/13 
 Pct Recovery = 79%  Analysis Date = 06/26/13 
 Pct Recovery = 79%  Analysis Date = 06/26/13 
 Pct Recovery = 79%  Analysis Date = 06/24/13 
 Pct Recovery = 79%  Analysis Date = 06/24/13 
 Pct Recovery = 79%  Analysis Date = 06/22/13 
 Pct Recovery = 79%  Analysis Date = 06/22/13 
 Pct Recovery = 79%  Analysis Date = 06/20/13 
 Pct Recovery = 79%  Analysis Date = 06/20/13 
 Pct Recovery = 79%  Analysis Date = 06/18/13 
 Pct Recovery = 79%  Analysis Date = 06/18/13 
 Pct Recovery = 79%  Analysis Date = 06/16/13 
 Pct Recovery = 79%  Analysis Date = 06/16/13 
 Pct Recovery = 79%  Analysis Date = 06/14/13 
 Pct Recovery = 79%  Analysis Date = 06/14/13 
 Pct Recovery = 79%  Analysis Date = 06/11/13 
 Pct Recovery = 79%  Analysis Date = 06/11/13 
 Pct Recovery = 79%  Analysis Date = 06/09/13 
 Pct Recovery = 79%  Analysis Date = 06/09/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 79%  Analysis Date = 05/26/13 
 Pct Recovery = 79%  Analysis Date = 05/26/13 
 Pct Recovery = 79%  Analysis Date = 05/23/13 
 Pct Recovery = 79%  Analysis Date = 05/23/13 
 Pct Recovery = 79%  Analysis Date = 05/21/13 
 Pct Recovery = 79%  Analysis Date = 05/21/13 
 Pct Recovery = 79%  Analysis Date = 05/19/13 
 Pct Recovery = 79%  Analysis Date = 05/19/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/11/13 
 Pct Recovery = 79%  Analysis Date = 05/11/13 
 Pct Recovery = 79%  Analysis Date = 05/09/13 
 Pct Recovery = 79%  Analysis Date = 05/09/13 
 Pct Recovery = 79%  Analysis Date = 05/07/13 
 Pct Recovery = 79%  Analysis Date = 05/07/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 79%  Analysis Date = 04/28/13 
 Pct Recovery = 80%  Analysis Date = 04/28/13 
 Pct Recovery = 80%  Analysis Date = 04/26/13 
 Pct Recovery = 80%  Analysis Date = 04/26/13 
 Pct Recovery = 80%  Analysis Date = 04/24/13 
 Pct Recovery = 81%  Analysis Date = 04/24/13 
 Pct Recovery = 81%  Analysis Date = 04/22/13 
 Pct Recovery = 81%  Analysis Date = 04/22/13 
 Pct Recovery = 81%  Analysis Date = 04/20/13 
 Pct Recovery = 81%  Analysis Date = 04/20/13 
 Pct Recovery = 81%  Analysis Date = 04/18/13 
 Pct Recovery = 82%  Analysis Date = 04/18/13 
 Pct Recovery = 82%  Analysis Date = 04/16/13 
 Pct Recovery = 82%  Analysis Date = 04/16/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 82%  Analysis Date = 04/11/13 
 Pct Recovery = 83%  Analysis Date = 04/11/13 
 Pct Recovery = 83%  Analysis Date = 04/09/13 
 Pct Recovery = 83%  Analysis Date = 04/09/13 
 Pct Recovery = 83%  Analysis Date = 04/07/13 
 Pct Recovery = 83%  Analysis Date = 04/07/13 
 Pct Recovery = 83%  Analysis Date = 04/05/13 
 Pct Recovery = 84%  Analysis Date = 04/05/13 
 Pct Recovery = 84%  Analysis Date = 04/03/13 
 Pct Recovery = 84%  Analysis Date = 04/03/13 
 Pct Recovery = 84%  Analysis Date = 04/01/13 
 Pct Recovery = 84%  Analysis Date = 04/01/13 
 Pct Recovery = 84%  Analysis Date = 03/30/13 
 Pct Recovery = 85%  Analysis Date = 03/30/13 
 Pct Recovery = 85%  Analysis Date = 03/28/13 
 Pct Recovery = 85%  Analysis Date = 03/28/13 
 Pct Recovery = 85%  Analysis Date = 03/26/13 
 Pct Recovery = 86%  Analysis Date = 03/26/13 
 Pct Recovery = 86%  Analysis Date = 03/23/13 
 Pct Recovery = 86%  Analysis Date = 03/23/13 
 Pct Recovery = 86%  Analysis Date = 03/21/13 
 Pct Recovery = 86%  Analysis Date = 03/21/13 
 Pct Recovery = 86%  Analysis Date = 03/19/13 
 Pct Recovery = 87%  Analysis Date = 03/19/13 
 Pct Recovery = 87%  Analysis Date = 03/17/13 
 Pct Recovery = 87%  Analysis Date = 03/17/13 
 Pct Recovery = 87%  Analysis Date = 03/15/13 
 Pct Recovery = 87%  Analysis Date = 03/15/13 
 Pct Recovery = 87%  Analysis Date = 03/13/13 
 Pct Recovery = 88%  Analysis Date = 03/13/13 
 Pct Recovery = 88%  Analysis Date = 03/11/13 
 Pct Recovery = 88%  Analysis Date = 03/11/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/07/13 
 Pct Recovery = 89%  Analysis Date = 03/07/13 
 Pct Recovery = 89%  Analysis Date = 03/04/13 
 Pct Recovery = 89%  Analysis Date = 03/04/13 
 Pct Recovery = 89%  Analysis Date = 03/02/13 
 Pct Recovery = 89%  Analysis Date = 03/02/13 
 Pct Recovery = 89%  Analysis Date = 02/28/13 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 Pct Recovery = 90%  Analysis Date = 02/26/13 
 Pct Recovery = 90%  Analysis Date = 02/26/13 
 Pct Recovery = 90%  Analysis Date = 02/24/13 
 Pct Recovery = 91%  Analysis Date = 02/24/13 
 Pct Recovery = 91%  Analysis Date = 02/22/13 
 Pct Recovery = 91%  Analysis Date = 02/22/13 
 Pct Recovery = 91%  Analysis Date = 02/20/13 
 Pct Recovery = 91%  Analysis Date = 02/20/13 
 Pct Recovery = 91%  Analysis Date = 02/18/13 
 Pct Recovery = 92%  Analysis Date = 02/18/13 
 Pct Recovery = 92%  Analysis Date = 02/16/13 
 Pct Recovery = 92%  Analysis Date = 02/16/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/11/13 
 Pct Recovery = 93%  Analysis Date = 02/11/13 
 Pct Recovery = 93%  Analysis Date = 02/09/13 
 Pct Recovery = 93%  Analysis Date = 02/09/13 
 Pct Recovery = 93%  Analysis Date = 02/07/13 
 Pct Recovery = 93%  Analysis Date = 02/07/13 
 Pct Recovery = 93%  Analysis Date = 02/05/13 
 Pct Recovery = 94%  Analysis Date = 02/05/13 
 Pct Recovery = 94%  Analysis Date = 02/03/13 
 Pct Recovery = 94%  Analysis Date = 02/03/13 
 Pct Recovery = 94%  Analysis Date = 02/01/13 
 Pct Recovery = 94%  Analysis Date = 02/01/13 
 Pct Recovery = 94%  Analysis Date = 01/30/13 
 Pct Recovery = 95%  Analysis Date = 01/30/13 
 Pct Recovery = 95%  Analysis Date = 01/28/13 
 Pct Recovery = 95%  Analysis Date = 01/28/13 
 Pct Recovery = 95%  Analysis Date = 01/26/13 
 Pct Recovery = 96%  Analysis Date = 01/26/13 
 Pct Recovery = 96%  Analysis Date = 01/24/13 
 Pct Recovery = 96%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
MEPROBAMATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 6 80% 8% 78% 3%
Total 6 80% 8% 78% 3%

Sample Statistics
MEPROBAMATE

Characteristic N % % Basis
Plotted 6 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 6 .  
False Negatives 0 0% 0 out of 6
Not Spiked 26 .  
False Positives 0 0% 0 out of 25

OBSP Determination:
METAXALONE
METHOD: LC9017 , TESTIDCODE: 67504LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 71%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 86%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 81%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 82%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 73%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 60%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 80%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 105%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 57%  Analysis Date = 03/21/14 
 Pct Recovery = 85%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/18/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 84%  Analysis Date = 03/16/14 
 Pct Recovery = 84%  Analysis Date = 03/14/14 
 Pct Recovery = 84%  Analysis Date = 03/14/14 
 Pct Recovery = 84%  Analysis Date = 03/11/14 
 Pct Recovery = 83%  Analysis Date = 03/11/14 
 Pct Recovery = 83%  Analysis Date = 03/09/14 
 Pct Recovery = 83%  Analysis Date = 03/09/14 
 Pct Recovery = 83%  Analysis Date = 03/07/14 
 Pct Recovery = 82%  Analysis Date = 03/07/14 
 Pct Recovery = 82%  Analysis Date = 03/04/14 
 Pct Recovery = 82%  Analysis Date = 03/04/14 
 Pct Recovery = 82%  Analysis Date = 03/02/14 
 Pct Recovery = 81%  Analysis Date = 03/02/14 
 Pct Recovery = 81%  Analysis Date = 02/28/14 
 Pct Recovery = 81%  Analysis Date = 02/28/14 
 Pct Recovery = 81%  Analysis Date = 02/25/14 
 Pct Recovery = 81%  Analysis Date = 02/25/14 
 Pct Recovery = 81%  Analysis Date = 02/23/14 
 Pct Recovery = 80%  Analysis Date = 02/23/14 
 Pct Recovery = 80%  Analysis Date = 02/21/14 
 Pct Recovery = 80%  Analysis Date = 02/21/14 
 Pct Recovery = 80%  Analysis Date = 02/18/14 
 Pct Recovery = 79%  Analysis Date = 02/18/14 
 Pct Recovery = 79%  Analysis Date = 02/16/14 
 Pct Recovery = 79%  Analysis Date = 02/16/14 
 Pct Recovery = 79%  Analysis Date = 02/14/14 
 Pct Recovery = 78%  Analysis Date = 02/14/14 
 Pct Recovery = 78%  Analysis Date = 02/12/14 
 Pct Recovery = 78%  Analysis Date = 02/12/14 
 Pct Recovery = 78%  Analysis Date = 02/09/14 
 Pct Recovery = 77%  Analysis Date = 02/09/14 
 Pct Recovery = 77%  Analysis Date = 02/07/14 
 Pct Recovery = 77%  Analysis Date = 02/07/14 
 Pct Recovery = 77%  Analysis Date = 02/05/14 
 Pct Recovery = 76%  Analysis Date = 02/05/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 01/31/14 
 Pct Recovery = 75%  Analysis Date = 01/31/14 
 Pct Recovery = 75%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/29/14 
 Pct Recovery = 75%  Analysis Date = 01/26/14 
 Pct Recovery = 74%  Analysis Date = 01/26/14 
 Pct Recovery = 74%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/24/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/19/14 
 Pct Recovery = 73%  Analysis Date = 01/19/14 
 Pct Recovery = 73%  Analysis Date = 01/17/14 
 Pct Recovery = 72%  Analysis Date = 01/17/14 
 Pct Recovery = 72%  Analysis Date = 01/15/14 
 Pct Recovery = 72%  Analysis Date = 01/15/14 
 Pct Recovery = 72%  Analysis Date = 01/13/14 
 Pct Recovery = 71%  Analysis Date = 01/13/14 
 Pct Recovery = 71%  Analysis Date = 01/10/14 
 Pct Recovery = 71%  Analysis Date = 01/10/14 
 Pct Recovery = 71%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/06/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/03/14 
 Pct Recovery = 70%  Analysis Date = 01/01/14 
 Pct Recovery = 69%  Analysis Date = 01/01/14 
 Pct Recovery = 69%  Analysis Date = 12/30/13 
 Pct Recovery = 69%  Analysis Date = 12/30/13 
 Pct Recovery = 69%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/25/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/23/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/18/13 
 Pct Recovery = 67%  Analysis Date = 12/18/13 
 Pct Recovery = 67%  Analysis Date = 12/16/13 
 Pct Recovery = 66%  Analysis Date = 12/16/13 
 Pct Recovery = 66%  Analysis Date = 12/13/13 
 Pct Recovery = 66%  Analysis Date = 12/13/13 
 Pct Recovery = 66%  Analysis Date = 12/11/13 
 Pct Recovery = 66%  Analysis Date = 12/11/13 
 Pct Recovery = 66%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 64%  Analysis Date = 12/04/13 
 Pct Recovery = 64%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/27/13 
 Pct Recovery = 63%  Analysis Date = 11/27/13 
 Pct Recovery = 63%  Analysis Date = 11/25/13 
 Pct Recovery = 63%  Analysis Date = 11/25/13 
 Pct Recovery = 63%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/23/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/20/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/18/13 
 Pct Recovery = 62%  Analysis Date = 11/16/13 
 Pct Recovery = 62%  Analysis Date = 11/16/13 
 Pct Recovery = 62%  Analysis Date = 11/13/13 
 Pct Recovery = 62%  Analysis Date = 11/13/13 
 Pct Recovery = 62%  Analysis Date = 11/11/13 
 Pct Recovery = 62%  Analysis Date = 11/11/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/07/13 
 Pct Recovery = 62%  Analysis Date = 11/07/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/02/13 
 Pct Recovery = 62%  Analysis Date = 11/02/13 
 Pct Recovery = 62%  Analysis Date = 10/31/13 
 Pct Recovery = 62%  Analysis Date = 10/31/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/26/13 
 Pct Recovery = 62%  Analysis Date = 10/26/13 
 Pct Recovery = 62%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/24/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/21/13 
 Pct Recovery = 62%  Analysis Date = 10/19/13 
 Pct Recovery = 62%  Analysis Date = 10/19/13 
 Pct Recovery = 62%  Analysis Date = 10/17/13 
 Pct Recovery = 63%  Analysis Date = 10/17/13 
 Pct Recovery = 63%  Analysis Date = 10/14/13 
 Pct Recovery = 63%  Analysis Date = 10/14/13 
 Pct Recovery = 63%  Analysis Date = 10/12/13 
 Pct Recovery = 63%  Analysis Date = 10/12/13 
 Pct Recovery = 63%  Analysis Date = 10/10/13 
 Pct Recovery = 63%  Analysis Date = 10/10/13 
 Pct Recovery = 63%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/07/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/05/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/03/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 10/01/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/28/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/26/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/24/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/19/13 
 Pct Recovery = 63%  Analysis Date = 09/19/13 
 Pct Recovery = 63%  Analysis Date = 09/17/13 
 Pct Recovery = 63%  Analysis Date = 09/17/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/07/13 
 Pct Recovery = 63%  Analysis Date = 09/07/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/29/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/27/13 
 Pct Recovery = 64%  Analysis Date = 08/25/13 
 Pct Recovery = 64%  Analysis Date = 08/25/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/22/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/20/13 
 Pct Recovery = 64%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 Pct Recovery = 65%  Analysis Date = 08/15/13 
 Pct Recovery = 65%  Analysis Date = 08/15/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/13/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/11/13 
 Pct Recovery = 65%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/08/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/06/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/04/13 
 Pct Recovery = 66%  Analysis Date = 08/02/13 
 Pct Recovery = 66%  Analysis Date = 08/02/13 
 Pct Recovery = 66%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/16/13 
 Pct Recovery = 68%  Analysis Date = 07/16/13 
 Pct Recovery = 68%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/14/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/05/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/30/13 
 Pct Recovery = 70%  Analysis Date = 06/28/13 
 Pct Recovery = 70%  Analysis Date = 06/28/13 
 Pct Recovery = 70%  Analysis Date = 06/26/13 
 Pct Recovery = 70%  Analysis Date = 06/26/13 
 Pct Recovery = 70%  Analysis Date = 06/23/13 
 Pct Recovery = 70%  Analysis Date = 06/23/13 
 Pct Recovery = 70%  Analysis Date = 06/21/13 
 Pct Recovery = 70%  Analysis Date = 06/21/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/16/13 
 Pct Recovery = 71%  Analysis Date = 06/16/13 
 Pct Recovery = 71%  Analysis Date = 06/14/13 
 Pct Recovery = 71%  Analysis Date = 06/14/13 
 Pct Recovery = 71%  Analysis Date = 06/12/13 
 Pct Recovery = 71%  Analysis Date = 06/12/13 
 Pct Recovery = 71%  Analysis Date = 06/09/13 
 Pct Recovery = 72%  Analysis Date = 06/09/13 
 Pct Recovery = 72%  Analysis Date = 06/07/13 
 Pct Recovery = 72%  Analysis Date = 06/07/13 
 Pct Recovery = 72%  Analysis Date = 06/05/13 
 Pct Recovery = 72%  Analysis Date = 06/05/13 
 Pct Recovery = 72%  Analysis Date = 06/02/13 
 Pct Recovery = 72%  Analysis Date = 06/02/13 
 Pct Recovery = 72%  Analysis Date = 05/31/13 
 Pct Recovery = 73%  Analysis Date = 05/31/13 
 Pct Recovery = 73%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/27/13 
 Pct Recovery = 73%  Analysis Date = 05/27/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/20/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/15/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/13/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/06/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/29/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/22/13 
 Pct Recovery = 76%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/17/13 
 Pct Recovery = 77%  Analysis Date = 04/17/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/10/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 77%  Analysis Date = 04/06/13 
 Pct Recovery = 78%  Analysis Date = 04/06/13 
 Pct Recovery = 78%  Analysis Date = 04/03/13 
 Pct Recovery = 78%  Analysis Date = 04/03/13 
 Pct Recovery = 78%  Analysis Date = 04/01/13 
 Pct Recovery = 78%  Analysis Date = 04/01/13 
 Pct Recovery = 78%  Analysis Date = 03/30/13 
 Pct Recovery = 78%  Analysis Date = 03/30/13 
 Pct Recovery = 78%  Analysis Date = 03/27/13 
 Pct Recovery = 78%  Analysis Date = 03/27/13 
 Pct Recovery = 78%  Analysis Date = 03/25/13 
 Pct Recovery = 78%  Analysis Date = 03/25/13 
 Pct Recovery = 78%  Analysis Date = 03/23/13 
 Pct Recovery = 79%  Analysis Date = 03/23/13 
 Pct Recovery = 79%  Analysis Date = 03/21/13 
 Pct Recovery = 79%  Analysis Date = 03/21/13 
 Pct Recovery = 79%  Analysis Date = 03/18/13 
 Pct Recovery = 79%  Analysis Date = 03/18/13 
 Pct Recovery = 79%  Analysis Date = 03/16/13 
 Pct Recovery = 79%  Analysis Date = 03/16/13 
 Pct Recovery = 79%  Analysis Date = 03/14/13 
 Pct Recovery = 79%  Analysis Date = 03/14/13 
 Pct Recovery = 79%  Analysis Date = 03/11/13 
 Pct Recovery = 79%  Analysis Date = 03/11/13 
 Pct Recovery = 79%  Analysis Date = 03/09/13 
 Pct Recovery = 80%  Analysis Date = 03/09/13 
 Pct Recovery = 80%  Analysis Date = 03/07/13 
 Pct Recovery = 80%  Analysis Date = 03/07/13 
 Pct Recovery = 80%  Analysis Date = 03/04/13 
 Pct Recovery = 80%  Analysis Date = 03/04/13 
 Pct Recovery = 80%  Analysis Date = 03/02/13 
 Pct Recovery = 80%  Analysis Date = 03/02/13 
 Pct Recovery = 80%  Analysis Date = 02/28/13 
 Pct Recovery = 80%  Analysis Date = 02/28/13 
 Pct Recovery = 80%  Analysis Date = 02/25/13 
 Pct Recovery = 80%  Analysis Date = 02/25/13 
 Pct Recovery = 80%  Analysis Date = 02/23/13 
 Pct Recovery = 81%  Analysis Date = 02/23/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/18/13 
 Pct Recovery = 81%  Analysis Date = 02/18/13 
 Pct Recovery = 81%  Analysis Date = 02/16/13 
 Pct Recovery = 81%  Analysis Date = 02/16/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/05/13 
 Pct Recovery = 81%  Analysis Date = 02/05/13 
 Pct Recovery = 81%  Analysis Date = 02/02/13 
 Pct Recovery = 82%  Analysis Date = 02/02/13 
 Pct Recovery = 82%  Analysis Date = 01/31/13 
 Pct Recovery = 82%  Analysis Date = 01/31/13 
 Pct Recovery = 82%  Analysis Date = 01/29/13 
 Pct Recovery = 82%  Analysis Date = 01/29/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/24/13 
 Pct Recovery = 82%  Analysis Date = 01/24/13 
 Pct Recovery = 82%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/22/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/19/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/17/13 
 Pct Recovery = 82%  Analysis Date = 01/15/13 
 Pct Recovery = 83%  Analysis Date = 01/15/13 
 Pct Recovery = 83%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/13/13 
 Pct Recovery = 83%  Analysis Date = 01/10/13 
 Pct Recovery = 83%  Analysis Date = 01/10/13 
 Pct Recovery = 83%  Analysis Date = 01/08/13 
 Pct Recovery = 83%  Analysis Date = 01/08/13 
 Pct Recovery = 83%  Analysis Date = 01/06/13 
 Pct Recovery = 83%  Analysis Date = 01/06/13 
 Pct Recovery = 83%  Analysis Date = 01/03/13 
 Pct Recovery = 83%  Analysis Date = 01/03/13 
 Pct Recovery = 83%  Analysis Date = 01/01/13 
 Pct Recovery = 83%  Analysis Date = 01/01/13 
 Pct Recovery = 83%  Analysis Date = 12/30/12 
 Pct Recovery = 83%  Analysis Date = 12/30/12 
 Pct Recovery = 83%  Analysis Date = 12/27/12 
 Pct Recovery = 84%  Analysis Date = 12/27/12 
 Pct Recovery = 84%  Analysis Date = 12/25/12 
 Pct Recovery = 84%  Analysis Date = 12/25/12 
 Pct Recovery = 84%  Analysis Date = 12/23/12 
 Pct Recovery = 84%  Analysis Date = 12/23/12 
 Pct Recovery = 84%  Analysis Date = 12/20/12 
 Pct Recovery = 84%  Analysis Date = 12/20/12 
 Pct Recovery = 84%  Analysis Date = 12/18/12 
 Pct Recovery = 84%  Analysis Date = 12/18/12 
 Pct Recovery = 84%  Analysis Date = 12/16/12 
 Pct Recovery = 84%  Analysis Date = 12/16/12 
 Pct Recovery = 84%  Analysis Date = 12/14/12 
 Pct Recovery = 84%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METAXALONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 76% 14% 75% 13%
Total 11 76% 14% 75% 13%

Sample Statistics
METAXALONE

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 11 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
METFORMIN
METHOD: LC9017 , TESTIDCODE: 67492LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 50%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 51%  Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 71%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 93%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 37%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 89%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 45%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 43%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 Pct Recovery = 51%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/11/14 
 Pct Recovery = 51%  Analysis Date = 03/11/14 
 Pct Recovery = 51%  Analysis Date = 03/09/14 
 Pct Recovery = 51%  Analysis Date = 03/09/14 
 Pct Recovery = 51%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/07/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/04/14 
 Pct Recovery = 51%  Analysis Date = 03/02/14 
 Pct Recovery = 51%  Analysis Date = 03/02/14 
 Pct Recovery = 51%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/28/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/25/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/23/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/21/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/18/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/16/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/14/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/12/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/09/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/07/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/05/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 02/02/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/31/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/29/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/26/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/24/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/19/14 
 Pct Recovery = 51%  Analysis Date = 01/17/14 
 Pct Recovery = 51%  Analysis Date = 01/17/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/10/14 
 Pct Recovery = 51%  Analysis Date = 01/10/14 
 Pct Recovery = 51%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/08/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/06/14 
 Pct Recovery = 50%  Analysis Date = 01/03/14 
 Pct Recovery = 50%  Analysis Date = 01/03/14 
 Pct Recovery = 50%  Analysis Date = 01/01/14 
 Pct Recovery = 50%  Analysis Date = 01/01/14 
 Pct Recovery = 50%  Analysis Date = 12/30/13 
 Pct Recovery = 50%  Analysis Date = 12/30/13 
 Pct Recovery = 50%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/27/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/25/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/23/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/20/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/18/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/16/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 50%  Analysis Date = 12/11/13 
 Pct Recovery = 50%  Analysis Date = 12/11/13 
 Pct Recovery = 50%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/07/13 
 Pct Recovery = 49%  Analysis Date = 12/07/13 
 Pct Recovery = 49%  Analysis Date = 12/04/13 
 Pct Recovery = 49%  Analysis Date = 12/04/13 
 Pct Recovery = 49%  Analysis Date = 12/02/13 
 Pct Recovery = 49%  Analysis Date = 12/02/13 
 Pct Recovery = 49%  Analysis Date = 11/30/13 
 Pct Recovery = 49%  Analysis Date = 11/30/13 
 Pct Recovery = 49%  Analysis Date = 11/27/13 
 Pct Recovery = 49%  Analysis Date = 11/27/13 
 Pct Recovery = 49%  Analysis Date = 11/25/13 
 Pct Recovery = 49%  Analysis Date = 11/25/13 
 Pct Recovery = 49%  Analysis Date = 11/23/13 
 Pct Recovery = 49%  Analysis Date = 11/23/13 
 Pct Recovery = 49%  Analysis Date = 11/20/13 
 Pct Recovery = 49%  Analysis Date = 11/20/13 
 Pct Recovery = 49%  Analysis Date = 11/18/13 
 Pct Recovery = 49%  Analysis Date = 11/18/13 
 Pct Recovery = 49%  Analysis Date = 11/16/13 
 Pct Recovery = 49%  Analysis Date = 11/16/13 
 Pct Recovery = 49%  Analysis Date = 11/13/13 
 Pct Recovery = 49%  Analysis Date = 11/13/13 
 Pct Recovery = 49%  Analysis Date = 11/11/13 
 Pct Recovery = 50%  Analysis Date = 11/11/13 
 Pct Recovery = 50%  Analysis Date = 11/09/13 
 Pct Recovery = 50%  Analysis Date = 11/09/13 
 Pct Recovery = 50%  Analysis Date = 11/07/13 
 Pct Recovery = 50%  Analysis Date = 11/07/13 
 Pct Recovery = 50%  Analysis Date = 11/04/13 
 Pct Recovery = 50%  Analysis Date = 11/04/13 
 Pct Recovery = 50%  Analysis Date = 11/02/13 
 Pct Recovery = 50%  Analysis Date = 11/02/13 
 Pct Recovery = 50%  Analysis Date = 10/31/13 
 Pct Recovery = 50%  Analysis Date = 10/31/13 
 Pct Recovery = 50%  Analysis Date = 10/28/13 
 Pct Recovery = 50%  Analysis Date = 10/28/13 
 Pct Recovery = 50%  Analysis Date = 10/26/13 
 Pct Recovery = 51%  Analysis Date = 10/26/13 
 Pct Recovery = 51%  Analysis Date = 10/24/13 
 Pct Recovery = 51%  Analysis Date = 10/24/13 
 Pct Recovery = 51%  Analysis Date = 10/21/13 
 Pct Recovery = 51%  Analysis Date = 10/21/13 
 Pct Recovery = 51%  Analysis Date = 10/19/13 
 Pct Recovery = 51%  Analysis Date = 10/19/13 
 Pct Recovery = 51%  Analysis Date = 10/17/13 
 Pct Recovery = 51%  Analysis Date = 10/17/13 
 Pct Recovery = 51%  Analysis Date = 10/14/13 
 Pct Recovery = 51%  Analysis Date = 10/14/13 
 Pct Recovery = 51%  Analysis Date = 10/12/13 
 Pct Recovery = 52%  Analysis Date = 10/12/13 
 Pct Recovery = 52%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/26/13 
 Pct Recovery = 53%  Analysis Date = 09/26/13 
 Pct Recovery = 53%  Analysis Date = 09/24/13 
 Pct Recovery = 53%  Analysis Date = 09/24/13 
 Pct Recovery = 53%  Analysis Date = 09/21/13 
 Pct Recovery = 53%  Analysis Date = 09/21/13 
 Pct Recovery = 53%  Analysis Date = 09/19/13 
 Pct Recovery = 53%  Analysis Date = 09/19/13 
 Pct Recovery = 53%  Analysis Date = 09/17/13 
 Pct Recovery = 53%  Analysis Date = 09/17/13 
 Pct Recovery = 53%  Analysis Date = 09/14/13 
 Pct Recovery = 53%  Analysis Date = 09/14/13 
 Pct Recovery = 53%  Analysis Date = 09/12/13 
 Pct Recovery = 54%  Analysis Date = 09/12/13 
 Pct Recovery = 54%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/07/13 
 Pct Recovery = 54%  Analysis Date = 09/07/13 
 Pct Recovery = 54%  Analysis Date = 09/05/13 
 Pct Recovery = 54%  Analysis Date = 09/05/13 
 Pct Recovery = 54%  Analysis Date = 09/03/13 
 Pct Recovery = 54%  Analysis Date = 09/03/13 
 Pct Recovery = 54%  Analysis Date = 09/01/13 
 Pct Recovery = 54%  Analysis Date = 09/01/13 
 Pct Recovery = 54%  Analysis Date = 08/29/13 
 Pct Recovery = 54%  Analysis Date = 08/29/13 
 Pct Recovery = 54%  Analysis Date = 08/27/13 
 Pct Recovery = 55%  Analysis Date = 08/27/13 
 Pct Recovery = 55%  Analysis Date = 08/25/13 
 Pct Recovery = 55%  Analysis Date = 08/25/13 
 Pct Recovery = 55%  Analysis Date = 08/22/13 
 Pct Recovery = 55%  Analysis Date = 08/22/13 
 Pct Recovery = 55%  Analysis Date = 08/20/13 
 Pct Recovery = 55%  Analysis Date = 08/20/13 
 Pct Recovery = 55%  Analysis Date = 08/18/13 
 Pct Recovery = 55%  Analysis Date = 08/18/13 
 Pct Recovery = 55%  Analysis Date = 08/15/13 
 Pct Recovery = 55%  Analysis Date = 08/15/13 
 Pct Recovery = 55%  Analysis Date = 08/13/13 
 Pct Recovery = 56%  Analysis Date = 08/13/13 
 Pct Recovery = 56%  Analysis Date = 08/11/13 
 Pct Recovery = 56%  Analysis Date = 08/11/13 
 Pct Recovery = 56%  Analysis Date = 08/08/13 
 Pct Recovery = 56%  Analysis Date = 08/08/13 
 Pct Recovery = 56%  Analysis Date = 08/06/13 
 Pct Recovery = 56%  Analysis Date = 08/06/13 
 Pct Recovery = 56%  Analysis Date = 08/04/13 
 Pct Recovery = 56%  Analysis Date = 08/04/13 
 Pct Recovery = 56%  Analysis Date = 08/02/13 
 Pct Recovery = 56%  Analysis Date = 08/02/13 
 Pct Recovery = 56%  Analysis Date = 07/30/13 
 Pct Recovery = 56%  Analysis Date = 07/30/13 
 Pct Recovery = 56%  Analysis Date = 07/28/13 
 Pct Recovery = 57%  Analysis Date = 07/28/13 
 Pct Recovery = 57%  Analysis Date = 07/26/13 
 Pct Recovery = 57%  Analysis Date = 07/26/13 
 Pct Recovery = 57%  Analysis Date = 07/23/13 
 Pct Recovery = 57%  Analysis Date = 07/23/13 
 Pct Recovery = 57%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/19/13 
 Pct Recovery = 57%  Analysis Date = 07/19/13 
 Pct Recovery = 57%  Analysis Date = 07/16/13 
 Pct Recovery = 57%  Analysis Date = 07/16/13 
 Pct Recovery = 57%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/12/13 
 Pct Recovery = 58%  Analysis Date = 07/12/13 
 Pct Recovery = 58%  Analysis Date = 07/09/13 
 Pct Recovery = 58%  Analysis Date = 07/09/13 
 Pct Recovery = 58%  Analysis Date = 07/07/13 
 Pct Recovery = 58%  Analysis Date = 07/07/13 
 Pct Recovery = 58%  Analysis Date = 07/05/13 
 Pct Recovery = 58%  Analysis Date = 07/05/13 
 Pct Recovery = 58%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 07/02/13 
 Pct Recovery = 58%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/30/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/28/13 
 Pct Recovery = 59%  Analysis Date = 06/26/13 
 Pct Recovery = 59%  Analysis Date = 06/26/13 
 Pct Recovery = 59%  Analysis Date = 06/23/13 
 Pct Recovery = 59%  Analysis Date = 06/23/13 
 Pct Recovery = 59%  Analysis Date = 06/21/13 
 Pct Recovery = 59%  Analysis Date = 06/21/13 
 Pct Recovery = 59%  Analysis Date = 06/19/13 
 Pct Recovery = 59%  Analysis Date = 06/19/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/14/13 
 Pct Recovery = 60%  Analysis Date = 06/14/13 
 Pct Recovery = 60%  Analysis Date = 06/12/13 
 Pct Recovery = 60%  Analysis Date = 06/12/13 
 Pct Recovery = 60%  Analysis Date = 06/09/13 
 Pct Recovery = 60%  Analysis Date = 06/09/13 
 Pct Recovery = 60%  Analysis Date = 06/07/13 
 Pct Recovery = 60%  Analysis Date = 06/07/13 
 Pct Recovery = 60%  Analysis Date = 06/05/13 
 Pct Recovery = 60%  Analysis Date = 06/05/13 
 Pct Recovery = 60%  Analysis Date = 06/02/13 
 Pct Recovery = 60%  Analysis Date = 06/02/13 
 Pct Recovery = 60%  Analysis Date = 05/31/13 
 Pct Recovery = 61%  Analysis Date = 05/31/13 
 Pct Recovery = 61%  Analysis Date = 05/29/13 
 Pct Recovery = 61%  Analysis Date = 05/29/13 
 Pct Recovery = 61%  Analysis Date = 05/27/13 
 Pct Recovery = 61%  Analysis Date = 05/27/13 
 Pct Recovery = 61%  Analysis Date = 05/24/13 
 Pct Recovery = 61%  Analysis Date = 05/24/13 
 Pct Recovery = 61%  Analysis Date = 05/22/13 
 Pct Recovery = 61%  Analysis Date = 05/22/13 
 Pct Recovery = 61%  Analysis Date = 05/20/13 
 Pct Recovery = 61%  Analysis Date = 05/20/13 
 Pct Recovery = 61%  Analysis Date = 05/17/13 
 Pct Recovery = 61%  Analysis Date = 05/17/13 
 Pct Recovery = 61%  Analysis Date = 05/15/13 
 Pct Recovery = 62%  Analysis Date = 05/15/13 
 Pct Recovery = 62%  Analysis Date = 05/13/13 
 Pct Recovery = 62%  Analysis Date = 05/13/13 
 Pct Recovery = 62%  Analysis Date = 05/10/13 
 Pct Recovery = 62%  Analysis Date = 05/10/13 
 Pct Recovery = 62%  Analysis Date = 05/08/13 
 Pct Recovery = 62%  Analysis Date = 05/08/13 
 Pct Recovery = 62%  Analysis Date = 05/06/13 
 Pct Recovery = 62%  Analysis Date = 05/06/13 
 Pct Recovery = 62%  Analysis Date = 05/03/13 
 Pct Recovery = 62%  Analysis Date = 05/03/13 
 Pct Recovery = 62%  Analysis Date = 05/01/13 
 Pct Recovery = 63%  Analysis Date = 05/01/13 
 Pct Recovery = 63%  Analysis Date = 04/29/13 
 Pct Recovery = 63%  Analysis Date = 04/29/13 
 Pct Recovery = 63%  Analysis Date = 04/26/13 
 Pct Recovery = 63%  Analysis Date = 04/26/13 
 Pct Recovery = 63%  Analysis Date = 04/24/13 
 Pct Recovery = 64%  Analysis Date = 04/24/13 
 Pct Recovery = 64%  Analysis Date = 04/22/13 
 Pct Recovery = 64%  Analysis Date = 04/22/13 
 Pct Recovery = 64%  Analysis Date = 04/20/13 
 Pct Recovery = 64%  Analysis Date = 04/20/13 
 Pct Recovery = 64%  Analysis Date = 04/17/13 
 Pct Recovery = 64%  Analysis Date = 04/17/13 
 Pct Recovery = 64%  Analysis Date = 04/15/13 
 Pct Recovery = 65%  Analysis Date = 04/15/13 
 Pct Recovery = 65%  Analysis Date = 04/13/13 
 Pct Recovery = 65%  Analysis Date = 04/13/13 
 Pct Recovery = 65%  Analysis Date = 04/10/13 
 Pct Recovery = 65%  Analysis Date = 04/10/13 
 Pct Recovery = 65%  Analysis Date = 04/08/13 
 Pct Recovery = 66%  Analysis Date = 04/08/13 
 Pct Recovery = 66%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/03/13 
 Pct Recovery = 66%  Analysis Date = 04/03/13 
 Pct Recovery = 66%  Analysis Date = 04/01/13 
 Pct Recovery = 67%  Analysis Date = 04/01/13 
 Pct Recovery = 67%  Analysis Date = 03/30/13 
 Pct Recovery = 67%  Analysis Date = 03/30/13 
 Pct Recovery = 67%  Analysis Date = 03/27/13 
 Pct Recovery = 67%  Analysis Date = 03/27/13 
 Pct Recovery = 67%  Analysis Date = 03/25/13 
 Pct Recovery = 68%  Analysis Date = 03/25/13 
 Pct Recovery = 68%  Analysis Date = 03/23/13 
 Pct Recovery = 68%  Analysis Date = 03/23/13 
 Pct Recovery = 68%  Analysis Date = 03/21/13 
 Pct Recovery = 68%  Analysis Date = 03/21/13 
 Pct Recovery = 68%  Analysis Date = 03/18/13 
 Pct Recovery = 69%  Analysis Date = 03/18/13 
 Pct Recovery = 69%  Analysis Date = 03/16/13 
 Pct Recovery = 69%  Analysis Date = 03/16/13 
 Pct Recovery = 69%  Analysis Date = 03/14/13 
 Pct Recovery = 69%  Analysis Date = 03/14/13 
 Pct Recovery = 69%  Analysis Date = 03/11/13 
 Pct Recovery = 69%  Analysis Date = 03/11/13 
 Pct Recovery = 69%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/09/13 
 Pct Recovery = 70%  Analysis Date = 03/07/13 
 Pct Recovery = 70%  Analysis Date = 03/07/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 71%  Analysis Date = 03/02/13 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 Pct Recovery = 71%  Analysis Date = 02/25/13 
 Pct Recovery = 71%  Analysis Date = 02/25/13 
 Pct Recovery = 71%  Analysis Date = 02/23/13 
 Pct Recovery = 72%  Analysis Date = 02/23/13 
 Pct Recovery = 72%  Analysis Date = 02/21/13 
 Pct Recovery = 72%  Analysis Date = 02/21/13 
 Pct Recovery = 72%  Analysis Date = 02/18/13 
 Pct Recovery = 73%  Analysis Date = 02/18/13 
 Pct Recovery = 73%  Analysis Date = 02/16/13 
 Pct Recovery = 73%  Analysis Date = 02/16/13 
 Pct Recovery = 73%  Analysis Date = 02/14/13 
 Pct Recovery = 73%  Analysis Date = 02/14/13 
 Pct Recovery = 73%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/09/13 
 Pct Recovery = 74%  Analysis Date = 02/09/13 
 Pct Recovery = 74%  Analysis Date = 02/07/13 
 Pct Recovery = 74%  Analysis Date = 02/07/13 
 Pct Recovery = 74%  Analysis Date = 02/05/13 
 Pct Recovery = 75%  Analysis Date = 02/05/13 
 Pct Recovery = 75%  Analysis Date = 02/02/13 
 Pct Recovery = 75%  Analysis Date = 02/02/13 
 Pct Recovery = 75%  Analysis Date = 01/31/13 
 Pct Recovery = 75%  Analysis Date = 01/31/13 
 Pct Recovery = 75%  Analysis Date = 01/29/13 
 Pct Recovery = 76%  Analysis Date = 01/29/13 
 Pct Recovery = 76%  Analysis Date = 01/26/13 
 Pct Recovery = 76%  Analysis Date = 01/26/13 
 Pct Recovery = 76%  Analysis Date = 01/24/13 
 Pct Recovery = 76%  Analysis Date = 01/24/13 
 Pct Recovery = 76%  Analysis Date = 01/22/13 
 Pct Recovery = 77%  Analysis Date = 01/22/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/17/13 
 Pct Recovery = 78%  Analysis Date = 01/17/13 
 Pct Recovery = 78%  Analysis Date = 01/15/13 
 Pct Recovery = 78%  Analysis Date = 01/15/13 
 Pct Recovery = 78%  Analysis Date = 01/13/13 
 Pct Recovery = 78%  Analysis Date = 01/13/13 
 Pct Recovery = 78%  Analysis Date = 01/10/13 
 Pct Recovery = 79%  Analysis Date = 01/10/13 
 Pct Recovery = 79%  Analysis Date = 01/08/13 
 Pct Recovery = 79%  Analysis Date = 01/08/13 
 Pct Recovery = 79%  Analysis Date = 01/06/13 
 Pct Recovery = 79%  Analysis Date = 01/06/13 
 Pct Recovery = 79%  Analysis Date = 01/03/13 
 Pct Recovery = 80%  Analysis Date = 01/03/13 
 Pct Recovery = 80%  Analysis Date = 01/01/13 
 Pct Recovery = 80%  Analysis Date = 01/01/13 
 Pct Recovery = 80%  Analysis Date = 12/30/12 
 Pct Recovery = 80%  Analysis Date = 12/30/12 
 Pct Recovery = 80%  Analysis Date = 12/27/12 
 Pct Recovery = 81%  Analysis Date = 12/27/12 
 Pct Recovery = 81%  Analysis Date = 12/25/12 
 Pct Recovery = 81%  Analysis Date = 12/25/12 
 Pct Recovery = 81%  Analysis Date = 12/23/12 
 Pct Recovery = 81%  Analysis Date = 12/23/12 
 Pct Recovery = 81%  Analysis Date = 12/20/12 
 Pct Recovery = 82%  Analysis Date = 12/20/12 
 Pct Recovery = 82%  Analysis Date = 12/18/12 
 Pct Recovery = 82%  Analysis Date = 12/18/12 
 Pct Recovery = 82%  Analysis Date = 12/16/12 
 Pct Recovery = 82%  Analysis Date = 12/16/12 
 Pct Recovery = 82%  Analysis Date = 12/14/12 
 Pct Recovery = 83%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METFORMIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 10 61% 20% 51% 25%
Total 10 61% 20% 51% 25%

Sample Statistics
METFORMIN

Characteristic N % % Basis
Plotted 10 91% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 1 9% 1 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
METHADONE
METHOD: LC9017 , TESTIDCODE: 67500LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 66%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 61%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 71%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 47%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 57%  Analysis Date = 02/19/14 
 Pct Recovery = 61%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/18/14 
 Pct Recovery = 65%  Analysis Date = 02/16/14 
 Pct Recovery = 66%  Analysis Date = 02/16/14 
 Pct Recovery = 66%  Analysis Date = 02/14/14 
 Pct Recovery = 66%  Analysis Date = 02/14/14 
 Pct Recovery = 66%  Analysis Date = 02/12/14 
 Pct Recovery = 66%  Analysis Date = 02/12/14 
 Pct Recovery = 66%  Analysis Date = 02/11/14 
 Pct Recovery = 66%  Analysis Date = 02/11/14 
 Pct Recovery = 66%  Analysis Date = 02/09/14 
 Pct Recovery = 66%  Analysis Date = 02/09/14 
 Pct Recovery = 66%  Analysis Date = 02/07/14 
 Pct Recovery = 66%  Analysis Date = 02/07/14 
 Pct Recovery = 66%  Analysis Date = 02/05/14 
 Pct Recovery = 66%  Analysis Date = 02/05/14 
 Pct Recovery = 66%  Analysis Date = 02/03/14 
 Pct Recovery = 67%  Analysis Date = 02/03/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/29/14 
 Pct Recovery = 67%  Analysis Date = 01/29/14 
 Pct Recovery = 67%  Analysis Date = 01/27/14 
 Pct Recovery = 67%  Analysis Date = 01/27/14 
 Pct Recovery = 67%  Analysis Date = 01/26/14 
 Pct Recovery = 67%  Analysis Date = 01/26/14 
 Pct Recovery = 67%  Analysis Date = 01/24/14 
 Pct Recovery = 67%  Analysis Date = 01/24/14 
 Pct Recovery = 67%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/20/14 
 Pct Recovery = 68%  Analysis Date = 01/20/14 
 Pct Recovery = 68%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/17/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/11/14 
 Pct Recovery = 68%  Analysis Date = 01/11/14 
 Pct Recovery = 68%  Analysis Date = 01/09/14 
 Pct Recovery = 68%  Analysis Date = 01/09/14 
 Pct Recovery = 68%  Analysis Date = 01/08/14 
 Pct Recovery = 69%  Analysis Date = 01/08/14 
 Pct Recovery = 69%  Analysis Date = 01/06/14 
 Pct Recovery = 69%  Analysis Date = 01/06/14 
 Pct Recovery = 69%  Analysis Date = 01/04/14 
 Pct Recovery = 69%  Analysis Date = 01/04/14 
 Pct Recovery = 69%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 01/02/14 
 Pct Recovery = 69%  Analysis Date = 01/01/14 
 Pct Recovery = 69%  Analysis Date = 01/01/14 
 Pct Recovery = 69%  Analysis Date = 12/30/13 
 Pct Recovery = 69%  Analysis Date = 12/30/13 
 Pct Recovery = 69%  Analysis Date = 12/28/13 
 Pct Recovery = 69%  Analysis Date = 12/28/13 
 Pct Recovery = 69%  Analysis Date = 12/26/13 
 Pct Recovery = 70%  Analysis Date = 12/26/13 
 Pct Recovery = 70%  Analysis Date = 12/24/13 
 Pct Recovery = 70%  Analysis Date = 12/24/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/23/13 
 Pct Recovery = 70%  Analysis Date = 12/21/13 
 Pct Recovery = 70%  Analysis Date = 12/21/13 
 Pct Recovery = 70%  Analysis Date = 12/19/13 
 Pct Recovery = 70%  Analysis Date = 12/19/13 
 Pct Recovery = 70%  Analysis Date = 12/17/13 
 Pct Recovery = 70%  Analysis Date = 12/17/13 
 Pct Recovery = 70%  Analysis Date = 12/15/13 
 Pct Recovery = 70%  Analysis Date = 12/15/13 
 Pct Recovery = 70%  Analysis Date = 12/14/13 
 Pct Recovery = 71%  Analysis Date = 12/14/13 
 Pct Recovery = 71%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/07/13 
 Pct Recovery = 71%  Analysis Date = 12/07/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/01/13 
 Pct Recovery = 71%  Analysis Date = 12/01/13 
 Pct Recovery = 71%  Analysis Date = 11/29/13 
 Pct Recovery = 71%  Analysis Date = 11/29/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/24/13 
 Pct Recovery = 71%  Analysis Date = 11/24/13 
 Pct Recovery = 71%  Analysis Date = 11/22/13 
 Pct Recovery = 71%  Analysis Date = 11/22/13 
 Pct Recovery = 71%  Analysis Date = 11/20/13 
 Pct Recovery = 71%  Analysis Date = 11/20/13 
 Pct Recovery = 71%  Analysis Date = 11/19/13 
 Pct Recovery = 71%  Analysis Date = 11/19/13 
 Pct Recovery = 71%  Analysis Date = 11/17/13 
 Pct Recovery = 71%  Analysis Date = 11/17/13 
 Pct Recovery = 71%  Analysis Date = 11/15/13 
 Pct Recovery = 71%  Analysis Date = 11/15/13 
 Pct Recovery = 71%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/12/13 
 Pct Recovery = 71%  Analysis Date = 11/12/13 
 Pct Recovery = 71%  Analysis Date = 11/10/13 
 Pct Recovery = 71%  Analysis Date = 11/10/13 
 Pct Recovery = 71%  Analysis Date = 11/08/13 
 Pct Recovery = 71%  Analysis Date = 11/08/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/03/13 
 Pct Recovery = 71%  Analysis Date = 11/03/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 70%  Analysis Date = 10/30/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/26/13 
 Pct Recovery = 70%  Analysis Date = 10/25/13 
 Pct Recovery = 70%  Analysis Date = 10/25/13 
 Pct Recovery = 70%  Analysis Date = 10/23/13 
 Pct Recovery = 70%  Analysis Date = 10/23/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/21/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/19/13 
 Pct Recovery = 70%  Analysis Date = 10/18/13 
 Pct Recovery = 70%  Analysis Date = 10/18/13 
 Pct Recovery = 70%  Analysis Date = 10/16/13 
 Pct Recovery = 70%  Analysis Date = 10/16/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/14/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/12/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/10/13 
 Pct Recovery = 70%  Analysis Date = 10/09/13 
 Pct Recovery = 70%  Analysis Date = 10/09/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/07/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/05/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/03/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 09/30/13 
 Pct Recovery = 70%  Analysis Date = 09/30/13 
 Pct Recovery = 70%  Analysis Date = 09/28/13 
 Pct Recovery = 70%  Analysis Date = 09/28/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/23/13 
 Pct Recovery = 70%  Analysis Date = 09/23/13 
 Pct Recovery = 70%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/17/13 
 Pct Recovery = 69%  Analysis Date = 09/17/13 
 Pct Recovery = 69%  Analysis Date = 09/15/13 
 Pct Recovery = 69%  Analysis Date = 09/15/13 
 Pct Recovery = 69%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/10/13 
 Pct Recovery = 69%  Analysis Date = 09/10/13 
 Pct Recovery = 69%  Analysis Date = 09/08/13 
 Pct Recovery = 69%  Analysis Date = 09/08/13 
 Pct Recovery = 69%  Analysis Date = 09/06/13 
 Pct Recovery = 69%  Analysis Date = 09/06/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/03/13 
 Pct Recovery = 69%  Analysis Date = 09/03/13 
 Pct Recovery = 69%  Analysis Date = 09/01/13 
 Pct Recovery = 69%  Analysis Date = 09/01/13 
 Pct Recovery = 69%  Analysis Date = 08/30/13 
 Pct Recovery = 69%  Analysis Date = 08/30/13 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 Pct Recovery = 69%  Analysis Date = 08/29/13 
 Pct Recovery = 69%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/27/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/25/13 
 Pct Recovery = 69%  Analysis Date = 08/23/13 
 Pct Recovery = 69%  Analysis Date = 08/23/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/20/13 
 Pct Recovery = 69%  Analysis Date = 08/20/13 
 Pct Recovery = 69%  Analysis Date = 08/18/13 
 Pct Recovery = 69%  Analysis Date = 08/18/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/13/13 
 Pct Recovery = 69%  Analysis Date = 08/13/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 68%  Analysis Date = 08/11/13 
 Pct Recovery = 68%  Analysis Date = 08/09/13 
 Pct Recovery = 68%  Analysis Date = 08/09/13 
 Pct Recovery = 68%  Analysis Date = 08/07/13 
 Pct Recovery = 68%  Analysis Date = 08/07/13 
 Pct Recovery = 68%  Analysis Date = 08/05/13 
 Pct Recovery = 68%  Analysis Date = 08/05/13 
 Pct Recovery = 68%  Analysis Date = 08/04/13 
 Pct Recovery = 68%  Analysis Date = 08/04/13 
 Pct Recovery = 68%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 07/31/13 
 Pct Recovery = 68%  Analysis Date = 07/31/13 
 Pct Recovery = 68%  Analysis Date = 07/29/13 
 Pct Recovery = 68%  Analysis Date = 07/29/13 
 Pct Recovery = 68%  Analysis Date = 07/27/13 
 Pct Recovery = 68%  Analysis Date = 07/27/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/24/13 
 Pct Recovery = 68%  Analysis Date = 07/24/13 
 Pct Recovery = 68%  Analysis Date = 07/22/13 
 Pct Recovery = 68%  Analysis Date = 07/22/13 
 Pct Recovery = 68%  Analysis Date = 07/20/13 
 Pct Recovery = 68%  Analysis Date = 07/20/13 
 Pct Recovery = 68%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/19/13 
 Pct Recovery = 68%  Analysis Date = 07/17/13 
 Pct Recovery = 68%  Analysis Date = 07/17/13 
 Pct Recovery = 68%  Analysis Date = 07/15/13 
 Pct Recovery = 68%  Analysis Date = 07/15/13 
 Pct Recovery = 68%  Analysis Date = 07/13/13 
 Pct Recovery = 68%  Analysis Date = 07/13/13 
 Pct Recovery = 68%  Analysis Date = 07/11/13 
 Pct Recovery = 68%  Analysis Date = 07/11/13 
 Pct Recovery = 68%  Analysis Date = 07/10/13 
 Pct Recovery = 68%  Analysis Date = 07/10/13 
 Pct Recovery = 68%  Analysis Date = 07/08/13 
 Pct Recovery = 68%  Analysis Date = 07/08/13 
 Pct Recovery = 68%  Analysis Date = 07/06/13 
 Pct Recovery = 68%  Analysis Date = 07/06/13 
 Pct Recovery = 68%  Analysis Date = 07/04/13 
 Pct Recovery = 68%  Analysis Date = 07/04/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/01/13 
 Pct Recovery = 67%  Analysis Date = 07/01/13 
 Pct Recovery = 67%  Analysis Date = 06/29/13 
 Pct Recovery = 67%  Analysis Date = 06/29/13 
 Pct Recovery = 67%  Analysis Date = 06/27/13 
 Pct Recovery = 67%  Analysis Date = 06/27/13 
 Pct Recovery = 67%  Analysis Date = 06/25/13 
 Pct Recovery = 67%  Analysis Date = 06/25/13 
 Pct Recovery = 67%  Analysis Date = 06/24/13 
 Pct Recovery = 67%  Analysis Date = 06/24/13 
 Pct Recovery = 67%  Analysis Date = 06/22/13 
 Pct Recovery = 67%  Analysis Date = 06/22/13 
 Pct Recovery = 67%  Analysis Date = 06/20/13 
 Pct Recovery = 67%  Analysis Date = 06/20/13 
 Pct Recovery = 67%  Analysis Date = 06/18/13 
 Pct Recovery = 67%  Analysis Date = 06/18/13 
 Pct Recovery = 67%  Analysis Date = 06/16/13 
 Pct Recovery = 67%  Analysis Date = 06/16/13 
 Pct Recovery = 67%  Analysis Date = 06/15/13 
 Pct Recovery = 67%  Analysis Date = 06/15/13 
 Pct Recovery = 67%  Analysis Date = 06/13/13 
 Pct Recovery = 67%  Analysis Date = 06/13/13 
 Pct Recovery = 67%  Analysis Date = 06/11/13 
 Pct Recovery = 67%  Analysis Date = 06/11/13 
 Pct Recovery = 67%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/06/13 
 Pct Recovery = 67%  Analysis Date = 06/06/13 
 Pct Recovery = 67%  Analysis Date = 06/04/13 
 Pct Recovery = 67%  Analysis Date = 06/04/13 
 Pct Recovery = 67%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 06/02/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 67%  Analysis Date = 05/30/13 
 Pct Recovery = 67%  Analysis Date = 05/30/13 
 Pct Recovery = 67%  Analysis Date = 05/28/13 
 Pct Recovery = 67%  Analysis Date = 05/28/13 
 Pct Recovery = 67%  Analysis Date = 05/26/13 
 Pct Recovery = 67%  Analysis Date = 05/26/13 
 Pct Recovery = 67%  Analysis Date = 05/24/13 
 Pct Recovery = 67%  Analysis Date = 05/24/13 
 Pct Recovery = 67%  Analysis Date = 05/22/13 
 Pct Recovery = 66%  Analysis Date = 05/22/13 
 Pct Recovery = 66%  Analysis Date = 05/21/13 
 Pct Recovery = 66%  Analysis Date = 05/21/13 
 Pct Recovery = 66%  Analysis Date = 05/19/13 
 Pct Recovery = 66%  Analysis Date = 05/19/13 
 Pct Recovery = 66%  Analysis Date = 05/17/13 
 Pct Recovery = 66%  Analysis Date = 05/17/13 
 Pct Recovery = 66%  Analysis Date = 05/15/13 
 Pct Recovery = 66%  Analysis Date = 05/15/13 
 Pct Recovery = 66%  Analysis Date = 05/13/13 
 Pct Recovery = 66%  Analysis Date = 05/13/13 
 Pct Recovery = 66%  Analysis Date = 05/12/13 
 Pct Recovery = 66%  Analysis Date = 05/12/13 
 Pct Recovery = 66%  Analysis Date = 05/10/13 
 Pct Recovery = 66%  Analysis Date = 05/10/13 
 Pct Recovery = 66%  Analysis Date = 05/08/13 
 Pct Recovery = 66%  Analysis Date = 05/08/13 
 Pct Recovery = 66%  Analysis Date = 05/06/13 
 Pct Recovery = 66%  Analysis Date = 05/06/13 
 Pct Recovery = 66%  Analysis Date = 05/05/13 
 Pct Recovery = 66%  Analysis Date = 05/05/13 
 Pct Recovery = 66%  Analysis Date = 05/03/13 
 Pct Recovery = 66%  Analysis Date = 05/03/13 
 Pct Recovery = 66%  Analysis Date = 05/01/13 
 Pct Recovery = 65%  Analysis Date = 05/01/13 
 Pct Recovery = 65%  Analysis Date = 04/29/13 
 Pct Recovery = 64%  Analysis Date = 04/29/13 
 Pct Recovery = 64%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/26/13 
 Pct Recovery = 62%  Analysis Date = 04/26/13 
 Pct Recovery = 62%  Analysis Date = 04/24/13 
 Pct Recovery = 62%  Analysis Date = 04/24/13 
 Pct Recovery = 62%  Analysis Date = 04/22/13 
 Pct Recovery = 61%  Analysis Date = 04/22/13 
 Pct Recovery = 61%  Analysis Date = 04/20/13 
 Pct Recovery = 60%  Analysis Date = 04/20/13 
 Pct Recovery = 60%  Analysis Date = 04/18/13 
 Pct Recovery = 59%  Analysis Date = 04/18/13 
 Pct Recovery = 59%  Analysis Date = 04/17/13 
 Pct Recovery = 58%  Analysis Date = 04/17/13 
 Pct Recovery = 58%  Analysis Date = 04/15/13 
 Pct Recovery = 57%  Analysis Date = 04/15/13 
 Pct Recovery = 57%  Analysis Date = 04/13/13 
 Pct Recovery = 56%  Analysis Date = 04/13/13 
 Pct Recovery = 56%  Analysis Date = 04/11/13 
 Pct Recovery = 55%  Analysis Date = 04/11/13 
 Pct Recovery = 55%  Analysis Date = 04/10/13 
 Pct Recovery = 54%  Analysis Date = 04/10/13 
 Pct Recovery = 54%  Analysis Date = 04/08/13 
 Pct Recovery = 53%  Analysis Date = 04/08/13 
 Pct Recovery = 53%  Analysis Date = 04/06/13 
 Pct Recovery = 52%  Analysis Date = 04/06/13 
 Pct Recovery = 52%  Analysis Date = 04/04/13 
 Pct Recovery = 51%  Analysis Date = 04/04/13 
 Pct Recovery = 51%  Analysis Date = 04/02/13 
 Pct Recovery = 51%  Analysis Date = 04/02/13 
 Pct Recovery = 51%  Analysis Date = 04/01/13 
 Pct Recovery = 50%  Analysis Date = 04/01/13 
 Pct Recovery = 50%  Analysis Date = 03/30/13 
 Pct Recovery = 49%  Analysis Date = 03/30/13 
 Pct Recovery = 49%  Analysis Date = 03/28/13 
 Pct Recovery = 48%  Analysis Date = 03/28/13 
 Pct Recovery = 48%  Analysis Date = 03/26/13 
 Pct Recovery = 47%  Analysis Date = 03/26/13 
 Pct Recovery = 47%  Analysis Date = 03/24/13 
 Pct Recovery = 48%  Analysis Date = 03/24/13 
 Pct Recovery = 48%  Analysis Date = 03/23/13 
 Pct Recovery = 48%  Analysis Date = 03/23/13 
 Pct Recovery = 48%  Analysis Date = 03/21/13 
 Pct Recovery = 49%  Analysis Date = 03/21/13 
 Pct Recovery = 49%  Analysis Date = 03/19/13 
 Pct Recovery = 50%  Analysis Date = 03/19/13 
 Pct Recovery = 50%  Analysis Date = 03/17/13 
 Pct Recovery = 50%  Analysis Date = 03/17/13 
 Pct Recovery = 50%  Analysis Date = 03/16/13 
 Pct Recovery = 51%  Analysis Date = 03/16/13 
 Pct Recovery = 51%  Analysis Date = 03/14/13 
 Pct Recovery = 51%  Analysis Date = 03/14/13 
 Pct Recovery = 51%  Analysis Date = 03/12/13 
 Pct Recovery = 52%  Analysis Date = 03/12/13 
 Pct Recovery = 52%  Analysis Date = 03/10/13 
 Pct Recovery = 53%  Analysis Date = 03/10/13 
 Pct Recovery = 53%  Analysis Date = 03/08/13 
 Pct Recovery = 53%  Analysis Date = 03/08/13 
 Pct Recovery = 53%  Analysis Date = 03/07/13 
 Pct Recovery = 54%  Analysis Date = 03/07/13 
 Pct Recovery = 54%  Analysis Date = 03/05/13 
 Pct Recovery = 55%  Analysis Date = 03/05/13 
 Pct Recovery = 55%  Analysis Date = 03/03/13 
 Pct Recovery = 55%  Analysis Date = 03/03/13 
 Pct Recovery = 55%  Analysis Date = 03/01/13 
 Pct Recovery = 56%  Analysis Date = 03/01/13 
 Pct Recovery = 56%  Analysis Date = 02/28/13 
 Pct Recovery = 57%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHADONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 57% . 57% 0%
>= Reporting Level 5 62% 9% 65% 4%
Total 6 61% 9% 63% 7%

Sample Statistics
METHADONE

Characteristic N % % Basis
Plotted 6 86% Spiked
Estimated Values 1 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 1 14% 1 out of 7
Not Spiked 25 .  
False Positives 0 0% 0 out of 24

OBSP Determination:
METHOCARBAMOL
METHOD: LC9017 , TESTIDCODE: 67501LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Spex Organics T1120802015: 40 µl 
 Pct Recovery = 99%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 105%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl 
 Pct Recovery = 61%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 61%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 112%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 71%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 56%  Analysis Date = 03/21/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/18/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 68%  Analysis Date = 03/14/14 
 Pct Recovery = 68%  Analysis Date = 03/14/14 
 Pct Recovery = 68%  Analysis Date = 03/11/14 
 Pct Recovery = 68%  Analysis Date = 03/11/14 
 Pct Recovery = 68%  Analysis Date = 03/09/14 
 Pct Recovery = 68%  Analysis Date = 03/09/14 
 Pct Recovery = 68%  Analysis Date = 03/07/14 
 Pct Recovery = 68%  Analysis Date = 03/07/14 
 Pct Recovery = 68%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/21/14 
 Pct Recovery = 67%  Analysis Date = 02/21/14 
 Pct Recovery = 67%  Analysis Date = 02/18/14 
 Pct Recovery = 67%  Analysis Date = 02/18/14 
 Pct Recovery = 67%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/14/14 
 Pct Recovery = 67%  Analysis Date = 02/14/14 
 Pct Recovery = 67%  Analysis Date = 02/12/14 
 Pct Recovery = 67%  Analysis Date = 02/12/14 
 Pct Recovery = 67%  Analysis Date = 02/09/14 
 Pct Recovery = 67%  Analysis Date = 02/09/14 
 Pct Recovery = 67%  Analysis Date = 02/07/14 
 Pct Recovery = 67%  Analysis Date = 02/07/14 
 Pct Recovery = 67%  Analysis Date = 02/05/14 
 Pct Recovery = 67%  Analysis Date = 02/05/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 02/02/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/31/14 
 Pct Recovery = 67%  Analysis Date = 01/29/14 
 Pct Recovery = 66%  Analysis Date = 01/29/14 
 Pct Recovery = 66%  Analysis Date = 01/26/14 
 Pct Recovery = 66%  Analysis Date = 01/26/14 
 Pct Recovery = 66%  Analysis Date = 01/24/14 
 Pct Recovery = 66%  Analysis Date = 01/24/14 
 Pct Recovery = 66%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/19/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/17/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/08/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/06/14 
 Pct Recovery = 66%  Analysis Date = 01/03/14 
 Pct Recovery = 66%  Analysis Date = 01/03/14 
 Pct Recovery = 66%  Analysis Date = 01/01/14 
 Pct Recovery = 66%  Analysis Date = 01/01/14 
 Pct Recovery = 66%  Analysis Date = 12/30/13 
 Pct Recovery = 65%  Analysis Date = 12/30/13 
 Pct Recovery = 65%  Analysis Date = 12/27/13 
 Pct Recovery = 65%  Analysis Date = 12/27/13 
 Pct Recovery = 65%  Analysis Date = 12/25/13 
 Pct Recovery = 65%  Analysis Date = 12/25/13 
 Pct Recovery = 65%  Analysis Date = 12/23/13 
 Pct Recovery = 65%  Analysis Date = 12/23/13 
 Pct Recovery = 65%  Analysis Date = 12/20/13 
 Pct Recovery = 65%  Analysis Date = 12/20/13 
 Pct Recovery = 65%  Analysis Date = 12/18/13 
 Pct Recovery = 65%  Analysis Date = 12/18/13 
 Pct Recovery = 65%  Analysis Date = 12/16/13 
 Pct Recovery = 65%  Analysis Date = 12/16/13 
 Pct Recovery = 65%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/13/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/11/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/09/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/07/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/04/13 
 Pct Recovery = 65%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 12/02/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/27/13 
 Pct Recovery = 64%  Analysis Date = 11/27/13 
 Pct Recovery = 64%  Analysis Date = 11/25/13 
 Pct Recovery = 64%  Analysis Date = 11/25/13 
 Pct Recovery = 64%  Analysis Date = 11/23/13 
 Pct Recovery = 64%  Analysis Date = 11/23/13 
 Pct Recovery = 64%  Analysis Date = 11/20/13 
 Pct Recovery = 64%  Analysis Date = 11/20/13 
 Pct Recovery = 64%  Analysis Date = 11/18/13 
 Pct Recovery = 64%  Analysis Date = 11/18/13 
 Pct Recovery = 64%  Analysis Date = 11/16/13 
 Pct Recovery = 64%  Analysis Date = 11/16/13 
 Pct Recovery = 64%  Analysis Date = 11/13/13 
 Pct Recovery = 65%  Analysis Date = 11/13/13 
 Pct Recovery = 65%  Analysis Date = 11/11/13 
 Pct Recovery = 65%  Analysis Date = 11/11/13 
 Pct Recovery = 65%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/07/13 
 Pct Recovery = 65%  Analysis Date = 11/07/13 
 Pct Recovery = 65%  Analysis Date = 11/04/13 
 Pct Recovery = 65%  Analysis Date = 11/04/13 
 Pct Recovery = 65%  Analysis Date = 11/02/13 
 Pct Recovery = 65%  Analysis Date = 11/02/13 
 Pct Recovery = 65%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/26/13 
 Pct Recovery = 66%  Analysis Date = 10/26/13 
 Pct Recovery = 66%  Analysis Date = 10/24/13 
 Pct Recovery = 66%  Analysis Date = 10/24/13 
 Pct Recovery = 66%  Analysis Date = 10/21/13 
 Pct Recovery = 66%  Analysis Date = 10/21/13 
 Pct Recovery = 66%  Analysis Date = 10/19/13 
 Pct Recovery = 66%  Analysis Date = 10/19/13 
 Pct Recovery = 66%  Analysis Date = 10/17/13 
 Pct Recovery = 67%  Analysis Date = 10/17/13 
 Pct Recovery = 67%  Analysis Date = 10/14/13 
 Pct Recovery = 67%  Analysis Date = 10/14/13 
 Pct Recovery = 67%  Analysis Date = 10/12/13 
 Pct Recovery = 67%  Analysis Date = 10/12/13 
 Pct Recovery = 67%  Analysis Date = 10/10/13 
 Pct Recovery = 67%  Analysis Date = 10/10/13 
 Pct Recovery = 67%  Analysis Date = 10/07/13 
 Pct Recovery = 67%  Analysis Date = 10/07/13 
 Pct Recovery = 67%  Analysis Date = 10/05/13 
 Pct Recovery = 68%  Analysis Date = 10/05/13 
 Pct Recovery = 68%  Analysis Date = 10/03/13 
 Pct Recovery = 68%  Analysis Date = 10/03/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 09/28/13 
 Pct Recovery = 68%  Analysis Date = 09/28/13 
 Pct Recovery = 68%  Analysis Date = 09/26/13 
 Pct Recovery = 68%  Analysis Date = 09/26/13 
 Pct Recovery = 68%  Analysis Date = 09/24/13 
 Pct Recovery = 68%  Analysis Date = 09/24/13 
 Pct Recovery = 68%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/17/13 
 Pct Recovery = 69%  Analysis Date = 09/17/13 
 Pct Recovery = 69%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/10/13 
 Pct Recovery = 70%  Analysis Date = 09/10/13 
 Pct Recovery = 70%  Analysis Date = 09/07/13 
 Pct Recovery = 70%  Analysis Date = 09/07/13 
 Pct Recovery = 70%  Analysis Date = 09/05/13 
 Pct Recovery = 70%  Analysis Date = 09/05/13 
 Pct Recovery = 70%  Analysis Date = 09/03/13 
 Pct Recovery = 70%  Analysis Date = 09/03/13 
 Pct Recovery = 70%  Analysis Date = 09/01/13 
 Pct Recovery = 70%  Analysis Date = 09/01/13 
 Pct Recovery = 70%  Analysis Date = 08/29/13 
 Pct Recovery = 70%  Analysis Date = 08/29/13 
 Pct Recovery = 70%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/27/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/25/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/22/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/20/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 Pct Recovery = 71%  Analysis Date = 08/15/13 
 Pct Recovery = 72%  Analysis Date = 08/15/13 
 Pct Recovery = 72%  Analysis Date = 08/13/13 
 Pct Recovery = 72%  Analysis Date = 08/13/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 72%  Analysis Date = 08/08/13 
 Pct Recovery = 72%  Analysis Date = 08/08/13 
 Pct Recovery = 72%  Analysis Date = 08/06/13 
 Pct Recovery = 72%  Analysis Date = 08/06/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/23/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/19/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/12/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/07/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/05/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/30/13 
 Pct Recovery = 75%  Analysis Date = 06/28/13 
 Pct Recovery = 76%  Analysis Date = 06/28/13 
 Pct Recovery = 76%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/26/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/16/13 
 Pct Recovery = 76%  Analysis Date = 06/16/13 
 Pct Recovery = 76%  Analysis Date = 06/14/13 
 Pct Recovery = 77%  Analysis Date = 06/14/13 
 Pct Recovery = 77%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/02/13 
 Pct Recovery = 78%  Analysis Date = 06/02/13 
 Pct Recovery = 78%  Analysis Date = 05/31/13 
 Pct Recovery = 78%  Analysis Date = 05/31/13 
 Pct Recovery = 78%  Analysis Date = 05/29/13 
 Pct Recovery = 78%  Analysis Date = 05/29/13 
 Pct Recovery = 78%  Analysis Date = 05/27/13 
 Pct Recovery = 78%  Analysis Date = 05/27/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/20/13 
 Pct Recovery = 79%  Analysis Date = 05/20/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/15/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/13/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/08/13 
 Pct Recovery = 80%  Analysis Date = 05/08/13 
 Pct Recovery = 80%  Analysis Date = 05/06/13 
 Pct Recovery = 80%  Analysis Date = 05/06/13 
 Pct Recovery = 80%  Analysis Date = 05/03/13 
 Pct Recovery = 80%  Analysis Date = 05/03/13 
 Pct Recovery = 80%  Analysis Date = 05/01/13 
 Pct Recovery = 81%  Analysis Date = 05/01/13 
 Pct Recovery = 81%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/29/13 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 Pct Recovery = 83%  Analysis Date = 04/26/13 
 Pct Recovery = 83%  Analysis Date = 04/24/13 
 Pct Recovery = 84%  Analysis Date = 04/24/13 
 Pct Recovery = 84%  Analysis Date = 04/22/13 
 Pct Recovery = 85%  Analysis Date = 04/22/13 
 Pct Recovery = 85%  Analysis Date = 04/20/13 
 Pct Recovery = 86%  Analysis Date = 04/20/13 
 Pct Recovery = 86%  Analysis Date = 04/17/13 
 Pct Recovery = 88%  Analysis Date = 04/17/13 
 Pct Recovery = 88%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/15/13 
 Pct Recovery = 89%  Analysis Date = 04/13/13 
 Pct Recovery = 90%  Analysis Date = 04/13/13 
 Pct Recovery = 90%  Analysis Date = 04/10/13 
 Pct Recovery = 91%  Analysis Date = 04/10/13 
 Pct Recovery = 91%  Analysis Date = 04/08/13 
 Pct Recovery = 92%  Analysis Date = 04/08/13 
 Pct Recovery = 92%  Analysis Date = 04/06/13 
 Pct Recovery = 93%  Analysis Date = 04/06/13 
 Pct Recovery = 93%  Analysis Date = 04/03/13 
 Pct Recovery = 94%  Analysis Date = 04/03/13 
 Pct Recovery = 94%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/27/13 
 Pct Recovery = 98%  Analysis Date = 03/27/13 
 Pct Recovery = 98%  Analysis Date = 03/25/13 
 Pct Recovery = 99%  Analysis Date = 03/25/13 
 Pct Recovery = 99%  Analysis Date = 03/23/13 
 Pct Recovery = 100%  Analysis Date = 03/23/13 
 Pct Recovery = 100%  Analysis Date = 03/21/13 
 Pct Recovery = 101%  Analysis Date = 03/21/13 
 Pct Recovery = 101%  Analysis Date = 03/18/13 
 Pct Recovery = 102%  Analysis Date = 03/18/13 
 Pct Recovery = 102%  Analysis Date = 03/16/13 
 Pct Recovery = 103%  Analysis Date = 03/16/13 
 Pct Recovery = 103%  Analysis Date = 03/14/13 
 Pct Recovery = 105%  Analysis Date = 03/14/13 
 Pct Recovery = 105%  Analysis Date = 03/11/13 
 Pct Recovery = 106%  Analysis Date = 03/11/13 
 Pct Recovery = 106%  Analysis Date = 03/09/13 
 Pct Recovery = 107%  Analysis Date = 03/09/13 
 Pct Recovery = 107%  Analysis Date = 03/07/13 
 Pct Recovery = 108%  Analysis Date = 03/07/13 
 Pct Recovery = 108%  Analysis Date = 03/04/13 
 Pct Recovery = 109%  Analysis Date = 03/04/13 
 Pct Recovery = 109%  Analysis Date = 03/02/13 
 Pct Recovery = 110%  Analysis Date = 03/02/13 
 Pct Recovery = 110%  Analysis Date = 02/28/13 
 Pct Recovery = 111%  Analysis Date = 02/28/13 
 Pct Recovery = 111%  Analysis Date = 02/25/13 
 Pct Recovery = 110%  Analysis Date = 02/25/13 
 Pct Recovery = 110%  Analysis Date = 02/23/13 
 Pct Recovery = 109%  Analysis Date = 02/23/13 
 Pct Recovery = 109%  Analysis Date = 02/21/13 
 Pct Recovery = 107%  Analysis Date = 02/21/13 
 Pct Recovery = 107%  Analysis Date = 02/18/13 
 Pct Recovery = 106%  Analysis Date = 02/18/13 
 Pct Recovery = 106%  Analysis Date = 02/16/13 
 Pct Recovery = 105%  Analysis Date = 02/16/13 
 Pct Recovery = 105%  Analysis Date = 02/14/13 
 Pct Recovery = 103%  Analysis Date = 02/14/13 
 Pct Recovery = 103%  Analysis Date = 02/12/13 
 Pct Recovery = 102%  Analysis Date = 02/12/13 
 Pct Recovery = 102%  Analysis Date = 02/09/13 
 Pct Recovery = 101%  Analysis Date = 02/09/13 
 Pct Recovery = 101%  Analysis Date = 02/07/13 
 Pct Recovery = 99%  Analysis Date = 02/07/13 
 Pct Recovery = 99%  Analysis Date = 02/05/13 
 Pct Recovery = 98%  Analysis Date = 02/05/13 
 Pct Recovery = 98%  Analysis Date = 02/02/13 
 Pct Recovery = 96%  Analysis Date = 02/02/13 
 Pct Recovery = 96%  Analysis Date = 01/31/13 
 Pct Recovery = 95%  Analysis Date = 01/31/13 
 Pct Recovery = 95%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/29/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 92%  Analysis Date = 01/26/13 
 Pct Recovery = 92%  Analysis Date = 01/24/13 
 Pct Recovery = 91%  Analysis Date = 01/24/13 
 Pct Recovery = 91%  Analysis Date = 01/22/13 
 Pct Recovery = 91%  Analysis Date = 01/22/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/17/13 
 Pct Recovery = 91%  Analysis Date = 01/15/13 
 Pct Recovery = 91%  Analysis Date = 01/15/13 
 Pct Recovery = 91%  Analysis Date = 01/13/13 
 Pct Recovery = 91%  Analysis Date = 01/13/13 
 Pct Recovery = 91%  Analysis Date = 01/10/13 
 Pct Recovery = 91%  Analysis Date = 01/10/13 
 Pct Recovery = 91%  Analysis Date = 01/08/13 
 Pct Recovery = 91%  Analysis Date = 01/08/13 
 Pct Recovery = 91%  Analysis Date = 01/06/13 
 Pct Recovery = 91%  Analysis Date = 01/06/13 
 Pct Recovery = 91%  Analysis Date = 01/03/13 
 Pct Recovery = 91%  Analysis Date = 01/03/13 
 Pct Recovery = 91%  Analysis Date = 01/01/13 
 Pct Recovery = 91%  Analysis Date = 01/01/13 
 Pct Recovery = 91%  Analysis Date = 12/30/12 
 Pct Recovery = 92%  Analysis Date = 12/30/12 
 Pct Recovery = 92%  Analysis Date = 12/27/12 
 Pct Recovery = 92%  Analysis Date = 12/27/12 
 Pct Recovery = 92%  Analysis Date = 12/25/12 
 Pct Recovery = 92%  Analysis Date = 12/25/12 
 Pct Recovery = 92%  Analysis Date = 12/23/12 
 Pct Recovery = 92%  Analysis Date = 12/23/12 
 Pct Recovery = 92%  Analysis Date = 12/20/12 
 Pct Recovery = 92%  Analysis Date = 12/20/12 
 Pct Recovery = 92%  Analysis Date = 12/18/12 
 Pct Recovery = 92%  Analysis Date = 12/18/12 
 Pct Recovery = 92%  Analysis Date = 12/16/12 
 Pct Recovery = 92%  Analysis Date = 12/16/12 
 Pct Recovery = 92%  Analysis Date = 12/14/12 
 Pct Recovery = 92%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOCARBAMOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 8 79% 22% 71% 30%
Total 8 79% 22% 71% 30%

Sample Statistics
METHOCARBAMOL

Characteristic N % % Basis
Plotted 8 73% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 3 27% 3 out of 11
Not Spiked 20 .  
False Positives 0 0% 0 out of 20

OBSP Determination:
METHOTREXATE
METHOD: LC9017 , TESTIDCODE: 67525LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 122%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 117%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 109%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 56%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 33%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 95%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 51%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 57%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 116%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 53%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 53%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 154%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/11/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 58%  Analysis Date = 03/07/14 
 Pct Recovery = 58%  Analysis Date = 03/07/14 
 Pct Recovery = 58%  Analysis Date = 03/04/14 
 Pct Recovery = 58%  Analysis Date = 03/04/14 
 Pct Recovery = 58%  Analysis Date = 03/02/14 
 Pct Recovery = 57%  Analysis Date = 03/02/14 
 Pct Recovery = 57%  Analysis Date = 02/28/14 
 Pct Recovery = 57%  Analysis Date = 02/28/14 
 Pct Recovery = 57%  Analysis Date = 02/25/14 
 Pct Recovery = 57%  Analysis Date = 02/25/14 
 Pct Recovery = 57%  Analysis Date = 02/23/14 
 Pct Recovery = 57%  Analysis Date = 02/23/14 
 Pct Recovery = 57%  Analysis Date = 02/21/14 
 Pct Recovery = 57%  Analysis Date = 02/21/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/14/14 
 Pct Recovery = 57%  Analysis Date = 02/14/14 
 Pct Recovery = 57%  Analysis Date = 02/12/14 
 Pct Recovery = 57%  Analysis Date = 02/12/14 
 Pct Recovery = 57%  Analysis Date = 02/09/14 
 Pct Recovery = 56%  Analysis Date = 02/09/14 
 Pct Recovery = 56%  Analysis Date = 02/07/14 
 Pct Recovery = 56%  Analysis Date = 02/07/14 
 Pct Recovery = 56%  Analysis Date = 02/05/14 
 Pct Recovery = 56%  Analysis Date = 02/05/14 
 Pct Recovery = 56%  Analysis Date = 02/02/14 
 Pct Recovery = 56%  Analysis Date = 02/02/14 
 Pct Recovery = 56%  Analysis Date = 01/31/14 
 Pct Recovery = 56%  Analysis Date = 01/31/14 
 Pct Recovery = 56%  Analysis Date = 01/29/14 
 Pct Recovery = 56%  Analysis Date = 01/29/14 
 Pct Recovery = 56%  Analysis Date = 01/26/14 
 Pct Recovery = 56%  Analysis Date = 01/26/14 
 Pct Recovery = 56%  Analysis Date = 01/24/14 
 Pct Recovery = 56%  Analysis Date = 01/24/14 
 Pct Recovery = 56%  Analysis Date = 01/22/14 
 Pct Recovery = 55%  Analysis Date = 01/22/14 
 Pct Recovery = 55%  Analysis Date = 01/19/14 
 Pct Recovery = 55%  Analysis Date = 01/19/14 
 Pct Recovery = 55%  Analysis Date = 01/17/14 
 Pct Recovery = 55%  Analysis Date = 01/17/14 
 Pct Recovery = 55%  Analysis Date = 01/15/14 
 Pct Recovery = 55%  Analysis Date = 01/15/14 
 Pct Recovery = 55%  Analysis Date = 01/13/14 
 Pct Recovery = 55%  Analysis Date = 01/13/14 
 Pct Recovery = 55%  Analysis Date = 01/10/14 
 Pct Recovery = 55%  Analysis Date = 01/10/14 
 Pct Recovery = 55%  Analysis Date = 01/08/14 
 Pct Recovery = 55%  Analysis Date = 01/08/14 
 Pct Recovery = 55%  Analysis Date = 01/06/14 
 Pct Recovery = 55%  Analysis Date = 01/06/14 
 Pct Recovery = 55%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/03/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 01/01/14 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/30/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/27/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/25/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/23/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/20/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 54%  Analysis Date = 12/18/13 
 Pct Recovery = 54%  Analysis Date = 12/16/13 
 Pct Recovery = 53%  Analysis Date = 12/16/13 
 Pct Recovery = 53%  Analysis Date = 12/13/13 
 Pct Recovery = 53%  Analysis Date = 12/13/13 
 Pct Recovery = 53%  Analysis Date = 12/11/13 
 Pct Recovery = 53%  Analysis Date = 12/11/13 
 Pct Recovery = 53%  Analysis Date = 12/09/13 
 Pct Recovery = 53%  Analysis Date = 12/09/13 
 Pct Recovery = 53%  Analysis Date = 12/07/13 
 Pct Recovery = 53%  Analysis Date = 12/07/13 
 Pct Recovery = 53%  Analysis Date = 12/04/13 
 Pct Recovery = 53%  Analysis Date = 12/04/13 
 Pct Recovery = 53%  Analysis Date = 12/02/13 
 Pct Recovery = 53%  Analysis Date = 12/02/13 
 Pct Recovery = 53%  Analysis Date = 11/30/13 
 Pct Recovery = 53%  Analysis Date = 11/30/13 
 Pct Recovery = 53%  Analysis Date = 11/27/13 
 Pct Recovery = 53%  Analysis Date = 11/27/13 
 Pct Recovery = 53%  Analysis Date = 11/25/13 
 Pct Recovery = 53%  Analysis Date = 11/25/13 
 Pct Recovery = 53%  Analysis Date = 11/23/13 
 Pct Recovery = 53%  Analysis Date = 11/23/13 
 Pct Recovery = 53%  Analysis Date = 11/20/13 
 Pct Recovery = 53%  Analysis Date = 11/20/13 
 Pct Recovery = 53%  Analysis Date = 11/18/13 
 Pct Recovery = 53%  Analysis Date = 11/18/13 
 Pct Recovery = 53%  Analysis Date = 11/16/13 
 Pct Recovery = 53%  Analysis Date = 11/16/13 
 Pct Recovery = 53%  Analysis Date = 11/13/13 
 Pct Recovery = 53%  Analysis Date = 11/13/13 
 Pct Recovery = 53%  Analysis Date = 11/11/13 
 Pct Recovery = 53%  Analysis Date = 11/11/13 
 Pct Recovery = 53%  Analysis Date = 11/09/13 
 Pct Recovery = 52%  Analysis Date = 11/09/13 
 Pct Recovery = 52%  Analysis Date = 11/07/13 
 Pct Recovery = 52%  Analysis Date = 11/07/13 
 Pct Recovery = 52%  Analysis Date = 11/04/13 
 Pct Recovery = 52%  Analysis Date = 11/04/13 
 Pct Recovery = 52%  Analysis Date = 11/02/13 
 Pct Recovery = 52%  Analysis Date = 11/02/13 
 Pct Recovery = 52%  Analysis Date = 10/31/13 
 Pct Recovery = 52%  Analysis Date = 10/31/13 
 Pct Recovery = 52%  Analysis Date = 10/28/13 
 Pct Recovery = 52%  Analysis Date = 10/28/13 
 Pct Recovery = 52%  Analysis Date = 10/26/13 
 Pct Recovery = 52%  Analysis Date = 10/26/13 
 Pct Recovery = 52%  Analysis Date = 10/24/13 
 Pct Recovery = 52%  Analysis Date = 10/24/13 
 Pct Recovery = 52%  Analysis Date = 10/21/13 
 Pct Recovery = 52%  Analysis Date = 10/21/13 
 Pct Recovery = 52%  Analysis Date = 10/19/13 
 Pct Recovery = 52%  Analysis Date = 10/19/13 
 Pct Recovery = 52%  Analysis Date = 10/17/13 
 Pct Recovery = 52%  Analysis Date = 10/17/13 
 Pct Recovery = 52%  Analysis Date = 10/14/13 
 Pct Recovery = 52%  Analysis Date = 10/14/13 
 Pct Recovery = 52%  Analysis Date = 10/12/13 
 Pct Recovery = 52%  Analysis Date = 10/12/13 
 Pct Recovery = 52%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/10/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/07/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/05/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/03/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 10/01/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/28/13 
 Pct Recovery = 52%  Analysis Date = 09/26/13 
 Pct Recovery = 52%  Analysis Date = 09/26/13 
 Pct Recovery = 52%  Analysis Date = 09/24/13 
 Pct Recovery = 52%  Analysis Date = 09/24/13 
 Pct Recovery = 52%  Analysis Date = 09/21/13 
 Pct Recovery = 52%  Analysis Date = 09/21/13 
 Pct Recovery = 52%  Analysis Date = 09/19/13 
 Pct Recovery = 52%  Analysis Date = 09/19/13 
 Pct Recovery = 52%  Analysis Date = 09/17/13 
 Pct Recovery = 52%  Analysis Date = 09/17/13 
 Pct Recovery = 52%  Analysis Date = 09/14/13 
 Pct Recovery = 52%  Analysis Date = 09/14/13 
 Pct Recovery = 52%  Analysis Date = 09/12/13 
 Pct Recovery = 52%  Analysis Date = 09/12/13 
 Pct Recovery = 52%  Analysis Date = 09/10/13 
 Pct Recovery = 52%  Analysis Date = 09/10/13 
 Pct Recovery = 52%  Analysis Date = 09/07/13 
 Pct Recovery = 52%  Analysis Date = 09/07/13 
 Pct Recovery = 52%  Analysis Date = 09/05/13 
 Pct Recovery = 52%  Analysis Date = 09/05/13 
 Pct Recovery = 52%  Analysis Date = 09/03/13 
 Pct Recovery = 51%  Analysis Date = 09/03/13 
 Pct Recovery = 51%  Analysis Date = 09/01/13 
 Pct Recovery = 51%  Analysis Date = 09/01/13 
 Pct Recovery = 51%  Analysis Date = 08/29/13 
 Pct Recovery = 51%  Analysis Date = 08/29/13 
 Pct Recovery = 51%  Analysis Date = 08/27/13 
 Pct Recovery = 51%  Analysis Date = 08/27/13 
 Pct Recovery = 51%  Analysis Date = 08/25/13 
 Pct Recovery = 51%  Analysis Date = 08/25/13 
 Pct Recovery = 51%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/22/13 
 Pct Recovery = 52%  Analysis Date = 08/20/13 
 Pct Recovery = 52%  Analysis Date = 08/20/13 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/18/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/13/13 
 Pct Recovery = 53%  Analysis Date = 08/13/13 
 Pct Recovery = 53%  Analysis Date = 08/11/13 
 Pct Recovery = 53%  Analysis Date = 08/11/13 
 Pct Recovery = 53%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 55%  Analysis Date = 08/06/13 
 Pct Recovery = 55%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/04/13 
 Pct Recovery = 55%  Analysis Date = 08/02/13 
 Pct Recovery = 56%  Analysis Date = 08/02/13 
 Pct Recovery = 56%  Analysis Date = 07/30/13 
 Pct Recovery = 57%  Analysis Date = 07/30/13 
 Pct Recovery = 57%  Analysis Date = 07/28/13 
 Pct Recovery = 58%  Analysis Date = 07/28/13 
 Pct Recovery = 58%  Analysis Date = 07/26/13 
 Pct Recovery = 60%  Analysis Date = 07/26/13 
 Pct Recovery = 60%  Analysis Date = 07/23/13 
 Pct Recovery = 61%  Analysis Date = 07/23/13 
 Pct Recovery = 61%  Analysis Date = 07/21/13 
 Pct Recovery = 62%  Analysis Date = 07/21/13 
 Pct Recovery = 62%  Analysis Date = 07/19/13 
 Pct Recovery = 64%  Analysis Date = 07/19/13 
 Pct Recovery = 64%  Analysis Date = 07/16/13 
 Pct Recovery = 65%  Analysis Date = 07/16/13 
 Pct Recovery = 65%  Analysis Date = 07/14/13 
 Pct Recovery = 66%  Analysis Date = 07/14/13 
 Pct Recovery = 66%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/12/13 
 Pct Recovery = 68%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/07/13 
 Pct Recovery = 70%  Analysis Date = 07/07/13 
 Pct Recovery = 70%  Analysis Date = 07/05/13 
 Pct Recovery = 72%  Analysis Date = 07/05/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 73%  Analysis Date = 07/02/13 
 Pct Recovery = 73%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/30/13 
 Pct Recovery = 74%  Analysis Date = 06/28/13 
 Pct Recovery = 76%  Analysis Date = 06/28/13 
 Pct Recovery = 76%  Analysis Date = 06/26/13 
 Pct Recovery = 77%  Analysis Date = 06/26/13 
 Pct Recovery = 77%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/21/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 81%  Analysis Date = 06/19/13 
 Pct Recovery = 81%  Analysis Date = 06/16/13 
 Pct Recovery = 82%  Analysis Date = 06/16/13 
 Pct Recovery = 82%  Analysis Date = 06/14/13 
 Pct Recovery = 84%  Analysis Date = 06/14/13 
 Pct Recovery = 84%  Analysis Date = 06/12/13 
 Pct Recovery = 85%  Analysis Date = 06/12/13 
 Pct Recovery = 85%  Analysis Date = 06/09/13 
 Pct Recovery = 86%  Analysis Date = 06/09/13 
 Pct Recovery = 86%  Analysis Date = 06/07/13 
 Pct Recovery = 88%  Analysis Date = 06/07/13 
 Pct Recovery = 88%  Analysis Date = 06/05/13 
 Pct Recovery = 89%  Analysis Date = 06/05/13 
 Pct Recovery = 89%  Analysis Date = 06/02/13 
 Pct Recovery = 90%  Analysis Date = 06/02/13 
 Pct Recovery = 90%  Analysis Date = 05/31/13 
 Pct Recovery = 92%  Analysis Date = 05/31/13 
 Pct Recovery = 92%  Analysis Date = 05/29/13 
 Pct Recovery = 93%  Analysis Date = 05/29/13 
 Pct Recovery = 93%  Analysis Date = 05/27/13 
 Pct Recovery = 94%  Analysis Date = 05/27/13 
 Pct Recovery = 94%  Analysis Date = 05/24/13 
 Pct Recovery = 96%  Analysis Date = 05/24/13 
 Pct Recovery = 96%  Analysis Date = 05/22/13 
 Pct Recovery = 97%  Analysis Date = 05/22/13 
 Pct Recovery = 97%  Analysis Date = 05/20/13 
 Pct Recovery = 98%  Analysis Date = 05/20/13 
 Pct Recovery = 98%  Analysis Date = 05/17/13 
 Pct Recovery = 100%  Analysis Date = 05/17/13 
 Pct Recovery = 100%  Analysis Date = 05/15/13 
 Pct Recovery = 101%  Analysis Date = 05/15/13 
 Pct Recovery = 101%  Analysis Date = 05/13/13 
 Pct Recovery = 102%  Analysis Date = 05/13/13 
 Pct Recovery = 102%  Analysis Date = 05/10/13 
 Pct Recovery = 104%  Analysis Date = 05/10/13 
 Pct Recovery = 104%  Analysis Date = 05/08/13 
 Pct Recovery = 105%  Analysis Date = 05/08/13 
 Pct Recovery = 105%  Analysis Date = 05/06/13 
 Pct Recovery = 106%  Analysis Date = 05/06/13 
 Pct Recovery = 106%  Analysis Date = 05/03/13 
 Pct Recovery = 107%  Analysis Date = 05/03/13 
 Pct Recovery = 107%  Analysis Date = 05/01/13 
 Pct Recovery = 108%  Analysis Date = 05/01/13 
 Pct Recovery = 108%  Analysis Date = 04/29/13 
 Pct Recovery = 109%  Analysis Date = 04/29/13 
 Pct Recovery = 109%  Analysis Date = 04/26/13 
 Pct Recovery = 110%  Analysis Date = 04/26/13 
 Pct Recovery = 110%  Analysis Date = 04/24/13 
 Pct Recovery = 111%  Analysis Date = 04/24/13 
 Pct Recovery = 111%  Analysis Date = 04/22/13 
 Pct Recovery = 112%  Analysis Date = 04/22/13 
 Pct Recovery = 112%  Analysis Date = 04/20/13 
 Pct Recovery = 112%  Analysis Date = 04/20/13 
 Pct Recovery = 112%  Analysis Date = 04/17/13 
 Pct Recovery = 113%  Analysis Date = 04/17/13 
 Pct Recovery = 113%  Analysis Date = 04/15/13 
 Pct Recovery = 114%  Analysis Date = 04/15/13 
 Pct Recovery = 114%  Analysis Date = 04/13/13 
 Pct Recovery = 115%  Analysis Date = 04/13/13 
 Pct Recovery = 115%  Analysis Date = 04/10/13 
 Pct Recovery = 116%  Analysis Date = 04/10/13 
 Pct Recovery = 116%  Analysis Date = 04/08/13 
 Pct Recovery = 116%  Analysis Date = 04/08/13 
 Pct Recovery = 116%  Analysis Date = 04/06/13 
 Pct Recovery = 117%  Analysis Date = 04/06/13 
 Pct Recovery = 117%  Analysis Date = 04/03/13 
 Pct Recovery = 118%  Analysis Date = 04/03/13 
 Pct Recovery = 118%  Analysis Date = 04/01/13 
 Pct Recovery = 119%  Analysis Date = 04/01/13 
 Pct Recovery = 119%  Analysis Date = 03/30/13 
 Pct Recovery = 120%  Analysis Date = 03/30/13 
 Pct Recovery = 120%  Analysis Date = 03/27/13 
 Pct Recovery = 120%  Analysis Date = 03/27/13 
 Pct Recovery = 120%  Analysis Date = 03/25/13 
 Pct Recovery = 121%  Analysis Date = 03/25/13 
 Pct Recovery = 121%  Analysis Date = 03/23/13 
 Pct Recovery = 121%  Analysis Date = 03/23/13 
 Pct Recovery = 121%  Analysis Date = 03/21/13 
 Pct Recovery = 121%  Analysis Date = 03/21/13 
 Pct Recovery = 121%  Analysis Date = 03/18/13 
 Pct Recovery = 121%  Analysis Date = 03/18/13 
 Pct Recovery = 121%  Analysis Date = 03/16/13 
 Pct Recovery = 121%  Analysis Date = 03/16/13 
 Pct Recovery = 121%  Analysis Date = 03/14/13 
 Pct Recovery = 121%  Analysis Date = 03/14/13 
 Pct Recovery = 121%  Analysis Date = 03/11/13 
 Pct Recovery = 121%  Analysis Date = 03/11/13 
 Pct Recovery = 121%  Analysis Date = 03/09/13 
 Pct Recovery = 121%  Analysis Date = 03/09/13 
 Pct Recovery = 121%  Analysis Date = 03/07/13 
 Pct Recovery = 121%  Analysis Date = 03/07/13 
 Pct Recovery = 121%  Analysis Date = 03/04/13 
 Pct Recovery = 121%  Analysis Date = 03/04/13 
 Pct Recovery = 121%  Analysis Date = 03/02/13 
 Pct Recovery = 121%  Analysis Date = 03/02/13 
 Pct Recovery = 121%  Analysis Date = 02/28/13 
 Pct Recovery = 121%  Analysis Date = 02/28/13 
 Pct Recovery = 121%  Analysis Date = 02/25/13 
 Pct Recovery = 121%  Analysis Date = 02/25/13 
 Pct Recovery = 121%  Analysis Date = 02/23/13 
 Pct Recovery = 122%  Analysis Date = 02/23/13 
 Pct Recovery = 122%  Analysis Date = 02/21/13 
 Pct Recovery = 122%  Analysis Date = 02/21/13 
 Pct Recovery = 122%  Analysis Date = 02/18/13 
 Pct Recovery = 122%  Analysis Date = 02/18/13 
 Pct Recovery = 122%  Analysis Date = 02/16/13 
 Pct Recovery = 122%  Analysis Date = 02/16/13 
 Pct Recovery = 122%  Analysis Date = 02/14/13 
 Pct Recovery = 122%  Analysis Date = 02/14/13 
 Pct Recovery = 122%  Analysis Date = 02/12/13 
 Pct Recovery = 122%  Analysis Date = 02/12/13 
 Pct Recovery = 122%  Analysis Date = 02/09/13 
 Pct Recovery = 122%  Analysis Date = 02/09/13 
 Pct Recovery = 122%  Analysis Date = 02/07/13 
 Pct Recovery = 122%  Analysis Date = 02/07/13 
 Pct Recovery = 122%  Analysis Date = 02/05/13 
 Pct Recovery = 123%  Analysis Date = 02/05/13 
 Pct Recovery = 123%  Analysis Date = 02/02/13 
 Pct Recovery = 123%  Analysis Date = 02/02/13 
 Pct Recovery = 123%  Analysis Date = 01/31/13 
 Pct Recovery = 123%  Analysis Date = 01/31/13 
 Pct Recovery = 123%  Analysis Date = 01/29/13 
 Pct Recovery = 123%  Analysis Date = 01/29/13 
 Pct Recovery = 123%  Analysis Date = 01/26/13 
 Pct Recovery = 123%  Analysis Date = 01/26/13 
 Pct Recovery = 123%  Analysis Date = 01/24/13 
 Pct Recovery = 123%  Analysis Date = 01/24/13 
 Pct Recovery = 123%  Analysis Date = 01/22/13 
 Pct Recovery = 123%  Analysis Date = 01/22/13 
 Pct Recovery = 123%  Analysis Date = 01/19/13 
 Pct Recovery = 123%  Analysis Date = 01/19/13 
 Pct Recovery = 123%  Analysis Date = 01/17/13 
 Pct Recovery = 124%  Analysis Date = 01/17/13 
 Pct Recovery = 124%  Analysis Date = 01/15/13 
 Pct Recovery = 124%  Analysis Date = 01/15/13 
 Pct Recovery = 124%  Analysis Date = 01/13/13 
 Pct Recovery = 124%  Analysis Date = 01/13/13 
 Pct Recovery = 124%  Analysis Date = 01/10/13 
 Pct Recovery = 124%  Analysis Date = 01/10/13 
 Pct Recovery = 124%  Analysis Date = 01/08/13 
 Pct Recovery = 124%  Analysis Date = 01/08/13 
 Pct Recovery = 124%  Analysis Date = 01/06/13 
 Pct Recovery = 124%  Analysis Date = 01/06/13 
 Pct Recovery = 124%  Analysis Date = 01/03/13 
 Pct Recovery = 124%  Analysis Date = 01/03/13 
 Pct Recovery = 124%  Analysis Date = 01/01/13 
 Pct Recovery = 124%  Analysis Date = 01/01/13 
 Pct Recovery = 124%  Analysis Date = 12/30/12 
 Pct Recovery = 125%  Analysis Date = 12/30/12 
 Pct Recovery = 125%  Analysis Date = 12/27/12 
 Pct Recovery = 125%  Analysis Date = 12/27/12 
 Pct Recovery = 125%  Analysis Date = 12/25/12 
 Pct Recovery = 125%  Analysis Date = 12/25/12 
 Pct Recovery = 125%  Analysis Date = 12/23/12 
 Pct Recovery = 125%  Analysis Date = 12/23/12 
 Pct Recovery = 125%  Analysis Date = 12/20/12 
 Pct Recovery = 125%  Analysis Date = 12/20/12 
 Pct Recovery = 125%  Analysis Date = 12/18/12 
 Pct Recovery = 125%  Analysis Date = 12/18/12 
 Pct Recovery = 125%  Analysis Date = 12/16/12 
 Pct Recovery = 125%  Analysis Date = 12/16/12 
 Pct Recovery = 125%  Analysis Date = 12/14/12 
 Pct Recovery = 125%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOTREXATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 83% 37% 65% 47%
Total 13 83% 37% 65% 47%

Sample Statistics
METHOTREXATE

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 13 87% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
METHYL-1H-BENZOTRIAZOLE
METHOD: LC9017 , TESTIDCODE: 67514LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 93%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 99%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 56%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 79%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 78%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 102%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 100%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 84%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 72%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 87%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 110%  Analysis Date = 04/09/14 
 Pct Recovery = 67%  Analysis Date = 04/07/14 
 Pct Recovery = 67%  Analysis Date = 04/07/14 
 Pct Recovery = 67%  Analysis Date = 04/05/14 
 Pct Recovery = 67%  Analysis Date = 04/05/14 
 Pct Recovery = 67%  Analysis Date = 04/02/14 
 Pct Recovery = 68%  Analysis Date = 04/02/14 
 Pct Recovery = 68%  Analysis Date = 03/31/14 
 Pct Recovery = 68%  Analysis Date = 03/31/14 
 Pct Recovery = 68%  Analysis Date = 03/28/14 
 Pct Recovery = 68%  Analysis Date = 03/28/14 
 Pct Recovery = 68%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 71%  Analysis Date = 03/04/14 
 Pct Recovery = 71%  Analysis Date = 03/02/14 
 Pct Recovery = 71%  Analysis Date = 03/02/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 72%  Analysis Date = 02/23/14 
 Pct Recovery = 72%  Analysis Date = 02/20/14 
 Pct Recovery = 72%  Analysis Date = 02/20/14 
 Pct Recovery = 72%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 73%  Analysis Date = 02/13/14 
 Pct Recovery = 73%  Analysis Date = 02/11/14 
 Pct Recovery = 73%  Analysis Date = 02/11/14 
 Pct Recovery = 73%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/20/14 
 Pct Recovery = 75%  Analysis Date = 01/20/14 
 Pct Recovery = 75%  Analysis Date = 01/18/14 
 Pct Recovery = 75%  Analysis Date = 01/18/14 
 Pct Recovery = 75%  Analysis Date = 01/15/14 
 Pct Recovery = 75%  Analysis Date = 01/15/14 
 Pct Recovery = 75%  Analysis Date = 01/13/14 
 Pct Recovery = 76%  Analysis Date = 01/13/14 
 Pct Recovery = 76%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/15/13 
 Pct Recovery = 77%  Analysis Date = 12/15/13 
 Pct Recovery = 77%  Analysis Date = 12/12/13 
 Pct Recovery = 77%  Analysis Date = 12/12/13 
 Pct Recovery = 77%  Analysis Date = 12/10/13 
 Pct Recovery = 77%  Analysis Date = 12/10/13 
 Pct Recovery = 77%  Analysis Date = 12/08/13 
 Pct Recovery = 77%  Analysis Date = 12/08/13 
 Pct Recovery = 77%  Analysis Date = 12/05/13 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 Pct Recovery = 78%  Analysis Date = 12/03/13 
 Pct Recovery = 78%  Analysis Date = 12/03/13 
 Pct Recovery = 78%  Analysis Date = 11/30/13 
 Pct Recovery = 77%  Analysis Date = 11/30/13 
 Pct Recovery = 77%  Analysis Date = 11/28/13 
 Pct Recovery = 77%  Analysis Date = 11/28/13 
 Pct Recovery = 77%  Analysis Date = 11/26/13 
 Pct Recovery = 77%  Analysis Date = 11/26/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/13/13 
 Pct Recovery = 77%  Analysis Date = 11/13/13 
 Pct Recovery = 77%  Analysis Date = 11/11/13 
 Pct Recovery = 77%  Analysis Date = 11/11/13 
 Pct Recovery = 77%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 77%  Analysis Date = 10/23/13 
 Pct Recovery = 77%  Analysis Date = 10/20/13 
 Pct Recovery = 77%  Analysis Date = 10/20/13 
 Pct Recovery = 77%  Analysis Date = 10/18/13 
 Pct Recovery = 77%  Analysis Date = 10/18/13 
 Pct Recovery = 77%  Analysis Date = 10/16/13 
 Pct Recovery = 77%  Analysis Date = 10/16/13 
 Pct Recovery = 77%  Analysis Date = 10/13/13 
 Pct Recovery = 77%  Analysis Date = 10/13/13 
 Pct Recovery = 77%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/04/13 
 Pct Recovery = 78%  Analysis Date = 10/04/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/26/13 
 Pct Recovery = 81%  Analysis Date = 08/26/13 
 Pct Recovery = 81%  Analysis Date = 08/24/13 
 Pct Recovery = 81%  Analysis Date = 08/24/13 
 Pct Recovery = 81%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/16/13 
 Pct Recovery = 82%  Analysis Date = 08/16/13 
 Pct Recovery = 82%  Analysis Date = 08/14/13 
 Pct Recovery = 82%  Analysis Date = 08/14/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/09/13 
 Pct Recovery = 83%  Analysis Date = 08/09/13 
 Pct Recovery = 83%  Analysis Date = 08/07/13 
 Pct Recovery = 83%  Analysis Date = 08/07/13 
 Pct Recovery = 83%  Analysis Date = 08/04/13 
 Pct Recovery = 83%  Analysis Date = 08/04/13 
 Pct Recovery = 83%  Analysis Date = 08/02/13 
 Pct Recovery = 83%  Analysis Date = 08/02/13 
 Pct Recovery = 83%  Analysis Date = 07/30/13 
 Pct Recovery = 83%  Analysis Date = 07/30/13 
 Pct Recovery = 83%  Analysis Date = 07/28/13 
 Pct Recovery = 84%  Analysis Date = 07/28/13 
 Pct Recovery = 84%  Analysis Date = 07/26/13 
 Pct Recovery = 84%  Analysis Date = 07/26/13 
 Pct Recovery = 84%  Analysis Date = 07/23/13 
 Pct Recovery = 84%  Analysis Date = 07/23/13 
 Pct Recovery = 84%  Analysis Date = 07/21/13 
 Pct Recovery = 85%  Analysis Date = 07/21/13 
 Pct Recovery = 85%  Analysis Date = 07/18/13 
 Pct Recovery = 85%  Analysis Date = 07/18/13 
 Pct Recovery = 85%  Analysis Date = 07/16/13 
 Pct Recovery = 85%  Analysis Date = 07/16/13 
 Pct Recovery = 85%  Analysis Date = 07/14/13 
 Pct Recovery = 86%  Analysis Date = 07/14/13 
 Pct Recovery = 86%  Analysis Date = 07/11/13 
 Pct Recovery = 86%  Analysis Date = 07/11/13 
 Pct Recovery = 86%  Analysis Date = 07/09/13 
 Pct Recovery = 86%  Analysis Date = 07/09/13 
 Pct Recovery = 86%  Analysis Date = 07/06/13 
 Pct Recovery = 86%  Analysis Date = 07/06/13 
 Pct Recovery = 86%  Analysis Date = 07/04/13 
 Pct Recovery = 87%  Analysis Date = 07/04/13 
 Pct Recovery = 87%  Analysis Date = 07/02/13 
 Pct Recovery = 87%  Analysis Date = 07/02/13 
 Pct Recovery = 87%  Analysis Date = 06/29/13 
 Pct Recovery = 87%  Analysis Date = 06/29/13 
 Pct Recovery = 87%  Analysis Date = 06/27/13 
 Pct Recovery = 88%  Analysis Date = 06/27/13 
 Pct Recovery = 88%  Analysis Date = 06/24/13 
 Pct Recovery = 88%  Analysis Date = 06/24/13 
 Pct Recovery = 88%  Analysis Date = 06/22/13 
 Pct Recovery = 88%  Analysis Date = 06/22/13 
 Pct Recovery = 88%  Analysis Date = 06/19/13 
 Pct Recovery = 89%  Analysis Date = 06/19/13 
 Pct Recovery = 89%  Analysis Date = 06/17/13 
 Pct Recovery = 89%  Analysis Date = 06/17/13 
 Pct Recovery = 89%  Analysis Date = 06/15/13 
 Pct Recovery = 89%  Analysis Date = 06/15/13 
 Pct Recovery = 89%  Analysis Date = 06/12/13 
 Pct Recovery = 89%  Analysis Date = 06/12/13 
 Pct Recovery = 89%  Analysis Date = 06/10/13 
 Pct Recovery = 90%  Analysis Date = 06/10/13 
 Pct Recovery = 90%  Analysis Date = 06/07/13 
 Pct Recovery = 90%  Analysis Date = 06/07/13 
 Pct Recovery = 90%  Analysis Date = 06/05/13 
 Pct Recovery = 90%  Analysis Date = 06/05/13 
 Pct Recovery = 90%  Analysis Date = 06/03/13 
 Pct Recovery = 91%  Analysis Date = 06/03/13 
 Pct Recovery = 91%  Analysis Date = 05/31/13 
 Pct Recovery = 91%  Analysis Date = 05/31/13 
 Pct Recovery = 91%  Analysis Date = 05/29/13 
 Pct Recovery = 91%  Analysis Date = 05/29/13 
 Pct Recovery = 91%  Analysis Date = 05/26/13 
 Pct Recovery = 92%  Analysis Date = 05/26/13 
 Pct Recovery = 92%  Analysis Date = 05/24/13 
 Pct Recovery = 92%  Analysis Date = 05/24/13 
 Pct Recovery = 92%  Analysis Date = 05/22/13 
 Pct Recovery = 92%  Analysis Date = 05/22/13 
 Pct Recovery = 92%  Analysis Date = 05/19/13 
 Pct Recovery = 92%  Analysis Date = 05/19/13 
 Pct Recovery = 92%  Analysis Date = 05/17/13 
 Pct Recovery = 93%  Analysis Date = 05/17/13 
 Pct Recovery = 93%  Analysis Date = 05/14/13 
 Pct Recovery = 93%  Analysis Date = 05/14/13 
 Pct Recovery = 93%  Analysis Date = 05/12/13 
 Pct Recovery = 93%  Analysis Date = 05/12/13 
 Pct Recovery = 93%  Analysis Date = 05/10/13 
 Pct Recovery = 94%  Analysis Date = 05/10/13 
 Pct Recovery = 94%  Analysis Date = 05/07/13 
 Pct Recovery = 94%  Analysis Date = 05/07/13 
 Pct Recovery = 94%  Analysis Date = 05/05/13 
 Pct Recovery = 94%  Analysis Date = 05/05/13 
 Pct Recovery = 94%  Analysis Date = 05/02/13 
 Pct Recovery = 94%  Analysis Date = 05/02/13 
 Pct Recovery = 94%  Analysis Date = 04/30/13 
 Pct Recovery = 95%  Analysis Date = 04/30/13 
 Pct Recovery = 95%  Analysis Date = 04/27/13 
 Pct Recovery = 95%  Analysis Date = 04/27/13 
 Pct Recovery = 95%  Analysis Date = 04/25/13 
 Pct Recovery = 95%  Analysis Date = 04/25/13 
 Pct Recovery = 95%  Analysis Date = 04/23/13 
 Pct Recovery = 95%  Analysis Date = 04/23/13 
 Pct Recovery = 95%  Analysis Date = 04/20/13 
 Pct Recovery = 96%  Analysis Date = 04/20/13 
 Pct Recovery = 96%  Analysis Date = 04/18/13 
 Pct Recovery = 96%  Analysis Date = 04/18/13 
 Pct Recovery = 96%  Analysis Date = 04/15/13 
 Pct Recovery = 96%  Analysis Date = 04/15/13 
 Pct Recovery = 96%  Analysis Date = 04/13/13 
 Pct Recovery = 96%  Analysis Date = 04/13/13 
 Pct Recovery = 96%  Analysis Date = 04/11/13 
 Pct Recovery = 96%  Analysis Date = 04/11/13 
 Pct Recovery = 96%  Analysis Date = 04/08/13 
 Pct Recovery = 96%  Analysis Date = 04/08/13 
 Pct Recovery = 96%  Analysis Date = 04/06/13 
 Pct Recovery = 96%  Analysis Date = 04/06/13 
 Pct Recovery = 96%  Analysis Date = 04/03/13 
 Pct Recovery = 96%  Analysis Date = 04/03/13 
 Pct Recovery = 96%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 03/30/13 
 Pct Recovery = 96%  Analysis Date = 03/30/13 
 Pct Recovery = 96%  Analysis Date = 03/27/13 
 Pct Recovery = 97%  Analysis Date = 03/27/13 
 Pct Recovery = 97%  Analysis Date = 03/25/13 
 Pct Recovery = 97%  Analysis Date = 03/25/13 
 Pct Recovery = 97%  Analysis Date = 03/22/13 
 Pct Recovery = 97%  Analysis Date = 03/22/13 
 Pct Recovery = 97%  Analysis Date = 03/20/13 
 Pct Recovery = 97%  Analysis Date = 03/20/13 
 Pct Recovery = 97%  Analysis Date = 03/17/13 
 Pct Recovery = 97%  Analysis Date = 03/17/13 
 Pct Recovery = 97%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/13/13 
 Pct Recovery = 97%  Analysis Date = 03/13/13 
 Pct Recovery = 97%  Analysis Date = 03/10/13 
 Pct Recovery = 97%  Analysis Date = 03/10/13 
 Pct Recovery = 97%  Analysis Date = 03/08/13 
 Pct Recovery = 97%  Analysis Date = 03/08/13 
 Pct Recovery = 97%  Analysis Date = 03/05/13 
 Pct Recovery = 97%  Analysis Date = 03/05/13 
 Pct Recovery = 97%  Analysis Date = 03/03/13 
 Pct Recovery = 98%  Analysis Date = 03/03/13 
 Pct Recovery = 98%  Analysis Date = 03/01/13 
 Pct Recovery = 98%  Analysis Date = 03/01/13 
 Pct Recovery = 98%  Analysis Date = 02/26/13 
 Pct Recovery = 98%  Analysis Date = 02/26/13 
 Pct Recovery = 98%  Analysis Date = 02/24/13 
 Pct Recovery = 98%  Analysis Date = 02/24/13 
 Pct Recovery = 98%  Analysis Date = 02/21/13 
 Pct Recovery = 98%  Analysis Date = 02/21/13 
 Pct Recovery = 98%  Analysis Date = 02/19/13 
 Pct Recovery = 98%  Analysis Date = 02/19/13 
 Pct Recovery = 98%  Analysis Date = 02/17/13 
 Pct Recovery = 98%  Analysis Date = 02/17/13 
 Pct Recovery = 98%  Analysis Date = 02/14/13 
 Pct Recovery = 98%  Analysis Date = 02/14/13 
 Pct Recovery = 98%  Analysis Date = 02/12/13 
 Pct Recovery = 98%  Analysis Date = 02/12/13 
 Pct Recovery = 98%  Analysis Date = 02/09/13 
 Pct Recovery = 98%  Analysis Date = 02/09/13 
 Pct Recovery = 98%  Analysis Date = 02/07/13 
 Pct Recovery = 98%  Analysis Date = 02/07/13 
 Pct Recovery = 98%  Analysis Date = 02/05/13 
 Pct Recovery = 98%  Analysis Date = 02/05/13 
 Pct Recovery = 98%  Analysis Date = 02/02/13 
 Pct Recovery = 98%  Analysis Date = 02/02/13 
 Pct Recovery = 98%  Analysis Date = 01/31/13 
 Pct Recovery = 98%  Analysis Date = 01/31/13 
 Pct Recovery = 98%  Analysis Date = 01/28/13 
 Pct Recovery = 98%  Analysis Date = 01/28/13 
 Pct Recovery = 98%  Analysis Date = 01/26/13 
 Pct Recovery = 98%  Analysis Date = 01/26/13 
 Pct Recovery = 98%  Analysis Date = 01/23/13 
 Pct Recovery = 98%  Analysis Date = 01/23/13 
 Pct Recovery = 98%  Analysis Date = 01/21/13 
 Pct Recovery = 98%  Analysis Date = 01/21/13 
 Pct Recovery = 98%  Analysis Date = 01/19/13 
 Pct Recovery = 98%  Analysis Date = 01/19/13 
 Pct Recovery = 98%  Analysis Date = 01/16/13 
 Pct Recovery = 98%  Analysis Date = 01/16/13 
 Pct Recovery = 98%  Analysis Date = 01/14/13 
 Pct Recovery = 98%  Analysis Date = 01/14/13 
 Pct Recovery = 98%  Analysis Date = 01/11/13 
 Pct Recovery = 98%  Analysis Date = 01/11/13 
 Pct Recovery = 98%  Analysis Date = 01/09/13 
 Pct Recovery = 98%  Analysis Date = 01/09/13 
 Pct Recovery = 98%  Analysis Date = 01/07/13 
 Pct Recovery = 97%  Analysis Date = 01/07/13 
 Pct Recovery = 97%  Analysis Date = 01/04/13 
 Pct Recovery = 97%  Analysis Date = 01/04/13 
 Pct Recovery = 97%  Analysis Date = 01/02/13 
 Pct Recovery = 97%  Analysis Date = 01/02/13 
 Pct Recovery = 97%  Analysis Date = 12/30/12 
 Pct Recovery = 97%  Analysis Date = 12/30/12 
 Pct Recovery = 97%  Analysis Date = 12/28/12 
 Pct Recovery = 97%  Analysis Date = 12/28/12 
 Pct Recovery = 97%  Analysis Date = 12/26/12 
 Pct Recovery = 97%  Analysis Date = 12/26/12 
 Pct Recovery = 97%  Analysis Date = 12/23/12 
 Pct Recovery = 97%  Analysis Date = 12/23/12 
 Pct Recovery = 97%  Analysis Date = 12/21/12 
 Pct Recovery = 97%  Analysis Date = 12/21/12 
 Pct Recovery = 97%  Analysis Date = 12/18/12 
 Pct Recovery = 97%  Analysis Date = 12/18/12 
 Pct Recovery = 97%  Analysis Date = 12/16/12 
 Pct Recovery = 97%  Analysis Date = 12/16/12 
 Pct Recovery = 97%  Analysis Date = 12/14/12 
 Pct Recovery = 97%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL-1H-BENZOTRIAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 110% . 110% 0%
>= Reporting Level 13 83% 13% 82% 13%
Total 14 85% 15% 83% 17%

Sample Statistics
METHYL-1H-BENZOTRIAZOLE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
METOPROLOL
METHOD: LC9017 , TESTIDCODE: 67523LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 36%  Analysis Date = 12/14/12 
 SpikeMix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Pct Recovery = 40%  Analysis Date = 05/03/13 
 SpikeMix = Abs 053112: 40 µl 
 Pct Recovery = 32%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 33%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 34%  Analysis Date = 08/29/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Pct Recovery = 34%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 37%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 30%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 31%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 44%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 24%  Analysis Date = 02/19/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Pct Recovery = 41%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 Pct Recovery = 35%  Analysis Date = 03/18/14 
 Pct Recovery = 35%  Analysis Date = 03/18/14 
 Pct Recovery = 35%  Analysis Date = 03/16/14 
 Pct Recovery = 35%  Analysis Date = 03/16/14 
 Pct Recovery = 35%  Analysis Date = 03/14/14 
 Pct Recovery = 34%  Analysis Date = 03/14/14 
 Pct Recovery = 34%  Analysis Date = 03/11/14 
 Pct Recovery = 34%  Analysis Date = 03/11/14 
 Pct Recovery = 34%  Analysis Date = 03/09/14 
 Pct Recovery = 34%  Analysis Date = 03/09/14 
 Pct Recovery = 34%  Analysis Date = 03/07/14 
 Pct Recovery = 34%  Analysis Date = 03/07/14 
 Pct Recovery = 34%  Analysis Date = 03/04/14 
 Pct Recovery = 34%  Analysis Date = 03/04/14 
 Pct Recovery = 34%  Analysis Date = 03/02/14 
 Pct Recovery = 34%  Analysis Date = 03/02/14 
 Pct Recovery = 34%  Analysis Date = 02/28/14 
 Pct Recovery = 34%  Analysis Date = 02/28/14 
 Pct Recovery = 34%  Analysis Date = 02/25/14 
 Pct Recovery = 34%  Analysis Date = 02/25/14 
 Pct Recovery = 34%  Analysis Date = 02/23/14 
 Pct Recovery = 34%  Analysis Date = 02/23/14 
 Pct Recovery = 34%  Analysis Date = 02/21/14 
 Pct Recovery = 34%  Analysis Date = 02/21/14 
 Pct Recovery = 34%  Analysis Date = 02/18/14 
 Pct Recovery = 34%  Analysis Date = 02/18/14 
 Pct Recovery = 34%  Analysis Date = 02/16/14 
 Pct Recovery = 34%  Analysis Date = 02/16/14 
 Pct Recovery = 34%  Analysis Date = 02/14/14 
 Pct Recovery = 34%  Analysis Date = 02/14/14 
 Pct Recovery = 34%  Analysis Date = 02/12/14 
 Pct Recovery = 34%  Analysis Date = 02/12/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/09/14 
 Pct Recovery = 34%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 34%  Analysis Date = 01/31/14 
 Pct Recovery = 34%  Analysis Date = 01/31/14 
 Pct Recovery = 34%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/26/14 
 Pct Recovery = 33%  Analysis Date = 01/26/14 
 Pct Recovery = 33%  Analysis Date = 01/24/14 
 Pct Recovery = 33%  Analysis Date = 01/24/14 
 Pct Recovery = 33%  Analysis Date = 01/22/14 
 Pct Recovery = 33%  Analysis Date = 01/22/14 
 Pct Recovery = 33%  Analysis Date = 01/19/14 
 Pct Recovery = 33%  Analysis Date = 01/19/14 
 Pct Recovery = 33%  Analysis Date = 01/17/14 
 Pct Recovery = 33%  Analysis Date = 01/17/14 
 Pct Recovery = 33%  Analysis Date = 01/15/14 
 Pct Recovery = 33%  Analysis Date = 01/15/14 
 Pct Recovery = 33%  Analysis Date = 01/13/14 
 Pct Recovery = 33%  Analysis Date = 01/13/14 
 Pct Recovery = 33%  Analysis Date = 01/10/14 
 Pct Recovery = 33%  Analysis Date = 01/10/14 
 Pct Recovery = 33%  Analysis Date = 01/08/14 
 Pct Recovery = 33%  Analysis Date = 01/08/14 
 Pct Recovery = 33%  Analysis Date = 01/06/14 
 Pct Recovery = 33%  Analysis Date = 01/06/14 
 Pct Recovery = 33%  Analysis Date = 01/03/14 
 Pct Recovery = 33%  Analysis Date = 01/03/14 
 Pct Recovery = 33%  Analysis Date = 01/01/14 
 Pct Recovery = 33%  Analysis Date = 01/01/14 
 Pct Recovery = 33%  Analysis Date = 12/30/13 
 Pct Recovery = 33%  Analysis Date = 12/30/13 
 Pct Recovery = 33%  Analysis Date = 12/27/13 
 Pct Recovery = 32%  Analysis Date = 12/27/13 
 Pct Recovery = 32%  Analysis Date = 12/25/13 
 Pct Recovery = 32%  Analysis Date = 12/25/13 
 Pct Recovery = 32%  Analysis Date = 12/23/13 
 Pct Recovery = 32%  Analysis Date = 12/23/13 
 Pct Recovery = 32%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/18/13 
 Pct Recovery = 32%  Analysis Date = 12/18/13 
 Pct Recovery = 32%  Analysis Date = 12/16/13 
 Pct Recovery = 32%  Analysis Date = 12/16/13 
 Pct Recovery = 32%  Analysis Date = 12/13/13 
 Pct Recovery = 32%  Analysis Date = 12/13/13 
 Pct Recovery = 32%  Analysis Date = 12/11/13 
 Pct Recovery = 32%  Analysis Date = 12/11/13 
 Pct Recovery = 32%  Analysis Date = 12/09/13 
 Pct Recovery = 32%  Analysis Date = 12/09/13 
 Pct Recovery = 32%  Analysis Date = 12/07/13 
 Pct Recovery = 32%  Analysis Date = 12/07/13 
 Pct Recovery = 32%  Analysis Date = 12/04/13 
 Pct Recovery = 32%  Analysis Date = 12/04/13 
 Pct Recovery = 32%  Analysis Date = 12/02/13 
 Pct Recovery = 32%  Analysis Date = 12/02/13 
 Pct Recovery = 32%  Analysis Date = 11/30/13 
 Pct Recovery = 32%  Analysis Date = 11/30/13 
 Pct Recovery = 32%  Analysis Date = 11/27/13 
 Pct Recovery = 32%  Analysis Date = 11/27/13 
 Pct Recovery = 32%  Analysis Date = 11/25/13 
 Pct Recovery = 32%  Analysis Date = 11/25/13 
 Pct Recovery = 32%  Analysis Date = 11/23/13 
 Pct Recovery = 32%  Analysis Date = 11/23/13 
 Pct Recovery = 32%  Analysis Date = 11/20/13 
 Pct Recovery = 32%  Analysis Date = 11/20/13 
 Pct Recovery = 32%  Analysis Date = 11/18/13 
 Pct Recovery = 31%  Analysis Date = 11/18/13 
 Pct Recovery = 31%  Analysis Date = 11/16/13 
 Pct Recovery = 31%  Analysis Date = 11/16/13 
 Pct Recovery = 31%  Analysis Date = 11/13/13 
 Pct Recovery = 31%  Analysis Date = 11/13/13 
 Pct Recovery = 31%  Analysis Date = 11/11/13 
 Pct Recovery = 31%  Analysis Date = 11/11/13 
 Pct Recovery = 31%  Analysis Date = 11/09/13 
 Pct Recovery = 31%  Analysis Date = 11/09/13 
 Pct Recovery = 31%  Analysis Date = 11/07/13 
 Pct Recovery = 31%  Analysis Date = 11/07/13 
 Pct Recovery = 31%  Analysis Date = 11/04/13 
 Pct Recovery = 31%  Analysis Date = 11/04/13 
 Pct Recovery = 31%  Analysis Date = 11/02/13 
 Pct Recovery = 31%  Analysis Date = 11/02/13 
 Pct Recovery = 31%  Analysis Date = 10/31/13 
 Pct Recovery = 31%  Analysis Date = 10/31/13 
 Pct Recovery = 31%  Analysis Date = 10/28/13 
 Pct Recovery = 31%  Analysis Date = 10/28/13 
 Pct Recovery = 31%  Analysis Date = 10/26/13 
 Pct Recovery = 31%  Analysis Date = 10/26/13 
 Pct Recovery = 31%  Analysis Date = 10/24/13 
 Pct Recovery = 31%  Analysis Date = 10/24/13 
 Pct Recovery = 31%  Analysis Date = 10/21/13 
 Pct Recovery = 31%  Analysis Date = 10/21/13 
 Pct Recovery = 31%  Analysis Date = 10/19/13 
 Pct Recovery = 31%  Analysis Date = 10/19/13 
 Pct Recovery = 31%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/14/13 
 Pct Recovery = 31%  Analysis Date = 10/14/13 
 Pct Recovery = 31%  Analysis Date = 10/12/13 
 Pct Recovery = 31%  Analysis Date = 10/12/13 
 Pct Recovery = 31%  Analysis Date = 10/10/13 
 Pct Recovery = 31%  Analysis Date = 10/10/13 
 Pct Recovery = 31%  Analysis Date = 10/07/13 
 Pct Recovery = 31%  Analysis Date = 10/07/13 
 Pct Recovery = 31%  Analysis Date = 10/05/13 
 Pct Recovery = 31%  Analysis Date = 10/05/13 
 Pct Recovery = 31%  Analysis Date = 10/03/13 
 Pct Recovery = 31%  Analysis Date = 10/03/13 
 Pct Recovery = 31%  Analysis Date = 10/01/13 
 Pct Recovery = 31%  Analysis Date = 10/01/13 
 Pct Recovery = 31%  Analysis Date = 09/28/13 
 Pct Recovery = 31%  Analysis Date = 09/28/13 
 Pct Recovery = 31%  Analysis Date = 09/26/13 
 Pct Recovery = 31%  Analysis Date = 09/26/13 
 Pct Recovery = 31%  Analysis Date = 09/24/13 
 Pct Recovery = 31%  Analysis Date = 09/24/13 
 Pct Recovery = 31%  Analysis Date = 09/21/13 
 Pct Recovery = 30%  Analysis Date = 09/21/13 
 Pct Recovery = 30%  Analysis Date = 09/19/13 
 Pct Recovery = 30%  Analysis Date = 09/19/13 
 Pct Recovery = 30%  Analysis Date = 09/17/13 
 Pct Recovery = 30%  Analysis Date = 09/17/13 
 Pct Recovery = 30%  Analysis Date = 09/14/13 
 Pct Recovery = 30%  Analysis Date = 09/14/13 
 Pct Recovery = 30%  Analysis Date = 09/12/13 
 Pct Recovery = 30%  Analysis Date = 09/12/13 
 Pct Recovery = 30%  Analysis Date = 09/10/13 
 Pct Recovery = 30%  Analysis Date = 09/10/13 
 Pct Recovery = 30%  Analysis Date = 09/07/13 
 Pct Recovery = 30%  Analysis Date = 09/07/13 
 Pct Recovery = 30%  Analysis Date = 09/05/13 
 Pct Recovery = 30%  Analysis Date = 09/05/13 
 Pct Recovery = 30%  Analysis Date = 09/03/13 
 Pct Recovery = 30%  Analysis Date = 09/03/13 
 Pct Recovery = 30%  Analysis Date = 09/01/13 
 Pct Recovery = 30%  Analysis Date = 09/01/13 
 Pct Recovery = 30%  Analysis Date = 08/29/13 
 Pct Recovery = 30%  Analysis Date = 08/29/13 
 Pct Recovery = 30%  Analysis Date = 08/27/13 
 Pct Recovery = 30%  Analysis Date = 08/27/13 
 Pct Recovery = 30%  Analysis Date = 08/25/13 
 Pct Recovery = 30%  Analysis Date = 08/25/13 
 Pct Recovery = 30%  Analysis Date = 08/22/13 
 Pct Recovery = 30%  Analysis Date = 08/22/13 
 Pct Recovery = 30%  Analysis Date = 08/20/13 
 Pct Recovery = 30%  Analysis Date = 08/20/13 
 Pct Recovery = 30%  Analysis Date = 08/18/13 
 Pct Recovery = 30%  Analysis Date = 08/18/13 
 Pct Recovery = 30%  Analysis Date = 08/15/13 
 Pct Recovery = 30%  Analysis Date = 08/15/13 
 Pct Recovery = 30%  Analysis Date = 08/13/13 
 Pct Recovery = 30%  Analysis Date = 08/13/13 
 Pct Recovery = 30%  Analysis Date = 08/11/13 
 Pct Recovery = 30%  Analysis Date = 08/11/13 
 Pct Recovery = 30%  Analysis Date = 08/08/13 
 Pct Recovery = 30%  Analysis Date = 08/08/13 
 Pct Recovery = 30%  Analysis Date = 08/06/13 
 Pct Recovery = 30%  Analysis Date = 08/06/13 
 Pct Recovery = 30%  Analysis Date = 08/04/13 
 Pct Recovery = 31%  Analysis Date = 08/04/13 
 Pct Recovery = 31%  Analysis Date = 08/02/13 
 Pct Recovery = 31%  Analysis Date = 08/02/13 
 Pct Recovery = 31%  Analysis Date = 07/30/13 
 Pct Recovery = 31%  Analysis Date = 07/30/13 
 Pct Recovery = 31%  Analysis Date = 07/28/13 
 Pct Recovery = 31%  Analysis Date = 07/28/13 
 Pct Recovery = 31%  Analysis Date = 07/26/13 
 Pct Recovery = 31%  Analysis Date = 07/26/13 
 Pct Recovery = 31%  Analysis Date = 07/23/13 
 Pct Recovery = 31%  Analysis Date = 07/23/13 
 Pct Recovery = 31%  Analysis Date = 07/21/13 
 Pct Recovery = 31%  Analysis Date = 07/21/13 
 Pct Recovery = 31%  Analysis Date = 07/19/13 
 Pct Recovery = 31%  Analysis Date = 07/19/13 
 Pct Recovery = 31%  Analysis Date = 07/16/13 
 Pct Recovery = 31%  Analysis Date = 07/16/13 
 Pct Recovery = 31%  Analysis Date = 07/14/13 
 Pct Recovery = 31%  Analysis Date = 07/14/13 
 Pct Recovery = 31%  Analysis Date = 07/12/13 
 Pct Recovery = 32%  Analysis Date = 07/12/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/07/13 
 Pct Recovery = 32%  Analysis Date = 07/07/13 
 Pct Recovery = 32%  Analysis Date = 07/05/13 
 Pct Recovery = 32%  Analysis Date = 07/05/13 
 Pct Recovery = 32%  Analysis Date = 07/02/13 
 Pct Recovery = 32%  Analysis Date = 07/02/13 
 Pct Recovery = 32%  Analysis Date = 06/30/13 
 Pct Recovery = 32%  Analysis Date = 06/30/13 
 Pct Recovery = 32%  Analysis Date = 06/28/13 
 Pct Recovery = 32%  Analysis Date = 06/28/13 
 Pct Recovery = 32%  Analysis Date = 06/26/13 
 Pct Recovery = 32%  Analysis Date = 06/26/13 
 Pct Recovery = 32%  Analysis Date = 06/23/13 
 Pct Recovery = 32%  Analysis Date = 06/23/13 
 Pct Recovery = 32%  Analysis Date = 06/21/13 
 Pct Recovery = 32%  Analysis Date = 06/21/13 
 Pct Recovery = 32%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/16/13 
 Pct Recovery = 33%  Analysis Date = 06/16/13 
 Pct Recovery = 33%  Analysis Date = 06/14/13 
 Pct Recovery = 33%  Analysis Date = 06/14/13 
 Pct Recovery = 33%  Analysis Date = 06/12/13 
 Pct Recovery = 33%  Analysis Date = 06/12/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/02/13 
 Pct Recovery = 33%  Analysis Date = 06/02/13 
 Pct Recovery = 33%  Analysis Date = 05/31/13 
 Pct Recovery = 33%  Analysis Date = 05/31/13 
 Pct Recovery = 33%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/29/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/27/13 
 Pct Recovery = 34%  Analysis Date = 05/24/13 
 Pct Recovery = 34%  Analysis Date = 05/24/13 
 Pct Recovery = 34%  Analysis Date = 05/22/13 
 Pct Recovery = 34%  Analysis Date = 05/22/13 
 Pct Recovery = 34%  Analysis Date = 05/20/13 
 Pct Recovery = 34%  Analysis Date = 05/20/13 
 Pct Recovery = 34%  Analysis Date = 05/17/13 
 Pct Recovery = 34%  Analysis Date = 05/17/13 
 Pct Recovery = 34%  Analysis Date = 05/15/13 
 Pct Recovery = 34%  Analysis Date = 05/15/13 
 Pct Recovery = 34%  Analysis Date = 05/13/13 
 Pct Recovery = 34%  Analysis Date = 05/13/13 
 Pct Recovery = 34%  Analysis Date = 05/10/13 
 Pct Recovery = 34%  Analysis Date = 05/10/13 
 Pct Recovery = 34%  Analysis Date = 05/08/13 
 Pct Recovery = 34%  Analysis Date = 05/08/13 
 Pct Recovery = 34%  Analysis Date = 05/06/13 
 Pct Recovery = 35%  Analysis Date = 05/06/13 
 Pct Recovery = 35%  Analysis Date = 05/03/13 
 Pct Recovery = 35%  Analysis Date = 05/03/13 
 Pct Recovery = 35%  Analysis Date = 05/01/13 
 Pct Recovery = 35%  Analysis Date = 05/01/13 
 Pct Recovery = 35%  Analysis Date = 04/29/13 
 Pct Recovery = 35%  Analysis Date = 04/29/13 
 Pct Recovery = 35%  Analysis Date = 04/26/13 
 Pct Recovery = 35%  Analysis Date = 04/26/13 
 Pct Recovery = 35%  Analysis Date = 04/24/13 
 Pct Recovery = 35%  Analysis Date = 04/24/13 
 Pct Recovery = 35%  Analysis Date = 04/22/13 
 Pct Recovery = 36%  Analysis Date = 04/22/13 
 Pct Recovery = 36%  Analysis Date = 04/20/13 
 Pct Recovery = 36%  Analysis Date = 04/20/13 
 Pct Recovery = 36%  Analysis Date = 04/17/13 
 Pct Recovery = 36%  Analysis Date = 04/17/13 
 Pct Recovery = 36%  Analysis Date = 04/15/13 
 Pct Recovery = 36%  Analysis Date = 04/15/13 
 Pct Recovery = 36%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/10/13 
 Pct Recovery = 37%  Analysis Date = 04/10/13 
 Pct Recovery = 37%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/08/13 
 Pct Recovery = 37%  Analysis Date = 04/06/13 
 Pct Recovery = 37%  Analysis Date = 04/06/13 
 Pct Recovery = 37%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 38%  Analysis Date = 03/30/13 
 Pct Recovery = 38%  Analysis Date = 03/27/13 
 Pct Recovery = 38%  Analysis Date = 03/27/13 
 Pct Recovery = 38%  Analysis Date = 03/25/13 
 Pct Recovery = 38%  Analysis Date = 03/25/13 
 Pct Recovery = 38%  Analysis Date = 03/23/13 
 Pct Recovery = 38%  Analysis Date = 03/23/13 
 Pct Recovery = 38%  Analysis Date = 03/21/13 
 Pct Recovery = 38%  Analysis Date = 03/21/13 
 Pct Recovery = 38%  Analysis Date = 03/18/13 
 Pct Recovery = 38%  Analysis Date = 03/18/13 
 Pct Recovery = 38%  Analysis Date = 03/16/13 
 Pct Recovery = 38%  Analysis Date = 03/16/13 
 Pct Recovery = 38%  Analysis Date = 03/14/13 
 Pct Recovery = 38%  Analysis Date = 03/14/13 
 Pct Recovery = 38%  Analysis Date = 03/11/13 
 Pct Recovery = 38%  Analysis Date = 03/11/13 
 Pct Recovery = 38%  Analysis Date = 03/09/13 
 Pct Recovery = 38%  Analysis Date = 03/09/13 
 Pct Recovery = 38%  Analysis Date = 03/07/13 
 Pct Recovery = 38%  Analysis Date = 03/07/13 
 Pct Recovery = 38%  Analysis Date = 03/04/13 
 Pct Recovery = 39%  Analysis Date = 03/04/13 
 Pct Recovery = 39%  Analysis Date = 03/02/13 
 Pct Recovery = 39%  Analysis Date = 03/02/13 
 Pct Recovery = 39%  Analysis Date = 02/28/13 
 Pct Recovery = 39%  Analysis Date = 02/28/13 
 Pct Recovery = 39%  Analysis Date = 02/25/13 
 Pct Recovery = 39%  Analysis Date = 02/25/13 
 Pct Recovery = 39%  Analysis Date = 02/23/13 
 Pct Recovery = 39%  Analysis Date = 02/23/13 
 Pct Recovery = 39%  Analysis Date = 02/21/13 
 Pct Recovery = 39%  Analysis Date = 02/21/13 
 Pct Recovery = 39%  Analysis Date = 02/18/13 
 Pct Recovery = 39%  Analysis Date = 02/18/13 
 Pct Recovery = 39%  Analysis Date = 02/16/13 
 Pct Recovery = 39%  Analysis Date = 02/16/13 
 Pct Recovery = 39%  Analysis Date = 02/14/13 
 Pct Recovery = 39%  Analysis Date = 02/14/13 
 Pct Recovery = 39%  Analysis Date = 02/12/13 
 Pct Recovery = 39%  Analysis Date = 02/12/13 
 Pct Recovery = 39%  Analysis Date = 02/09/13 
 Pct Recovery = 39%  Analysis Date = 02/09/13 
 Pct Recovery = 39%  Analysis Date = 02/07/13 
 Pct Recovery = 39%  Analysis Date = 02/07/13 
 Pct Recovery = 39%  Analysis Date = 02/05/13 
 Pct Recovery = 39%  Analysis Date = 02/05/13 
 Pct Recovery = 39%  Analysis Date = 02/02/13 
 Pct Recovery = 39%  Analysis Date = 02/02/13 
 Pct Recovery = 39%  Analysis Date = 01/31/13 
 Pct Recovery = 40%  Analysis Date = 01/31/13 
 Pct Recovery = 40%  Analysis Date = 01/29/13 
 Pct Recovery = 40%  Analysis Date = 01/29/13 
 Pct Recovery = 40%  Analysis Date = 01/26/13 
 Pct Recovery = 40%  Analysis Date = 01/26/13 
 Pct Recovery = 40%  Analysis Date = 01/24/13 
 Pct Recovery = 40%  Analysis Date = 01/24/13 
 Pct Recovery = 40%  Analysis Date = 01/22/13 
 Pct Recovery = 40%  Analysis Date = 01/22/13 
 Pct Recovery = 40%  Analysis Date = 01/19/13 
 Pct Recovery = 40%  Analysis Date = 01/19/13 
 Pct Recovery = 40%  Analysis Date = 01/17/13 
 Pct Recovery = 40%  Analysis Date = 01/17/13 
 Pct Recovery = 40%  Analysis Date = 01/15/13 
 Pct Recovery = 40%  Analysis Date = 01/15/13 
 Pct Recovery = 40%  Analysis Date = 01/13/13 
 Pct Recovery = 40%  Analysis Date = 01/13/13 
 Pct Recovery = 40%  Analysis Date = 01/10/13 
 Pct Recovery = 40%  Analysis Date = 01/10/13 
 Pct Recovery = 40%  Analysis Date = 01/08/13 
 Pct Recovery = 40%  Analysis Date = 01/08/13 
 Pct Recovery = 40%  Analysis Date = 01/06/13 
 Pct Recovery = 40%  Analysis Date = 01/06/13 
 Pct Recovery = 40%  Analysis Date = 01/03/13 
 Pct Recovery = 40%  Analysis Date = 01/03/13 
 Pct Recovery = 40%  Analysis Date = 01/01/13 
 Pct Recovery = 40%  Analysis Date = 01/01/13 
 Pct Recovery = 40%  Analysis Date = 12/30/12 
 Pct Recovery = 41%  Analysis Date = 12/30/12 
 Pct Recovery = 41%  Analysis Date = 12/27/12 
 Pct Recovery = 41%  Analysis Date = 12/27/12 
 Pct Recovery = 41%  Analysis Date = 12/25/12 
 Pct Recovery = 41%  Analysis Date = 12/25/12 
 Pct Recovery = 41%  Analysis Date = 12/23/12 
 Pct Recovery = 41%  Analysis Date = 12/23/12 
 Pct Recovery = 41%  Analysis Date = 12/20/12 
 Pct Recovery = 41%  Analysis Date = 12/20/12 
 Pct Recovery = 41%  Analysis Date = 12/18/12 
 Pct Recovery = 41%  Analysis Date = 12/18/12 
 Pct Recovery = 41%  Analysis Date = 12/16/12 
 Pct Recovery = 41%  Analysis Date = 12/16/12 
 Pct Recovery = 41%  Analysis Date = 12/14/12 
 Pct Recovery = 41%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOPROLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 35% 5% 34% 5%
Total 13 35% 5% 34% 5%

Sample Statistics
METOPROLOL

Characteristic N % % Basis
Plotted 13 87% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 13% 2 out of 15
Not Spiked 17 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
MORPHINE
METHOD: LC9017 , TESTIDCODE: 67458LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 87%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 69%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 115%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 83%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 49%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 59%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 31%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 65%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 63%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 62%  Analysis Date = 04/09/14 
 Pct Recovery = 50%  Analysis Date = 04/07/14 
 Pct Recovery = 50%  Analysis Date = 04/07/14 
 Pct Recovery = 50%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/02/14 
 Pct Recovery = 51%  Analysis Date = 04/02/14 
 Pct Recovery = 51%  Analysis Date = 03/31/14 
 Pct Recovery = 51%  Analysis Date = 03/31/14 
 Pct Recovery = 51%  Analysis Date = 03/28/14 
 Pct Recovery = 51%  Analysis Date = 03/28/14 
 Pct Recovery = 51%  Analysis Date = 03/26/14 
 Pct Recovery = 52%  Analysis Date = 03/26/14 
 Pct Recovery = 52%  Analysis Date = 03/24/14 
 Pct Recovery = 52%  Analysis Date = 03/24/14 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 Pct Recovery = 52%  Analysis Date = 03/19/14 
 Pct Recovery = 52%  Analysis Date = 03/19/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 53%  Analysis Date = 03/16/14 
 Pct Recovery = 53%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/12/14 
 Pct Recovery = 53%  Analysis Date = 03/12/14 
 Pct Recovery = 53%  Analysis Date = 03/09/14 
 Pct Recovery = 54%  Analysis Date = 03/09/14 
 Pct Recovery = 54%  Analysis Date = 03/07/14 
 Pct Recovery = 54%  Analysis Date = 03/07/14 
 Pct Recovery = 54%  Analysis Date = 03/04/14 
 Pct Recovery = 54%  Analysis Date = 03/04/14 
 Pct Recovery = 54%  Analysis Date = 03/02/14 
 Pct Recovery = 54%  Analysis Date = 03/02/14 
 Pct Recovery = 54%  Analysis Date = 02/28/14 
 Pct Recovery = 55%  Analysis Date = 02/28/14 
 Pct Recovery = 55%  Analysis Date = 02/25/14 
 Pct Recovery = 55%  Analysis Date = 02/25/14 
 Pct Recovery = 55%  Analysis Date = 02/23/14 
 Pct Recovery = 55%  Analysis Date = 02/23/14 
 Pct Recovery = 55%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/15/14 
 Pct Recovery = 56%  Analysis Date = 02/15/14 
 Pct Recovery = 56%  Analysis Date = 02/13/14 
 Pct Recovery = 56%  Analysis Date = 02/13/14 
 Pct Recovery = 56%  Analysis Date = 02/11/14 
 Pct Recovery = 56%  Analysis Date = 02/11/14 
 Pct Recovery = 56%  Analysis Date = 02/08/14 
 Pct Recovery = 57%  Analysis Date = 02/08/14 
 Pct Recovery = 57%  Analysis Date = 02/06/14 
 Pct Recovery = 57%  Analysis Date = 02/06/14 
 Pct Recovery = 57%  Analysis Date = 02/03/14 
 Pct Recovery = 57%  Analysis Date = 02/03/14 
 Pct Recovery = 57%  Analysis Date = 02/01/14 
 Pct Recovery = 58%  Analysis Date = 02/01/14 
 Pct Recovery = 58%  Analysis Date = 01/30/14 
 Pct Recovery = 58%  Analysis Date = 01/30/14 
 Pct Recovery = 58%  Analysis Date = 01/27/14 
 Pct Recovery = 58%  Analysis Date = 01/27/14 
 Pct Recovery = 58%  Analysis Date = 01/25/14 
 Pct Recovery = 58%  Analysis Date = 01/25/14 
 Pct Recovery = 58%  Analysis Date = 01/22/14 
 Pct Recovery = 59%  Analysis Date = 01/22/14 
 Pct Recovery = 59%  Analysis Date = 01/20/14 
 Pct Recovery = 59%  Analysis Date = 01/20/14 
 Pct Recovery = 59%  Analysis Date = 01/18/14 
 Pct Recovery = 59%  Analysis Date = 01/18/14 
 Pct Recovery = 59%  Analysis Date = 01/15/14 
 Pct Recovery = 59%  Analysis Date = 01/15/14 
 Pct Recovery = 59%  Analysis Date = 01/13/14 
 Pct Recovery = 60%  Analysis Date = 01/13/14 
 Pct Recovery = 60%  Analysis Date = 01/10/14 
 Pct Recovery = 60%  Analysis Date = 01/10/14 
 Pct Recovery = 60%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/08/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 61%  Analysis Date = 01/03/14 
 Pct Recovery = 61%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 12/29/13 
 Pct Recovery = 61%  Analysis Date = 12/29/13 
 Pct Recovery = 61%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/27/13 
 Pct Recovery = 61%  Analysis Date = 12/24/13 
 Pct Recovery = 62%  Analysis Date = 12/24/13 
 Pct Recovery = 62%  Analysis Date = 12/22/13 
 Pct Recovery = 62%  Analysis Date = 12/22/13 
 Pct Recovery = 62%  Analysis Date = 12/20/13 
 Pct Recovery = 62%  Analysis Date = 12/20/13 
 Pct Recovery = 62%  Analysis Date = 12/17/13 
 Pct Recovery = 62%  Analysis Date = 12/17/13 
 Pct Recovery = 62%  Analysis Date = 12/15/13 
 Pct Recovery = 62%  Analysis Date = 12/15/13 
 Pct Recovery = 62%  Analysis Date = 12/12/13 
 Pct Recovery = 63%  Analysis Date = 12/12/13 
 Pct Recovery = 63%  Analysis Date = 12/10/13 
 Pct Recovery = 63%  Analysis Date = 12/10/13 
 Pct Recovery = 63%  Analysis Date = 12/08/13 
 Pct Recovery = 63%  Analysis Date = 12/08/13 
 Pct Recovery = 63%  Analysis Date = 12/05/13 
 Pct Recovery = 63%  Analysis Date = 12/05/13 
 Pct Recovery = 63%  Analysis Date = 12/03/13 
 Pct Recovery = 64%  Analysis Date = 12/03/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/28/13 
 Pct Recovery = 64%  Analysis Date = 11/28/13 
 Pct Recovery = 64%  Analysis Date = 11/26/13 
 Pct Recovery = 64%  Analysis Date = 11/26/13 
 Pct Recovery = 64%  Analysis Date = 11/23/13 
 Pct Recovery = 65%  Analysis Date = 11/23/13 
 Pct Recovery = 65%  Analysis Date = 11/21/13 
 Pct Recovery = 65%  Analysis Date = 11/21/13 
 Pct Recovery = 65%  Analysis Date = 11/18/13 
 Pct Recovery = 65%  Analysis Date = 11/18/13 
 Pct Recovery = 65%  Analysis Date = 11/16/13 
 Pct Recovery = 65%  Analysis Date = 11/16/13 
 Pct Recovery = 65%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/09/13 
 Pct Recovery = 66%  Analysis Date = 11/09/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 67%  Analysis Date = 11/04/13 
 Pct Recovery = 67%  Analysis Date = 11/01/13 
 Pct Recovery = 67%  Analysis Date = 11/01/13 
 Pct Recovery = 67%  Analysis Date = 10/30/13 
 Pct Recovery = 67%  Analysis Date = 10/30/13 
 Pct Recovery = 67%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/25/13 
 Pct Recovery = 67%  Analysis Date = 10/25/13 
 Pct Recovery = 67%  Analysis Date = 10/23/13 
 Pct Recovery = 67%  Analysis Date = 10/23/13 
 Pct Recovery = 67%  Analysis Date = 10/20/13 
 Pct Recovery = 67%  Analysis Date = 10/20/13 
 Pct Recovery = 67%  Analysis Date = 10/18/13 
 Pct Recovery = 67%  Analysis Date = 10/18/13 
 Pct Recovery = 67%  Analysis Date = 10/16/13 
 Pct Recovery = 67%  Analysis Date = 10/16/13 
 Pct Recovery = 67%  Analysis Date = 10/13/13 
 Pct Recovery = 68%  Analysis Date = 10/13/13 
 Pct Recovery = 68%  Analysis Date = 10/11/13 
 Pct Recovery = 68%  Analysis Date = 10/11/13 
 Pct Recovery = 68%  Analysis Date = 10/08/13 
 Pct Recovery = 68%  Analysis Date = 10/08/13 
 Pct Recovery = 68%  Analysis Date = 10/06/13 
 Pct Recovery = 68%  Analysis Date = 10/06/13 
 Pct Recovery = 68%  Analysis Date = 10/04/13 
 Pct Recovery = 68%  Analysis Date = 10/04/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 10/01/13 
 Pct Recovery = 68%  Analysis Date = 09/29/13 
 Pct Recovery = 68%  Analysis Date = 09/29/13 
 Pct Recovery = 68%  Analysis Date = 09/26/13 
 Pct Recovery = 68%  Analysis Date = 09/26/13 
 Pct Recovery = 68%  Analysis Date = 09/24/13 
 Pct Recovery = 68%  Analysis Date = 09/24/13 
 Pct Recovery = 68%  Analysis Date = 09/21/13 
 Pct Recovery = 68%  Analysis Date = 09/21/13 
 Pct Recovery = 68%  Analysis Date = 09/19/13 
 Pct Recovery = 68%  Analysis Date = 09/19/13 
 Pct Recovery = 68%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/07/13 
 Pct Recovery = 69%  Analysis Date = 09/07/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/02/13 
 Pct Recovery = 69%  Analysis Date = 09/02/13 
 Pct Recovery = 69%  Analysis Date = 08/31/13 
 Pct Recovery = 69%  Analysis Date = 08/31/13 
 Pct Recovery = 69%  Analysis Date = 08/28/13 
 Pct Recovery = 69%  Analysis Date = 08/28/13 
 Pct Recovery = 69%  Analysis Date = 08/26/13 
 Pct Recovery = 69%  Analysis Date = 08/26/13 
 Pct Recovery = 69%  Analysis Date = 08/24/13 
 Pct Recovery = 69%  Analysis Date = 08/24/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/04/13 
 Pct Recovery = 68%  Analysis Date = 08/04/13 
 Pct Recovery = 68%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 08/02/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/23/13 
 Pct Recovery = 68%  Analysis Date = 07/23/13 
 Pct Recovery = 68%  Analysis Date = 07/21/13 
 Pct Recovery = 68%  Analysis Date = 07/21/13 
 Pct Recovery = 68%  Analysis Date = 07/18/13 
 Pct Recovery = 68%  Analysis Date = 07/18/13 
 Pct Recovery = 68%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/06/13 
 Pct Recovery = 67%  Analysis Date = 07/06/13 
 Pct Recovery = 67%  Analysis Date = 07/04/13 
 Pct Recovery = 67%  Analysis Date = 07/04/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 06/29/13 
 Pct Recovery = 67%  Analysis Date = 06/29/13 
 Pct Recovery = 67%  Analysis Date = 06/27/13 
 Pct Recovery = 66%  Analysis Date = 06/27/13 
 Pct Recovery = 66%  Analysis Date = 06/24/13 
 Pct Recovery = 66%  Analysis Date = 06/24/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/17/13 
 Pct Recovery = 66%  Analysis Date = 06/17/13 
 Pct Recovery = 66%  Analysis Date = 06/15/13 
 Pct Recovery = 66%  Analysis Date = 06/15/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/10/13 
 Pct Recovery = 66%  Analysis Date = 06/10/13 
 Pct Recovery = 66%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/19/13 
 Pct Recovery = 64%  Analysis Date = 05/19/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/12/13 
 Pct Recovery = 64%  Analysis Date = 05/12/13 
 Pct Recovery = 64%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/07/13 
 Pct Recovery = 64%  Analysis Date = 05/07/13 
 Pct Recovery = 64%  Analysis Date = 05/05/13 
 Pct Recovery = 64%  Analysis Date = 05/05/13 
 Pct Recovery = 64%  Analysis Date = 05/02/13 
 Pct Recovery = 64%  Analysis Date = 05/02/13 
 Pct Recovery = 64%  Analysis Date = 04/30/13 
 Pct Recovery = 64%  Analysis Date = 04/30/13 
 Pct Recovery = 64%  Analysis Date = 04/27/13 
 Pct Recovery = 64%  Analysis Date = 04/27/13 
 Pct Recovery = 64%  Analysis Date = 04/25/13 
 Pct Recovery = 64%  Analysis Date = 04/25/13 
 Pct Recovery = 64%  Analysis Date = 04/23/13 
 Pct Recovery = 65%  Analysis Date = 04/23/13 
 Pct Recovery = 65%  Analysis Date = 04/20/13 
 Pct Recovery = 65%  Analysis Date = 04/20/13 
 Pct Recovery = 65%  Analysis Date = 04/18/13 
 Pct Recovery = 66%  Analysis Date = 04/18/13 
 Pct Recovery = 66%  Analysis Date = 04/15/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 67%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/11/13 
 Pct Recovery = 68%  Analysis Date = 04/11/13 
 Pct Recovery = 68%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/08/13 
 Pct Recovery = 69%  Analysis Date = 04/06/13 
 Pct Recovery = 70%  Analysis Date = 04/06/13 
 Pct Recovery = 70%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 04/01/13 
 Pct Recovery = 71%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/27/13 
 Pct Recovery = 73%  Analysis Date = 03/27/13 
 Pct Recovery = 73%  Analysis Date = 03/25/13 
 Pct Recovery = 73%  Analysis Date = 03/25/13 
 Pct Recovery = 73%  Analysis Date = 03/22/13 
 Pct Recovery = 74%  Analysis Date = 03/22/13 
 Pct Recovery = 74%  Analysis Date = 03/20/13 
 Pct Recovery = 74%  Analysis Date = 03/20/13 
 Pct Recovery = 74%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 76%  Analysis Date = 03/13/13 
 Pct Recovery = 76%  Analysis Date = 03/10/13 
 Pct Recovery = 76%  Analysis Date = 03/10/13 
 Pct Recovery = 76%  Analysis Date = 03/08/13 
 Pct Recovery = 77%  Analysis Date = 03/08/13 
 Pct Recovery = 77%  Analysis Date = 03/05/13 
 Pct Recovery = 77%  Analysis Date = 03/05/13 
 Pct Recovery = 77%  Analysis Date = 03/03/13 
 Pct Recovery = 77%  Analysis Date = 03/03/13 
 Pct Recovery = 77%  Analysis Date = 03/01/13 
 Pct Recovery = 78%  Analysis Date = 03/01/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/24/13 
 Pct Recovery = 79%  Analysis Date = 02/24/13 
 Pct Recovery = 79%  Analysis Date = 02/21/13 
 Pct Recovery = 79%  Analysis Date = 02/21/13 
 Pct Recovery = 79%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 82%  Analysis Date = 02/07/13 
 Pct Recovery = 82%  Analysis Date = 02/05/13 
 Pct Recovery = 82%  Analysis Date = 02/05/13 
 Pct Recovery = 82%  Analysis Date = 02/02/13 
 Pct Recovery = 83%  Analysis Date = 02/02/13 
 Pct Recovery = 83%  Analysis Date = 01/31/13 
 Pct Recovery = 83%  Analysis Date = 01/31/13 
 Pct Recovery = 83%  Analysis Date = 01/28/13 
 Pct Recovery = 84%  Analysis Date = 01/28/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/26/13 
 Pct Recovery = 84%  Analysis Date = 01/23/13 
 Pct Recovery = 84%  Analysis Date = 01/23/13 
 Pct Recovery = 84%  Analysis Date = 01/21/13 
 Pct Recovery = 84%  Analysis Date = 01/21/13 
 Pct Recovery = 84%  Analysis Date = 01/19/13 
 Pct Recovery = 84%  Analysis Date = 01/19/13 
 Pct Recovery = 84%  Analysis Date = 01/16/13 
 Pct Recovery = 83%  Analysis Date = 01/16/13 
 Pct Recovery = 83%  Analysis Date = 01/14/13 
 Pct Recovery = 83%  Analysis Date = 01/14/13 
 Pct Recovery = 83%  Analysis Date = 01/11/13 
 Pct Recovery = 83%  Analysis Date = 01/11/13 
 Pct Recovery = 83%  Analysis Date = 01/09/13 
 Pct Recovery = 82%  Analysis Date = 01/09/13 
 Pct Recovery = 82%  Analysis Date = 01/07/13 
 Pct Recovery = 82%  Analysis Date = 01/07/13 
 Pct Recovery = 82%  Analysis Date = 01/04/13 
 Pct Recovery = 82%  Analysis Date = 01/04/13 
 Pct Recovery = 82%  Analysis Date = 01/02/13 
 Pct Recovery = 81%  Analysis Date = 01/02/13 
 Pct Recovery = 81%  Analysis Date = 12/30/12 
 Pct Recovery = 81%  Analysis Date = 12/30/12 
 Pct Recovery = 81%  Analysis Date = 12/28/12 
 Pct Recovery = 80%  Analysis Date = 12/28/12 
 Pct Recovery = 80%  Analysis Date = 12/26/12 
 Pct Recovery = 80%  Analysis Date = 12/26/12 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 12/21/12 
 Pct Recovery = 79%  Analysis Date = 12/21/12 
 Pct Recovery = 79%  Analysis Date = 12/18/12 
 Pct Recovery = 79%  Analysis Date = 12/18/12 
 Pct Recovery = 79%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/14/12 
 Pct Recovery = 78%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
MORPHINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 68% 20% 67% 12%
Total 14 68% 20% 67% 12%

Sample Statistics
MORPHINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NADALOL
METHOD: LC9017 , TESTIDCODE: 68006LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 81%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 89%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 51%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 79%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 96%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 79%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 77%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 68%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 70%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 74%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 82%  Analysis Date = 04/09/14 
 Pct Recovery = 64%  Analysis Date = 04/07/14 
 Pct Recovery = 64%  Analysis Date = 04/07/14 
 Pct Recovery = 64%  Analysis Date = 04/05/14 
 Pct Recovery = 64%  Analysis Date = 04/05/14 
 Pct Recovery = 64%  Analysis Date = 04/02/14 
 Pct Recovery = 64%  Analysis Date = 04/02/14 
 Pct Recovery = 64%  Analysis Date = 03/31/14 
 Pct Recovery = 64%  Analysis Date = 03/31/14 
 Pct Recovery = 64%  Analysis Date = 03/28/14 
 Pct Recovery = 65%  Analysis Date = 03/28/14 
 Pct Recovery = 65%  Analysis Date = 03/26/14 
 Pct Recovery = 65%  Analysis Date = 03/26/14 
 Pct Recovery = 65%  Analysis Date = 03/24/14 
 Pct Recovery = 65%  Analysis Date = 03/24/14 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 Pct Recovery = 65%  Analysis Date = 03/19/14 
 Pct Recovery = 65%  Analysis Date = 03/19/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 66%  Analysis Date = 03/16/14 
 Pct Recovery = 66%  Analysis Date = 03/14/14 
 Pct Recovery = 66%  Analysis Date = 03/14/14 
 Pct Recovery = 66%  Analysis Date = 03/12/14 
 Pct Recovery = 66%  Analysis Date = 03/12/14 
 Pct Recovery = 66%  Analysis Date = 03/09/14 
 Pct Recovery = 66%  Analysis Date = 03/09/14 
 Pct Recovery = 66%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 67%  Analysis Date = 03/04/14 
 Pct Recovery = 67%  Analysis Date = 03/02/14 
 Pct Recovery = 67%  Analysis Date = 03/02/14 
 Pct Recovery = 67%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/11/14 
 Pct Recovery = 68%  Analysis Date = 02/11/14 
 Pct Recovery = 68%  Analysis Date = 02/08/14 
 Pct Recovery = 69%  Analysis Date = 02/08/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/03/14 
 Pct Recovery = 69%  Analysis Date = 02/03/14 
 Pct Recovery = 69%  Analysis Date = 02/01/14 
 Pct Recovery = 69%  Analysis Date = 02/01/14 
 Pct Recovery = 69%  Analysis Date = 01/30/14 
 Pct Recovery = 69%  Analysis Date = 01/30/14 
 Pct Recovery = 69%  Analysis Date = 01/27/14 
 Pct Recovery = 70%  Analysis Date = 01/27/14 
 Pct Recovery = 70%  Analysis Date = 01/25/14 
 Pct Recovery = 70%  Analysis Date = 01/25/14 
 Pct Recovery = 70%  Analysis Date = 01/22/14 
 Pct Recovery = 70%  Analysis Date = 01/22/14 
 Pct Recovery = 70%  Analysis Date = 01/20/14 
 Pct Recovery = 70%  Analysis Date = 01/20/14 
 Pct Recovery = 70%  Analysis Date = 01/18/14 
 Pct Recovery = 70%  Analysis Date = 01/18/14 
 Pct Recovery = 70%  Analysis Date = 01/15/14 
 Pct Recovery = 70%  Analysis Date = 01/15/14 
 Pct Recovery = 70%  Analysis Date = 01/13/14 
 Pct Recovery = 71%  Analysis Date = 01/13/14 
 Pct Recovery = 71%  Analysis Date = 01/10/14 
 Pct Recovery = 71%  Analysis Date = 01/10/14 
 Pct Recovery = 71%  Analysis Date = 01/08/14 
 Pct Recovery = 71%  Analysis Date = 01/08/14 
 Pct Recovery = 71%  Analysis Date = 01/06/14 
 Pct Recovery = 71%  Analysis Date = 01/06/14 
 Pct Recovery = 71%  Analysis Date = 01/03/14 
 Pct Recovery = 71%  Analysis Date = 01/03/14 
 Pct Recovery = 71%  Analysis Date = 01/01/14 
 Pct Recovery = 71%  Analysis Date = 01/01/14 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/24/13 
 Pct Recovery = 71%  Analysis Date = 12/24/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/17/13 
 Pct Recovery = 71%  Analysis Date = 12/17/13 
 Pct Recovery = 71%  Analysis Date = 12/15/13 
 Pct Recovery = 71%  Analysis Date = 12/15/13 
 Pct Recovery = 71%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/21/13 
 Pct Recovery = 71%  Analysis Date = 11/21/13 
 Pct Recovery = 71%  Analysis Date = 11/18/13 
 Pct Recovery = 71%  Analysis Date = 11/18/13 
 Pct Recovery = 71%  Analysis Date = 11/16/13 
 Pct Recovery = 71%  Analysis Date = 11/16/13 
 Pct Recovery = 71%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 71%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 72%  Analysis Date = 10/20/13 
 Pct Recovery = 72%  Analysis Date = 10/18/13 
 Pct Recovery = 72%  Analysis Date = 10/18/13 
 Pct Recovery = 72%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 73%  Analysis Date = 10/06/13 
 Pct Recovery = 73%  Analysis Date = 10/04/13 
 Pct Recovery = 73%  Analysis Date = 10/04/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/02/13 
 Pct Recovery = 75%  Analysis Date = 09/02/13 
 Pct Recovery = 75%  Analysis Date = 08/31/13 
 Pct Recovery = 75%  Analysis Date = 08/31/13 
 Pct Recovery = 75%  Analysis Date = 08/28/13 
 Pct Recovery = 75%  Analysis Date = 08/28/13 
 Pct Recovery = 75%  Analysis Date = 08/26/13 
 Pct Recovery = 75%  Analysis Date = 08/26/13 
 Pct Recovery = 75%  Analysis Date = 08/24/13 
 Pct Recovery = 76%  Analysis Date = 08/24/13 
 Pct Recovery = 76%  Analysis Date = 08/21/13 
 Pct Recovery = 76%  Analysis Date = 08/21/13 
 Pct Recovery = 76%  Analysis Date = 08/19/13 
 Pct Recovery = 76%  Analysis Date = 08/19/13 
 Pct Recovery = 76%  Analysis Date = 08/16/13 
 Pct Recovery = 76%  Analysis Date = 08/16/13 
 Pct Recovery = 76%  Analysis Date = 08/14/13 
 Pct Recovery = 76%  Analysis Date = 08/14/13 
 Pct Recovery = 76%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/11/13 
 Pct Recovery = 76%  Analysis Date = 08/09/13 
 Pct Recovery = 76%  Analysis Date = 08/09/13 
 Pct Recovery = 76%  Analysis Date = 08/07/13 
 Pct Recovery = 77%  Analysis Date = 08/07/13 
 Pct Recovery = 77%  Analysis Date = 08/04/13 
 Pct Recovery = 77%  Analysis Date = 08/04/13 
 Pct Recovery = 77%  Analysis Date = 08/02/13 
 Pct Recovery = 77%  Analysis Date = 08/02/13 
 Pct Recovery = 77%  Analysis Date = 07/30/13 
 Pct Recovery = 77%  Analysis Date = 07/30/13 
 Pct Recovery = 77%  Analysis Date = 07/28/13 
 Pct Recovery = 77%  Analysis Date = 07/28/13 
 Pct Recovery = 77%  Analysis Date = 07/26/13 
 Pct Recovery = 77%  Analysis Date = 07/26/13 
 Pct Recovery = 77%  Analysis Date = 07/23/13 
 Pct Recovery = 78%  Analysis Date = 07/23/13 
 Pct Recovery = 78%  Analysis Date = 07/21/13 
 Pct Recovery = 78%  Analysis Date = 07/21/13 
 Pct Recovery = 78%  Analysis Date = 07/18/13 
 Pct Recovery = 78%  Analysis Date = 07/18/13 
 Pct Recovery = 78%  Analysis Date = 07/16/13 
 Pct Recovery = 78%  Analysis Date = 07/16/13 
 Pct Recovery = 78%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/14/13 
 Pct Recovery = 78%  Analysis Date = 07/11/13 
 Pct Recovery = 78%  Analysis Date = 07/11/13 
 Pct Recovery = 78%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/06/13 
 Pct Recovery = 79%  Analysis Date = 07/06/13 
 Pct Recovery = 79%  Analysis Date = 07/04/13 
 Pct Recovery = 79%  Analysis Date = 07/04/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 07/02/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/10/13 
 Pct Recovery = 81%  Analysis Date = 06/10/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/03/13 
 Pct Recovery = 81%  Analysis Date = 06/03/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/31/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/26/13 
 Pct Recovery = 82%  Analysis Date = 05/26/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/10/13 
 Pct Recovery = 83%  Analysis Date = 05/10/13 
 Pct Recovery = 83%  Analysis Date = 05/07/13 
 Pct Recovery = 83%  Analysis Date = 05/07/13 
 Pct Recovery = 83%  Analysis Date = 05/05/13 
 Pct Recovery = 83%  Analysis Date = 05/05/13 
 Pct Recovery = 83%  Analysis Date = 05/02/13 
 Pct Recovery = 83%  Analysis Date = 05/02/13 
 Pct Recovery = 83%  Analysis Date = 04/30/13 
 Pct Recovery = 83%  Analysis Date = 04/30/13 
 Pct Recovery = 83%  Analysis Date = 04/27/13 
 Pct Recovery = 83%  Analysis Date = 04/27/13 
 Pct Recovery = 83%  Analysis Date = 04/25/13 
 Pct Recovery = 83%  Analysis Date = 04/25/13 
 Pct Recovery = 83%  Analysis Date = 04/23/13 
 Pct Recovery = 83%  Analysis Date = 04/23/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/18/13 
 Pct Recovery = 83%  Analysis Date = 04/18/13 
 Pct Recovery = 83%  Analysis Date = 04/15/13 
 Pct Recovery = 83%  Analysis Date = 04/15/13 
 Pct Recovery = 83%  Analysis Date = 04/13/13 
 Pct Recovery = 83%  Analysis Date = 04/13/13 
 Pct Recovery = 83%  Analysis Date = 04/11/13 
 Pct Recovery = 83%  Analysis Date = 04/11/13 
 Pct Recovery = 83%  Analysis Date = 04/08/13 
 Pct Recovery = 83%  Analysis Date = 04/08/13 
 Pct Recovery = 83%  Analysis Date = 04/06/13 
 Pct Recovery = 83%  Analysis Date = 04/06/13 
 Pct Recovery = 83%  Analysis Date = 04/03/13 
 Pct Recovery = 83%  Analysis Date = 04/03/13 
 Pct Recovery = 83%  Analysis Date = 04/01/13 
 Pct Recovery = 83%  Analysis Date = 04/01/13 
 Pct Recovery = 83%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 82%  Analysis Date = 03/27/13 
 Pct Recovery = 82%  Analysis Date = 03/25/13 
 Pct Recovery = 82%  Analysis Date = 03/25/13 
 Pct Recovery = 82%  Analysis Date = 03/22/13 
 Pct Recovery = 82%  Analysis Date = 03/22/13 
 Pct Recovery = 82%  Analysis Date = 03/20/13 
 Pct Recovery = 82%  Analysis Date = 03/20/13 
 Pct Recovery = 82%  Analysis Date = 03/17/13 
 Pct Recovery = 82%  Analysis Date = 03/17/13 
 Pct Recovery = 82%  Analysis Date = 03/15/13 
 Pct Recovery = 82%  Analysis Date = 03/15/13 
 Pct Recovery = 82%  Analysis Date = 03/13/13 
 Pct Recovery = 82%  Analysis Date = 03/13/13 
 Pct Recovery = 82%  Analysis Date = 03/10/13 
 Pct Recovery = 82%  Analysis Date = 03/10/13 
 Pct Recovery = 82%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/05/13 
 Pct Recovery = 82%  Analysis Date = 03/05/13 
 Pct Recovery = 82%  Analysis Date = 03/03/13 
 Pct Recovery = 82%  Analysis Date = 03/03/13 
 Pct Recovery = 82%  Analysis Date = 03/01/13 
 Pct Recovery = 82%  Analysis Date = 03/01/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/24/13 
 Pct Recovery = 82%  Analysis Date = 02/24/13 
 Pct Recovery = 82%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 81%  Analysis Date = 02/19/13 
 Pct Recovery = 81%  Analysis Date = 02/19/13 
 Pct Recovery = 81%  Analysis Date = 02/17/13 
 Pct Recovery = 81%  Analysis Date = 02/17/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/14/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/12/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/09/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/07/13 
 Pct Recovery = 81%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/28/13 
 Pct Recovery = 80%  Analysis Date = 01/28/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 80%  Analysis Date = 01/23/13 
 Pct Recovery = 80%  Analysis Date = 01/23/13 
 Pct Recovery = 80%  Analysis Date = 01/21/13 
 Pct Recovery = 80%  Analysis Date = 01/21/13 
 Pct Recovery = 80%  Analysis Date = 01/19/13 
 Pct Recovery = 79%  Analysis Date = 01/19/13 
 Pct Recovery = 79%  Analysis Date = 01/16/13 
 Pct Recovery = 79%  Analysis Date = 01/16/13 
 Pct Recovery = 79%  Analysis Date = 01/14/13 
 Pct Recovery = 79%  Analysis Date = 01/14/13 
 Pct Recovery = 79%  Analysis Date = 01/11/13 
 Pct Recovery = 79%  Analysis Date = 01/11/13 
 Pct Recovery = 79%  Analysis Date = 01/09/13 
 Pct Recovery = 79%  Analysis Date = 01/09/13 
 Pct Recovery = 79%  Analysis Date = 01/07/13 
 Pct Recovery = 79%  Analysis Date = 01/07/13 
 Pct Recovery = 79%  Analysis Date = 01/04/13 
 Pct Recovery = 79%  Analysis Date = 01/04/13 
 Pct Recovery = 79%  Analysis Date = 01/02/13 
 Pct Recovery = 78%  Analysis Date = 01/02/13 
 Pct Recovery = 78%  Analysis Date = 12/30/12 
 Pct Recovery = 78%  Analysis Date = 12/30/12 
 Pct Recovery = 78%  Analysis Date = 12/28/12 
 Pct Recovery = 78%  Analysis Date = 12/28/12 
 Pct Recovery = 78%  Analysis Date = 12/26/12 
 Pct Recovery = 78%  Analysis Date = 12/26/12 
 Pct Recovery = 78%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/23/12 
 Pct Recovery = 78%  Analysis Date = 12/21/12 
 Pct Recovery = 78%  Analysis Date = 12/21/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/18/12 
 Pct Recovery = 78%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/14/12 
 Pct Recovery = 77%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NADALOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 82% . 82% 0%
>= Reporting Level 13 75% 11% 74% 7%
Total 14 76% 11% 76% 8%

Sample Statistics
NADALOL

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NEVIRAPINE
METHOD: LC9017 , TESTIDCODE: 68017LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 78%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 77%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 52%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 70%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 63%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 73%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 71%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 83%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 83%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 67%  Analysis Date = 04/09/14 
 Pct Recovery = 58%  Analysis Date = 04/07/14 
 Pct Recovery = 58%  Analysis Date = 04/07/14 
 Pct Recovery = 58%  Analysis Date = 04/05/14 
 Pct Recovery = 59%  Analysis Date = 04/05/14 
 Pct Recovery = 59%  Analysis Date = 04/03/14 
 Pct Recovery = 59%  Analysis Date = 04/03/14 
 Pct Recovery = 59%  Analysis Date = 04/01/14 
 Pct Recovery = 59%  Analysis Date = 04/01/14 
 Pct Recovery = 59%  Analysis Date = 03/30/14 
 Pct Recovery = 60%  Analysis Date = 03/30/14 
 Pct Recovery = 60%  Analysis Date = 03/28/14 
 Pct Recovery = 60%  Analysis Date = 03/28/14 
 Pct Recovery = 60%  Analysis Date = 03/26/14 
 Pct Recovery = 60%  Analysis Date = 03/26/14 
 Pct Recovery = 60%  Analysis Date = 03/24/14 
 Pct Recovery = 61%  Analysis Date = 03/24/14 
 Pct Recovery = 61%  Analysis Date = 03/22/14 
 Pct Recovery = 61%  Analysis Date = 03/22/14 
 Pct Recovery = 61%  Analysis Date = 03/20/14 
 Pct Recovery = 61%  Analysis Date = 03/20/14 
 Pct Recovery = 61%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/18/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/16/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/14/14 
 Pct Recovery = 62%  Analysis Date = 03/12/14 
 Pct Recovery = 63%  Analysis Date = 03/12/14 
 Pct Recovery = 63%  Analysis Date = 03/10/14 
 Pct Recovery = 63%  Analysis Date = 03/10/14 
 Pct Recovery = 63%  Analysis Date = 03/08/14 
 Pct Recovery = 63%  Analysis Date = 03/08/14 
 Pct Recovery = 63%  Analysis Date = 03/06/14 
 Pct Recovery = 64%  Analysis Date = 03/06/14 
 Pct Recovery = 64%  Analysis Date = 03/04/14 
 Pct Recovery = 64%  Analysis Date = 03/04/14 
 Pct Recovery = 64%  Analysis Date = 03/02/14 
 Pct Recovery = 64%  Analysis Date = 03/02/14 
 Pct Recovery = 64%  Analysis Date = 02/28/14 
 Pct Recovery = 65%  Analysis Date = 02/28/14 
 Pct Recovery = 65%  Analysis Date = 02/26/14 
 Pct Recovery = 65%  Analysis Date = 02/26/14 
 Pct Recovery = 65%  Analysis Date = 02/24/14 
 Pct Recovery = 65%  Analysis Date = 02/24/14 
 Pct Recovery = 65%  Analysis Date = 02/22/14 
 Pct Recovery = 66%  Analysis Date = 02/22/14 
 Pct Recovery = 66%  Analysis Date = 02/20/14 
 Pct Recovery = 66%  Analysis Date = 02/20/14 
 Pct Recovery = 66%  Analysis Date = 02/18/14 
 Pct Recovery = 66%  Analysis Date = 02/18/14 
 Pct Recovery = 66%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/14/14 
 Pct Recovery = 67%  Analysis Date = 02/14/14 
 Pct Recovery = 67%  Analysis Date = 02/12/14 
 Pct Recovery = 67%  Analysis Date = 02/12/14 
 Pct Recovery = 67%  Analysis Date = 02/10/14 
 Pct Recovery = 67%  Analysis Date = 02/10/14 
 Pct Recovery = 67%  Analysis Date = 02/08/14 
 Pct Recovery = 67%  Analysis Date = 02/08/14 
 Pct Recovery = 67%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/04/14 
 Pct Recovery = 68%  Analysis Date = 02/04/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 01/30/14 
 Pct Recovery = 68%  Analysis Date = 01/30/14 
 Pct Recovery = 68%  Analysis Date = 01/28/14 
 Pct Recovery = 69%  Analysis Date = 01/28/14 
 Pct Recovery = 69%  Analysis Date = 01/26/14 
 Pct Recovery = 69%  Analysis Date = 01/26/14 
 Pct Recovery = 69%  Analysis Date = 01/24/14 
 Pct Recovery = 69%  Analysis Date = 01/24/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/20/14 
 Pct Recovery = 69%  Analysis Date = 01/20/14 
 Pct Recovery = 69%  Analysis Date = 01/18/14 
 Pct Recovery = 70%  Analysis Date = 01/18/14 
 Pct Recovery = 70%  Analysis Date = 01/16/14 
 Pct Recovery = 70%  Analysis Date = 01/16/14 
 Pct Recovery = 70%  Analysis Date = 01/14/14 
 Pct Recovery = 70%  Analysis Date = 01/14/14 
 Pct Recovery = 70%  Analysis Date = 01/12/14 
 Pct Recovery = 70%  Analysis Date = 01/12/14 
 Pct Recovery = 70%  Analysis Date = 01/10/14 
 Pct Recovery = 70%  Analysis Date = 01/10/14 
 Pct Recovery = 70%  Analysis Date = 01/08/14 
 Pct Recovery = 71%  Analysis Date = 01/08/14 
 Pct Recovery = 71%  Analysis Date = 01/06/14 
 Pct Recovery = 71%  Analysis Date = 01/06/14 
 Pct Recovery = 71%  Analysis Date = 01/04/14 
 Pct Recovery = 71%  Analysis Date = 01/04/14 
 Pct Recovery = 71%  Analysis Date = 01/02/14 
 Pct Recovery = 71%  Analysis Date = 01/02/14 
 Pct Recovery = 71%  Analysis Date = 12/31/13 
 Pct Recovery = 71%  Analysis Date = 12/31/13 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/23/13 
 Pct Recovery = 72%  Analysis Date = 12/23/13 
 Pct Recovery = 72%  Analysis Date = 12/21/13 
 Pct Recovery = 72%  Analysis Date = 12/21/13 
 Pct Recovery = 72%  Analysis Date = 12/19/13 
 Pct Recovery = 72%  Analysis Date = 12/19/13 
 Pct Recovery = 72%  Analysis Date = 12/17/13 
 Pct Recovery = 72%  Analysis Date = 12/17/13 
 Pct Recovery = 72%  Analysis Date = 12/15/13 
 Pct Recovery = 72%  Analysis Date = 12/15/13 
 Pct Recovery = 72%  Analysis Date = 12/13/13 
 Pct Recovery = 72%  Analysis Date = 12/13/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/09/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/07/13 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 Pct Recovery = 73%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 12/01/13 
 Pct Recovery = 73%  Analysis Date = 12/01/13 
 Pct Recovery = 73%  Analysis Date = 11/29/13 
 Pct Recovery = 73%  Analysis Date = 11/29/13 
 Pct Recovery = 73%  Analysis Date = 11/27/13 
 Pct Recovery = 74%  Analysis Date = 11/27/13 
 Pct Recovery = 74%  Analysis Date = 11/24/13 
 Pct Recovery = 74%  Analysis Date = 11/24/13 
 Pct Recovery = 74%  Analysis Date = 11/22/13 
 Pct Recovery = 74%  Analysis Date = 11/22/13 
 Pct Recovery = 74%  Analysis Date = 11/20/13 
 Pct Recovery = 74%  Analysis Date = 11/20/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/14/13 
 Pct Recovery = 75%  Analysis Date = 11/14/13 
 Pct Recovery = 75%  Analysis Date = 11/12/13 
 Pct Recovery = 75%  Analysis Date = 11/12/13 
 Pct Recovery = 75%  Analysis Date = 11/10/13 
 Pct Recovery = 75%  Analysis Date = 11/10/13 
 Pct Recovery = 75%  Analysis Date = 11/08/13 
 Pct Recovery = 76%  Analysis Date = 11/08/13 
 Pct Recovery = 76%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/29/13 
 Pct Recovery = 77%  Analysis Date = 10/29/13 
 Pct Recovery = 77%  Analysis Date = 10/27/13 
 Pct Recovery = 77%  Analysis Date = 10/27/13 
 Pct Recovery = 77%  Analysis Date = 10/25/13 
 Pct Recovery = 77%  Analysis Date = 10/25/13 
 Pct Recovery = 77%  Analysis Date = 10/23/13 
 Pct Recovery = 77%  Analysis Date = 10/23/13 
 Pct Recovery = 77%  Analysis Date = 10/21/13 
 Pct Recovery = 77%  Analysis Date = 10/21/13 
 Pct Recovery = 77%  Analysis Date = 10/19/13 
 Pct Recovery = 77%  Analysis Date = 10/19/13 
 Pct Recovery = 77%  Analysis Date = 10/17/13 
 Pct Recovery = 77%  Analysis Date = 10/17/13 
 Pct Recovery = 77%  Analysis Date = 10/15/13 
 Pct Recovery = 77%  Analysis Date = 10/15/13 
 Pct Recovery = 77%  Analysis Date = 10/13/13 
 Pct Recovery = 78%  Analysis Date = 10/13/13 
 Pct Recovery = 78%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/09/13 
 Pct Recovery = 78%  Analysis Date = 10/09/13 
 Pct Recovery = 78%  Analysis Date = 10/07/13 
 Pct Recovery = 78%  Analysis Date = 10/07/13 
 Pct Recovery = 78%  Analysis Date = 10/05/13 
 Pct Recovery = 78%  Analysis Date = 10/05/13 
 Pct Recovery = 78%  Analysis Date = 10/03/13 
 Pct Recovery = 78%  Analysis Date = 10/03/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 78%  Analysis Date = 09/27/13 
 Pct Recovery = 78%  Analysis Date = 09/27/13 
 Pct Recovery = 78%  Analysis Date = 09/25/13 
 Pct Recovery = 78%  Analysis Date = 09/25/13 
 Pct Recovery = 78%  Analysis Date = 09/23/13 
 Pct Recovery = 79%  Analysis Date = 09/23/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/18/13 
 Pct Recovery = 79%  Analysis Date = 09/18/13 
 Pct Recovery = 79%  Analysis Date = 09/16/13 
 Pct Recovery = 79%  Analysis Date = 09/16/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/10/13 
 Pct Recovery = 79%  Analysis Date = 09/10/13 
 Pct Recovery = 79%  Analysis Date = 09/08/13 
 Pct Recovery = 79%  Analysis Date = 09/08/13 
 Pct Recovery = 79%  Analysis Date = 09/06/13 
 Pct Recovery = 79%  Analysis Date = 09/06/13 
 Pct Recovery = 79%  Analysis Date = 09/04/13 
 Pct Recovery = 79%  Analysis Date = 09/04/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 08/31/13 
 Pct Recovery = 80%  Analysis Date = 08/31/13 
 Pct Recovery = 80%  Analysis Date = 08/29/13 
 Pct Recovery = 80%  Analysis Date = 08/29/13 
 Pct Recovery = 80%  Analysis Date = 08/27/13 
 Pct Recovery = 80%  Analysis Date = 08/27/13 
 Pct Recovery = 80%  Analysis Date = 08/25/13 
 Pct Recovery = 80%  Analysis Date = 08/25/13 
 Pct Recovery = 80%  Analysis Date = 08/23/13 
 Pct Recovery = 80%  Analysis Date = 08/23/13 
 Pct Recovery = 80%  Analysis Date = 08/21/13 
 Pct Recovery = 80%  Analysis Date = 08/21/13 
 Pct Recovery = 80%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/17/13 
 Pct Recovery = 80%  Analysis Date = 08/17/13 
 Pct Recovery = 80%  Analysis Date = 08/15/13 
 Pct Recovery = 80%  Analysis Date = 08/15/13 
 Pct Recovery = 80%  Analysis Date = 08/13/13 
 Pct Recovery = 80%  Analysis Date = 08/13/13 
 Pct Recovery = 80%  Analysis Date = 08/11/13 
 Pct Recovery = 81%  Analysis Date = 08/11/13 
 Pct Recovery = 81%  Analysis Date = 08/09/13 
 Pct Recovery = 81%  Analysis Date = 08/09/13 
 Pct Recovery = 81%  Analysis Date = 08/07/13 
 Pct Recovery = 81%  Analysis Date = 08/07/13 
 Pct Recovery = 81%  Analysis Date = 08/05/13 
 Pct Recovery = 81%  Analysis Date = 08/05/13 
 Pct Recovery = 81%  Analysis Date = 08/03/13 
 Pct Recovery = 81%  Analysis Date = 08/03/13 
 Pct Recovery = 81%  Analysis Date = 08/01/13 
 Pct Recovery = 81%  Analysis Date = 08/01/13 
 Pct Recovery = 81%  Analysis Date = 07/30/13 
 Pct Recovery = 81%  Analysis Date = 07/30/13 
 Pct Recovery = 81%  Analysis Date = 07/28/13 
 Pct Recovery = 81%  Analysis Date = 07/28/13 
 Pct Recovery = 81%  Analysis Date = 07/26/13 
 Pct Recovery = 81%  Analysis Date = 07/26/13 
 Pct Recovery = 81%  Analysis Date = 07/24/13 
 Pct Recovery = 80%  Analysis Date = 07/24/13 
 Pct Recovery = 80%  Analysis Date = 07/22/13 
 Pct Recovery = 80%  Analysis Date = 07/22/13 
 Pct Recovery = 80%  Analysis Date = 07/20/13 
 Pct Recovery = 80%  Analysis Date = 07/20/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/09/13 
 Pct Recovery = 79%  Analysis Date = 07/07/13 
 Pct Recovery = 79%  Analysis Date = 07/07/13 
 Pct Recovery = 79%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/05/13 
 Pct Recovery = 79%  Analysis Date = 07/03/13 
 Pct Recovery = 79%  Analysis Date = 07/03/13 
 Pct Recovery = 79%  Analysis Date = 07/01/13 
 Pct Recovery = 79%  Analysis Date = 07/01/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/25/13 
 Pct Recovery = 79%  Analysis Date = 06/25/13 
 Pct Recovery = 79%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/23/13 
 Pct Recovery = 78%  Analysis Date = 06/21/13 
 Pct Recovery = 78%  Analysis Date = 06/21/13 
 Pct Recovery = 78%  Analysis Date = 06/19/13 
 Pct Recovery = 78%  Analysis Date = 06/19/13 
 Pct Recovery = 78%  Analysis Date = 06/17/13 
 Pct Recovery = 78%  Analysis Date = 06/17/13 
 Pct Recovery = 78%  Analysis Date = 06/15/13 
 Pct Recovery = 78%  Analysis Date = 06/15/13 
 Pct Recovery = 78%  Analysis Date = 06/13/13 
 Pct Recovery = 78%  Analysis Date = 06/13/13 
 Pct Recovery = 78%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/09/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/01/13 
 Pct Recovery = 77%  Analysis Date = 06/01/13 
 Pct Recovery = 77%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/30/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/28/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 76%  Analysis Date = 05/24/13 
 Pct Recovery = 76%  Analysis Date = 05/22/13 
 Pct Recovery = 76%  Analysis Date = 05/22/13 
 Pct Recovery = 76%  Analysis Date = 05/20/13 
 Pct Recovery = 76%  Analysis Date = 05/20/13 
 Pct Recovery = 76%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 75%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/29/13 
 Pct Recovery = 75%  Analysis Date = 04/27/13 
 Pct Recovery = 75%  Analysis Date = 04/27/13 
 Pct Recovery = 75%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/21/13 
 Pct Recovery = 74%  Analysis Date = 04/21/13 
 Pct Recovery = 74%  Analysis Date = 04/19/13 
 Pct Recovery = 74%  Analysis Date = 04/19/13 
 Pct Recovery = 74%  Analysis Date = 04/17/13 
 Pct Recovery = 74%  Analysis Date = 04/17/13 
 Pct Recovery = 74%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/05/13 
 Pct Recovery = 72%  Analysis Date = 04/05/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/26/13 
 Pct Recovery = 71%  Analysis Date = 03/26/13 
 Pct Recovery = 71%  Analysis Date = 03/24/13 
 Pct Recovery = 71%  Analysis Date = 03/24/13 
 Pct Recovery = 71%  Analysis Date = 03/22/13 
 Pct Recovery = 71%  Analysis Date = 03/22/13 
 Pct Recovery = 71%  Analysis Date = 03/20/13 
 Pct Recovery = 71%  Analysis Date = 03/20/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/16/13 
 Pct Recovery = 71%  Analysis Date = 03/16/13 
 Pct Recovery = 71%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/14/13 
 Pct Recovery = 70%  Analysis Date = 03/12/13 
 Pct Recovery = 70%  Analysis Date = 03/12/13 
 Pct Recovery = 70%  Analysis Date = 03/10/13 
 Pct Recovery = 70%  Analysis Date = 03/10/13 
 Pct Recovery = 70%  Analysis Date = 03/08/13 
 Pct Recovery = 70%  Analysis Date = 03/08/13 
 Pct Recovery = 70%  Analysis Date = 03/06/13 
 Pct Recovery = 70%  Analysis Date = 03/06/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 69%  Analysis Date = 03/04/13 
 Pct Recovery = 69%  Analysis Date = 03/02/13 
 Pct Recovery = 69%  Analysis Date = 03/02/13 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 Pct Recovery = 69%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NEVIRAPINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 72% 9% 73% 8%
Total 13 72% 9% 73% 8%

Sample Statistics
NEVIRAPINE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NICOTINE
METHOD: LC9017 , TESTIDCODE: 67493LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 25%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 71%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 159%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 42%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 78%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 62%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 60%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 93%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 48%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 83%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 50%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 40%  Analysis Date = 04/09/14 
 Pct Recovery = 50%  Analysis Date = 04/07/14 
 Pct Recovery = 50%  Analysis Date = 04/07/14 
 Pct Recovery = 50%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/02/14 
 Pct Recovery = 51%  Analysis Date = 04/02/14 
 Pct Recovery = 51%  Analysis Date = 03/31/14 
 Pct Recovery = 51%  Analysis Date = 03/31/14 
 Pct Recovery = 51%  Analysis Date = 03/28/14 
 Pct Recovery = 51%  Analysis Date = 03/28/14 
 Pct Recovery = 51%  Analysis Date = 03/26/14 
 Pct Recovery = 52%  Analysis Date = 03/26/14 
 Pct Recovery = 52%  Analysis Date = 03/24/14 
 Pct Recovery = 52%  Analysis Date = 03/24/14 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 Pct Recovery = 52%  Analysis Date = 03/21/14 
 Pct Recovery = 52%  Analysis Date = 03/19/14 
 Pct Recovery = 52%  Analysis Date = 03/19/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/16/14 
 Pct Recovery = 52%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/14/14 
 Pct Recovery = 53%  Analysis Date = 03/12/14 
 Pct Recovery = 53%  Analysis Date = 03/12/14 
 Pct Recovery = 53%  Analysis Date = 03/09/14 
 Pct Recovery = 53%  Analysis Date = 03/09/14 
 Pct Recovery = 53%  Analysis Date = 03/07/14 
 Pct Recovery = 53%  Analysis Date = 03/07/14 
 Pct Recovery = 53%  Analysis Date = 03/04/14 
 Pct Recovery = 54%  Analysis Date = 03/04/14 
 Pct Recovery = 54%  Analysis Date = 03/02/14 
 Pct Recovery = 54%  Analysis Date = 03/02/14 
 Pct Recovery = 54%  Analysis Date = 02/28/14 
 Pct Recovery = 54%  Analysis Date = 02/28/14 
 Pct Recovery = 54%  Analysis Date = 02/25/14 
 Pct Recovery = 54%  Analysis Date = 02/25/14 
 Pct Recovery = 54%  Analysis Date = 02/23/14 
 Pct Recovery = 54%  Analysis Date = 02/23/14 
 Pct Recovery = 54%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/18/14 
 Pct Recovery = 55%  Analysis Date = 02/18/14 
 Pct Recovery = 55%  Analysis Date = 02/15/14 
 Pct Recovery = 55%  Analysis Date = 02/15/14 
 Pct Recovery = 55%  Analysis Date = 02/13/14 
 Pct Recovery = 55%  Analysis Date = 02/13/14 
 Pct Recovery = 55%  Analysis Date = 02/11/14 
 Pct Recovery = 56%  Analysis Date = 02/11/14 
 Pct Recovery = 56%  Analysis Date = 02/08/14 
 Pct Recovery = 56%  Analysis Date = 02/08/14 
 Pct Recovery = 56%  Analysis Date = 02/06/14 
 Pct Recovery = 56%  Analysis Date = 02/06/14 
 Pct Recovery = 56%  Analysis Date = 02/03/14 
 Pct Recovery = 56%  Analysis Date = 02/03/14 
 Pct Recovery = 56%  Analysis Date = 02/01/14 
 Pct Recovery = 56%  Analysis Date = 02/01/14 
 Pct Recovery = 56%  Analysis Date = 01/30/14 
 Pct Recovery = 57%  Analysis Date = 01/30/14 
 Pct Recovery = 57%  Analysis Date = 01/27/14 
 Pct Recovery = 57%  Analysis Date = 01/27/14 
 Pct Recovery = 57%  Analysis Date = 01/25/14 
 Pct Recovery = 57%  Analysis Date = 01/25/14 
 Pct Recovery = 57%  Analysis Date = 01/22/14 
 Pct Recovery = 57%  Analysis Date = 01/22/14 
 Pct Recovery = 57%  Analysis Date = 01/20/14 
 Pct Recovery = 57%  Analysis Date = 01/20/14 
 Pct Recovery = 57%  Analysis Date = 01/18/14 
 Pct Recovery = 58%  Analysis Date = 01/18/14 
 Pct Recovery = 58%  Analysis Date = 01/15/14 
 Pct Recovery = 58%  Analysis Date = 01/15/14 
 Pct Recovery = 58%  Analysis Date = 01/13/14 
 Pct Recovery = 58%  Analysis Date = 01/13/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 58%  Analysis Date = 01/06/14 
 Pct Recovery = 58%  Analysis Date = 01/06/14 
 Pct Recovery = 58%  Analysis Date = 01/03/14 
 Pct Recovery = 59%  Analysis Date = 01/03/14 
 Pct Recovery = 59%  Analysis Date = 01/01/14 
 Pct Recovery = 59%  Analysis Date = 01/01/14 
 Pct Recovery = 59%  Analysis Date = 12/29/13 
 Pct Recovery = 59%  Analysis Date = 12/29/13 
 Pct Recovery = 59%  Analysis Date = 12/27/13 
 Pct Recovery = 59%  Analysis Date = 12/27/13 
 Pct Recovery = 59%  Analysis Date = 12/24/13 
 Pct Recovery = 59%  Analysis Date = 12/24/13 
 Pct Recovery = 59%  Analysis Date = 12/22/13 
 Pct Recovery = 59%  Analysis Date = 12/22/13 
 Pct Recovery = 59%  Analysis Date = 12/20/13 
 Pct Recovery = 59%  Analysis Date = 12/20/13 
 Pct Recovery = 59%  Analysis Date = 12/17/13 
 Pct Recovery = 60%  Analysis Date = 12/17/13 
 Pct Recovery = 60%  Analysis Date = 12/15/13 
 Pct Recovery = 60%  Analysis Date = 12/15/13 
 Pct Recovery = 60%  Analysis Date = 12/12/13 
 Pct Recovery = 60%  Analysis Date = 12/12/13 
 Pct Recovery = 60%  Analysis Date = 12/10/13 
 Pct Recovery = 60%  Analysis Date = 12/10/13 
 Pct Recovery = 60%  Analysis Date = 12/08/13 
 Pct Recovery = 60%  Analysis Date = 12/08/13 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 Pct Recovery = 60%  Analysis Date = 12/03/13 
 Pct Recovery = 60%  Analysis Date = 12/03/13 
 Pct Recovery = 60%  Analysis Date = 11/30/13 
 Pct Recovery = 60%  Analysis Date = 11/30/13 
 Pct Recovery = 60%  Analysis Date = 11/28/13 
 Pct Recovery = 61%  Analysis Date = 11/28/13 
 Pct Recovery = 61%  Analysis Date = 11/26/13 
 Pct Recovery = 61%  Analysis Date = 11/26/13 
 Pct Recovery = 61%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/21/13 
 Pct Recovery = 61%  Analysis Date = 11/21/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/11/13 
 Pct Recovery = 61%  Analysis Date = 11/11/13 
 Pct Recovery = 61%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 10/30/13 
 Pct Recovery = 62%  Analysis Date = 10/30/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 62%  Analysis Date = 10/25/13 
 Pct Recovery = 62%  Analysis Date = 10/25/13 
 Pct Recovery = 62%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/20/13 
 Pct Recovery = 63%  Analysis Date = 10/20/13 
 Pct Recovery = 63%  Analysis Date = 10/18/13 
 Pct Recovery = 63%  Analysis Date = 10/18/13 
 Pct Recovery = 63%  Analysis Date = 10/16/13 
 Pct Recovery = 63%  Analysis Date = 10/16/13 
 Pct Recovery = 63%  Analysis Date = 10/13/13 
 Pct Recovery = 63%  Analysis Date = 10/13/13 
 Pct Recovery = 63%  Analysis Date = 10/11/13 
 Pct Recovery = 64%  Analysis Date = 10/11/13 
 Pct Recovery = 64%  Analysis Date = 10/08/13 
 Pct Recovery = 64%  Analysis Date = 10/08/13 
 Pct Recovery = 64%  Analysis Date = 10/06/13 
 Pct Recovery = 64%  Analysis Date = 10/06/13 
 Pct Recovery = 64%  Analysis Date = 10/04/13 
 Pct Recovery = 64%  Analysis Date = 10/04/13 
 Pct Recovery = 64%  Analysis Date = 10/01/13 
 Pct Recovery = 64%  Analysis Date = 10/01/13 
 Pct Recovery = 64%  Analysis Date = 09/29/13 
 Pct Recovery = 65%  Analysis Date = 09/29/13 
 Pct Recovery = 65%  Analysis Date = 09/26/13 
 Pct Recovery = 65%  Analysis Date = 09/26/13 
 Pct Recovery = 65%  Analysis Date = 09/24/13 
 Pct Recovery = 65%  Analysis Date = 09/24/13 
 Pct Recovery = 65%  Analysis Date = 09/21/13 
 Pct Recovery = 65%  Analysis Date = 09/21/13 
 Pct Recovery = 65%  Analysis Date = 09/19/13 
 Pct Recovery = 65%  Analysis Date = 09/19/13 
 Pct Recovery = 65%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/14/13 
 Pct Recovery = 66%  Analysis Date = 09/14/13 
 Pct Recovery = 66%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/12/13 
 Pct Recovery = 66%  Analysis Date = 09/09/13 
 Pct Recovery = 66%  Analysis Date = 09/09/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/07/13 
 Pct Recovery = 66%  Analysis Date = 09/05/13 
 Pct Recovery = 66%  Analysis Date = 09/05/13 
 Pct Recovery = 66%  Analysis Date = 09/02/13 
 Pct Recovery = 67%  Analysis Date = 09/02/13 
 Pct Recovery = 67%  Analysis Date = 08/31/13 
 Pct Recovery = 67%  Analysis Date = 08/31/13 
 Pct Recovery = 67%  Analysis Date = 08/28/13 
 Pct Recovery = 67%  Analysis Date = 08/28/13 
 Pct Recovery = 67%  Analysis Date = 08/26/13 
 Pct Recovery = 67%  Analysis Date = 08/26/13 
 Pct Recovery = 67%  Analysis Date = 08/24/13 
 Pct Recovery = 67%  Analysis Date = 08/24/13 
 Pct Recovery = 67%  Analysis Date = 08/21/13 
 Pct Recovery = 67%  Analysis Date = 08/21/13 
 Pct Recovery = 67%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/16/13 
 Pct Recovery = 68%  Analysis Date = 08/16/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/11/13 
 Pct Recovery = 68%  Analysis Date = 08/11/13 
 Pct Recovery = 68%  Analysis Date = 08/09/13 
 Pct Recovery = 68%  Analysis Date = 08/09/13 
 Pct Recovery = 68%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/04/13 
 Pct Recovery = 69%  Analysis Date = 08/04/13 
 Pct Recovery = 69%  Analysis Date = 08/02/13 
 Pct Recovery = 69%  Analysis Date = 08/02/13 
 Pct Recovery = 69%  Analysis Date = 07/30/13 
 Pct Recovery = 69%  Analysis Date = 07/30/13 
 Pct Recovery = 69%  Analysis Date = 07/28/13 
 Pct Recovery = 69%  Analysis Date = 07/28/13 
 Pct Recovery = 69%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 70%  Analysis Date = 07/18/13 
 Pct Recovery = 70%  Analysis Date = 07/18/13 
 Pct Recovery = 70%  Analysis Date = 07/16/13 
 Pct Recovery = 70%  Analysis Date = 07/16/13 
 Pct Recovery = 70%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/11/13 
 Pct Recovery = 71%  Analysis Date = 07/11/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/06/13 
 Pct Recovery = 71%  Analysis Date = 07/06/13 
 Pct Recovery = 71%  Analysis Date = 07/04/13 
 Pct Recovery = 71%  Analysis Date = 07/04/13 
 Pct Recovery = 71%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 06/29/13 
 Pct Recovery = 72%  Analysis Date = 06/29/13 
 Pct Recovery = 72%  Analysis Date = 06/27/13 
 Pct Recovery = 72%  Analysis Date = 06/27/13 
 Pct Recovery = 72%  Analysis Date = 06/24/13 
 Pct Recovery = 72%  Analysis Date = 06/24/13 
 Pct Recovery = 72%  Analysis Date = 06/22/13 
 Pct Recovery = 72%  Analysis Date = 06/22/13 
 Pct Recovery = 72%  Analysis Date = 06/19/13 
 Pct Recovery = 73%  Analysis Date = 06/19/13 
 Pct Recovery = 73%  Analysis Date = 06/17/13 
 Pct Recovery = 73%  Analysis Date = 06/17/13 
 Pct Recovery = 73%  Analysis Date = 06/15/13 
 Pct Recovery = 73%  Analysis Date = 06/15/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/10/13 
 Pct Recovery = 73%  Analysis Date = 06/10/13 
 Pct Recovery = 73%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/03/13 
 Pct Recovery = 74%  Analysis Date = 06/03/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/26/13 
 Pct Recovery = 75%  Analysis Date = 05/26/13 
 Pct Recovery = 75%  Analysis Date = 05/24/13 
 Pct Recovery = 75%  Analysis Date = 05/24/13 
 Pct Recovery = 75%  Analysis Date = 05/22/13 
 Pct Recovery = 75%  Analysis Date = 05/22/13 
 Pct Recovery = 75%  Analysis Date = 05/19/13 
 Pct Recovery = 75%  Analysis Date = 05/19/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/10/13 
 Pct Recovery = 76%  Analysis Date = 05/10/13 
 Pct Recovery = 76%  Analysis Date = 05/07/13 
 Pct Recovery = 76%  Analysis Date = 05/07/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 Pct Recovery = 77%  Analysis Date = 04/30/13 
 Pct Recovery = 77%  Analysis Date = 04/30/13 
 Pct Recovery = 77%  Analysis Date = 04/27/13 
 Pct Recovery = 78%  Analysis Date = 04/27/13 
 Pct Recovery = 78%  Analysis Date = 04/25/13 
 Pct Recovery = 79%  Analysis Date = 04/25/13 
 Pct Recovery = 79%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/20/13 
 Pct Recovery = 79%  Analysis Date = 04/20/13 
 Pct Recovery = 79%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/13/13 
 Pct Recovery = 81%  Analysis Date = 04/11/13 
 Pct Recovery = 81%  Analysis Date = 04/11/13 
 Pct Recovery = 81%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/08/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/06/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/03/13 
 Pct Recovery = 82%  Analysis Date = 04/01/13 
 Pct Recovery = 83%  Analysis Date = 04/01/13 
 Pct Recovery = 83%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/30/13 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 Pct Recovery = 84%  Analysis Date = 03/27/13 
 Pct Recovery = 84%  Analysis Date = 03/25/13 
 Pct Recovery = 84%  Analysis Date = 03/25/13 
 Pct Recovery = 84%  Analysis Date = 03/22/13 
 Pct Recovery = 83%  Analysis Date = 03/22/13 
 Pct Recovery = 83%  Analysis Date = 03/20/13 
 Pct Recovery = 83%  Analysis Date = 03/20/13 
 Pct Recovery = 83%  Analysis Date = 03/17/13 
 Pct Recovery = 83%  Analysis Date = 03/17/13 
 Pct Recovery = 83%  Analysis Date = 03/15/13 
 Pct Recovery = 83%  Analysis Date = 03/15/13 
 Pct Recovery = 83%  Analysis Date = 03/13/13 
 Pct Recovery = 82%  Analysis Date = 03/13/13 
 Pct Recovery = 82%  Analysis Date = 03/10/13 
 Pct Recovery = 82%  Analysis Date = 03/10/13 
 Pct Recovery = 82%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/05/13 
 Pct Recovery = 82%  Analysis Date = 03/05/13 
 Pct Recovery = 82%  Analysis Date = 03/03/13 
 Pct Recovery = 81%  Analysis Date = 03/03/13 
 Pct Recovery = 81%  Analysis Date = 03/01/13 
 Pct Recovery = 81%  Analysis Date = 03/01/13 
 Pct Recovery = 81%  Analysis Date = 02/26/13 
 Pct Recovery = 81%  Analysis Date = 02/26/13 
 Pct Recovery = 81%  Analysis Date = 02/24/13 
 Pct Recovery = 81%  Analysis Date = 02/24/13 
 Pct Recovery = 81%  Analysis Date = 02/21/13 
 Pct Recovery = 80%  Analysis Date = 02/21/13 
 Pct Recovery = 80%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 79%  Analysis Date = 02/12/13 
 Pct Recovery = 79%  Analysis Date = 02/09/13 
 Pct Recovery = 79%  Analysis Date = 02/09/13 
 Pct Recovery = 79%  Analysis Date = 02/07/13 
 Pct Recovery = 79%  Analysis Date = 02/07/13 
 Pct Recovery = 79%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/05/13 
 Pct Recovery = 79%  Analysis Date = 02/02/13 
 Pct Recovery = 78%  Analysis Date = 02/02/13 
 Pct Recovery = 78%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/23/13 
 Pct Recovery = 77%  Analysis Date = 01/23/13 
 Pct Recovery = 77%  Analysis Date = 01/21/13 
 Pct Recovery = 76%  Analysis Date = 01/21/13 
 Pct Recovery = 76%  Analysis Date = 01/19/13 
 Pct Recovery = 75%  Analysis Date = 01/19/13 
 Pct Recovery = 75%  Analysis Date = 01/16/13 
 Pct Recovery = 74%  Analysis Date = 01/16/13 
 Pct Recovery = 74%  Analysis Date = 01/14/13 
 Pct Recovery = 72%  Analysis Date = 01/14/13 
 Pct Recovery = 72%  Analysis Date = 01/11/13 
 Pct Recovery = 71%  Analysis Date = 01/11/13 
 Pct Recovery = 71%  Analysis Date = 01/09/13 
 Pct Recovery = 70%  Analysis Date = 01/09/13 
 Pct Recovery = 70%  Analysis Date = 01/07/13 
 Pct Recovery = 69%  Analysis Date = 01/07/13 
 Pct Recovery = 69%  Analysis Date = 01/04/13 
 Pct Recovery = 67%  Analysis Date = 01/04/13 
 Pct Recovery = 67%  Analysis Date = 01/02/13 
 Pct Recovery = 66%  Analysis Date = 01/02/13 
 Pct Recovery = 66%  Analysis Date = 12/30/12 
 Pct Recovery = 65%  Analysis Date = 12/30/12 
 Pct Recovery = 65%  Analysis Date = 12/28/12 
 Pct Recovery = 64%  Analysis Date = 12/28/12 
 Pct Recovery = 64%  Analysis Date = 12/26/12 
 Pct Recovery = 62%  Analysis Date = 12/26/12 
 Pct Recovery = 62%  Analysis Date = 12/23/12 
 Pct Recovery = 61%  Analysis Date = 12/23/12 
 Pct Recovery = 61%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/16/12 
 Pct Recovery = 57%  Analysis Date = 12/16/12 
 Pct Recovery = 57%  Analysis Date = 12/14/12 
 Pct Recovery = 56%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NICOTINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 40% . 40% 0%
>= Reporting Level 13 72% 33% 71% 24%
Total 14 70% 32% 66% 26%

Sample Statistics
NICOTINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 2 12% 2 out of 17

OBSP Determination:
NIZATIDINE
METHOD: LC9017 , TESTIDCODE: 67479LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 71%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 61%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 147%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 48%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 82%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 30%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 36%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 45%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 78%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 49%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 47%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 04/10/14 
 Pct Recovery = 37%  Analysis Date = 04/07/14 
 Pct Recovery = 37%  Analysis Date = 04/07/14 
 Pct Recovery = 37%  Analysis Date = 04/05/14 
 Pct Recovery = 37%  Analysis Date = 04/05/14 
 Pct Recovery = 37%  Analysis Date = 04/03/14 
 Pct Recovery = 38%  Analysis Date = 04/03/14 
 Pct Recovery = 38%  Analysis Date = 04/01/14 
 Pct Recovery = 38%  Analysis Date = 04/01/14 
 Pct Recovery = 38%  Analysis Date = 03/29/14 
 Pct Recovery = 38%  Analysis Date = 03/29/14 
 Pct Recovery = 38%  Analysis Date = 03/27/14 
 Pct Recovery = 38%  Analysis Date = 03/27/14 
 Pct Recovery = 38%  Analysis Date = 03/25/14 
 Pct Recovery = 38%  Analysis Date = 03/25/14 
 Pct Recovery = 38%  Analysis Date = 03/23/14 
 Pct Recovery = 38%  Analysis Date = 03/23/14 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 Pct Recovery = 39%  Analysis Date = 03/21/14 
 Pct Recovery = 39%  Analysis Date = 03/18/14 
 Pct Recovery = 39%  Analysis Date = 03/18/14 
 Pct Recovery = 39%  Analysis Date = 03/16/14 
 Pct Recovery = 39%  Analysis Date = 03/16/14 
 Pct Recovery = 39%  Analysis Date = 03/14/14 
 Pct Recovery = 39%  Analysis Date = 03/14/14 
 Pct Recovery = 39%  Analysis Date = 03/12/14 
 Pct Recovery = 39%  Analysis Date = 03/12/14 
 Pct Recovery = 39%  Analysis Date = 03/10/14 
 Pct Recovery = 39%  Analysis Date = 03/10/14 
 Pct Recovery = 39%  Analysis Date = 03/07/14 
 Pct Recovery = 40%  Analysis Date = 03/07/14 
 Pct Recovery = 40%  Analysis Date = 03/05/14 
 Pct Recovery = 40%  Analysis Date = 03/05/14 
 Pct Recovery = 40%  Analysis Date = 03/03/14 
 Pct Recovery = 40%  Analysis Date = 03/03/14 
 Pct Recovery = 40%  Analysis Date = 03/01/14 
 Pct Recovery = 40%  Analysis Date = 03/01/14 
 Pct Recovery = 40%  Analysis Date = 02/27/14 
 Pct Recovery = 40%  Analysis Date = 02/27/14 
 Pct Recovery = 40%  Analysis Date = 02/24/14 
 Pct Recovery = 41%  Analysis Date = 02/24/14 
 Pct Recovery = 41%  Analysis Date = 02/22/14 
 Pct Recovery = 41%  Analysis Date = 02/22/14 
 Pct Recovery = 41%  Analysis Date = 02/20/14 
 Pct Recovery = 41%  Analysis Date = 02/20/14 
 Pct Recovery = 41%  Analysis Date = 02/18/14 
 Pct Recovery = 41%  Analysis Date = 02/18/14 
 Pct Recovery = 41%  Analysis Date = 02/16/14 
 Pct Recovery = 41%  Analysis Date = 02/16/14 
 Pct Recovery = 41%  Analysis Date = 02/13/14 
 Pct Recovery = 41%  Analysis Date = 02/13/14 
 Pct Recovery = 41%  Analysis Date = 02/11/14 
 Pct Recovery = 42%  Analysis Date = 02/11/14 
 Pct Recovery = 42%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/09/14 
 Pct Recovery = 42%  Analysis Date = 02/07/14 
 Pct Recovery = 42%  Analysis Date = 02/07/14 
 Pct Recovery = 42%  Analysis Date = 02/05/14 
 Pct Recovery = 42%  Analysis Date = 02/05/14 
 Pct Recovery = 42%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/31/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/27/14 
 Pct Recovery = 43%  Analysis Date = 01/27/14 
 Pct Recovery = 43%  Analysis Date = 01/25/14 
 Pct Recovery = 43%  Analysis Date = 01/25/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/20/14 
 Pct Recovery = 43%  Analysis Date = 01/20/14 
 Pct Recovery = 43%  Analysis Date = 01/18/14 
 Pct Recovery = 44%  Analysis Date = 01/18/14 
 Pct Recovery = 44%  Analysis Date = 01/16/14 
 Pct Recovery = 44%  Analysis Date = 01/16/14 
 Pct Recovery = 44%  Analysis Date = 01/14/14 
 Pct Recovery = 44%  Analysis Date = 01/14/14 
 Pct Recovery = 44%  Analysis Date = 01/11/14 
 Pct Recovery = 44%  Analysis Date = 01/11/14 
 Pct Recovery = 44%  Analysis Date = 01/09/14 
 Pct Recovery = 44%  Analysis Date = 01/09/14 
 Pct Recovery = 44%  Analysis Date = 01/07/14 
 Pct Recovery = 45%  Analysis Date = 01/07/14 
 Pct Recovery = 45%  Analysis Date = 01/05/14 
 Pct Recovery = 45%  Analysis Date = 01/05/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 12/31/13 
 Pct Recovery = 45%  Analysis Date = 12/31/13 
 Pct Recovery = 45%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/27/13 
 Pct Recovery = 46%  Analysis Date = 12/27/13 
 Pct Recovery = 46%  Analysis Date = 12/25/13 
 Pct Recovery = 46%  Analysis Date = 12/25/13 
 Pct Recovery = 46%  Analysis Date = 12/22/13 
 Pct Recovery = 46%  Analysis Date = 12/22/13 
 Pct Recovery = 46%  Analysis Date = 12/20/13 
 Pct Recovery = 47%  Analysis Date = 12/20/13 
 Pct Recovery = 47%  Analysis Date = 12/18/13 
 Pct Recovery = 47%  Analysis Date = 12/18/13 
 Pct Recovery = 47%  Analysis Date = 12/16/13 
 Pct Recovery = 47%  Analysis Date = 12/16/13 
 Pct Recovery = 47%  Analysis Date = 12/14/13 
 Pct Recovery = 47%  Analysis Date = 12/14/13 
 Pct Recovery = 47%  Analysis Date = 12/11/13 
 Pct Recovery = 48%  Analysis Date = 12/11/13 
 Pct Recovery = 48%  Analysis Date = 12/09/13 
 Pct Recovery = 48%  Analysis Date = 12/09/13 
 Pct Recovery = 48%  Analysis Date = 12/07/13 
 Pct Recovery = 48%  Analysis Date = 12/07/13 
 Pct Recovery = 48%  Analysis Date = 12/05/13 
 Pct Recovery = 48%  Analysis Date = 12/05/13 
 Pct Recovery = 48%  Analysis Date = 12/03/13 
 Pct Recovery = 48%  Analysis Date = 12/03/13 
 Pct Recovery = 48%  Analysis Date = 11/30/13 
 Pct Recovery = 49%  Analysis Date = 11/30/13 
 Pct Recovery = 49%  Analysis Date = 11/28/13 
 Pct Recovery = 49%  Analysis Date = 11/28/13 
 Pct Recovery = 49%  Analysis Date = 11/26/13 
 Pct Recovery = 49%  Analysis Date = 11/26/13 
 Pct Recovery = 49%  Analysis Date = 11/24/13 
 Pct Recovery = 49%  Analysis Date = 11/24/13 
 Pct Recovery = 49%  Analysis Date = 11/22/13 
 Pct Recovery = 50%  Analysis Date = 11/22/13 
 Pct Recovery = 50%  Analysis Date = 11/19/13 
 Pct Recovery = 50%  Analysis Date = 11/19/13 
 Pct Recovery = 50%  Analysis Date = 11/17/13 
 Pct Recovery = 50%  Analysis Date = 11/17/13 
 Pct Recovery = 50%  Analysis Date = 11/15/13 
 Pct Recovery = 50%  Analysis Date = 11/15/13 
 Pct Recovery = 50%  Analysis Date = 11/13/13 
 Pct Recovery = 51%  Analysis Date = 11/13/13 
 Pct Recovery = 51%  Analysis Date = 11/11/13 
 Pct Recovery = 51%  Analysis Date = 11/11/13 
 Pct Recovery = 51%  Analysis Date = 11/08/13 
 Pct Recovery = 51%  Analysis Date = 11/08/13 
 Pct Recovery = 51%  Analysis Date = 11/06/13 
 Pct Recovery = 51%  Analysis Date = 11/06/13 
 Pct Recovery = 51%  Analysis Date = 11/04/13 
 Pct Recovery = 52%  Analysis Date = 11/04/13 
 Pct Recovery = 52%  Analysis Date = 11/02/13 
 Pct Recovery = 52%  Analysis Date = 11/02/13 
 Pct Recovery = 52%  Analysis Date = 10/31/13 
 Pct Recovery = 52%  Analysis Date = 10/31/13 
 Pct Recovery = 52%  Analysis Date = 10/28/13 
 Pct Recovery = 52%  Analysis Date = 10/28/13 
 Pct Recovery = 52%  Analysis Date = 10/26/13 
 Pct Recovery = 52%  Analysis Date = 10/26/13 
 Pct Recovery = 52%  Analysis Date = 10/24/13 
 Pct Recovery = 53%  Analysis Date = 10/24/13 
 Pct Recovery = 53%  Analysis Date = 10/22/13 
 Pct Recovery = 53%  Analysis Date = 10/22/13 
 Pct Recovery = 53%  Analysis Date = 10/20/13 
 Pct Recovery = 53%  Analysis Date = 10/20/13 
 Pct Recovery = 53%  Analysis Date = 10/17/13 
 Pct Recovery = 53%  Analysis Date = 10/17/13 
 Pct Recovery = 53%  Analysis Date = 10/15/13 
 Pct Recovery = 53%  Analysis Date = 10/15/13 
 Pct Recovery = 53%  Analysis Date = 10/13/13 
 Pct Recovery = 54%  Analysis Date = 10/13/13 
 Pct Recovery = 54%  Analysis Date = 10/11/13 
 Pct Recovery = 54%  Analysis Date = 10/11/13 
 Pct Recovery = 54%  Analysis Date = 10/08/13 
 Pct Recovery = 54%  Analysis Date = 10/08/13 
 Pct Recovery = 54%  Analysis Date = 10/06/13 
 Pct Recovery = 54%  Analysis Date = 10/06/13 
 Pct Recovery = 54%  Analysis Date = 10/04/13 
 Pct Recovery = 54%  Analysis Date = 10/04/13 
 Pct Recovery = 54%  Analysis Date = 10/02/13 
 Pct Recovery = 55%  Analysis Date = 10/02/13 
 Pct Recovery = 55%  Analysis Date = 09/30/13 
 Pct Recovery = 55%  Analysis Date = 09/30/13 
 Pct Recovery = 55%  Analysis Date = 09/27/13 
 Pct Recovery = 55%  Analysis Date = 09/27/13 
 Pct Recovery = 55%  Analysis Date = 09/25/13 
 Pct Recovery = 55%  Analysis Date = 09/25/13 
 Pct Recovery = 55%  Analysis Date = 09/23/13 
 Pct Recovery = 55%  Analysis Date = 09/23/13 
 Pct Recovery = 55%  Analysis Date = 09/21/13 
 Pct Recovery = 56%  Analysis Date = 09/21/13 
 Pct Recovery = 56%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/19/13 
 Pct Recovery = 56%  Analysis Date = 09/16/13 
 Pct Recovery = 56%  Analysis Date = 09/16/13 
 Pct Recovery = 56%  Analysis Date = 09/14/13 
 Pct Recovery = 56%  Analysis Date = 09/14/13 
 Pct Recovery = 56%  Analysis Date = 09/12/13 
 Pct Recovery = 56%  Analysis Date = 09/12/13 
 Pct Recovery = 56%  Analysis Date = 09/10/13 
 Pct Recovery = 57%  Analysis Date = 09/10/13 
 Pct Recovery = 57%  Analysis Date = 09/08/13 
 Pct Recovery = 57%  Analysis Date = 09/08/13 
 Pct Recovery = 57%  Analysis Date = 09/05/13 
 Pct Recovery = 57%  Analysis Date = 09/05/13 
 Pct Recovery = 57%  Analysis Date = 09/03/13 
 Pct Recovery = 57%  Analysis Date = 09/03/13 
 Pct Recovery = 57%  Analysis Date = 09/01/13 
 Pct Recovery = 57%  Analysis Date = 09/01/13 
 Pct Recovery = 57%  Analysis Date = 08/30/13 
 Pct Recovery = 58%  Analysis Date = 08/30/13 
 Pct Recovery = 58%  Analysis Date = 08/28/13 
 Pct Recovery = 58%  Analysis Date = 08/28/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/25/13 
 Pct Recovery = 58%  Analysis Date = 08/23/13 
 Pct Recovery = 58%  Analysis Date = 08/23/13 
 Pct Recovery = 58%  Analysis Date = 08/21/13 
 Pct Recovery = 58%  Analysis Date = 08/21/13 
 Pct Recovery = 58%  Analysis Date = 08/19/13 
 Pct Recovery = 59%  Analysis Date = 08/19/13 
 Pct Recovery = 59%  Analysis Date = 08/17/13 
 Pct Recovery = 59%  Analysis Date = 08/17/13 
 Pct Recovery = 59%  Analysis Date = 08/14/13 
 Pct Recovery = 59%  Analysis Date = 08/14/13 
 Pct Recovery = 59%  Analysis Date = 08/12/13 
 Pct Recovery = 59%  Analysis Date = 08/12/13 
 Pct Recovery = 59%  Analysis Date = 08/10/13 
 Pct Recovery = 59%  Analysis Date = 08/10/13 
 Pct Recovery = 59%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/06/13 
 Pct Recovery = 59%  Analysis Date = 08/06/13 
 Pct Recovery = 59%  Analysis Date = 08/03/13 
 Pct Recovery = 59%  Analysis Date = 08/03/13 
 Pct Recovery = 59%  Analysis Date = 08/01/13 
 Pct Recovery = 59%  Analysis Date = 08/01/13 
 Pct Recovery = 59%  Analysis Date = 07/30/13 
 Pct Recovery = 59%  Analysis Date = 07/30/13 
 Pct Recovery = 59%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/26/13 
 Pct Recovery = 59%  Analysis Date = 07/26/13 
 Pct Recovery = 59%  Analysis Date = 07/23/13 
 Pct Recovery = 59%  Analysis Date = 07/23/13 
 Pct Recovery = 59%  Analysis Date = 07/21/13 
 Pct Recovery = 59%  Analysis Date = 07/21/13 
 Pct Recovery = 59%  Analysis Date = 07/19/13 
 Pct Recovery = 59%  Analysis Date = 07/19/13 
 Pct Recovery = 59%  Analysis Date = 07/17/13 
 Pct Recovery = 59%  Analysis Date = 07/17/13 
 Pct Recovery = 59%  Analysis Date = 07/14/13 
 Pct Recovery = 59%  Analysis Date = 07/14/13 
 Pct Recovery = 59%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/10/13 
 Pct Recovery = 59%  Analysis Date = 07/10/13 
 Pct Recovery = 59%  Analysis Date = 07/08/13 
 Pct Recovery = 59%  Analysis Date = 07/08/13 
 Pct Recovery = 59%  Analysis Date = 07/06/13 
 Pct Recovery = 59%  Analysis Date = 07/06/13 
 Pct Recovery = 59%  Analysis Date = 07/03/13 
 Pct Recovery = 59%  Analysis Date = 07/03/13 
 Pct Recovery = 59%  Analysis Date = 07/01/13 
 Pct Recovery = 59%  Analysis Date = 07/01/13 
 Pct Recovery = 59%  Analysis Date = 06/29/13 
 Pct Recovery = 59%  Analysis Date = 06/29/13 
 Pct Recovery = 59%  Analysis Date = 06/27/13 
 Pct Recovery = 59%  Analysis Date = 06/27/13 
 Pct Recovery = 59%  Analysis Date = 06/25/13 
 Pct Recovery = 59%  Analysis Date = 06/25/13 
 Pct Recovery = 59%  Analysis Date = 06/22/13 
 Pct Recovery = 59%  Analysis Date = 06/22/13 
 Pct Recovery = 59%  Analysis Date = 06/20/13 
 Pct Recovery = 59%  Analysis Date = 06/20/13 
 Pct Recovery = 59%  Analysis Date = 06/18/13 
 Pct Recovery = 59%  Analysis Date = 06/18/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/16/13 
 Pct Recovery = 59%  Analysis Date = 06/14/13 
 Pct Recovery = 59%  Analysis Date = 06/14/13 
 Pct Recovery = 59%  Analysis Date = 06/11/13 
 Pct Recovery = 59%  Analysis Date = 06/11/13 
 Pct Recovery = 59%  Analysis Date = 06/09/13 
 Pct Recovery = 59%  Analysis Date = 06/09/13 
 Pct Recovery = 59%  Analysis Date = 06/07/13 
 Pct Recovery = 59%  Analysis Date = 06/07/13 
 Pct Recovery = 59%  Analysis Date = 06/05/13 
 Pct Recovery = 59%  Analysis Date = 06/05/13 
 Pct Recovery = 59%  Analysis Date = 06/03/13 
 Pct Recovery = 59%  Analysis Date = 06/03/13 
 Pct Recovery = 59%  Analysis Date = 05/31/13 
 Pct Recovery = 59%  Analysis Date = 05/31/13 
 Pct Recovery = 59%  Analysis Date = 05/29/13 
 Pct Recovery = 59%  Analysis Date = 05/29/13 
 Pct Recovery = 59%  Analysis Date = 05/27/13 
 Pct Recovery = 59%  Analysis Date = 05/27/13 
 Pct Recovery = 59%  Analysis Date = 05/25/13 
 Pct Recovery = 59%  Analysis Date = 05/25/13 
 Pct Recovery = 59%  Analysis Date = 05/23/13 
 Pct Recovery = 59%  Analysis Date = 05/23/13 
 Pct Recovery = 59%  Analysis Date = 05/20/13 
 Pct Recovery = 59%  Analysis Date = 05/20/13 
 Pct Recovery = 59%  Analysis Date = 05/18/13 
 Pct Recovery = 59%  Analysis Date = 05/18/13 
 Pct Recovery = 59%  Analysis Date = 05/16/13 
 Pct Recovery = 59%  Analysis Date = 05/16/13 
 Pct Recovery = 59%  Analysis Date = 05/14/13 
 Pct Recovery = 59%  Analysis Date = 05/14/13 
 Pct Recovery = 59%  Analysis Date = 05/12/13 
 Pct Recovery = 59%  Analysis Date = 05/12/13 
 Pct Recovery = 59%  Analysis Date = 05/09/13 
 Pct Recovery = 59%  Analysis Date = 05/09/13 
 Pct Recovery = 59%  Analysis Date = 05/07/13 
 Pct Recovery = 59%  Analysis Date = 05/07/13 
 Pct Recovery = 59%  Analysis Date = 05/05/13 
 Pct Recovery = 59%  Analysis Date = 05/05/13 
 Pct Recovery = 59%  Analysis Date = 05/03/13 
 Pct Recovery = 59%  Analysis Date = 05/03/13 
 Pct Recovery = 59%  Analysis Date = 05/01/13 
 Pct Recovery = 60%  Analysis Date = 05/01/13 
 Pct Recovery = 60%  Analysis Date = 04/28/13 
 Pct Recovery = 61%  Analysis Date = 04/28/13 
 Pct Recovery = 61%  Analysis Date = 04/26/13 
 Pct Recovery = 62%  Analysis Date = 04/26/13 
 Pct Recovery = 62%  Analysis Date = 04/24/13 
 Pct Recovery = 63%  Analysis Date = 04/24/13 
 Pct Recovery = 63%  Analysis Date = 04/22/13 
 Pct Recovery = 64%  Analysis Date = 04/22/13 
 Pct Recovery = 64%  Analysis Date = 04/19/13 
 Pct Recovery = 66%  Analysis Date = 04/19/13 
 Pct Recovery = 66%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/17/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/13/13 
 Pct Recovery = 69%  Analysis Date = 04/11/13 
 Pct Recovery = 70%  Analysis Date = 04/11/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/04/13 
 Pct Recovery = 74%  Analysis Date = 04/04/13 
 Pct Recovery = 74%  Analysis Date = 04/02/13 
 Pct Recovery = 75%  Analysis Date = 04/02/13 
 Pct Recovery = 75%  Analysis Date = 03/31/13 
 Pct Recovery = 76%  Analysis Date = 03/31/13 
 Pct Recovery = 76%  Analysis Date = 03/28/13 
 Pct Recovery = 78%  Analysis Date = 03/28/13 
 Pct Recovery = 78%  Analysis Date = 03/26/13 
 Pct Recovery = 79%  Analysis Date = 03/26/13 
 Pct Recovery = 79%  Analysis Date = 03/24/13 
 Pct Recovery = 80%  Analysis Date = 03/24/13 
 Pct Recovery = 80%  Analysis Date = 03/22/13 
 Pct Recovery = 81%  Analysis Date = 03/22/13 
 Pct Recovery = 81%  Analysis Date = 03/20/13 
 Pct Recovery = 82%  Analysis Date = 03/20/13 
 Pct Recovery = 82%  Analysis Date = 03/17/13 
 Pct Recovery = 84%  Analysis Date = 03/17/13 
 Pct Recovery = 84%  Analysis Date = 03/15/13 
 Pct Recovery = 85%  Analysis Date = 03/15/13 
 Pct Recovery = 85%  Analysis Date = 03/13/13 
 Pct Recovery = 86%  Analysis Date = 03/13/13 
 Pct Recovery = 86%  Analysis Date = 03/11/13 
 Pct Recovery = 87%  Analysis Date = 03/11/13 
 Pct Recovery = 87%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/09/13 
 Pct Recovery = 88%  Analysis Date = 03/06/13 
 Pct Recovery = 89%  Analysis Date = 03/06/13 
 Pct Recovery = 89%  Analysis Date = 03/04/13 
 Pct Recovery = 91%  Analysis Date = 03/04/13 
 Pct Recovery = 91%  Analysis Date = 03/02/13 
 Pct Recovery = 92%  Analysis Date = 03/02/13 
 Pct Recovery = 92%  Analysis Date = 02/28/13 
 Pct Recovery = 93%  Analysis Date = 02/28/13 
 Pct Recovery = 93%  Analysis Date = 02/26/13 
 Pct Recovery = 94%  Analysis Date = 02/26/13 
 Pct Recovery = 94%  Analysis Date = 02/23/13 
 Pct Recovery = 95%  Analysis Date = 02/23/13 
 Pct Recovery = 95%  Analysis Date = 02/21/13 
 Pct Recovery = 97%  Analysis Date = 02/21/13 
 Pct Recovery = 97%  Analysis Date = 02/19/13 
 Pct Recovery = 98%  Analysis Date = 02/19/13 
 Pct Recovery = 98%  Analysis Date = 02/17/13 
 Pct Recovery = 99%  Analysis Date = 02/17/13 
 Pct Recovery = 99%  Analysis Date = 02/15/13 
 Pct Recovery = 100%  Analysis Date = 02/15/13 
 Pct Recovery = 100%  Analysis Date = 02/12/13 
 Pct Recovery = 101%  Analysis Date = 02/12/13 
 Pct Recovery = 101%  Analysis Date = 02/10/13 
 Pct Recovery = 102%  Analysis Date = 02/10/13 
 Pct Recovery = 102%  Analysis Date = 02/08/13 
 Pct Recovery = 104%  Analysis Date = 02/08/13 
 Pct Recovery = 104%  Analysis Date = 02/06/13 
 Pct Recovery = 105%  Analysis Date = 02/06/13 
 Pct Recovery = 105%  Analysis Date = 02/04/13 
 Pct Recovery = 106%  Analysis Date = 02/04/13 
 Pct Recovery = 106%  Analysis Date = 02/01/13 
 Pct Recovery = 107%  Analysis Date = 02/01/13 
 Pct Recovery = 107%  Analysis Date = 01/30/13 
 Pct Recovery = 108%  Analysis Date = 01/30/13 
 Pct Recovery = 108%  Analysis Date = 01/28/13 
 Pct Recovery = 110%  Analysis Date = 01/28/13 
 Pct Recovery = 110%  Analysis Date = 01/26/13 
 Pct Recovery = 111%  Analysis Date = 01/26/13 
 Pct Recovery = 111%  Analysis Date = 01/24/13 
 Pct Recovery = 112%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NIZATIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 64% 30% 61% 22%
Total 13 64% 30% 61% 22%

Sample Statistics
NIZATIDINE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 13 93% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NORDIAZEPAM
METHOD: LC9017 , TESTIDCODE: 68252LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 87%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 155%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 74%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 81%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 79%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 81%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 107%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 97%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 54%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 90%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 87%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 87%  Analysis Date = 04/09/14 
 Pct Recovery = 67%  Analysis Date = 04/07/14 
 Pct Recovery = 67%  Analysis Date = 04/07/14 
 Pct Recovery = 67%  Analysis Date = 04/05/14 
 Pct Recovery = 67%  Analysis Date = 04/05/14 
 Pct Recovery = 67%  Analysis Date = 04/02/14 
 Pct Recovery = 68%  Analysis Date = 04/02/14 
 Pct Recovery = 68%  Analysis Date = 03/31/14 
 Pct Recovery = 68%  Analysis Date = 03/31/14 
 Pct Recovery = 68%  Analysis Date = 03/28/14 
 Pct Recovery = 68%  Analysis Date = 03/28/14 
 Pct Recovery = 68%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/18/14 
 Pct Recovery = 71%  Analysis Date = 02/18/14 
 Pct Recovery = 71%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 73%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 75%  Analysis Date = 01/10/14 
 Pct Recovery = 75%  Analysis Date = 01/08/14 
 Pct Recovery = 75%  Analysis Date = 01/08/14 
 Pct Recovery = 75%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/01/14 
 Pct Recovery = 75%  Analysis Date = 01/01/14 
 Pct Recovery = 75%  Analysis Date = 12/29/13 
 Pct Recovery = 75%  Analysis Date = 12/29/13 
 Pct Recovery = 75%  Analysis Date = 12/27/13 
 Pct Recovery = 75%  Analysis Date = 12/27/13 
 Pct Recovery = 75%  Analysis Date = 12/24/13 
 Pct Recovery = 75%  Analysis Date = 12/24/13 
 Pct Recovery = 75%  Analysis Date = 12/22/13 
 Pct Recovery = 76%  Analysis Date = 12/22/13 
 Pct Recovery = 76%  Analysis Date = 12/20/13 
 Pct Recovery = 76%  Analysis Date = 12/20/13 
 Pct Recovery = 76%  Analysis Date = 12/17/13 
 Pct Recovery = 76%  Analysis Date = 12/17/13 
 Pct Recovery = 76%  Analysis Date = 12/15/13 
 Pct Recovery = 76%  Analysis Date = 12/15/13 
 Pct Recovery = 76%  Analysis Date = 12/12/13 
 Pct Recovery = 76%  Analysis Date = 12/12/13 
 Pct Recovery = 76%  Analysis Date = 12/10/13 
 Pct Recovery = 76%  Analysis Date = 12/10/13 
 Pct Recovery = 76%  Analysis Date = 12/08/13 
 Pct Recovery = 76%  Analysis Date = 12/08/13 
 Pct Recovery = 76%  Analysis Date = 12/05/13 
 Pct Recovery = 76%  Analysis Date = 12/05/13 
 Pct Recovery = 76%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 12/03/13 
 Pct Recovery = 76%  Analysis Date = 11/30/13 
 Pct Recovery = 77%  Analysis Date = 11/30/13 
 Pct Recovery = 77%  Analysis Date = 11/28/13 
 Pct Recovery = 77%  Analysis Date = 11/28/13 
 Pct Recovery = 77%  Analysis Date = 11/26/13 
 Pct Recovery = 77%  Analysis Date = 11/26/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/23/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/21/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/18/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/16/13 
 Pct Recovery = 77%  Analysis Date = 11/13/13 
 Pct Recovery = 77%  Analysis Date = 11/13/13 
 Pct Recovery = 77%  Analysis Date = 11/11/13 
 Pct Recovery = 78%  Analysis Date = 11/11/13 
 Pct Recovery = 78%  Analysis Date = 11/09/13 
 Pct Recovery = 78%  Analysis Date = 11/09/13 
 Pct Recovery = 78%  Analysis Date = 11/06/13 
 Pct Recovery = 78%  Analysis Date = 11/06/13 
 Pct Recovery = 78%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/01/13 
 Pct Recovery = 78%  Analysis Date = 11/01/13 
 Pct Recovery = 78%  Analysis Date = 10/30/13 
 Pct Recovery = 78%  Analysis Date = 10/30/13 
 Pct Recovery = 78%  Analysis Date = 10/28/13 
 Pct Recovery = 78%  Analysis Date = 10/28/13 
 Pct Recovery = 78%  Analysis Date = 10/25/13 
 Pct Recovery = 78%  Analysis Date = 10/25/13 
 Pct Recovery = 78%  Analysis Date = 10/23/13 
 Pct Recovery = 78%  Analysis Date = 10/23/13 
 Pct Recovery = 78%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/18/13 
 Pct Recovery = 79%  Analysis Date = 10/18/13 
 Pct Recovery = 79%  Analysis Date = 10/16/13 
 Pct Recovery = 79%  Analysis Date = 10/16/13 
 Pct Recovery = 79%  Analysis Date = 10/13/13 
 Pct Recovery = 79%  Analysis Date = 10/13/13 
 Pct Recovery = 79%  Analysis Date = 10/11/13 
 Pct Recovery = 79%  Analysis Date = 10/11/13 
 Pct Recovery = 79%  Analysis Date = 10/08/13 
 Pct Recovery = 79%  Analysis Date = 10/08/13 
 Pct Recovery = 79%  Analysis Date = 10/06/13 
 Pct Recovery = 79%  Analysis Date = 10/06/13 
 Pct Recovery = 79%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/01/13 
 Pct Recovery = 79%  Analysis Date = 10/01/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 80%  Analysis Date = 09/02/13 
 Pct Recovery = 80%  Analysis Date = 09/02/13 
 Pct Recovery = 80%  Analysis Date = 08/31/13 
 Pct Recovery = 80%  Analysis Date = 08/31/13 
 Pct Recovery = 80%  Analysis Date = 08/28/13 
 Pct Recovery = 80%  Analysis Date = 08/28/13 
 Pct Recovery = 80%  Analysis Date = 08/26/13 
 Pct Recovery = 80%  Analysis Date = 08/26/13 
 Pct Recovery = 80%  Analysis Date = 08/24/13 
 Pct Recovery = 80%  Analysis Date = 08/24/13 
 Pct Recovery = 80%  Analysis Date = 08/21/13 
 Pct Recovery = 80%  Analysis Date = 08/21/13 
 Pct Recovery = 80%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/16/13 
 Pct Recovery = 81%  Analysis Date = 08/16/13 
 Pct Recovery = 81%  Analysis Date = 08/14/13 
 Pct Recovery = 81%  Analysis Date = 08/14/13 
 Pct Recovery = 81%  Analysis Date = 08/11/13 
 Pct Recovery = 81%  Analysis Date = 08/11/13 
 Pct Recovery = 81%  Analysis Date = 08/09/13 
 Pct Recovery = 81%  Analysis Date = 08/09/13 
 Pct Recovery = 81%  Analysis Date = 08/07/13 
 Pct Recovery = 81%  Analysis Date = 08/07/13 
 Pct Recovery = 81%  Analysis Date = 08/04/13 
 Pct Recovery = 81%  Analysis Date = 08/04/13 
 Pct Recovery = 81%  Analysis Date = 08/02/13 
 Pct Recovery = 81%  Analysis Date = 08/02/13 
 Pct Recovery = 81%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/18/13 
 Pct Recovery = 82%  Analysis Date = 07/18/13 
 Pct Recovery = 82%  Analysis Date = 07/16/13 
 Pct Recovery = 83%  Analysis Date = 07/16/13 
 Pct Recovery = 83%  Analysis Date = 07/14/13 
 Pct Recovery = 83%  Analysis Date = 07/14/13 
 Pct Recovery = 83%  Analysis Date = 07/11/13 
 Pct Recovery = 83%  Analysis Date = 07/11/13 
 Pct Recovery = 83%  Analysis Date = 07/09/13 
 Pct Recovery = 83%  Analysis Date = 07/09/13 
 Pct Recovery = 83%  Analysis Date = 07/06/13 
 Pct Recovery = 83%  Analysis Date = 07/06/13 
 Pct Recovery = 83%  Analysis Date = 07/04/13 
 Pct Recovery = 83%  Analysis Date = 07/04/13 
 Pct Recovery = 83%  Analysis Date = 07/02/13 
 Pct Recovery = 84%  Analysis Date = 07/02/13 
 Pct Recovery = 84%  Analysis Date = 06/29/13 
 Pct Recovery = 84%  Analysis Date = 06/29/13 
 Pct Recovery = 84%  Analysis Date = 06/27/13 
 Pct Recovery = 84%  Analysis Date = 06/27/13 
 Pct Recovery = 84%  Analysis Date = 06/24/13 
 Pct Recovery = 84%  Analysis Date = 06/24/13 
 Pct Recovery = 84%  Analysis Date = 06/22/13 
 Pct Recovery = 84%  Analysis Date = 06/22/13 
 Pct Recovery = 84%  Analysis Date = 06/19/13 
 Pct Recovery = 84%  Analysis Date = 06/19/13 
 Pct Recovery = 84%  Analysis Date = 06/17/13 
 Pct Recovery = 85%  Analysis Date = 06/17/13 
 Pct Recovery = 85%  Analysis Date = 06/15/13 
 Pct Recovery = 85%  Analysis Date = 06/15/13 
 Pct Recovery = 85%  Analysis Date = 06/12/13 
 Pct Recovery = 85%  Analysis Date = 06/12/13 
 Pct Recovery = 85%  Analysis Date = 06/10/13 
 Pct Recovery = 85%  Analysis Date = 06/10/13 
 Pct Recovery = 85%  Analysis Date = 06/07/13 
 Pct Recovery = 85%  Analysis Date = 06/07/13 
 Pct Recovery = 85%  Analysis Date = 06/05/13 
 Pct Recovery = 85%  Analysis Date = 06/05/13 
 Pct Recovery = 85%  Analysis Date = 06/03/13 
 Pct Recovery = 85%  Analysis Date = 06/03/13 
 Pct Recovery = 85%  Analysis Date = 05/31/13 
 Pct Recovery = 86%  Analysis Date = 05/31/13 
 Pct Recovery = 86%  Analysis Date = 05/29/13 
 Pct Recovery = 86%  Analysis Date = 05/29/13 
 Pct Recovery = 86%  Analysis Date = 05/26/13 
 Pct Recovery = 86%  Analysis Date = 05/26/13 
 Pct Recovery = 86%  Analysis Date = 05/24/13 
 Pct Recovery = 86%  Analysis Date = 05/24/13 
 Pct Recovery = 86%  Analysis Date = 05/22/13 
 Pct Recovery = 86%  Analysis Date = 05/22/13 
 Pct Recovery = 86%  Analysis Date = 05/19/13 
 Pct Recovery = 86%  Analysis Date = 05/19/13 
 Pct Recovery = 86%  Analysis Date = 05/17/13 
 Pct Recovery = 87%  Analysis Date = 05/17/13 
 Pct Recovery = 87%  Analysis Date = 05/14/13 
 Pct Recovery = 87%  Analysis Date = 05/14/13 
 Pct Recovery = 87%  Analysis Date = 05/12/13 
 Pct Recovery = 87%  Analysis Date = 05/12/13 
 Pct Recovery = 87%  Analysis Date = 05/10/13 
 Pct Recovery = 87%  Analysis Date = 05/10/13 
 Pct Recovery = 87%  Analysis Date = 05/07/13 
 Pct Recovery = 87%  Analysis Date = 05/07/13 
 Pct Recovery = 87%  Analysis Date = 05/05/13 
 Pct Recovery = 87%  Analysis Date = 05/05/13 
 Pct Recovery = 87%  Analysis Date = 05/02/13 
 Pct Recovery = 88%  Analysis Date = 05/02/13 
 Pct Recovery = 88%  Analysis Date = 04/30/13 
 Pct Recovery = 88%  Analysis Date = 04/30/13 
 Pct Recovery = 88%  Analysis Date = 04/27/13 
 Pct Recovery = 88%  Analysis Date = 04/27/13 
 Pct Recovery = 88%  Analysis Date = 04/25/13 
 Pct Recovery = 89%  Analysis Date = 04/25/13 
 Pct Recovery = 89%  Analysis Date = 04/23/13 
 Pct Recovery = 90%  Analysis Date = 04/23/13 
 Pct Recovery = 90%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/18/13 
 Pct Recovery = 91%  Analysis Date = 04/18/13 
 Pct Recovery = 91%  Analysis Date = 04/15/13 
 Pct Recovery = 92%  Analysis Date = 04/15/13 
 Pct Recovery = 92%  Analysis Date = 04/13/13 
 Pct Recovery = 92%  Analysis Date = 04/13/13 
 Pct Recovery = 92%  Analysis Date = 04/11/13 
 Pct Recovery = 93%  Analysis Date = 04/11/13 
 Pct Recovery = 93%  Analysis Date = 04/08/13 
 Pct Recovery = 94%  Analysis Date = 04/08/13 
 Pct Recovery = 94%  Analysis Date = 04/06/13 
 Pct Recovery = 94%  Analysis Date = 04/06/13 
 Pct Recovery = 94%  Analysis Date = 04/03/13 
 Pct Recovery = 95%  Analysis Date = 04/03/13 
 Pct Recovery = 95%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 04/01/13 
 Pct Recovery = 96%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/30/13 
 Pct Recovery = 97%  Analysis Date = 03/27/13 
 Pct Recovery = 97%  Analysis Date = 03/27/13 
 Pct Recovery = 97%  Analysis Date = 03/25/13 
 Pct Recovery = 98%  Analysis Date = 03/25/13 
 Pct Recovery = 98%  Analysis Date = 03/22/13 
 Pct Recovery = 98%  Analysis Date = 03/22/13 
 Pct Recovery = 98%  Analysis Date = 03/20/13 
 Pct Recovery = 98%  Analysis Date = 03/20/13 
 Pct Recovery = 98%  Analysis Date = 03/17/13 
 Pct Recovery = 99%  Analysis Date = 03/17/13 
 Pct Recovery = 99%  Analysis Date = 03/15/13 
 Pct Recovery = 99%  Analysis Date = 03/15/13 
 Pct Recovery = 99%  Analysis Date = 03/13/13 
 Pct Recovery = 99%  Analysis Date = 03/13/13 
 Pct Recovery = 99%  Analysis Date = 03/10/13 
 Pct Recovery = 100%  Analysis Date = 03/10/13 
 Pct Recovery = 100%  Analysis Date = 03/08/13 
 Pct Recovery = 100%  Analysis Date = 03/08/13 
 Pct Recovery = 100%  Analysis Date = 03/05/13 
 Pct Recovery = 100%  Analysis Date = 03/05/13 
 Pct Recovery = 100%  Analysis Date = 03/03/13 
 Pct Recovery = 101%  Analysis Date = 03/03/13 
 Pct Recovery = 101%  Analysis Date = 03/01/13 
 Pct Recovery = 101%  Analysis Date = 03/01/13 
 Pct Recovery = 101%  Analysis Date = 02/26/13 
 Pct Recovery = 101%  Analysis Date = 02/26/13 
 Pct Recovery = 101%  Analysis Date = 02/24/13 
 Pct Recovery = 101%  Analysis Date = 02/24/13 
 Pct Recovery = 101%  Analysis Date = 02/21/13 
 Pct Recovery = 102%  Analysis Date = 02/21/13 
 Pct Recovery = 102%  Analysis Date = 02/19/13 
 Pct Recovery = 102%  Analysis Date = 02/19/13 
 Pct Recovery = 102%  Analysis Date = 02/17/13 
 Pct Recovery = 102%  Analysis Date = 02/17/13 
 Pct Recovery = 102%  Analysis Date = 02/14/13 
 Pct Recovery = 103%  Analysis Date = 02/14/13 
 Pct Recovery = 103%  Analysis Date = 02/12/13 
 Pct Recovery = 103%  Analysis Date = 02/12/13 
 Pct Recovery = 103%  Analysis Date = 02/09/13 
 Pct Recovery = 103%  Analysis Date = 02/09/13 
 Pct Recovery = 103%  Analysis Date = 02/07/13 
 Pct Recovery = 104%  Analysis Date = 02/07/13 
 Pct Recovery = 104%  Analysis Date = 02/05/13 
 Pct Recovery = 104%  Analysis Date = 02/05/13 
 Pct Recovery = 104%  Analysis Date = 02/02/13 
 Pct Recovery = 104%  Analysis Date = 02/02/13 
 Pct Recovery = 104%  Analysis Date = 01/31/13 
 Pct Recovery = 105%  Analysis Date = 01/31/13 
 Pct Recovery = 105%  Analysis Date = 01/28/13 
 Pct Recovery = 105%  Analysis Date = 01/28/13 
 Pct Recovery = 105%  Analysis Date = 01/26/13 
 Pct Recovery = 105%  Analysis Date = 01/26/13 
 Pct Recovery = 105%  Analysis Date = 01/23/13 
 Pct Recovery = 106%  Analysis Date = 01/23/13 
 Pct Recovery = 106%  Analysis Date = 01/21/13 
 Pct Recovery = 105%  Analysis Date = 01/21/13 
 Pct Recovery = 105%  Analysis Date = 01/19/13 
 Pct Recovery = 105%  Analysis Date = 01/19/13 
 Pct Recovery = 105%  Analysis Date = 01/16/13 
 Pct Recovery = 105%  Analysis Date = 01/16/13 
 Pct Recovery = 105%  Analysis Date = 01/14/13 
 Pct Recovery = 104%  Analysis Date = 01/14/13 
 Pct Recovery = 104%  Analysis Date = 01/11/13 
 Pct Recovery = 104%  Analysis Date = 01/11/13 
 Pct Recovery = 104%  Analysis Date = 01/09/13 
 Pct Recovery = 104%  Analysis Date = 01/09/13 
 Pct Recovery = 104%  Analysis Date = 01/07/13 
 Pct Recovery = 103%  Analysis Date = 01/07/13 
 Pct Recovery = 103%  Analysis Date = 01/04/13 
 Pct Recovery = 103%  Analysis Date = 01/04/13 
 Pct Recovery = 103%  Analysis Date = 01/02/13 
 Pct Recovery = 103%  Analysis Date = 01/02/13 
 Pct Recovery = 103%  Analysis Date = 12/30/12 
 Pct Recovery = 102%  Analysis Date = 12/30/12 
 Pct Recovery = 102%  Analysis Date = 12/28/12 
 Pct Recovery = 102%  Analysis Date = 12/28/12 
 Pct Recovery = 102%  Analysis Date = 12/26/12 
 Pct Recovery = 102%  Analysis Date = 12/26/12 
 Pct Recovery = 102%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/23/12 
 Pct Recovery = 101%  Analysis Date = 12/21/12 
 Pct Recovery = 101%  Analysis Date = 12/21/12 
 Pct Recovery = 101%  Analysis Date = 12/18/12 
 Pct Recovery = 101%  Analysis Date = 12/18/12 
 Pct Recovery = 101%  Analysis Date = 12/16/12 
 Pct Recovery = 100%  Analysis Date = 12/16/12 
 Pct Recovery = 100%  Analysis Date = 12/14/12 
 Pct Recovery = 100%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORDIAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 87% 23% 84% 12%
Total 14 87% 23% 84% 12%

Sample Statistics
NORDIAZEPAM

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NORETHINDRONE
METHOD: LC9017 , TESTIDCODE: 67434LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 78%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 77%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 44%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 54%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 63%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 86%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 70%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 90%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 67%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 63%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 92%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 78%  Analysis Date = 04/09/14 
 Pct Recovery = 46%  Analysis Date = 04/07/14 
 Pct Recovery = 46%  Analysis Date = 04/07/14 
 Pct Recovery = 46%  Analysis Date = 04/05/14 
 Pct Recovery = 47%  Analysis Date = 04/05/14 
 Pct Recovery = 47%  Analysis Date = 04/02/14 
 Pct Recovery = 47%  Analysis Date = 04/02/14 
 Pct Recovery = 47%  Analysis Date = 03/31/14 
 Pct Recovery = 48%  Analysis Date = 03/31/14 
 Pct Recovery = 48%  Analysis Date = 03/28/14 
 Pct Recovery = 48%  Analysis Date = 03/28/14 
 Pct Recovery = 48%  Analysis Date = 03/26/14 
 Pct Recovery = 49%  Analysis Date = 03/26/14 
 Pct Recovery = 49%  Analysis Date = 03/24/14 
 Pct Recovery = 49%  Analysis Date = 03/24/14 
 Pct Recovery = 49%  Analysis Date = 03/21/14 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 Pct Recovery = 50%  Analysis Date = 03/19/14 
 Pct Recovery = 50%  Analysis Date = 03/19/14 
 Pct Recovery = 50%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/12/14 
 Pct Recovery = 52%  Analysis Date = 03/12/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/09/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 52%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/04/14 
 Pct Recovery = 53%  Analysis Date = 03/02/14 
 Pct Recovery = 53%  Analysis Date = 03/02/14 
 Pct Recovery = 53%  Analysis Date = 02/28/14 
 Pct Recovery = 54%  Analysis Date = 02/28/14 
 Pct Recovery = 54%  Analysis Date = 02/25/14 
 Pct Recovery = 54%  Analysis Date = 02/25/14 
 Pct Recovery = 54%  Analysis Date = 02/23/14 
 Pct Recovery = 55%  Analysis Date = 02/23/14 
 Pct Recovery = 55%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/20/14 
 Pct Recovery = 55%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/18/14 
 Pct Recovery = 56%  Analysis Date = 02/15/14 
 Pct Recovery = 56%  Analysis Date = 02/15/14 
 Pct Recovery = 56%  Analysis Date = 02/13/14 
 Pct Recovery = 57%  Analysis Date = 02/13/14 
 Pct Recovery = 57%  Analysis Date = 02/11/14 
 Pct Recovery = 57%  Analysis Date = 02/11/14 
 Pct Recovery = 57%  Analysis Date = 02/08/14 
 Pct Recovery = 58%  Analysis Date = 02/08/14 
 Pct Recovery = 58%  Analysis Date = 02/06/14 
 Pct Recovery = 58%  Analysis Date = 02/06/14 
 Pct Recovery = 58%  Analysis Date = 02/03/14 
 Pct Recovery = 59%  Analysis Date = 02/03/14 
 Pct Recovery = 59%  Analysis Date = 02/01/14 
 Pct Recovery = 59%  Analysis Date = 02/01/14 
 Pct Recovery = 59%  Analysis Date = 01/30/14 
 Pct Recovery = 60%  Analysis Date = 01/30/14 
 Pct Recovery = 60%  Analysis Date = 01/27/14 
 Pct Recovery = 60%  Analysis Date = 01/27/14 
 Pct Recovery = 60%  Analysis Date = 01/25/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/06/14 
 Pct Recovery = 64%  Analysis Date = 01/06/14 
 Pct Recovery = 64%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/01/14 
 Pct Recovery = 65%  Analysis Date = 01/01/14 
 Pct Recovery = 65%  Analysis Date = 12/29/13 
 Pct Recovery = 66%  Analysis Date = 12/29/13 
 Pct Recovery = 66%  Analysis Date = 12/27/13 
 Pct Recovery = 66%  Analysis Date = 12/27/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 67%  Analysis Date = 12/24/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/17/13 
 Pct Recovery = 68%  Analysis Date = 12/17/13 
 Pct Recovery = 68%  Analysis Date = 12/15/13 
 Pct Recovery = 69%  Analysis Date = 12/15/13 
 Pct Recovery = 69%  Analysis Date = 12/12/13 
 Pct Recovery = 69%  Analysis Date = 12/12/13 
 Pct Recovery = 69%  Analysis Date = 12/10/13 
 Pct Recovery = 70%  Analysis Date = 12/10/13 
 Pct Recovery = 70%  Analysis Date = 12/08/13 
 Pct Recovery = 70%  Analysis Date = 12/08/13 
 Pct Recovery = 70%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 72%  Analysis Date = 11/21/13 
 Pct Recovery = 72%  Analysis Date = 11/21/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/13/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/06/13 
 Pct Recovery = 72%  Analysis Date = 11/06/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 72%  Analysis Date = 11/01/13 
 Pct Recovery = 72%  Analysis Date = 11/01/13 
 Pct Recovery = 72%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/20/13 
 Pct Recovery = 72%  Analysis Date = 10/20/13 
 Pct Recovery = 72%  Analysis Date = 10/18/13 
 Pct Recovery = 72%  Analysis Date = 10/18/13 
 Pct Recovery = 72%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 09/29/13 
 Pct Recovery = 72%  Analysis Date = 09/29/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/26/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/24/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 73%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/09/13 
 Pct Recovery = 73%  Analysis Date = 09/09/13 
 Pct Recovery = 73%  Analysis Date = 09/07/13 
 Pct Recovery = 73%  Analysis Date = 09/07/13 
 Pct Recovery = 73%  Analysis Date = 09/05/13 
 Pct Recovery = 73%  Analysis Date = 09/05/13 
 Pct Recovery = 73%  Analysis Date = 09/02/13 
 Pct Recovery = 73%  Analysis Date = 09/02/13 
 Pct Recovery = 73%  Analysis Date = 08/31/13 
 Pct Recovery = 73%  Analysis Date = 08/31/13 
 Pct Recovery = 73%  Analysis Date = 08/28/13 
 Pct Recovery = 73%  Analysis Date = 08/28/13 
 Pct Recovery = 73%  Analysis Date = 08/26/13 
 Pct Recovery = 73%  Analysis Date = 08/26/13 
 Pct Recovery = 73%  Analysis Date = 08/24/13 
 Pct Recovery = 73%  Analysis Date = 08/24/13 
 Pct Recovery = 73%  Analysis Date = 08/21/13 
 Pct Recovery = 74%  Analysis Date = 08/21/13 
 Pct Recovery = 74%  Analysis Date = 08/19/13 
 Pct Recovery = 74%  Analysis Date = 08/19/13 
 Pct Recovery = 74%  Analysis Date = 08/16/13 
 Pct Recovery = 74%  Analysis Date = 08/16/13 
 Pct Recovery = 74%  Analysis Date = 08/14/13 
 Pct Recovery = 74%  Analysis Date = 08/14/13 
 Pct Recovery = 74%  Analysis Date = 08/11/13 
 Pct Recovery = 74%  Analysis Date = 08/11/13 
 Pct Recovery = 74%  Analysis Date = 08/09/13 
 Pct Recovery = 74%  Analysis Date = 08/09/13 
 Pct Recovery = 74%  Analysis Date = 08/07/13 
 Pct Recovery = 74%  Analysis Date = 08/07/13 
 Pct Recovery = 74%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/04/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/30/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/28/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 75%  Analysis Date = 07/23/13 
 Pct Recovery = 75%  Analysis Date = 07/21/13 
 Pct Recovery = 75%  Analysis Date = 07/21/13 
 Pct Recovery = 75%  Analysis Date = 07/18/13 
 Pct Recovery = 75%  Analysis Date = 07/18/13 
 Pct Recovery = 75%  Analysis Date = 07/16/13 
 Pct Recovery = 75%  Analysis Date = 07/16/13 
 Pct Recovery = 75%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/14/13 
 Pct Recovery = 75%  Analysis Date = 07/11/13 
 Pct Recovery = 75%  Analysis Date = 07/11/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/04/13 
 Pct Recovery = 76%  Analysis Date = 07/04/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/24/13 
 Pct Recovery = 76%  Analysis Date = 06/24/13 
 Pct Recovery = 76%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/15/13 
 Pct Recovery = 76%  Analysis Date = 06/15/13 
 Pct Recovery = 76%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/10/13 
 Pct Recovery = 77%  Analysis Date = 06/10/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 78%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/14/13 
 Pct Recovery = 78%  Analysis Date = 05/14/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/07/13 
 Pct Recovery = 78%  Analysis Date = 05/07/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 79%  Analysis Date = 04/27/13 
 Pct Recovery = 79%  Analysis Date = 04/27/13 
 Pct Recovery = 79%  Analysis Date = 04/25/13 
 Pct Recovery = 79%  Analysis Date = 04/25/13 
 Pct Recovery = 79%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/20/13 
 Pct Recovery = 79%  Analysis Date = 04/20/13 
 Pct Recovery = 79%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 80%  Analysis Date = 04/11/13 
 Pct Recovery = 80%  Analysis Date = 04/11/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/06/13 
 Pct Recovery = 80%  Analysis Date = 04/06/13 
 Pct Recovery = 80%  Analysis Date = 04/03/13 
 Pct Recovery = 80%  Analysis Date = 04/03/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 04/01/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/30/13 
 Pct Recovery = 80%  Analysis Date = 03/27/13 
 Pct Recovery = 80%  Analysis Date = 03/27/13 
 Pct Recovery = 80%  Analysis Date = 03/25/13 
 Pct Recovery = 80%  Analysis Date = 03/25/13 
 Pct Recovery = 80%  Analysis Date = 03/22/13 
 Pct Recovery = 80%  Analysis Date = 03/22/13 
 Pct Recovery = 80%  Analysis Date = 03/20/13 
 Pct Recovery = 80%  Analysis Date = 03/20/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 03/15/13 
 Pct Recovery = 80%  Analysis Date = 03/15/13 
 Pct Recovery = 80%  Analysis Date = 03/13/13 
 Pct Recovery = 80%  Analysis Date = 03/13/13 
 Pct Recovery = 80%  Analysis Date = 03/10/13 
 Pct Recovery = 80%  Analysis Date = 03/10/13 
 Pct Recovery = 80%  Analysis Date = 03/08/13 
 Pct Recovery = 80%  Analysis Date = 03/08/13 
 Pct Recovery = 80%  Analysis Date = 03/05/13 
 Pct Recovery = 80%  Analysis Date = 03/05/13 
 Pct Recovery = 80%  Analysis Date = 03/03/13 
 Pct Recovery = 80%  Analysis Date = 03/03/13 
 Pct Recovery = 80%  Analysis Date = 03/01/13 
 Pct Recovery = 80%  Analysis Date = 03/01/13 
 Pct Recovery = 80%  Analysis Date = 02/26/13 
 Pct Recovery = 80%  Analysis Date = 02/26/13 
 Pct Recovery = 80%  Analysis Date = 02/24/13 
 Pct Recovery = 80%  Analysis Date = 02/24/13 
 Pct Recovery = 80%  Analysis Date = 02/21/13 
 Pct Recovery = 80%  Analysis Date = 02/21/13 
 Pct Recovery = 80%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/19/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/14/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 80%  Analysis Date = 02/09/13 
 Pct Recovery = 80%  Analysis Date = 02/09/13 
 Pct Recovery = 80%  Analysis Date = 02/07/13 
 Pct Recovery = 80%  Analysis Date = 02/07/13 
 Pct Recovery = 80%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/05/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 02/02/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/31/13 
 Pct Recovery = 80%  Analysis Date = 01/28/13 
 Pct Recovery = 80%  Analysis Date = 01/28/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 80%  Analysis Date = 01/26/13 
 Pct Recovery = 80%  Analysis Date = 01/23/13 
 Pct Recovery = 80%  Analysis Date = 01/23/13 
 Pct Recovery = 80%  Analysis Date = 01/21/13 
 Pct Recovery = 80%  Analysis Date = 01/21/13 
 Pct Recovery = 80%  Analysis Date = 01/19/13 
 Pct Recovery = 80%  Analysis Date = 01/19/13 
 Pct Recovery = 80%  Analysis Date = 01/16/13 
 Pct Recovery = 80%  Analysis Date = 01/16/13 
 Pct Recovery = 80%  Analysis Date = 01/14/13 
 Pct Recovery = 80%  Analysis Date = 01/14/13 
 Pct Recovery = 80%  Analysis Date = 01/11/13 
 Pct Recovery = 80%  Analysis Date = 01/11/13 
 Pct Recovery = 80%  Analysis Date = 01/09/13 
 Pct Recovery = 80%  Analysis Date = 01/09/13 
 Pct Recovery = 80%  Analysis Date = 01/07/13 
 Pct Recovery = 80%  Analysis Date = 01/07/13 
 Pct Recovery = 80%  Analysis Date = 01/04/13 
 Pct Recovery = 79%  Analysis Date = 01/04/13 
 Pct Recovery = 79%  Analysis Date = 01/02/13 
 Pct Recovery = 79%  Analysis Date = 01/02/13 
 Pct Recovery = 79%  Analysis Date = 12/30/12 
 Pct Recovery = 79%  Analysis Date = 12/30/12 
 Pct Recovery = 79%  Analysis Date = 12/28/12 
 Pct Recovery = 79%  Analysis Date = 12/28/12 
 Pct Recovery = 79%  Analysis Date = 12/26/12 
 Pct Recovery = 79%  Analysis Date = 12/26/12 
 Pct Recovery = 79%  Analysis Date = 12/23/12 
 Pct Recovery = 79%  Analysis Date = 12/23/12 
 Pct Recovery = 79%  Analysis Date = 12/21/12 
 Pct Recovery = 79%  Analysis Date = 12/21/12 
 Pct Recovery = 79%  Analysis Date = 12/18/12 
 Pct Recovery = 79%  Analysis Date = 12/18/12 
 Pct Recovery = 79%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/16/12 
 Pct Recovery = 79%  Analysis Date = 12/14/12 
 Pct Recovery = 79%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 72% 14% 73% 11%
Total 13 72% 14% 73% 11%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NORFLUOXETINE
METHOD: LC9017 , TESTIDCODE: 67451LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 90%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 106%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 169%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 100%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 43%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 80%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 52%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 110%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 53%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 77%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 73%  Analysis Date = 04/09/14 
 Pct Recovery = 54%  Analysis Date = 04/07/14 
 Pct Recovery = 54%  Analysis Date = 04/07/14 
 Pct Recovery = 54%  Analysis Date = 04/05/14 
 Pct Recovery = 55%  Analysis Date = 04/05/14 
 Pct Recovery = 55%  Analysis Date = 04/02/14 
 Pct Recovery = 55%  Analysis Date = 04/02/14 
 Pct Recovery = 55%  Analysis Date = 03/31/14 
 Pct Recovery = 55%  Analysis Date = 03/31/14 
 Pct Recovery = 55%  Analysis Date = 03/28/14 
 Pct Recovery = 55%  Analysis Date = 03/28/14 
 Pct Recovery = 55%  Analysis Date = 03/26/14 
 Pct Recovery = 56%  Analysis Date = 03/26/14 
 Pct Recovery = 56%  Analysis Date = 03/24/14 
 Pct Recovery = 56%  Analysis Date = 03/24/14 
 Pct Recovery = 56%  Analysis Date = 03/21/14 
 Pct Recovery = 56%  Analysis Date = 03/21/14 
 Pct Recovery = 56%  Analysis Date = 03/19/14 
 Pct Recovery = 56%  Analysis Date = 03/19/14 
 Pct Recovery = 56%  Analysis Date = 03/16/14 
 Pct Recovery = 57%  Analysis Date = 03/16/14 
 Pct Recovery = 57%  Analysis Date = 03/14/14 
 Pct Recovery = 57%  Analysis Date = 03/14/14 
 Pct Recovery = 57%  Analysis Date = 03/12/14 
 Pct Recovery = 57%  Analysis Date = 03/12/14 
 Pct Recovery = 57%  Analysis Date = 03/09/14 
 Pct Recovery = 57%  Analysis Date = 03/09/14 
 Pct Recovery = 57%  Analysis Date = 03/07/14 
 Pct Recovery = 58%  Analysis Date = 03/07/14 
 Pct Recovery = 58%  Analysis Date = 03/04/14 
 Pct Recovery = 58%  Analysis Date = 03/04/14 
 Pct Recovery = 58%  Analysis Date = 03/02/14 
 Pct Recovery = 58%  Analysis Date = 03/02/14 
 Pct Recovery = 58%  Analysis Date = 02/28/14 
 Pct Recovery = 58%  Analysis Date = 02/28/14 
 Pct Recovery = 58%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 59%  Analysis Date = 02/20/14 
 Pct Recovery = 59%  Analysis Date = 02/20/14 
 Pct Recovery = 59%  Analysis Date = 02/18/14 
 Pct Recovery = 59%  Analysis Date = 02/18/14 
 Pct Recovery = 59%  Analysis Date = 02/15/14 
 Pct Recovery = 60%  Analysis Date = 02/15/14 
 Pct Recovery = 60%  Analysis Date = 02/13/14 
 Pct Recovery = 60%  Analysis Date = 02/13/14 
 Pct Recovery = 60%  Analysis Date = 02/11/14 
 Pct Recovery = 60%  Analysis Date = 02/11/14 
 Pct Recovery = 60%  Analysis Date = 02/08/14 
 Pct Recovery = 60%  Analysis Date = 02/08/14 
 Pct Recovery = 60%  Analysis Date = 02/06/14 
 Pct Recovery = 61%  Analysis Date = 02/06/14 
 Pct Recovery = 61%  Analysis Date = 02/03/14 
 Pct Recovery = 61%  Analysis Date = 02/03/14 
 Pct Recovery = 61%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 62%  Analysis Date = 01/27/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/10/14 
 Pct Recovery = 63%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/06/14 
 Pct Recovery = 64%  Analysis Date = 01/06/14 
 Pct Recovery = 64%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/03/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 01/01/14 
 Pct Recovery = 64%  Analysis Date = 12/29/13 
 Pct Recovery = 65%  Analysis Date = 12/29/13 
 Pct Recovery = 65%  Analysis Date = 12/27/13 
 Pct Recovery = 65%  Analysis Date = 12/27/13 
 Pct Recovery = 65%  Analysis Date = 12/24/13 
 Pct Recovery = 65%  Analysis Date = 12/24/13 
 Pct Recovery = 65%  Analysis Date = 12/22/13 
 Pct Recovery = 65%  Analysis Date = 12/22/13 
 Pct Recovery = 65%  Analysis Date = 12/20/13 
 Pct Recovery = 66%  Analysis Date = 12/20/13 
 Pct Recovery = 66%  Analysis Date = 12/17/13 
 Pct Recovery = 66%  Analysis Date = 12/17/13 
 Pct Recovery = 66%  Analysis Date = 12/15/13 
 Pct Recovery = 66%  Analysis Date = 12/15/13 
 Pct Recovery = 66%  Analysis Date = 12/12/13 
 Pct Recovery = 66%  Analysis Date = 12/12/13 
 Pct Recovery = 66%  Analysis Date = 12/10/13 
 Pct Recovery = 67%  Analysis Date = 12/10/13 
 Pct Recovery = 67%  Analysis Date = 12/08/13 
 Pct Recovery = 67%  Analysis Date = 12/08/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/03/13 
 Pct Recovery = 67%  Analysis Date = 12/03/13 
 Pct Recovery = 67%  Analysis Date = 11/30/13 
 Pct Recovery = 68%  Analysis Date = 11/30/13 
 Pct Recovery = 68%  Analysis Date = 11/28/13 
 Pct Recovery = 68%  Analysis Date = 11/28/13 
 Pct Recovery = 68%  Analysis Date = 11/26/13 
 Pct Recovery = 68%  Analysis Date = 11/26/13 
 Pct Recovery = 68%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/23/13 
 Pct Recovery = 68%  Analysis Date = 11/21/13 
 Pct Recovery = 69%  Analysis Date = 11/21/13 
 Pct Recovery = 69%  Analysis Date = 11/18/13 
 Pct Recovery = 69%  Analysis Date = 11/18/13 
 Pct Recovery = 69%  Analysis Date = 11/16/13 
 Pct Recovery = 69%  Analysis Date = 11/16/13 
 Pct Recovery = 69%  Analysis Date = 11/13/13 
 Pct Recovery = 69%  Analysis Date = 11/13/13 
 Pct Recovery = 69%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/06/13 
 Pct Recovery = 70%  Analysis Date = 11/06/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 70%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/18/13 
 Pct Recovery = 73%  Analysis Date = 10/18/13 
 Pct Recovery = 73%  Analysis Date = 10/16/13 
 Pct Recovery = 73%  Analysis Date = 10/16/13 
 Pct Recovery = 73%  Analysis Date = 10/13/13 
 Pct Recovery = 74%  Analysis Date = 10/13/13 
 Pct Recovery = 74%  Analysis Date = 10/11/13 
 Pct Recovery = 74%  Analysis Date = 10/11/13 
 Pct Recovery = 74%  Analysis Date = 10/08/13 
 Pct Recovery = 75%  Analysis Date = 10/08/13 
 Pct Recovery = 75%  Analysis Date = 10/06/13 
 Pct Recovery = 75%  Analysis Date = 10/06/13 
 Pct Recovery = 75%  Analysis Date = 10/04/13 
 Pct Recovery = 76%  Analysis Date = 10/04/13 
 Pct Recovery = 76%  Analysis Date = 10/01/13 
 Pct Recovery = 76%  Analysis Date = 10/01/13 
 Pct Recovery = 76%  Analysis Date = 09/29/13 
 Pct Recovery = 77%  Analysis Date = 09/29/13 
 Pct Recovery = 77%  Analysis Date = 09/26/13 
 Pct Recovery = 77%  Analysis Date = 09/26/13 
 Pct Recovery = 77%  Analysis Date = 09/24/13 
 Pct Recovery = 77%  Analysis Date = 09/24/13 
 Pct Recovery = 77%  Analysis Date = 09/21/13 
 Pct Recovery = 78%  Analysis Date = 09/21/13 
 Pct Recovery = 78%  Analysis Date = 09/19/13 
 Pct Recovery = 78%  Analysis Date = 09/19/13 
 Pct Recovery = 78%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 82%  Analysis Date = 08/31/13 
 Pct Recovery = 82%  Analysis Date = 08/28/13 
 Pct Recovery = 82%  Analysis Date = 08/28/13 
 Pct Recovery = 82%  Analysis Date = 08/26/13 
 Pct Recovery = 83%  Analysis Date = 08/26/13 
 Pct Recovery = 83%  Analysis Date = 08/24/13 
 Pct Recovery = 83%  Analysis Date = 08/24/13 
 Pct Recovery = 83%  Analysis Date = 08/21/13 
 Pct Recovery = 83%  Analysis Date = 08/21/13 
 Pct Recovery = 83%  Analysis Date = 08/19/13 
 Pct Recovery = 84%  Analysis Date = 08/19/13 
 Pct Recovery = 84%  Analysis Date = 08/16/13 
 Pct Recovery = 84%  Analysis Date = 08/16/13 
 Pct Recovery = 84%  Analysis Date = 08/14/13 
 Pct Recovery = 85%  Analysis Date = 08/14/13 
 Pct Recovery = 85%  Analysis Date = 08/11/13 
 Pct Recovery = 85%  Analysis Date = 08/11/13 
 Pct Recovery = 85%  Analysis Date = 08/09/13 
 Pct Recovery = 85%  Analysis Date = 08/09/13 
 Pct Recovery = 85%  Analysis Date = 08/07/13 
 Pct Recovery = 86%  Analysis Date = 08/07/13 
 Pct Recovery = 86%  Analysis Date = 08/04/13 
 Pct Recovery = 86%  Analysis Date = 08/04/13 
 Pct Recovery = 86%  Analysis Date = 08/02/13 
 Pct Recovery = 87%  Analysis Date = 08/02/13 
 Pct Recovery = 87%  Analysis Date = 07/30/13 
 Pct Recovery = 87%  Analysis Date = 07/30/13 
 Pct Recovery = 87%  Analysis Date = 07/28/13 
 Pct Recovery = 87%  Analysis Date = 07/28/13 
 Pct Recovery = 87%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/23/13 
 Pct Recovery = 88%  Analysis Date = 07/23/13 
 Pct Recovery = 88%  Analysis Date = 07/21/13 
 Pct Recovery = 88%  Analysis Date = 07/21/13 
 Pct Recovery = 88%  Analysis Date = 07/18/13 
 Pct Recovery = 89%  Analysis Date = 07/18/13 
 Pct Recovery = 89%  Analysis Date = 07/16/13 
 Pct Recovery = 89%  Analysis Date = 07/16/13 
 Pct Recovery = 89%  Analysis Date = 07/14/13 
 Pct Recovery = 89%  Analysis Date = 07/14/13 
 Pct Recovery = 89%  Analysis Date = 07/11/13 
 Pct Recovery = 90%  Analysis Date = 07/11/13 
 Pct Recovery = 90%  Analysis Date = 07/09/13 
 Pct Recovery = 90%  Analysis Date = 07/09/13 
 Pct Recovery = 90%  Analysis Date = 07/06/13 
 Pct Recovery = 91%  Analysis Date = 07/06/13 
 Pct Recovery = 91%  Analysis Date = 07/04/13 
 Pct Recovery = 91%  Analysis Date = 07/04/13 
 Pct Recovery = 91%  Analysis Date = 07/02/13 
 Pct Recovery = 91%  Analysis Date = 07/02/13 
 Pct Recovery = 91%  Analysis Date = 06/29/13 
 Pct Recovery = 92%  Analysis Date = 06/29/13 
 Pct Recovery = 92%  Analysis Date = 06/27/13 
 Pct Recovery = 92%  Analysis Date = 06/27/13 
 Pct Recovery = 92%  Analysis Date = 06/24/13 
 Pct Recovery = 92%  Analysis Date = 06/24/13 
 Pct Recovery = 92%  Analysis Date = 06/22/13 
 Pct Recovery = 93%  Analysis Date = 06/22/13 
 Pct Recovery = 93%  Analysis Date = 06/19/13 
 Pct Recovery = 93%  Analysis Date = 06/19/13 
 Pct Recovery = 93%  Analysis Date = 06/17/13 
 Pct Recovery = 94%  Analysis Date = 06/17/13 
 Pct Recovery = 94%  Analysis Date = 06/15/13 
 Pct Recovery = 94%  Analysis Date = 06/15/13 
 Pct Recovery = 94%  Analysis Date = 06/12/13 
 Pct Recovery = 94%  Analysis Date = 06/12/13 
 Pct Recovery = 94%  Analysis Date = 06/10/13 
 Pct Recovery = 95%  Analysis Date = 06/10/13 
 Pct Recovery = 95%  Analysis Date = 06/07/13 
 Pct Recovery = 95%  Analysis Date = 06/07/13 
 Pct Recovery = 95%  Analysis Date = 06/05/13 
 Pct Recovery = 95%  Analysis Date = 06/05/13 
 Pct Recovery = 95%  Analysis Date = 06/03/13 
 Pct Recovery = 96%  Analysis Date = 06/03/13 
 Pct Recovery = 96%  Analysis Date = 05/31/13 
 Pct Recovery = 96%  Analysis Date = 05/31/13 
 Pct Recovery = 96%  Analysis Date = 05/29/13 
 Pct Recovery = 96%  Analysis Date = 05/29/13 
 Pct Recovery = 96%  Analysis Date = 05/26/13 
 Pct Recovery = 97%  Analysis Date = 05/26/13 
 Pct Recovery = 97%  Analysis Date = 05/24/13 
 Pct Recovery = 97%  Analysis Date = 05/24/13 
 Pct Recovery = 97%  Analysis Date = 05/22/13 
 Pct Recovery = 98%  Analysis Date = 05/22/13 
 Pct Recovery = 98%  Analysis Date = 05/19/13 
 Pct Recovery = 98%  Analysis Date = 05/19/13 
 Pct Recovery = 98%  Analysis Date = 05/17/13 
 Pct Recovery = 98%  Analysis Date = 05/17/13 
 Pct Recovery = 98%  Analysis Date = 05/14/13 
 Pct Recovery = 99%  Analysis Date = 05/14/13 
 Pct Recovery = 99%  Analysis Date = 05/12/13 
 Pct Recovery = 99%  Analysis Date = 05/12/13 
 Pct Recovery = 99%  Analysis Date = 05/10/13 
 Pct Recovery = 99%  Analysis Date = 05/10/13 
 Pct Recovery = 99%  Analysis Date = 05/07/13 
 Pct Recovery = 100%  Analysis Date = 05/07/13 
 Pct Recovery = 100%  Analysis Date = 05/05/13 
 Pct Recovery = 100%  Analysis Date = 05/05/13 
 Pct Recovery = 100%  Analysis Date = 05/02/13 
 Pct Recovery = 101%  Analysis Date = 05/02/13 
 Pct Recovery = 101%  Analysis Date = 04/30/13 
 Pct Recovery = 99%  Analysis Date = 04/30/13 
 Pct Recovery = 99%  Analysis Date = 04/27/13 
 Pct Recovery = 97%  Analysis Date = 04/27/13 
 Pct Recovery = 97%  Analysis Date = 04/25/13 
 Pct Recovery = 95%  Analysis Date = 04/25/13 
 Pct Recovery = 95%  Analysis Date = 04/23/13 
 Pct Recovery = 95%  Analysis Date = 04/23/13 
 Pct Recovery = 95%  Analysis Date = 04/20/13 
 Pct Recovery = 96%  Analysis Date = 04/20/13 
 Pct Recovery = 96%  Analysis Date = 04/18/13 
 Pct Recovery = 96%  Analysis Date = 04/18/13 
 Pct Recovery = 96%  Analysis Date = 04/15/13 
 Pct Recovery = 96%  Analysis Date = 04/15/13 
 Pct Recovery = 96%  Analysis Date = 04/13/13 
 Pct Recovery = 97%  Analysis Date = 04/13/13 
 Pct Recovery = 97%  Analysis Date = 04/11/13 
 Pct Recovery = 97%  Analysis Date = 04/11/13 
 Pct Recovery = 97%  Analysis Date = 04/08/13 
 Pct Recovery = 98%  Analysis Date = 04/08/13 
 Pct Recovery = 98%  Analysis Date = 04/06/13 
 Pct Recovery = 98%  Analysis Date = 04/06/13 
 Pct Recovery = 98%  Analysis Date = 04/03/13 
 Pct Recovery = 98%  Analysis Date = 04/03/13 
 Pct Recovery = 98%  Analysis Date = 04/01/13 
 Pct Recovery = 99%  Analysis Date = 04/01/13 
 Pct Recovery = 99%  Analysis Date = 03/30/13 
 Pct Recovery = 99%  Analysis Date = 03/30/13 
 Pct Recovery = 99%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/25/13 
 Pct Recovery = 100%  Analysis Date = 03/25/13 
 Pct Recovery = 100%  Analysis Date = 03/22/13 
 Pct Recovery = 100%  Analysis Date = 03/22/13 
 Pct Recovery = 100%  Analysis Date = 03/20/13 
 Pct Recovery = 100%  Analysis Date = 03/20/13 
 Pct Recovery = 100%  Analysis Date = 03/17/13 
 Pct Recovery = 101%  Analysis Date = 03/17/13 
 Pct Recovery = 101%  Analysis Date = 03/15/13 
 Pct Recovery = 101%  Analysis Date = 03/15/13 
 Pct Recovery = 101%  Analysis Date = 03/13/13 
 Pct Recovery = 101%  Analysis Date = 03/13/13 
 Pct Recovery = 101%  Analysis Date = 03/10/13 
 Pct Recovery = 102%  Analysis Date = 03/10/13 
 Pct Recovery = 102%  Analysis Date = 03/08/13 
 Pct Recovery = 102%  Analysis Date = 03/08/13 
 Pct Recovery = 102%  Analysis Date = 03/05/13 
 Pct Recovery = 102%  Analysis Date = 03/05/13 
 Pct Recovery = 102%  Analysis Date = 03/03/13 
 Pct Recovery = 103%  Analysis Date = 03/03/13 
 Pct Recovery = 103%  Analysis Date = 03/01/13 
 Pct Recovery = 103%  Analysis Date = 03/01/13 
 Pct Recovery = 103%  Analysis Date = 02/26/13 
 Pct Recovery = 103%  Analysis Date = 02/26/13 
 Pct Recovery = 103%  Analysis Date = 02/24/13 
 Pct Recovery = 104%  Analysis Date = 02/24/13 
 Pct Recovery = 104%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/19/13 
 Pct Recovery = 104%  Analysis Date = 02/19/13 
 Pct Recovery = 104%  Analysis Date = 02/17/13 
 Pct Recovery = 105%  Analysis Date = 02/17/13 
 Pct Recovery = 105%  Analysis Date = 02/14/13 
 Pct Recovery = 105%  Analysis Date = 02/14/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 106%  Analysis Date = 02/09/13 
 Pct Recovery = 106%  Analysis Date = 02/07/13 
 Pct Recovery = 106%  Analysis Date = 02/07/13 
 Pct Recovery = 106%  Analysis Date = 02/05/13 
 Pct Recovery = 106%  Analysis Date = 02/05/13 
 Pct Recovery = 106%  Analysis Date = 02/02/13 
 Pct Recovery = 107%  Analysis Date = 02/02/13 
 Pct Recovery = 107%  Analysis Date = 01/31/13 
 Pct Recovery = 107%  Analysis Date = 01/31/13 
 Pct Recovery = 107%  Analysis Date = 01/28/13 
 Pct Recovery = 107%  Analysis Date = 01/28/13 
 Pct Recovery = 107%  Analysis Date = 01/26/13 
 Pct Recovery = 108%  Analysis Date = 01/26/13 
 Pct Recovery = 108%  Analysis Date = 01/23/13 
 Pct Recovery = 108%  Analysis Date = 01/23/13 
 Pct Recovery = 108%  Analysis Date = 01/21/13 
 Pct Recovery = 107%  Analysis Date = 01/21/13 
 Pct Recovery = 107%  Analysis Date = 01/19/13 
 Pct Recovery = 107%  Analysis Date = 01/19/13 
 Pct Recovery = 107%  Analysis Date = 01/16/13 
 Pct Recovery = 107%  Analysis Date = 01/16/13 
 Pct Recovery = 107%  Analysis Date = 01/14/13 
 Pct Recovery = 106%  Analysis Date = 01/14/13 
 Pct Recovery = 106%  Analysis Date = 01/11/13 
 Pct Recovery = 106%  Analysis Date = 01/11/13 
 Pct Recovery = 106%  Analysis Date = 01/09/13 
 Pct Recovery = 105%  Analysis Date = 01/09/13 
 Pct Recovery = 105%  Analysis Date = 01/07/13 
 Pct Recovery = 105%  Analysis Date = 01/07/13 
 Pct Recovery = 105%  Analysis Date = 01/04/13 
 Pct Recovery = 105%  Analysis Date = 01/04/13 
 Pct Recovery = 105%  Analysis Date = 01/02/13 
 Pct Recovery = 104%  Analysis Date = 01/02/13 
 Pct Recovery = 104%  Analysis Date = 12/30/12 
 Pct Recovery = 104%  Analysis Date = 12/30/12 
 Pct Recovery = 104%  Analysis Date = 12/28/12 
 Pct Recovery = 103%  Analysis Date = 12/28/12 
 Pct Recovery = 103%  Analysis Date = 12/26/12 
 Pct Recovery = 103%  Analysis Date = 12/26/12 
 Pct Recovery = 103%  Analysis Date = 12/23/12 
 Pct Recovery = 103%  Analysis Date = 12/23/12 
 Pct Recovery = 103%  Analysis Date = 12/21/12 
 Pct Recovery = 102%  Analysis Date = 12/21/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/18/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 101%  Analysis Date = 12/16/12 
 Pct Recovery = 101%  Analysis Date = 12/14/12 
 Pct Recovery = 101%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORFLUOXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 73% . 73% 0%
>= Reporting Level 13 85% 32% 80% 19%
Total 14 85% 31% 79% 20%

Sample Statistics
NORFLUOXETINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 14 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
NORSERTRALINE
METHOD: LC9017 , TESTIDCODE: 67532LCM56

The SGPlot Procedure

Sample Statistics
NORSERTRALINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 1 3% 1 out of 31

OBSP Determination:
NORVERAPAMIL
METHOD: LC9017 , TESTIDCODE: 68007LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 52%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 47%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 51%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 45%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 20%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 10%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 14%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 22%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 13%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 6%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 48%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 25%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 26%  Analysis Date = 04/09/14 
 Pct Recovery = 15%  Analysis Date = 04/07/14 
 Pct Recovery = 15%  Analysis Date = 04/07/14 
 Pct Recovery = 15%  Analysis Date = 04/05/14 
 Pct Recovery = 15%  Analysis Date = 04/05/14 
 Pct Recovery = 15%  Analysis Date = 04/02/14 
 Pct Recovery = 15%  Analysis Date = 04/02/14 
 Pct Recovery = 15%  Analysis Date = 03/31/14 
 Pct Recovery = 15%  Analysis Date = 03/31/14 
 Pct Recovery = 15%  Analysis Date = 03/28/14 
 Pct Recovery = 15%  Analysis Date = 03/28/14 
 Pct Recovery = 15%  Analysis Date = 03/26/14 
 Pct Recovery = 16%  Analysis Date = 03/26/14 
 Pct Recovery = 16%  Analysis Date = 03/24/14 
 Pct Recovery = 16%  Analysis Date = 03/24/14 
 Pct Recovery = 16%  Analysis Date = 03/21/14 
 Pct Recovery = 16%  Analysis Date = 03/21/14 
 Pct Recovery = 16%  Analysis Date = 03/19/14 
 Pct Recovery = 16%  Analysis Date = 03/19/14 
 Pct Recovery = 16%  Analysis Date = 03/16/14 
 Pct Recovery = 16%  Analysis Date = 03/16/14 
 Pct Recovery = 16%  Analysis Date = 03/14/14 
 Pct Recovery = 17%  Analysis Date = 03/14/14 
 Pct Recovery = 17%  Analysis Date = 03/12/14 
 Pct Recovery = 17%  Analysis Date = 03/12/14 
 Pct Recovery = 17%  Analysis Date = 03/09/14 
 Pct Recovery = 17%  Analysis Date = 03/09/14 
 Pct Recovery = 17%  Analysis Date = 03/07/14 
 Pct Recovery = 17%  Analysis Date = 03/07/14 
 Pct Recovery = 17%  Analysis Date = 03/04/14 
 Pct Recovery = 17%  Analysis Date = 03/04/14 
 Pct Recovery = 17%  Analysis Date = 03/02/14 
 Pct Recovery = 18%  Analysis Date = 03/02/14 
 Pct Recovery = 18%  Analysis Date = 02/28/14 
 Pct Recovery = 18%  Analysis Date = 02/28/14 
 Pct Recovery = 18%  Analysis Date = 02/25/14 
 Pct Recovery = 18%  Analysis Date = 02/25/14 
 Pct Recovery = 18%  Analysis Date = 02/23/14 
 Pct Recovery = 18%  Analysis Date = 02/23/14 
 Pct Recovery = 18%  Analysis Date = 02/20/14 
 Pct Recovery = 18%  Analysis Date = 02/20/14 
 Pct Recovery = 18%  Analysis Date = 02/18/14 
 Pct Recovery = 18%  Analysis Date = 02/18/14 
 Pct Recovery = 18%  Analysis Date = 02/15/14 
 Pct Recovery = 19%  Analysis Date = 02/15/14 
 Pct Recovery = 19%  Analysis Date = 02/13/14 
 Pct Recovery = 19%  Analysis Date = 02/13/14 
 Pct Recovery = 19%  Analysis Date = 02/11/14 
 Pct Recovery = 19%  Analysis Date = 02/11/14 
 Pct Recovery = 19%  Analysis Date = 02/08/14 
 Pct Recovery = 19%  Analysis Date = 02/08/14 
 Pct Recovery = 19%  Analysis Date = 02/06/14 
 Pct Recovery = 19%  Analysis Date = 02/06/14 
 Pct Recovery = 19%  Analysis Date = 02/03/14 
 Pct Recovery = 20%  Analysis Date = 02/03/14 
 Pct Recovery = 20%  Analysis Date = 02/01/14 
 Pct Recovery = 20%  Analysis Date = 02/01/14 
 Pct Recovery = 20%  Analysis Date = 01/30/14 
 Pct Recovery = 20%  Analysis Date = 01/30/14 
 Pct Recovery = 20%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/27/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/22/14 
 Pct Recovery = 21%  Analysis Date = 01/22/14 
 Pct Recovery = 21%  Analysis Date = 01/20/14 
 Pct Recovery = 21%  Analysis Date = 01/20/14 
 Pct Recovery = 21%  Analysis Date = 01/18/14 
 Pct Recovery = 21%  Analysis Date = 01/18/14 
 Pct Recovery = 21%  Analysis Date = 01/15/14 
 Pct Recovery = 21%  Analysis Date = 01/15/14 
 Pct Recovery = 21%  Analysis Date = 01/13/14 
 Pct Recovery = 21%  Analysis Date = 01/13/14 
 Pct Recovery = 21%  Analysis Date = 01/10/14 
 Pct Recovery = 22%  Analysis Date = 01/10/14 
 Pct Recovery = 22%  Analysis Date = 01/08/14 
 Pct Recovery = 22%  Analysis Date = 01/08/14 
 Pct Recovery = 22%  Analysis Date = 01/06/14 
 Pct Recovery = 22%  Analysis Date = 01/06/14 
 Pct Recovery = 22%  Analysis Date = 01/03/14 
 Pct Recovery = 22%  Analysis Date = 01/03/14 
 Pct Recovery = 22%  Analysis Date = 01/01/14 
 Pct Recovery = 22%  Analysis Date = 01/01/14 
 Pct Recovery = 22%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/27/13 
 Pct Recovery = 23%  Analysis Date = 12/27/13 
 Pct Recovery = 23%  Analysis Date = 12/24/13 
 Pct Recovery = 23%  Analysis Date = 12/24/13 
 Pct Recovery = 23%  Analysis Date = 12/22/13 
 Pct Recovery = 23%  Analysis Date = 12/22/13 
 Pct Recovery = 23%  Analysis Date = 12/20/13 
 Pct Recovery = 23%  Analysis Date = 12/20/13 
 Pct Recovery = 23%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/15/13 
 Pct Recovery = 24%  Analysis Date = 12/15/13 
 Pct Recovery = 24%  Analysis Date = 12/12/13 
 Pct Recovery = 24%  Analysis Date = 12/12/13 
 Pct Recovery = 24%  Analysis Date = 12/10/13 
 Pct Recovery = 24%  Analysis Date = 12/10/13 
 Pct Recovery = 24%  Analysis Date = 12/08/13 
 Pct Recovery = 24%  Analysis Date = 12/08/13 
 Pct Recovery = 24%  Analysis Date = 12/05/13 
 Pct Recovery = 24%  Analysis Date = 12/05/13 
 Pct Recovery = 24%  Analysis Date = 12/03/13 
 Pct Recovery = 25%  Analysis Date = 12/03/13 
 Pct Recovery = 25%  Analysis Date = 11/30/13 
 Pct Recovery = 25%  Analysis Date = 11/30/13 
 Pct Recovery = 25%  Analysis Date = 11/28/13 
 Pct Recovery = 25%  Analysis Date = 11/28/13 
 Pct Recovery = 25%  Analysis Date = 11/26/13 
 Pct Recovery = 25%  Analysis Date = 11/26/13 
 Pct Recovery = 25%  Analysis Date = 11/23/13 
 Pct Recovery = 25%  Analysis Date = 11/23/13 
 Pct Recovery = 25%  Analysis Date = 11/21/13 
 Pct Recovery = 26%  Analysis Date = 11/21/13 
 Pct Recovery = 26%  Analysis Date = 11/18/13 
 Pct Recovery = 26%  Analysis Date = 11/18/13 
 Pct Recovery = 26%  Analysis Date = 11/16/13 
 Pct Recovery = 26%  Analysis Date = 11/16/13 
 Pct Recovery = 26%  Analysis Date = 11/13/13 
 Pct Recovery = 26%  Analysis Date = 11/13/13 
 Pct Recovery = 26%  Analysis Date = 11/11/13 
 Pct Recovery = 26%  Analysis Date = 11/11/13 
 Pct Recovery = 26%  Analysis Date = 11/09/13 
 Pct Recovery = 27%  Analysis Date = 11/09/13 
 Pct Recovery = 27%  Analysis Date = 11/06/13 
 Pct Recovery = 27%  Analysis Date = 11/06/13 
 Pct Recovery = 27%  Analysis Date = 11/04/13 
 Pct Recovery = 27%  Analysis Date = 11/04/13 
 Pct Recovery = 27%  Analysis Date = 11/01/13 
 Pct Recovery = 27%  Analysis Date = 11/01/13 
 Pct Recovery = 27%  Analysis Date = 10/30/13 
 Pct Recovery = 27%  Analysis Date = 10/30/13 
 Pct Recovery = 27%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/23/13 
 Pct Recovery = 28%  Analysis Date = 10/23/13 
 Pct Recovery = 28%  Analysis Date = 10/20/13 
 Pct Recovery = 29%  Analysis Date = 10/20/13 
 Pct Recovery = 29%  Analysis Date = 10/18/13 
 Pct Recovery = 29%  Analysis Date = 10/18/13 
 Pct Recovery = 29%  Analysis Date = 10/16/13 
 Pct Recovery = 30%  Analysis Date = 10/16/13 
 Pct Recovery = 30%  Analysis Date = 10/13/13 
 Pct Recovery = 30%  Analysis Date = 10/13/13 
 Pct Recovery = 30%  Analysis Date = 10/11/13 
 Pct Recovery = 30%  Analysis Date = 10/11/13 
 Pct Recovery = 30%  Analysis Date = 10/08/13 
 Pct Recovery = 31%  Analysis Date = 10/08/13 
 Pct Recovery = 31%  Analysis Date = 10/06/13 
 Pct Recovery = 31%  Analysis Date = 10/06/13 
 Pct Recovery = 31%  Analysis Date = 10/04/13 
 Pct Recovery = 31%  Analysis Date = 10/04/13 
 Pct Recovery = 31%  Analysis Date = 10/01/13 
 Pct Recovery = 32%  Analysis Date = 10/01/13 
 Pct Recovery = 32%  Analysis Date = 09/29/13 
 Pct Recovery = 32%  Analysis Date = 09/29/13 
 Pct Recovery = 32%  Analysis Date = 09/26/13 
 Pct Recovery = 33%  Analysis Date = 09/26/13 
 Pct Recovery = 33%  Analysis Date = 09/24/13 
 Pct Recovery = 33%  Analysis Date = 09/24/13 
 Pct Recovery = 33%  Analysis Date = 09/21/13 
 Pct Recovery = 33%  Analysis Date = 09/21/13 
 Pct Recovery = 33%  Analysis Date = 09/19/13 
 Pct Recovery = 34%  Analysis Date = 09/19/13 
 Pct Recovery = 34%  Analysis Date = 09/17/13 
 Pct Recovery = 34%  Analysis Date = 09/17/13 
 Pct Recovery = 34%  Analysis Date = 09/14/13 
 Pct Recovery = 35%  Analysis Date = 09/14/13 
 Pct Recovery = 35%  Analysis Date = 09/12/13 
 Pct Recovery = 35%  Analysis Date = 09/12/13 
 Pct Recovery = 35%  Analysis Date = 09/09/13 
 Pct Recovery = 35%  Analysis Date = 09/09/13 
 Pct Recovery = 35%  Analysis Date = 09/07/13 
 Pct Recovery = 36%  Analysis Date = 09/07/13 
 Pct Recovery = 36%  Analysis Date = 09/05/13 
 Pct Recovery = 36%  Analysis Date = 09/05/13 
 Pct Recovery = 36%  Analysis Date = 09/02/13 
 Pct Recovery = 37%  Analysis Date = 09/02/13 
 Pct Recovery = 37%  Analysis Date = 08/31/13 
 Pct Recovery = 37%  Analysis Date = 08/31/13 
 Pct Recovery = 37%  Analysis Date = 08/28/13 
 Pct Recovery = 37%  Analysis Date = 08/28/13 
 Pct Recovery = 37%  Analysis Date = 08/26/13 
 Pct Recovery = 38%  Analysis Date = 08/26/13 
 Pct Recovery = 38%  Analysis Date = 08/24/13 
 Pct Recovery = 38%  Analysis Date = 08/24/13 
 Pct Recovery = 38%  Analysis Date = 08/21/13 
 Pct Recovery = 38%  Analysis Date = 08/21/13 
 Pct Recovery = 38%  Analysis Date = 08/19/13 
 Pct Recovery = 39%  Analysis Date = 08/19/13 
 Pct Recovery = 39%  Analysis Date = 08/16/13 
 Pct Recovery = 39%  Analysis Date = 08/16/13 
 Pct Recovery = 39%  Analysis Date = 08/14/13 
 Pct Recovery = 39%  Analysis Date = 08/14/13 
 Pct Recovery = 39%  Analysis Date = 08/11/13 
 Pct Recovery = 40%  Analysis Date = 08/11/13 
 Pct Recovery = 40%  Analysis Date = 08/09/13 
 Pct Recovery = 40%  Analysis Date = 08/09/13 
 Pct Recovery = 40%  Analysis Date = 08/07/13 
 Pct Recovery = 40%  Analysis Date = 08/07/13 
 Pct Recovery = 40%  Analysis Date = 08/04/13 
 Pct Recovery = 41%  Analysis Date = 08/04/13 
 Pct Recovery = 41%  Analysis Date = 08/02/13 
 Pct Recovery = 41%  Analysis Date = 08/02/13 
 Pct Recovery = 41%  Analysis Date = 07/30/13 
 Pct Recovery = 41%  Analysis Date = 07/30/13 
 Pct Recovery = 41%  Analysis Date = 07/28/13 
 Pct Recovery = 41%  Analysis Date = 07/28/13 
 Pct Recovery = 41%  Analysis Date = 07/26/13 
 Pct Recovery = 42%  Analysis Date = 07/26/13 
 Pct Recovery = 42%  Analysis Date = 07/23/13 
 Pct Recovery = 42%  Analysis Date = 07/23/13 
 Pct Recovery = 42%  Analysis Date = 07/21/13 
 Pct Recovery = 42%  Analysis Date = 07/21/13 
 Pct Recovery = 42%  Analysis Date = 07/18/13 
 Pct Recovery = 42%  Analysis Date = 07/18/13 
 Pct Recovery = 42%  Analysis Date = 07/16/13 
 Pct Recovery = 43%  Analysis Date = 07/16/13 
 Pct Recovery = 43%  Analysis Date = 07/14/13 
 Pct Recovery = 43%  Analysis Date = 07/14/13 
 Pct Recovery = 43%  Analysis Date = 07/11/13 
 Pct Recovery = 43%  Analysis Date = 07/11/13 
 Pct Recovery = 43%  Analysis Date = 07/09/13 
 Pct Recovery = 43%  Analysis Date = 07/09/13 
 Pct Recovery = 43%  Analysis Date = 07/06/13 
 Pct Recovery = 44%  Analysis Date = 07/06/13 
 Pct Recovery = 44%  Analysis Date = 07/04/13 
 Pct Recovery = 44%  Analysis Date = 07/04/13 
 Pct Recovery = 44%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 07/02/13 
 Pct Recovery = 44%  Analysis Date = 06/29/13 
 Pct Recovery = 44%  Analysis Date = 06/29/13 
 Pct Recovery = 44%  Analysis Date = 06/27/13 
 Pct Recovery = 45%  Analysis Date = 06/27/13 
 Pct Recovery = 45%  Analysis Date = 06/24/13 
 Pct Recovery = 45%  Analysis Date = 06/24/13 
 Pct Recovery = 45%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/19/13 
 Pct Recovery = 46%  Analysis Date = 06/17/13 
 Pct Recovery = 46%  Analysis Date = 06/17/13 
 Pct Recovery = 46%  Analysis Date = 06/15/13 
 Pct Recovery = 46%  Analysis Date = 06/15/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/12/13 
 Pct Recovery = 46%  Analysis Date = 06/10/13 
 Pct Recovery = 47%  Analysis Date = 06/10/13 
 Pct Recovery = 47%  Analysis Date = 06/07/13 
 Pct Recovery = 47%  Analysis Date = 06/07/13 
 Pct Recovery = 47%  Analysis Date = 06/05/13 
 Pct Recovery = 47%  Analysis Date = 06/05/13 
 Pct Recovery = 47%  Analysis Date = 06/03/13 
 Pct Recovery = 47%  Analysis Date = 06/03/13 
 Pct Recovery = 47%  Analysis Date = 05/31/13 
 Pct Recovery = 48%  Analysis Date = 05/31/13 
 Pct Recovery = 48%  Analysis Date = 05/29/13 
 Pct Recovery = 48%  Analysis Date = 05/29/13 
 Pct Recovery = 48%  Analysis Date = 05/26/13 
 Pct Recovery = 48%  Analysis Date = 05/26/13 
 Pct Recovery = 48%  Analysis Date = 05/24/13 
 Pct Recovery = 48%  Analysis Date = 05/24/13 
 Pct Recovery = 48%  Analysis Date = 05/22/13 
 Pct Recovery = 49%  Analysis Date = 05/22/13 
 Pct Recovery = 49%  Analysis Date = 05/19/13 
 Pct Recovery = 49%  Analysis Date = 05/19/13 
 Pct Recovery = 49%  Analysis Date = 05/17/13 
 Pct Recovery = 49%  Analysis Date = 05/17/13 
 Pct Recovery = 49%  Analysis Date = 05/14/13 
 Pct Recovery = 50%  Analysis Date = 05/14/13 
 Pct Recovery = 50%  Analysis Date = 05/12/13 
 Pct Recovery = 50%  Analysis Date = 05/12/13 
 Pct Recovery = 50%  Analysis Date = 05/10/13 
 Pct Recovery = 50%  Analysis Date = 05/10/13 
 Pct Recovery = 50%  Analysis Date = 05/07/13 
 Pct Recovery = 50%  Analysis Date = 05/07/13 
 Pct Recovery = 50%  Analysis Date = 05/05/13 
 Pct Recovery = 51%  Analysis Date = 05/05/13 
 Pct Recovery = 51%  Analysis Date = 05/02/13 
 Pct Recovery = 51%  Analysis Date = 05/02/13 
 Pct Recovery = 51%  Analysis Date = 04/30/13 
 Pct Recovery = 49%  Analysis Date = 04/30/13 
 Pct Recovery = 49%  Analysis Date = 04/27/13 
 Pct Recovery = 45%  Analysis Date = 04/27/13 
 Pct Recovery = 45%  Analysis Date = 04/25/13 
 Pct Recovery = 43%  Analysis Date = 04/25/13 
 Pct Recovery = 43%  Analysis Date = 04/23/13 
 Pct Recovery = 42%  Analysis Date = 04/23/13 
 Pct Recovery = 42%  Analysis Date = 04/20/13 
 Pct Recovery = 42%  Analysis Date = 04/20/13 
 Pct Recovery = 42%  Analysis Date = 04/18/13 
 Pct Recovery = 41%  Analysis Date = 04/18/13 
 Pct Recovery = 41%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/11/13 
 Pct Recovery = 40%  Analysis Date = 04/11/13 
 Pct Recovery = 40%  Analysis Date = 04/08/13 
 Pct Recovery = 39%  Analysis Date = 04/08/13 
 Pct Recovery = 39%  Analysis Date = 04/06/13 
 Pct Recovery = 38%  Analysis Date = 04/06/13 
 Pct Recovery = 38%  Analysis Date = 04/03/13 
 Pct Recovery = 38%  Analysis Date = 04/03/13 
 Pct Recovery = 38%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 Pct Recovery = 36%  Analysis Date = 03/27/13 
 Pct Recovery = 36%  Analysis Date = 03/25/13 
 Pct Recovery = 36%  Analysis Date = 03/25/13 
 Pct Recovery = 36%  Analysis Date = 03/22/13 
 Pct Recovery = 36%  Analysis Date = 03/22/13 
 Pct Recovery = 36%  Analysis Date = 03/20/13 
 Pct Recovery = 36%  Analysis Date = 03/20/13 
 Pct Recovery = 36%  Analysis Date = 03/17/13 
 Pct Recovery = 36%  Analysis Date = 03/17/13 
 Pct Recovery = 36%  Analysis Date = 03/15/13 
 Pct Recovery = 36%  Analysis Date = 03/15/13 
 Pct Recovery = 36%  Analysis Date = 03/13/13 
 Pct Recovery = 36%  Analysis Date = 03/13/13 
 Pct Recovery = 36%  Analysis Date = 03/10/13 
 Pct Recovery = 36%  Analysis Date = 03/10/13 
 Pct Recovery = 36%  Analysis Date = 03/08/13 
 Pct Recovery = 36%  Analysis Date = 03/08/13 
 Pct Recovery = 36%  Analysis Date = 03/05/13 
 Pct Recovery = 36%  Analysis Date = 03/05/13 
 Pct Recovery = 36%  Analysis Date = 03/03/13 
 Pct Recovery = 36%  Analysis Date = 03/03/13 
 Pct Recovery = 36%  Analysis Date = 03/01/13 
 Pct Recovery = 36%  Analysis Date = 03/01/13 
 Pct Recovery = 36%  Analysis Date = 02/26/13 
 Pct Recovery = 36%  Analysis Date = 02/26/13 
 Pct Recovery = 36%  Analysis Date = 02/24/13 
 Pct Recovery = 36%  Analysis Date = 02/24/13 
 Pct Recovery = 36%  Analysis Date = 02/21/13 
 Pct Recovery = 36%  Analysis Date = 02/21/13 
 Pct Recovery = 36%  Analysis Date = 02/19/13 
 Pct Recovery = 36%  Analysis Date = 02/19/13 
 Pct Recovery = 36%  Analysis Date = 02/17/13 
 Pct Recovery = 36%  Analysis Date = 02/17/13 
 Pct Recovery = 36%  Analysis Date = 02/14/13 
 Pct Recovery = 36%  Analysis Date = 02/14/13 
 Pct Recovery = 36%  Analysis Date = 02/12/13 
 Pct Recovery = 36%  Analysis Date = 02/12/13 
 Pct Recovery = 36%  Analysis Date = 02/09/13 
 Pct Recovery = 36%  Analysis Date = 02/09/13 
 Pct Recovery = 36%  Analysis Date = 02/07/13 
 Pct Recovery = 36%  Analysis Date = 02/07/13 
 Pct Recovery = 36%  Analysis Date = 02/05/13 
 Pct Recovery = 35%  Analysis Date = 02/05/13 
 Pct Recovery = 35%  Analysis Date = 02/02/13 
 Pct Recovery = 35%  Analysis Date = 02/02/13 
 Pct Recovery = 35%  Analysis Date = 01/31/13 
 Pct Recovery = 35%  Analysis Date = 01/31/13 
 Pct Recovery = 35%  Analysis Date = 01/28/13 
 Pct Recovery = 35%  Analysis Date = 01/28/13 
 Pct Recovery = 35%  Analysis Date = 01/26/13 
 Pct Recovery = 35%  Analysis Date = 01/26/13 
 Pct Recovery = 35%  Analysis Date = 01/23/13 
 Pct Recovery = 35%  Analysis Date = 01/23/13 
 Pct Recovery = 35%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/19/13 
 Pct Recovery = 36%  Analysis Date = 01/19/13 
 Pct Recovery = 36%  Analysis Date = 01/16/13 
 Pct Recovery = 36%  Analysis Date = 01/16/13 
 Pct Recovery = 36%  Analysis Date = 01/14/13 
 Pct Recovery = 36%  Analysis Date = 01/14/13 
 Pct Recovery = 36%  Analysis Date = 01/11/13 
 Pct Recovery = 36%  Analysis Date = 01/11/13 
 Pct Recovery = 36%  Analysis Date = 01/09/13 
 Pct Recovery = 36%  Analysis Date = 01/09/13 
 Pct Recovery = 36%  Analysis Date = 01/07/13 
 Pct Recovery = 36%  Analysis Date = 01/07/13 
 Pct Recovery = 36%  Analysis Date = 01/04/13 
 Pct Recovery = 37%  Analysis Date = 01/04/13 
 Pct Recovery = 37%  Analysis Date = 01/02/13 
 Pct Recovery = 37%  Analysis Date = 01/02/13 
 Pct Recovery = 37%  Analysis Date = 12/30/12 
 Pct Recovery = 37%  Analysis Date = 12/30/12 
 Pct Recovery = 37%  Analysis Date = 12/28/12 
 Pct Recovery = 37%  Analysis Date = 12/28/12 
 Pct Recovery = 37%  Analysis Date = 12/26/12 
 Pct Recovery = 37%  Analysis Date = 12/26/12 
 Pct Recovery = 37%  Analysis Date = 12/23/12 
 Pct Recovery = 37%  Analysis Date = 12/23/12 
 Pct Recovery = 37%  Analysis Date = 12/21/12 
 Pct Recovery = 37%  Analysis Date = 12/21/12 
 Pct Recovery = 37%  Analysis Date = 12/18/12 
 Pct Recovery = 38%  Analysis Date = 12/18/12 
 Pct Recovery = 38%  Analysis Date = 12/16/12 
 Pct Recovery = 38%  Analysis Date = 12/16/12 
 Pct Recovery = 38%  Analysis Date = 12/14/12 
 Pct Recovery = 38%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
NORVERAPAMIL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 26% . 26% 0%
>= Reporting Level 13 31% 18% 25% 25%
Total 14 31% 17% 26% 25%

Sample Statistics
NORVERAPAMIL

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 14 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
OMEPRAZOLE + ESOMEPRAZOLE
METHOD: LC9017 , TESTIDCODE: 67512LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 15%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 38%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 29%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 37%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 31%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 41%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 28%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 33%  Analysis Date = 04/09/14 
 Pct Recovery = 30%  Analysis Date = 04/07/14 
 Pct Recovery = 31%  Analysis Date = 04/07/14 
 Pct Recovery = 31%  Analysis Date = 04/05/14 
 Pct Recovery = 31%  Analysis Date = 04/05/14 
 Pct Recovery = 31%  Analysis Date = 04/02/14 
 Pct Recovery = 31%  Analysis Date = 04/02/14 
 Pct Recovery = 31%  Analysis Date = 03/31/14 
 Pct Recovery = 31%  Analysis Date = 03/31/14 
 Pct Recovery = 31%  Analysis Date = 03/28/14 
 Pct Recovery = 31%  Analysis Date = 03/28/14 
 Pct Recovery = 31%  Analysis Date = 03/26/14 
 Pct Recovery = 31%  Analysis Date = 03/26/14 
 Pct Recovery = 31%  Analysis Date = 03/24/14 
 Pct Recovery = 31%  Analysis Date = 03/24/14 
 Pct Recovery = 31%  Analysis Date = 03/21/14 
 Pct Recovery = 31%  Analysis Date = 03/21/14 
 Pct Recovery = 31%  Analysis Date = 03/19/14 
 Pct Recovery = 31%  Analysis Date = 03/19/14 
 Pct Recovery = 31%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/14/14 
 Pct Recovery = 32%  Analysis Date = 03/14/14 
 Pct Recovery = 32%  Analysis Date = 03/12/14 
 Pct Recovery = 32%  Analysis Date = 03/12/14 
 Pct Recovery = 32%  Analysis Date = 03/09/14 
 Pct Recovery = 32%  Analysis Date = 03/09/14 
 Pct Recovery = 32%  Analysis Date = 03/07/14 
 Pct Recovery = 32%  Analysis Date = 03/07/14 
 Pct Recovery = 32%  Analysis Date = 03/04/14 
 Pct Recovery = 32%  Analysis Date = 03/04/14 
 Pct Recovery = 32%  Analysis Date = 03/02/14 
 Pct Recovery = 32%  Analysis Date = 03/02/14 
 Pct Recovery = 32%  Analysis Date = 02/28/14 
 Pct Recovery = 32%  Analysis Date = 02/28/14 
 Pct Recovery = 32%  Analysis Date = 02/25/14 
 Pct Recovery = 33%  Analysis Date = 02/25/14 
 Pct Recovery = 33%  Analysis Date = 02/23/14 
 Pct Recovery = 33%  Analysis Date = 02/23/14 
 Pct Recovery = 33%  Analysis Date = 02/20/14 
 Pct Recovery = 33%  Analysis Date = 02/20/14 
 Pct Recovery = 33%  Analysis Date = 02/18/14 
 Pct Recovery = 33%  Analysis Date = 02/18/14 
 Pct Recovery = 33%  Analysis Date = 02/15/14 
 Pct Recovery = 33%  Analysis Date = 02/15/14 
 Pct Recovery = 33%  Analysis Date = 02/13/14 
 Pct Recovery = 33%  Analysis Date = 02/13/14 
 Pct Recovery = 33%  Analysis Date = 02/11/14 
 Pct Recovery = 33%  Analysis Date = 02/11/14 
 Pct Recovery = 33%  Analysis Date = 02/08/14 
 Pct Recovery = 33%  Analysis Date = 02/08/14 
 Pct Recovery = 33%  Analysis Date = 02/06/14 
 Pct Recovery = 33%  Analysis Date = 02/06/14 
 Pct Recovery = 33%  Analysis Date = 02/03/14 
 Pct Recovery = 33%  Analysis Date = 02/03/14 
 Pct Recovery = 33%  Analysis Date = 02/01/14 
 Pct Recovery = 33%  Analysis Date = 02/01/14 
 Pct Recovery = 33%  Analysis Date = 01/30/14 
 Pct Recovery = 32%  Analysis Date = 01/30/14 
 Pct Recovery = 32%  Analysis Date = 01/27/14 
 Pct Recovery = 32%  Analysis Date = 01/27/14 
 Pct Recovery = 32%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/25/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/20/14 
 Pct Recovery = 32%  Analysis Date = 01/20/14 
 Pct Recovery = 32%  Analysis Date = 01/18/14 
 Pct Recovery = 32%  Analysis Date = 01/18/14 
 Pct Recovery = 32%  Analysis Date = 01/15/14 
 Pct Recovery = 32%  Analysis Date = 01/15/14 
 Pct Recovery = 32%  Analysis Date = 01/13/14 
 Pct Recovery = 32%  Analysis Date = 01/13/14 
 Pct Recovery = 32%  Analysis Date = 01/10/14 
 Pct Recovery = 32%  Analysis Date = 01/10/14 
 Pct Recovery = 32%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/08/14 
 Pct Recovery = 32%  Analysis Date = 01/06/14 
 Pct Recovery = 31%  Analysis Date = 01/06/14 
 Pct Recovery = 31%  Analysis Date = 01/03/14 
 Pct Recovery = 31%  Analysis Date = 01/03/14 
 Pct Recovery = 31%  Analysis Date = 01/01/14 
 Pct Recovery = 31%  Analysis Date = 01/01/14 
 Pct Recovery = 31%  Analysis Date = 12/29/13 
 Pct Recovery = 31%  Analysis Date = 12/29/13 
 Pct Recovery = 31%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/24/13 
 Pct Recovery = 30%  Analysis Date = 12/24/13 
 Pct Recovery = 30%  Analysis Date = 12/22/13 
 Pct Recovery = 30%  Analysis Date = 12/22/13 
 Pct Recovery = 30%  Analysis Date = 12/20/13 
 Pct Recovery = 30%  Analysis Date = 12/20/13 
 Pct Recovery = 30%  Analysis Date = 12/17/13 
 Pct Recovery = 30%  Analysis Date = 12/17/13 
 Pct Recovery = 30%  Analysis Date = 12/15/13 
 Pct Recovery = 30%  Analysis Date = 12/15/13 
 Pct Recovery = 30%  Analysis Date = 12/12/13 
 Pct Recovery = 30%  Analysis Date = 12/12/13 
 Pct Recovery = 30%  Analysis Date = 12/10/13 
 Pct Recovery = 29%  Analysis Date = 12/10/13 
 Pct Recovery = 29%  Analysis Date = 12/08/13 
 Pct Recovery = 29%  Analysis Date = 12/08/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 11/30/13 
 Pct Recovery = 29%  Analysis Date = 11/30/13 
 Pct Recovery = 29%  Analysis Date = 11/28/13 
 Pct Recovery = 28%  Analysis Date = 11/28/13 
 Pct Recovery = 28%  Analysis Date = 11/26/13 
 Pct Recovery = 28%  Analysis Date = 11/26/13 
 Pct Recovery = 28%  Analysis Date = 11/23/13 
 Pct Recovery = 28%  Analysis Date = 11/23/13 
 Pct Recovery = 28%  Analysis Date = 11/21/13 
 Pct Recovery = 28%  Analysis Date = 11/21/13 
 Pct Recovery = 28%  Analysis Date = 11/18/13 
 Pct Recovery = 28%  Analysis Date = 11/18/13 
 Pct Recovery = 28%  Analysis Date = 11/16/13 
 Pct Recovery = 28%  Analysis Date = 11/16/13 
 Pct Recovery = 28%  Analysis Date = 11/13/13 
 Pct Recovery = 28%  Analysis Date = 11/13/13 
 Pct Recovery = 28%  Analysis Date = 11/11/13 
 Pct Recovery = 28%  Analysis Date = 11/11/13 
 Pct Recovery = 28%  Analysis Date = 11/09/13 
 Pct Recovery = 28%  Analysis Date = 11/09/13 
 Pct Recovery = 28%  Analysis Date = 11/06/13 
 Pct Recovery = 28%  Analysis Date = 11/06/13 
 Pct Recovery = 28%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/23/13 
 Pct Recovery = 28%  Analysis Date = 10/23/13 
 Pct Recovery = 28%  Analysis Date = 10/20/13 
 Pct Recovery = 28%  Analysis Date = 10/20/13 
 Pct Recovery = 28%  Analysis Date = 10/18/13 
 Pct Recovery = 28%  Analysis Date = 10/18/13 
 Pct Recovery = 28%  Analysis Date = 10/16/13 
 Pct Recovery = 27%  Analysis Date = 10/16/13 
 Pct Recovery = 27%  Analysis Date = 10/13/13 
 Pct Recovery = 27%  Analysis Date = 10/13/13 
 Pct Recovery = 27%  Analysis Date = 10/11/13 
 Pct Recovery = 27%  Analysis Date = 10/11/13 
 Pct Recovery = 27%  Analysis Date = 10/08/13 
 Pct Recovery = 27%  Analysis Date = 10/08/13 
 Pct Recovery = 27%  Analysis Date = 10/06/13 
 Pct Recovery = 27%  Analysis Date = 10/06/13 
 Pct Recovery = 27%  Analysis Date = 10/04/13 
 Pct Recovery = 27%  Analysis Date = 10/04/13 
 Pct Recovery = 27%  Analysis Date = 10/01/13 
 Pct Recovery = 27%  Analysis Date = 10/01/13 
 Pct Recovery = 27%  Analysis Date = 09/29/13 
 Pct Recovery = 27%  Analysis Date = 09/29/13 
 Pct Recovery = 27%  Analysis Date = 09/26/13 
 Pct Recovery = 27%  Analysis Date = 09/26/13 
 Pct Recovery = 27%  Analysis Date = 09/24/13 
 Pct Recovery = 27%  Analysis Date = 09/24/13 
 Pct Recovery = 27%  Analysis Date = 09/21/13 
 Pct Recovery = 27%  Analysis Date = 09/21/13 
 Pct Recovery = 27%  Analysis Date = 09/19/13 
 Pct Recovery = 27%  Analysis Date = 09/19/13 
 Pct Recovery = 27%  Analysis Date = 09/17/13 
 Pct Recovery = 27%  Analysis Date = 09/17/13 
 Pct Recovery = 27%  Analysis Date = 09/14/13 
 Pct Recovery = 27%  Analysis Date = 09/14/13 
 Pct Recovery = 27%  Analysis Date = 09/12/13 
 Pct Recovery = 27%  Analysis Date = 09/12/13 
 Pct Recovery = 27%  Analysis Date = 09/09/13 
 Pct Recovery = 27%  Analysis Date = 09/09/13 
 Pct Recovery = 27%  Analysis Date = 09/07/13 
 Pct Recovery = 27%  Analysis Date = 09/07/13 
 Pct Recovery = 27%  Analysis Date = 09/05/13 
 Pct Recovery = 27%  Analysis Date = 09/05/13 
 Pct Recovery = 27%  Analysis Date = 09/02/13 
 Pct Recovery = 27%  Analysis Date = 09/02/13 
 Pct Recovery = 27%  Analysis Date = 08/31/13 
 Pct Recovery = 27%  Analysis Date = 08/31/13 
 Pct Recovery = 27%  Analysis Date = 08/28/13 
 Pct Recovery = 27%  Analysis Date = 08/28/13 
 Pct Recovery = 27%  Analysis Date = 08/26/13 
 Pct Recovery = 27%  Analysis Date = 08/26/13 
 Pct Recovery = 27%  Analysis Date = 08/24/13 
 Pct Recovery = 27%  Analysis Date = 08/24/13 
 Pct Recovery = 27%  Analysis Date = 08/21/13 
 Pct Recovery = 27%  Analysis Date = 08/21/13 
 Pct Recovery = 27%  Analysis Date = 08/19/13 
 Pct Recovery = 27%  Analysis Date = 08/19/13 
 Pct Recovery = 27%  Analysis Date = 08/16/13 
 Pct Recovery = 27%  Analysis Date = 08/16/13 
 Pct Recovery = 27%  Analysis Date = 08/14/13 
 Pct Recovery = 27%  Analysis Date = 08/14/13 
 Pct Recovery = 27%  Analysis Date = 08/11/13 
 Pct Recovery = 27%  Analysis Date = 08/11/13 
 Pct Recovery = 27%  Analysis Date = 08/09/13 
 Pct Recovery = 27%  Analysis Date = 08/09/13 
 Pct Recovery = 27%  Analysis Date = 08/07/13 
 Pct Recovery = 27%  Analysis Date = 08/07/13 
 Pct Recovery = 27%  Analysis Date = 08/04/13 
 Pct Recovery = 27%  Analysis Date = 08/04/13 
 Pct Recovery = 27%  Analysis Date = 08/02/13 
 Pct Recovery = 27%  Analysis Date = 08/02/13 
 Pct Recovery = 27%  Analysis Date = 07/30/13 
 Pct Recovery = 27%  Analysis Date = 07/30/13 
 Pct Recovery = 27%  Analysis Date = 07/28/13 
 Pct Recovery = 27%  Analysis Date = 07/28/13 
 Pct Recovery = 27%  Analysis Date = 07/26/13 
 Pct Recovery = 27%  Analysis Date = 07/26/13 
 Pct Recovery = 27%  Analysis Date = 07/23/13 
 Pct Recovery = 27%  Analysis Date = 07/23/13 
 Pct Recovery = 27%  Analysis Date = 07/21/13 
 Pct Recovery = 27%  Analysis Date = 07/21/13 
 Pct Recovery = 27%  Analysis Date = 07/18/13 
 Pct Recovery = 27%  Analysis Date = 07/18/13 
 Pct Recovery = 27%  Analysis Date = 07/16/13 
 Pct Recovery = 27%  Analysis Date = 07/16/13 
 Pct Recovery = 27%  Analysis Date = 07/14/13 
 Pct Recovery = 27%  Analysis Date = 07/14/13 
 Pct Recovery = 27%  Analysis Date = 07/11/13 
 Pct Recovery = 27%  Analysis Date = 07/11/13 
 Pct Recovery = 27%  Analysis Date = 07/09/13 
 Pct Recovery = 27%  Analysis Date = 07/09/13 
 Pct Recovery = 27%  Analysis Date = 07/06/13 
 Pct Recovery = 27%  Analysis Date = 07/06/13 
 Pct Recovery = 27%  Analysis Date = 07/04/13 
 Pct Recovery = 27%  Analysis Date = 07/04/13 
 Pct Recovery = 27%  Analysis Date = 07/02/13 
 Pct Recovery = 27%  Analysis Date = 07/02/13 
 Pct Recovery = 27%  Analysis Date = 06/29/13 
 Pct Recovery = 27%  Analysis Date = 06/29/13 
 Pct Recovery = 27%  Analysis Date = 06/27/13 
 Pct Recovery = 27%  Analysis Date = 06/27/13 
 Pct Recovery = 27%  Analysis Date = 06/24/13 
 Pct Recovery = 27%  Analysis Date = 06/24/13 
 Pct Recovery = 27%  Analysis Date = 06/22/13 
 Pct Recovery = 27%  Analysis Date = 06/22/13 
 Pct Recovery = 27%  Analysis Date = 06/19/13 
 Pct Recovery = 27%  Analysis Date = 06/19/13 
 Pct Recovery = 27%  Analysis Date = 06/17/13 
 Pct Recovery = 27%  Analysis Date = 06/17/13 
 Pct Recovery = 27%  Analysis Date = 06/15/13 
 Pct Recovery = 27%  Analysis Date = 06/15/13 
 Pct Recovery = 27%  Analysis Date = 06/12/13 
 Pct Recovery = 27%  Analysis Date = 06/12/13 
 Pct Recovery = 27%  Analysis Date = 06/10/13 
 Pct Recovery = 27%  Analysis Date = 06/10/13 
 Pct Recovery = 27%  Analysis Date = 06/07/13 
 Pct Recovery = 27%  Analysis Date = 06/07/13 
 Pct Recovery = 27%  Analysis Date = 06/05/13 
 Pct Recovery = 27%  Analysis Date = 06/05/13 
 Pct Recovery = 27%  Analysis Date = 06/03/13 
 Pct Recovery = 27%  Analysis Date = 06/03/13 
 Pct Recovery = 27%  Analysis Date = 05/31/13 
 Pct Recovery = 27%  Analysis Date = 05/31/13 
 Pct Recovery = 27%  Analysis Date = 05/29/13 
 Pct Recovery = 27%  Analysis Date = 05/29/13 
 Pct Recovery = 27%  Analysis Date = 05/26/13 
 Pct Recovery = 27%  Analysis Date = 05/26/13 
 Pct Recovery = 27%  Analysis Date = 05/24/13 
 Pct Recovery = 27%  Analysis Date = 05/24/13 
 Pct Recovery = 27%  Analysis Date = 05/22/13 
 Pct Recovery = 27%  Analysis Date = 05/22/13 
 Pct Recovery = 27%  Analysis Date = 05/19/13 
 Pct Recovery = 27%  Analysis Date = 05/19/13 
 Pct Recovery = 27%  Analysis Date = 05/17/13 
 Pct Recovery = 27%  Analysis Date = 05/17/13 
 Pct Recovery = 27%  Analysis Date = 05/14/13 
 Pct Recovery = 27%  Analysis Date = 05/14/13 
 Pct Recovery = 27%  Analysis Date = 05/12/13 
 Pct Recovery = 27%  Analysis Date = 05/12/13 
 Pct Recovery = 27%  Analysis Date = 05/10/13 
 Pct Recovery = 26%  Analysis Date = 05/10/13 
 Pct Recovery = 26%  Analysis Date = 05/07/13 
 Pct Recovery = 26%  Analysis Date = 05/07/13 
 Pct Recovery = 26%  Analysis Date = 05/05/13 
 Pct Recovery = 26%  Analysis Date = 05/05/13 
 Pct Recovery = 26%  Analysis Date = 05/02/13 
 Pct Recovery = 27%  Analysis Date = 05/02/13 
 Pct Recovery = 27%  Analysis Date = 04/30/13 
 Pct Recovery = 32%  Analysis Date = 04/30/13 
 Pct Recovery = 32%  Analysis Date = 04/27/13 
 Pct Recovery = 37%  Analysis Date = 04/27/13 
 Pct Recovery = 37%  Analysis Date = 04/25/13 
 Pct Recovery = 41%  Analysis Date = 04/25/13 
 Pct Recovery = 41%  Analysis Date = 04/23/13 
 Pct Recovery = 40%  Analysis Date = 04/23/13 
 Pct Recovery = 40%  Analysis Date = 04/20/13 
 Pct Recovery = 40%  Analysis Date = 04/20/13 
 Pct Recovery = 40%  Analysis Date = 04/18/13 
 Pct Recovery = 40%  Analysis Date = 04/18/13 
 Pct Recovery = 40%  Analysis Date = 04/15/13 
 Pct Recovery = 40%  Analysis Date = 04/15/13 
 Pct Recovery = 40%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/13/13 
 Pct Recovery = 40%  Analysis Date = 04/11/13 
 Pct Recovery = 40%  Analysis Date = 04/11/13 
 Pct Recovery = 40%  Analysis Date = 04/08/13 
 Pct Recovery = 40%  Analysis Date = 04/08/13 
 Pct Recovery = 40%  Analysis Date = 04/06/13 
 Pct Recovery = 39%  Analysis Date = 04/06/13 
 Pct Recovery = 39%  Analysis Date = 04/03/13 
 Pct Recovery = 39%  Analysis Date = 04/03/13 
 Pct Recovery = 39%  Analysis Date = 04/01/13 
 Pct Recovery = 39%  Analysis Date = 04/01/13 
 Pct Recovery = 39%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/22/13 
 Pct Recovery = 39%  Analysis Date = 03/22/13 
 Pct Recovery = 39%  Analysis Date = 03/20/13 
 Pct Recovery = 39%  Analysis Date = 03/20/13 
 Pct Recovery = 39%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/15/13 
 Pct Recovery = 38%  Analysis Date = 03/15/13 
 Pct Recovery = 38%  Analysis Date = 03/13/13 
 Pct Recovery = 38%  Analysis Date = 03/13/13 
 Pct Recovery = 38%  Analysis Date = 03/10/13 
 Pct Recovery = 38%  Analysis Date = 03/10/13 
 Pct Recovery = 38%  Analysis Date = 03/08/13 
 Pct Recovery = 38%  Analysis Date = 03/08/13 
 Pct Recovery = 38%  Analysis Date = 03/05/13 
 Pct Recovery = 38%  Analysis Date = 03/05/13 
 Pct Recovery = 38%  Analysis Date = 03/03/13 
 Pct Recovery = 38%  Analysis Date = 03/03/13 
 Pct Recovery = 38%  Analysis Date = 03/01/13 
 Pct Recovery = 37%  Analysis Date = 03/01/13 
 Pct Recovery = 37%  Analysis Date = 02/26/13 
 Pct Recovery = 37%  Analysis Date = 02/26/13 
 Pct Recovery = 37%  Analysis Date = 02/24/13 
 Pct Recovery = 37%  Analysis Date = 02/24/13 
 Pct Recovery = 37%  Analysis Date = 02/21/13 
 Pct Recovery = 37%  Analysis Date = 02/21/13 
 Pct Recovery = 37%  Analysis Date = 02/19/13 
 Pct Recovery = 37%  Analysis Date = 02/19/13 
 Pct Recovery = 37%  Analysis Date = 02/17/13 
 Pct Recovery = 37%  Analysis Date = 02/17/13 
 Pct Recovery = 37%  Analysis Date = 02/14/13 
 Pct Recovery = 37%  Analysis Date = 02/14/13 
 Pct Recovery = 37%  Analysis Date = 02/12/13 
 Pct Recovery = 37%  Analysis Date = 02/12/13 
 Pct Recovery = 37%  Analysis Date = 02/09/13 
 Pct Recovery = 36%  Analysis Date = 02/09/13 
 Pct Recovery = 36%  Analysis Date = 02/07/13 
 Pct Recovery = 36%  Analysis Date = 02/07/13 
 Pct Recovery = 36%  Analysis Date = 02/05/13 
 Pct Recovery = 36%  Analysis Date = 02/05/13 
 Pct Recovery = 36%  Analysis Date = 02/02/13 
 Pct Recovery = 36%  Analysis Date = 02/02/13 
 Pct Recovery = 36%  Analysis Date = 01/31/13 
 Pct Recovery = 36%  Analysis Date = 01/31/13 
 Pct Recovery = 36%  Analysis Date = 01/28/13 
 Pct Recovery = 36%  Analysis Date = 01/28/13 
 Pct Recovery = 36%  Analysis Date = 01/26/13 
 Pct Recovery = 36%  Analysis Date = 01/26/13 
 Pct Recovery = 36%  Analysis Date = 01/23/13 
 Pct Recovery = 36%  Analysis Date = 01/23/13 
 Pct Recovery = 36%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/21/13 
 Pct Recovery = 35%  Analysis Date = 01/19/13 
 Pct Recovery = 35%  Analysis Date = 01/19/13 
 Pct Recovery = 35%  Analysis Date = 01/16/13 
 Pct Recovery = 35%  Analysis Date = 01/16/13 
 Pct Recovery = 35%  Analysis Date = 01/14/13 
 Pct Recovery = 35%  Analysis Date = 01/14/13 
 Pct Recovery = 35%  Analysis Date = 01/11/13 
 Pct Recovery = 35%  Analysis Date = 01/11/13 
 Pct Recovery = 35%  Analysis Date = 01/09/13 
 Pct Recovery = 35%  Analysis Date = 01/09/13 
 Pct Recovery = 35%  Analysis Date = 01/07/13 
 Pct Recovery = 35%  Analysis Date = 01/07/13 
 Pct Recovery = 35%  Analysis Date = 01/04/13 
 Pct Recovery = 34%  Analysis Date = 01/04/13 
 Pct Recovery = 34%  Analysis Date = 01/02/13 
 Pct Recovery = 34%  Analysis Date = 01/02/13 
 Pct Recovery = 34%  Analysis Date = 12/30/12 
 Pct Recovery = 34%  Analysis Date = 12/30/12 
 Pct Recovery = 34%  Analysis Date = 12/28/12 
 Pct Recovery = 34%  Analysis Date = 12/28/12 
 Pct Recovery = 34%  Analysis Date = 12/26/12 
 Pct Recovery = 34%  Analysis Date = 12/26/12 
 Pct Recovery = 34%  Analysis Date = 12/23/12 
 Pct Recovery = 34%  Analysis Date = 12/23/12 
 Pct Recovery = 34%  Analysis Date = 12/21/12 
 Pct Recovery = 34%  Analysis Date = 12/21/12 
 Pct Recovery = 34%  Analysis Date = 12/18/12 
 Pct Recovery = 34%  Analysis Date = 12/18/12 
 Pct Recovery = 34%  Analysis Date = 12/16/12 
 Pct Recovery = 33%  Analysis Date = 12/16/12 
 Pct Recovery = 33%  Analysis Date = 12/14/12 
 Pct Recovery = 33%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
OMEPRAZOLE + ESOMEPRAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 33% . 33% 0%
>= Reporting Level 7 31% 9% 31% 7%
Total 8 31% 8% 32% 7%

Sample Statistics
OMEPRAZOLE + ESOMEPRAZOLE

Characteristic N % % Basis
Plotted 8 57% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 6 43% 6 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
ORLISTAT
METHOD: LC9017 , TESTIDCODE: 67490LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 10%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 55%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 12%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 34%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 14%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 17%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 2%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 25%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 25%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 4%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 30%  Analysis Date = 04/09/14 
 Pct Recovery = 4%  Analysis Date = 04/07/14 
 Pct Recovery = 4%  Analysis Date = 04/07/14 
 Pct Recovery = 4%  Analysis Date = 04/05/14 
 Pct Recovery = 5%  Analysis Date = 04/05/14 
 Pct Recovery = 5%  Analysis Date = 04/02/14 
 Pct Recovery = 5%  Analysis Date = 04/02/14 
 Pct Recovery = 5%  Analysis Date = 03/31/14 
 Pct Recovery = 5%  Analysis Date = 03/31/14 
 Pct Recovery = 5%  Analysis Date = 03/28/14 
 Pct Recovery = 5%  Analysis Date = 03/28/14 
 Pct Recovery = 5%  Analysis Date = 03/26/14 
 Pct Recovery = 6%  Analysis Date = 03/26/14 
 Pct Recovery = 6%  Analysis Date = 03/24/14 
 Pct Recovery = 6%  Analysis Date = 03/24/14 
 Pct Recovery = 6%  Analysis Date = 03/21/14 
 Pct Recovery = 6%  Analysis Date = 03/21/14 
 Pct Recovery = 6%  Analysis Date = 03/19/14 
 Pct Recovery = 6%  Analysis Date = 03/19/14 
 Pct Recovery = 6%  Analysis Date = 03/16/14 
 Pct Recovery = 6%  Analysis Date = 03/16/14 
 Pct Recovery = 6%  Analysis Date = 03/14/14 
 Pct Recovery = 7%  Analysis Date = 03/14/14 
 Pct Recovery = 7%  Analysis Date = 03/12/14 
 Pct Recovery = 7%  Analysis Date = 03/12/14 
 Pct Recovery = 7%  Analysis Date = 03/09/14 
 Pct Recovery = 7%  Analysis Date = 03/09/14 
 Pct Recovery = 7%  Analysis Date = 03/07/14 
 Pct Recovery = 7%  Analysis Date = 03/07/14 
 Pct Recovery = 7%  Analysis Date = 03/04/14 
 Pct Recovery = 8%  Analysis Date = 03/04/14 
 Pct Recovery = 8%  Analysis Date = 03/02/14 
 Pct Recovery = 8%  Analysis Date = 03/02/14 
 Pct Recovery = 8%  Analysis Date = 02/28/14 
 Pct Recovery = 8%  Analysis Date = 02/28/14 
 Pct Recovery = 8%  Analysis Date = 02/25/14 
 Pct Recovery = 8%  Analysis Date = 02/25/14 
 Pct Recovery = 8%  Analysis Date = 02/23/14 
 Pct Recovery = 9%  Analysis Date = 02/23/14 
 Pct Recovery = 9%  Analysis Date = 02/20/14 
 Pct Recovery = 9%  Analysis Date = 02/20/14 
 Pct Recovery = 9%  Analysis Date = 02/18/14 
 Pct Recovery = 9%  Analysis Date = 02/18/14 
 Pct Recovery = 9%  Analysis Date = 02/15/14 
 Pct Recovery = 9%  Analysis Date = 02/15/14 
 Pct Recovery = 9%  Analysis Date = 02/13/14 
 Pct Recovery = 9%  Analysis Date = 02/13/14 
 Pct Recovery = 9%  Analysis Date = 02/11/14 
 Pct Recovery = 10%  Analysis Date = 02/11/14 
 Pct Recovery = 10%  Analysis Date = 02/08/14 
 Pct Recovery = 10%  Analysis Date = 02/08/14 
 Pct Recovery = 10%  Analysis Date = 02/06/14 
 Pct Recovery = 10%  Analysis Date = 02/06/14 
 Pct Recovery = 10%  Analysis Date = 02/03/14 
 Pct Recovery = 10%  Analysis Date = 02/03/14 
 Pct Recovery = 10%  Analysis Date = 02/01/14 
 Pct Recovery = 11%  Analysis Date = 02/01/14 
 Pct Recovery = 11%  Analysis Date = 01/30/14 
 Pct Recovery = 11%  Analysis Date = 01/30/14 
 Pct Recovery = 11%  Analysis Date = 01/27/14 
 Pct Recovery = 11%  Analysis Date = 01/27/14 
 Pct Recovery = 11%  Analysis Date = 01/25/14 
 Pct Recovery = 11%  Analysis Date = 01/25/14 
 Pct Recovery = 11%  Analysis Date = 01/22/14 
 Pct Recovery = 12%  Analysis Date = 01/22/14 
 Pct Recovery = 12%  Analysis Date = 01/20/14 
 Pct Recovery = 12%  Analysis Date = 01/20/14 
 Pct Recovery = 12%  Analysis Date = 01/18/14 
 Pct Recovery = 12%  Analysis Date = 01/18/14 
 Pct Recovery = 12%  Analysis Date = 01/15/14 
 Pct Recovery = 12%  Analysis Date = 01/15/14 
 Pct Recovery = 12%  Analysis Date = 01/13/14 
 Pct Recovery = 12%  Analysis Date = 01/13/14 
 Pct Recovery = 12%  Analysis Date = 01/10/14 
 Pct Recovery = 13%  Analysis Date = 01/10/14 
 Pct Recovery = 13%  Analysis Date = 01/08/14 
 Pct Recovery = 13%  Analysis Date = 01/08/14 
 Pct Recovery = 13%  Analysis Date = 01/06/14 
 Pct Recovery = 13%  Analysis Date = 01/06/14 
 Pct Recovery = 13%  Analysis Date = 01/03/14 
 Pct Recovery = 13%  Analysis Date = 01/03/14 
 Pct Recovery = 13%  Analysis Date = 01/01/14 
 Pct Recovery = 14%  Analysis Date = 01/01/14 
 Pct Recovery = 14%  Analysis Date = 12/29/13 
 Pct Recovery = 14%  Analysis Date = 12/29/13 
 Pct Recovery = 14%  Analysis Date = 12/27/13 
 Pct Recovery = 14%  Analysis Date = 12/27/13 
 Pct Recovery = 14%  Analysis Date = 12/24/13 
 Pct Recovery = 14%  Analysis Date = 12/24/13 
 Pct Recovery = 14%  Analysis Date = 12/22/13 
 Pct Recovery = 14%  Analysis Date = 12/22/13 
 Pct Recovery = 14%  Analysis Date = 12/20/13 
 Pct Recovery = 15%  Analysis Date = 12/20/13 
 Pct Recovery = 15%  Analysis Date = 12/17/13 
 Pct Recovery = 15%  Analysis Date = 12/17/13 
 Pct Recovery = 15%  Analysis Date = 12/15/13 
 Pct Recovery = 15%  Analysis Date = 12/15/13 
 Pct Recovery = 15%  Analysis Date = 12/12/13 
 Pct Recovery = 15%  Analysis Date = 12/12/13 
 Pct Recovery = 15%  Analysis Date = 12/10/13 
 Pct Recovery = 16%  Analysis Date = 12/10/13 
 Pct Recovery = 16%  Analysis Date = 12/08/13 
 Pct Recovery = 16%  Analysis Date = 12/08/13 
 Pct Recovery = 16%  Analysis Date = 12/05/13 
 Pct Recovery = 16%  Analysis Date = 12/05/13 
 Pct Recovery = 16%  Analysis Date = 12/03/13 
 Pct Recovery = 16%  Analysis Date = 12/03/13 
 Pct Recovery = 16%  Analysis Date = 11/30/13 
 Pct Recovery = 17%  Analysis Date = 11/30/13 
 Pct Recovery = 17%  Analysis Date = 11/28/13 
 Pct Recovery = 17%  Analysis Date = 11/28/13 
 Pct Recovery = 17%  Analysis Date = 11/26/13 
 Pct Recovery = 17%  Analysis Date = 11/26/13 
 Pct Recovery = 17%  Analysis Date = 11/23/13 
 Pct Recovery = 17%  Analysis Date = 11/23/13 
 Pct Recovery = 17%  Analysis Date = 11/21/13 
 Pct Recovery = 17%  Analysis Date = 11/21/13 
 Pct Recovery = 17%  Analysis Date = 11/18/13 
 Pct Recovery = 18%  Analysis Date = 11/18/13 
 Pct Recovery = 18%  Analysis Date = 11/16/13 
 Pct Recovery = 18%  Analysis Date = 11/16/13 
 Pct Recovery = 18%  Analysis Date = 11/13/13 
 Pct Recovery = 18%  Analysis Date = 11/13/13 
 Pct Recovery = 18%  Analysis Date = 11/11/13 
 Pct Recovery = 18%  Analysis Date = 11/11/13 
 Pct Recovery = 18%  Analysis Date = 11/09/13 
 Pct Recovery = 19%  Analysis Date = 11/09/13 
 Pct Recovery = 19%  Analysis Date = 11/06/13 
 Pct Recovery = 19%  Analysis Date = 11/06/13 
 Pct Recovery = 19%  Analysis Date = 11/04/13 
 Pct Recovery = 19%  Analysis Date = 11/04/13 
 Pct Recovery = 19%  Analysis Date = 11/01/13 
 Pct Recovery = 19%  Analysis Date = 11/01/13 
 Pct Recovery = 19%  Analysis Date = 10/30/13 
 Pct Recovery = 20%  Analysis Date = 10/30/13 
 Pct Recovery = 20%  Analysis Date = 10/28/13 
 Pct Recovery = 20%  Analysis Date = 10/28/13 
 Pct Recovery = 20%  Analysis Date = 10/25/13 
 Pct Recovery = 19%  Analysis Date = 10/25/13 
 Pct Recovery = 19%  Analysis Date = 10/23/13 
 Pct Recovery = 19%  Analysis Date = 10/23/13 
 Pct Recovery = 19%  Analysis Date = 10/20/13 
 Pct Recovery = 19%  Analysis Date = 10/20/13 
 Pct Recovery = 19%  Analysis Date = 10/18/13 
 Pct Recovery = 19%  Analysis Date = 10/18/13 
 Pct Recovery = 19%  Analysis Date = 10/16/13 
 Pct Recovery = 18%  Analysis Date = 10/16/13 
 Pct Recovery = 18%  Analysis Date = 10/13/13 
 Pct Recovery = 18%  Analysis Date = 10/13/13 
 Pct Recovery = 18%  Analysis Date = 10/11/13 
 Pct Recovery = 18%  Analysis Date = 10/11/13 
 Pct Recovery = 18%  Analysis Date = 10/08/13 
 Pct Recovery = 18%  Analysis Date = 10/08/13 
 Pct Recovery = 18%  Analysis Date = 10/06/13 
 Pct Recovery = 17%  Analysis Date = 10/06/13 
 Pct Recovery = 17%  Analysis Date = 10/04/13 
 Pct Recovery = 17%  Analysis Date = 10/04/13 
 Pct Recovery = 17%  Analysis Date = 10/01/13 
 Pct Recovery = 17%  Analysis Date = 10/01/13 
 Pct Recovery = 17%  Analysis Date = 09/29/13 
 Pct Recovery = 17%  Analysis Date = 09/29/13 
 Pct Recovery = 17%  Analysis Date = 09/26/13 
 Pct Recovery = 16%  Analysis Date = 09/26/13 
 Pct Recovery = 16%  Analysis Date = 09/24/13 
 Pct Recovery = 16%  Analysis Date = 09/24/13 
 Pct Recovery = 16%  Analysis Date = 09/21/13 
 Pct Recovery = 16%  Analysis Date = 09/21/13 
 Pct Recovery = 16%  Analysis Date = 09/19/13 
 Pct Recovery = 16%  Analysis Date = 09/19/13 
 Pct Recovery = 16%  Analysis Date = 09/17/13 
 Pct Recovery = 15%  Analysis Date = 09/17/13 
 Pct Recovery = 15%  Analysis Date = 09/14/13 
 Pct Recovery = 15%  Analysis Date = 09/14/13 
 Pct Recovery = 15%  Analysis Date = 09/12/13 
 Pct Recovery = 15%  Analysis Date = 09/12/13 
 Pct Recovery = 15%  Analysis Date = 09/09/13 
 Pct Recovery = 15%  Analysis Date = 09/09/13 
 Pct Recovery = 15%  Analysis Date = 09/07/13 
 Pct Recovery = 14%  Analysis Date = 09/07/13 
 Pct Recovery = 14%  Analysis Date = 09/05/13 
 Pct Recovery = 14%  Analysis Date = 09/05/13 
 Pct Recovery = 14%  Analysis Date = 09/02/13 
 Pct Recovery = 14%  Analysis Date = 09/02/13 
 Pct Recovery = 14%  Analysis Date = 08/31/13 
 Pct Recovery = 14%  Analysis Date = 08/31/13 
 Pct Recovery = 14%  Analysis Date = 08/28/13 
 Pct Recovery = 13%  Analysis Date = 08/28/13 
 Pct Recovery = 13%  Analysis Date = 08/26/13 
 Pct Recovery = 13%  Analysis Date = 08/26/13 
 Pct Recovery = 13%  Analysis Date = 08/24/13 
 Pct Recovery = 13%  Analysis Date = 08/24/13 
 Pct Recovery = 13%  Analysis Date = 08/21/13 
 Pct Recovery = 13%  Analysis Date = 08/21/13 
 Pct Recovery = 13%  Analysis Date = 08/19/13 
 Pct Recovery = 12%  Analysis Date = 08/19/13 
 Pct Recovery = 12%  Analysis Date = 08/16/13 
 Pct Recovery = 12%  Analysis Date = 08/16/13 
 Pct Recovery = 12%  Analysis Date = 08/14/13 
 Pct Recovery = 12%  Analysis Date = 08/14/13 
 Pct Recovery = 12%  Analysis Date = 08/11/13 
 Pct Recovery = 12%  Analysis Date = 08/11/13 
 Pct Recovery = 12%  Analysis Date = 08/09/13 
 Pct Recovery = 12%  Analysis Date = 08/09/13 
 Pct Recovery = 12%  Analysis Date = 08/07/13 
 Pct Recovery = 12%  Analysis Date = 08/07/13 
 Pct Recovery = 12%  Analysis Date = 08/04/13 
 Pct Recovery = 12%  Analysis Date = 08/04/13 
 Pct Recovery = 12%  Analysis Date = 08/02/13 
 Pct Recovery = 12%  Analysis Date = 08/02/13 
 Pct Recovery = 12%  Analysis Date = 07/30/13 
 Pct Recovery = 12%  Analysis Date = 07/30/13 
 Pct Recovery = 12%  Analysis Date = 07/28/13 
 Pct Recovery = 12%  Analysis Date = 07/28/13 
 Pct Recovery = 12%  Analysis Date = 07/26/13 
 Pct Recovery = 12%  Analysis Date = 07/26/13 
 Pct Recovery = 12%  Analysis Date = 07/23/13 
 Pct Recovery = 12%  Analysis Date = 07/23/13 
 Pct Recovery = 12%  Analysis Date = 07/21/13 
 Pct Recovery = 12%  Analysis Date = 07/21/13 
 Pct Recovery = 12%  Analysis Date = 07/18/13 
 Pct Recovery = 12%  Analysis Date = 07/18/13 
 Pct Recovery = 12%  Analysis Date = 07/16/13 
 Pct Recovery = 12%  Analysis Date = 07/16/13 
 Pct Recovery = 12%  Analysis Date = 07/14/13 
 Pct Recovery = 12%  Analysis Date = 07/14/13 
 Pct Recovery = 12%  Analysis Date = 07/11/13 
 Pct Recovery = 12%  Analysis Date = 07/11/13 
 Pct Recovery = 12%  Analysis Date = 07/09/13 
 Pct Recovery = 12%  Analysis Date = 07/09/13 
 Pct Recovery = 12%  Analysis Date = 07/06/13 
 Pct Recovery = 12%  Analysis Date = 07/06/13 
 Pct Recovery = 12%  Analysis Date = 07/04/13 
 Pct Recovery = 12%  Analysis Date = 07/04/13 
 Pct Recovery = 12%  Analysis Date = 07/02/13 
 Pct Recovery = 12%  Analysis Date = 07/02/13 
 Pct Recovery = 12%  Analysis Date = 06/29/13 
 Pct Recovery = 12%  Analysis Date = 06/29/13 
 Pct Recovery = 12%  Analysis Date = 06/27/13 
 Pct Recovery = 12%  Analysis Date = 06/27/13 
 Pct Recovery = 12%  Analysis Date = 06/24/13 
 Pct Recovery = 12%  Analysis Date = 06/24/13 
 Pct Recovery = 12%  Analysis Date = 06/22/13 
 Pct Recovery = 12%  Analysis Date = 06/22/13 
 Pct Recovery = 12%  Analysis Date = 06/19/13 
 Pct Recovery = 12%  Analysis Date = 06/19/13 
 Pct Recovery = 12%  Analysis Date = 06/17/13 
 Pct Recovery = 12%  Analysis Date = 06/17/13 
 Pct Recovery = 12%  Analysis Date = 06/15/13 
 Pct Recovery = 12%  Analysis Date = 06/15/13 
 Pct Recovery = 12%  Analysis Date = 06/12/13 
 Pct Recovery = 12%  Analysis Date = 06/12/13 
 Pct Recovery = 12%  Analysis Date = 06/10/13 
 Pct Recovery = 12%  Analysis Date = 06/10/13 
 Pct Recovery = 12%  Analysis Date = 06/07/13 
 Pct Recovery = 12%  Analysis Date = 06/07/13 
 Pct Recovery = 12%  Analysis Date = 06/05/13 
 Pct Recovery = 11%  Analysis Date = 06/05/13 
 Pct Recovery = 11%  Analysis Date = 06/03/13 
 Pct Recovery = 11%  Analysis Date = 06/03/13 
 Pct Recovery = 11%  Analysis Date = 05/31/13 
 Pct Recovery = 11%  Analysis Date = 05/31/13 
 Pct Recovery = 11%  Analysis Date = 05/29/13 
 Pct Recovery = 11%  Analysis Date = 05/29/13 
 Pct Recovery = 11%  Analysis Date = 05/26/13 
 Pct Recovery = 11%  Analysis Date = 05/26/13 
 Pct Recovery = 11%  Analysis Date = 05/24/13 
 Pct Recovery = 11%  Analysis Date = 05/24/13 
 Pct Recovery = 11%  Analysis Date = 05/22/13 
 Pct Recovery = 11%  Analysis Date = 05/22/13 
 Pct Recovery = 11%  Analysis Date = 05/19/13 
 Pct Recovery = 11%  Analysis Date = 05/19/13 
 Pct Recovery = 11%  Analysis Date = 05/17/13 
 Pct Recovery = 11%  Analysis Date = 05/17/13 
 Pct Recovery = 11%  Analysis Date = 05/14/13 
 Pct Recovery = 11%  Analysis Date = 05/14/13 
 Pct Recovery = 11%  Analysis Date = 05/12/13 
 Pct Recovery = 11%  Analysis Date = 05/12/13 
 Pct Recovery = 11%  Analysis Date = 05/10/13 
 Pct Recovery = 11%  Analysis Date = 05/10/13 
 Pct Recovery = 11%  Analysis Date = 05/07/13 
 Pct Recovery = 11%  Analysis Date = 05/07/13 
 Pct Recovery = 11%  Analysis Date = 05/05/13 
 Pct Recovery = 11%  Analysis Date = 05/05/13 
 Pct Recovery = 11%  Analysis Date = 05/02/13 
 Pct Recovery = 11%  Analysis Date = 05/02/13 
 Pct Recovery = 11%  Analysis Date = 04/30/13 
 Pct Recovery = 12%  Analysis Date = 04/30/13 
 Pct Recovery = 12%  Analysis Date = 04/27/13 
 Pct Recovery = 12%  Analysis Date = 04/27/13 
 Pct Recovery = 12%  Analysis Date = 04/25/13 
 Pct Recovery = 13%  Analysis Date = 04/25/13 
 Pct Recovery = 13%  Analysis Date = 04/23/13 
 Pct Recovery = 14%  Analysis Date = 04/23/13 
 Pct Recovery = 14%  Analysis Date = 04/20/13 
 Pct Recovery = 14%  Analysis Date = 04/20/13 
 Pct Recovery = 14%  Analysis Date = 04/18/13 
 Pct Recovery = 15%  Analysis Date = 04/18/13 
 Pct Recovery = 15%  Analysis Date = 04/15/13 
 Pct Recovery = 16%  Analysis Date = 04/15/13 
 Pct Recovery = 16%  Analysis Date = 04/13/13 
 Pct Recovery = 16%  Analysis Date = 04/13/13 
 Pct Recovery = 16%  Analysis Date = 04/11/13 
 Pct Recovery = 17%  Analysis Date = 04/11/13 
 Pct Recovery = 17%  Analysis Date = 04/08/13 
 Pct Recovery = 18%  Analysis Date = 04/08/13 
 Pct Recovery = 18%  Analysis Date = 04/06/13 
 Pct Recovery = 18%  Analysis Date = 04/06/13 
 Pct Recovery = 18%  Analysis Date = 04/03/13 
 Pct Recovery = 19%  Analysis Date = 04/03/13 
 Pct Recovery = 19%  Analysis Date = 04/01/13 
 Pct Recovery = 20%  Analysis Date = 04/01/13 
 Pct Recovery = 20%  Analysis Date = 03/30/13 
 Pct Recovery = 20%  Analysis Date = 03/30/13 
 Pct Recovery = 20%  Analysis Date = 03/27/13 
 Pct Recovery = 21%  Analysis Date = 03/27/13 
 Pct Recovery = 21%  Analysis Date = 03/25/13 
 Pct Recovery = 22%  Analysis Date = 03/25/13 
 Pct Recovery = 22%  Analysis Date = 03/22/13 
 Pct Recovery = 22%  Analysis Date = 03/22/13 
 Pct Recovery = 22%  Analysis Date = 03/20/13 
 Pct Recovery = 23%  Analysis Date = 03/20/13 
 Pct Recovery = 23%  Analysis Date = 03/17/13 
 Pct Recovery = 23%  Analysis Date = 03/17/13 
 Pct Recovery = 23%  Analysis Date = 03/15/13 
 Pct Recovery = 24%  Analysis Date = 03/15/13 
 Pct Recovery = 24%  Analysis Date = 03/13/13 
 Pct Recovery = 25%  Analysis Date = 03/13/13 
 Pct Recovery = 25%  Analysis Date = 03/10/13 
 Pct Recovery = 25%  Analysis Date = 03/10/13 
 Pct Recovery = 25%  Analysis Date = 03/08/13 
 Pct Recovery = 26%  Analysis Date = 03/08/13 
 Pct Recovery = 26%  Analysis Date = 03/05/13 
 Pct Recovery = 27%  Analysis Date = 03/05/13 
 Pct Recovery = 27%  Analysis Date = 03/03/13 
 Pct Recovery = 27%  Analysis Date = 03/03/13 
 Pct Recovery = 27%  Analysis Date = 03/01/13 
 Pct Recovery = 28%  Analysis Date = 03/01/13 
 Pct Recovery = 28%  Analysis Date = 02/26/13 
 Pct Recovery = 28%  Analysis Date = 02/26/13 
 Pct Recovery = 28%  Analysis Date = 02/24/13 
 Pct Recovery = 29%  Analysis Date = 02/24/13 
 Pct Recovery = 29%  Analysis Date = 02/21/13 
 Pct Recovery = 30%  Analysis Date = 02/21/13 
 Pct Recovery = 30%  Analysis Date = 02/19/13 
 Pct Recovery = 30%  Analysis Date = 02/19/13 
 Pct Recovery = 30%  Analysis Date = 02/17/13 
 Pct Recovery = 31%  Analysis Date = 02/17/13 
 Pct Recovery = 31%  Analysis Date = 02/14/13 
 Pct Recovery = 31%  Analysis Date = 02/14/13 
 Pct Recovery = 31%  Analysis Date = 02/12/13 
 Pct Recovery = 32%  Analysis Date = 02/12/13 
 Pct Recovery = 32%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/07/13 
 Pct Recovery = 33%  Analysis Date = 02/07/13 
 Pct Recovery = 33%  Analysis Date = 02/05/13 
 Pct Recovery = 34%  Analysis Date = 02/05/13 
 Pct Recovery = 34%  Analysis Date = 02/02/13 
 Pct Recovery = 35%  Analysis Date = 02/02/13 
 Pct Recovery = 35%  Analysis Date = 01/31/13 
 Pct Recovery = 35%  Analysis Date = 01/31/13 
 Pct Recovery = 35%  Analysis Date = 01/28/13 
 Pct Recovery = 36%  Analysis Date = 01/28/13 
 Pct Recovery = 36%  Analysis Date = 01/26/13 
 Pct Recovery = 36%  Analysis Date = 01/26/13 
 Pct Recovery = 36%  Analysis Date = 01/23/13 
 Pct Recovery = 37%  Analysis Date = 01/23/13 
 Pct Recovery = 37%  Analysis Date = 01/21/13 
 Pct Recovery = 37%  Analysis Date = 01/21/13 
 Pct Recovery = 37%  Analysis Date = 01/19/13 
 Pct Recovery = 37%  Analysis Date = 01/19/13 
 Pct Recovery = 37%  Analysis Date = 01/16/13 
 Pct Recovery = 37%  Analysis Date = 01/16/13 
 Pct Recovery = 37%  Analysis Date = 01/14/13 
 Pct Recovery = 37%  Analysis Date = 01/14/13 
 Pct Recovery = 37%  Analysis Date = 01/11/13 
 Pct Recovery = 37%  Analysis Date = 01/11/13 
 Pct Recovery = 37%  Analysis Date = 01/09/13 
 Pct Recovery = 37%  Analysis Date = 01/09/13 
 Pct Recovery = 37%  Analysis Date = 01/07/13 
 Pct Recovery = 37%  Analysis Date = 01/07/13 
 Pct Recovery = 37%  Analysis Date = 01/04/13 
 Pct Recovery = 37%  Analysis Date = 01/04/13 
 Pct Recovery = 37%  Analysis Date = 01/02/13 
 Pct Recovery = 37%  Analysis Date = 01/02/13 
 Pct Recovery = 37%  Analysis Date = 12/30/12 
 Pct Recovery = 37%  Analysis Date = 12/30/12 
 Pct Recovery = 37%  Analysis Date = 12/28/12 
 Pct Recovery = 37%  Analysis Date = 12/28/12 
 Pct Recovery = 37%  Analysis Date = 12/26/12 
 Pct Recovery = 37%  Analysis Date = 12/26/12 
 Pct Recovery = 37%  Analysis Date = 12/23/12 
 Pct Recovery = 37%  Analysis Date = 12/23/12 
 Pct Recovery = 37%  Analysis Date = 12/21/12 
 Pct Recovery = 37%  Analysis Date = 12/21/12 
 Pct Recovery = 37%  Analysis Date = 12/18/12 
 Pct Recovery = 38%  Analysis Date = 12/18/12 
 Pct Recovery = 38%  Analysis Date = 12/16/12 
 Pct Recovery = 38%  Analysis Date = 12/16/12 
 Pct Recovery = 38%  Analysis Date = 12/14/12 
 Pct Recovery = 38%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
ORLISTAT

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 21% 15% 17% 15%
Total 11 21% 15% 17% 15%

Sample Statistics
ORLISTAT

Characteristic N % % Basis
Plotted 11 92% Spiked
Estimated Values 11 92% Spiked
Deleted Values 4 13% Spiked + Not Spiked
Spiked, Censored 1 8% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 12
Not Spiked 18 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
OSELTAMIVIR
METHOD: LC9017 , TESTIDCODE: 67511LCM56

The SGPlot Procedure

Sample Statistics
OSELTAMIVIR

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
OXAZEPAM
METHOD: LC9017 , TESTIDCODE: 67469LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 6%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 16%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 8%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 8%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 71%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 57%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 8%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 8%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 7%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 97%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 67%  Analysis Date = 04/10/14 
 Pct Recovery = 62%  Analysis Date = 04/07/14 
 Pct Recovery = 63%  Analysis Date = 04/07/14 
 Pct Recovery = 63%  Analysis Date = 04/05/14 
 Pct Recovery = 63%  Analysis Date = 04/05/14 
 Pct Recovery = 63%  Analysis Date = 04/03/14 
 Pct Recovery = 63%  Analysis Date = 04/03/14 
 Pct Recovery = 63%  Analysis Date = 04/01/14 
 Pct Recovery = 63%  Analysis Date = 04/01/14 
 Pct Recovery = 63%  Analysis Date = 03/29/14 
 Pct Recovery = 63%  Analysis Date = 03/29/14 
 Pct Recovery = 63%  Analysis Date = 03/27/14 
 Pct Recovery = 64%  Analysis Date = 03/27/14 
 Pct Recovery = 64%  Analysis Date = 03/25/14 
 Pct Recovery = 64%  Analysis Date = 03/25/14 
 Pct Recovery = 64%  Analysis Date = 03/23/14 
 Pct Recovery = 64%  Analysis Date = 03/23/14 
 Pct Recovery = 64%  Analysis Date = 03/21/14 
 Pct Recovery = 64%  Analysis Date = 03/21/14 
 Pct Recovery = 64%  Analysis Date = 03/18/14 
 Pct Recovery = 64%  Analysis Date = 03/18/14 
 Pct Recovery = 64%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/12/14 
 Pct Recovery = 65%  Analysis Date = 03/12/14 
 Pct Recovery = 65%  Analysis Date = 03/10/14 
 Pct Recovery = 65%  Analysis Date = 03/10/14 
 Pct Recovery = 65%  Analysis Date = 03/07/14 
 Pct Recovery = 65%  Analysis Date = 03/07/14 
 Pct Recovery = 65%  Analysis Date = 03/05/14 
 Pct Recovery = 65%  Analysis Date = 03/05/14 
 Pct Recovery = 65%  Analysis Date = 03/03/14 
 Pct Recovery = 66%  Analysis Date = 03/03/14 
 Pct Recovery = 66%  Analysis Date = 03/01/14 
 Pct Recovery = 66%  Analysis Date = 03/01/14 
 Pct Recovery = 66%  Analysis Date = 02/27/14 
 Pct Recovery = 66%  Analysis Date = 02/27/14 
 Pct Recovery = 66%  Analysis Date = 02/24/14 
 Pct Recovery = 66%  Analysis Date = 02/24/14 
 Pct Recovery = 66%  Analysis Date = 02/22/14 
 Pct Recovery = 66%  Analysis Date = 02/22/14 
 Pct Recovery = 66%  Analysis Date = 02/20/14 
 Pct Recovery = 67%  Analysis Date = 02/20/14 
 Pct Recovery = 67%  Analysis Date = 02/18/14 
 Pct Recovery = 67%  Analysis Date = 02/18/14 
 Pct Recovery = 67%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/16/14 
 Pct Recovery = 67%  Analysis Date = 02/13/14 
 Pct Recovery = 67%  Analysis Date = 02/13/14 
 Pct Recovery = 67%  Analysis Date = 02/11/14 
 Pct Recovery = 67%  Analysis Date = 02/11/14 
 Pct Recovery = 67%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/09/14 
 Pct Recovery = 68%  Analysis Date = 02/07/14 
 Pct Recovery = 68%  Analysis Date = 02/07/14 
 Pct Recovery = 68%  Analysis Date = 02/05/14 
 Pct Recovery = 68%  Analysis Date = 02/05/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 02/02/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/31/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/29/14 
 Pct Recovery = 68%  Analysis Date = 01/27/14 
 Pct Recovery = 69%  Analysis Date = 01/27/14 
 Pct Recovery = 69%  Analysis Date = 01/25/14 
 Pct Recovery = 69%  Analysis Date = 01/25/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/22/14 
 Pct Recovery = 69%  Analysis Date = 01/20/14 
 Pct Recovery = 69%  Analysis Date = 01/20/14 
 Pct Recovery = 69%  Analysis Date = 01/18/14 
 Pct Recovery = 69%  Analysis Date = 01/18/14 
 Pct Recovery = 69%  Analysis Date = 01/16/14 
 Pct Recovery = 70%  Analysis Date = 01/16/14 
 Pct Recovery = 70%  Analysis Date = 01/14/14 
 Pct Recovery = 70%  Analysis Date = 01/14/14 
 Pct Recovery = 70%  Analysis Date = 01/11/14 
 Pct Recovery = 70%  Analysis Date = 01/11/14 
 Pct Recovery = 70%  Analysis Date = 01/09/14 
 Pct Recovery = 70%  Analysis Date = 01/09/14 
 Pct Recovery = 70%  Analysis Date = 01/07/14 
 Pct Recovery = 70%  Analysis Date = 01/07/14 
 Pct Recovery = 70%  Analysis Date = 01/05/14 
 Pct Recovery = 70%  Analysis Date = 01/05/14 
 Pct Recovery = 70%  Analysis Date = 01/02/14 
 Pct Recovery = 70%  Analysis Date = 01/02/14 
 Pct Recovery = 70%  Analysis Date = 12/31/13 
 Pct Recovery = 71%  Analysis Date = 12/31/13 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/29/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/27/13 
 Pct Recovery = 71%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/25/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/22/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/20/13 
 Pct Recovery = 71%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/18/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/16/13 
 Pct Recovery = 72%  Analysis Date = 12/14/13 
 Pct Recovery = 72%  Analysis Date = 12/14/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/11/13 
 Pct Recovery = 72%  Analysis Date = 12/09/13 
 Pct Recovery = 72%  Analysis Date = 12/09/13 
 Pct Recovery = 72%  Analysis Date = 12/07/13 
 Pct Recovery = 72%  Analysis Date = 12/07/13 
 Pct Recovery = 72%  Analysis Date = 12/05/13 
 Pct Recovery = 72%  Analysis Date = 12/05/13 
 Pct Recovery = 72%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/28/13 
 Pct Recovery = 73%  Analysis Date = 11/28/13 
 Pct Recovery = 73%  Analysis Date = 11/26/13 
 Pct Recovery = 73%  Analysis Date = 11/26/13 
 Pct Recovery = 73%  Analysis Date = 11/24/13 
 Pct Recovery = 73%  Analysis Date = 11/24/13 
 Pct Recovery = 73%  Analysis Date = 11/22/13 
 Pct Recovery = 73%  Analysis Date = 11/22/13 
 Pct Recovery = 73%  Analysis Date = 11/19/13 
 Pct Recovery = 73%  Analysis Date = 11/19/13 
 Pct Recovery = 73%  Analysis Date = 11/17/13 
 Pct Recovery = 74%  Analysis Date = 11/17/13 
 Pct Recovery = 74%  Analysis Date = 11/15/13 
 Pct Recovery = 74%  Analysis Date = 11/15/13 
 Pct Recovery = 74%  Analysis Date = 11/13/13 
 Pct Recovery = 74%  Analysis Date = 11/13/13 
 Pct Recovery = 74%  Analysis Date = 11/11/13 
 Pct Recovery = 74%  Analysis Date = 11/11/13 
 Pct Recovery = 74%  Analysis Date = 11/08/13 
 Pct Recovery = 74%  Analysis Date = 11/08/13 
 Pct Recovery = 74%  Analysis Date = 11/06/13 
 Pct Recovery = 74%  Analysis Date = 11/06/13 
 Pct Recovery = 74%  Analysis Date = 11/04/13 
 Pct Recovery = 74%  Analysis Date = 11/04/13 
 Pct Recovery = 74%  Analysis Date = 11/02/13 
 Pct Recovery = 75%  Analysis Date = 11/02/13 
 Pct Recovery = 75%  Analysis Date = 10/31/13 
 Pct Recovery = 75%  Analysis Date = 10/31/13 
 Pct Recovery = 75%  Analysis Date = 10/28/13 
 Pct Recovery = 75%  Analysis Date = 10/28/13 
 Pct Recovery = 75%  Analysis Date = 10/26/13 
 Pct Recovery = 74%  Analysis Date = 10/26/13 
 Pct Recovery = 74%  Analysis Date = 10/24/13 
 Pct Recovery = 74%  Analysis Date = 10/24/13 
 Pct Recovery = 74%  Analysis Date = 10/22/13 
 Pct Recovery = 74%  Analysis Date = 10/22/13 
 Pct Recovery = 74%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/17/13 
 Pct Recovery = 73%  Analysis Date = 10/17/13 
 Pct Recovery = 73%  Analysis Date = 10/15/13 
 Pct Recovery = 73%  Analysis Date = 10/15/13 
 Pct Recovery = 73%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 71%  Analysis Date = 10/06/13 
 Pct Recovery = 71%  Analysis Date = 10/04/13 
 Pct Recovery = 71%  Analysis Date = 10/04/13 
 Pct Recovery = 71%  Analysis Date = 10/02/13 
 Pct Recovery = 71%  Analysis Date = 10/02/13 
 Pct Recovery = 71%  Analysis Date = 09/30/13 
 Pct Recovery = 70%  Analysis Date = 09/30/13 
 Pct Recovery = 70%  Analysis Date = 09/27/13 
 Pct Recovery = 70%  Analysis Date = 09/27/13 
 Pct Recovery = 70%  Analysis Date = 09/25/13 
 Pct Recovery = 70%  Analysis Date = 09/25/13 
 Pct Recovery = 70%  Analysis Date = 09/23/13 
 Pct Recovery = 69%  Analysis Date = 09/23/13 
 Pct Recovery = 69%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/21/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/19/13 
 Pct Recovery = 69%  Analysis Date = 09/16/13 
 Pct Recovery = 68%  Analysis Date = 09/16/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/03/13 
 Pct Recovery = 66%  Analysis Date = 09/03/13 
 Pct Recovery = 66%  Analysis Date = 09/01/13 
 Pct Recovery = 66%  Analysis Date = 09/01/13 
 Pct Recovery = 66%  Analysis Date = 08/30/13 
 Pct Recovery = 66%  Analysis Date = 08/30/13 
 Pct Recovery = 66%  Analysis Date = 08/28/13 
 Pct Recovery = 65%  Analysis Date = 08/28/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/25/13 
 Pct Recovery = 65%  Analysis Date = 08/23/13 
 Pct Recovery = 65%  Analysis Date = 08/23/13 
 Pct Recovery = 65%  Analysis Date = 08/21/13 
 Pct Recovery = 64%  Analysis Date = 08/21/13 
 Pct Recovery = 64%  Analysis Date = 08/19/13 
 Pct Recovery = 64%  Analysis Date = 08/19/13 
 Pct Recovery = 64%  Analysis Date = 08/17/13 
 Pct Recovery = 63%  Analysis Date = 08/17/13 
 Pct Recovery = 63%  Analysis Date = 08/14/13 
 Pct Recovery = 62%  Analysis Date = 08/14/13 
 Pct Recovery = 62%  Analysis Date = 08/12/13 
 Pct Recovery = 61%  Analysis Date = 08/12/13 
 Pct Recovery = 61%  Analysis Date = 08/10/13 
 Pct Recovery = 60%  Analysis Date = 08/10/13 
 Pct Recovery = 60%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/08/13 
 Pct Recovery = 59%  Analysis Date = 08/06/13 
 Pct Recovery = 57%  Analysis Date = 08/06/13 
 Pct Recovery = 57%  Analysis Date = 08/03/13 
 Pct Recovery = 56%  Analysis Date = 08/03/13 
 Pct Recovery = 56%  Analysis Date = 08/01/13 
 Pct Recovery = 55%  Analysis Date = 08/01/13 
 Pct Recovery = 55%  Analysis Date = 07/30/13 
 Pct Recovery = 54%  Analysis Date = 07/30/13 
 Pct Recovery = 54%  Analysis Date = 07/28/13 
 Pct Recovery = 53%  Analysis Date = 07/28/13 
 Pct Recovery = 53%  Analysis Date = 07/26/13 
 Pct Recovery = 52%  Analysis Date = 07/26/13 
 Pct Recovery = 52%  Analysis Date = 07/23/13 
 Pct Recovery = 51%  Analysis Date = 07/23/13 
 Pct Recovery = 51%  Analysis Date = 07/21/13 
 Pct Recovery = 49%  Analysis Date = 07/21/13 
 Pct Recovery = 49%  Analysis Date = 07/19/13 
 Pct Recovery = 48%  Analysis Date = 07/19/13 
 Pct Recovery = 48%  Analysis Date = 07/17/13 
 Pct Recovery = 47%  Analysis Date = 07/17/13 
 Pct Recovery = 47%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/12/13 
 Pct Recovery = 45%  Analysis Date = 07/12/13 
 Pct Recovery = 45%  Analysis Date = 07/10/13 
 Pct Recovery = 44%  Analysis Date = 07/10/13 
 Pct Recovery = 44%  Analysis Date = 07/08/13 
 Pct Recovery = 43%  Analysis Date = 07/08/13 
 Pct Recovery = 43%  Analysis Date = 07/06/13 
 Pct Recovery = 41%  Analysis Date = 07/06/13 
 Pct Recovery = 41%  Analysis Date = 07/03/13 
 Pct Recovery = 40%  Analysis Date = 07/03/13 
 Pct Recovery = 40%  Analysis Date = 07/01/13 
 Pct Recovery = 39%  Analysis Date = 07/01/13 
 Pct Recovery = 39%  Analysis Date = 06/29/13 
 Pct Recovery = 38%  Analysis Date = 06/29/13 
 Pct Recovery = 38%  Analysis Date = 06/27/13 
 Pct Recovery = 37%  Analysis Date = 06/27/13 
 Pct Recovery = 37%  Analysis Date = 06/25/13 
 Pct Recovery = 36%  Analysis Date = 06/25/13 
 Pct Recovery = 36%  Analysis Date = 06/22/13 
 Pct Recovery = 34%  Analysis Date = 06/22/13 
 Pct Recovery = 34%  Analysis Date = 06/20/13 
 Pct Recovery = 33%  Analysis Date = 06/20/13 
 Pct Recovery = 33%  Analysis Date = 06/18/13 
 Pct Recovery = 32%  Analysis Date = 06/18/13 
 Pct Recovery = 32%  Analysis Date = 06/16/13 
 Pct Recovery = 31%  Analysis Date = 06/16/13 
 Pct Recovery = 31%  Analysis Date = 06/14/13 
 Pct Recovery = 30%  Analysis Date = 06/14/13 
 Pct Recovery = 30%  Analysis Date = 06/11/13 
 Pct Recovery = 29%  Analysis Date = 06/11/13 
 Pct Recovery = 29%  Analysis Date = 06/09/13 
 Pct Recovery = 28%  Analysis Date = 06/09/13 
 Pct Recovery = 28%  Analysis Date = 06/07/13 
 Pct Recovery = 26%  Analysis Date = 06/07/13 
 Pct Recovery = 26%  Analysis Date = 06/05/13 
 Pct Recovery = 25%  Analysis Date = 06/05/13 
 Pct Recovery = 25%  Analysis Date = 06/03/13 
 Pct Recovery = 24%  Analysis Date = 06/03/13 
 Pct Recovery = 24%  Analysis Date = 05/31/13 
 Pct Recovery = 23%  Analysis Date = 05/31/13 
 Pct Recovery = 23%  Analysis Date = 05/29/13 
 Pct Recovery = 22%  Analysis Date = 05/29/13 
 Pct Recovery = 22%  Analysis Date = 05/27/13 
 Pct Recovery = 21%  Analysis Date = 05/27/13 
 Pct Recovery = 21%  Analysis Date = 05/25/13 
 Pct Recovery = 19%  Analysis Date = 05/25/13 
 Pct Recovery = 19%  Analysis Date = 05/23/13 
 Pct Recovery = 18%  Analysis Date = 05/23/13 
 Pct Recovery = 18%  Analysis Date = 05/20/13 
 Pct Recovery = 17%  Analysis Date = 05/20/13 
 Pct Recovery = 17%  Analysis Date = 05/18/13 
 Pct Recovery = 16%  Analysis Date = 05/18/13 
 Pct Recovery = 16%  Analysis Date = 05/16/13 
 Pct Recovery = 15%  Analysis Date = 05/16/13 
 Pct Recovery = 15%  Analysis Date = 05/14/13 
 Pct Recovery = 14%  Analysis Date = 05/14/13 
 Pct Recovery = 14%  Analysis Date = 05/12/13 
 Pct Recovery = 13%  Analysis Date = 05/12/13 
 Pct Recovery = 13%  Analysis Date = 05/09/13 
 Pct Recovery = 11%  Analysis Date = 05/09/13 
 Pct Recovery = 11%  Analysis Date = 05/07/13 
 Pct Recovery = 10%  Analysis Date = 05/07/13 
 Pct Recovery = 10%  Analysis Date = 05/05/13 
 Pct Recovery = 9%  Analysis Date = 05/05/13 
 Pct Recovery = 9%  Analysis Date = 05/03/13 
 Pct Recovery = 8%  Analysis Date = 05/03/13 
 Pct Recovery = 8%  Analysis Date = 05/01/13 
 Pct Recovery = 7%  Analysis Date = 05/01/13 
 Pct Recovery = 7%  Analysis Date = 04/28/13 
 Pct Recovery = 7%  Analysis Date = 04/28/13 
 Pct Recovery = 7%  Analysis Date = 04/26/13 
 Pct Recovery = 7%  Analysis Date = 04/26/13 
 Pct Recovery = 7%  Analysis Date = 04/24/13 
 Pct Recovery = 7%  Analysis Date = 04/24/13 
 Pct Recovery = 7%  Analysis Date = 04/22/13 
 Pct Recovery = 7%  Analysis Date = 04/22/13 
 Pct Recovery = 7%  Analysis Date = 04/19/13 
 Pct Recovery = 7%  Analysis Date = 04/19/13 
 Pct Recovery = 7%  Analysis Date = 04/17/13 
 Pct Recovery = 7%  Analysis Date = 04/17/13 
 Pct Recovery = 7%  Analysis Date = 04/15/13 
 Pct Recovery = 7%  Analysis Date = 04/15/13 
 Pct Recovery = 7%  Analysis Date = 04/13/13 
 Pct Recovery = 7%  Analysis Date = 04/13/13 
 Pct Recovery = 7%  Analysis Date = 04/11/13 
 Pct Recovery = 7%  Analysis Date = 04/11/13 
 Pct Recovery = 7%  Analysis Date = 04/08/13 
 Pct Recovery = 7%  Analysis Date = 04/08/13 
 Pct Recovery = 7%  Analysis Date = 04/06/13 
 Pct Recovery = 7%  Analysis Date = 04/06/13 
 Pct Recovery = 7%  Analysis Date = 04/04/13 
 Pct Recovery = 7%  Analysis Date = 04/04/13 
 Pct Recovery = 7%  Analysis Date = 04/02/13 
 Pct Recovery = 7%  Analysis Date = 04/02/13 
 Pct Recovery = 7%  Analysis Date = 03/31/13 
 Pct Recovery = 7%  Analysis Date = 03/31/13 
 Pct Recovery = 7%  Analysis Date = 03/28/13 
 Pct Recovery = 7%  Analysis Date = 03/28/13 
 Pct Recovery = 7%  Analysis Date = 03/26/13 
 Pct Recovery = 7%  Analysis Date = 03/26/13 
 Pct Recovery = 7%  Analysis Date = 03/24/13 
 Pct Recovery = 8%  Analysis Date = 03/24/13 
 Pct Recovery = 8%  Analysis Date = 03/22/13 
 Pct Recovery = 8%  Analysis Date = 03/22/13 
 Pct Recovery = 8%  Analysis Date = 03/20/13 
 Pct Recovery = 8%  Analysis Date = 03/20/13 
 Pct Recovery = 8%  Analysis Date = 03/17/13 
 Pct Recovery = 8%  Analysis Date = 03/17/13 
 Pct Recovery = 8%  Analysis Date = 03/15/13 
 Pct Recovery = 8%  Analysis Date = 03/15/13 
 Pct Recovery = 8%  Analysis Date = 03/13/13 
 Pct Recovery = 8%  Analysis Date = 03/13/13 
 Pct Recovery = 8%  Analysis Date = 03/11/13 
 Pct Recovery = 9%  Analysis Date = 03/11/13 
 Pct Recovery = 9%  Analysis Date = 03/09/13 
 Pct Recovery = 9%  Analysis Date = 03/09/13 
 Pct Recovery = 9%  Analysis Date = 03/06/13 
 Pct Recovery = 9%  Analysis Date = 03/06/13 
 Pct Recovery = 9%  Analysis Date = 03/04/13 
 Pct Recovery = 9%  Analysis Date = 03/04/13 
 Pct Recovery = 9%  Analysis Date = 03/02/13 
 Pct Recovery = 9%  Analysis Date = 03/02/13 
 Pct Recovery = 9%  Analysis Date = 02/28/13 
 Pct Recovery = 9%  Analysis Date = 02/28/13 
 Pct Recovery = 9%  Analysis Date = 02/26/13 
 Pct Recovery = 10%  Analysis Date = 02/26/13 
 Pct Recovery = 10%  Analysis Date = 02/23/13 
 Pct Recovery = 10%  Analysis Date = 02/23/13 
 Pct Recovery = 10%  Analysis Date = 02/21/13 
 Pct Recovery = 10%  Analysis Date = 02/21/13 
 Pct Recovery = 10%  Analysis Date = 02/19/13 
 Pct Recovery = 10%  Analysis Date = 02/19/13 
 Pct Recovery = 10%  Analysis Date = 02/17/13 
 Pct Recovery = 10%  Analysis Date = 02/17/13 
 Pct Recovery = 10%  Analysis Date = 02/15/13 
 Pct Recovery = 10%  Analysis Date = 02/15/13 
 Pct Recovery = 10%  Analysis Date = 02/12/13 
 Pct Recovery = 11%  Analysis Date = 02/12/13 
 Pct Recovery = 11%  Analysis Date = 02/10/13 
 Pct Recovery = 11%  Analysis Date = 02/10/13 
 Pct Recovery = 11%  Analysis Date = 02/08/13 
 Pct Recovery = 11%  Analysis Date = 02/08/13 
 Pct Recovery = 11%  Analysis Date = 02/06/13 
 Pct Recovery = 11%  Analysis Date = 02/06/13 
 Pct Recovery = 11%  Analysis Date = 02/04/13 
 Pct Recovery = 11%  Analysis Date = 02/04/13 
 Pct Recovery = 11%  Analysis Date = 02/01/13 
 Pct Recovery = 11%  Analysis Date = 02/01/13 
 Pct Recovery = 11%  Analysis Date = 01/30/13 
 Pct Recovery = 11%  Analysis Date = 01/30/13 
 Pct Recovery = 11%  Analysis Date = 01/28/13 
 Pct Recovery = 12%  Analysis Date = 01/28/13 
 Pct Recovery = 12%  Analysis Date = 01/26/13 
 Pct Recovery = 12%  Analysis Date = 01/26/13 
 Pct Recovery = 12%  Analysis Date = 01/24/13 
 Pct Recovery = 12%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 37% 33% 16% 43%
Total 13 37% 33% 16% 43%

Sample Statistics
OXAZEPAM

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 5 36% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 1 7% 1 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
OXYCODONE
METHOD: LC9017 , TESTIDCODE: 67495LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 80%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 47%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 67%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 71%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 04/10/14 
 Pct Recovery = 51%  Analysis Date = 04/07/14 
 Pct Recovery = 51%  Analysis Date = 04/07/14 
 Pct Recovery = 51%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/05/14 
 Pct Recovery = 51%  Analysis Date = 04/03/14 
 Pct Recovery = 51%  Analysis Date = 04/03/14 
 Pct Recovery = 51%  Analysis Date = 04/01/14 
 Pct Recovery = 52%  Analysis Date = 04/01/14 
 Pct Recovery = 52%  Analysis Date = 03/29/14 
 Pct Recovery = 52%  Analysis Date = 03/29/14 
 Pct Recovery = 52%  Analysis Date = 03/27/14 
 Pct Recovery = 52%  Analysis Date = 03/27/14 
 Pct Recovery = 52%  Analysis Date = 03/25/14 
 Pct Recovery = 53%  Analysis Date = 03/25/14 
 Pct Recovery = 53%  Analysis Date = 03/23/14 
 Pct Recovery = 53%  Analysis Date = 03/23/14 
 Pct Recovery = 53%  Analysis Date = 03/21/14 
 Pct Recovery = 53%  Analysis Date = 03/21/14 
 Pct Recovery = 53%  Analysis Date = 03/18/14 
 Pct Recovery = 54%  Analysis Date = 03/18/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/14/14 
 Pct Recovery = 54%  Analysis Date = 03/14/14 
 Pct Recovery = 54%  Analysis Date = 03/12/14 
 Pct Recovery = 54%  Analysis Date = 03/12/14 
 Pct Recovery = 54%  Analysis Date = 03/10/14 
 Pct Recovery = 55%  Analysis Date = 03/10/14 
 Pct Recovery = 55%  Analysis Date = 03/07/14 
 Pct Recovery = 55%  Analysis Date = 03/07/14 
 Pct Recovery = 55%  Analysis Date = 03/05/14 
 Pct Recovery = 55%  Analysis Date = 03/05/14 
 Pct Recovery = 55%  Analysis Date = 03/03/14 
 Pct Recovery = 56%  Analysis Date = 03/03/14 
 Pct Recovery = 56%  Analysis Date = 03/01/14 
 Pct Recovery = 56%  Analysis Date = 03/01/14 
 Pct Recovery = 56%  Analysis Date = 02/27/14 
 Pct Recovery = 56%  Analysis Date = 02/27/14 
 Pct Recovery = 56%  Analysis Date = 02/24/14 
 Pct Recovery = 57%  Analysis Date = 02/24/14 
 Pct Recovery = 57%  Analysis Date = 02/22/14 
 Pct Recovery = 57%  Analysis Date = 02/22/14 
 Pct Recovery = 57%  Analysis Date = 02/20/14 
 Pct Recovery = 57%  Analysis Date = 02/20/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 58%  Analysis Date = 02/18/14 
 Pct Recovery = 58%  Analysis Date = 02/16/14 
 Pct Recovery = 58%  Analysis Date = 02/16/14 
 Pct Recovery = 58%  Analysis Date = 02/13/14 
 Pct Recovery = 58%  Analysis Date = 02/13/14 
 Pct Recovery = 58%  Analysis Date = 02/11/14 
 Pct Recovery = 58%  Analysis Date = 02/11/14 
 Pct Recovery = 58%  Analysis Date = 02/09/14 
 Pct Recovery = 59%  Analysis Date = 02/09/14 
 Pct Recovery = 59%  Analysis Date = 02/07/14 
 Pct Recovery = 59%  Analysis Date = 02/07/14 
 Pct Recovery = 59%  Analysis Date = 02/05/14 
 Pct Recovery = 59%  Analysis Date = 02/05/14 
 Pct Recovery = 59%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/29/14 
 Pct Recovery = 60%  Analysis Date = 01/29/14 
 Pct Recovery = 60%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/22/14 
 Pct Recovery = 61%  Analysis Date = 01/20/14 
 Pct Recovery = 61%  Analysis Date = 01/20/14 
 Pct Recovery = 61%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/16/14 
 Pct Recovery = 62%  Analysis Date = 01/16/14 
 Pct Recovery = 62%  Analysis Date = 01/14/14 
 Pct Recovery = 62%  Analysis Date = 01/14/14 
 Pct Recovery = 62%  Analysis Date = 01/11/14 
 Pct Recovery = 62%  Analysis Date = 01/11/14 
 Pct Recovery = 62%  Analysis Date = 01/09/14 
 Pct Recovery = 62%  Analysis Date = 01/09/14 
 Pct Recovery = 62%  Analysis Date = 01/07/14 
 Pct Recovery = 63%  Analysis Date = 01/07/14 
 Pct Recovery = 63%  Analysis Date = 01/05/14 
 Pct Recovery = 63%  Analysis Date = 01/05/14 
 Pct Recovery = 63%  Analysis Date = 01/02/14 
 Pct Recovery = 63%  Analysis Date = 01/02/14 
 Pct Recovery = 63%  Analysis Date = 12/31/13 
 Pct Recovery = 63%  Analysis Date = 12/31/13 
 Pct Recovery = 63%  Analysis Date = 12/29/13 
 Pct Recovery = 63%  Analysis Date = 12/29/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/25/13 
 Pct Recovery = 63%  Analysis Date = 12/25/13 
 Pct Recovery = 63%  Analysis Date = 12/22/13 
 Pct Recovery = 63%  Analysis Date = 12/22/13 
 Pct Recovery = 63%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 64%  Analysis Date = 12/18/13 
 Pct Recovery = 64%  Analysis Date = 12/16/13 
 Pct Recovery = 64%  Analysis Date = 12/16/13 
 Pct Recovery = 64%  Analysis Date = 12/14/13 
 Pct Recovery = 64%  Analysis Date = 12/14/13 
 Pct Recovery = 64%  Analysis Date = 12/11/13 
 Pct Recovery = 64%  Analysis Date = 12/11/13 
 Pct Recovery = 64%  Analysis Date = 12/09/13 
 Pct Recovery = 64%  Analysis Date = 12/09/13 
 Pct Recovery = 64%  Analysis Date = 12/07/13 
 Pct Recovery = 64%  Analysis Date = 12/07/13 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 Pct Recovery = 64%  Analysis Date = 12/03/13 
 Pct Recovery = 65%  Analysis Date = 12/03/13 
 Pct Recovery = 65%  Analysis Date = 11/30/13 
 Pct Recovery = 65%  Analysis Date = 11/30/13 
 Pct Recovery = 65%  Analysis Date = 11/28/13 
 Pct Recovery = 65%  Analysis Date = 11/28/13 
 Pct Recovery = 65%  Analysis Date = 11/26/13 
 Pct Recovery = 65%  Analysis Date = 11/26/13 
 Pct Recovery = 65%  Analysis Date = 11/24/13 
 Pct Recovery = 65%  Analysis Date = 11/24/13 
 Pct Recovery = 65%  Analysis Date = 11/22/13 
 Pct Recovery = 65%  Analysis Date = 11/22/13 
 Pct Recovery = 65%  Analysis Date = 11/19/13 
 Pct Recovery = 65%  Analysis Date = 11/19/13 
 Pct Recovery = 65%  Analysis Date = 11/17/13 
 Pct Recovery = 65%  Analysis Date = 11/17/13 
 Pct Recovery = 65%  Analysis Date = 11/15/13 
 Pct Recovery = 66%  Analysis Date = 11/15/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/08/13 
 Pct Recovery = 66%  Analysis Date = 11/08/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/28/13 
 Pct Recovery = 67%  Analysis Date = 10/26/13 
 Pct Recovery = 67%  Analysis Date = 10/26/13 
 Pct Recovery = 67%  Analysis Date = 10/24/13 
 Pct Recovery = 67%  Analysis Date = 10/24/13 
 Pct Recovery = 67%  Analysis Date = 10/22/13 
 Pct Recovery = 67%  Analysis Date = 10/22/13 
 Pct Recovery = 67%  Analysis Date = 10/20/13 
 Pct Recovery = 67%  Analysis Date = 10/20/13 
 Pct Recovery = 67%  Analysis Date = 10/17/13 
 Pct Recovery = 67%  Analysis Date = 10/17/13 
 Pct Recovery = 67%  Analysis Date = 10/15/13 
 Pct Recovery = 67%  Analysis Date = 10/15/13 
 Pct Recovery = 67%  Analysis Date = 10/13/13 
 Pct Recovery = 67%  Analysis Date = 10/13/13 
 Pct Recovery = 67%  Analysis Date = 10/11/13 
 Pct Recovery = 67%  Analysis Date = 10/11/13 
 Pct Recovery = 67%  Analysis Date = 10/08/13 
 Pct Recovery = 67%  Analysis Date = 10/08/13 
 Pct Recovery = 67%  Analysis Date = 10/06/13 
 Pct Recovery = 67%  Analysis Date = 10/06/13 
 Pct Recovery = 67%  Analysis Date = 10/04/13 
 Pct Recovery = 67%  Analysis Date = 10/04/13 
 Pct Recovery = 67%  Analysis Date = 10/02/13 
 Pct Recovery = 67%  Analysis Date = 10/02/13 
 Pct Recovery = 67%  Analysis Date = 09/30/13 
 Pct Recovery = 67%  Analysis Date = 09/30/13 
 Pct Recovery = 67%  Analysis Date = 09/27/13 
 Pct Recovery = 67%  Analysis Date = 09/27/13 
 Pct Recovery = 67%  Analysis Date = 09/25/13 
 Pct Recovery = 67%  Analysis Date = 09/25/13 
 Pct Recovery = 67%  Analysis Date = 09/23/13 
 Pct Recovery = 67%  Analysis Date = 09/23/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/16/13 
 Pct Recovery = 67%  Analysis Date = 09/16/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/10/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/08/13 
 Pct Recovery = 67%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/05/13 
 Pct Recovery = 67%  Analysis Date = 09/03/13 
 Pct Recovery = 67%  Analysis Date = 09/03/13 
 Pct Recovery = 67%  Analysis Date = 09/01/13 
 Pct Recovery = 67%  Analysis Date = 09/01/13 
 Pct Recovery = 67%  Analysis Date = 08/30/13 
 Pct Recovery = 67%  Analysis Date = 08/30/13 
 Pct Recovery = 67%  Analysis Date = 08/28/13 
 Pct Recovery = 67%  Analysis Date = 08/28/13 
 Pct Recovery = 67%  Analysis Date = 08/25/13 
 Pct Recovery = 67%  Analysis Date = 08/25/13 
 Pct Recovery = 67%  Analysis Date = 08/23/13 
 Pct Recovery = 68%  Analysis Date = 08/23/13 
 Pct Recovery = 68%  Analysis Date = 08/21/13 
 Pct Recovery = 68%  Analysis Date = 08/21/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/17/13 
 Pct Recovery = 68%  Analysis Date = 08/17/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/12/13 
 Pct Recovery = 68%  Analysis Date = 08/12/13 
 Pct Recovery = 68%  Analysis Date = 08/10/13 
 Pct Recovery = 68%  Analysis Date = 08/10/13 
 Pct Recovery = 68%  Analysis Date = 08/08/13 
 Pct Recovery = 68%  Analysis Date = 08/08/13 
 Pct Recovery = 68%  Analysis Date = 08/06/13 
 Pct Recovery = 68%  Analysis Date = 08/06/13 
 Pct Recovery = 68%  Analysis Date = 08/03/13 
 Pct Recovery = 68%  Analysis Date = 08/03/13 
 Pct Recovery = 68%  Analysis Date = 08/01/13 
 Pct Recovery = 68%  Analysis Date = 08/01/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/30/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/28/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/26/13 
 Pct Recovery = 68%  Analysis Date = 07/23/13 
 Pct Recovery = 69%  Analysis Date = 07/23/13 
 Pct Recovery = 69%  Analysis Date = 07/21/13 
 Pct Recovery = 69%  Analysis Date = 07/21/13 
 Pct Recovery = 69%  Analysis Date = 07/19/13 
 Pct Recovery = 69%  Analysis Date = 07/19/13 
 Pct Recovery = 69%  Analysis Date = 07/17/13 
 Pct Recovery = 69%  Analysis Date = 07/17/13 
 Pct Recovery = 69%  Analysis Date = 07/14/13 
 Pct Recovery = 69%  Analysis Date = 07/14/13 
 Pct Recovery = 69%  Analysis Date = 07/12/13 
 Pct Recovery = 69%  Analysis Date = 07/12/13 
 Pct Recovery = 69%  Analysis Date = 07/10/13 
 Pct Recovery = 69%  Analysis Date = 07/10/13 
 Pct Recovery = 69%  Analysis Date = 07/08/13 
 Pct Recovery = 69%  Analysis Date = 07/08/13 
 Pct Recovery = 69%  Analysis Date = 07/06/13 
 Pct Recovery = 69%  Analysis Date = 07/06/13 
 Pct Recovery = 69%  Analysis Date = 07/03/13 
 Pct Recovery = 69%  Analysis Date = 07/03/13 
 Pct Recovery = 69%  Analysis Date = 07/01/13 
 Pct Recovery = 69%  Analysis Date = 07/01/13 
 Pct Recovery = 69%  Analysis Date = 06/29/13 
 Pct Recovery = 70%  Analysis Date = 06/29/13 
 Pct Recovery = 70%  Analysis Date = 06/27/13 
 Pct Recovery = 70%  Analysis Date = 06/27/13 
 Pct Recovery = 70%  Analysis Date = 06/25/13 
 Pct Recovery = 70%  Analysis Date = 06/25/13 
 Pct Recovery = 70%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/20/13 
 Pct Recovery = 70%  Analysis Date = 06/20/13 
 Pct Recovery = 70%  Analysis Date = 06/18/13 
 Pct Recovery = 70%  Analysis Date = 06/18/13 
 Pct Recovery = 70%  Analysis Date = 06/16/13 
 Pct Recovery = 70%  Analysis Date = 06/16/13 
 Pct Recovery = 70%  Analysis Date = 06/14/13 
 Pct Recovery = 70%  Analysis Date = 06/14/13 
 Pct Recovery = 70%  Analysis Date = 06/11/13 
 Pct Recovery = 70%  Analysis Date = 06/11/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/09/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/07/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/05/13 
 Pct Recovery = 70%  Analysis Date = 06/03/13 
 Pct Recovery = 71%  Analysis Date = 06/03/13 
 Pct Recovery = 71%  Analysis Date = 05/31/13 
 Pct Recovery = 71%  Analysis Date = 05/31/13 
 Pct Recovery = 71%  Analysis Date = 05/29/13 
 Pct Recovery = 71%  Analysis Date = 05/29/13 
 Pct Recovery = 71%  Analysis Date = 05/27/13 
 Pct Recovery = 71%  Analysis Date = 05/27/13 
 Pct Recovery = 71%  Analysis Date = 05/25/13 
 Pct Recovery = 71%  Analysis Date = 05/25/13 
 Pct Recovery = 71%  Analysis Date = 05/23/13 
 Pct Recovery = 71%  Analysis Date = 05/23/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/20/13 
 Pct Recovery = 71%  Analysis Date = 05/18/13 
 Pct Recovery = 71%  Analysis Date = 05/18/13 
 Pct Recovery = 71%  Analysis Date = 05/16/13 
 Pct Recovery = 71%  Analysis Date = 05/16/13 
 Pct Recovery = 71%  Analysis Date = 05/14/13 
 Pct Recovery = 71%  Analysis Date = 05/14/13 
 Pct Recovery = 71%  Analysis Date = 05/12/13 
 Pct Recovery = 71%  Analysis Date = 05/12/13 
 Pct Recovery = 71%  Analysis Date = 05/09/13 
 Pct Recovery = 71%  Analysis Date = 05/09/13 
 Pct Recovery = 71%  Analysis Date = 05/07/13 
 Pct Recovery = 72%  Analysis Date = 05/07/13 
 Pct Recovery = 72%  Analysis Date = 05/05/13 
 Pct Recovery = 72%  Analysis Date = 05/05/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/03/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 05/01/13 
 Pct Recovery = 72%  Analysis Date = 04/28/13 
 Pct Recovery = 72%  Analysis Date = 04/28/13 
 Pct Recovery = 72%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/26/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/24/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/22/13 
 Pct Recovery = 72%  Analysis Date = 04/19/13 
 Pct Recovery = 72%  Analysis Date = 04/19/13 
 Pct Recovery = 72%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/15/13 
 Pct Recovery = 72%  Analysis Date = 04/15/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/11/13 
 Pct Recovery = 72%  Analysis Date = 04/11/13 
 Pct Recovery = 72%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/08/13 
 Pct Recovery = 72%  Analysis Date = 04/06/13 
 Pct Recovery = 72%  Analysis Date = 04/06/13 
 Pct Recovery = 72%  Analysis Date = 04/04/13 
 Pct Recovery = 72%  Analysis Date = 04/04/13 
 Pct Recovery = 72%  Analysis Date = 04/02/13 
 Pct Recovery = 72%  Analysis Date = 04/02/13 
 Pct Recovery = 72%  Analysis Date = 03/31/13 
 Pct Recovery = 72%  Analysis Date = 03/31/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/26/13 
 Pct Recovery = 72%  Analysis Date = 03/26/13 
 Pct Recovery = 72%  Analysis Date = 03/24/13 
 Pct Recovery = 72%  Analysis Date = 03/24/13 
 Pct Recovery = 72%  Analysis Date = 03/22/13 
 Pct Recovery = 73%  Analysis Date = 03/22/13 
 Pct Recovery = 73%  Analysis Date = 03/20/13 
 Pct Recovery = 73%  Analysis Date = 03/20/13 
 Pct Recovery = 73%  Analysis Date = 03/17/13 
 Pct Recovery = 73%  Analysis Date = 03/17/13 
 Pct Recovery = 73%  Analysis Date = 03/15/13 
 Pct Recovery = 73%  Analysis Date = 03/15/13 
 Pct Recovery = 73%  Analysis Date = 03/13/13 
 Pct Recovery = 74%  Analysis Date = 03/13/13 
 Pct Recovery = 74%  Analysis Date = 03/11/13 
 Pct Recovery = 74%  Analysis Date = 03/11/13 
 Pct Recovery = 74%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/09/13 
 Pct Recovery = 74%  Analysis Date = 03/06/13 
 Pct Recovery = 74%  Analysis Date = 03/06/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/04/13 
 Pct Recovery = 74%  Analysis Date = 03/02/13 
 Pct Recovery = 75%  Analysis Date = 03/02/13 
 Pct Recovery = 75%  Analysis Date = 02/28/13 
 Pct Recovery = 75%  Analysis Date = 02/28/13 
 Pct Recovery = 75%  Analysis Date = 02/26/13 
 Pct Recovery = 75%  Analysis Date = 02/26/13 
 Pct Recovery = 75%  Analysis Date = 02/23/13 
 Pct Recovery = 75%  Analysis Date = 02/23/13 
 Pct Recovery = 75%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/19/13 
 Pct Recovery = 76%  Analysis Date = 02/19/13 
 Pct Recovery = 76%  Analysis Date = 02/17/13 
 Pct Recovery = 76%  Analysis Date = 02/17/13 
 Pct Recovery = 76%  Analysis Date = 02/15/13 
 Pct Recovery = 76%  Analysis Date = 02/15/13 
 Pct Recovery = 76%  Analysis Date = 02/12/13 
 Pct Recovery = 76%  Analysis Date = 02/12/13 
 Pct Recovery = 76%  Analysis Date = 02/10/13 
 Pct Recovery = 77%  Analysis Date = 02/10/13 
 Pct Recovery = 77%  Analysis Date = 02/08/13 
 Pct Recovery = 77%  Analysis Date = 02/08/13 
 Pct Recovery = 77%  Analysis Date = 02/06/13 
 Pct Recovery = 77%  Analysis Date = 02/06/13 
 Pct Recovery = 77%  Analysis Date = 02/04/13 
 Pct Recovery = 77%  Analysis Date = 02/04/13 
 Pct Recovery = 77%  Analysis Date = 02/01/13 
 Pct Recovery = 78%  Analysis Date = 02/01/13 
 Pct Recovery = 78%  Analysis Date = 01/30/13 
 Pct Recovery = 78%  Analysis Date = 01/30/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 Pct Recovery = 78%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXYCODONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 7 67% 10% 69% 8%
Total 7 67% 10% 69% 8%

Sample Statistics
OXYCODONE

Characteristic N % % Basis
Plotted 7 100% Spiked
Estimated Values 1 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 0 0% 0 out of 7
Not Spiked 25 .  
False Positives 1 4% 1 out of 24

OBSP Determination:
PAROXETINE
METHOD: LC9017 , TESTIDCODE: 67527LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 50%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 49%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 14%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 18%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 45%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 42%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 17%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 25%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 11%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 14%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 12%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 32%  Analysis Date = 04/09/14 
 Pct Recovery = 29%  Analysis Date = 04/07/14 
 Pct Recovery = 29%  Analysis Date = 04/07/14 
 Pct Recovery = 29%  Analysis Date = 04/05/14 
 Pct Recovery = 29%  Analysis Date = 04/05/14 
 Pct Recovery = 29%  Analysis Date = 04/02/14 
 Pct Recovery = 29%  Analysis Date = 04/02/14 
 Pct Recovery = 29%  Analysis Date = 03/31/14 
 Pct Recovery = 28%  Analysis Date = 03/31/14 
 Pct Recovery = 28%  Analysis Date = 03/28/14 
 Pct Recovery = 28%  Analysis Date = 03/28/14 
 Pct Recovery = 28%  Analysis Date = 03/26/14 
 Pct Recovery = 28%  Analysis Date = 03/26/14 
 Pct Recovery = 28%  Analysis Date = 03/24/14 
 Pct Recovery = 28%  Analysis Date = 03/24/14 
 Pct Recovery = 28%  Analysis Date = 03/21/14 
 Pct Recovery = 28%  Analysis Date = 03/21/14 
 Pct Recovery = 28%  Analysis Date = 03/19/14 
 Pct Recovery = 28%  Analysis Date = 03/19/14 
 Pct Recovery = 28%  Analysis Date = 03/16/14 
 Pct Recovery = 28%  Analysis Date = 03/16/14 
 Pct Recovery = 28%  Analysis Date = 03/14/14 
 Pct Recovery = 28%  Analysis Date = 03/14/14 
 Pct Recovery = 28%  Analysis Date = 03/12/14 
 Pct Recovery = 28%  Analysis Date = 03/12/14 
 Pct Recovery = 28%  Analysis Date = 03/09/14 
 Pct Recovery = 28%  Analysis Date = 03/09/14 
 Pct Recovery = 28%  Analysis Date = 03/07/14 
 Pct Recovery = 28%  Analysis Date = 03/07/14 
 Pct Recovery = 28%  Analysis Date = 03/04/14 
 Pct Recovery = 28%  Analysis Date = 03/04/14 
 Pct Recovery = 28%  Analysis Date = 03/02/14 
 Pct Recovery = 27%  Analysis Date = 03/02/14 
 Pct Recovery = 27%  Analysis Date = 02/28/14 
 Pct Recovery = 27%  Analysis Date = 02/28/14 
 Pct Recovery = 27%  Analysis Date = 02/25/14 
 Pct Recovery = 27%  Analysis Date = 02/25/14 
 Pct Recovery = 27%  Analysis Date = 02/23/14 
 Pct Recovery = 27%  Analysis Date = 02/23/14 
 Pct Recovery = 27%  Analysis Date = 02/20/14 
 Pct Recovery = 27%  Analysis Date = 02/20/14 
 Pct Recovery = 27%  Analysis Date = 02/18/14 
 Pct Recovery = 27%  Analysis Date = 02/18/14 
 Pct Recovery = 27%  Analysis Date = 02/15/14 
 Pct Recovery = 27%  Analysis Date = 02/15/14 
 Pct Recovery = 27%  Analysis Date = 02/13/14 
 Pct Recovery = 27%  Analysis Date = 02/13/14 
 Pct Recovery = 27%  Analysis Date = 02/11/14 
 Pct Recovery = 27%  Analysis Date = 02/11/14 
 Pct Recovery = 27%  Analysis Date = 02/08/14 
 Pct Recovery = 27%  Analysis Date = 02/08/14 
 Pct Recovery = 27%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/06/14 
 Pct Recovery = 26%  Analysis Date = 02/03/14 
 Pct Recovery = 26%  Analysis Date = 02/03/14 
 Pct Recovery = 26%  Analysis Date = 02/01/14 
 Pct Recovery = 26%  Analysis Date = 02/01/14 
 Pct Recovery = 26%  Analysis Date = 01/30/14 
 Pct Recovery = 26%  Analysis Date = 01/30/14 
 Pct Recovery = 26%  Analysis Date = 01/27/14 
 Pct Recovery = 26%  Analysis Date = 01/27/14 
 Pct Recovery = 26%  Analysis Date = 01/25/14 
 Pct Recovery = 26%  Analysis Date = 01/25/14 
 Pct Recovery = 26%  Analysis Date = 01/22/14 
 Pct Recovery = 26%  Analysis Date = 01/22/14 
 Pct Recovery = 26%  Analysis Date = 01/20/14 
 Pct Recovery = 26%  Analysis Date = 01/20/14 
 Pct Recovery = 26%  Analysis Date = 01/18/14 
 Pct Recovery = 26%  Analysis Date = 01/18/14 
 Pct Recovery = 26%  Analysis Date = 01/15/14 
 Pct Recovery = 26%  Analysis Date = 01/15/14 
 Pct Recovery = 26%  Analysis Date = 01/13/14 
 Pct Recovery = 25%  Analysis Date = 01/13/14 
 Pct Recovery = 25%  Analysis Date = 01/10/14 
 Pct Recovery = 25%  Analysis Date = 01/10/14 
 Pct Recovery = 25%  Analysis Date = 01/08/14 
 Pct Recovery = 25%  Analysis Date = 01/08/14 
 Pct Recovery = 25%  Analysis Date = 01/06/14 
 Pct Recovery = 25%  Analysis Date = 01/06/14 
 Pct Recovery = 25%  Analysis Date = 01/03/14 
 Pct Recovery = 25%  Analysis Date = 01/03/14 
 Pct Recovery = 25%  Analysis Date = 01/01/14 
 Pct Recovery = 24%  Analysis Date = 01/01/14 
 Pct Recovery = 24%  Analysis Date = 12/29/13 
 Pct Recovery = 24%  Analysis Date = 12/29/13 
 Pct Recovery = 24%  Analysis Date = 12/27/13 
 Pct Recovery = 24%  Analysis Date = 12/27/13 
 Pct Recovery = 24%  Analysis Date = 12/24/13 
 Pct Recovery = 24%  Analysis Date = 12/24/13 
 Pct Recovery = 24%  Analysis Date = 12/22/13 
 Pct Recovery = 24%  Analysis Date = 12/22/13 
 Pct Recovery = 24%  Analysis Date = 12/20/13 
 Pct Recovery = 23%  Analysis Date = 12/20/13 
 Pct Recovery = 23%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/15/13 
 Pct Recovery = 23%  Analysis Date = 12/15/13 
 Pct Recovery = 23%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/10/13 
 Pct Recovery = 22%  Analysis Date = 12/10/13 
 Pct Recovery = 22%  Analysis Date = 12/08/13 
 Pct Recovery = 22%  Analysis Date = 12/08/13 
 Pct Recovery = 22%  Analysis Date = 12/05/13 
 Pct Recovery = 22%  Analysis Date = 12/05/13 
 Pct Recovery = 22%  Analysis Date = 12/03/13 
 Pct Recovery = 22%  Analysis Date = 12/03/13 
 Pct Recovery = 22%  Analysis Date = 11/30/13 
 Pct Recovery = 22%  Analysis Date = 11/30/13 
 Pct Recovery = 22%  Analysis Date = 11/28/13 
 Pct Recovery = 21%  Analysis Date = 11/28/13 
 Pct Recovery = 21%  Analysis Date = 11/26/13 
 Pct Recovery = 21%  Analysis Date = 11/26/13 
 Pct Recovery = 21%  Analysis Date = 11/23/13 
 Pct Recovery = 21%  Analysis Date = 11/23/13 
 Pct Recovery = 21%  Analysis Date = 11/21/13 
 Pct Recovery = 21%  Analysis Date = 11/21/13 
 Pct Recovery = 21%  Analysis Date = 11/18/13 
 Pct Recovery = 21%  Analysis Date = 11/18/13 
 Pct Recovery = 21%  Analysis Date = 11/16/13 
 Pct Recovery = 20%  Analysis Date = 11/16/13 
 Pct Recovery = 20%  Analysis Date = 11/13/13 
 Pct Recovery = 20%  Analysis Date = 11/13/13 
 Pct Recovery = 20%  Analysis Date = 11/11/13 
 Pct Recovery = 20%  Analysis Date = 11/11/13 
 Pct Recovery = 20%  Analysis Date = 11/09/13 
 Pct Recovery = 20%  Analysis Date = 11/09/13 
 Pct Recovery = 20%  Analysis Date = 11/06/13 
 Pct Recovery = 20%  Analysis Date = 11/06/13 
 Pct Recovery = 20%  Analysis Date = 11/04/13 
 Pct Recovery = 19%  Analysis Date = 11/04/13 
 Pct Recovery = 19%  Analysis Date = 11/01/13 
 Pct Recovery = 19%  Analysis Date = 11/01/13 
 Pct Recovery = 19%  Analysis Date = 10/30/13 
 Pct Recovery = 19%  Analysis Date = 10/30/13 
 Pct Recovery = 19%  Analysis Date = 10/28/13 
 Pct Recovery = 19%  Analysis Date = 10/28/13 
 Pct Recovery = 19%  Analysis Date = 10/25/13 
 Pct Recovery = 18%  Analysis Date = 10/25/13 
 Pct Recovery = 18%  Analysis Date = 10/23/13 
 Pct Recovery = 18%  Analysis Date = 10/23/13 
 Pct Recovery = 18%  Analysis Date = 10/20/13 
 Pct Recovery = 18%  Analysis Date = 10/20/13 
 Pct Recovery = 18%  Analysis Date = 10/18/13 
 Pct Recovery = 18%  Analysis Date = 10/18/13 
 Pct Recovery = 18%  Analysis Date = 10/16/13 
 Pct Recovery = 18%  Analysis Date = 10/16/13 
 Pct Recovery = 18%  Analysis Date = 10/13/13 
 Pct Recovery = 17%  Analysis Date = 10/13/13 
 Pct Recovery = 17%  Analysis Date = 10/11/13 
 Pct Recovery = 17%  Analysis Date = 10/11/13 
 Pct Recovery = 17%  Analysis Date = 10/08/13 
 Pct Recovery = 17%  Analysis Date = 10/08/13 
 Pct Recovery = 17%  Analysis Date = 10/06/13 
 Pct Recovery = 17%  Analysis Date = 10/06/13 
 Pct Recovery = 17%  Analysis Date = 10/04/13 
 Pct Recovery = 17%  Analysis Date = 10/04/13 
 Pct Recovery = 17%  Analysis Date = 10/01/13 
 Pct Recovery = 16%  Analysis Date = 10/01/13 
 Pct Recovery = 16%  Analysis Date = 09/29/13 
 Pct Recovery = 16%  Analysis Date = 09/29/13 
 Pct Recovery = 16%  Analysis Date = 09/26/13 
 Pct Recovery = 16%  Analysis Date = 09/26/13 
 Pct Recovery = 16%  Analysis Date = 09/24/13 
 Pct Recovery = 16%  Analysis Date = 09/24/13 
 Pct Recovery = 16%  Analysis Date = 09/21/13 
 Pct Recovery = 16%  Analysis Date = 09/21/13 
 Pct Recovery = 16%  Analysis Date = 09/19/13 
 Pct Recovery = 15%  Analysis Date = 09/19/13 
 Pct Recovery = 15%  Analysis Date = 09/17/13 
 Pct Recovery = 15%  Analysis Date = 09/17/13 
 Pct Recovery = 15%  Analysis Date = 09/14/13 
 Pct Recovery = 15%  Analysis Date = 09/14/13 
 Pct Recovery = 15%  Analysis Date = 09/12/13 
 Pct Recovery = 15%  Analysis Date = 09/12/13 
 Pct Recovery = 15%  Analysis Date = 09/09/13 
 Pct Recovery = 14%  Analysis Date = 09/09/13 
 Pct Recovery = 14%  Analysis Date = 09/07/13 
 Pct Recovery = 14%  Analysis Date = 09/07/13 
 Pct Recovery = 14%  Analysis Date = 09/05/13 
 Pct Recovery = 14%  Analysis Date = 09/05/13 
 Pct Recovery = 14%  Analysis Date = 09/02/13 
 Pct Recovery = 14%  Analysis Date = 09/02/13 
 Pct Recovery = 14%  Analysis Date = 08/31/13 
 Pct Recovery = 14%  Analysis Date = 08/31/13 
 Pct Recovery = 14%  Analysis Date = 08/28/13 
 Pct Recovery = 13%  Analysis Date = 08/28/13 
 Pct Recovery = 13%  Analysis Date = 08/26/13 
 Pct Recovery = 13%  Analysis Date = 08/26/13 
 Pct Recovery = 13%  Analysis Date = 08/24/13 
 Pct Recovery = 13%  Analysis Date = 08/24/13 
 Pct Recovery = 13%  Analysis Date = 08/21/13 
 Pct Recovery = 13%  Analysis Date = 08/21/13 
 Pct Recovery = 13%  Analysis Date = 08/19/13 
 Pct Recovery = 13%  Analysis Date = 08/19/13 
 Pct Recovery = 13%  Analysis Date = 08/16/13 
 Pct Recovery = 13%  Analysis Date = 08/16/13 
 Pct Recovery = 13%  Analysis Date = 08/14/13 
 Pct Recovery = 13%  Analysis Date = 08/14/13 
 Pct Recovery = 13%  Analysis Date = 08/11/13 
 Pct Recovery = 13%  Analysis Date = 08/11/13 
 Pct Recovery = 13%  Analysis Date = 08/09/13 
 Pct Recovery = 14%  Analysis Date = 08/09/13 
 Pct Recovery = 14%  Analysis Date = 08/07/13 
 Pct Recovery = 14%  Analysis Date = 08/07/13 
 Pct Recovery = 14%  Analysis Date = 08/04/13 
 Pct Recovery = 14%  Analysis Date = 08/04/13 
 Pct Recovery = 14%  Analysis Date = 08/02/13 
 Pct Recovery = 15%  Analysis Date = 08/02/13 
 Pct Recovery = 15%  Analysis Date = 07/30/13 
 Pct Recovery = 15%  Analysis Date = 07/30/13 
 Pct Recovery = 15%  Analysis Date = 07/28/13 
 Pct Recovery = 15%  Analysis Date = 07/28/13 
 Pct Recovery = 15%  Analysis Date = 07/26/13 
 Pct Recovery = 16%  Analysis Date = 07/26/13 
 Pct Recovery = 16%  Analysis Date = 07/23/13 
 Pct Recovery = 16%  Analysis Date = 07/23/13 
 Pct Recovery = 16%  Analysis Date = 07/21/13 
 Pct Recovery = 16%  Analysis Date = 07/21/13 
 Pct Recovery = 16%  Analysis Date = 07/18/13 
 Pct Recovery = 17%  Analysis Date = 07/18/13 
 Pct Recovery = 17%  Analysis Date = 07/16/13 
 Pct Recovery = 17%  Analysis Date = 07/16/13 
 Pct Recovery = 17%  Analysis Date = 07/14/13 
 Pct Recovery = 17%  Analysis Date = 07/14/13 
 Pct Recovery = 17%  Analysis Date = 07/11/13 
 Pct Recovery = 18%  Analysis Date = 07/11/13 
 Pct Recovery = 18%  Analysis Date = 07/09/13 
 Pct Recovery = 18%  Analysis Date = 07/09/13 
 Pct Recovery = 18%  Analysis Date = 07/06/13 
 Pct Recovery = 18%  Analysis Date = 07/06/13 
 Pct Recovery = 18%  Analysis Date = 07/04/13 
 Pct Recovery = 19%  Analysis Date = 07/04/13 
 Pct Recovery = 19%  Analysis Date = 07/02/13 
 Pct Recovery = 19%  Analysis Date = 07/02/13 
 Pct Recovery = 19%  Analysis Date = 06/29/13 
 Pct Recovery = 19%  Analysis Date = 06/29/13 
 Pct Recovery = 19%  Analysis Date = 06/27/13 
 Pct Recovery = 20%  Analysis Date = 06/27/13 
 Pct Recovery = 20%  Analysis Date = 06/24/13 
 Pct Recovery = 20%  Analysis Date = 06/24/13 
 Pct Recovery = 20%  Analysis Date = 06/22/13 
 Pct Recovery = 20%  Analysis Date = 06/22/13 
 Pct Recovery = 20%  Analysis Date = 06/19/13 
 Pct Recovery = 21%  Analysis Date = 06/19/13 
 Pct Recovery = 21%  Analysis Date = 06/17/13 
 Pct Recovery = 21%  Analysis Date = 06/17/13 
 Pct Recovery = 21%  Analysis Date = 06/15/13 
 Pct Recovery = 21%  Analysis Date = 06/15/13 
 Pct Recovery = 21%  Analysis Date = 06/12/13 
 Pct Recovery = 21%  Analysis Date = 06/12/13 
 Pct Recovery = 21%  Analysis Date = 06/10/13 
 Pct Recovery = 22%  Analysis Date = 06/10/13 
 Pct Recovery = 22%  Analysis Date = 06/07/13 
 Pct Recovery = 22%  Analysis Date = 06/07/13 
 Pct Recovery = 22%  Analysis Date = 06/05/13 
 Pct Recovery = 22%  Analysis Date = 06/05/13 
 Pct Recovery = 22%  Analysis Date = 06/03/13 
 Pct Recovery = 23%  Analysis Date = 06/03/13 
 Pct Recovery = 23%  Analysis Date = 05/31/13 
 Pct Recovery = 23%  Analysis Date = 05/31/13 
 Pct Recovery = 23%  Analysis Date = 05/29/13 
 Pct Recovery = 23%  Analysis Date = 05/29/13 
 Pct Recovery = 23%  Analysis Date = 05/26/13 
 Pct Recovery = 24%  Analysis Date = 05/26/13 
 Pct Recovery = 24%  Analysis Date = 05/24/13 
 Pct Recovery = 24%  Analysis Date = 05/24/13 
 Pct Recovery = 24%  Analysis Date = 05/22/13 
 Pct Recovery = 24%  Analysis Date = 05/22/13 
 Pct Recovery = 24%  Analysis Date = 05/19/13 
 Pct Recovery = 25%  Analysis Date = 05/19/13 
 Pct Recovery = 25%  Analysis Date = 05/17/13 
 Pct Recovery = 25%  Analysis Date = 05/17/13 
 Pct Recovery = 25%  Analysis Date = 05/14/13 
 Pct Recovery = 25%  Analysis Date = 05/14/13 
 Pct Recovery = 25%  Analysis Date = 05/12/13 
 Pct Recovery = 26%  Analysis Date = 05/12/13 
 Pct Recovery = 26%  Analysis Date = 05/10/13 
 Pct Recovery = 26%  Analysis Date = 05/10/13 
 Pct Recovery = 26%  Analysis Date = 05/07/13 
 Pct Recovery = 26%  Analysis Date = 05/07/13 
 Pct Recovery = 26%  Analysis Date = 05/05/13 
 Pct Recovery = 27%  Analysis Date = 05/05/13 
 Pct Recovery = 27%  Analysis Date = 05/02/13 
 Pct Recovery = 27%  Analysis Date = 05/02/13 
 Pct Recovery = 27%  Analysis Date = 04/30/13 
 Pct Recovery = 27%  Analysis Date = 04/30/13 
 Pct Recovery = 27%  Analysis Date = 04/27/13 
 Pct Recovery = 27%  Analysis Date = 04/27/13 
 Pct Recovery = 27%  Analysis Date = 04/25/13 
 Pct Recovery = 27%  Analysis Date = 04/25/13 
 Pct Recovery = 27%  Analysis Date = 04/23/13 
 Pct Recovery = 27%  Analysis Date = 04/23/13 
 Pct Recovery = 27%  Analysis Date = 04/20/13 
 Pct Recovery = 27%  Analysis Date = 04/20/13 
 Pct Recovery = 27%  Analysis Date = 04/18/13 
 Pct Recovery = 27%  Analysis Date = 04/18/13 
 Pct Recovery = 27%  Analysis Date = 04/15/13 
 Pct Recovery = 27%  Analysis Date = 04/15/13 
 Pct Recovery = 27%  Analysis Date = 04/13/13 
 Pct Recovery = 27%  Analysis Date = 04/13/13 
 Pct Recovery = 27%  Analysis Date = 04/11/13 
 Pct Recovery = 27%  Analysis Date = 04/11/13 
 Pct Recovery = 27%  Analysis Date = 04/08/13 
 Pct Recovery = 27%  Analysis Date = 04/08/13 
 Pct Recovery = 27%  Analysis Date = 04/06/13 
 Pct Recovery = 27%  Analysis Date = 04/06/13 
 Pct Recovery = 27%  Analysis Date = 04/03/13 
 Pct Recovery = 28%  Analysis Date = 04/03/13 
 Pct Recovery = 28%  Analysis Date = 04/01/13 
 Pct Recovery = 28%  Analysis Date = 04/01/13 
 Pct Recovery = 28%  Analysis Date = 03/30/13 
 Pct Recovery = 28%  Analysis Date = 03/30/13 
 Pct Recovery = 28%  Analysis Date = 03/27/13 
 Pct Recovery = 28%  Analysis Date = 03/27/13 
 Pct Recovery = 28%  Analysis Date = 03/25/13 
 Pct Recovery = 28%  Analysis Date = 03/25/13 
 Pct Recovery = 28%  Analysis Date = 03/22/13 
 Pct Recovery = 28%  Analysis Date = 03/22/13 
 Pct Recovery = 28%  Analysis Date = 03/20/13 
 Pct Recovery = 28%  Analysis Date = 03/20/13 
 Pct Recovery = 28%  Analysis Date = 03/17/13 
 Pct Recovery = 29%  Analysis Date = 03/17/13 
 Pct Recovery = 29%  Analysis Date = 03/15/13 
 Pct Recovery = 29%  Analysis Date = 03/15/13 
 Pct Recovery = 29%  Analysis Date = 03/13/13 
 Pct Recovery = 29%  Analysis Date = 03/13/13 
 Pct Recovery = 29%  Analysis Date = 03/10/13 
 Pct Recovery = 29%  Analysis Date = 03/10/13 
 Pct Recovery = 29%  Analysis Date = 03/08/13 
 Pct Recovery = 29%  Analysis Date = 03/08/13 
 Pct Recovery = 29%  Analysis Date = 03/05/13 
 Pct Recovery = 29%  Analysis Date = 03/05/13 
 Pct Recovery = 29%  Analysis Date = 03/03/13 
 Pct Recovery = 29%  Analysis Date = 03/03/13 
 Pct Recovery = 29%  Analysis Date = 03/01/13 
 Pct Recovery = 30%  Analysis Date = 03/01/13 
 Pct Recovery = 30%  Analysis Date = 02/26/13 
 Pct Recovery = 30%  Analysis Date = 02/26/13 
 Pct Recovery = 30%  Analysis Date = 02/24/13 
 Pct Recovery = 30%  Analysis Date = 02/24/13 
 Pct Recovery = 30%  Analysis Date = 02/21/13 
 Pct Recovery = 30%  Analysis Date = 02/21/13 
 Pct Recovery = 30%  Analysis Date = 02/19/13 
 Pct Recovery = 30%  Analysis Date = 02/19/13 
 Pct Recovery = 30%  Analysis Date = 02/17/13 
 Pct Recovery = 30%  Analysis Date = 02/17/13 
 Pct Recovery = 30%  Analysis Date = 02/14/13 
 Pct Recovery = 30%  Analysis Date = 02/14/13 
 Pct Recovery = 30%  Analysis Date = 02/12/13 
 Pct Recovery = 31%  Analysis Date = 02/12/13 
 Pct Recovery = 31%  Analysis Date = 02/09/13 
 Pct Recovery = 31%  Analysis Date = 02/09/13 
 Pct Recovery = 31%  Analysis Date = 02/07/13 
 Pct Recovery = 31%  Analysis Date = 02/07/13 
 Pct Recovery = 31%  Analysis Date = 02/05/13 
 Pct Recovery = 31%  Analysis Date = 02/05/13 
 Pct Recovery = 31%  Analysis Date = 02/02/13 
 Pct Recovery = 31%  Analysis Date = 02/02/13 
 Pct Recovery = 31%  Analysis Date = 01/31/13 
 Pct Recovery = 31%  Analysis Date = 01/31/13 
 Pct Recovery = 31%  Analysis Date = 01/28/13 
 Pct Recovery = 32%  Analysis Date = 01/28/13 
 Pct Recovery = 32%  Analysis Date = 01/26/13 
 Pct Recovery = 32%  Analysis Date = 01/26/13 
 Pct Recovery = 32%  Analysis Date = 01/23/13 
 Pct Recovery = 32%  Analysis Date = 01/23/13 
 Pct Recovery = 32%  Analysis Date = 01/21/13 
 Pct Recovery = 32%  Analysis Date = 01/21/13 
 Pct Recovery = 32%  Analysis Date = 01/19/13 
 Pct Recovery = 32%  Analysis Date = 01/19/13 
 Pct Recovery = 32%  Analysis Date = 01/16/13 
 Pct Recovery = 32%  Analysis Date = 01/16/13 
 Pct Recovery = 32%  Analysis Date = 01/14/13 
 Pct Recovery = 32%  Analysis Date = 01/14/13 
 Pct Recovery = 32%  Analysis Date = 01/11/13 
 Pct Recovery = 32%  Analysis Date = 01/11/13 
 Pct Recovery = 32%  Analysis Date = 01/09/13 
 Pct Recovery = 33%  Analysis Date = 01/09/13 
 Pct Recovery = 33%  Analysis Date = 01/07/13 
 Pct Recovery = 33%  Analysis Date = 01/07/13 
 Pct Recovery = 33%  Analysis Date = 01/04/13 
 Pct Recovery = 33%  Analysis Date = 01/04/13 
 Pct Recovery = 33%  Analysis Date = 01/02/13 
 Pct Recovery = 33%  Analysis Date = 01/02/13 
 Pct Recovery = 33%  Analysis Date = 12/30/12 
 Pct Recovery = 33%  Analysis Date = 12/30/12 
 Pct Recovery = 33%  Analysis Date = 12/28/12 
 Pct Recovery = 33%  Analysis Date = 12/28/12 
 Pct Recovery = 33%  Analysis Date = 12/26/12 
 Pct Recovery = 33%  Analysis Date = 12/26/12 
 Pct Recovery = 33%  Analysis Date = 12/23/12 
 Pct Recovery = 33%  Analysis Date = 12/23/12 
 Pct Recovery = 33%  Analysis Date = 12/21/12 
 Pct Recovery = 33%  Analysis Date = 12/21/12 
 Pct Recovery = 33%  Analysis Date = 12/18/12 
 Pct Recovery = 34%  Analysis Date = 12/18/12 
 Pct Recovery = 34%  Analysis Date = 12/16/12 
 Pct Recovery = 34%  Analysis Date = 12/16/12 
 Pct Recovery = 34%  Analysis Date = 12/14/12 
 Pct Recovery = 34%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PAROXETINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 12 27% 15% 21% 22%
Total 12 27% 15% 21% 22%

Sample Statistics
PAROXETINE

Characteristic N % % Basis
Plotted 12 86% Spiked
Estimated Values 12 86% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 2 14% 2 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PENCICLOVIR
METHOD: LC9017 , TESTIDCODE: 68021LCM56

 Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 249%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 119%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 88%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 128%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 73%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 90%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 93%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 122%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 105%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 80%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 97%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 75%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 98%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 116%  Analysis Date = 04/09/14 
 Pct Recovery = 84%  Analysis Date = 04/07/14 
 Pct Recovery = 84%  Analysis Date = 04/07/14 
 Pct Recovery = 84%  Analysis Date = 04/05/14 
 Pct Recovery = 84%  Analysis Date = 04/05/14 
 Pct Recovery = 84%  Analysis Date = 04/02/14 
 Pct Recovery = 84%  Analysis Date = 04/02/14 
 Pct Recovery = 84%  Analysis Date = 03/31/14 
 Pct Recovery = 84%  Analysis Date = 03/31/14 
 Pct Recovery = 84%  Analysis Date = 03/28/14 
 Pct Recovery = 84%  Analysis Date = 03/28/14 
 Pct Recovery = 84%  Analysis Date = 03/26/14 
 Pct Recovery = 85%  Analysis Date = 03/26/14 
 Pct Recovery = 85%  Analysis Date = 03/24/14 
 Pct Recovery = 85%  Analysis Date = 03/24/14 
 Pct Recovery = 85%  Analysis Date = 03/21/14 
 Pct Recovery = 85%  Analysis Date = 03/21/14 
 Pct Recovery = 85%  Analysis Date = 03/19/14 
 Pct Recovery = 85%  Analysis Date = 03/19/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/16/14 
 Pct Recovery = 85%  Analysis Date = 03/14/14 
 Pct Recovery = 85%  Analysis Date = 03/14/14 
 Pct Recovery = 85%  Analysis Date = 03/12/14 
 Pct Recovery = 85%  Analysis Date = 03/12/14 
 Pct Recovery = 85%  Analysis Date = 03/09/14 
 Pct Recovery = 85%  Analysis Date = 03/09/14 
 Pct Recovery = 85%  Analysis Date = 03/07/14 
 Pct Recovery = 85%  Analysis Date = 03/07/14 
 Pct Recovery = 85%  Analysis Date = 03/04/14 
 Pct Recovery = 85%  Analysis Date = 03/04/14 
 Pct Recovery = 85%  Analysis Date = 03/02/14 
 Pct Recovery = 85%  Analysis Date = 03/02/14 
 Pct Recovery = 85%  Analysis Date = 02/28/14 
 Pct Recovery = 86%  Analysis Date = 02/28/14 
 Pct Recovery = 86%  Analysis Date = 02/25/14 
 Pct Recovery = 86%  Analysis Date = 02/25/14 
 Pct Recovery = 86%  Analysis Date = 02/23/14 
 Pct Recovery = 86%  Analysis Date = 02/23/14 
 Pct Recovery = 86%  Analysis Date = 02/20/14 
 Pct Recovery = 86%  Analysis Date = 02/20/14 
 Pct Recovery = 86%  Analysis Date = 02/18/14 
 Pct Recovery = 86%  Analysis Date = 02/18/14 
 Pct Recovery = 86%  Analysis Date = 02/15/14 
 Pct Recovery = 86%  Analysis Date = 02/15/14 
 Pct Recovery = 86%  Analysis Date = 02/13/14 
 Pct Recovery = 86%  Analysis Date = 02/13/14 
 Pct Recovery = 86%  Analysis Date = 02/11/14 
 Pct Recovery = 86%  Analysis Date = 02/11/14 
 Pct Recovery = 86%  Analysis Date = 02/08/14 
 Pct Recovery = 86%  Analysis Date = 02/08/14 
 Pct Recovery = 86%  Analysis Date = 02/06/14 
 Pct Recovery = 86%  Analysis Date = 02/06/14 
 Pct Recovery = 86%  Analysis Date = 02/03/14 
 Pct Recovery = 86%  Analysis Date = 02/03/14 
 Pct Recovery = 86%  Analysis Date = 02/01/14 
 Pct Recovery = 86%  Analysis Date = 02/01/14 
 Pct Recovery = 86%  Analysis Date = 01/30/14 
 Pct Recovery = 87%  Analysis Date = 01/30/14 
 Pct Recovery = 87%  Analysis Date = 01/27/14 
 Pct Recovery = 87%  Analysis Date = 01/27/14 
 Pct Recovery = 87%  Analysis Date = 01/25/14 
 Pct Recovery = 87%  Analysis Date = 01/25/14 
 Pct Recovery = 87%  Analysis Date = 01/22/14 
 Pct Recovery = 87%  Analysis Date = 01/22/14 
 Pct Recovery = 87%  Analysis Date = 01/20/14 
 Pct Recovery = 87%  Analysis Date = 01/20/14 
 Pct Recovery = 87%  Analysis Date = 01/18/14 
 Pct Recovery = 87%  Analysis Date = 01/18/14 
 Pct Recovery = 87%  Analysis Date = 01/15/14 
 Pct Recovery = 87%  Analysis Date = 01/15/14 
 Pct Recovery = 87%  Analysis Date = 01/13/14 
 Pct Recovery = 87%  Analysis Date = 01/13/14 
 Pct Recovery = 87%  Analysis Date = 01/10/14 
 Pct Recovery = 87%  Analysis Date = 01/10/14 
 Pct Recovery = 87%  Analysis Date = 01/08/14 
 Pct Recovery = 87%  Analysis Date = 01/08/14 
 Pct Recovery = 87%  Analysis Date = 01/06/14 
 Pct Recovery = 87%  Analysis Date = 01/06/14 
 Pct Recovery = 87%  Analysis Date = 01/03/14 
 Pct Recovery = 87%  Analysis Date = 01/03/14 
 Pct Recovery = 87%  Analysis Date = 01/01/14 
 Pct Recovery = 88%  Analysis Date = 01/01/14 
 Pct Recovery = 88%  Analysis Date = 12/29/13 
 Pct Recovery = 88%  Analysis Date = 12/29/13 
 Pct Recovery = 88%  Analysis Date = 12/27/13 
 Pct Recovery = 88%  Analysis Date = 12/27/13 
 Pct Recovery = 88%  Analysis Date = 12/24/13 
 Pct Recovery = 88%  Analysis Date = 12/24/13 
 Pct Recovery = 88%  Analysis Date = 12/22/13 
 Pct Recovery = 88%  Analysis Date = 12/22/13 
 Pct Recovery = 88%  Analysis Date = 12/20/13 
 Pct Recovery = 88%  Analysis Date = 12/20/13 
 Pct Recovery = 88%  Analysis Date = 12/17/13 
 Pct Recovery = 88%  Analysis Date = 12/17/13 
 Pct Recovery = 88%  Analysis Date = 12/15/13 
 Pct Recovery = 88%  Analysis Date = 12/15/13 
 Pct Recovery = 88%  Analysis Date = 12/12/13 
 Pct Recovery = 88%  Analysis Date = 12/12/13 
 Pct Recovery = 88%  Analysis Date = 12/10/13 
 Pct Recovery = 88%  Analysis Date = 12/10/13 
 Pct Recovery = 88%  Analysis Date = 12/08/13 
 Pct Recovery = 88%  Analysis Date = 12/08/13 
 Pct Recovery = 88%  Analysis Date = 12/05/13 
 Pct Recovery = 88%  Analysis Date = 12/05/13 
 Pct Recovery = 88%  Analysis Date = 12/03/13 
 Pct Recovery = 88%  Analysis Date = 12/03/13 
 Pct Recovery = 88%  Analysis Date = 11/30/13 
 Pct Recovery = 89%  Analysis Date = 11/30/13 
 Pct Recovery = 89%  Analysis Date = 11/28/13 
 Pct Recovery = 89%  Analysis Date = 11/28/13 
 Pct Recovery = 89%  Analysis Date = 11/26/13 
 Pct Recovery = 89%  Analysis Date = 11/26/13 
 Pct Recovery = 89%  Analysis Date = 11/23/13 
 Pct Recovery = 89%  Analysis Date = 11/23/13 
 Pct Recovery = 89%  Analysis Date = 11/21/13 
 Pct Recovery = 89%  Analysis Date = 11/21/13 
 Pct Recovery = 89%  Analysis Date = 11/18/13 
 Pct Recovery = 89%  Analysis Date = 11/18/13 
 Pct Recovery = 89%  Analysis Date = 11/16/13 
 Pct Recovery = 89%  Analysis Date = 11/16/13 
 Pct Recovery = 89%  Analysis Date = 11/13/13 
 Pct Recovery = 89%  Analysis Date = 11/13/13 
 Pct Recovery = 89%  Analysis Date = 11/11/13 
 Pct Recovery = 89%  Analysis Date = 11/11/13 
 Pct Recovery = 89%  Analysis Date = 11/09/13 
 Pct Recovery = 89%  Analysis Date = 11/09/13 
 Pct Recovery = 89%  Analysis Date = 11/06/13 
 Pct Recovery = 89%  Analysis Date = 11/06/13 
 Pct Recovery = 89%  Analysis Date = 11/04/13 
 Pct Recovery = 89%  Analysis Date = 11/04/13 
 Pct Recovery = 89%  Analysis Date = 11/01/13 
 Pct Recovery = 89%  Analysis Date = 11/01/13 
 Pct Recovery = 89%  Analysis Date = 10/30/13 
 Pct Recovery = 90%  Analysis Date = 10/30/13 
 Pct Recovery = 90%  Analysis Date = 10/28/13 
 Pct Recovery = 90%  Analysis Date = 10/28/13 
 Pct Recovery = 90%  Analysis Date = 10/25/13 
 Pct Recovery = 90%  Analysis Date = 10/25/13 
 Pct Recovery = 90%  Analysis Date = 10/23/13 
 Pct Recovery = 90%  Analysis Date = 10/23/13 
 Pct Recovery = 90%  Analysis Date = 10/20/13 
 Pct Recovery = 90%  Analysis Date = 10/20/13 
 Pct Recovery = 90%  Analysis Date = 10/18/13 
 Pct Recovery = 90%  Analysis Date = 10/18/13 
 Pct Recovery = 90%  Analysis Date = 10/16/13 
 Pct Recovery = 90%  Analysis Date = 10/16/13 
 Pct Recovery = 90%  Analysis Date = 10/13/13 
 Pct Recovery = 90%  Analysis Date = 10/13/13 
 Pct Recovery = 90%  Analysis Date = 10/11/13 
 Pct Recovery = 90%  Analysis Date = 10/11/13 
 Pct Recovery = 90%  Analysis Date = 10/08/13 
 Pct Recovery = 90%  Analysis Date = 10/08/13 
 Pct Recovery = 90%  Analysis Date = 10/06/13 
 Pct Recovery = 90%  Analysis Date = 10/06/13 
 Pct Recovery = 90%  Analysis Date = 10/04/13 
 Pct Recovery = 91%  Analysis Date = 10/04/13 
 Pct Recovery = 91%  Analysis Date = 10/01/13 
 Pct Recovery = 91%  Analysis Date = 10/01/13 
 Pct Recovery = 91%  Analysis Date = 09/29/13 
 Pct Recovery = 91%  Analysis Date = 09/29/13 
 Pct Recovery = 91%  Analysis Date = 09/26/13 
 Pct Recovery = 91%  Analysis Date = 09/26/13 
 Pct Recovery = 91%  Analysis Date = 09/24/13 
 Pct Recovery = 91%  Analysis Date = 09/24/13 
 Pct Recovery = 91%  Analysis Date = 09/21/13 
 Pct Recovery = 91%  Analysis Date = 09/21/13 
 Pct Recovery = 91%  Analysis Date = 09/19/13 
 Pct Recovery = 91%  Analysis Date = 09/19/13 
 Pct Recovery = 91%  Analysis Date = 09/17/13 
 Pct Recovery = 91%  Analysis Date = 09/17/13 
 Pct Recovery = 91%  Analysis Date = 09/14/13 
 Pct Recovery = 91%  Analysis Date = 09/14/13 
 Pct Recovery = 91%  Analysis Date = 09/12/13 
 Pct Recovery = 91%  Analysis Date = 09/12/13 
 Pct Recovery = 91%  Analysis Date = 09/09/13 
 Pct Recovery = 91%  Analysis Date = 09/09/13 
 Pct Recovery = 91%  Analysis Date = 09/07/13 
 Pct Recovery = 92%  Analysis Date = 09/07/13 
 Pct Recovery = 92%  Analysis Date = 09/05/13 
 Pct Recovery = 92%  Analysis Date = 09/05/13 
 Pct Recovery = 92%  Analysis Date = 09/02/13 
 Pct Recovery = 92%  Analysis Date = 09/02/13 
 Pct Recovery = 92%  Analysis Date = 08/31/13 
 Pct Recovery = 92%  Analysis Date = 08/31/13 
 Pct Recovery = 92%  Analysis Date = 08/28/13 
 Pct Recovery = 92%  Analysis Date = 08/28/13 
 Pct Recovery = 92%  Analysis Date = 08/26/13 
 Pct Recovery = 92%  Analysis Date = 08/26/13 
 Pct Recovery = 92%  Analysis Date = 08/24/13 
 Pct Recovery = 92%  Analysis Date = 08/24/13 
 Pct Recovery = 92%  Analysis Date = 08/21/13 
 Pct Recovery = 92%  Analysis Date = 08/21/13 
 Pct Recovery = 92%  Analysis Date = 08/19/13 
 Pct Recovery = 92%  Analysis Date = 08/19/13 
 Pct Recovery = 92%  Analysis Date = 08/16/13 
 Pct Recovery = 93%  Analysis Date = 08/16/13 
 Pct Recovery = 93%  Analysis Date = 08/14/13 
 Pct Recovery = 93%  Analysis Date = 08/14/13 
 Pct Recovery = 93%  Analysis Date = 08/11/13 
 Pct Recovery = 93%  Analysis Date = 08/11/13 
 Pct Recovery = 93%  Analysis Date = 08/09/13 
 Pct Recovery = 94%  Analysis Date = 08/09/13 
 Pct Recovery = 94%  Analysis Date = 08/07/13 
 Pct Recovery = 94%  Analysis Date = 08/07/13 
 Pct Recovery = 94%  Analysis Date = 08/04/13 
 Pct Recovery = 94%  Analysis Date = 08/04/13 
 Pct Recovery = 94%  Analysis Date = 08/02/13 
 Pct Recovery = 95%  Analysis Date = 08/02/13 
 Pct Recovery = 95%  Analysis Date = 07/30/13 
 Pct Recovery = 95%  Analysis Date = 07/30/13 
 Pct Recovery = 95%  Analysis Date = 07/28/13 
 Pct Recovery = 95%  Analysis Date = 07/28/13 
 Pct Recovery = 95%  Analysis Date = 07/26/13 
 Pct Recovery = 95%  Analysis Date = 07/26/13 
 Pct Recovery = 95%  Analysis Date = 07/23/13 
 Pct Recovery = 96%  Analysis Date = 07/23/13 
 Pct Recovery = 96%  Analysis Date = 07/21/13 
 Pct Recovery = 96%  Analysis Date = 07/21/13 
 Pct Recovery = 96%  Analysis Date = 07/18/13 
 Pct Recovery = 96%  Analysis Date = 07/18/13 
 Pct Recovery = 96%  Analysis Date = 07/16/13 
 Pct Recovery = 97%  Analysis Date = 07/16/13 
 Pct Recovery = 97%  Analysis Date = 07/14/13 
 Pct Recovery = 97%  Analysis Date = 07/14/13 
 Pct Recovery = 97%  Analysis Date = 07/11/13 
 Pct Recovery = 97%  Analysis Date = 07/11/13 
 Pct Recovery = 97%  Analysis Date = 07/09/13 
 Pct Recovery = 98%  Analysis Date = 07/09/13 
 Pct Recovery = 98%  Analysis Date = 07/06/13 
 Pct Recovery = 98%  Analysis Date = 07/06/13 
 Pct Recovery = 98%  Analysis Date = 07/04/13 
 Pct Recovery = 98%  Analysis Date = 07/04/13 
 Pct Recovery = 98%  Analysis Date = 07/02/13 
 Pct Recovery = 99%  Analysis Date = 07/02/13 
 Pct Recovery = 99%  Analysis Date = 06/29/13 
 Pct Recovery = 99%  Analysis Date = 06/29/13 
 Pct Recovery = 99%  Analysis Date = 06/27/13 
 Pct Recovery = 99%  Analysis Date = 06/27/13 
 Pct Recovery = 99%  Analysis Date = 06/24/13 
 Pct Recovery = 100%  Analysis Date = 06/24/13 
 Pct Recovery = 100%  Analysis Date = 06/22/13 
 Pct Recovery = 100%  Analysis Date = 06/22/13 
 Pct Recovery = 100%  Analysis Date = 06/19/13 
 Pct Recovery = 100%  Analysis Date = 06/19/13 
 Pct Recovery = 100%  Analysis Date = 06/17/13 
 Pct Recovery = 101%  Analysis Date = 06/17/13 
 Pct Recovery = 101%  Analysis Date = 06/15/13 
 Pct Recovery = 101%  Analysis Date = 06/15/13 
 Pct Recovery = 101%  Analysis Date = 06/12/13 
 Pct Recovery = 101%  Analysis Date = 06/12/13 
 Pct Recovery = 101%  Analysis Date = 06/10/13 
 Pct Recovery = 102%  Analysis Date = 06/10/13 
 Pct Recovery = 102%  Analysis Date = 06/07/13 
 Pct Recovery = 102%  Analysis Date = 06/07/13 
 Pct Recovery = 102%  Analysis Date = 06/05/13 
 Pct Recovery = 102%  Analysis Date = 06/05/13 
 Pct Recovery = 102%  Analysis Date = 06/03/13 
 Pct Recovery = 103%  Analysis Date = 06/03/13 
 Pct Recovery = 103%  Analysis Date = 05/31/13 
 Pct Recovery = 103%  Analysis Date = 05/31/13 
 Pct Recovery = 103%  Analysis Date = 05/29/13 
 Pct Recovery = 103%  Analysis Date = 05/29/13 
 Pct Recovery = 103%  Analysis Date = 05/26/13 
 Pct Recovery = 104%  Analysis Date = 05/26/13 
 Pct Recovery = 104%  Analysis Date = 05/24/13 
 Pct Recovery = 104%  Analysis Date = 05/24/13 
 Pct Recovery = 104%  Analysis Date = 05/22/13 
 Pct Recovery = 104%  Analysis Date = 05/22/13 
 Pct Recovery = 104%  Analysis Date = 05/19/13 
 Pct Recovery = 105%  Analysis Date = 05/19/13 
 Pct Recovery = 105%  Analysis Date = 05/17/13 
 Pct Recovery = 105%  Analysis Date = 05/17/13 
 Pct Recovery = 105%  Analysis Date = 05/14/13 
 Pct Recovery = 105%  Analysis Date = 05/14/13 
 Pct Recovery = 105%  Analysis Date = 05/12/13 
 Pct Recovery = 106%  Analysis Date = 05/12/13 
 Pct Recovery = 106%  Analysis Date = 05/10/13 
 Pct Recovery = 106%  Analysis Date = 05/10/13 
 Pct Recovery = 106%  Analysis Date = 05/07/13 
 Pct Recovery = 106%  Analysis Date = 05/07/13 
 Pct Recovery = 106%  Analysis Date = 05/05/13 
 Pct Recovery = 107%  Analysis Date = 05/05/13 
 Pct Recovery = 107%  Analysis Date = 05/02/13 
 Pct Recovery = 107%  Analysis Date = 05/02/13 
 Pct Recovery = 107%  Analysis Date = 04/30/13 
 Pct Recovery = 106%  Analysis Date = 04/30/13 
 Pct Recovery = 106%  Analysis Date = 04/27/13 
 Pct Recovery = 104%  Analysis Date = 04/27/13 
 Pct Recovery = 104%  Analysis Date = 04/25/13 
 Pct Recovery = 103%  Analysis Date = 04/25/13 
 Pct Recovery = 103%  Analysis Date = 04/23/13 
 Pct Recovery = 104%  Analysis Date = 04/23/13 
 Pct Recovery = 104%  Analysis Date = 04/20/13 
 Pct Recovery = 106%  Analysis Date = 04/20/13 
 Pct Recovery = 106%  Analysis Date = 04/18/13 
 Pct Recovery = 107%  Analysis Date = 04/18/13 
 Pct Recovery = 107%  Analysis Date = 04/15/13 
 Pct Recovery = 109%  Analysis Date = 04/15/13 
 Pct Recovery = 109%  Analysis Date = 04/13/13 
 Pct Recovery = 110%  Analysis Date = 04/13/13 
 Pct Recovery = 110%  Analysis Date = 04/11/13 
 Pct Recovery = 112%  Analysis Date = 04/11/13 
 Pct Recovery = 112%  Analysis Date = 04/08/13 
 Pct Recovery = 113%  Analysis Date = 04/08/13 
 Pct Recovery = 113%  Analysis Date = 04/06/13 
 Pct Recovery = 115%  Analysis Date = 04/06/13 
 Pct Recovery = 115%  Analysis Date = 04/03/13 
 Pct Recovery = 116%  Analysis Date = 04/03/13 
 Pct Recovery = 116%  Analysis Date = 04/01/13 
 Pct Recovery = 118%  Analysis Date = 04/01/13 
 Pct Recovery = 118%  Analysis Date = 03/30/13 
 Pct Recovery = 119%  Analysis Date = 03/30/13 
 Pct Recovery = 119%  Analysis Date = 03/27/13 
 Pct Recovery = 121%  Analysis Date = 03/27/13 
 Pct Recovery = 121%  Analysis Date = 03/25/13 
 Pct Recovery = 122%  Analysis Date = 03/25/13 
 Pct Recovery = 122%  Analysis Date = 03/22/13 
 Pct Recovery = 123%  Analysis Date = 03/22/13 
 Pct Recovery = 123%  Analysis Date = 03/20/13 
 Pct Recovery = 125%  Analysis Date = 03/20/13 
 Pct Recovery = 125%  Analysis Date = 03/17/13 
 Pct Recovery = 126%  Analysis Date = 03/17/13 
 Pct Recovery = 126%  Analysis Date = 03/15/13 
 Pct Recovery = 127%  Analysis Date = 03/15/13 
 Pct Recovery = 127%  Analysis Date = 03/13/13 
 Pct Recovery = 128%  Analysis Date = 03/13/13 
 Pct Recovery = 128%  Analysis Date = 03/10/13 
 Pct Recovery = 130%  Analysis Date = 03/10/13 
 Pct Recovery = 130%  Analysis Date = 03/08/13 
 Pct Recovery = 131%  Analysis Date = 03/08/13 
 Pct Recovery = 131%  Analysis Date = 03/05/13 
 Pct Recovery = 132%  Analysis Date = 03/05/13 
 Pct Recovery = 132%  Analysis Date = 03/03/13 
 Pct Recovery = 133%  Analysis Date = 03/03/13 
 Pct Recovery = 133%  Analysis Date = 03/01/13 
 Pct Recovery = 135%  Analysis Date = 03/01/13 
 Pct Recovery = 135%  Analysis Date = 02/26/13 
 Pct Recovery = 136%  Analysis Date = 02/26/13 
 Pct Recovery = 136%  Analysis Date = 02/24/13 
 Pct Recovery = 137%  Analysis Date = 02/24/13 
 Pct Recovery = 137%  Analysis Date = 02/21/13 
 Pct Recovery = 138%  Analysis Date = 02/21/13 
 Pct Recovery = 138%  Analysis Date = 02/19/13 
 Pct Recovery = 139%  Analysis Date = 02/19/13 
 Pct Recovery = 139%  Analysis Date = 02/17/13 
 Pct Recovery = 141%  Analysis Date = 02/17/13 
 Pct Recovery = 141%  Analysis Date = 02/14/13 
 Pct Recovery = 142%  Analysis Date = 02/14/13 
 Pct Recovery = 142%  Analysis Date = 02/12/13 
 Pct Recovery = 143%  Analysis Date = 02/12/13 
 Pct Recovery = 143%  Analysis Date = 02/09/13 
 Pct Recovery = 144%  Analysis Date = 02/09/13 
 Pct Recovery = 144%  Analysis Date = 02/07/13 
 Pct Recovery = 146%  Analysis Date = 02/07/13 
 Pct Recovery = 146%  Analysis Date = 02/05/13 
 Pct Recovery = 147%  Analysis Date = 02/05/13 
 Pct Recovery = 147%  Analysis Date = 02/02/13 
 Pct Recovery = 148%  Analysis Date = 02/02/13 
 Pct Recovery = 148%  Analysis Date = 01/31/13 
 Pct Recovery = 149%  Analysis Date = 01/31/13 
 Pct Recovery = 149%  Analysis Date = 01/28/13 
 Pct Recovery = 151%  Analysis Date = 01/28/13 
 Pct Recovery = 151%  Analysis Date = 01/26/13 
 Pct Recovery = 152%  Analysis Date = 01/26/13 
 Pct Recovery = 152%  Analysis Date = 01/23/13 
 Pct Recovery = 153%  Analysis Date = 01/23/13 
 Pct Recovery = 153%  Analysis Date = 01/21/13 
 Pct Recovery = 153%  Analysis Date = 01/21/13 
 Pct Recovery = 153%  Analysis Date = 01/19/13 
 Pct Recovery = 153%  Analysis Date = 01/19/13 
 Pct Recovery = 153%  Analysis Date = 01/16/13 
 Pct Recovery = 153%  Analysis Date = 01/16/13 
 Pct Recovery = 153%  Analysis Date = 01/14/13 
 Pct Recovery = 153%  Analysis Date = 01/14/13 
 Pct Recovery = 153%  Analysis Date = 01/11/13 
 Pct Recovery = 153%  Analysis Date = 01/11/13 
 Pct Recovery = 153%  Analysis Date = 01/09/13 
 Pct Recovery = 153%  Analysis Date = 01/09/13 
 Pct Recovery = 153%  Analysis Date = 01/07/13 
 Pct Recovery = 154%  Analysis Date = 01/07/13 
 Pct Recovery = 154%  Analysis Date = 01/04/13 
 Pct Recovery = 154%  Analysis Date = 01/04/13 
 Pct Recovery = 154%  Analysis Date = 01/02/13 
 Pct Recovery = 154%  Analysis Date = 01/02/13 
 Pct Recovery = 154%  Analysis Date = 12/30/12 
 Pct Recovery = 154%  Analysis Date = 12/30/12 
 Pct Recovery = 154%  Analysis Date = 12/28/12 
 Pct Recovery = 154%  Analysis Date = 12/28/12 
 Pct Recovery = 154%  Analysis Date = 12/26/12 
 Pct Recovery = 154%  Analysis Date = 12/26/12 
 Pct Recovery = 154%  Analysis Date = 12/23/12 
 Pct Recovery = 154%  Analysis Date = 12/23/12 
 Pct Recovery = 154%  Analysis Date = 12/21/12 
 Pct Recovery = 154%  Analysis Date = 12/21/12 
 Pct Recovery = 154%  Analysis Date = 12/18/12 
 Pct Recovery = 154%  Analysis Date = 12/18/12 
 Pct Recovery = 154%  Analysis Date = 12/16/12 
 Pct Recovery = 154%  Analysis Date = 12/16/12 
 Pct Recovery = 154%  Analysis Date = 12/14/12 
 Pct Recovery = 154%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENCICLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 110% 44% 98% 22%
Total 14 110% 44% 98% 22%

Sample Statistics
PENCICLOVIR

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PENTOXIFYLLINE
METHOD: LC9017 , TESTIDCODE: 67480LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 74%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 174%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 76%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 92%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 50%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 55%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 83%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 79%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 91%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 51%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 60%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 56%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 103%  Analysis Date = 04/09/14 
 Pct Recovery = 44%  Analysis Date = 04/07/14 
 Pct Recovery = 44%  Analysis Date = 04/07/14 
 Pct Recovery = 44%  Analysis Date = 04/05/14 
 Pct Recovery = 44%  Analysis Date = 04/05/14 
 Pct Recovery = 44%  Analysis Date = 04/02/14 
 Pct Recovery = 45%  Analysis Date = 04/02/14 
 Pct Recovery = 45%  Analysis Date = 03/31/14 
 Pct Recovery = 45%  Analysis Date = 03/31/14 
 Pct Recovery = 45%  Analysis Date = 03/28/14 
 Pct Recovery = 45%  Analysis Date = 03/28/14 
 Pct Recovery = 45%  Analysis Date = 03/26/14 
 Pct Recovery = 45%  Analysis Date = 03/26/14 
 Pct Recovery = 45%  Analysis Date = 03/24/14 
 Pct Recovery = 46%  Analysis Date = 03/24/14 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 Pct Recovery = 46%  Analysis Date = 03/19/14 
 Pct Recovery = 46%  Analysis Date = 03/19/14 
 Pct Recovery = 46%  Analysis Date = 03/16/14 
 Pct Recovery = 46%  Analysis Date = 03/16/14 
 Pct Recovery = 46%  Analysis Date = 03/14/14 
 Pct Recovery = 46%  Analysis Date = 03/14/14 
 Pct Recovery = 46%  Analysis Date = 03/12/14 
 Pct Recovery = 47%  Analysis Date = 03/12/14 
 Pct Recovery = 47%  Analysis Date = 03/09/14 
 Pct Recovery = 47%  Analysis Date = 03/09/14 
 Pct Recovery = 47%  Analysis Date = 03/07/14 
 Pct Recovery = 47%  Analysis Date = 03/07/14 
 Pct Recovery = 47%  Analysis Date = 03/04/14 
 Pct Recovery = 47%  Analysis Date = 03/04/14 
 Pct Recovery = 47%  Analysis Date = 03/02/14 
 Pct Recovery = 47%  Analysis Date = 03/02/14 
 Pct Recovery = 47%  Analysis Date = 02/28/14 
 Pct Recovery = 48%  Analysis Date = 02/28/14 
 Pct Recovery = 48%  Analysis Date = 02/25/14 
 Pct Recovery = 48%  Analysis Date = 02/25/14 
 Pct Recovery = 48%  Analysis Date = 02/23/14 
 Pct Recovery = 48%  Analysis Date = 02/23/14 
 Pct Recovery = 48%  Analysis Date = 02/20/14 
 Pct Recovery = 48%  Analysis Date = 02/20/14 
 Pct Recovery = 48%  Analysis Date = 02/18/14 
 Pct Recovery = 48%  Analysis Date = 02/18/14 
 Pct Recovery = 48%  Analysis Date = 02/15/14 
 Pct Recovery = 49%  Analysis Date = 02/15/14 
 Pct Recovery = 49%  Analysis Date = 02/13/14 
 Pct Recovery = 49%  Analysis Date = 02/13/14 
 Pct Recovery = 49%  Analysis Date = 02/11/14 
 Pct Recovery = 49%  Analysis Date = 02/11/14 
 Pct Recovery = 49%  Analysis Date = 02/08/14 
 Pct Recovery = 49%  Analysis Date = 02/08/14 
 Pct Recovery = 49%  Analysis Date = 02/06/14 
 Pct Recovery = 49%  Analysis Date = 02/06/14 
 Pct Recovery = 49%  Analysis Date = 02/03/14 
 Pct Recovery = 50%  Analysis Date = 02/03/14 
 Pct Recovery = 50%  Analysis Date = 02/01/14 
 Pct Recovery = 50%  Analysis Date = 02/01/14 
 Pct Recovery = 50%  Analysis Date = 01/30/14 
 Pct Recovery = 50%  Analysis Date = 01/30/14 
 Pct Recovery = 50%  Analysis Date = 01/27/14 
 Pct Recovery = 50%  Analysis Date = 01/27/14 
 Pct Recovery = 50%  Analysis Date = 01/25/14 
 Pct Recovery = 50%  Analysis Date = 01/25/14 
 Pct Recovery = 50%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/22/14 
 Pct Recovery = 51%  Analysis Date = 01/20/14 
 Pct Recovery = 51%  Analysis Date = 01/20/14 
 Pct Recovery = 51%  Analysis Date = 01/18/14 
 Pct Recovery = 51%  Analysis Date = 01/18/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/15/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/13/14 
 Pct Recovery = 51%  Analysis Date = 01/10/14 
 Pct Recovery = 52%  Analysis Date = 01/10/14 
 Pct Recovery = 52%  Analysis Date = 01/08/14 
 Pct Recovery = 52%  Analysis Date = 01/08/14 
 Pct Recovery = 52%  Analysis Date = 01/06/14 
 Pct Recovery = 52%  Analysis Date = 01/06/14 
 Pct Recovery = 52%  Analysis Date = 01/03/14 
 Pct Recovery = 52%  Analysis Date = 01/03/14 
 Pct Recovery = 52%  Analysis Date = 01/01/14 
 Pct Recovery = 52%  Analysis Date = 01/01/14 
 Pct Recovery = 52%  Analysis Date = 12/29/13 
 Pct Recovery = 52%  Analysis Date = 12/29/13 
 Pct Recovery = 52%  Analysis Date = 12/27/13 
 Pct Recovery = 53%  Analysis Date = 12/27/13 
 Pct Recovery = 53%  Analysis Date = 12/24/13 
 Pct Recovery = 53%  Analysis Date = 12/24/13 
 Pct Recovery = 53%  Analysis Date = 12/22/13 
 Pct Recovery = 53%  Analysis Date = 12/22/13 
 Pct Recovery = 53%  Analysis Date = 12/20/13 
 Pct Recovery = 53%  Analysis Date = 12/20/13 
 Pct Recovery = 53%  Analysis Date = 12/17/13 
 Pct Recovery = 53%  Analysis Date = 12/17/13 
 Pct Recovery = 53%  Analysis Date = 12/15/13 
 Pct Recovery = 53%  Analysis Date = 12/15/13 
 Pct Recovery = 53%  Analysis Date = 12/12/13 
 Pct Recovery = 54%  Analysis Date = 12/12/13 
 Pct Recovery = 54%  Analysis Date = 12/10/13 
 Pct Recovery = 54%  Analysis Date = 12/10/13 
 Pct Recovery = 54%  Analysis Date = 12/08/13 
 Pct Recovery = 54%  Analysis Date = 12/08/13 
 Pct Recovery = 54%  Analysis Date = 12/05/13 
 Pct Recovery = 54%  Analysis Date = 12/05/13 
 Pct Recovery = 54%  Analysis Date = 12/03/13 
 Pct Recovery = 54%  Analysis Date = 12/03/13 
 Pct Recovery = 54%  Analysis Date = 11/30/13 
 Pct Recovery = 54%  Analysis Date = 11/30/13 
 Pct Recovery = 54%  Analysis Date = 11/28/13 
 Pct Recovery = 55%  Analysis Date = 11/28/13 
 Pct Recovery = 55%  Analysis Date = 11/26/13 
 Pct Recovery = 55%  Analysis Date = 11/26/13 
 Pct Recovery = 55%  Analysis Date = 11/23/13 
 Pct Recovery = 55%  Analysis Date = 11/23/13 
 Pct Recovery = 55%  Analysis Date = 11/21/13 
 Pct Recovery = 55%  Analysis Date = 11/21/13 
 Pct Recovery = 55%  Analysis Date = 11/18/13 
 Pct Recovery = 55%  Analysis Date = 11/18/13 
 Pct Recovery = 55%  Analysis Date = 11/16/13 
 Pct Recovery = 55%  Analysis Date = 11/16/13 
 Pct Recovery = 55%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/13/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/11/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/09/13 
 Pct Recovery = 56%  Analysis Date = 11/06/13 
 Pct Recovery = 56%  Analysis Date = 11/06/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/01/13 
 Pct Recovery = 56%  Analysis Date = 11/01/13 
 Pct Recovery = 56%  Analysis Date = 10/30/13 
 Pct Recovery = 56%  Analysis Date = 10/30/13 
 Pct Recovery = 56%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/28/13 
 Pct Recovery = 57%  Analysis Date = 10/25/13 
 Pct Recovery = 57%  Analysis Date = 10/25/13 
 Pct Recovery = 57%  Analysis Date = 10/23/13 
 Pct Recovery = 57%  Analysis Date = 10/23/13 
 Pct Recovery = 57%  Analysis Date = 10/20/13 
 Pct Recovery = 57%  Analysis Date = 10/20/13 
 Pct Recovery = 57%  Analysis Date = 10/18/13 
 Pct Recovery = 57%  Analysis Date = 10/18/13 
 Pct Recovery = 57%  Analysis Date = 10/16/13 
 Pct Recovery = 58%  Analysis Date = 10/16/13 
 Pct Recovery = 58%  Analysis Date = 10/13/13 
 Pct Recovery = 58%  Analysis Date = 10/13/13 
 Pct Recovery = 58%  Analysis Date = 10/11/13 
 Pct Recovery = 58%  Analysis Date = 10/11/13 
 Pct Recovery = 58%  Analysis Date = 10/08/13 
 Pct Recovery = 58%  Analysis Date = 10/08/13 
 Pct Recovery = 58%  Analysis Date = 10/06/13 
 Pct Recovery = 58%  Analysis Date = 10/06/13 
 Pct Recovery = 58%  Analysis Date = 10/04/13 
 Pct Recovery = 59%  Analysis Date = 10/04/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 10/01/13 
 Pct Recovery = 59%  Analysis Date = 09/29/13 
 Pct Recovery = 59%  Analysis Date = 09/29/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/26/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/24/13 
 Pct Recovery = 59%  Analysis Date = 09/21/13 
 Pct Recovery = 60%  Analysis Date = 09/21/13 
 Pct Recovery = 60%  Analysis Date = 09/19/13 
 Pct Recovery = 60%  Analysis Date = 09/19/13 
 Pct Recovery = 60%  Analysis Date = 09/17/13 
 Pct Recovery = 60%  Analysis Date = 09/17/13 
 Pct Recovery = 60%  Analysis Date = 09/14/13 
 Pct Recovery = 60%  Analysis Date = 09/14/13 
 Pct Recovery = 60%  Analysis Date = 09/12/13 
 Pct Recovery = 60%  Analysis Date = 09/12/13 
 Pct Recovery = 60%  Analysis Date = 09/09/13 
 Pct Recovery = 61%  Analysis Date = 09/09/13 
 Pct Recovery = 61%  Analysis Date = 09/07/13 
 Pct Recovery = 61%  Analysis Date = 09/07/13 
 Pct Recovery = 61%  Analysis Date = 09/05/13 
 Pct Recovery = 61%  Analysis Date = 09/05/13 
 Pct Recovery = 61%  Analysis Date = 09/02/13 
 Pct Recovery = 61%  Analysis Date = 09/02/13 
 Pct Recovery = 61%  Analysis Date = 08/31/13 
 Pct Recovery = 61%  Analysis Date = 08/31/13 
 Pct Recovery = 61%  Analysis Date = 08/28/13 
 Pct Recovery = 62%  Analysis Date = 08/28/13 
 Pct Recovery = 62%  Analysis Date = 08/26/13 
 Pct Recovery = 62%  Analysis Date = 08/26/13 
 Pct Recovery = 62%  Analysis Date = 08/24/13 
 Pct Recovery = 62%  Analysis Date = 08/24/13 
 Pct Recovery = 62%  Analysis Date = 08/21/13 
 Pct Recovery = 62%  Analysis Date = 08/21/13 
 Pct Recovery = 62%  Analysis Date = 08/19/13 
 Pct Recovery = 62%  Analysis Date = 08/19/13 
 Pct Recovery = 62%  Analysis Date = 08/16/13 
 Pct Recovery = 63%  Analysis Date = 08/16/13 
 Pct Recovery = 63%  Analysis Date = 08/14/13 
 Pct Recovery = 63%  Analysis Date = 08/14/13 
 Pct Recovery = 63%  Analysis Date = 08/11/13 
 Pct Recovery = 63%  Analysis Date = 08/11/13 
 Pct Recovery = 63%  Analysis Date = 08/09/13 
 Pct Recovery = 64%  Analysis Date = 08/09/13 
 Pct Recovery = 64%  Analysis Date = 08/07/13 
 Pct Recovery = 64%  Analysis Date = 08/07/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/04/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 Pct Recovery = 64%  Analysis Date = 07/30/13 
 Pct Recovery = 65%  Analysis Date = 07/30/13 
 Pct Recovery = 65%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/28/13 
 Pct Recovery = 65%  Analysis Date = 07/26/13 
 Pct Recovery = 65%  Analysis Date = 07/26/13 
 Pct Recovery = 65%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/18/13 
 Pct Recovery = 66%  Analysis Date = 07/18/13 
 Pct Recovery = 66%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 67%  Analysis Date = 07/06/13 
 Pct Recovery = 68%  Analysis Date = 07/06/13 
 Pct Recovery = 68%  Analysis Date = 07/04/13 
 Pct Recovery = 68%  Analysis Date = 07/04/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 07/02/13 
 Pct Recovery = 68%  Analysis Date = 06/29/13 
 Pct Recovery = 69%  Analysis Date = 06/29/13 
 Pct Recovery = 69%  Analysis Date = 06/27/13 
 Pct Recovery = 69%  Analysis Date = 06/27/13 
 Pct Recovery = 69%  Analysis Date = 06/24/13 
 Pct Recovery = 69%  Analysis Date = 06/24/13 
 Pct Recovery = 69%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 70%  Analysis Date = 06/17/13 
 Pct Recovery = 70%  Analysis Date = 06/17/13 
 Pct Recovery = 70%  Analysis Date = 06/15/13 
 Pct Recovery = 71%  Analysis Date = 06/15/13 
 Pct Recovery = 71%  Analysis Date = 06/12/13 
 Pct Recovery = 71%  Analysis Date = 06/12/13 
 Pct Recovery = 71%  Analysis Date = 06/10/13 
 Pct Recovery = 71%  Analysis Date = 06/10/13 
 Pct Recovery = 71%  Analysis Date = 06/07/13 
 Pct Recovery = 71%  Analysis Date = 06/07/13 
 Pct Recovery = 71%  Analysis Date = 06/05/13 
 Pct Recovery = 72%  Analysis Date = 06/05/13 
 Pct Recovery = 72%  Analysis Date = 06/03/13 
 Pct Recovery = 72%  Analysis Date = 06/03/13 
 Pct Recovery = 72%  Analysis Date = 05/31/13 
 Pct Recovery = 72%  Analysis Date = 05/31/13 
 Pct Recovery = 72%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/29/13 
 Pct Recovery = 73%  Analysis Date = 05/26/13 
 Pct Recovery = 73%  Analysis Date = 05/26/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/24/13 
 Pct Recovery = 73%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/19/13 
 Pct Recovery = 74%  Analysis Date = 05/19/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/17/13 
 Pct Recovery = 74%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/07/13 
 Pct Recovery = 75%  Analysis Date = 05/07/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 Pct Recovery = 76%  Analysis Date = 04/30/13 
 Pct Recovery = 76%  Analysis Date = 04/30/13 
 Pct Recovery = 76%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/23/13 
 Pct Recovery = 79%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 81%  Analysis Date = 04/18/13 
 Pct Recovery = 81%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 84%  Analysis Date = 04/13/13 
 Pct Recovery = 84%  Analysis Date = 04/11/13 
 Pct Recovery = 85%  Analysis Date = 04/11/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/03/13 
 Pct Recovery = 89%  Analysis Date = 04/03/13 
 Pct Recovery = 89%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/20/13 
 Pct Recovery = 95%  Analysis Date = 03/20/13 
 Pct Recovery = 95%  Analysis Date = 03/17/13 
 Pct Recovery = 96%  Analysis Date = 03/17/13 
 Pct Recovery = 96%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/13/13 
 Pct Recovery = 98%  Analysis Date = 03/13/13 
 Pct Recovery = 98%  Analysis Date = 03/10/13 
 Pct Recovery = 99%  Analysis Date = 03/10/13 
 Pct Recovery = 99%  Analysis Date = 03/08/13 
 Pct Recovery = 100%  Analysis Date = 03/08/13 
 Pct Recovery = 100%  Analysis Date = 03/05/13 
 Pct Recovery = 101%  Analysis Date = 03/05/13 
 Pct Recovery = 101%  Analysis Date = 03/03/13 
 Pct Recovery = 102%  Analysis Date = 03/03/13 
 Pct Recovery = 102%  Analysis Date = 03/01/13 
 Pct Recovery = 103%  Analysis Date = 03/01/13 
 Pct Recovery = 103%  Analysis Date = 02/26/13 
 Pct Recovery = 104%  Analysis Date = 02/26/13 
 Pct Recovery = 104%  Analysis Date = 02/24/13 
 Pct Recovery = 105%  Analysis Date = 02/24/13 
 Pct Recovery = 105%  Analysis Date = 02/21/13 
 Pct Recovery = 106%  Analysis Date = 02/21/13 
 Pct Recovery = 106%  Analysis Date = 02/19/13 
 Pct Recovery = 106%  Analysis Date = 02/19/13 
 Pct Recovery = 106%  Analysis Date = 02/17/13 
 Pct Recovery = 107%  Analysis Date = 02/17/13 
 Pct Recovery = 107%  Analysis Date = 02/14/13 
 Pct Recovery = 108%  Analysis Date = 02/14/13 
 Pct Recovery = 108%  Analysis Date = 02/12/13 
 Pct Recovery = 109%  Analysis Date = 02/12/13 
 Pct Recovery = 109%  Analysis Date = 02/09/13 
 Pct Recovery = 110%  Analysis Date = 02/09/13 
 Pct Recovery = 110%  Analysis Date = 02/07/13 
 Pct Recovery = 111%  Analysis Date = 02/07/13 
 Pct Recovery = 111%  Analysis Date = 02/05/13 
 Pct Recovery = 112%  Analysis Date = 02/05/13 
 Pct Recovery = 112%  Analysis Date = 02/02/13 
 Pct Recovery = 113%  Analysis Date = 02/02/13 
 Pct Recovery = 113%  Analysis Date = 01/31/13 
 Pct Recovery = 114%  Analysis Date = 01/31/13 
 Pct Recovery = 114%  Analysis Date = 01/28/13 
 Pct Recovery = 115%  Analysis Date = 01/28/13 
 Pct Recovery = 115%  Analysis Date = 01/26/13 
 Pct Recovery = 116%  Analysis Date = 01/26/13 
 Pct Recovery = 116%  Analysis Date = 01/23/13 
 Pct Recovery = 117%  Analysis Date = 01/23/13 
 Pct Recovery = 117%  Analysis Date = 01/21/13 
 Pct Recovery = 117%  Analysis Date = 01/21/13 
 Pct Recovery = 117%  Analysis Date = 01/19/13 
 Pct Recovery = 117%  Analysis Date = 01/19/13 
 Pct Recovery = 117%  Analysis Date = 01/16/13 
 Pct Recovery = 117%  Analysis Date = 01/16/13 
 Pct Recovery = 117%  Analysis Date = 01/14/13 
 Pct Recovery = 118%  Analysis Date = 01/14/13 
 Pct Recovery = 118%  Analysis Date = 01/11/13 
 Pct Recovery = 118%  Analysis Date = 01/11/13 
 Pct Recovery = 118%  Analysis Date = 01/09/13 
 Pct Recovery = 118%  Analysis Date = 01/09/13 
 Pct Recovery = 118%  Analysis Date = 01/07/13 
 Pct Recovery = 118%  Analysis Date = 01/07/13 
 Pct Recovery = 118%  Analysis Date = 01/04/13 
 Pct Recovery = 118%  Analysis Date = 01/04/13 
 Pct Recovery = 118%  Analysis Date = 01/02/13 
 Pct Recovery = 119%  Analysis Date = 01/02/13 
 Pct Recovery = 119%  Analysis Date = 12/30/12 
 Pct Recovery = 119%  Analysis Date = 12/30/12 
 Pct Recovery = 119%  Analysis Date = 12/28/12 
 Pct Recovery = 119%  Analysis Date = 12/28/12 
 Pct Recovery = 119%  Analysis Date = 12/26/12 
 Pct Recovery = 119%  Analysis Date = 12/26/12 
 Pct Recovery = 119%  Analysis Date = 12/23/12 
 Pct Recovery = 119%  Analysis Date = 12/23/12 
 Pct Recovery = 119%  Analysis Date = 12/21/12 
 Pct Recovery = 120%  Analysis Date = 12/21/12 
 Pct Recovery = 120%  Analysis Date = 12/18/12 
 Pct Recovery = 120%  Analysis Date = 12/18/12 
 Pct Recovery = 120%  Analysis Date = 12/16/12 
 Pct Recovery = 120%  Analysis Date = 12/16/12 
 Pct Recovery = 120%  Analysis Date = 12/14/12 
 Pct Recovery = 120%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENTOXIFYLLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 77% 34% 75% 26%
Total 14 77% 34% 75% 26%

Sample Statistics
PENTOXIFYLLINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 4 29% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PHENAZOPYRIDINE
METHOD: LC9017 , TESTIDCODE: 68008LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 86%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 97%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 86%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 187%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 47%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 96%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 94%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 70%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 87%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 60%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 93%  Analysis Date = 04/09/14 
 Pct Recovery = 69%  Analysis Date = 04/07/14 
 Pct Recovery = 69%  Analysis Date = 04/07/14 
 Pct Recovery = 69%  Analysis Date = 04/05/14 
 Pct Recovery = 69%  Analysis Date = 04/05/14 
 Pct Recovery = 69%  Analysis Date = 04/02/14 
 Pct Recovery = 69%  Analysis Date = 04/02/14 
 Pct Recovery = 69%  Analysis Date = 03/31/14 
 Pct Recovery = 69%  Analysis Date = 03/31/14 
 Pct Recovery = 69%  Analysis Date = 03/28/14 
 Pct Recovery = 69%  Analysis Date = 03/28/14 
 Pct Recovery = 69%  Analysis Date = 03/26/14 
 Pct Recovery = 69%  Analysis Date = 03/26/14 
 Pct Recovery = 69%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/24/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/21/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/19/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/12/14 
 Pct Recovery = 68%  Analysis Date = 03/12/14 
 Pct Recovery = 68%  Analysis Date = 03/09/14 
 Pct Recovery = 68%  Analysis Date = 03/09/14 
 Pct Recovery = 68%  Analysis Date = 03/07/14 
 Pct Recovery = 68%  Analysis Date = 03/07/14 
 Pct Recovery = 68%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 02/28/14 
 Pct Recovery = 68%  Analysis Date = 02/28/14 
 Pct Recovery = 68%  Analysis Date = 02/25/14 
 Pct Recovery = 68%  Analysis Date = 02/25/14 
 Pct Recovery = 68%  Analysis Date = 02/23/14 
 Pct Recovery = 68%  Analysis Date = 02/23/14 
 Pct Recovery = 68%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/11/14 
 Pct Recovery = 68%  Analysis Date = 02/11/14 
 Pct Recovery = 68%  Analysis Date = 02/08/14 
 Pct Recovery = 68%  Analysis Date = 02/08/14 
 Pct Recovery = 68%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/06/14 
 Pct Recovery = 68%  Analysis Date = 02/03/14 
 Pct Recovery = 68%  Analysis Date = 02/03/14 
 Pct Recovery = 68%  Analysis Date = 02/01/14 
 Pct Recovery = 68%  Analysis Date = 02/01/14 
 Pct Recovery = 68%  Analysis Date = 01/30/14 
 Pct Recovery = 68%  Analysis Date = 01/30/14 
 Pct Recovery = 68%  Analysis Date = 01/27/14 
 Pct Recovery = 68%  Analysis Date = 01/27/14 
 Pct Recovery = 68%  Analysis Date = 01/25/14 
 Pct Recovery = 68%  Analysis Date = 01/25/14 
 Pct Recovery = 68%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/22/14 
 Pct Recovery = 68%  Analysis Date = 01/20/14 
 Pct Recovery = 68%  Analysis Date = 01/20/14 
 Pct Recovery = 68%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/18/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/15/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/13/14 
 Pct Recovery = 68%  Analysis Date = 01/10/14 
 Pct Recovery = 68%  Analysis Date = 01/10/14 
 Pct Recovery = 68%  Analysis Date = 01/08/14 
 Pct Recovery = 68%  Analysis Date = 01/08/14 
 Pct Recovery = 68%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/06/14 
 Pct Recovery = 68%  Analysis Date = 01/03/14 
 Pct Recovery = 68%  Analysis Date = 01/03/14 
 Pct Recovery = 68%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 67%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/24/13 
 Pct Recovery = 67%  Analysis Date = 12/24/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/17/13 
 Pct Recovery = 67%  Analysis Date = 12/17/13 
 Pct Recovery = 67%  Analysis Date = 12/15/13 
 Pct Recovery = 67%  Analysis Date = 12/15/13 
 Pct Recovery = 67%  Analysis Date = 12/12/13 
 Pct Recovery = 67%  Analysis Date = 12/12/13 
 Pct Recovery = 67%  Analysis Date = 12/10/13 
 Pct Recovery = 67%  Analysis Date = 12/10/13 
 Pct Recovery = 67%  Analysis Date = 12/08/13 
 Pct Recovery = 67%  Analysis Date = 12/08/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/03/13 
 Pct Recovery = 66%  Analysis Date = 12/03/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/30/13 
 Pct Recovery = 66%  Analysis Date = 11/28/13 
 Pct Recovery = 66%  Analysis Date = 11/28/13 
 Pct Recovery = 66%  Analysis Date = 11/26/13 
 Pct Recovery = 66%  Analysis Date = 11/26/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/23/13 
 Pct Recovery = 66%  Analysis Date = 11/21/13 
 Pct Recovery = 66%  Analysis Date = 11/21/13 
 Pct Recovery = 66%  Analysis Date = 11/18/13 
 Pct Recovery = 66%  Analysis Date = 11/18/13 
 Pct Recovery = 66%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/16/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/09/13 
 Pct Recovery = 66%  Analysis Date = 11/09/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 65%  Analysis Date = 11/04/13 
 Pct Recovery = 65%  Analysis Date = 11/01/13 
 Pct Recovery = 65%  Analysis Date = 11/01/13 
 Pct Recovery = 65%  Analysis Date = 10/30/13 
 Pct Recovery = 65%  Analysis Date = 10/30/13 
 Pct Recovery = 65%  Analysis Date = 10/28/13 
 Pct Recovery = 65%  Analysis Date = 10/28/13 
 Pct Recovery = 65%  Analysis Date = 10/25/13 
 Pct Recovery = 65%  Analysis Date = 10/25/13 
 Pct Recovery = 65%  Analysis Date = 10/23/13 
 Pct Recovery = 66%  Analysis Date = 10/23/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/13/13 
 Pct Recovery = 66%  Analysis Date = 10/13/13 
 Pct Recovery = 66%  Analysis Date = 10/11/13 
 Pct Recovery = 66%  Analysis Date = 10/11/13 
 Pct Recovery = 66%  Analysis Date = 10/08/13 
 Pct Recovery = 66%  Analysis Date = 10/08/13 
 Pct Recovery = 66%  Analysis Date = 10/06/13 
 Pct Recovery = 66%  Analysis Date = 10/06/13 
 Pct Recovery = 66%  Analysis Date = 10/04/13 
 Pct Recovery = 66%  Analysis Date = 10/04/13 
 Pct Recovery = 66%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 09/29/13 
 Pct Recovery = 67%  Analysis Date = 09/29/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/14/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/12/13 
 Pct Recovery = 67%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/07/13 
 Pct Recovery = 68%  Analysis Date = 09/07/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/02/13 
 Pct Recovery = 68%  Analysis Date = 09/02/13 
 Pct Recovery = 68%  Analysis Date = 08/31/13 
 Pct Recovery = 68%  Analysis Date = 08/31/13 
 Pct Recovery = 68%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/24/13 
 Pct Recovery = 68%  Analysis Date = 08/24/13 
 Pct Recovery = 68%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/11/13 
 Pct Recovery = 70%  Analysis Date = 08/09/13 
 Pct Recovery = 70%  Analysis Date = 08/09/13 
 Pct Recovery = 70%  Analysis Date = 08/07/13 
 Pct Recovery = 70%  Analysis Date = 08/07/13 
 Pct Recovery = 70%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/04/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 08/02/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 72%  Analysis Date = 07/28/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/26/13 
 Pct Recovery = 72%  Analysis Date = 07/23/13 
 Pct Recovery = 72%  Analysis Date = 07/23/13 
 Pct Recovery = 72%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/21/13 
 Pct Recovery = 73%  Analysis Date = 07/18/13 
 Pct Recovery = 73%  Analysis Date = 07/18/13 
 Pct Recovery = 73%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/04/13 
 Pct Recovery = 75%  Analysis Date = 07/04/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/24/13 
 Pct Recovery = 77%  Analysis Date = 06/24/13 
 Pct Recovery = 77%  Analysis Date = 06/22/13 
 Pct Recovery = 77%  Analysis Date = 06/22/13 
 Pct Recovery = 77%  Analysis Date = 06/19/13 
 Pct Recovery = 77%  Analysis Date = 06/19/13 
 Pct Recovery = 77%  Analysis Date = 06/17/13 
 Pct Recovery = 78%  Analysis Date = 06/17/13 
 Pct Recovery = 78%  Analysis Date = 06/15/13 
 Pct Recovery = 78%  Analysis Date = 06/15/13 
 Pct Recovery = 78%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/10/13 
 Pct Recovery = 79%  Analysis Date = 06/10/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 05/31/13 
 Pct Recovery = 80%  Analysis Date = 05/31/13 
 Pct Recovery = 80%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/29/13 
 Pct Recovery = 81%  Analysis Date = 05/26/13 
 Pct Recovery = 81%  Analysis Date = 05/26/13 
 Pct Recovery = 81%  Analysis Date = 05/24/13 
 Pct Recovery = 81%  Analysis Date = 05/24/13 
 Pct Recovery = 81%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 83%  Analysis Date = 05/14/13 
 Pct Recovery = 83%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/07/13 
 Pct Recovery = 84%  Analysis Date = 05/07/13 
 Pct Recovery = 84%  Analysis Date = 05/05/13 
 Pct Recovery = 84%  Analysis Date = 05/05/13 
 Pct Recovery = 84%  Analysis Date = 05/02/13 
 Pct Recovery = 85%  Analysis Date = 05/02/13 
 Pct Recovery = 85%  Analysis Date = 04/30/13 
 Pct Recovery = 85%  Analysis Date = 04/30/13 
 Pct Recovery = 85%  Analysis Date = 04/27/13 
 Pct Recovery = 86%  Analysis Date = 04/27/13 
 Pct Recovery = 86%  Analysis Date = 04/25/13 
 Pct Recovery = 88%  Analysis Date = 04/25/13 
 Pct Recovery = 88%  Analysis Date = 04/23/13 
 Pct Recovery = 89%  Analysis Date = 04/23/13 
 Pct Recovery = 89%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/18/13 
 Pct Recovery = 91%  Analysis Date = 04/18/13 
 Pct Recovery = 91%  Analysis Date = 04/15/13 
 Pct Recovery = 92%  Analysis Date = 04/15/13 
 Pct Recovery = 92%  Analysis Date = 04/13/13 
 Pct Recovery = 93%  Analysis Date = 04/13/13 
 Pct Recovery = 93%  Analysis Date = 04/11/13 
 Pct Recovery = 94%  Analysis Date = 04/11/13 
 Pct Recovery = 94%  Analysis Date = 04/08/13 
 Pct Recovery = 95%  Analysis Date = 04/08/13 
 Pct Recovery = 95%  Analysis Date = 04/06/13 
 Pct Recovery = 96%  Analysis Date = 04/06/13 
 Pct Recovery = 96%  Analysis Date = 04/03/13 
 Pct Recovery = 97%  Analysis Date = 04/03/13 
 Pct Recovery = 97%  Analysis Date = 04/01/13 
 Pct Recovery = 98%  Analysis Date = 04/01/13 
 Pct Recovery = 98%  Analysis Date = 03/30/13 
 Pct Recovery = 99%  Analysis Date = 03/30/13 
 Pct Recovery = 99%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/27/13 
 Pct Recovery = 100%  Analysis Date = 03/25/13 
 Pct Recovery = 101%  Analysis Date = 03/25/13 
 Pct Recovery = 101%  Analysis Date = 03/22/13 
 Pct Recovery = 102%  Analysis Date = 03/22/13 
 Pct Recovery = 102%  Analysis Date = 03/20/13 
 Pct Recovery = 102%  Analysis Date = 03/20/13 
 Pct Recovery = 102%  Analysis Date = 03/17/13 
 Pct Recovery = 103%  Analysis Date = 03/17/13 
 Pct Recovery = 103%  Analysis Date = 03/15/13 
 Pct Recovery = 104%  Analysis Date = 03/15/13 
 Pct Recovery = 104%  Analysis Date = 03/13/13 
 Pct Recovery = 105%  Analysis Date = 03/13/13 
 Pct Recovery = 105%  Analysis Date = 03/10/13 
 Pct Recovery = 105%  Analysis Date = 03/10/13 
 Pct Recovery = 105%  Analysis Date = 03/08/13 
 Pct Recovery = 106%  Analysis Date = 03/08/13 
 Pct Recovery = 106%  Analysis Date = 03/05/13 
 Pct Recovery = 107%  Analysis Date = 03/05/13 
 Pct Recovery = 107%  Analysis Date = 03/03/13 
 Pct Recovery = 108%  Analysis Date = 03/03/13 
 Pct Recovery = 108%  Analysis Date = 03/01/13 
 Pct Recovery = 109%  Analysis Date = 03/01/13 
 Pct Recovery = 109%  Analysis Date = 02/26/13 
 Pct Recovery = 109%  Analysis Date = 02/26/13 
 Pct Recovery = 109%  Analysis Date = 02/24/13 
 Pct Recovery = 110%  Analysis Date = 02/24/13 
 Pct Recovery = 110%  Analysis Date = 02/21/13 
 Pct Recovery = 111%  Analysis Date = 02/21/13 
 Pct Recovery = 111%  Analysis Date = 02/19/13 
 Pct Recovery = 112%  Analysis Date = 02/19/13 
 Pct Recovery = 112%  Analysis Date = 02/17/13 
 Pct Recovery = 113%  Analysis Date = 02/17/13 
 Pct Recovery = 113%  Analysis Date = 02/14/13 
 Pct Recovery = 113%  Analysis Date = 02/14/13 
 Pct Recovery = 113%  Analysis Date = 02/12/13 
 Pct Recovery = 114%  Analysis Date = 02/12/13 
 Pct Recovery = 114%  Analysis Date = 02/09/13 
 Pct Recovery = 115%  Analysis Date = 02/09/13 
 Pct Recovery = 115%  Analysis Date = 02/07/13 
 Pct Recovery = 116%  Analysis Date = 02/07/13 
 Pct Recovery = 116%  Analysis Date = 02/05/13 
 Pct Recovery = 116%  Analysis Date = 02/05/13 
 Pct Recovery = 116%  Analysis Date = 02/02/13 
 Pct Recovery = 117%  Analysis Date = 02/02/13 
 Pct Recovery = 117%  Analysis Date = 01/31/13 
 Pct Recovery = 118%  Analysis Date = 01/31/13 
 Pct Recovery = 118%  Analysis Date = 01/28/13 
 Pct Recovery = 119%  Analysis Date = 01/28/13 
 Pct Recovery = 119%  Analysis Date = 01/26/13 
 Pct Recovery = 120%  Analysis Date = 01/26/13 
 Pct Recovery = 120%  Analysis Date = 01/23/13 
 Pct Recovery = 120%  Analysis Date = 01/23/13 
 Pct Recovery = 120%  Analysis Date = 01/21/13 
 Pct Recovery = 120%  Analysis Date = 01/21/13 
 Pct Recovery = 120%  Analysis Date = 01/19/13 
 Pct Recovery = 120%  Analysis Date = 01/19/13 
 Pct Recovery = 120%  Analysis Date = 01/16/13 
 Pct Recovery = 120%  Analysis Date = 01/16/13 
 Pct Recovery = 120%  Analysis Date = 01/14/13 
 Pct Recovery = 119%  Analysis Date = 01/14/13 
 Pct Recovery = 119%  Analysis Date = 01/11/13 
 Pct Recovery = 119%  Analysis Date = 01/11/13 
 Pct Recovery = 119%  Analysis Date = 01/09/13 
 Pct Recovery = 119%  Analysis Date = 01/09/13 
 Pct Recovery = 119%  Analysis Date = 01/07/13 
 Pct Recovery = 119%  Analysis Date = 01/07/13 
 Pct Recovery = 119%  Analysis Date = 01/04/13 
 Pct Recovery = 118%  Analysis Date = 01/04/13 
 Pct Recovery = 118%  Analysis Date = 01/02/13 
 Pct Recovery = 118%  Analysis Date = 01/02/13 
 Pct Recovery = 118%  Analysis Date = 12/30/12 
 Pct Recovery = 118%  Analysis Date = 12/30/12 
 Pct Recovery = 118%  Analysis Date = 12/28/12 
 Pct Recovery = 118%  Analysis Date = 12/28/12 
 Pct Recovery = 118%  Analysis Date = 12/26/12 
 Pct Recovery = 117%  Analysis Date = 12/26/12 
 Pct Recovery = 117%  Analysis Date = 12/23/12 
 Pct Recovery = 117%  Analysis Date = 12/23/12 
 Pct Recovery = 117%  Analysis Date = 12/21/12 
 Pct Recovery = 117%  Analysis Date = 12/21/12 
 Pct Recovery = 117%  Analysis Date = 12/18/12 
 Pct Recovery = 117%  Analysis Date = 12/18/12 
 Pct Recovery = 117%  Analysis Date = 12/16/12 
 Pct Recovery = 116%  Analysis Date = 12/16/12 
 Pct Recovery = 116%  Analysis Date = 12/14/12 
 Pct Recovery = 116%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHENAZOPYRIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 93% . 93% 0%
>= Reporting Level 12 87% 36% 86% 22%
Total 13 87% 34% 86% 19%

Sample Statistics
PHENAZOPYRIDINE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 5 36% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 1 7% 1 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PHENDIMETRAZINE
METHOD: LC9017 , TESTIDCODE: 67496LCM56

The SGPlot Procedure

Sample Statistics
PHENDIMETRAZINE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
PHENYTOIN
METHOD: LC9017 , TESTIDCODE: 67466LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 94%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 94%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 58%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 80%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 69%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 109%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 88%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 83%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 57%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 96%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 52%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 79%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 103%  Analysis Date = 04/09/14 
 Pct Recovery = 69%  Analysis Date = 04/07/14 
 Pct Recovery = 69%  Analysis Date = 04/07/14 
 Pct Recovery = 69%  Analysis Date = 04/05/14 
 Pct Recovery = 69%  Analysis Date = 04/05/14 
 Pct Recovery = 69%  Analysis Date = 04/02/14 
 Pct Recovery = 69%  Analysis Date = 04/02/14 
 Pct Recovery = 69%  Analysis Date = 03/31/14 
 Pct Recovery = 69%  Analysis Date = 03/31/14 
 Pct Recovery = 69%  Analysis Date = 03/28/14 
 Pct Recovery = 69%  Analysis Date = 03/28/14 
 Pct Recovery = 69%  Analysis Date = 03/26/14 
 Pct Recovery = 69%  Analysis Date = 03/26/14 
 Pct Recovery = 69%  Analysis Date = 03/24/14 
 Pct Recovery = 70%  Analysis Date = 03/24/14 
 Pct Recovery = 70%  Analysis Date = 03/21/14 
 Pct Recovery = 70%  Analysis Date = 03/21/14 
 Pct Recovery = 70%  Analysis Date = 03/19/14 
 Pct Recovery = 70%  Analysis Date = 03/19/14 
 Pct Recovery = 70%  Analysis Date = 03/16/14 
 Pct Recovery = 70%  Analysis Date = 03/16/14 
 Pct Recovery = 70%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/14/14 
 Pct Recovery = 70%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/12/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 71%  Analysis Date = 03/07/14 
 Pct Recovery = 71%  Analysis Date = 03/04/14 
 Pct Recovery = 71%  Analysis Date = 03/04/14 
 Pct Recovery = 71%  Analysis Date = 03/02/14 
 Pct Recovery = 71%  Analysis Date = 03/02/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/18/14 
 Pct Recovery = 71%  Analysis Date = 02/18/14 
 Pct Recovery = 71%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/03/14 
 Pct Recovery = 72%  Analysis Date = 02/03/14 
 Pct Recovery = 72%  Analysis Date = 02/01/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 73%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 74%  Analysis Date = 01/03/14 
 Pct Recovery = 74%  Analysis Date = 01/03/14 
 Pct Recovery = 74%  Analysis Date = 01/01/14 
 Pct Recovery = 74%  Analysis Date = 01/01/14 
 Pct Recovery = 74%  Analysis Date = 12/29/13 
 Pct Recovery = 74%  Analysis Date = 12/29/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/27/13 
 Pct Recovery = 74%  Analysis Date = 12/24/13 
 Pct Recovery = 74%  Analysis Date = 12/24/13 
 Pct Recovery = 74%  Analysis Date = 12/22/13 
 Pct Recovery = 75%  Analysis Date = 12/22/13 
 Pct Recovery = 75%  Analysis Date = 12/20/13 
 Pct Recovery = 75%  Analysis Date = 12/20/13 
 Pct Recovery = 75%  Analysis Date = 12/17/13 
 Pct Recovery = 75%  Analysis Date = 12/17/13 
 Pct Recovery = 75%  Analysis Date = 12/15/13 
 Pct Recovery = 75%  Analysis Date = 12/15/13 
 Pct Recovery = 75%  Analysis Date = 12/12/13 
 Pct Recovery = 75%  Analysis Date = 12/12/13 
 Pct Recovery = 75%  Analysis Date = 12/10/13 
 Pct Recovery = 75%  Analysis Date = 12/10/13 
 Pct Recovery = 75%  Analysis Date = 12/08/13 
 Pct Recovery = 75%  Analysis Date = 12/08/13 
 Pct Recovery = 75%  Analysis Date = 12/05/13 
 Pct Recovery = 75%  Analysis Date = 12/05/13 
 Pct Recovery = 75%  Analysis Date = 12/03/13 
 Pct Recovery = 75%  Analysis Date = 12/03/13 
 Pct Recovery = 75%  Analysis Date = 11/30/13 
 Pct Recovery = 75%  Analysis Date = 11/30/13 
 Pct Recovery = 75%  Analysis Date = 11/28/13 
 Pct Recovery = 75%  Analysis Date = 11/28/13 
 Pct Recovery = 75%  Analysis Date = 11/26/13 
 Pct Recovery = 75%  Analysis Date = 11/26/13 
 Pct Recovery = 75%  Analysis Date = 11/23/13 
 Pct Recovery = 74%  Analysis Date = 11/23/13 
 Pct Recovery = 74%  Analysis Date = 11/21/13 
 Pct Recovery = 74%  Analysis Date = 11/21/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/11/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/09/13 
 Pct Recovery = 72%  Analysis Date = 11/06/13 
 Pct Recovery = 72%  Analysis Date = 11/06/13 
 Pct Recovery = 72%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 70%  Analysis Date = 10/30/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/28/13 
 Pct Recovery = 70%  Analysis Date = 10/25/13 
 Pct Recovery = 70%  Analysis Date = 10/25/13 
 Pct Recovery = 70%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/16/13 
 Pct Recovery = 71%  Analysis Date = 10/16/13 
 Pct Recovery = 71%  Analysis Date = 10/13/13 
 Pct Recovery = 71%  Analysis Date = 10/13/13 
 Pct Recovery = 71%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/21/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/19/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/17/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 75%  Analysis Date = 09/09/13 
 Pct Recovery = 75%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/07/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/05/13 
 Pct Recovery = 75%  Analysis Date = 09/02/13 
 Pct Recovery = 75%  Analysis Date = 09/02/13 
 Pct Recovery = 75%  Analysis Date = 08/31/13 
 Pct Recovery = 76%  Analysis Date = 08/31/13 
 Pct Recovery = 76%  Analysis Date = 08/28/13 
 Pct Recovery = 76%  Analysis Date = 08/28/13 
 Pct Recovery = 76%  Analysis Date = 08/26/13 
 Pct Recovery = 76%  Analysis Date = 08/26/13 
 Pct Recovery = 76%  Analysis Date = 08/24/13 
 Pct Recovery = 76%  Analysis Date = 08/24/13 
 Pct Recovery = 76%  Analysis Date = 08/21/13 
 Pct Recovery = 77%  Analysis Date = 08/21/13 
 Pct Recovery = 77%  Analysis Date = 08/19/13 
 Pct Recovery = 77%  Analysis Date = 08/19/13 
 Pct Recovery = 77%  Analysis Date = 08/16/13 
 Pct Recovery = 77%  Analysis Date = 08/16/13 
 Pct Recovery = 77%  Analysis Date = 08/14/13 
 Pct Recovery = 77%  Analysis Date = 08/14/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 77%  Analysis Date = 08/11/13 
 Pct Recovery = 77%  Analysis Date = 08/09/13 
 Pct Recovery = 78%  Analysis Date = 08/09/13 
 Pct Recovery = 78%  Analysis Date = 08/07/13 
 Pct Recovery = 78%  Analysis Date = 08/07/13 
 Pct Recovery = 78%  Analysis Date = 08/04/13 
 Pct Recovery = 78%  Analysis Date = 08/04/13 
 Pct Recovery = 78%  Analysis Date = 08/02/13 
 Pct Recovery = 78%  Analysis Date = 08/02/13 
 Pct Recovery = 78%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/28/13 
 Pct Recovery = 79%  Analysis Date = 07/28/13 
 Pct Recovery = 79%  Analysis Date = 07/26/13 
 Pct Recovery = 79%  Analysis Date = 07/26/13 
 Pct Recovery = 79%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/23/13 
 Pct Recovery = 79%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 81%  Analysis Date = 07/14/13 
 Pct Recovery = 81%  Analysis Date = 07/11/13 
 Pct Recovery = 81%  Analysis Date = 07/11/13 
 Pct Recovery = 81%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/09/13 
 Pct Recovery = 81%  Analysis Date = 07/06/13 
 Pct Recovery = 81%  Analysis Date = 07/06/13 
 Pct Recovery = 81%  Analysis Date = 07/04/13 
 Pct Recovery = 82%  Analysis Date = 07/04/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 06/29/13 
 Pct Recovery = 82%  Analysis Date = 06/29/13 
 Pct Recovery = 82%  Analysis Date = 06/27/13 
 Pct Recovery = 83%  Analysis Date = 06/27/13 
 Pct Recovery = 83%  Analysis Date = 06/24/13 
 Pct Recovery = 83%  Analysis Date = 06/24/13 
 Pct Recovery = 83%  Analysis Date = 06/22/13 
 Pct Recovery = 83%  Analysis Date = 06/22/13 
 Pct Recovery = 83%  Analysis Date = 06/19/13 
 Pct Recovery = 83%  Analysis Date = 06/19/13 
 Pct Recovery = 83%  Analysis Date = 06/17/13 
 Pct Recovery = 84%  Analysis Date = 06/17/13 
 Pct Recovery = 84%  Analysis Date = 06/15/13 
 Pct Recovery = 84%  Analysis Date = 06/15/13 
 Pct Recovery = 84%  Analysis Date = 06/12/13 
 Pct Recovery = 84%  Analysis Date = 06/12/13 
 Pct Recovery = 84%  Analysis Date = 06/10/13 
 Pct Recovery = 85%  Analysis Date = 06/10/13 
 Pct Recovery = 85%  Analysis Date = 06/07/13 
 Pct Recovery = 85%  Analysis Date = 06/07/13 
 Pct Recovery = 85%  Analysis Date = 06/05/13 
 Pct Recovery = 85%  Analysis Date = 06/05/13 
 Pct Recovery = 85%  Analysis Date = 06/03/13 
 Pct Recovery = 85%  Analysis Date = 06/03/13 
 Pct Recovery = 85%  Analysis Date = 05/31/13 
 Pct Recovery = 86%  Analysis Date = 05/31/13 
 Pct Recovery = 86%  Analysis Date = 05/29/13 
 Pct Recovery = 86%  Analysis Date = 05/29/13 
 Pct Recovery = 86%  Analysis Date = 05/26/13 
 Pct Recovery = 86%  Analysis Date = 05/26/13 
 Pct Recovery = 86%  Analysis Date = 05/24/13 
 Pct Recovery = 87%  Analysis Date = 05/24/13 
 Pct Recovery = 87%  Analysis Date = 05/22/13 
 Pct Recovery = 87%  Analysis Date = 05/22/13 
 Pct Recovery = 87%  Analysis Date = 05/19/13 
 Pct Recovery = 87%  Analysis Date = 05/19/13 
 Pct Recovery = 87%  Analysis Date = 05/17/13 
 Pct Recovery = 87%  Analysis Date = 05/17/13 
 Pct Recovery = 87%  Analysis Date = 05/14/13 
 Pct Recovery = 88%  Analysis Date = 05/14/13 
 Pct Recovery = 88%  Analysis Date = 05/12/13 
 Pct Recovery = 88%  Analysis Date = 05/12/13 
 Pct Recovery = 88%  Analysis Date = 05/10/13 
 Pct Recovery = 88%  Analysis Date = 05/10/13 
 Pct Recovery = 88%  Analysis Date = 05/07/13 
 Pct Recovery = 89%  Analysis Date = 05/07/13 
 Pct Recovery = 89%  Analysis Date = 05/05/13 
 Pct Recovery = 89%  Analysis Date = 05/05/13 
 Pct Recovery = 89%  Analysis Date = 05/02/13 
 Pct Recovery = 89%  Analysis Date = 05/02/13 
 Pct Recovery = 89%  Analysis Date = 04/30/13 
 Pct Recovery = 89%  Analysis Date = 04/30/13 
 Pct Recovery = 89%  Analysis Date = 04/27/13 
 Pct Recovery = 90%  Analysis Date = 04/27/13 
 Pct Recovery = 90%  Analysis Date = 04/25/13 
 Pct Recovery = 90%  Analysis Date = 04/25/13 
 Pct Recovery = 90%  Analysis Date = 04/23/13 
 Pct Recovery = 90%  Analysis Date = 04/23/13 
 Pct Recovery = 90%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/20/13 
 Pct Recovery = 90%  Analysis Date = 04/18/13 
 Pct Recovery = 90%  Analysis Date = 04/18/13 
 Pct Recovery = 90%  Analysis Date = 04/15/13 
 Pct Recovery = 90%  Analysis Date = 04/15/13 
 Pct Recovery = 90%  Analysis Date = 04/13/13 
 Pct Recovery = 91%  Analysis Date = 04/13/13 
 Pct Recovery = 91%  Analysis Date = 04/11/13 
 Pct Recovery = 91%  Analysis Date = 04/11/13 
 Pct Recovery = 91%  Analysis Date = 04/08/13 
 Pct Recovery = 91%  Analysis Date = 04/08/13 
 Pct Recovery = 91%  Analysis Date = 04/06/13 
 Pct Recovery = 91%  Analysis Date = 04/06/13 
 Pct Recovery = 91%  Analysis Date = 04/03/13 
 Pct Recovery = 91%  Analysis Date = 04/03/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 91%  Analysis Date = 03/25/13 
 Pct Recovery = 91%  Analysis Date = 03/25/13 
 Pct Recovery = 91%  Analysis Date = 03/22/13 
 Pct Recovery = 91%  Analysis Date = 03/22/13 
 Pct Recovery = 91%  Analysis Date = 03/20/13 
 Pct Recovery = 91%  Analysis Date = 03/20/13 
 Pct Recovery = 91%  Analysis Date = 03/17/13 
 Pct Recovery = 92%  Analysis Date = 03/17/13 
 Pct Recovery = 92%  Analysis Date = 03/15/13 
 Pct Recovery = 92%  Analysis Date = 03/15/13 
 Pct Recovery = 92%  Analysis Date = 03/13/13 
 Pct Recovery = 92%  Analysis Date = 03/13/13 
 Pct Recovery = 92%  Analysis Date = 03/10/13 
 Pct Recovery = 92%  Analysis Date = 03/10/13 
 Pct Recovery = 92%  Analysis Date = 03/08/13 
 Pct Recovery = 92%  Analysis Date = 03/08/13 
 Pct Recovery = 92%  Analysis Date = 03/05/13 
 Pct Recovery = 92%  Analysis Date = 03/05/13 
 Pct Recovery = 92%  Analysis Date = 03/03/13 
 Pct Recovery = 92%  Analysis Date = 03/03/13 
 Pct Recovery = 92%  Analysis Date = 03/01/13 
 Pct Recovery = 92%  Analysis Date = 03/01/13 
 Pct Recovery = 92%  Analysis Date = 02/26/13 
 Pct Recovery = 92%  Analysis Date = 02/26/13 
 Pct Recovery = 92%  Analysis Date = 02/24/13 
 Pct Recovery = 92%  Analysis Date = 02/24/13 
 Pct Recovery = 92%  Analysis Date = 02/21/13 
 Pct Recovery = 92%  Analysis Date = 02/21/13 
 Pct Recovery = 92%  Analysis Date = 02/19/13 
 Pct Recovery = 92%  Analysis Date = 02/19/13 
 Pct Recovery = 92%  Analysis Date = 02/17/13 
 Pct Recovery = 92%  Analysis Date = 02/17/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/14/13 
 Pct Recovery = 92%  Analysis Date = 02/12/13 
 Pct Recovery = 92%  Analysis Date = 02/12/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/09/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/07/13 
 Pct Recovery = 92%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/05/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 02/02/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/31/13 
 Pct Recovery = 91%  Analysis Date = 01/28/13 
 Pct Recovery = 91%  Analysis Date = 01/28/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/23/13 
 Pct Recovery = 91%  Analysis Date = 01/23/13 
 Pct Recovery = 91%  Analysis Date = 01/21/13 
 Pct Recovery = 91%  Analysis Date = 01/21/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/19/13 
 Pct Recovery = 91%  Analysis Date = 01/16/13 
 Pct Recovery = 91%  Analysis Date = 01/16/13 
 Pct Recovery = 91%  Analysis Date = 01/14/13 
 Pct Recovery = 91%  Analysis Date = 01/14/13 
 Pct Recovery = 91%  Analysis Date = 01/11/13 
 Pct Recovery = 91%  Analysis Date = 01/11/13 
 Pct Recovery = 91%  Analysis Date = 01/09/13 
 Pct Recovery = 90%  Analysis Date = 01/09/13 
 Pct Recovery = 90%  Analysis Date = 01/07/13 
 Pct Recovery = 90%  Analysis Date = 01/07/13 
 Pct Recovery = 90%  Analysis Date = 01/04/13 
 Pct Recovery = 90%  Analysis Date = 01/04/13 
 Pct Recovery = 90%  Analysis Date = 01/02/13 
 Pct Recovery = 90%  Analysis Date = 01/02/13 
 Pct Recovery = 90%  Analysis Date = 12/30/12 
 Pct Recovery = 90%  Analysis Date = 12/30/12 
 Pct Recovery = 90%  Analysis Date = 12/28/12 
 Pct Recovery = 90%  Analysis Date = 12/28/12 
 Pct Recovery = 90%  Analysis Date = 12/26/12 
 Pct Recovery = 90%  Analysis Date = 12/26/12 
 Pct Recovery = 90%  Analysis Date = 12/23/12 
 Pct Recovery = 90%  Analysis Date = 12/23/12 
 Pct Recovery = 90%  Analysis Date = 12/21/12 
 Pct Recovery = 90%  Analysis Date = 12/21/12 
 Pct Recovery = 90%  Analysis Date = 12/18/12 
 Pct Recovery = 90%  Analysis Date = 12/18/12 
 Pct Recovery = 90%  Analysis Date = 12/16/12 
 Pct Recovery = 90%  Analysis Date = 12/16/12 
 Pct Recovery = 90%  Analysis Date = 12/14/12 
 Pct Recovery = 90%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHENYTOIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 81% 18% 81% 18%
Total 14 81% 18% 81% 18%

Sample Statistics
PHENYTOIN

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PIPERONYL BUTOXIDE
METHOD: LC9017 , TESTIDCODE: 67435LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 55%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 59%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 110%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 59%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 17%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 21%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 51%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 63%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 32%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 68%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 42%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 55%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 33%  Analysis Date = 04/10/14 
 Pct Recovery = 24%  Analysis Date = 04/07/14 
 Pct Recovery = 24%  Analysis Date = 04/07/14 
 Pct Recovery = 24%  Analysis Date = 04/05/14 
 Pct Recovery = 25%  Analysis Date = 04/05/14 
 Pct Recovery = 25%  Analysis Date = 04/03/14 
 Pct Recovery = 25%  Analysis Date = 04/03/14 
 Pct Recovery = 25%  Analysis Date = 04/01/14 
 Pct Recovery = 25%  Analysis Date = 04/01/14 
 Pct Recovery = 25%  Analysis Date = 03/29/14 
 Pct Recovery = 26%  Analysis Date = 03/29/14 
 Pct Recovery = 26%  Analysis Date = 03/27/14 
 Pct Recovery = 26%  Analysis Date = 03/27/14 
 Pct Recovery = 26%  Analysis Date = 03/25/14 
 Pct Recovery = 27%  Analysis Date = 03/25/14 
 Pct Recovery = 27%  Analysis Date = 03/23/14 
 Pct Recovery = 27%  Analysis Date = 03/23/14 
 Pct Recovery = 27%  Analysis Date = 03/21/14 
 Pct Recovery = 27%  Analysis Date = 03/21/14 
 Pct Recovery = 27%  Analysis Date = 03/18/14 
 Pct Recovery = 28%  Analysis Date = 03/18/14 
 Pct Recovery = 28%  Analysis Date = 03/16/14 
 Pct Recovery = 28%  Analysis Date = 03/16/14 
 Pct Recovery = 28%  Analysis Date = 03/14/14 
 Pct Recovery = 28%  Analysis Date = 03/14/14 
 Pct Recovery = 28%  Analysis Date = 03/12/14 
 Pct Recovery = 29%  Analysis Date = 03/12/14 
 Pct Recovery = 29%  Analysis Date = 03/10/14 
 Pct Recovery = 29%  Analysis Date = 03/10/14 
 Pct Recovery = 29%  Analysis Date = 03/07/14 
 Pct Recovery = 29%  Analysis Date = 03/07/14 
 Pct Recovery = 29%  Analysis Date = 03/05/14 
 Pct Recovery = 30%  Analysis Date = 03/05/14 
 Pct Recovery = 30%  Analysis Date = 03/03/14 
 Pct Recovery = 30%  Analysis Date = 03/03/14 
 Pct Recovery = 30%  Analysis Date = 03/01/14 
 Pct Recovery = 30%  Analysis Date = 03/01/14 
 Pct Recovery = 30%  Analysis Date = 02/27/14 
 Pct Recovery = 31%  Analysis Date = 02/27/14 
 Pct Recovery = 31%  Analysis Date = 02/24/14 
 Pct Recovery = 31%  Analysis Date = 02/24/14 
 Pct Recovery = 31%  Analysis Date = 02/22/14 
 Pct Recovery = 31%  Analysis Date = 02/22/14 
 Pct Recovery = 31%  Analysis Date = 02/20/14 
 Pct Recovery = 32%  Analysis Date = 02/20/14 
 Pct Recovery = 32%  Analysis Date = 02/18/14 
 Pct Recovery = 32%  Analysis Date = 02/18/14 
 Pct Recovery = 32%  Analysis Date = 02/16/14 
 Pct Recovery = 32%  Analysis Date = 02/16/14 
 Pct Recovery = 32%  Analysis Date = 02/13/14 
 Pct Recovery = 32%  Analysis Date = 02/13/14 
 Pct Recovery = 32%  Analysis Date = 02/11/14 
 Pct Recovery = 33%  Analysis Date = 02/11/14 
 Pct Recovery = 33%  Analysis Date = 02/09/14 
 Pct Recovery = 33%  Analysis Date = 02/09/14 
 Pct Recovery = 33%  Analysis Date = 02/07/14 
 Pct Recovery = 33%  Analysis Date = 02/07/14 
 Pct Recovery = 33%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 34%  Analysis Date = 01/31/14 
 Pct Recovery = 34%  Analysis Date = 01/31/14 
 Pct Recovery = 34%  Analysis Date = 01/29/14 
 Pct Recovery = 35%  Analysis Date = 01/29/14 
 Pct Recovery = 35%  Analysis Date = 01/27/14 
 Pct Recovery = 35%  Analysis Date = 01/27/14 
 Pct Recovery = 35%  Analysis Date = 01/25/14 
 Pct Recovery = 35%  Analysis Date = 01/25/14 
 Pct Recovery = 35%  Analysis Date = 01/22/14 
 Pct Recovery = 36%  Analysis Date = 01/22/14 
 Pct Recovery = 36%  Analysis Date = 01/20/14 
 Pct Recovery = 36%  Analysis Date = 01/20/14 
 Pct Recovery = 36%  Analysis Date = 01/18/14 
 Pct Recovery = 36%  Analysis Date = 01/18/14 
 Pct Recovery = 36%  Analysis Date = 01/16/14 
 Pct Recovery = 37%  Analysis Date = 01/16/14 
 Pct Recovery = 37%  Analysis Date = 01/14/14 
 Pct Recovery = 37%  Analysis Date = 01/14/14 
 Pct Recovery = 37%  Analysis Date = 01/11/14 
 Pct Recovery = 37%  Analysis Date = 01/11/14 
 Pct Recovery = 37%  Analysis Date = 01/09/14 
 Pct Recovery = 37%  Analysis Date = 01/09/14 
 Pct Recovery = 37%  Analysis Date = 01/07/14 
 Pct Recovery = 37%  Analysis Date = 01/07/14 
 Pct Recovery = 37%  Analysis Date = 01/05/14 
 Pct Recovery = 38%  Analysis Date = 01/05/14 
 Pct Recovery = 38%  Analysis Date = 01/02/14 
 Pct Recovery = 38%  Analysis Date = 01/02/14 
 Pct Recovery = 38%  Analysis Date = 12/31/13 
 Pct Recovery = 38%  Analysis Date = 12/31/13 
 Pct Recovery = 38%  Analysis Date = 12/29/13 
 Pct Recovery = 38%  Analysis Date = 12/29/13 
 Pct Recovery = 38%  Analysis Date = 12/27/13 
 Pct Recovery = 39%  Analysis Date = 12/27/13 
 Pct Recovery = 39%  Analysis Date = 12/25/13 
 Pct Recovery = 39%  Analysis Date = 12/25/13 
 Pct Recovery = 39%  Analysis Date = 12/22/13 
 Pct Recovery = 39%  Analysis Date = 12/22/13 
 Pct Recovery = 39%  Analysis Date = 12/20/13 
 Pct Recovery = 39%  Analysis Date = 12/20/13 
 Pct Recovery = 39%  Analysis Date = 12/18/13 
 Pct Recovery = 39%  Analysis Date = 12/18/13 
 Pct Recovery = 39%  Analysis Date = 12/16/13 
 Pct Recovery = 40%  Analysis Date = 12/16/13 
 Pct Recovery = 40%  Analysis Date = 12/14/13 
 Pct Recovery = 40%  Analysis Date = 12/14/13 
 Pct Recovery = 40%  Analysis Date = 12/11/13 
 Pct Recovery = 40%  Analysis Date = 12/11/13 
 Pct Recovery = 40%  Analysis Date = 12/09/13 
 Pct Recovery = 40%  Analysis Date = 12/09/13 
 Pct Recovery = 40%  Analysis Date = 12/07/13 
 Pct Recovery = 40%  Analysis Date = 12/07/13 
 Pct Recovery = 40%  Analysis Date = 12/05/13 
 Pct Recovery = 41%  Analysis Date = 12/05/13 
 Pct Recovery = 41%  Analysis Date = 12/03/13 
 Pct Recovery = 41%  Analysis Date = 12/03/13 
 Pct Recovery = 41%  Analysis Date = 11/30/13 
 Pct Recovery = 41%  Analysis Date = 11/30/13 
 Pct Recovery = 41%  Analysis Date = 11/28/13 
 Pct Recovery = 41%  Analysis Date = 11/28/13 
 Pct Recovery = 41%  Analysis Date = 11/26/13 
 Pct Recovery = 41%  Analysis Date = 11/26/13 
 Pct Recovery = 41%  Analysis Date = 11/24/13 
 Pct Recovery = 42%  Analysis Date = 11/24/13 
 Pct Recovery = 42%  Analysis Date = 11/22/13 
 Pct Recovery = 42%  Analysis Date = 11/22/13 
 Pct Recovery = 42%  Analysis Date = 11/19/13 
 Pct Recovery = 42%  Analysis Date = 11/19/13 
 Pct Recovery = 42%  Analysis Date = 11/17/13 
 Pct Recovery = 42%  Analysis Date = 11/17/13 
 Pct Recovery = 42%  Analysis Date = 11/15/13 
 Pct Recovery = 42%  Analysis Date = 11/15/13 
 Pct Recovery = 42%  Analysis Date = 11/13/13 
 Pct Recovery = 43%  Analysis Date = 11/13/13 
 Pct Recovery = 43%  Analysis Date = 11/11/13 
 Pct Recovery = 43%  Analysis Date = 11/11/13 
 Pct Recovery = 43%  Analysis Date = 11/08/13 
 Pct Recovery = 43%  Analysis Date = 11/08/13 
 Pct Recovery = 43%  Analysis Date = 11/06/13 
 Pct Recovery = 43%  Analysis Date = 11/06/13 
 Pct Recovery = 43%  Analysis Date = 11/04/13 
 Pct Recovery = 43%  Analysis Date = 11/04/13 
 Pct Recovery = 43%  Analysis Date = 11/02/13 
 Pct Recovery = 44%  Analysis Date = 11/02/13 
 Pct Recovery = 44%  Analysis Date = 10/31/13 
 Pct Recovery = 44%  Analysis Date = 10/31/13 
 Pct Recovery = 44%  Analysis Date = 10/28/13 
 Pct Recovery = 44%  Analysis Date = 10/28/13 
 Pct Recovery = 44%  Analysis Date = 10/26/13 
 Pct Recovery = 44%  Analysis Date = 10/26/13 
 Pct Recovery = 44%  Analysis Date = 10/24/13 
 Pct Recovery = 44%  Analysis Date = 10/24/13 
 Pct Recovery = 44%  Analysis Date = 10/22/13 
 Pct Recovery = 44%  Analysis Date = 10/22/13 
 Pct Recovery = 44%  Analysis Date = 10/20/13 
 Pct Recovery = 44%  Analysis Date = 10/20/13 
 Pct Recovery = 44%  Analysis Date = 10/17/13 
 Pct Recovery = 44%  Analysis Date = 10/17/13 
 Pct Recovery = 44%  Analysis Date = 10/15/13 
 Pct Recovery = 44%  Analysis Date = 10/15/13 
 Pct Recovery = 44%  Analysis Date = 10/13/13 
 Pct Recovery = 44%  Analysis Date = 10/13/13 
 Pct Recovery = 44%  Analysis Date = 10/11/13 
 Pct Recovery = 44%  Analysis Date = 10/11/13 
 Pct Recovery = 44%  Analysis Date = 10/08/13 
 Pct Recovery = 45%  Analysis Date = 10/08/13 
 Pct Recovery = 45%  Analysis Date = 10/06/13 
 Pct Recovery = 45%  Analysis Date = 10/06/13 
 Pct Recovery = 45%  Analysis Date = 10/04/13 
 Pct Recovery = 45%  Analysis Date = 10/04/13 
 Pct Recovery = 45%  Analysis Date = 10/02/13 
 Pct Recovery = 45%  Analysis Date = 10/02/13 
 Pct Recovery = 45%  Analysis Date = 09/30/13 
 Pct Recovery = 45%  Analysis Date = 09/30/13 
 Pct Recovery = 45%  Analysis Date = 09/27/13 
 Pct Recovery = 45%  Analysis Date = 09/27/13 
 Pct Recovery = 45%  Analysis Date = 09/25/13 
 Pct Recovery = 45%  Analysis Date = 09/25/13 
 Pct Recovery = 45%  Analysis Date = 09/23/13 
 Pct Recovery = 45%  Analysis Date = 09/23/13 
 Pct Recovery = 45%  Analysis Date = 09/21/13 
 Pct Recovery = 45%  Analysis Date = 09/21/13 
 Pct Recovery = 45%  Analysis Date = 09/19/13 
 Pct Recovery = 45%  Analysis Date = 09/19/13 
 Pct Recovery = 45%  Analysis Date = 09/16/13 
 Pct Recovery = 45%  Analysis Date = 09/16/13 
 Pct Recovery = 45%  Analysis Date = 09/14/13 
 Pct Recovery = 45%  Analysis Date = 09/14/13 
 Pct Recovery = 45%  Analysis Date = 09/12/13 
 Pct Recovery = 45%  Analysis Date = 09/12/13 
 Pct Recovery = 45%  Analysis Date = 09/10/13 
 Pct Recovery = 45%  Analysis Date = 09/10/13 
 Pct Recovery = 45%  Analysis Date = 09/08/13 
 Pct Recovery = 45%  Analysis Date = 09/08/13 
 Pct Recovery = 45%  Analysis Date = 09/05/13 
 Pct Recovery = 45%  Analysis Date = 09/05/13 
 Pct Recovery = 45%  Analysis Date = 09/03/13 
 Pct Recovery = 45%  Analysis Date = 09/03/13 
 Pct Recovery = 45%  Analysis Date = 09/01/13 
 Pct Recovery = 45%  Analysis Date = 09/01/13 
 Pct Recovery = 45%  Analysis Date = 08/30/13 
 Pct Recovery = 45%  Analysis Date = 08/30/13 
 Pct Recovery = 45%  Analysis Date = 08/28/13 
 Pct Recovery = 45%  Analysis Date = 08/28/13 
 Pct Recovery = 45%  Analysis Date = 08/25/13 
 Pct Recovery = 45%  Analysis Date = 08/25/13 
 Pct Recovery = 45%  Analysis Date = 08/23/13 
 Pct Recovery = 46%  Analysis Date = 08/23/13 
 Pct Recovery = 46%  Analysis Date = 08/21/13 
 Pct Recovery = 46%  Analysis Date = 08/21/13 
 Pct Recovery = 46%  Analysis Date = 08/19/13 
 Pct Recovery = 46%  Analysis Date = 08/19/13 
 Pct Recovery = 46%  Analysis Date = 08/17/13 
 Pct Recovery = 46%  Analysis Date = 08/17/13 
 Pct Recovery = 46%  Analysis Date = 08/14/13 
 Pct Recovery = 46%  Analysis Date = 08/14/13 
 Pct Recovery = 46%  Analysis Date = 08/12/13 
 Pct Recovery = 46%  Analysis Date = 08/12/13 
 Pct Recovery = 46%  Analysis Date = 08/10/13 
 Pct Recovery = 47%  Analysis Date = 08/10/13 
 Pct Recovery = 47%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/06/13 
 Pct Recovery = 47%  Analysis Date = 08/06/13 
 Pct Recovery = 47%  Analysis Date = 08/03/13 
 Pct Recovery = 47%  Analysis Date = 08/03/13 
 Pct Recovery = 47%  Analysis Date = 08/01/13 
 Pct Recovery = 48%  Analysis Date = 08/01/13 
 Pct Recovery = 48%  Analysis Date = 07/30/13 
 Pct Recovery = 48%  Analysis Date = 07/30/13 
 Pct Recovery = 48%  Analysis Date = 07/28/13 
 Pct Recovery = 48%  Analysis Date = 07/28/13 
 Pct Recovery = 48%  Analysis Date = 07/26/13 
 Pct Recovery = 49%  Analysis Date = 07/26/13 
 Pct Recovery = 49%  Analysis Date = 07/23/13 
 Pct Recovery = 49%  Analysis Date = 07/23/13 
 Pct Recovery = 49%  Analysis Date = 07/21/13 
 Pct Recovery = 49%  Analysis Date = 07/21/13 
 Pct Recovery = 49%  Analysis Date = 07/19/13 
 Pct Recovery = 49%  Analysis Date = 07/19/13 
 Pct Recovery = 49%  Analysis Date = 07/17/13 
 Pct Recovery = 50%  Analysis Date = 07/17/13 
 Pct Recovery = 50%  Analysis Date = 07/14/13 
 Pct Recovery = 50%  Analysis Date = 07/14/13 
 Pct Recovery = 50%  Analysis Date = 07/12/13 
 Pct Recovery = 50%  Analysis Date = 07/12/13 
 Pct Recovery = 50%  Analysis Date = 07/10/13 
 Pct Recovery = 50%  Analysis Date = 07/10/13 
 Pct Recovery = 50%  Analysis Date = 07/08/13 
 Pct Recovery = 51%  Analysis Date = 07/08/13 
 Pct Recovery = 51%  Analysis Date = 07/06/13 
 Pct Recovery = 51%  Analysis Date = 07/06/13 
 Pct Recovery = 51%  Analysis Date = 07/03/13 
 Pct Recovery = 51%  Analysis Date = 07/03/13 
 Pct Recovery = 51%  Analysis Date = 07/01/13 
 Pct Recovery = 52%  Analysis Date = 07/01/13 
 Pct Recovery = 52%  Analysis Date = 06/29/13 
 Pct Recovery = 52%  Analysis Date = 06/29/13 
 Pct Recovery = 52%  Analysis Date = 06/27/13 
 Pct Recovery = 52%  Analysis Date = 06/27/13 
 Pct Recovery = 52%  Analysis Date = 06/25/13 
 Pct Recovery = 52%  Analysis Date = 06/25/13 
 Pct Recovery = 52%  Analysis Date = 06/22/13 
 Pct Recovery = 53%  Analysis Date = 06/22/13 
 Pct Recovery = 53%  Analysis Date = 06/20/13 
 Pct Recovery = 53%  Analysis Date = 06/20/13 
 Pct Recovery = 53%  Analysis Date = 06/18/13 
 Pct Recovery = 53%  Analysis Date = 06/18/13 
 Pct Recovery = 53%  Analysis Date = 06/16/13 
 Pct Recovery = 53%  Analysis Date = 06/16/13 
 Pct Recovery = 53%  Analysis Date = 06/14/13 
 Pct Recovery = 54%  Analysis Date = 06/14/13 
 Pct Recovery = 54%  Analysis Date = 06/11/13 
 Pct Recovery = 54%  Analysis Date = 06/11/13 
 Pct Recovery = 54%  Analysis Date = 06/09/13 
 Pct Recovery = 54%  Analysis Date = 06/09/13 
 Pct Recovery = 54%  Analysis Date = 06/07/13 
 Pct Recovery = 55%  Analysis Date = 06/07/13 
 Pct Recovery = 55%  Analysis Date = 06/05/13 
 Pct Recovery = 55%  Analysis Date = 06/05/13 
 Pct Recovery = 55%  Analysis Date = 06/03/13 
 Pct Recovery = 55%  Analysis Date = 06/03/13 
 Pct Recovery = 55%  Analysis Date = 05/31/13 
 Pct Recovery = 55%  Analysis Date = 05/31/13 
 Pct Recovery = 55%  Analysis Date = 05/29/13 
 Pct Recovery = 56%  Analysis Date = 05/29/13 
 Pct Recovery = 56%  Analysis Date = 05/27/13 
 Pct Recovery = 56%  Analysis Date = 05/27/13 
 Pct Recovery = 56%  Analysis Date = 05/25/13 
 Pct Recovery = 56%  Analysis Date = 05/25/13 
 Pct Recovery = 56%  Analysis Date = 05/23/13 
 Pct Recovery = 56%  Analysis Date = 05/23/13 
 Pct Recovery = 56%  Analysis Date = 05/20/13 
 Pct Recovery = 57%  Analysis Date = 05/20/13 
 Pct Recovery = 57%  Analysis Date = 05/18/13 
 Pct Recovery = 57%  Analysis Date = 05/18/13 
 Pct Recovery = 57%  Analysis Date = 05/16/13 
 Pct Recovery = 57%  Analysis Date = 05/16/13 
 Pct Recovery = 57%  Analysis Date = 05/14/13 
 Pct Recovery = 58%  Analysis Date = 05/14/13 
 Pct Recovery = 58%  Analysis Date = 05/12/13 
 Pct Recovery = 58%  Analysis Date = 05/12/13 
 Pct Recovery = 58%  Analysis Date = 05/09/13 
 Pct Recovery = 58%  Analysis Date = 05/09/13 
 Pct Recovery = 58%  Analysis Date = 05/07/13 
 Pct Recovery = 58%  Analysis Date = 05/07/13 
 Pct Recovery = 58%  Analysis Date = 05/05/13 
 Pct Recovery = 59%  Analysis Date = 05/05/13 
 Pct Recovery = 59%  Analysis Date = 05/03/13 
 Pct Recovery = 59%  Analysis Date = 05/03/13 
 Pct Recovery = 59%  Analysis Date = 05/01/13 
 Pct Recovery = 59%  Analysis Date = 05/01/13 
 Pct Recovery = 59%  Analysis Date = 04/28/13 
 Pct Recovery = 58%  Analysis Date = 04/28/13 
 Pct Recovery = 58%  Analysis Date = 04/26/13 
 Pct Recovery = 58%  Analysis Date = 04/26/13 
 Pct Recovery = 58%  Analysis Date = 04/24/13 
 Pct Recovery = 57%  Analysis Date = 04/24/13 
 Pct Recovery = 57%  Analysis Date = 04/22/13 
 Pct Recovery = 57%  Analysis Date = 04/22/13 
 Pct Recovery = 57%  Analysis Date = 04/19/13 
 Pct Recovery = 56%  Analysis Date = 04/19/13 
 Pct Recovery = 56%  Analysis Date = 04/17/13 
 Pct Recovery = 56%  Analysis Date = 04/17/13 
 Pct Recovery = 56%  Analysis Date = 04/15/13 
 Pct Recovery = 55%  Analysis Date = 04/15/13 
 Pct Recovery = 55%  Analysis Date = 04/13/13 
 Pct Recovery = 55%  Analysis Date = 04/13/13 
 Pct Recovery = 55%  Analysis Date = 04/11/13 
 Pct Recovery = 54%  Analysis Date = 04/11/13 
 Pct Recovery = 54%  Analysis Date = 04/08/13 
 Pct Recovery = 54%  Analysis Date = 04/08/13 
 Pct Recovery = 54%  Analysis Date = 04/06/13 
 Pct Recovery = 53%  Analysis Date = 04/06/13 
 Pct Recovery = 53%  Analysis Date = 04/04/13 
 Pct Recovery = 52%  Analysis Date = 04/04/13 
 Pct Recovery = 52%  Analysis Date = 04/02/13 
 Pct Recovery = 52%  Analysis Date = 04/02/13 
 Pct Recovery = 52%  Analysis Date = 03/31/13 
 Pct Recovery = 51%  Analysis Date = 03/31/13 
 Pct Recovery = 51%  Analysis Date = 03/28/13 
 Pct Recovery = 51%  Analysis Date = 03/28/13 
 Pct Recovery = 51%  Analysis Date = 03/26/13 
 Pct Recovery = 51%  Analysis Date = 03/26/13 
 Pct Recovery = 51%  Analysis Date = 03/24/13 
 Pct Recovery = 52%  Analysis Date = 03/24/13 
 Pct Recovery = 52%  Analysis Date = 03/22/13 
 Pct Recovery = 53%  Analysis Date = 03/22/13 
 Pct Recovery = 53%  Analysis Date = 03/20/13 
 Pct Recovery = 54%  Analysis Date = 03/20/13 
 Pct Recovery = 54%  Analysis Date = 03/17/13 
 Pct Recovery = 55%  Analysis Date = 03/17/13 
 Pct Recovery = 55%  Analysis Date = 03/15/13 
 Pct Recovery = 57%  Analysis Date = 03/15/13 
 Pct Recovery = 57%  Analysis Date = 03/13/13 
 Pct Recovery = 58%  Analysis Date = 03/13/13 
 Pct Recovery = 58%  Analysis Date = 03/11/13 
 Pct Recovery = 59%  Analysis Date = 03/11/13 
 Pct Recovery = 59%  Analysis Date = 03/09/13 
 Pct Recovery = 60%  Analysis Date = 03/09/13 
 Pct Recovery = 60%  Analysis Date = 03/06/13 
 Pct Recovery = 61%  Analysis Date = 03/06/13 
 Pct Recovery = 61%  Analysis Date = 03/04/13 
 Pct Recovery = 63%  Analysis Date = 03/04/13 
 Pct Recovery = 63%  Analysis Date = 03/02/13 
 Pct Recovery = 64%  Analysis Date = 03/02/13 
 Pct Recovery = 64%  Analysis Date = 02/28/13 
 Pct Recovery = 65%  Analysis Date = 02/28/13 
 Pct Recovery = 65%  Analysis Date = 02/26/13 
 Pct Recovery = 66%  Analysis Date = 02/26/13 
 Pct Recovery = 66%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/23/13 
 Pct Recovery = 67%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/21/13 
 Pct Recovery = 69%  Analysis Date = 02/19/13 
 Pct Recovery = 70%  Analysis Date = 02/19/13 
 Pct Recovery = 70%  Analysis Date = 02/17/13 
 Pct Recovery = 71%  Analysis Date = 02/17/13 
 Pct Recovery = 71%  Analysis Date = 02/15/13 
 Pct Recovery = 72%  Analysis Date = 02/15/13 
 Pct Recovery = 72%  Analysis Date = 02/12/13 
 Pct Recovery = 73%  Analysis Date = 02/12/13 
 Pct Recovery = 73%  Analysis Date = 02/10/13 
 Pct Recovery = 75%  Analysis Date = 02/10/13 
 Pct Recovery = 75%  Analysis Date = 02/08/13 
 Pct Recovery = 76%  Analysis Date = 02/08/13 
 Pct Recovery = 76%  Analysis Date = 02/06/13 
 Pct Recovery = 77%  Analysis Date = 02/06/13 
 Pct Recovery = 77%  Analysis Date = 02/04/13 
 Pct Recovery = 78%  Analysis Date = 02/04/13 
 Pct Recovery = 78%  Analysis Date = 02/01/13 
 Pct Recovery = 80%  Analysis Date = 02/01/13 
 Pct Recovery = 80%  Analysis Date = 01/30/13 
 Pct Recovery = 81%  Analysis Date = 01/30/13 
 Pct Recovery = 81%  Analysis Date = 01/28/13 
 Pct Recovery = 82%  Analysis Date = 01/28/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 83%  Analysis Date = 01/26/13 
 Pct Recovery = 83%  Analysis Date = 01/24/13 
 Pct Recovery = 84%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PIPERONYL BUTOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 51% 24% 55% 19%
Total 13 51% 24% 55% 19%

Sample Statistics
PIPERONYL BUTOXIDE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 5 36% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PREDNISOLONE
METHOD: LC9017 , TESTIDCODE: 67483LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 66%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 70%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 61%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 145%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 66%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 69%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 87%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 64%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 67%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 94%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 61%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 74%  Analysis Date = 04/09/14 
 Pct Recovery = 62%  Analysis Date = 04/07/14 
 Pct Recovery = 62%  Analysis Date = 04/07/14 
 Pct Recovery = 62%  Analysis Date = 04/05/14 
 Pct Recovery = 62%  Analysis Date = 04/05/14 
 Pct Recovery = 62%  Analysis Date = 04/02/14 
 Pct Recovery = 63%  Analysis Date = 04/02/14 
 Pct Recovery = 63%  Analysis Date = 03/31/14 
 Pct Recovery = 63%  Analysis Date = 03/31/14 
 Pct Recovery = 63%  Analysis Date = 03/28/14 
 Pct Recovery = 63%  Analysis Date = 03/28/14 
 Pct Recovery = 63%  Analysis Date = 03/26/14 
 Pct Recovery = 64%  Analysis Date = 03/26/14 
 Pct Recovery = 64%  Analysis Date = 03/24/14 
 Pct Recovery = 64%  Analysis Date = 03/24/14 
 Pct Recovery = 64%  Analysis Date = 03/21/14 
 Pct Recovery = 64%  Analysis Date = 03/21/14 
 Pct Recovery = 64%  Analysis Date = 03/19/14 
 Pct Recovery = 65%  Analysis Date = 03/19/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/16/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/14/14 
 Pct Recovery = 65%  Analysis Date = 03/12/14 
 Pct Recovery = 65%  Analysis Date = 03/12/14 
 Pct Recovery = 65%  Analysis Date = 03/09/14 
 Pct Recovery = 66%  Analysis Date = 03/09/14 
 Pct Recovery = 66%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/07/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/04/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 03/02/14 
 Pct Recovery = 66%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/28/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/25/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/23/14 
 Pct Recovery = 67%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/20/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/18/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/15/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/13/14 
 Pct Recovery = 68%  Analysis Date = 02/11/14 
 Pct Recovery = 69%  Analysis Date = 02/11/14 
 Pct Recovery = 69%  Analysis Date = 02/08/14 
 Pct Recovery = 69%  Analysis Date = 02/08/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/06/14 
 Pct Recovery = 69%  Analysis Date = 02/03/14 
 Pct Recovery = 69%  Analysis Date = 02/03/14 
 Pct Recovery = 69%  Analysis Date = 02/01/14 
 Pct Recovery = 70%  Analysis Date = 02/01/14 
 Pct Recovery = 70%  Analysis Date = 01/30/14 
 Pct Recovery = 70%  Analysis Date = 01/30/14 
 Pct Recovery = 70%  Analysis Date = 01/27/14 
 Pct Recovery = 70%  Analysis Date = 01/27/14 
 Pct Recovery = 70%  Analysis Date = 01/25/14 
 Pct Recovery = 71%  Analysis Date = 01/25/14 
 Pct Recovery = 71%  Analysis Date = 01/22/14 
 Pct Recovery = 71%  Analysis Date = 01/22/14 
 Pct Recovery = 71%  Analysis Date = 01/20/14 
 Pct Recovery = 71%  Analysis Date = 01/20/14 
 Pct Recovery = 71%  Analysis Date = 01/18/14 
 Pct Recovery = 71%  Analysis Date = 01/18/14 
 Pct Recovery = 71%  Analysis Date = 01/15/14 
 Pct Recovery = 72%  Analysis Date = 01/15/14 
 Pct Recovery = 72%  Analysis Date = 01/13/14 
 Pct Recovery = 72%  Analysis Date = 01/13/14 
 Pct Recovery = 72%  Analysis Date = 01/10/14 
 Pct Recovery = 72%  Analysis Date = 01/10/14 
 Pct Recovery = 72%  Analysis Date = 01/08/14 
 Pct Recovery = 72%  Analysis Date = 01/08/14 
 Pct Recovery = 72%  Analysis Date = 01/06/14 
 Pct Recovery = 72%  Analysis Date = 01/06/14 
 Pct Recovery = 72%  Analysis Date = 01/03/14 
 Pct Recovery = 72%  Analysis Date = 01/03/14 
 Pct Recovery = 72%  Analysis Date = 01/01/14 
 Pct Recovery = 72%  Analysis Date = 01/01/14 
 Pct Recovery = 72%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/24/13 
 Pct Recovery = 73%  Analysis Date = 12/24/13 
 Pct Recovery = 73%  Analysis Date = 12/22/13 
 Pct Recovery = 73%  Analysis Date = 12/22/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/17/13 
 Pct Recovery = 73%  Analysis Date = 12/17/13 
 Pct Recovery = 73%  Analysis Date = 12/15/13 
 Pct Recovery = 73%  Analysis Date = 12/15/13 
 Pct Recovery = 73%  Analysis Date = 12/12/13 
 Pct Recovery = 74%  Analysis Date = 12/12/13 
 Pct Recovery = 74%  Analysis Date = 12/10/13 
 Pct Recovery = 74%  Analysis Date = 12/10/13 
 Pct Recovery = 74%  Analysis Date = 12/08/13 
 Pct Recovery = 74%  Analysis Date = 12/08/13 
 Pct Recovery = 74%  Analysis Date = 12/05/13 
 Pct Recovery = 74%  Analysis Date = 12/05/13 
 Pct Recovery = 74%  Analysis Date = 12/03/13 
 Pct Recovery = 74%  Analysis Date = 12/03/13 
 Pct Recovery = 74%  Analysis Date = 11/30/13 
 Pct Recovery = 74%  Analysis Date = 11/30/13 
 Pct Recovery = 74%  Analysis Date = 11/28/13 
 Pct Recovery = 74%  Analysis Date = 11/28/13 
 Pct Recovery = 74%  Analysis Date = 11/26/13 
 Pct Recovery = 75%  Analysis Date = 11/26/13 
 Pct Recovery = 75%  Analysis Date = 11/23/13 
 Pct Recovery = 75%  Analysis Date = 11/23/13 
 Pct Recovery = 75%  Analysis Date = 11/21/13 
 Pct Recovery = 75%  Analysis Date = 11/21/13 
 Pct Recovery = 75%  Analysis Date = 11/18/13 
 Pct Recovery = 75%  Analysis Date = 11/18/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/13/13 
 Pct Recovery = 75%  Analysis Date = 11/13/13 
 Pct Recovery = 75%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/09/13 
 Pct Recovery = 76%  Analysis Date = 11/09/13 
 Pct Recovery = 76%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/20/13 
 Pct Recovery = 76%  Analysis Date = 10/20/13 
 Pct Recovery = 76%  Analysis Date = 10/18/13 
 Pct Recovery = 76%  Analysis Date = 10/18/13 
 Pct Recovery = 76%  Analysis Date = 10/16/13 
 Pct Recovery = 76%  Analysis Date = 10/16/13 
 Pct Recovery = 76%  Analysis Date = 10/13/13 
 Pct Recovery = 76%  Analysis Date = 10/13/13 
 Pct Recovery = 76%  Analysis Date = 10/11/13 
 Pct Recovery = 76%  Analysis Date = 10/11/13 
 Pct Recovery = 76%  Analysis Date = 10/08/13 
 Pct Recovery = 75%  Analysis Date = 10/08/13 
 Pct Recovery = 75%  Analysis Date = 10/06/13 
 Pct Recovery = 75%  Analysis Date = 10/06/13 
 Pct Recovery = 75%  Analysis Date = 10/04/13 
 Pct Recovery = 75%  Analysis Date = 10/04/13 
 Pct Recovery = 75%  Analysis Date = 10/01/13 
 Pct Recovery = 75%  Analysis Date = 10/01/13 
 Pct Recovery = 75%  Analysis Date = 09/29/13 
 Pct Recovery = 75%  Analysis Date = 09/29/13 
 Pct Recovery = 75%  Analysis Date = 09/26/13 
 Pct Recovery = 75%  Analysis Date = 09/26/13 
 Pct Recovery = 75%  Analysis Date = 09/24/13 
 Pct Recovery = 75%  Analysis Date = 09/24/13 
 Pct Recovery = 75%  Analysis Date = 09/21/13 
 Pct Recovery = 75%  Analysis Date = 09/21/13 
 Pct Recovery = 75%  Analysis Date = 09/19/13 
 Pct Recovery = 75%  Analysis Date = 09/19/13 
 Pct Recovery = 75%  Analysis Date = 09/17/13 
 Pct Recovery = 75%  Analysis Date = 09/17/13 
 Pct Recovery = 75%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/14/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/12/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/02/13 
 Pct Recovery = 74%  Analysis Date = 09/02/13 
 Pct Recovery = 74%  Analysis Date = 08/31/13 
 Pct Recovery = 74%  Analysis Date = 08/31/13 
 Pct Recovery = 74%  Analysis Date = 08/28/13 
 Pct Recovery = 74%  Analysis Date = 08/28/13 
 Pct Recovery = 74%  Analysis Date = 08/26/13 
 Pct Recovery = 74%  Analysis Date = 08/26/13 
 Pct Recovery = 74%  Analysis Date = 08/24/13 
 Pct Recovery = 74%  Analysis Date = 08/24/13 
 Pct Recovery = 74%  Analysis Date = 08/21/13 
 Pct Recovery = 73%  Analysis Date = 08/21/13 
 Pct Recovery = 73%  Analysis Date = 08/19/13 
 Pct Recovery = 73%  Analysis Date = 08/19/13 
 Pct Recovery = 73%  Analysis Date = 08/16/13 
 Pct Recovery = 73%  Analysis Date = 08/16/13 
 Pct Recovery = 73%  Analysis Date = 08/14/13 
 Pct Recovery = 73%  Analysis Date = 08/14/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/09/13 
 Pct Recovery = 72%  Analysis Date = 08/09/13 
 Pct Recovery = 72%  Analysis Date = 08/07/13 
 Pct Recovery = 72%  Analysis Date = 08/07/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/04/13 
 Pct Recovery = 72%  Analysis Date = 08/02/13 
 Pct Recovery = 72%  Analysis Date = 08/02/13 
 Pct Recovery = 72%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/30/13 
 Pct Recovery = 72%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/23/13 
 Pct Recovery = 71%  Analysis Date = 07/23/13 
 Pct Recovery = 71%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/18/13 
 Pct Recovery = 70%  Analysis Date = 07/18/13 
 Pct Recovery = 70%  Analysis Date = 07/16/13 
 Pct Recovery = 70%  Analysis Date = 07/16/13 
 Pct Recovery = 70%  Analysis Date = 07/14/13 
 Pct Recovery = 70%  Analysis Date = 07/14/13 
 Pct Recovery = 70%  Analysis Date = 07/11/13 
 Pct Recovery = 70%  Analysis Date = 07/11/13 
 Pct Recovery = 70%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/09/13 
 Pct Recovery = 69%  Analysis Date = 07/06/13 
 Pct Recovery = 69%  Analysis Date = 07/06/13 
 Pct Recovery = 69%  Analysis Date = 07/04/13 
 Pct Recovery = 69%  Analysis Date = 07/04/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 07/02/13 
 Pct Recovery = 69%  Analysis Date = 06/29/13 
 Pct Recovery = 68%  Analysis Date = 06/29/13 
 Pct Recovery = 68%  Analysis Date = 06/27/13 
 Pct Recovery = 68%  Analysis Date = 06/27/13 
 Pct Recovery = 68%  Analysis Date = 06/24/13 
 Pct Recovery = 68%  Analysis Date = 06/24/13 
 Pct Recovery = 68%  Analysis Date = 06/22/13 
 Pct Recovery = 68%  Analysis Date = 06/22/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/19/13 
 Pct Recovery = 68%  Analysis Date = 06/17/13 
 Pct Recovery = 67%  Analysis Date = 06/17/13 
 Pct Recovery = 67%  Analysis Date = 06/15/13 
 Pct Recovery = 67%  Analysis Date = 06/15/13 
 Pct Recovery = 67%  Analysis Date = 06/12/13 
 Pct Recovery = 67%  Analysis Date = 06/12/13 
 Pct Recovery = 67%  Analysis Date = 06/10/13 
 Pct Recovery = 67%  Analysis Date = 06/10/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 66%  Analysis Date = 06/07/13 
 Pct Recovery = 66%  Analysis Date = 06/05/13 
 Pct Recovery = 66%  Analysis Date = 06/05/13 
 Pct Recovery = 66%  Analysis Date = 06/03/13 
 Pct Recovery = 66%  Analysis Date = 06/03/13 
 Pct Recovery = 66%  Analysis Date = 05/31/13 
 Pct Recovery = 66%  Analysis Date = 05/31/13 
 Pct Recovery = 66%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/19/13 
 Pct Recovery = 65%  Analysis Date = 05/19/13 
 Pct Recovery = 65%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/12/13 
 Pct Recovery = 64%  Analysis Date = 05/12/13 
 Pct Recovery = 64%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/07/13 
 Pct Recovery = 63%  Analysis Date = 05/07/13 
 Pct Recovery = 63%  Analysis Date = 05/05/13 
 Pct Recovery = 63%  Analysis Date = 05/05/13 
 Pct Recovery = 63%  Analysis Date = 05/02/13 
 Pct Recovery = 63%  Analysis Date = 05/02/13 
 Pct Recovery = 63%  Analysis Date = 04/30/13 
 Pct Recovery = 63%  Analysis Date = 04/30/13 
 Pct Recovery = 63%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/25/13 
 Pct Recovery = 63%  Analysis Date = 04/25/13 
 Pct Recovery = 63%  Analysis Date = 04/23/13 
 Pct Recovery = 64%  Analysis Date = 04/23/13 
 Pct Recovery = 64%  Analysis Date = 04/20/13 
 Pct Recovery = 65%  Analysis Date = 04/20/13 
 Pct Recovery = 65%  Analysis Date = 04/18/13 
 Pct Recovery = 66%  Analysis Date = 04/18/13 
 Pct Recovery = 66%  Analysis Date = 04/15/13 
 Pct Recovery = 67%  Analysis Date = 04/15/13 
 Pct Recovery = 67%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 68%  Analysis Date = 04/11/13 
 Pct Recovery = 69%  Analysis Date = 04/11/13 
 Pct Recovery = 69%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/08/13 
 Pct Recovery = 70%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/06/13 
 Pct Recovery = 71%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 73%  Analysis Date = 04/01/13 
 Pct Recovery = 73%  Analysis Date = 03/30/13 
 Pct Recovery = 73%  Analysis Date = 03/30/13 
 Pct Recovery = 73%  Analysis Date = 03/27/13 
 Pct Recovery = 74%  Analysis Date = 03/27/13 
 Pct Recovery = 74%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 76%  Analysis Date = 03/22/13 
 Pct Recovery = 76%  Analysis Date = 03/20/13 
 Pct Recovery = 77%  Analysis Date = 03/20/13 
 Pct Recovery = 77%  Analysis Date = 03/17/13 
 Pct Recovery = 77%  Analysis Date = 03/17/13 
 Pct Recovery = 77%  Analysis Date = 03/15/13 
 Pct Recovery = 78%  Analysis Date = 03/15/13 
 Pct Recovery = 78%  Analysis Date = 03/13/13 
 Pct Recovery = 78%  Analysis Date = 03/13/13 
 Pct Recovery = 78%  Analysis Date = 03/10/13 
 Pct Recovery = 79%  Analysis Date = 03/10/13 
 Pct Recovery = 79%  Analysis Date = 03/08/13 
 Pct Recovery = 80%  Analysis Date = 03/08/13 
 Pct Recovery = 80%  Analysis Date = 03/05/13 
 Pct Recovery = 80%  Analysis Date = 03/05/13 
 Pct Recovery = 80%  Analysis Date = 03/03/13 
 Pct Recovery = 81%  Analysis Date = 03/03/13 
 Pct Recovery = 81%  Analysis Date = 03/01/13 
 Pct Recovery = 82%  Analysis Date = 03/01/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/26/13 
 Pct Recovery = 82%  Analysis Date = 02/24/13 
 Pct Recovery = 83%  Analysis Date = 02/24/13 
 Pct Recovery = 83%  Analysis Date = 02/21/13 
 Pct Recovery = 84%  Analysis Date = 02/21/13 
 Pct Recovery = 84%  Analysis Date = 02/19/13 
 Pct Recovery = 84%  Analysis Date = 02/19/13 
 Pct Recovery = 84%  Analysis Date = 02/17/13 
 Pct Recovery = 85%  Analysis Date = 02/17/13 
 Pct Recovery = 85%  Analysis Date = 02/14/13 
 Pct Recovery = 86%  Analysis Date = 02/14/13 
 Pct Recovery = 86%  Analysis Date = 02/12/13 
 Pct Recovery = 86%  Analysis Date = 02/12/13 
 Pct Recovery = 86%  Analysis Date = 02/09/13 
 Pct Recovery = 87%  Analysis Date = 02/09/13 
 Pct Recovery = 87%  Analysis Date = 02/07/13 
 Pct Recovery = 88%  Analysis Date = 02/07/13 
 Pct Recovery = 88%  Analysis Date = 02/05/13 
 Pct Recovery = 88%  Analysis Date = 02/05/13 
 Pct Recovery = 88%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 02/02/13 
 Pct Recovery = 89%  Analysis Date = 01/31/13 
 Pct Recovery = 90%  Analysis Date = 01/31/13 
 Pct Recovery = 90%  Analysis Date = 01/28/13 
 Pct Recovery = 90%  Analysis Date = 01/28/13 
 Pct Recovery = 90%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/26/13 
 Pct Recovery = 91%  Analysis Date = 01/23/13 
 Pct Recovery = 92%  Analysis Date = 01/23/13 
 Pct Recovery = 92%  Analysis Date = 01/21/13 
 Pct Recovery = 92%  Analysis Date = 01/21/13 
 Pct Recovery = 92%  Analysis Date = 01/19/13 
 Pct Recovery = 92%  Analysis Date = 01/19/13 
 Pct Recovery = 92%  Analysis Date = 01/16/13 
 Pct Recovery = 92%  Analysis Date = 01/16/13 
 Pct Recovery = 92%  Analysis Date = 01/14/13 
 Pct Recovery = 92%  Analysis Date = 01/14/13 
 Pct Recovery = 92%  Analysis Date = 01/11/13 
 Pct Recovery = 92%  Analysis Date = 01/11/13 
 Pct Recovery = 92%  Analysis Date = 01/09/13 
 Pct Recovery = 91%  Analysis Date = 01/09/13 
 Pct Recovery = 91%  Analysis Date = 01/07/13 
 Pct Recovery = 91%  Analysis Date = 01/07/13 
 Pct Recovery = 91%  Analysis Date = 01/04/13 
 Pct Recovery = 91%  Analysis Date = 01/04/13 
 Pct Recovery = 91%  Analysis Date = 01/02/13 
 Pct Recovery = 91%  Analysis Date = 01/02/13 
 Pct Recovery = 91%  Analysis Date = 12/30/12 
 Pct Recovery = 91%  Analysis Date = 12/30/12 
 Pct Recovery = 91%  Analysis Date = 12/28/12 
 Pct Recovery = 91%  Analysis Date = 12/28/12 
 Pct Recovery = 91%  Analysis Date = 12/26/12 
 Pct Recovery = 91%  Analysis Date = 12/26/12 
 Pct Recovery = 91%  Analysis Date = 12/23/12 
 Pct Recovery = 91%  Analysis Date = 12/23/12 
 Pct Recovery = 91%  Analysis Date = 12/21/12 
 Pct Recovery = 91%  Analysis Date = 12/21/12 
 Pct Recovery = 91%  Analysis Date = 12/18/12 
 Pct Recovery = 91%  Analysis Date = 12/18/12 
 Pct Recovery = 91%  Analysis Date = 12/16/12 
 Pct Recovery = 91%  Analysis Date = 12/16/12 
 Pct Recovery = 91%  Analysis Date = 12/14/12 
 Pct Recovery = 91%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PREDNISOLONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 74% . 74% 0%
>= Reporting Level 13 74% 24% 66% 4%
Total 14 74% 23% 67% 7%

Sample Statistics
PREDNISOLONE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PREDNISONE
METHOD: LC9017 , TESTIDCODE: 67467LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 96%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 161%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 80%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 84%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 104%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 80%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 73%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 102%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 106%  Analysis Date = 04/09/14 
 Pct Recovery = 66%  Analysis Date = 04/07/14 
 Pct Recovery = 66%  Analysis Date = 04/07/14 
 Pct Recovery = 66%  Analysis Date = 04/05/14 
 Pct Recovery = 66%  Analysis Date = 04/05/14 
 Pct Recovery = 66%  Analysis Date = 04/02/14 
 Pct Recovery = 67%  Analysis Date = 04/02/14 
 Pct Recovery = 67%  Analysis Date = 03/31/14 
 Pct Recovery = 67%  Analysis Date = 03/31/14 
 Pct Recovery = 67%  Analysis Date = 03/28/14 
 Pct Recovery = 67%  Analysis Date = 03/28/14 
 Pct Recovery = 67%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/26/14 
 Pct Recovery = 68%  Analysis Date = 03/24/14 
 Pct Recovery = 68%  Analysis Date = 03/24/14 
 Pct Recovery = 68%  Analysis Date = 03/21/14 
 Pct Recovery = 68%  Analysis Date = 03/21/14 
 Pct Recovery = 68%  Analysis Date = 03/19/14 
 Pct Recovery = 68%  Analysis Date = 03/19/14 
 Pct Recovery = 68%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/16/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/14/14 
 Pct Recovery = 69%  Analysis Date = 03/12/14 
 Pct Recovery = 69%  Analysis Date = 03/12/14 
 Pct Recovery = 69%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/09/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/07/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/04/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 03/02/14 
 Pct Recovery = 70%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/28/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/25/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/23/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/20/14 
 Pct Recovery = 71%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/22/14 
 Pct Recovery = 75%  Analysis Date = 01/20/14 
 Pct Recovery = 75%  Analysis Date = 01/20/14 
 Pct Recovery = 75%  Analysis Date = 01/18/14 
 Pct Recovery = 75%  Analysis Date = 01/18/14 
 Pct Recovery = 75%  Analysis Date = 01/15/14 
 Pct Recovery = 75%  Analysis Date = 01/15/14 
 Pct Recovery = 75%  Analysis Date = 01/13/14 
 Pct Recovery = 76%  Analysis Date = 01/13/14 
 Pct Recovery = 76%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/10/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/08/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/06/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/03/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/15/13 
 Pct Recovery = 77%  Analysis Date = 12/15/13 
 Pct Recovery = 77%  Analysis Date = 12/12/13 
 Pct Recovery = 77%  Analysis Date = 12/12/13 
 Pct Recovery = 77%  Analysis Date = 12/10/13 
 Pct Recovery = 77%  Analysis Date = 12/10/13 
 Pct Recovery = 77%  Analysis Date = 12/08/13 
 Pct Recovery = 78%  Analysis Date = 12/08/13 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 Pct Recovery = 78%  Analysis Date = 12/03/13 
 Pct Recovery = 78%  Analysis Date = 12/03/13 
 Pct Recovery = 78%  Analysis Date = 11/30/13 
 Pct Recovery = 78%  Analysis Date = 11/30/13 
 Pct Recovery = 78%  Analysis Date = 11/28/13 
 Pct Recovery = 78%  Analysis Date = 11/28/13 
 Pct Recovery = 78%  Analysis Date = 11/26/13 
 Pct Recovery = 78%  Analysis Date = 11/26/13 
 Pct Recovery = 78%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/21/13 
 Pct Recovery = 79%  Analysis Date = 11/21/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/18/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/16/13 
 Pct Recovery = 79%  Analysis Date = 11/13/13 
 Pct Recovery = 79%  Analysis Date = 11/13/13 
 Pct Recovery = 79%  Analysis Date = 11/11/13 
 Pct Recovery = 79%  Analysis Date = 11/11/13 
 Pct Recovery = 79%  Analysis Date = 11/09/13 
 Pct Recovery = 79%  Analysis Date = 11/09/13 
 Pct Recovery = 79%  Analysis Date = 11/06/13 
 Pct Recovery = 79%  Analysis Date = 11/06/13 
 Pct Recovery = 79%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/04/13 
 Pct Recovery = 80%  Analysis Date = 11/01/13 
 Pct Recovery = 80%  Analysis Date = 11/01/13 
 Pct Recovery = 80%  Analysis Date = 10/30/13 
 Pct Recovery = 80%  Analysis Date = 10/30/13 
 Pct Recovery = 80%  Analysis Date = 10/28/13 
 Pct Recovery = 80%  Analysis Date = 10/28/13 
 Pct Recovery = 80%  Analysis Date = 10/25/13 
 Pct Recovery = 80%  Analysis Date = 10/25/13 
 Pct Recovery = 80%  Analysis Date = 10/23/13 
 Pct Recovery = 80%  Analysis Date = 10/23/13 
 Pct Recovery = 80%  Analysis Date = 10/20/13 
 Pct Recovery = 80%  Analysis Date = 10/20/13 
 Pct Recovery = 80%  Analysis Date = 10/18/13 
 Pct Recovery = 80%  Analysis Date = 10/18/13 
 Pct Recovery = 80%  Analysis Date = 10/16/13 
 Pct Recovery = 80%  Analysis Date = 10/16/13 
 Pct Recovery = 80%  Analysis Date = 10/13/13 
 Pct Recovery = 80%  Analysis Date = 10/13/13 
 Pct Recovery = 80%  Analysis Date = 10/11/13 
 Pct Recovery = 80%  Analysis Date = 10/11/13 
 Pct Recovery = 80%  Analysis Date = 10/08/13 
 Pct Recovery = 80%  Analysis Date = 10/08/13 
 Pct Recovery = 80%  Analysis Date = 10/06/13 
 Pct Recovery = 80%  Analysis Date = 10/06/13 
 Pct Recovery = 80%  Analysis Date = 10/04/13 
 Pct Recovery = 80%  Analysis Date = 10/04/13 
 Pct Recovery = 80%  Analysis Date = 10/01/13 
 Pct Recovery = 81%  Analysis Date = 10/01/13 
 Pct Recovery = 81%  Analysis Date = 09/29/13 
 Pct Recovery = 81%  Analysis Date = 09/29/13 
 Pct Recovery = 81%  Analysis Date = 09/26/13 
 Pct Recovery = 81%  Analysis Date = 09/26/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/24/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/21/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/19/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 Pct Recovery = 81%  Analysis Date = 09/14/13 
 Pct Recovery = 81%  Analysis Date = 09/14/13 
 Pct Recovery = 81%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/12/13 
 Pct Recovery = 81%  Analysis Date = 09/09/13 
 Pct Recovery = 81%  Analysis Date = 09/09/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/26/13 
 Pct Recovery = 81%  Analysis Date = 08/26/13 
 Pct Recovery = 81%  Analysis Date = 08/24/13 
 Pct Recovery = 81%  Analysis Date = 08/24/13 
 Pct Recovery = 81%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/16/13 
 Pct Recovery = 82%  Analysis Date = 08/16/13 
 Pct Recovery = 82%  Analysis Date = 08/14/13 
 Pct Recovery = 82%  Analysis Date = 08/14/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/11/13 
 Pct Recovery = 82%  Analysis Date = 08/09/13 
 Pct Recovery = 82%  Analysis Date = 08/09/13 
 Pct Recovery = 82%  Analysis Date = 08/07/13 
 Pct Recovery = 82%  Analysis Date = 08/07/13 
 Pct Recovery = 82%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/04/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/30/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/28/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/26/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/23/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/21/13 
 Pct Recovery = 82%  Analysis Date = 07/18/13 
 Pct Recovery = 82%  Analysis Date = 07/18/13 
 Pct Recovery = 82%  Analysis Date = 07/16/13 
 Pct Recovery = 82%  Analysis Date = 07/16/13 
 Pct Recovery = 82%  Analysis Date = 07/14/13 
 Pct Recovery = 82%  Analysis Date = 07/14/13 
 Pct Recovery = 82%  Analysis Date = 07/11/13 
 Pct Recovery = 82%  Analysis Date = 07/11/13 
 Pct Recovery = 82%  Analysis Date = 07/09/13 
 Pct Recovery = 82%  Analysis Date = 07/09/13 
 Pct Recovery = 82%  Analysis Date = 07/06/13 
 Pct Recovery = 82%  Analysis Date = 07/06/13 
 Pct Recovery = 82%  Analysis Date = 07/04/13 
 Pct Recovery = 82%  Analysis Date = 07/04/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 07/02/13 
 Pct Recovery = 82%  Analysis Date = 06/29/13 
 Pct Recovery = 82%  Analysis Date = 06/29/13 
 Pct Recovery = 82%  Analysis Date = 06/27/13 
 Pct Recovery = 82%  Analysis Date = 06/27/13 
 Pct Recovery = 82%  Analysis Date = 06/24/13 
 Pct Recovery = 82%  Analysis Date = 06/24/13 
 Pct Recovery = 82%  Analysis Date = 06/22/13 
 Pct Recovery = 82%  Analysis Date = 06/22/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/17/13 
 Pct Recovery = 82%  Analysis Date = 06/17/13 
 Pct Recovery = 82%  Analysis Date = 06/15/13 
 Pct Recovery = 82%  Analysis Date = 06/15/13 
 Pct Recovery = 82%  Analysis Date = 06/12/13 
 Pct Recovery = 82%  Analysis Date = 06/12/13 
 Pct Recovery = 82%  Analysis Date = 06/10/13 
 Pct Recovery = 82%  Analysis Date = 06/10/13 
 Pct Recovery = 82%  Analysis Date = 06/07/13 
 Pct Recovery = 82%  Analysis Date = 06/07/13 
 Pct Recovery = 82%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/05/13 
 Pct Recovery = 82%  Analysis Date = 06/03/13 
 Pct Recovery = 82%  Analysis Date = 06/03/13 
 Pct Recovery = 82%  Analysis Date = 05/31/13 
 Pct Recovery = 82%  Analysis Date = 05/31/13 
 Pct Recovery = 82%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/29/13 
 Pct Recovery = 82%  Analysis Date = 05/26/13 
 Pct Recovery = 82%  Analysis Date = 05/26/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/24/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/19/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/17/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/07/13 
 Pct Recovery = 82%  Analysis Date = 05/07/13 
 Pct Recovery = 82%  Analysis Date = 05/05/13 
 Pct Recovery = 82%  Analysis Date = 05/05/13 
 Pct Recovery = 82%  Analysis Date = 05/02/13 
 Pct Recovery = 82%  Analysis Date = 05/02/13 
 Pct Recovery = 82%  Analysis Date = 04/30/13 
 Pct Recovery = 82%  Analysis Date = 04/30/13 
 Pct Recovery = 82%  Analysis Date = 04/27/13 
 Pct Recovery = 81%  Analysis Date = 04/27/13 
 Pct Recovery = 81%  Analysis Date = 04/25/13 
 Pct Recovery = 81%  Analysis Date = 04/25/13 
 Pct Recovery = 81%  Analysis Date = 04/23/13 
 Pct Recovery = 82%  Analysis Date = 04/23/13 
 Pct Recovery = 82%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/20/13 
 Pct Recovery = 83%  Analysis Date = 04/18/13 
 Pct Recovery = 84%  Analysis Date = 04/18/13 
 Pct Recovery = 84%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 86%  Analysis Date = 04/13/13 
 Pct Recovery = 86%  Analysis Date = 04/11/13 
 Pct Recovery = 87%  Analysis Date = 04/11/13 
 Pct Recovery = 87%  Analysis Date = 04/08/13 
 Pct Recovery = 88%  Analysis Date = 04/08/13 
 Pct Recovery = 88%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/06/13 
 Pct Recovery = 89%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 04/01/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 92%  Analysis Date = 03/30/13 
 Pct Recovery = 92%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/20/13 
 Pct Recovery = 95%  Analysis Date = 03/20/13 
 Pct Recovery = 95%  Analysis Date = 03/17/13 
 Pct Recovery = 96%  Analysis Date = 03/17/13 
 Pct Recovery = 96%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/15/13 
 Pct Recovery = 97%  Analysis Date = 03/13/13 
 Pct Recovery = 97%  Analysis Date = 03/13/13 
 Pct Recovery = 97%  Analysis Date = 03/10/13 
 Pct Recovery = 98%  Analysis Date = 03/10/13 
 Pct Recovery = 98%  Analysis Date = 03/08/13 
 Pct Recovery = 99%  Analysis Date = 03/08/13 
 Pct Recovery = 99%  Analysis Date = 03/05/13 
 Pct Recovery = 100%  Analysis Date = 03/05/13 
 Pct Recovery = 100%  Analysis Date = 03/03/13 
 Pct Recovery = 101%  Analysis Date = 03/03/13 
 Pct Recovery = 101%  Analysis Date = 03/01/13 
 Pct Recovery = 102%  Analysis Date = 03/01/13 
 Pct Recovery = 102%  Analysis Date = 02/26/13 
 Pct Recovery = 102%  Analysis Date = 02/26/13 
 Pct Recovery = 102%  Analysis Date = 02/24/13 
 Pct Recovery = 103%  Analysis Date = 02/24/13 
 Pct Recovery = 103%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/21/13 
 Pct Recovery = 104%  Analysis Date = 02/19/13 
 Pct Recovery = 105%  Analysis Date = 02/19/13 
 Pct Recovery = 105%  Analysis Date = 02/17/13 
 Pct Recovery = 106%  Analysis Date = 02/17/13 
 Pct Recovery = 106%  Analysis Date = 02/14/13 
 Pct Recovery = 107%  Analysis Date = 02/14/13 
 Pct Recovery = 107%  Analysis Date = 02/12/13 
 Pct Recovery = 107%  Analysis Date = 02/12/13 
 Pct Recovery = 107%  Analysis Date = 02/09/13 
 Pct Recovery = 108%  Analysis Date = 02/09/13 
 Pct Recovery = 108%  Analysis Date = 02/07/13 
 Pct Recovery = 109%  Analysis Date = 02/07/13 
 Pct Recovery = 109%  Analysis Date = 02/05/13 
 Pct Recovery = 110%  Analysis Date = 02/05/13 
 Pct Recovery = 110%  Analysis Date = 02/02/13 
 Pct Recovery = 111%  Analysis Date = 02/02/13 
 Pct Recovery = 111%  Analysis Date = 01/31/13 
 Pct Recovery = 112%  Analysis Date = 01/31/13 
 Pct Recovery = 112%  Analysis Date = 01/28/13 
 Pct Recovery = 112%  Analysis Date = 01/28/13 
 Pct Recovery = 112%  Analysis Date = 01/26/13 
 Pct Recovery = 113%  Analysis Date = 01/26/13 
 Pct Recovery = 113%  Analysis Date = 01/23/13 
 Pct Recovery = 114%  Analysis Date = 01/23/13 
 Pct Recovery = 114%  Analysis Date = 01/21/13 
 Pct Recovery = 114%  Analysis Date = 01/21/13 
 Pct Recovery = 114%  Analysis Date = 01/19/13 
 Pct Recovery = 115%  Analysis Date = 01/19/13 
 Pct Recovery = 115%  Analysis Date = 01/16/13 
 Pct Recovery = 115%  Analysis Date = 01/16/13 
 Pct Recovery = 115%  Analysis Date = 01/14/13 
 Pct Recovery = 116%  Analysis Date = 01/14/13 
 Pct Recovery = 116%  Analysis Date = 01/11/13 
 Pct Recovery = 116%  Analysis Date = 01/11/13 
 Pct Recovery = 116%  Analysis Date = 01/09/13 
 Pct Recovery = 116%  Analysis Date = 01/09/13 
 Pct Recovery = 116%  Analysis Date = 01/07/13 
 Pct Recovery = 117%  Analysis Date = 01/07/13 
 Pct Recovery = 117%  Analysis Date = 01/04/13 
 Pct Recovery = 117%  Analysis Date = 01/04/13 
 Pct Recovery = 117%  Analysis Date = 01/02/13 
 Pct Recovery = 118%  Analysis Date = 01/02/13 
 Pct Recovery = 118%  Analysis Date = 12/30/12 
 Pct Recovery = 118%  Analysis Date = 12/30/12 
 Pct Recovery = 118%  Analysis Date = 12/28/12 
 Pct Recovery = 119%  Analysis Date = 12/28/12 
 Pct Recovery = 119%  Analysis Date = 12/26/12 
 Pct Recovery = 119%  Analysis Date = 12/26/12 
 Pct Recovery = 119%  Analysis Date = 12/23/12 
 Pct Recovery = 119%  Analysis Date = 12/23/12 
 Pct Recovery = 119%  Analysis Date = 12/21/12 
 Pct Recovery = 120%  Analysis Date = 12/21/12 
 Pct Recovery = 120%  Analysis Date = 12/18/12 
 Pct Recovery = 120%  Analysis Date = 12/18/12 
 Pct Recovery = 120%  Analysis Date = 12/16/12 
 Pct Recovery = 121%  Analysis Date = 12/16/12 
 Pct Recovery = 121%  Analysis Date = 12/14/12 
 Pct Recovery = 121%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PREDNISONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 106% . 106% 0%
>= Reporting Level 13 86% 27% 80% 17%
Total 14 87% 27% 80% 22%

Sample Statistics
PREDNISONE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PROMETHAZINE
METHOD: LC9017 , TESTIDCODE: 67524LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 33%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 32%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 30%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 22%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 35%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 39%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 26%  Analysis Date = 04/09/14 
 Pct Recovery = 33%  Analysis Date = 04/07/14 
 Pct Recovery = 33%  Analysis Date = 04/07/14 
 Pct Recovery = 33%  Analysis Date = 04/05/14 
 Pct Recovery = 33%  Analysis Date = 04/05/14 
 Pct Recovery = 33%  Analysis Date = 04/03/14 
 Pct Recovery = 32%  Analysis Date = 04/03/14 
 Pct Recovery = 32%  Analysis Date = 04/01/14 
 Pct Recovery = 32%  Analysis Date = 04/01/14 
 Pct Recovery = 32%  Analysis Date = 03/30/14 
 Pct Recovery = 32%  Analysis Date = 03/30/14 
 Pct Recovery = 32%  Analysis Date = 03/28/14 
 Pct Recovery = 32%  Analysis Date = 03/28/14 
 Pct Recovery = 32%  Analysis Date = 03/26/14 
 Pct Recovery = 32%  Analysis Date = 03/26/14 
 Pct Recovery = 32%  Analysis Date = 03/24/14 
 Pct Recovery = 31%  Analysis Date = 03/24/14 
 Pct Recovery = 31%  Analysis Date = 03/22/14 
 Pct Recovery = 31%  Analysis Date = 03/22/14 
 Pct Recovery = 31%  Analysis Date = 03/20/14 
 Pct Recovery = 31%  Analysis Date = 03/20/14 
 Pct Recovery = 31%  Analysis Date = 03/18/14 
 Pct Recovery = 31%  Analysis Date = 03/18/14 
 Pct Recovery = 31%  Analysis Date = 03/16/14 
 Pct Recovery = 31%  Analysis Date = 03/16/14 
 Pct Recovery = 31%  Analysis Date = 03/14/14 
 Pct Recovery = 30%  Analysis Date = 03/14/14 
 Pct Recovery = 30%  Analysis Date = 03/12/14 
 Pct Recovery = 30%  Analysis Date = 03/12/14 
 Pct Recovery = 30%  Analysis Date = 03/10/14 
 Pct Recovery = 30%  Analysis Date = 03/10/14 
 Pct Recovery = 30%  Analysis Date = 03/08/14 
 Pct Recovery = 30%  Analysis Date = 03/08/14 
 Pct Recovery = 30%  Analysis Date = 03/06/14 
 Pct Recovery = 30%  Analysis Date = 03/06/14 
 Pct Recovery = 30%  Analysis Date = 03/04/14 
 Pct Recovery = 29%  Analysis Date = 03/04/14 
 Pct Recovery = 29%  Analysis Date = 03/02/14 
 Pct Recovery = 29%  Analysis Date = 03/02/14 
 Pct Recovery = 29%  Analysis Date = 02/28/14 
 Pct Recovery = 29%  Analysis Date = 02/28/14 
 Pct Recovery = 29%  Analysis Date = 02/26/14 
 Pct Recovery = 29%  Analysis Date = 02/26/14 
 Pct Recovery = 29%  Analysis Date = 02/24/14 
 Pct Recovery = 29%  Analysis Date = 02/24/14 
 Pct Recovery = 29%  Analysis Date = 02/22/14 
 Pct Recovery = 28%  Analysis Date = 02/22/14 
 Pct Recovery = 28%  Analysis Date = 02/20/14 
 Pct Recovery = 28%  Analysis Date = 02/20/14 
 Pct Recovery = 28%  Analysis Date = 02/18/14 
 Pct Recovery = 28%  Analysis Date = 02/18/14 
 Pct Recovery = 28%  Analysis Date = 02/16/14 
 Pct Recovery = 28%  Analysis Date = 02/16/14 
 Pct Recovery = 28%  Analysis Date = 02/14/14 
 Pct Recovery = 28%  Analysis Date = 02/14/14 
 Pct Recovery = 28%  Analysis Date = 02/12/14 
 Pct Recovery = 28%  Analysis Date = 02/12/14 
 Pct Recovery = 28%  Analysis Date = 02/10/14 
 Pct Recovery = 27%  Analysis Date = 02/10/14 
 Pct Recovery = 27%  Analysis Date = 02/08/14 
 Pct Recovery = 27%  Analysis Date = 02/08/14 
 Pct Recovery = 27%  Analysis Date = 02/06/14 
 Pct Recovery = 27%  Analysis Date = 02/06/14 
 Pct Recovery = 27%  Analysis Date = 02/04/14 
 Pct Recovery = 27%  Analysis Date = 02/04/14 
 Pct Recovery = 27%  Analysis Date = 02/02/14 
 Pct Recovery = 27%  Analysis Date = 02/02/14 
 Pct Recovery = 27%  Analysis Date = 01/30/14 
 Pct Recovery = 27%  Analysis Date = 01/30/14 
 Pct Recovery = 27%  Analysis Date = 01/28/14 
 Pct Recovery = 27%  Analysis Date = 01/28/14 
 Pct Recovery = 27%  Analysis Date = 01/26/14 
 Pct Recovery = 27%  Analysis Date = 01/26/14 
 Pct Recovery = 27%  Analysis Date = 01/24/14 
 Pct Recovery = 27%  Analysis Date = 01/24/14 
 Pct Recovery = 27%  Analysis Date = 01/22/14 
 Pct Recovery = 26%  Analysis Date = 01/22/14 
 Pct Recovery = 26%  Analysis Date = 01/20/14 
 Pct Recovery = 26%  Analysis Date = 01/20/14 
 Pct Recovery = 26%  Analysis Date = 01/18/14 
 Pct Recovery = 26%  Analysis Date = 01/18/14 
 Pct Recovery = 26%  Analysis Date = 01/16/14 
 Pct Recovery = 26%  Analysis Date = 01/16/14 
 Pct Recovery = 26%  Analysis Date = 01/14/14 
 Pct Recovery = 26%  Analysis Date = 01/14/14 
 Pct Recovery = 26%  Analysis Date = 01/12/14 
 Pct Recovery = 26%  Analysis Date = 01/12/14 
 Pct Recovery = 26%  Analysis Date = 01/10/14 
 Pct Recovery = 26%  Analysis Date = 01/10/14 
 Pct Recovery = 26%  Analysis Date = 01/08/14 
 Pct Recovery = 27%  Analysis Date = 01/08/14 
 Pct Recovery = 27%  Analysis Date = 01/06/14 
 Pct Recovery = 27%  Analysis Date = 01/06/14 
 Pct Recovery = 27%  Analysis Date = 01/04/14 
 Pct Recovery = 27%  Analysis Date = 01/04/14 
 Pct Recovery = 27%  Analysis Date = 01/02/14 
 Pct Recovery = 27%  Analysis Date = 01/02/14 
 Pct Recovery = 27%  Analysis Date = 12/31/13 
 Pct Recovery = 27%  Analysis Date = 12/31/13 
 Pct Recovery = 27%  Analysis Date = 12/29/13 
 Pct Recovery = 27%  Analysis Date = 12/29/13 
 Pct Recovery = 27%  Analysis Date = 12/27/13 
 Pct Recovery = 27%  Analysis Date = 12/27/13 
 Pct Recovery = 27%  Analysis Date = 12/25/13 
 Pct Recovery = 27%  Analysis Date = 12/25/13 
 Pct Recovery = 27%  Analysis Date = 12/23/13 
 Pct Recovery = 28%  Analysis Date = 12/23/13 
 Pct Recovery = 28%  Analysis Date = 12/21/13 
 Pct Recovery = 28%  Analysis Date = 12/21/13 
 Pct Recovery = 28%  Analysis Date = 12/19/13 
 Pct Recovery = 28%  Analysis Date = 12/19/13 
 Pct Recovery = 28%  Analysis Date = 12/17/13 
 Pct Recovery = 28%  Analysis Date = 12/17/13 
 Pct Recovery = 28%  Analysis Date = 12/15/13 
 Pct Recovery = 28%  Analysis Date = 12/15/13 
 Pct Recovery = 28%  Analysis Date = 12/13/13 
 Pct Recovery = 28%  Analysis Date = 12/13/13 
 Pct Recovery = 28%  Analysis Date = 12/11/13 
 Pct Recovery = 28%  Analysis Date = 12/11/13 
 Pct Recovery = 28%  Analysis Date = 12/09/13 
 Pct Recovery = 28%  Analysis Date = 12/09/13 
 Pct Recovery = 28%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/07/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 12/03/13 
 Pct Recovery = 29%  Analysis Date = 12/01/13 
 Pct Recovery = 29%  Analysis Date = 12/01/13 
 Pct Recovery = 29%  Analysis Date = 11/29/13 
 Pct Recovery = 29%  Analysis Date = 11/29/13 
 Pct Recovery = 29%  Analysis Date = 11/27/13 
 Pct Recovery = 29%  Analysis Date = 11/27/13 
 Pct Recovery = 29%  Analysis Date = 11/24/13 
 Pct Recovery = 30%  Analysis Date = 11/24/13 
 Pct Recovery = 30%  Analysis Date = 11/22/13 
 Pct Recovery = 30%  Analysis Date = 11/22/13 
 Pct Recovery = 30%  Analysis Date = 11/20/13 
 Pct Recovery = 30%  Analysis Date = 11/20/13 
 Pct Recovery = 30%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/14/13 
 Pct Recovery = 30%  Analysis Date = 11/14/13 
 Pct Recovery = 30%  Analysis Date = 11/12/13 
 Pct Recovery = 30%  Analysis Date = 11/12/13 
 Pct Recovery = 30%  Analysis Date = 11/10/13 
 Pct Recovery = 30%  Analysis Date = 11/10/13 
 Pct Recovery = 30%  Analysis Date = 11/08/13 
 Pct Recovery = 30%  Analysis Date = 11/08/13 
 Pct Recovery = 30%  Analysis Date = 11/06/13 
 Pct Recovery = 30%  Analysis Date = 11/06/13 
 Pct Recovery = 30%  Analysis Date = 11/04/13 
 Pct Recovery = 30%  Analysis Date = 11/04/13 
 Pct Recovery = 30%  Analysis Date = 11/02/13 
 Pct Recovery = 30%  Analysis Date = 11/02/13 
 Pct Recovery = 30%  Analysis Date = 10/31/13 
 Pct Recovery = 30%  Analysis Date = 10/31/13 
 Pct Recovery = 30%  Analysis Date = 10/29/13 
 Pct Recovery = 30%  Analysis Date = 10/29/13 
 Pct Recovery = 30%  Analysis Date = 10/27/13 
 Pct Recovery = 30%  Analysis Date = 10/27/13 
 Pct Recovery = 30%  Analysis Date = 10/25/13 
 Pct Recovery = 30%  Analysis Date = 10/25/13 
 Pct Recovery = 30%  Analysis Date = 10/23/13 
 Pct Recovery = 30%  Analysis Date = 10/23/13 
 Pct Recovery = 30%  Analysis Date = 10/21/13 
 Pct Recovery = 30%  Analysis Date = 10/21/13 
 Pct Recovery = 30%  Analysis Date = 10/19/13 
 Pct Recovery = 30%  Analysis Date = 10/19/13 
 Pct Recovery = 30%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/17/13 
 Pct Recovery = 31%  Analysis Date = 10/15/13 
 Pct Recovery = 31%  Analysis Date = 10/15/13 
 Pct Recovery = 31%  Analysis Date = 10/13/13 
 Pct Recovery = 31%  Analysis Date = 10/13/13 
 Pct Recovery = 31%  Analysis Date = 10/11/13 
 Pct Recovery = 31%  Analysis Date = 10/11/13 
 Pct Recovery = 31%  Analysis Date = 10/09/13 
 Pct Recovery = 31%  Analysis Date = 10/09/13 
 Pct Recovery = 31%  Analysis Date = 10/07/13 
 Pct Recovery = 31%  Analysis Date = 10/07/13 
 Pct Recovery = 31%  Analysis Date = 10/05/13 
 Pct Recovery = 31%  Analysis Date = 10/05/13 
 Pct Recovery = 31%  Analysis Date = 10/03/13 
 Pct Recovery = 31%  Analysis Date = 10/03/13 
 Pct Recovery = 31%  Analysis Date = 10/01/13 
 Pct Recovery = 31%  Analysis Date = 10/01/13 
 Pct Recovery = 31%  Analysis Date = 09/29/13 
 Pct Recovery = 31%  Analysis Date = 09/29/13 
 Pct Recovery = 31%  Analysis Date = 09/27/13 
 Pct Recovery = 31%  Analysis Date = 09/27/13 
 Pct Recovery = 31%  Analysis Date = 09/25/13 
 Pct Recovery = 31%  Analysis Date = 09/25/13 
 Pct Recovery = 31%  Analysis Date = 09/23/13 
 Pct Recovery = 31%  Analysis Date = 09/23/13 
 Pct Recovery = 31%  Analysis Date = 09/21/13 
 Pct Recovery = 31%  Analysis Date = 09/21/13 
 Pct Recovery = 31%  Analysis Date = 09/18/13 
 Pct Recovery = 31%  Analysis Date = 09/18/13 
 Pct Recovery = 31%  Analysis Date = 09/16/13 
 Pct Recovery = 31%  Analysis Date = 09/16/13 
 Pct Recovery = 31%  Analysis Date = 09/14/13 
 Pct Recovery = 31%  Analysis Date = 09/14/13 
 Pct Recovery = 31%  Analysis Date = 09/12/13 
 Pct Recovery = 31%  Analysis Date = 09/12/13 
 Pct Recovery = 31%  Analysis Date = 09/10/13 
 Pct Recovery = 31%  Analysis Date = 09/10/13 
 Pct Recovery = 31%  Analysis Date = 09/08/13 
 Pct Recovery = 31%  Analysis Date = 09/08/13 
 Pct Recovery = 31%  Analysis Date = 09/06/13 
 Pct Recovery = 31%  Analysis Date = 09/06/13 
 Pct Recovery = 31%  Analysis Date = 09/04/13 
 Pct Recovery = 31%  Analysis Date = 09/04/13 
 Pct Recovery = 31%  Analysis Date = 09/02/13 
 Pct Recovery = 31%  Analysis Date = 09/02/13 
 Pct Recovery = 31%  Analysis Date = 08/31/13 
 Pct Recovery = 31%  Analysis Date = 08/31/13 
 Pct Recovery = 31%  Analysis Date = 08/29/13 
 Pct Recovery = 31%  Analysis Date = 08/29/13 
 Pct Recovery = 31%  Analysis Date = 08/27/13 
 Pct Recovery = 31%  Analysis Date = 08/27/13 
 Pct Recovery = 31%  Analysis Date = 08/25/13 
 Pct Recovery = 32%  Analysis Date = 08/25/13 
 Pct Recovery = 32%  Analysis Date = 08/23/13 
 Pct Recovery = 32%  Analysis Date = 08/23/13 
 Pct Recovery = 32%  Analysis Date = 08/21/13 
 Pct Recovery = 32%  Analysis Date = 08/21/13 
 Pct Recovery = 32%  Analysis Date = 08/19/13 
 Pct Recovery = 32%  Analysis Date = 08/19/13 
 Pct Recovery = 32%  Analysis Date = 08/17/13 
 Pct Recovery = 32%  Analysis Date = 08/17/13 
 Pct Recovery = 32%  Analysis Date = 08/15/13 
 Pct Recovery = 32%  Analysis Date = 08/15/13 
 Pct Recovery = 32%  Analysis Date = 08/13/13 
 Pct Recovery = 32%  Analysis Date = 08/13/13 
 Pct Recovery = 32%  Analysis Date = 08/11/13 
 Pct Recovery = 32%  Analysis Date = 08/11/13 
 Pct Recovery = 32%  Analysis Date = 08/09/13 
 Pct Recovery = 32%  Analysis Date = 08/09/13 
 Pct Recovery = 32%  Analysis Date = 08/07/13 
 Pct Recovery = 32%  Analysis Date = 08/07/13 
 Pct Recovery = 32%  Analysis Date = 08/05/13 
 Pct Recovery = 32%  Analysis Date = 08/05/13 
 Pct Recovery = 32%  Analysis Date = 08/03/13 
 Pct Recovery = 32%  Analysis Date = 08/03/13 
 Pct Recovery = 32%  Analysis Date = 08/01/13 
 Pct Recovery = 32%  Analysis Date = 08/01/13 
 Pct Recovery = 32%  Analysis Date = 07/30/13 
 Pct Recovery = 32%  Analysis Date = 07/30/13 
 Pct Recovery = 32%  Analysis Date = 07/28/13 
 Pct Recovery = 32%  Analysis Date = 07/28/13 
 Pct Recovery = 32%  Analysis Date = 07/26/13 
 Pct Recovery = 32%  Analysis Date = 07/26/13 
 Pct Recovery = 32%  Analysis Date = 07/24/13 
 Pct Recovery = 32%  Analysis Date = 07/24/13 
 Pct Recovery = 32%  Analysis Date = 07/22/13 
 Pct Recovery = 32%  Analysis Date = 07/22/13 
 Pct Recovery = 32%  Analysis Date = 07/20/13 
 Pct Recovery = 32%  Analysis Date = 07/20/13 
 Pct Recovery = 32%  Analysis Date = 07/18/13 
 Pct Recovery = 32%  Analysis Date = 07/18/13 
 Pct Recovery = 32%  Analysis Date = 07/16/13 
 Pct Recovery = 32%  Analysis Date = 07/16/13 
 Pct Recovery = 32%  Analysis Date = 07/14/13 
 Pct Recovery = 32%  Analysis Date = 07/14/13 
 Pct Recovery = 32%  Analysis Date = 07/11/13 
 Pct Recovery = 32%  Analysis Date = 07/11/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/07/13 
 Pct Recovery = 32%  Analysis Date = 07/07/13 
 Pct Recovery = 32%  Analysis Date = 07/05/13 
 Pct Recovery = 32%  Analysis Date = 07/05/13 
 Pct Recovery = 32%  Analysis Date = 07/03/13 
 Pct Recovery = 32%  Analysis Date = 07/03/13 
 Pct Recovery = 32%  Analysis Date = 07/01/13 
 Pct Recovery = 33%  Analysis Date = 07/01/13 
 Pct Recovery = 33%  Analysis Date = 06/29/13 
 Pct Recovery = 33%  Analysis Date = 06/29/13 
 Pct Recovery = 33%  Analysis Date = 06/27/13 
 Pct Recovery = 33%  Analysis Date = 06/27/13 
 Pct Recovery = 33%  Analysis Date = 06/25/13 
 Pct Recovery = 33%  Analysis Date = 06/25/13 
 Pct Recovery = 33%  Analysis Date = 06/23/13 
 Pct Recovery = 33%  Analysis Date = 06/23/13 
 Pct Recovery = 33%  Analysis Date = 06/21/13 
 Pct Recovery = 33%  Analysis Date = 06/21/13 
 Pct Recovery = 33%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/17/13 
 Pct Recovery = 33%  Analysis Date = 06/17/13 
 Pct Recovery = 33%  Analysis Date = 06/15/13 
 Pct Recovery = 33%  Analysis Date = 06/15/13 
 Pct Recovery = 33%  Analysis Date = 06/13/13 
 Pct Recovery = 33%  Analysis Date = 06/13/13 
 Pct Recovery = 33%  Analysis Date = 06/11/13 
 Pct Recovery = 33%  Analysis Date = 06/11/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/09/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/05/13 
 Pct Recovery = 33%  Analysis Date = 06/03/13 
 Pct Recovery = 33%  Analysis Date = 06/03/13 
 Pct Recovery = 33%  Analysis Date = 06/01/13 
 Pct Recovery = 33%  Analysis Date = 06/01/13 
 Pct Recovery = 33%  Analysis Date = 05/30/13 
 Pct Recovery = 33%  Analysis Date = 05/30/13 
 Pct Recovery = 33%  Analysis Date = 05/28/13 
 Pct Recovery = 33%  Analysis Date = 05/28/13 
 Pct Recovery = 33%  Analysis Date = 05/26/13 
 Pct Recovery = 33%  Analysis Date = 05/26/13 
 Pct Recovery = 33%  Analysis Date = 05/24/13 
 Pct Recovery = 33%  Analysis Date = 05/24/13 
 Pct Recovery = 33%  Analysis Date = 05/22/13 
 Pct Recovery = 33%  Analysis Date = 05/22/13 
 Pct Recovery = 33%  Analysis Date = 05/20/13 
 Pct Recovery = 33%  Analysis Date = 05/20/13 
 Pct Recovery = 33%  Analysis Date = 05/18/13 
 Pct Recovery = 33%  Analysis Date = 05/18/13 
 Pct Recovery = 33%  Analysis Date = 05/16/13 
 Pct Recovery = 33%  Analysis Date = 05/16/13 
 Pct Recovery = 33%  Analysis Date = 05/14/13 
 Pct Recovery = 33%  Analysis Date = 05/14/13 
 Pct Recovery = 33%  Analysis Date = 05/12/13 
 Pct Recovery = 33%  Analysis Date = 05/12/13 
 Pct Recovery = 33%  Analysis Date = 05/10/13 
 Pct Recovery = 34%  Analysis Date = 05/10/13 
 Pct Recovery = 34%  Analysis Date = 05/08/13 
 Pct Recovery = 34%  Analysis Date = 05/08/13 
 Pct Recovery = 34%  Analysis Date = 05/05/13 
 Pct Recovery = 34%  Analysis Date = 05/05/13 
 Pct Recovery = 34%  Analysis Date = 05/03/13 
 Pct Recovery = 34%  Analysis Date = 05/03/13 
 Pct Recovery = 34%  Analysis Date = 05/01/13 
 Pct Recovery = 34%  Analysis Date = 05/01/13 
 Pct Recovery = 34%  Analysis Date = 04/29/13 
 Pct Recovery = 34%  Analysis Date = 04/29/13 
 Pct Recovery = 34%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/25/13 
 Pct Recovery = 34%  Analysis Date = 04/25/13 
 Pct Recovery = 34%  Analysis Date = 04/23/13 
 Pct Recovery = 34%  Analysis Date = 04/23/13 
 Pct Recovery = 34%  Analysis Date = 04/21/13 
 Pct Recovery = 35%  Analysis Date = 04/21/13 
 Pct Recovery = 35%  Analysis Date = 04/19/13 
 Pct Recovery = 35%  Analysis Date = 04/19/13 
 Pct Recovery = 35%  Analysis Date = 04/17/13 
 Pct Recovery = 35%  Analysis Date = 04/17/13 
 Pct Recovery = 35%  Analysis Date = 04/15/13 
 Pct Recovery = 35%  Analysis Date = 04/15/13 
 Pct Recovery = 35%  Analysis Date = 04/13/13 
 Pct Recovery = 35%  Analysis Date = 04/13/13 
 Pct Recovery = 35%  Analysis Date = 04/11/13 
 Pct Recovery = 35%  Analysis Date = 04/11/13 
 Pct Recovery = 35%  Analysis Date = 04/09/13 
 Pct Recovery = 35%  Analysis Date = 04/09/13 
 Pct Recovery = 35%  Analysis Date = 04/07/13 
 Pct Recovery = 36%  Analysis Date = 04/07/13 
 Pct Recovery = 36%  Analysis Date = 04/05/13 
 Pct Recovery = 36%  Analysis Date = 04/05/13 
 Pct Recovery = 36%  Analysis Date = 04/03/13 
 Pct Recovery = 36%  Analysis Date = 04/03/13 
 Pct Recovery = 36%  Analysis Date = 04/01/13 
 Pct Recovery = 36%  Analysis Date = 04/01/13 
 Pct Recovery = 36%  Analysis Date = 03/30/13 
 Pct Recovery = 36%  Analysis Date = 03/30/13 
 Pct Recovery = 36%  Analysis Date = 03/28/13 
 Pct Recovery = 36%  Analysis Date = 03/28/13 
 Pct Recovery = 36%  Analysis Date = 03/26/13 
 Pct Recovery = 37%  Analysis Date = 03/26/13 
 Pct Recovery = 37%  Analysis Date = 03/24/13 
 Pct Recovery = 37%  Analysis Date = 03/24/13 
 Pct Recovery = 37%  Analysis Date = 03/22/13 
 Pct Recovery = 37%  Analysis Date = 03/22/13 
 Pct Recovery = 37%  Analysis Date = 03/20/13 
 Pct Recovery = 37%  Analysis Date = 03/20/13 
 Pct Recovery = 37%  Analysis Date = 03/18/13 
 Pct Recovery = 37%  Analysis Date = 03/18/13 
 Pct Recovery = 37%  Analysis Date = 03/16/13 
 Pct Recovery = 37%  Analysis Date = 03/16/13 
 Pct Recovery = 37%  Analysis Date = 03/14/13 
 Pct Recovery = 37%  Analysis Date = 03/14/13 
 Pct Recovery = 37%  Analysis Date = 03/12/13 
 Pct Recovery = 38%  Analysis Date = 03/12/13 
 Pct Recovery = 38%  Analysis Date = 03/10/13 
 Pct Recovery = 38%  Analysis Date = 03/10/13 
 Pct Recovery = 38%  Analysis Date = 03/08/13 
 Pct Recovery = 38%  Analysis Date = 03/08/13 
 Pct Recovery = 38%  Analysis Date = 03/06/13 
 Pct Recovery = 38%  Analysis Date = 03/06/13 
 Pct Recovery = 38%  Analysis Date = 03/04/13 
 Pct Recovery = 38%  Analysis Date = 03/04/13 
 Pct Recovery = 38%  Analysis Date = 03/02/13 
 Pct Recovery = 38%  Analysis Date = 03/02/13 
 Pct Recovery = 38%  Analysis Date = 02/28/13 
 Pct Recovery = 39%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETHAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 7 31% 6% 32% 7%
Total 7 31% 6% 32% 7%

Sample Statistics
PROMETHAZINE

Characteristic N % % Basis
Plotted 7 50% Spiked
Estimated Values 7 50% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 7 50% 7 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PROPOXYPHENE
METHOD: LC9017 , TESTIDCODE: 68009LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 86%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 36%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 43%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 37%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 65%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 42%  Analysis Date = 04/10/14 
 Pct Recovery = 33%  Analysis Date = 04/07/14 
 Pct Recovery = 33%  Analysis Date = 04/07/14 
 Pct Recovery = 33%  Analysis Date = 04/05/14 
 Pct Recovery = 33%  Analysis Date = 04/05/14 
 Pct Recovery = 33%  Analysis Date = 04/03/14 
 Pct Recovery = 34%  Analysis Date = 04/03/14 
 Pct Recovery = 34%  Analysis Date = 04/01/14 
 Pct Recovery = 34%  Analysis Date = 04/01/14 
 Pct Recovery = 34%  Analysis Date = 03/29/14 
 Pct Recovery = 34%  Analysis Date = 03/29/14 
 Pct Recovery = 34%  Analysis Date = 03/27/14 
 Pct Recovery = 35%  Analysis Date = 03/27/14 
 Pct Recovery = 35%  Analysis Date = 03/25/14 
 Pct Recovery = 35%  Analysis Date = 03/25/14 
 Pct Recovery = 35%  Analysis Date = 03/23/14 
 Pct Recovery = 35%  Analysis Date = 03/23/14 
 Pct Recovery = 35%  Analysis Date = 03/21/14 
 Pct Recovery = 36%  Analysis Date = 03/21/14 
 Pct Recovery = 36%  Analysis Date = 03/18/14 
 Pct Recovery = 36%  Analysis Date = 03/18/14 
 Pct Recovery = 36%  Analysis Date = 03/16/14 
 Pct Recovery = 36%  Analysis Date = 03/16/14 
 Pct Recovery = 36%  Analysis Date = 03/14/14 
 Pct Recovery = 36%  Analysis Date = 03/14/14 
 Pct Recovery = 36%  Analysis Date = 03/12/14 
 Pct Recovery = 37%  Analysis Date = 03/12/14 
 Pct Recovery = 37%  Analysis Date = 03/10/14 
 Pct Recovery = 37%  Analysis Date = 03/10/14 
 Pct Recovery = 37%  Analysis Date = 03/07/14 
 Pct Recovery = 37%  Analysis Date = 03/07/14 
 Pct Recovery = 37%  Analysis Date = 03/05/14 
 Pct Recovery = 38%  Analysis Date = 03/05/14 
 Pct Recovery = 38%  Analysis Date = 03/03/14 
 Pct Recovery = 38%  Analysis Date = 03/03/14 
 Pct Recovery = 38%  Analysis Date = 03/01/14 
 Pct Recovery = 38%  Analysis Date = 03/01/14 
 Pct Recovery = 38%  Analysis Date = 02/27/14 
 Pct Recovery = 39%  Analysis Date = 02/27/14 
 Pct Recovery = 39%  Analysis Date = 02/24/14 
 Pct Recovery = 39%  Analysis Date = 02/24/14 
 Pct Recovery = 39%  Analysis Date = 02/22/14 
 Pct Recovery = 39%  Analysis Date = 02/22/14 
 Pct Recovery = 39%  Analysis Date = 02/20/14 
 Pct Recovery = 40%  Analysis Date = 02/20/14 
 Pct Recovery = 40%  Analysis Date = 02/18/14 
 Pct Recovery = 40%  Analysis Date = 02/18/14 
 Pct Recovery = 40%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/16/14 
 Pct Recovery = 40%  Analysis Date = 02/13/14 
 Pct Recovery = 40%  Analysis Date = 02/13/14 
 Pct Recovery = 40%  Analysis Date = 02/11/14 
 Pct Recovery = 41%  Analysis Date = 02/11/14 
 Pct Recovery = 41%  Analysis Date = 02/09/14 
 Pct Recovery = 41%  Analysis Date = 02/09/14 
 Pct Recovery = 41%  Analysis Date = 02/07/14 
 Pct Recovery = 41%  Analysis Date = 02/07/14 
 Pct Recovery = 41%  Analysis Date = 02/05/14 
 Pct Recovery = 42%  Analysis Date = 02/05/14 
 Pct Recovery = 42%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 02/02/14 
 Pct Recovery = 42%  Analysis Date = 01/31/14 
 Pct Recovery = 42%  Analysis Date = 01/31/14 
 Pct Recovery = 42%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/29/14 
 Pct Recovery = 43%  Analysis Date = 01/27/14 
 Pct Recovery = 43%  Analysis Date = 01/27/14 
 Pct Recovery = 43%  Analysis Date = 01/25/14 
 Pct Recovery = 43%  Analysis Date = 01/25/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/20/14 
 Pct Recovery = 44%  Analysis Date = 01/20/14 
 Pct Recovery = 44%  Analysis Date = 01/18/14 
 Pct Recovery = 44%  Analysis Date = 01/18/14 
 Pct Recovery = 44%  Analysis Date = 01/16/14 
 Pct Recovery = 44%  Analysis Date = 01/16/14 
 Pct Recovery = 44%  Analysis Date = 01/14/14 
 Pct Recovery = 44%  Analysis Date = 01/14/14 
 Pct Recovery = 44%  Analysis Date = 01/11/14 
 Pct Recovery = 45%  Analysis Date = 01/11/14 
 Pct Recovery = 45%  Analysis Date = 01/09/14 
 Pct Recovery = 45%  Analysis Date = 01/09/14 
 Pct Recovery = 45%  Analysis Date = 01/07/14 
 Pct Recovery = 45%  Analysis Date = 01/07/14 
 Pct Recovery = 45%  Analysis Date = 01/05/14 
 Pct Recovery = 45%  Analysis Date = 01/05/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 12/31/13 
 Pct Recovery = 45%  Analysis Date = 12/31/13 
 Pct Recovery = 45%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/27/13 
 Pct Recovery = 46%  Analysis Date = 12/27/13 
 Pct Recovery = 46%  Analysis Date = 12/25/13 
 Pct Recovery = 46%  Analysis Date = 12/25/13 
 Pct Recovery = 46%  Analysis Date = 12/22/13 
 Pct Recovery = 46%  Analysis Date = 12/22/13 
 Pct Recovery = 46%  Analysis Date = 12/20/13 
 Pct Recovery = 46%  Analysis Date = 12/20/13 
 Pct Recovery = 46%  Analysis Date = 12/18/13 
 Pct Recovery = 46%  Analysis Date = 12/18/13 
 Pct Recovery = 46%  Analysis Date = 12/16/13 
 Pct Recovery = 46%  Analysis Date = 12/16/13 
 Pct Recovery = 46%  Analysis Date = 12/14/13 
 Pct Recovery = 47%  Analysis Date = 12/14/13 
 Pct Recovery = 47%  Analysis Date = 12/11/13 
 Pct Recovery = 47%  Analysis Date = 12/11/13 
 Pct Recovery = 47%  Analysis Date = 12/09/13 
 Pct Recovery = 47%  Analysis Date = 12/09/13 
 Pct Recovery = 47%  Analysis Date = 12/07/13 
 Pct Recovery = 47%  Analysis Date = 12/07/13 
 Pct Recovery = 47%  Analysis Date = 12/05/13 
 Pct Recovery = 47%  Analysis Date = 12/05/13 
 Pct Recovery = 47%  Analysis Date = 12/03/13 
 Pct Recovery = 47%  Analysis Date = 12/03/13 
 Pct Recovery = 47%  Analysis Date = 11/30/13 
 Pct Recovery = 47%  Analysis Date = 11/30/13 
 Pct Recovery = 47%  Analysis Date = 11/28/13 
 Pct Recovery = 48%  Analysis Date = 11/28/13 
 Pct Recovery = 48%  Analysis Date = 11/26/13 
 Pct Recovery = 48%  Analysis Date = 11/26/13 
 Pct Recovery = 48%  Analysis Date = 11/24/13 
 Pct Recovery = 48%  Analysis Date = 11/24/13 
 Pct Recovery = 48%  Analysis Date = 11/22/13 
 Pct Recovery = 48%  Analysis Date = 11/22/13 
 Pct Recovery = 48%  Analysis Date = 11/19/13 
 Pct Recovery = 48%  Analysis Date = 11/19/13 
 Pct Recovery = 48%  Analysis Date = 11/17/13 
 Pct Recovery = 48%  Analysis Date = 11/17/13 
 Pct Recovery = 48%  Analysis Date = 11/15/13 
 Pct Recovery = 49%  Analysis Date = 11/15/13 
 Pct Recovery = 49%  Analysis Date = 11/13/13 
 Pct Recovery = 49%  Analysis Date = 11/13/13 
 Pct Recovery = 49%  Analysis Date = 11/11/13 
 Pct Recovery = 49%  Analysis Date = 11/11/13 
 Pct Recovery = 49%  Analysis Date = 11/08/13 
 Pct Recovery = 49%  Analysis Date = 11/08/13 
 Pct Recovery = 49%  Analysis Date = 11/06/13 
 Pct Recovery = 49%  Analysis Date = 11/06/13 
 Pct Recovery = 49%  Analysis Date = 11/04/13 
 Pct Recovery = 49%  Analysis Date = 11/04/13 
 Pct Recovery = 49%  Analysis Date = 11/02/13 
 Pct Recovery = 49%  Analysis Date = 11/02/13 
 Pct Recovery = 49%  Analysis Date = 10/31/13 
 Pct Recovery = 50%  Analysis Date = 10/31/13 
 Pct Recovery = 50%  Analysis Date = 10/28/13 
 Pct Recovery = 50%  Analysis Date = 10/28/13 
 Pct Recovery = 50%  Analysis Date = 10/26/13 
 Pct Recovery = 50%  Analysis Date = 10/26/13 
 Pct Recovery = 50%  Analysis Date = 10/24/13 
 Pct Recovery = 50%  Analysis Date = 10/24/13 
 Pct Recovery = 50%  Analysis Date = 10/22/13 
 Pct Recovery = 50%  Analysis Date = 10/22/13 
 Pct Recovery = 50%  Analysis Date = 10/20/13 
 Pct Recovery = 50%  Analysis Date = 10/20/13 
 Pct Recovery = 50%  Analysis Date = 10/17/13 
 Pct Recovery = 50%  Analysis Date = 10/17/13 
 Pct Recovery = 50%  Analysis Date = 10/15/13 
 Pct Recovery = 50%  Analysis Date = 10/15/13 
 Pct Recovery = 50%  Analysis Date = 10/13/13 
 Pct Recovery = 50%  Analysis Date = 10/13/13 
 Pct Recovery = 50%  Analysis Date = 10/11/13 
 Pct Recovery = 50%  Analysis Date = 10/11/13 
 Pct Recovery = 50%  Analysis Date = 10/08/13 
 Pct Recovery = 51%  Analysis Date = 10/08/13 
 Pct Recovery = 51%  Analysis Date = 10/06/13 
 Pct Recovery = 51%  Analysis Date = 10/06/13 
 Pct Recovery = 51%  Analysis Date = 10/04/13 
 Pct Recovery = 51%  Analysis Date = 10/04/13 
 Pct Recovery = 51%  Analysis Date = 10/02/13 
 Pct Recovery = 51%  Analysis Date = 10/02/13 
 Pct Recovery = 51%  Analysis Date = 09/30/13 
 Pct Recovery = 51%  Analysis Date = 09/30/13 
 Pct Recovery = 51%  Analysis Date = 09/27/13 
 Pct Recovery = 51%  Analysis Date = 09/27/13 
 Pct Recovery = 51%  Analysis Date = 09/25/13 
 Pct Recovery = 51%  Analysis Date = 09/25/13 
 Pct Recovery = 51%  Analysis Date = 09/23/13 
 Pct Recovery = 51%  Analysis Date = 09/23/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/21/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/19/13 
 Pct Recovery = 51%  Analysis Date = 09/16/13 
 Pct Recovery = 52%  Analysis Date = 09/16/13 
 Pct Recovery = 52%  Analysis Date = 09/14/13 
 Pct Recovery = 52%  Analysis Date = 09/14/13 
 Pct Recovery = 52%  Analysis Date = 09/12/13 
 Pct Recovery = 52%  Analysis Date = 09/12/13 
 Pct Recovery = 52%  Analysis Date = 09/10/13 
 Pct Recovery = 52%  Analysis Date = 09/10/13 
 Pct Recovery = 52%  Analysis Date = 09/08/13 
 Pct Recovery = 52%  Analysis Date = 09/08/13 
 Pct Recovery = 52%  Analysis Date = 09/05/13 
 Pct Recovery = 52%  Analysis Date = 09/05/13 
 Pct Recovery = 52%  Analysis Date = 09/03/13 
 Pct Recovery = 52%  Analysis Date = 09/03/13 
 Pct Recovery = 52%  Analysis Date = 09/01/13 
 Pct Recovery = 52%  Analysis Date = 09/01/13 
 Pct Recovery = 52%  Analysis Date = 08/30/13 
 Pct Recovery = 52%  Analysis Date = 08/30/13 
 Pct Recovery = 52%  Analysis Date = 08/28/13 
 Pct Recovery = 52%  Analysis Date = 08/28/13 
 Pct Recovery = 52%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/25/13 
 Pct Recovery = 52%  Analysis Date = 08/23/13 
 Pct Recovery = 53%  Analysis Date = 08/23/13 
 Pct Recovery = 53%  Analysis Date = 08/21/13 
 Pct Recovery = 53%  Analysis Date = 08/21/13 
 Pct Recovery = 53%  Analysis Date = 08/19/13 
 Pct Recovery = 53%  Analysis Date = 08/19/13 
 Pct Recovery = 53%  Analysis Date = 08/17/13 
 Pct Recovery = 53%  Analysis Date = 08/17/13 
 Pct Recovery = 53%  Analysis Date = 08/14/13 
 Pct Recovery = 53%  Analysis Date = 08/14/13 
 Pct Recovery = 53%  Analysis Date = 08/12/13 
 Pct Recovery = 54%  Analysis Date = 08/12/13 
 Pct Recovery = 54%  Analysis Date = 08/10/13 
 Pct Recovery = 54%  Analysis Date = 08/10/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/08/13 
 Pct Recovery = 54%  Analysis Date = 08/06/13 
 Pct Recovery = 55%  Analysis Date = 08/06/13 
 Pct Recovery = 55%  Analysis Date = 08/03/13 
 Pct Recovery = 55%  Analysis Date = 08/03/13 
 Pct Recovery = 55%  Analysis Date = 08/01/13 
 Pct Recovery = 55%  Analysis Date = 08/01/13 
 Pct Recovery = 55%  Analysis Date = 07/30/13 
 Pct Recovery = 56%  Analysis Date = 07/30/13 
 Pct Recovery = 56%  Analysis Date = 07/28/13 
 Pct Recovery = 56%  Analysis Date = 07/28/13 
 Pct Recovery = 56%  Analysis Date = 07/26/13 
 Pct Recovery = 56%  Analysis Date = 07/26/13 
 Pct Recovery = 56%  Analysis Date = 07/23/13 
 Pct Recovery = 57%  Analysis Date = 07/23/13 
 Pct Recovery = 57%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/21/13 
 Pct Recovery = 57%  Analysis Date = 07/19/13 
 Pct Recovery = 58%  Analysis Date = 07/19/13 
 Pct Recovery = 58%  Analysis Date = 07/17/13 
 Pct Recovery = 58%  Analysis Date = 07/17/13 
 Pct Recovery = 58%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/14/13 
 Pct Recovery = 58%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/12/13 
 Pct Recovery = 59%  Analysis Date = 07/10/13 
 Pct Recovery = 59%  Analysis Date = 07/10/13 
 Pct Recovery = 59%  Analysis Date = 07/08/13 
 Pct Recovery = 59%  Analysis Date = 07/08/13 
 Pct Recovery = 59%  Analysis Date = 07/06/13 
 Pct Recovery = 60%  Analysis Date = 07/06/13 
 Pct Recovery = 60%  Analysis Date = 07/03/13 
 Pct Recovery = 60%  Analysis Date = 07/03/13 
 Pct Recovery = 60%  Analysis Date = 07/01/13 
 Pct Recovery = 60%  Analysis Date = 07/01/13 
 Pct Recovery = 60%  Analysis Date = 06/29/13 
 Pct Recovery = 61%  Analysis Date = 06/29/13 
 Pct Recovery = 61%  Analysis Date = 06/27/13 
 Pct Recovery = 61%  Analysis Date = 06/27/13 
 Pct Recovery = 61%  Analysis Date = 06/25/13 
 Pct Recovery = 61%  Analysis Date = 06/25/13 
 Pct Recovery = 61%  Analysis Date = 06/22/13 
 Pct Recovery = 62%  Analysis Date = 06/22/13 
 Pct Recovery = 62%  Analysis Date = 06/20/13 
 Pct Recovery = 62%  Analysis Date = 06/20/13 
 Pct Recovery = 62%  Analysis Date = 06/18/13 
 Pct Recovery = 63%  Analysis Date = 06/18/13 
 Pct Recovery = 63%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/16/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/14/13 
 Pct Recovery = 63%  Analysis Date = 06/11/13 
 Pct Recovery = 64%  Analysis Date = 06/11/13 
 Pct Recovery = 64%  Analysis Date = 06/09/13 
 Pct Recovery = 64%  Analysis Date = 06/09/13 
 Pct Recovery = 64%  Analysis Date = 06/07/13 
 Pct Recovery = 64%  Analysis Date = 06/07/13 
 Pct Recovery = 64%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 66%  Analysis Date = 05/29/13 
 Pct Recovery = 66%  Analysis Date = 05/27/13 
 Pct Recovery = 66%  Analysis Date = 05/27/13 
 Pct Recovery = 66%  Analysis Date = 05/25/13 
 Pct Recovery = 66%  Analysis Date = 05/25/13 
 Pct Recovery = 66%  Analysis Date = 05/23/13 
 Pct Recovery = 67%  Analysis Date = 05/23/13 
 Pct Recovery = 67%  Analysis Date = 05/20/13 
 Pct Recovery = 67%  Analysis Date = 05/20/13 
 Pct Recovery = 67%  Analysis Date = 05/18/13 
 Pct Recovery = 67%  Analysis Date = 05/18/13 
 Pct Recovery = 67%  Analysis Date = 05/16/13 
 Pct Recovery = 68%  Analysis Date = 05/16/13 
 Pct Recovery = 68%  Analysis Date = 05/14/13 
 Pct Recovery = 68%  Analysis Date = 05/14/13 
 Pct Recovery = 68%  Analysis Date = 05/12/13 
 Pct Recovery = 69%  Analysis Date = 05/12/13 
 Pct Recovery = 69%  Analysis Date = 05/09/13 
 Pct Recovery = 69%  Analysis Date = 05/09/13 
 Pct Recovery = 69%  Analysis Date = 05/07/13 
 Pct Recovery = 69%  Analysis Date = 05/07/13 
 Pct Recovery = 69%  Analysis Date = 05/05/13 
 Pct Recovery = 70%  Analysis Date = 05/05/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 04/28/13 
 Pct Recovery = 70%  Analysis Date = 04/28/13 
 Pct Recovery = 70%  Analysis Date = 04/26/13 
 Pct Recovery = 69%  Analysis Date = 04/26/13 
 Pct Recovery = 69%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/24/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/22/13 
 Pct Recovery = 69%  Analysis Date = 04/19/13 
 Pct Recovery = 68%  Analysis Date = 04/19/13 
 Pct Recovery = 68%  Analysis Date = 04/17/13 
 Pct Recovery = 68%  Analysis Date = 04/17/13 
 Pct Recovery = 68%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/15/13 
 Pct Recovery = 68%  Analysis Date = 04/13/13 
 Pct Recovery = 67%  Analysis Date = 04/13/13 
 Pct Recovery = 67%  Analysis Date = 04/11/13 
 Pct Recovery = 67%  Analysis Date = 04/11/13 
 Pct Recovery = 67%  Analysis Date = 04/08/13 
 Pct Recovery = 67%  Analysis Date = 04/08/13 
 Pct Recovery = 67%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/06/13 
 Pct Recovery = 66%  Analysis Date = 04/04/13 
 Pct Recovery = 66%  Analysis Date = 04/04/13 
 Pct Recovery = 66%  Analysis Date = 04/02/13 
 Pct Recovery = 66%  Analysis Date = 04/02/13 
 Pct Recovery = 66%  Analysis Date = 03/31/13 
 Pct Recovery = 65%  Analysis Date = 03/31/13 
 Pct Recovery = 65%  Analysis Date = 03/28/13 
 Pct Recovery = 65%  Analysis Date = 03/28/13 
 Pct Recovery = 65%  Analysis Date = 03/26/13 
 Pct Recovery = 65%  Analysis Date = 03/26/13 
 Pct Recovery = 65%  Analysis Date = 03/24/13 
 Pct Recovery = 65%  Analysis Date = 03/24/13 
 Pct Recovery = 65%  Analysis Date = 03/22/13 
 Pct Recovery = 66%  Analysis Date = 03/22/13 
 Pct Recovery = 66%  Analysis Date = 03/20/13 
 Pct Recovery = 66%  Analysis Date = 03/20/13 
 Pct Recovery = 66%  Analysis Date = 03/17/13 
 Pct Recovery = 67%  Analysis Date = 03/17/13 
 Pct Recovery = 67%  Analysis Date = 03/15/13 
 Pct Recovery = 67%  Analysis Date = 03/15/13 
 Pct Recovery = 67%  Analysis Date = 03/13/13 
 Pct Recovery = 68%  Analysis Date = 03/13/13 
 Pct Recovery = 68%  Analysis Date = 03/11/13 
 Pct Recovery = 68%  Analysis Date = 03/11/13 
 Pct Recovery = 68%  Analysis Date = 03/09/13 
 Pct Recovery = 69%  Analysis Date = 03/09/13 
 Pct Recovery = 69%  Analysis Date = 03/06/13 
 Pct Recovery = 69%  Analysis Date = 03/06/13 
 Pct Recovery = 69%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/04/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 02/28/13 
 Pct Recovery = 71%  Analysis Date = 02/28/13 
 Pct Recovery = 71%  Analysis Date = 02/26/13 
 Pct Recovery = 71%  Analysis Date = 02/26/13 
 Pct Recovery = 71%  Analysis Date = 02/23/13 
 Pct Recovery = 72%  Analysis Date = 02/23/13 
 Pct Recovery = 72%  Analysis Date = 02/21/13 
 Pct Recovery = 72%  Analysis Date = 02/21/13 
 Pct Recovery = 72%  Analysis Date = 02/19/13 
 Pct Recovery = 73%  Analysis Date = 02/19/13 
 Pct Recovery = 73%  Analysis Date = 02/17/13 
 Pct Recovery = 73%  Analysis Date = 02/17/13 
 Pct Recovery = 73%  Analysis Date = 02/15/13 
 Pct Recovery = 74%  Analysis Date = 02/15/13 
 Pct Recovery = 74%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/12/13 
 Pct Recovery = 74%  Analysis Date = 02/10/13 
 Pct Recovery = 75%  Analysis Date = 02/10/13 
 Pct Recovery = 75%  Analysis Date = 02/08/13 
 Pct Recovery = 75%  Analysis Date = 02/08/13 
 Pct Recovery = 75%  Analysis Date = 02/06/13 
 Pct Recovery = 76%  Analysis Date = 02/06/13 
 Pct Recovery = 76%  Analysis Date = 02/04/13 
 Pct Recovery = 76%  Analysis Date = 02/04/13 
 Pct Recovery = 76%  Analysis Date = 02/01/13 
 Pct Recovery = 77%  Analysis Date = 02/01/13 
 Pct Recovery = 77%  Analysis Date = 01/30/13 
 Pct Recovery = 77%  Analysis Date = 01/30/13 
 Pct Recovery = 77%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/24/13 
 Pct Recovery = 79%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPOXYPHENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 7 54% 20% 43% 27%
Total 7 54% 20% 43% 27%

Sample Statistics
PROPOXYPHENE

Characteristic N % % Basis
Plotted 7 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 0 0% 0 out of 7
Not Spiked 25 .  
False Positives 1 4% 1 out of 24

OBSP Determination:
PROPRANOLOL
METHOD: LC9017 , TESTIDCODE: 67516LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 66%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 82%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 44%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 61%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 61%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 57%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 90%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 67%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 69%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 84%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 72%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 65%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 86%  Analysis Date = 04/09/14 
 Pct Recovery = 51%  Analysis Date = 04/07/14 
 Pct Recovery = 51%  Analysis Date = 04/07/14 
 Pct Recovery = 51%  Analysis Date = 04/05/14 
 Pct Recovery = 52%  Analysis Date = 04/05/14 
 Pct Recovery = 52%  Analysis Date = 04/02/14 
 Pct Recovery = 52%  Analysis Date = 04/02/14 
 Pct Recovery = 52%  Analysis Date = 03/31/14 
 Pct Recovery = 52%  Analysis Date = 03/31/14 
 Pct Recovery = 52%  Analysis Date = 03/28/14 
 Pct Recovery = 53%  Analysis Date = 03/28/14 
 Pct Recovery = 53%  Analysis Date = 03/26/14 
 Pct Recovery = 53%  Analysis Date = 03/26/14 
 Pct Recovery = 53%  Analysis Date = 03/24/14 
 Pct Recovery = 53%  Analysis Date = 03/24/14 
 Pct Recovery = 53%  Analysis Date = 03/21/14 
 Pct Recovery = 54%  Analysis Date = 03/21/14 
 Pct Recovery = 54%  Analysis Date = 03/19/14 
 Pct Recovery = 54%  Analysis Date = 03/19/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/16/14 
 Pct Recovery = 54%  Analysis Date = 03/14/14 
 Pct Recovery = 55%  Analysis Date = 03/14/14 
 Pct Recovery = 55%  Analysis Date = 03/12/14 
 Pct Recovery = 55%  Analysis Date = 03/12/14 
 Pct Recovery = 55%  Analysis Date = 03/09/14 
 Pct Recovery = 55%  Analysis Date = 03/09/14 
 Pct Recovery = 55%  Analysis Date = 03/07/14 
 Pct Recovery = 56%  Analysis Date = 03/07/14 
 Pct Recovery = 56%  Analysis Date = 03/04/14 
 Pct Recovery = 56%  Analysis Date = 03/04/14 
 Pct Recovery = 56%  Analysis Date = 03/02/14 
 Pct Recovery = 56%  Analysis Date = 03/02/14 
 Pct Recovery = 56%  Analysis Date = 02/28/14 
 Pct Recovery = 57%  Analysis Date = 02/28/14 
 Pct Recovery = 57%  Analysis Date = 02/25/14 
 Pct Recovery = 57%  Analysis Date = 02/25/14 
 Pct Recovery = 57%  Analysis Date = 02/23/14 
 Pct Recovery = 57%  Analysis Date = 02/23/14 
 Pct Recovery = 57%  Analysis Date = 02/20/14 
 Pct Recovery = 58%  Analysis Date = 02/20/14 
 Pct Recovery = 58%  Analysis Date = 02/18/14 
 Pct Recovery = 58%  Analysis Date = 02/18/14 
 Pct Recovery = 58%  Analysis Date = 02/15/14 
 Pct Recovery = 59%  Analysis Date = 02/15/14 
 Pct Recovery = 59%  Analysis Date = 02/13/14 
 Pct Recovery = 59%  Analysis Date = 02/13/14 
 Pct Recovery = 59%  Analysis Date = 02/11/14 
 Pct Recovery = 59%  Analysis Date = 02/11/14 
 Pct Recovery = 59%  Analysis Date = 02/08/14 
 Pct Recovery = 60%  Analysis Date = 02/08/14 
 Pct Recovery = 60%  Analysis Date = 02/06/14 
 Pct Recovery = 60%  Analysis Date = 02/06/14 
 Pct Recovery = 60%  Analysis Date = 02/03/14 
 Pct Recovery = 60%  Analysis Date = 02/03/14 
 Pct Recovery = 60%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 63%  Analysis Date = 01/20/14 
 Pct Recovery = 63%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/15/14 
 Pct Recovery = 63%  Analysis Date = 01/13/14 
 Pct Recovery = 64%  Analysis Date = 01/13/14 
 Pct Recovery = 64%  Analysis Date = 01/10/14 
 Pct Recovery = 64%  Analysis Date = 01/10/14 
 Pct Recovery = 64%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/08/14 
 Pct Recovery = 64%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/06/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/03/14 
 Pct Recovery = 65%  Analysis Date = 01/01/14 
 Pct Recovery = 65%  Analysis Date = 01/01/14 
 Pct Recovery = 65%  Analysis Date = 12/29/13 
 Pct Recovery = 66%  Analysis Date = 12/29/13 
 Pct Recovery = 66%  Analysis Date = 12/27/13 
 Pct Recovery = 66%  Analysis Date = 12/27/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/24/13 
 Pct Recovery = 66%  Analysis Date = 12/22/13 
 Pct Recovery = 66%  Analysis Date = 12/22/13 
 Pct Recovery = 66%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/17/13 
 Pct Recovery = 67%  Analysis Date = 12/17/13 
 Pct Recovery = 67%  Analysis Date = 12/15/13 
 Pct Recovery = 67%  Analysis Date = 12/15/13 
 Pct Recovery = 67%  Analysis Date = 12/12/13 
 Pct Recovery = 68%  Analysis Date = 12/12/13 
 Pct Recovery = 68%  Analysis Date = 12/10/13 
 Pct Recovery = 68%  Analysis Date = 12/10/13 
 Pct Recovery = 68%  Analysis Date = 12/08/13 
 Pct Recovery = 68%  Analysis Date = 12/08/13 
 Pct Recovery = 68%  Analysis Date = 12/05/13 
 Pct Recovery = 69%  Analysis Date = 12/05/13 
 Pct Recovery = 69%  Analysis Date = 12/03/13 
 Pct Recovery = 69%  Analysis Date = 12/03/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/30/13 
 Pct Recovery = 69%  Analysis Date = 11/28/13 
 Pct Recovery = 69%  Analysis Date = 11/28/13 
 Pct Recovery = 69%  Analysis Date = 11/26/13 
 Pct Recovery = 70%  Analysis Date = 11/26/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/21/13 
 Pct Recovery = 70%  Analysis Date = 11/21/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/11/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/09/13 
 Pct Recovery = 70%  Analysis Date = 11/06/13 
 Pct Recovery = 70%  Analysis Date = 11/06/13 
 Pct Recovery = 70%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/30/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/28/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 71%  Analysis Date = 10/25/13 
 Pct Recovery = 71%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/23/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/16/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/13/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/11/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/08/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/06/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/04/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 10/01/13 
 Pct Recovery = 72%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 73%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/19/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/14/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/12/13 
 Pct Recovery = 73%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/09/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/07/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/05/13 
 Pct Recovery = 74%  Analysis Date = 09/02/13 
 Pct Recovery = 74%  Analysis Date = 09/02/13 
 Pct Recovery = 74%  Analysis Date = 08/31/13 
 Pct Recovery = 74%  Analysis Date = 08/31/13 
 Pct Recovery = 74%  Analysis Date = 08/28/13 
 Pct Recovery = 74%  Analysis Date = 08/28/13 
 Pct Recovery = 74%  Analysis Date = 08/26/13 
 Pct Recovery = 74%  Analysis Date = 08/26/13 
 Pct Recovery = 74%  Analysis Date = 08/24/13 
 Pct Recovery = 75%  Analysis Date = 08/24/13 
 Pct Recovery = 75%  Analysis Date = 08/21/13 
 Pct Recovery = 75%  Analysis Date = 08/21/13 
 Pct Recovery = 75%  Analysis Date = 08/19/13 
 Pct Recovery = 75%  Analysis Date = 08/19/13 
 Pct Recovery = 75%  Analysis Date = 08/16/13 
 Pct Recovery = 75%  Analysis Date = 08/16/13 
 Pct Recovery = 75%  Analysis Date = 08/14/13 
 Pct Recovery = 75%  Analysis Date = 08/14/13 
 Pct Recovery = 75%  Analysis Date = 08/11/13 
 Pct Recovery = 75%  Analysis Date = 08/11/13 
 Pct Recovery = 75%  Analysis Date = 08/09/13 
 Pct Recovery = 75%  Analysis Date = 08/09/13 
 Pct Recovery = 75%  Analysis Date = 08/07/13 
 Pct Recovery = 76%  Analysis Date = 08/07/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/04/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 08/02/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/30/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/28/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/26/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/23/13 
 Pct Recovery = 76%  Analysis Date = 07/21/13 
 Pct Recovery = 76%  Analysis Date = 07/21/13 
 Pct Recovery = 76%  Analysis Date = 07/18/13 
 Pct Recovery = 76%  Analysis Date = 07/18/13 
 Pct Recovery = 76%  Analysis Date = 07/16/13 
 Pct Recovery = 76%  Analysis Date = 07/16/13 
 Pct Recovery = 76%  Analysis Date = 07/14/13 
 Pct Recovery = 76%  Analysis Date = 07/14/13 
 Pct Recovery = 76%  Analysis Date = 07/11/13 
 Pct Recovery = 76%  Analysis Date = 07/11/13 
 Pct Recovery = 76%  Analysis Date = 07/09/13 
 Pct Recovery = 76%  Analysis Date = 07/09/13 
 Pct Recovery = 76%  Analysis Date = 07/06/13 
 Pct Recovery = 76%  Analysis Date = 07/06/13 
 Pct Recovery = 76%  Analysis Date = 07/04/13 
 Pct Recovery = 76%  Analysis Date = 07/04/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 07/02/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/29/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/27/13 
 Pct Recovery = 76%  Analysis Date = 06/24/13 
 Pct Recovery = 76%  Analysis Date = 06/24/13 
 Pct Recovery = 76%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/15/13 
 Pct Recovery = 77%  Analysis Date = 06/15/13 
 Pct Recovery = 77%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/12/13 
 Pct Recovery = 77%  Analysis Date = 06/10/13 
 Pct Recovery = 77%  Analysis Date = 06/10/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/17/13 
 Pct Recovery = 77%  Analysis Date = 05/14/13 
 Pct Recovery = 77%  Analysis Date = 05/14/13 
 Pct Recovery = 77%  Analysis Date = 05/12/13 
 Pct Recovery = 77%  Analysis Date = 05/12/13 
 Pct Recovery = 77%  Analysis Date = 05/10/13 
 Pct Recovery = 77%  Analysis Date = 05/10/13 
 Pct Recovery = 77%  Analysis Date = 05/07/13 
 Pct Recovery = 77%  Analysis Date = 05/07/13 
 Pct Recovery = 77%  Analysis Date = 05/05/13 
 Pct Recovery = 77%  Analysis Date = 05/05/13 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 Pct Recovery = 77%  Analysis Date = 05/02/13 
 Pct Recovery = 77%  Analysis Date = 04/30/13 
 Pct Recovery = 77%  Analysis Date = 04/30/13 
 Pct Recovery = 77%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/23/13 
 Pct Recovery = 77%  Analysis Date = 04/23/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/18/13 
 Pct Recovery = 77%  Analysis Date = 04/18/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 76%  Analysis Date = 04/15/13 
 Pct Recovery = 76%  Analysis Date = 04/13/13 
 Pct Recovery = 76%  Analysis Date = 04/13/13 
 Pct Recovery = 76%  Analysis Date = 04/11/13 
 Pct Recovery = 76%  Analysis Date = 04/11/13 
 Pct Recovery = 76%  Analysis Date = 04/08/13 
 Pct Recovery = 76%  Analysis Date = 04/08/13 
 Pct Recovery = 76%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 76%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/10/13 
 Pct Recovery = 75%  Analysis Date = 03/10/13 
 Pct Recovery = 75%  Analysis Date = 03/08/13 
 Pct Recovery = 75%  Analysis Date = 03/08/13 
 Pct Recovery = 75%  Analysis Date = 03/05/13 
 Pct Recovery = 74%  Analysis Date = 03/05/13 
 Pct Recovery = 74%  Analysis Date = 03/03/13 
 Pct Recovery = 74%  Analysis Date = 03/03/13 
 Pct Recovery = 74%  Analysis Date = 03/01/13 
 Pct Recovery = 74%  Analysis Date = 03/01/13 
 Pct Recovery = 74%  Analysis Date = 02/26/13 
 Pct Recovery = 74%  Analysis Date = 02/26/13 
 Pct Recovery = 74%  Analysis Date = 02/24/13 
 Pct Recovery = 74%  Analysis Date = 02/24/13 
 Pct Recovery = 74%  Analysis Date = 02/21/13 
 Pct Recovery = 74%  Analysis Date = 02/21/13 
 Pct Recovery = 74%  Analysis Date = 02/19/13 
 Pct Recovery = 74%  Analysis Date = 02/19/13 
 Pct Recovery = 74%  Analysis Date = 02/17/13 
 Pct Recovery = 73%  Analysis Date = 02/17/13 
 Pct Recovery = 73%  Analysis Date = 02/14/13 
 Pct Recovery = 73%  Analysis Date = 02/14/13 
 Pct Recovery = 73%  Analysis Date = 02/12/13 
 Pct Recovery = 73%  Analysis Date = 02/12/13 
 Pct Recovery = 73%  Analysis Date = 02/09/13 
 Pct Recovery = 73%  Analysis Date = 02/09/13 
 Pct Recovery = 73%  Analysis Date = 02/07/13 
 Pct Recovery = 73%  Analysis Date = 02/07/13 
 Pct Recovery = 73%  Analysis Date = 02/05/13 
 Pct Recovery = 73%  Analysis Date = 02/05/13 
 Pct Recovery = 73%  Analysis Date = 02/02/13 
 Pct Recovery = 72%  Analysis Date = 02/02/13 
 Pct Recovery = 72%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/31/13 
 Pct Recovery = 72%  Analysis Date = 01/28/13 
 Pct Recovery = 72%  Analysis Date = 01/28/13 
 Pct Recovery = 72%  Analysis Date = 01/26/13 
 Pct Recovery = 72%  Analysis Date = 01/26/13 
 Pct Recovery = 72%  Analysis Date = 01/23/13 
 Pct Recovery = 72%  Analysis Date = 01/23/13 
 Pct Recovery = 72%  Analysis Date = 01/21/13 
 Pct Recovery = 72%  Analysis Date = 01/21/13 
 Pct Recovery = 72%  Analysis Date = 01/19/13 
 Pct Recovery = 71%  Analysis Date = 01/19/13 
 Pct Recovery = 71%  Analysis Date = 01/16/13 
 Pct Recovery = 71%  Analysis Date = 01/16/13 
 Pct Recovery = 71%  Analysis Date = 01/14/13 
 Pct Recovery = 71%  Analysis Date = 01/14/13 
 Pct Recovery = 71%  Analysis Date = 01/11/13 
 Pct Recovery = 71%  Analysis Date = 01/11/13 
 Pct Recovery = 71%  Analysis Date = 01/09/13 
 Pct Recovery = 71%  Analysis Date = 01/09/13 
 Pct Recovery = 71%  Analysis Date = 01/07/13 
 Pct Recovery = 71%  Analysis Date = 01/07/13 
 Pct Recovery = 71%  Analysis Date = 01/04/13 
 Pct Recovery = 70%  Analysis Date = 01/04/13 
 Pct Recovery = 70%  Analysis Date = 01/02/13 
 Pct Recovery = 70%  Analysis Date = 01/02/13 
 Pct Recovery = 70%  Analysis Date = 12/30/12 
 Pct Recovery = 70%  Analysis Date = 12/30/12 
 Pct Recovery = 70%  Analysis Date = 12/28/12 
 Pct Recovery = 70%  Analysis Date = 12/28/12 
 Pct Recovery = 70%  Analysis Date = 12/26/12 
 Pct Recovery = 70%  Analysis Date = 12/26/12 
 Pct Recovery = 70%  Analysis Date = 12/23/12 
 Pct Recovery = 70%  Analysis Date = 12/23/12 
 Pct Recovery = 70%  Analysis Date = 12/21/12 
 Pct Recovery = 69%  Analysis Date = 12/21/12 
 Pct Recovery = 69%  Analysis Date = 12/18/12 
 Pct Recovery = 69%  Analysis Date = 12/18/12 
 Pct Recovery = 69%  Analysis Date = 12/16/12 
 Pct Recovery = 69%  Analysis Date = 12/16/12 
 Pct Recovery = 69%  Analysis Date = 12/14/12 
 Pct Recovery = 69%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPRANOLOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 69% 12% 68% 15%
Total 14 69% 12% 68% 15%

Sample Statistics
PROPRANOLOL

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
PSEUDOEPHEDRINE+EPHEDRINE
METHOD: LC9017 , TESTIDCODE: 67460LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 95%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 46%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 84%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 62%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 83%  Analysis Date = 04/10/14 
 Pct Recovery = 46%  Analysis Date = 04/07/14 
 Pct Recovery = 46%  Analysis Date = 04/07/14 
 Pct Recovery = 46%  Analysis Date = 04/05/14 
 Pct Recovery = 47%  Analysis Date = 04/05/14 
 Pct Recovery = 47%  Analysis Date = 04/03/14 
 Pct Recovery = 47%  Analysis Date = 04/03/14 
 Pct Recovery = 47%  Analysis Date = 04/01/14 
 Pct Recovery = 48%  Analysis Date = 04/01/14 
 Pct Recovery = 48%  Analysis Date = 03/29/14 
 Pct Recovery = 48%  Analysis Date = 03/29/14 
 Pct Recovery = 48%  Analysis Date = 03/27/14 
 Pct Recovery = 49%  Analysis Date = 03/27/14 
 Pct Recovery = 49%  Analysis Date = 03/25/14 
 Pct Recovery = 49%  Analysis Date = 03/25/14 
 Pct Recovery = 49%  Analysis Date = 03/23/14 
 Pct Recovery = 50%  Analysis Date = 03/23/14 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 Pct Recovery = 50%  Analysis Date = 03/21/14 
 Pct Recovery = 50%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/18/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/16/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/14/14 
 Pct Recovery = 51%  Analysis Date = 03/12/14 
 Pct Recovery = 52%  Analysis Date = 03/12/14 
 Pct Recovery = 52%  Analysis Date = 03/10/14 
 Pct Recovery = 52%  Analysis Date = 03/10/14 
 Pct Recovery = 52%  Analysis Date = 03/07/14 
 Pct Recovery = 53%  Analysis Date = 03/07/14 
 Pct Recovery = 53%  Analysis Date = 03/05/14 
 Pct Recovery = 53%  Analysis Date = 03/05/14 
 Pct Recovery = 53%  Analysis Date = 03/03/14 
 Pct Recovery = 54%  Analysis Date = 03/03/14 
 Pct Recovery = 54%  Analysis Date = 03/01/14 
 Pct Recovery = 54%  Analysis Date = 03/01/14 
 Pct Recovery = 54%  Analysis Date = 02/27/14 
 Pct Recovery = 55%  Analysis Date = 02/27/14 
 Pct Recovery = 55%  Analysis Date = 02/24/14 
 Pct Recovery = 55%  Analysis Date = 02/24/14 
 Pct Recovery = 55%  Analysis Date = 02/22/14 
 Pct Recovery = 56%  Analysis Date = 02/22/14 
 Pct Recovery = 56%  Analysis Date = 02/20/14 
 Pct Recovery = 56%  Analysis Date = 02/20/14 
 Pct Recovery = 56%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/18/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/16/14 
 Pct Recovery = 57%  Analysis Date = 02/13/14 
 Pct Recovery = 58%  Analysis Date = 02/13/14 
 Pct Recovery = 58%  Analysis Date = 02/11/14 
 Pct Recovery = 58%  Analysis Date = 02/11/14 
 Pct Recovery = 58%  Analysis Date = 02/09/14 
 Pct Recovery = 59%  Analysis Date = 02/09/14 
 Pct Recovery = 59%  Analysis Date = 02/07/14 
 Pct Recovery = 59%  Analysis Date = 02/07/14 
 Pct Recovery = 59%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/05/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 02/02/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/31/14 
 Pct Recovery = 60%  Analysis Date = 01/29/14 
 Pct Recovery = 61%  Analysis Date = 01/29/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 63%  Analysis Date = 01/20/14 
 Pct Recovery = 63%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/18/14 
 Pct Recovery = 63%  Analysis Date = 01/16/14 
 Pct Recovery = 64%  Analysis Date = 01/16/14 
 Pct Recovery = 64%  Analysis Date = 01/14/14 
 Pct Recovery = 64%  Analysis Date = 01/14/14 
 Pct Recovery = 64%  Analysis Date = 01/11/14 
 Pct Recovery = 64%  Analysis Date = 01/11/14 
 Pct Recovery = 64%  Analysis Date = 01/09/14 
 Pct Recovery = 65%  Analysis Date = 01/09/14 
 Pct Recovery = 65%  Analysis Date = 01/07/14 
 Pct Recovery = 65%  Analysis Date = 01/07/14 
 Pct Recovery = 65%  Analysis Date = 01/05/14 
 Pct Recovery = 66%  Analysis Date = 01/05/14 
 Pct Recovery = 66%  Analysis Date = 01/02/14 
 Pct Recovery = 66%  Analysis Date = 01/02/14 
 Pct Recovery = 66%  Analysis Date = 12/31/13 
 Pct Recovery = 66%  Analysis Date = 12/31/13 
 Pct Recovery = 66%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 68%  Analysis Date = 12/22/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 68%  Analysis Date = 12/18/13 
 Pct Recovery = 69%  Analysis Date = 12/18/13 
 Pct Recovery = 69%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/16/13 
 Pct Recovery = 69%  Analysis Date = 12/14/13 
 Pct Recovery = 69%  Analysis Date = 12/14/13 
 Pct Recovery = 69%  Analysis Date = 12/11/13 
 Pct Recovery = 70%  Analysis Date = 12/11/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/09/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/07/13 
 Pct Recovery = 70%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 72%  Analysis Date = 11/28/13 
 Pct Recovery = 72%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/24/13 
 Pct Recovery = 73%  Analysis Date = 11/24/13 
 Pct Recovery = 73%  Analysis Date = 11/22/13 
 Pct Recovery = 73%  Analysis Date = 11/22/13 
 Pct Recovery = 73%  Analysis Date = 11/19/13 
 Pct Recovery = 73%  Analysis Date = 11/19/13 
 Pct Recovery = 73%  Analysis Date = 11/17/13 
 Pct Recovery = 74%  Analysis Date = 11/17/13 
 Pct Recovery = 74%  Analysis Date = 11/15/13 
 Pct Recovery = 74%  Analysis Date = 11/15/13 
 Pct Recovery = 74%  Analysis Date = 11/13/13 
 Pct Recovery = 74%  Analysis Date = 11/13/13 
 Pct Recovery = 74%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/11/13 
 Pct Recovery = 75%  Analysis Date = 11/08/13 
 Pct Recovery = 75%  Analysis Date = 11/08/13 
 Pct Recovery = 75%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/06/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/04/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 11/02/13 
 Pct Recovery = 76%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/31/13 
 Pct Recovery = 77%  Analysis Date = 10/28/13 
 Pct Recovery = 77%  Analysis Date = 10/28/13 
 Pct Recovery = 77%  Analysis Date = 10/26/13 
 Pct Recovery = 77%  Analysis Date = 10/26/13 
 Pct Recovery = 77%  Analysis Date = 10/24/13 
 Pct Recovery = 77%  Analysis Date = 10/24/13 
 Pct Recovery = 77%  Analysis Date = 10/22/13 
 Pct Recovery = 77%  Analysis Date = 10/22/13 
 Pct Recovery = 77%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/20/13 
 Pct Recovery = 78%  Analysis Date = 10/17/13 
 Pct Recovery = 78%  Analysis Date = 10/17/13 
 Pct Recovery = 78%  Analysis Date = 10/15/13 
 Pct Recovery = 78%  Analysis Date = 10/15/13 
 Pct Recovery = 78%  Analysis Date = 10/13/13 
 Pct Recovery = 78%  Analysis Date = 10/13/13 
 Pct Recovery = 78%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/11/13 
 Pct Recovery = 78%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/02/13 
 Pct Recovery = 79%  Analysis Date = 10/02/13 
 Pct Recovery = 79%  Analysis Date = 09/30/13 
 Pct Recovery = 79%  Analysis Date = 09/30/13 
 Pct Recovery = 79%  Analysis Date = 09/27/13 
 Pct Recovery = 79%  Analysis Date = 09/27/13 
 Pct Recovery = 79%  Analysis Date = 09/25/13 
 Pct Recovery = 79%  Analysis Date = 09/25/13 
 Pct Recovery = 79%  Analysis Date = 09/23/13 
 Pct Recovery = 79%  Analysis Date = 09/23/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 80%  Analysis Date = 09/19/13 
 Pct Recovery = 80%  Analysis Date = 09/16/13 
 Pct Recovery = 80%  Analysis Date = 09/16/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/10/13 
 Pct Recovery = 80%  Analysis Date = 09/10/13 
 Pct Recovery = 80%  Analysis Date = 09/08/13 
 Pct Recovery = 80%  Analysis Date = 09/08/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 80%  Analysis Date = 09/05/13 
 Pct Recovery = 80%  Analysis Date = 09/03/13 
 Pct Recovery = 80%  Analysis Date = 09/03/13 
 Pct Recovery = 80%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 09/01/13 
 Pct Recovery = 81%  Analysis Date = 08/30/13 
 Pct Recovery = 81%  Analysis Date = 08/30/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/25/13 
 Pct Recovery = 81%  Analysis Date = 08/25/13 
 Pct Recovery = 81%  Analysis Date = 08/23/13 
 Pct Recovery = 81%  Analysis Date = 08/23/13 
 Pct Recovery = 81%  Analysis Date = 08/21/13 
 Pct Recovery = 81%  Analysis Date = 08/21/13 
 Pct Recovery = 81%  Analysis Date = 08/19/13 
 Pct Recovery = 81%  Analysis Date = 08/19/13 
 Pct Recovery = 81%  Analysis Date = 08/17/13 
 Pct Recovery = 82%  Analysis Date = 08/17/13 
 Pct Recovery = 82%  Analysis Date = 08/14/13 
 Pct Recovery = 81%  Analysis Date = 08/14/13 
 Pct Recovery = 81%  Analysis Date = 08/12/13 
 Pct Recovery = 81%  Analysis Date = 08/12/13 
 Pct Recovery = 81%  Analysis Date = 08/10/13 
 Pct Recovery = 81%  Analysis Date = 08/10/13 
 Pct Recovery = 81%  Analysis Date = 08/08/13 
 Pct Recovery = 81%  Analysis Date = 08/08/13 
 Pct Recovery = 81%  Analysis Date = 08/06/13 
 Pct Recovery = 81%  Analysis Date = 08/06/13 
 Pct Recovery = 81%  Analysis Date = 08/03/13 
 Pct Recovery = 81%  Analysis Date = 08/03/13 
 Pct Recovery = 81%  Analysis Date = 08/01/13 
 Pct Recovery = 81%  Analysis Date = 08/01/13 
 Pct Recovery = 81%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/19/13 
 Pct Recovery = 80%  Analysis Date = 07/19/13 
 Pct Recovery = 80%  Analysis Date = 07/17/13 
 Pct Recovery = 80%  Analysis Date = 07/17/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/12/13 
 Pct Recovery = 79%  Analysis Date = 07/12/13 
 Pct Recovery = 79%  Analysis Date = 07/10/13 
 Pct Recovery = 79%  Analysis Date = 07/10/13 
 Pct Recovery = 79%  Analysis Date = 07/08/13 
 Pct Recovery = 79%  Analysis Date = 07/08/13 
 Pct Recovery = 79%  Analysis Date = 07/06/13 
 Pct Recovery = 79%  Analysis Date = 07/06/13 
 Pct Recovery = 79%  Analysis Date = 07/03/13 
 Pct Recovery = 79%  Analysis Date = 07/03/13 
 Pct Recovery = 79%  Analysis Date = 07/01/13 
 Pct Recovery = 79%  Analysis Date = 07/01/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/29/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/27/13 
 Pct Recovery = 79%  Analysis Date = 06/25/13 
 Pct Recovery = 78%  Analysis Date = 06/25/13 
 Pct Recovery = 78%  Analysis Date = 06/22/13 
 Pct Recovery = 78%  Analysis Date = 06/22/13 
 Pct Recovery = 78%  Analysis Date = 06/20/13 
 Pct Recovery = 78%  Analysis Date = 06/20/13 
 Pct Recovery = 78%  Analysis Date = 06/18/13 
 Pct Recovery = 78%  Analysis Date = 06/18/13 
 Pct Recovery = 78%  Analysis Date = 06/16/13 
 Pct Recovery = 78%  Analysis Date = 06/16/13 
 Pct Recovery = 78%  Analysis Date = 06/14/13 
 Pct Recovery = 78%  Analysis Date = 06/14/13 
 Pct Recovery = 78%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/09/13 
 Pct Recovery = 78%  Analysis Date = 06/09/13 
 Pct Recovery = 78%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/07/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/27/13 
 Pct Recovery = 77%  Analysis Date = 05/27/13 
 Pct Recovery = 77%  Analysis Date = 05/25/13 
 Pct Recovery = 77%  Analysis Date = 05/25/13 
 Pct Recovery = 77%  Analysis Date = 05/23/13 
 Pct Recovery = 77%  Analysis Date = 05/23/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 76%  Analysis Date = 05/20/13 
 Pct Recovery = 76%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/09/13 
 Pct Recovery = 76%  Analysis Date = 05/09/13 
 Pct Recovery = 76%  Analysis Date = 05/07/13 
 Pct Recovery = 76%  Analysis Date = 05/07/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 05/01/13 
 Pct Recovery = 76%  Analysis Date = 04/28/13 
 Pct Recovery = 76%  Analysis Date = 04/28/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 Pct Recovery = 76%  Analysis Date = 04/24/13 
 Pct Recovery = 77%  Analysis Date = 04/24/13 
 Pct Recovery = 77%  Analysis Date = 04/22/13 
 Pct Recovery = 77%  Analysis Date = 04/22/13 
 Pct Recovery = 77%  Analysis Date = 04/19/13 
 Pct Recovery = 78%  Analysis Date = 04/19/13 
 Pct Recovery = 78%  Analysis Date = 04/17/13 
 Pct Recovery = 78%  Analysis Date = 04/17/13 
 Pct Recovery = 78%  Analysis Date = 04/15/13 
 Pct Recovery = 79%  Analysis Date = 04/15/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/13/13 
 Pct Recovery = 79%  Analysis Date = 04/11/13 
 Pct Recovery = 80%  Analysis Date = 04/11/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/08/13 
 Pct Recovery = 80%  Analysis Date = 04/06/13 
 Pct Recovery = 81%  Analysis Date = 04/06/13 
 Pct Recovery = 81%  Analysis Date = 04/04/13 
 Pct Recovery = 81%  Analysis Date = 04/04/13 
 Pct Recovery = 81%  Analysis Date = 04/02/13 
 Pct Recovery = 81%  Analysis Date = 04/02/13 
 Pct Recovery = 81%  Analysis Date = 03/31/13 
 Pct Recovery = 82%  Analysis Date = 03/31/13 
 Pct Recovery = 82%  Analysis Date = 03/28/13 
 Pct Recovery = 82%  Analysis Date = 03/28/13 
 Pct Recovery = 82%  Analysis Date = 03/26/13 
 Pct Recovery = 83%  Analysis Date = 03/26/13 
 Pct Recovery = 83%  Analysis Date = 03/24/13 
 Pct Recovery = 83%  Analysis Date = 03/24/13 
 Pct Recovery = 83%  Analysis Date = 03/22/13 
 Pct Recovery = 84%  Analysis Date = 03/22/13 
 Pct Recovery = 84%  Analysis Date = 03/20/13 
 Pct Recovery = 84%  Analysis Date = 03/20/13 
 Pct Recovery = 84%  Analysis Date = 03/17/13 
 Pct Recovery = 85%  Analysis Date = 03/17/13 
 Pct Recovery = 85%  Analysis Date = 03/15/13 
 Pct Recovery = 85%  Analysis Date = 03/15/13 
 Pct Recovery = 85%  Analysis Date = 03/13/13 
 Pct Recovery = 85%  Analysis Date = 03/13/13 
 Pct Recovery = 85%  Analysis Date = 03/11/13 
 Pct Recovery = 86%  Analysis Date = 03/11/13 
 Pct Recovery = 86%  Analysis Date = 03/09/13 
 Pct Recovery = 86%  Analysis Date = 03/09/13 
 Pct Recovery = 86%  Analysis Date = 03/06/13 
 Pct Recovery = 87%  Analysis Date = 03/06/13 
 Pct Recovery = 87%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/04/13 
 Pct Recovery = 87%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Analysis Date = 02/26/13 
 Pct Recovery = 88%  Analysis Date = 02/26/13 
 Pct Recovery = 88%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/23/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/21/13 
 Pct Recovery = 89%  Analysis Date = 02/19/13 
 Pct Recovery = 90%  Analysis Date = 02/19/13 
 Pct Recovery = 90%  Analysis Date = 02/17/13 
 Pct Recovery = 90%  Analysis Date = 02/17/13 
 Pct Recovery = 90%  Analysis Date = 02/15/13 
 Pct Recovery = 91%  Analysis Date = 02/15/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/12/13 
 Pct Recovery = 91%  Analysis Date = 02/10/13 
 Pct Recovery = 91%  Analysis Date = 02/10/13 
 Pct Recovery = 91%  Analysis Date = 02/08/13 
 Pct Recovery = 92%  Analysis Date = 02/08/13 
 Pct Recovery = 92%  Analysis Date = 02/06/13 
 Pct Recovery = 92%  Analysis Date = 02/06/13 
 Pct Recovery = 92%  Analysis Date = 02/04/13 
 Pct Recovery = 93%  Analysis Date = 02/04/13 
 Pct Recovery = 93%  Analysis Date = 02/01/13 
 Pct Recovery = 93%  Analysis Date = 02/01/13 
 Pct Recovery = 93%  Analysis Date = 01/30/13 
 Pct Recovery = 94%  Analysis Date = 01/30/13 
 Pct Recovery = 94%  Analysis Date = 01/28/13 
 Pct Recovery = 94%  Analysis Date = 01/28/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/26/13 
 Pct Recovery = 94%  Analysis Date = 01/24/13 
 Pct Recovery = 95%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
PSEUDOEPHEDRINE+EPHEDRINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 7 75% 16% 82% 16%
Total 7 75% 16% 82% 16%

Sample Statistics
PSEUDOEPHEDRINE+EPHEDRINE

Characteristic N % % Basis
Plotted 7 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 0 0% 0 out of 7
Not Spiked 25 .  
False Positives 1 4% 1 out of 24

OBSP Determination:
QUININE
METHOD: LC9017 , TESTIDCODE: 68011LCM56

 Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 72%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 153%  Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 74%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 60%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 61%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 75%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 86%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 65%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 50%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 38%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 61%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 35%  Analysis Date = 04/09/14 
 Pct Recovery = 56%  Analysis Date = 04/07/14 
 Pct Recovery = 56%  Analysis Date = 04/07/14 
 Pct Recovery = 56%  Analysis Date = 04/05/14 
 Pct Recovery = 57%  Analysis Date = 04/05/14 
 Pct Recovery = 57%  Analysis Date = 04/02/14 
 Pct Recovery = 57%  Analysis Date = 04/02/14 
 Pct Recovery = 57%  Analysis Date = 03/31/14 
 Pct Recovery = 57%  Analysis Date = 03/31/14 
 Pct Recovery = 57%  Analysis Date = 03/28/14 
 Pct Recovery = 57%  Analysis Date = 03/28/14 
 Pct Recovery = 57%  Analysis Date = 03/26/14 
 Pct Recovery = 57%  Analysis Date = 03/26/14 
 Pct Recovery = 57%  Analysis Date = 03/24/14 
 Pct Recovery = 58%  Analysis Date = 03/24/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/19/14 
 Pct Recovery = 58%  Analysis Date = 03/19/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 58%  Analysis Date = 03/12/14 
 Pct Recovery = 58%  Analysis Date = 03/12/14 
 Pct Recovery = 58%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/04/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 03/02/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/28/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/25/14 
 Pct Recovery = 59%  Analysis Date = 02/23/14 
 Pct Recovery = 60%  Analysis Date = 02/23/14 
 Pct Recovery = 60%  Analysis Date = 02/20/14 
 Pct Recovery = 60%  Analysis Date = 02/20/14 
 Pct Recovery = 60%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/18/14 
 Pct Recovery = 60%  Analysis Date = 02/15/14 
 Pct Recovery = 60%  Analysis Date = 02/15/14 
 Pct Recovery = 60%  Analysis Date = 02/13/14 
 Pct Recovery = 60%  Analysis Date = 02/13/14 
 Pct Recovery = 60%  Analysis Date = 02/11/14 
 Pct Recovery = 60%  Analysis Date = 02/11/14 
 Pct Recovery = 60%  Analysis Date = 02/08/14 
 Pct Recovery = 61%  Analysis Date = 02/08/14 
 Pct Recovery = 61%  Analysis Date = 02/06/14 
 Pct Recovery = 61%  Analysis Date = 02/06/14 
 Pct Recovery = 61%  Analysis Date = 02/03/14 
 Pct Recovery = 61%  Analysis Date = 02/03/14 
 Pct Recovery = 61%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 02/01/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/30/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/27/14 
 Pct Recovery = 61%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/25/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/22/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/20/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/18/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/15/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/13/14 
 Pct Recovery = 62%  Analysis Date = 01/10/14 
 Pct Recovery = 62%  Analysis Date = 01/10/14 
 Pct Recovery = 62%  Analysis Date = 01/08/14 
 Pct Recovery = 63%  Analysis Date = 01/08/14 
 Pct Recovery = 63%  Analysis Date = 01/06/14 
 Pct Recovery = 63%  Analysis Date = 01/06/14 
 Pct Recovery = 63%  Analysis Date = 01/03/14 
 Pct Recovery = 63%  Analysis Date = 01/03/14 
 Pct Recovery = 63%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 01/01/14 
 Pct Recovery = 63%  Analysis Date = 12/29/13 
 Pct Recovery = 63%  Analysis Date = 12/29/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/24/13 
 Pct Recovery = 63%  Analysis Date = 12/24/13 
 Pct Recovery = 63%  Analysis Date = 12/22/13 
 Pct Recovery = 63%  Analysis Date = 12/22/13 
 Pct Recovery = 63%  Analysis Date = 12/20/13 
 Pct Recovery = 63%  Analysis Date = 12/20/13 
 Pct Recovery = 63%  Analysis Date = 12/17/13 
 Pct Recovery = 64%  Analysis Date = 12/17/13 
 Pct Recovery = 64%  Analysis Date = 12/15/13 
 Pct Recovery = 64%  Analysis Date = 12/15/13 
 Pct Recovery = 64%  Analysis Date = 12/12/13 
 Pct Recovery = 64%  Analysis Date = 12/12/13 
 Pct Recovery = 64%  Analysis Date = 12/10/13 
 Pct Recovery = 64%  Analysis Date = 12/10/13 
 Pct Recovery = 64%  Analysis Date = 12/08/13 
 Pct Recovery = 64%  Analysis Date = 12/08/13 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 Pct Recovery = 64%  Analysis Date = 12/05/13 
 Pct Recovery = 64%  Analysis Date = 12/03/13 
 Pct Recovery = 64%  Analysis Date = 12/03/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/30/13 
 Pct Recovery = 64%  Analysis Date = 11/28/13 
 Pct Recovery = 64%  Analysis Date = 11/28/13 
 Pct Recovery = 64%  Analysis Date = 11/26/13 
 Pct Recovery = 65%  Analysis Date = 11/26/13 
 Pct Recovery = 65%  Analysis Date = 11/23/13 
 Pct Recovery = 65%  Analysis Date = 11/23/13 
 Pct Recovery = 65%  Analysis Date = 11/21/13 
 Pct Recovery = 65%  Analysis Date = 11/21/13 
 Pct Recovery = 65%  Analysis Date = 11/18/13 
 Pct Recovery = 65%  Analysis Date = 11/18/13 
 Pct Recovery = 65%  Analysis Date = 11/16/13 
 Pct Recovery = 65%  Analysis Date = 11/16/13 
 Pct Recovery = 65%  Analysis Date = 11/13/13 
 Pct Recovery = 65%  Analysis Date = 11/13/13 
 Pct Recovery = 65%  Analysis Date = 11/11/13 
 Pct Recovery = 65%  Analysis Date = 11/11/13 
 Pct Recovery = 65%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/09/13 
 Pct Recovery = 65%  Analysis Date = 11/06/13 
 Pct Recovery = 65%  Analysis Date = 11/06/13 
 Pct Recovery = 65%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/01/13 
 Pct Recovery = 66%  Analysis Date = 11/01/13 
 Pct Recovery = 66%  Analysis Date = 10/30/13 
 Pct Recovery = 66%  Analysis Date = 10/30/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/25/13 
 Pct Recovery = 66%  Analysis Date = 10/25/13 
 Pct Recovery = 66%  Analysis Date = 10/23/13 
 Pct Recovery = 66%  Analysis Date = 10/23/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/18/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/16/13 
 Pct Recovery = 66%  Analysis Date = 10/13/13 
 Pct Recovery = 66%  Analysis Date = 10/13/13 
 Pct Recovery = 66%  Analysis Date = 10/11/13 
 Pct Recovery = 67%  Analysis Date = 10/11/13 
 Pct Recovery = 67%  Analysis Date = 10/08/13 
 Pct Recovery = 67%  Analysis Date = 10/08/13 
 Pct Recovery = 67%  Analysis Date = 10/06/13 
 Pct Recovery = 67%  Analysis Date = 10/06/13 
 Pct Recovery = 67%  Analysis Date = 10/04/13 
 Pct Recovery = 67%  Analysis Date = 10/04/13 
 Pct Recovery = 67%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 10/01/13 
 Pct Recovery = 67%  Analysis Date = 09/29/13 
 Pct Recovery = 67%  Analysis Date = 09/29/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/26/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/24/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/21/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/19/13 
 Pct Recovery = 67%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/17/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/14/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/12/13 
 Pct Recovery = 68%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/09/13 
 Pct Recovery = 68%  Analysis Date = 09/07/13 
 Pct Recovery = 68%  Analysis Date = 09/07/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/05/13 
 Pct Recovery = 68%  Analysis Date = 09/02/13 
 Pct Recovery = 68%  Analysis Date = 09/02/13 
 Pct Recovery = 68%  Analysis Date = 08/31/13 
 Pct Recovery = 68%  Analysis Date = 08/31/13 
 Pct Recovery = 68%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/24/13 
 Pct Recovery = 69%  Analysis Date = 08/24/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/21/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/19/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/16/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/14/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/04/13 
 Pct Recovery = 70%  Analysis Date = 08/04/13 
 Pct Recovery = 70%  Analysis Date = 08/02/13 
 Pct Recovery = 70%  Analysis Date = 08/02/13 
 Pct Recovery = 70%  Analysis Date = 07/30/13 
 Pct Recovery = 70%  Analysis Date = 07/30/13 
 Pct Recovery = 70%  Analysis Date = 07/28/13 
 Pct Recovery = 70%  Analysis Date = 07/28/13 
 Pct Recovery = 70%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/26/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/23/13 
 Pct Recovery = 70%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/21/13 
 Pct Recovery = 71%  Analysis Date = 07/18/13 
 Pct Recovery = 71%  Analysis Date = 07/18/13 
 Pct Recovery = 71%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/16/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/14/13 
 Pct Recovery = 71%  Analysis Date = 07/11/13 
 Pct Recovery = 71%  Analysis Date = 07/11/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/09/13 
 Pct Recovery = 71%  Analysis Date = 07/06/13 
 Pct Recovery = 72%  Analysis Date = 07/06/13 
 Pct Recovery = 72%  Analysis Date = 07/04/13 
 Pct Recovery = 72%  Analysis Date = 07/04/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 07/02/13 
 Pct Recovery = 72%  Analysis Date = 06/29/13 
 Pct Recovery = 72%  Analysis Date = 06/29/13 
 Pct Recovery = 72%  Analysis Date = 06/27/13 
 Pct Recovery = 72%  Analysis Date = 06/27/13 
 Pct Recovery = 72%  Analysis Date = 06/24/13 
 Pct Recovery = 72%  Analysis Date = 06/24/13 
 Pct Recovery = 72%  Analysis Date = 06/22/13 
 Pct Recovery = 72%  Analysis Date = 06/22/13 
 Pct Recovery = 72%  Analysis Date = 06/19/13 
 Pct Recovery = 73%  Analysis Date = 06/19/13 
 Pct Recovery = 73%  Analysis Date = 06/17/13 
 Pct Recovery = 73%  Analysis Date = 06/17/13 
 Pct Recovery = 73%  Analysis Date = 06/15/13 
 Pct Recovery = 73%  Analysis Date = 06/15/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/10/13 
 Pct Recovery = 73%  Analysis Date = 06/10/13 
 Pct Recovery = 73%  Analysis Date = 06/07/13 
 Pct Recovery = 73%  Analysis Date = 06/07/13 
 Pct Recovery = 73%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/05/13 
 Pct Recovery = 74%  Analysis Date = 06/03/13 
 Pct Recovery = 74%  Analysis Date = 06/03/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/31/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/29/13 
 Pct Recovery = 74%  Analysis Date = 05/26/13 
 Pct Recovery = 74%  Analysis Date = 05/26/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/24/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 Pct Recovery = 74%  Analysis Date = 05/19/13 
 Pct Recovery = 75%  Analysis Date = 05/19/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/17/13 
 Pct Recovery = 75%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/07/13 
 Pct Recovery = 75%  Analysis Date = 05/07/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/05/13 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 Pct Recovery = 76%  Analysis Date = 05/02/13 
 Pct Recovery = 76%  Analysis Date = 04/30/13 
 Pct Recovery = 74%  Analysis Date = 04/30/13 
 Pct Recovery = 74%  Analysis Date = 04/27/13 
 Pct Recovery = 72%  Analysis Date = 04/27/13 
 Pct Recovery = 72%  Analysis Date = 04/25/13 
 Pct Recovery = 70%  Analysis Date = 04/25/13 
 Pct Recovery = 70%  Analysis Date = 04/23/13 
 Pct Recovery = 70%  Analysis Date = 04/23/13 
 Pct Recovery = 70%  Analysis Date = 04/20/13 
 Pct Recovery = 71%  Analysis Date = 04/20/13 
 Pct Recovery = 71%  Analysis Date = 04/18/13 
 Pct Recovery = 71%  Analysis Date = 04/18/13 
 Pct Recovery = 71%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/15/13 
 Pct Recovery = 71%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/11/13 
 Pct Recovery = 72%  Analysis Date = 04/11/13 
 Pct Recovery = 72%  Analysis Date = 04/08/13 
 Pct Recovery = 73%  Analysis Date = 04/08/13 
 Pct Recovery = 73%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/03/13 
 Pct Recovery = 73%  Analysis Date = 04/03/13 
 Pct Recovery = 73%  Analysis Date = 04/01/13 
 Pct Recovery = 74%  Analysis Date = 04/01/13 
 Pct Recovery = 74%  Analysis Date = 03/30/13 
 Pct Recovery = 74%  Analysis Date = 03/30/13 
 Pct Recovery = 74%  Analysis Date = 03/27/13 
 Pct Recovery = 74%  Analysis Date = 03/27/13 
 Pct Recovery = 74%  Analysis Date = 03/25/13 
 Pct Recovery = 74%  Analysis Date = 03/25/13 
 Pct Recovery = 74%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/13/13 
 Pct Recovery = 75%  Analysis Date = 03/10/13 
 Pct Recovery = 75%  Analysis Date = 03/10/13 
 Pct Recovery = 75%  Analysis Date = 03/08/13 
 Pct Recovery = 75%  Analysis Date = 03/08/13 
 Pct Recovery = 75%  Analysis Date = 03/05/13 
 Pct Recovery = 76%  Analysis Date = 03/05/13 
 Pct Recovery = 76%  Analysis Date = 03/03/13 
 Pct Recovery = 76%  Analysis Date = 03/03/13 
 Pct Recovery = 76%  Analysis Date = 03/01/13 
 Pct Recovery = 76%  Analysis Date = 03/01/13 
 Pct Recovery = 76%  Analysis Date = 02/26/13 
 Pct Recovery = 76%  Analysis Date = 02/26/13 
 Pct Recovery = 76%  Analysis Date = 02/24/13 
 Pct Recovery = 76%  Analysis Date = 02/24/13 
 Pct Recovery = 76%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/21/13 
 Pct Recovery = 76%  Analysis Date = 02/19/13 
 Pct Recovery = 76%  Analysis Date = 02/19/13 
 Pct Recovery = 76%  Analysis Date = 02/17/13 
 Pct Recovery = 77%  Analysis Date = 02/17/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/14/13 
 Pct Recovery = 77%  Analysis Date = 02/12/13 
 Pct Recovery = 77%  Analysis Date = 02/12/13 
 Pct Recovery = 77%  Analysis Date = 02/09/13 
 Pct Recovery = 77%  Analysis Date = 02/09/13 
 Pct Recovery = 77%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/02/13 
 Pct Recovery = 77%  Analysis Date = 02/02/13 
 Pct Recovery = 77%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/31/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/28/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/26/13 
 Pct Recovery = 78%  Analysis Date = 01/23/13 
 Pct Recovery = 78%  Analysis Date = 01/23/13 
 Pct Recovery = 78%  Analysis Date = 01/21/13 
 Pct Recovery = 77%  Analysis Date = 01/21/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/16/13 
 Pct Recovery = 76%  Analysis Date = 01/16/13 
 Pct Recovery = 76%  Analysis Date = 01/14/13 
 Pct Recovery = 75%  Analysis Date = 01/14/13 
 Pct Recovery = 75%  Analysis Date = 01/11/13 
 Pct Recovery = 74%  Analysis Date = 01/11/13 
 Pct Recovery = 74%  Analysis Date = 01/09/13 
 Pct Recovery = 74%  Analysis Date = 01/09/13 
 Pct Recovery = 74%  Analysis Date = 01/07/13 
 Pct Recovery = 73%  Analysis Date = 01/07/13 
 Pct Recovery = 73%  Analysis Date = 01/04/13 
 Pct Recovery = 72%  Analysis Date = 01/04/13 
 Pct Recovery = 72%  Analysis Date = 01/02/13 
 Pct Recovery = 71%  Analysis Date = 01/02/13 
 Pct Recovery = 71%  Analysis Date = 12/30/12 
 Pct Recovery = 71%  Analysis Date = 12/30/12 
 Pct Recovery = 71%  Analysis Date = 12/28/12 
 Pct Recovery = 70%  Analysis Date = 12/28/12 
 Pct Recovery = 70%  Analysis Date = 12/26/12 
 Pct Recovery = 69%  Analysis Date = 12/26/12 
 Pct Recovery = 69%  Analysis Date = 12/23/12 
 Pct Recovery = 68%  Analysis Date = 12/23/12 
 Pct Recovery = 68%  Analysis Date = 12/21/12 
 Pct Recovery = 68%  Analysis Date = 12/21/12 
 Pct Recovery = 68%  Analysis Date = 12/18/12 
 Pct Recovery = 67%  Analysis Date = 12/18/12 
 Pct Recovery = 67%  Analysis Date = 12/16/12 
 Pct Recovery = 66%  Analysis Date = 12/16/12 
 Pct Recovery = 66%  Analysis Date = 12/14/12 
 Pct Recovery = 66%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
QUININE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 68% 28% 63% 16%
Total 14 68% 28% 63% 16%

Sample Statistics
QUININE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 6 43% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
RALOXIFENE
METHOD: LC9017 , TESTIDCODE: 67530LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 30%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 19%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 60%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 31%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 26%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 22%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 25%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 48%  Analysis Date = 04/09/14 
 Pct Recovery = 35%  Analysis Date = 04/08/14 
 Pct Recovery = 35%  Analysis Date = 04/08/14 
 Pct Recovery = 35%  Analysis Date = 04/06/14 
 Pct Recovery = 35%  Analysis Date = 04/06/14 
 Pct Recovery = 35%  Analysis Date = 04/04/14 
 Pct Recovery = 35%  Analysis Date = 04/04/14 
 Pct Recovery = 35%  Analysis Date = 04/03/14 
 Pct Recovery = 35%  Analysis Date = 04/03/14 
 Pct Recovery = 35%  Analysis Date = 04/01/14 
 Pct Recovery = 35%  Analysis Date = 04/01/14 
 Pct Recovery = 35%  Analysis Date = 03/30/14 
 Pct Recovery = 35%  Analysis Date = 03/30/14 
 Pct Recovery = 35%  Analysis Date = 03/29/14 
 Pct Recovery = 35%  Analysis Date = 03/29/14 
 Pct Recovery = 35%  Analysis Date = 03/27/14 
 Pct Recovery = 35%  Analysis Date = 03/27/14 
 Pct Recovery = 35%  Analysis Date = 03/25/14 
 Pct Recovery = 35%  Analysis Date = 03/25/14 
 Pct Recovery = 35%  Analysis Date = 03/23/14 
 Pct Recovery = 35%  Analysis Date = 03/23/14 
 Pct Recovery = 35%  Analysis Date = 03/22/14 
 Pct Recovery = 36%  Analysis Date = 03/22/14 
 Pct Recovery = 36%  Analysis Date = 03/20/14 
 Pct Recovery = 36%  Analysis Date = 03/20/14 
 Pct Recovery = 36%  Analysis Date = 03/18/14 
 Pct Recovery = 36%  Analysis Date = 03/18/14 
 Pct Recovery = 36%  Analysis Date = 03/17/14 
 Pct Recovery = 36%  Analysis Date = 03/17/14 
 Pct Recovery = 36%  Analysis Date = 03/15/14 
 Pct Recovery = 36%  Analysis Date = 03/15/14 
 Pct Recovery = 36%  Analysis Date = 03/13/14 
 Pct Recovery = 36%  Analysis Date = 03/13/14 
 Pct Recovery = 36%  Analysis Date = 03/11/14 
 Pct Recovery = 36%  Analysis Date = 03/11/14 
 Pct Recovery = 36%  Analysis Date = 03/10/14 
 Pct Recovery = 36%  Analysis Date = 03/10/14 
 Pct Recovery = 36%  Analysis Date = 03/08/14 
 Pct Recovery = 36%  Analysis Date = 03/08/14 
 Pct Recovery = 36%  Analysis Date = 03/06/14 
 Pct Recovery = 36%  Analysis Date = 03/06/14 
 Pct Recovery = 36%  Analysis Date = 03/05/14 
 Pct Recovery = 36%  Analysis Date = 03/05/14 
 Pct Recovery = 36%  Analysis Date = 03/03/14 
 Pct Recovery = 36%  Analysis Date = 03/03/14 
 Pct Recovery = 36%  Analysis Date = 03/01/14 
 Pct Recovery = 36%  Analysis Date = 03/01/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/27/14 
 Pct Recovery = 36%  Analysis Date = 02/26/14 
 Pct Recovery = 36%  Analysis Date = 02/26/14 
 Pct Recovery = 36%  Analysis Date = 02/24/14 
 Pct Recovery = 36%  Analysis Date = 02/24/14 
 Pct Recovery = 36%  Analysis Date = 02/22/14 
 Pct Recovery = 37%  Analysis Date = 02/22/14 
 Pct Recovery = 37%  Analysis Date = 02/21/14 
 Pct Recovery = 37%  Analysis Date = 02/21/14 
 Pct Recovery = 37%  Analysis Date = 02/19/14 
 Pct Recovery = 36%  Analysis Date = 02/19/14 
 Pct Recovery = 36%  Analysis Date = 02/17/14 
 Pct Recovery = 36%  Analysis Date = 02/17/14 
 Pct Recovery = 36%  Analysis Date = 02/15/14 
 Pct Recovery = 36%  Analysis Date = 02/15/14 
 Pct Recovery = 36%  Analysis Date = 02/14/14 
 Pct Recovery = 36%  Analysis Date = 02/14/14 
 Pct Recovery = 36%  Analysis Date = 02/12/14 
 Pct Recovery = 35%  Analysis Date = 02/12/14 
 Pct Recovery = 35%  Analysis Date = 02/10/14 
 Pct Recovery = 35%  Analysis Date = 02/10/14 
 Pct Recovery = 35%  Analysis Date = 02/09/14 
 Pct Recovery = 35%  Analysis Date = 02/09/14 
 Pct Recovery = 35%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/07/14 
 Pct Recovery = 34%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/05/14 
 Pct Recovery = 34%  Analysis Date = 02/04/14 
 Pct Recovery = 34%  Analysis Date = 02/04/14 
 Pct Recovery = 34%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 02/02/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/31/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/29/14 
 Pct Recovery = 33%  Analysis Date = 01/28/14 
 Pct Recovery = 32%  Analysis Date = 01/28/14 
 Pct Recovery = 32%  Analysis Date = 01/26/14 
 Pct Recovery = 32%  Analysis Date = 01/26/14 
 Pct Recovery = 32%  Analysis Date = 01/24/14 
 Pct Recovery = 32%  Analysis Date = 01/24/14 
 Pct Recovery = 32%  Analysis Date = 01/23/14 
 Pct Recovery = 32%  Analysis Date = 01/23/14 
 Pct Recovery = 32%  Analysis Date = 01/21/14 
 Pct Recovery = 31%  Analysis Date = 01/21/14 
 Pct Recovery = 31%  Analysis Date = 01/19/14 
 Pct Recovery = 31%  Analysis Date = 01/19/14 
 Pct Recovery = 31%  Analysis Date = 01/17/14 
 Pct Recovery = 31%  Analysis Date = 01/17/14 
 Pct Recovery = 31%  Analysis Date = 01/16/14 
 Pct Recovery = 30%  Analysis Date = 01/16/14 
 Pct Recovery = 30%  Analysis Date = 01/14/14 
 Pct Recovery = 30%  Analysis Date = 01/14/14 
 Pct Recovery = 30%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/12/14 
 Pct Recovery = 31%  Analysis Date = 01/11/14 
 Pct Recovery = 31%  Analysis Date = 01/11/14 
 Pct Recovery = 31%  Analysis Date = 01/09/14 
 Pct Recovery = 31%  Analysis Date = 01/09/14 
 Pct Recovery = 31%  Analysis Date = 01/07/14 
 Pct Recovery = 31%  Analysis Date = 01/07/14 
 Pct Recovery = 31%  Analysis Date = 01/05/14 
 Pct Recovery = 32%  Analysis Date = 01/05/14 
 Pct Recovery = 32%  Analysis Date = 01/04/14 
 Pct Recovery = 32%  Analysis Date = 01/04/14 
 Pct Recovery = 32%  Analysis Date = 01/02/14 
 Pct Recovery = 32%  Analysis Date = 01/02/14 
 Pct Recovery = 32%  Analysis Date = 12/31/13 
 Pct Recovery = 32%  Analysis Date = 12/31/13 
 Pct Recovery = 32%  Analysis Date = 12/30/13 
 Pct Recovery = 33%  Analysis Date = 12/30/13 
 Pct Recovery = 33%  Analysis Date = 12/28/13 
 Pct Recovery = 33%  Analysis Date = 12/28/13 
 Pct Recovery = 33%  Analysis Date = 12/26/13 
 Pct Recovery = 33%  Analysis Date = 12/26/13 
 Pct Recovery = 33%  Analysis Date = 12/24/13 
 Pct Recovery = 33%  Analysis Date = 12/24/13 
 Pct Recovery = 33%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/23/13 
 Pct Recovery = 33%  Analysis Date = 12/21/13 
 Pct Recovery = 34%  Analysis Date = 12/21/13 
 Pct Recovery = 34%  Analysis Date = 12/19/13 
 Pct Recovery = 34%  Analysis Date = 12/19/13 
 Pct Recovery = 34%  Analysis Date = 12/18/13 
 Pct Recovery = 34%  Analysis Date = 12/18/13 
 Pct Recovery = 34%  Analysis Date = 12/16/13 
 Pct Recovery = 34%  Analysis Date = 12/16/13 
 Pct Recovery = 34%  Analysis Date = 12/14/13 
 Pct Recovery = 35%  Analysis Date = 12/14/13 
 Pct Recovery = 35%  Analysis Date = 12/13/13 
 Pct Recovery = 35%  Analysis Date = 12/13/13 
 Pct Recovery = 35%  Analysis Date = 12/11/13 
 Pct Recovery = 35%  Analysis Date = 12/11/13 
 Pct Recovery = 35%  Analysis Date = 12/09/13 
 Pct Recovery = 35%  Analysis Date = 12/09/13 
 Pct Recovery = 35%  Analysis Date = 12/07/13 
 Pct Recovery = 35%  Analysis Date = 12/07/13 
 Pct Recovery = 35%  Analysis Date = 12/06/13 
 Pct Recovery = 36%  Analysis Date = 12/06/13 
 Pct Recovery = 36%  Analysis Date = 12/04/13 
 Pct Recovery = 36%  Analysis Date = 12/04/13 
 Pct Recovery = 36%  Analysis Date = 12/02/13 
 Pct Recovery = 37%  Analysis Date = 12/02/13 
 Pct Recovery = 37%  Analysis Date = 12/01/13 
 Pct Recovery = 37%  Analysis Date = 12/01/13 
 Pct Recovery = 37%  Analysis Date = 11/29/13 
 Pct Recovery = 38%  Analysis Date = 11/29/13 
 Pct Recovery = 38%  Analysis Date = 11/27/13 
 Pct Recovery = 38%  Analysis Date = 11/27/13 
 Pct Recovery = 38%  Analysis Date = 11/25/13 
 Pct Recovery = 39%  Analysis Date = 11/25/13 
 Pct Recovery = 39%  Analysis Date = 11/24/13 
 Pct Recovery = 40%  Analysis Date = 11/24/13 
 Pct Recovery = 40%  Analysis Date = 11/22/13 
 Pct Recovery = 40%  Analysis Date = 11/22/13 
 Pct Recovery = 40%  Analysis Date = 11/20/13 
 Pct Recovery = 41%  Analysis Date = 11/20/13 
 Pct Recovery = 41%  Analysis Date = 11/19/13 
 Pct Recovery = 41%  Analysis Date = 11/19/13 
 Pct Recovery = 41%  Analysis Date = 11/17/13 
 Pct Recovery = 42%  Analysis Date = 11/17/13 
 Pct Recovery = 42%  Analysis Date = 11/15/13 
 Pct Recovery = 43%  Analysis Date = 11/15/13 
 Pct Recovery = 43%  Analysis Date = 11/13/13 
 Pct Recovery = 43%  Analysis Date = 11/13/13 
 Pct Recovery = 43%  Analysis Date = 11/12/13 
 Pct Recovery = 44%  Analysis Date = 11/12/13 
 Pct Recovery = 44%  Analysis Date = 11/10/13 
 Pct Recovery = 44%  Analysis Date = 11/10/13 
 Pct Recovery = 44%  Analysis Date = 11/08/13 
 Pct Recovery = 45%  Analysis Date = 11/08/13 
 Pct Recovery = 45%  Analysis Date = 11/07/13 
 Pct Recovery = 46%  Analysis Date = 11/07/13 
 Pct Recovery = 46%  Analysis Date = 11/05/13 
 Pct Recovery = 46%  Analysis Date = 11/05/13 
 Pct Recovery = 46%  Analysis Date = 11/03/13 
 Pct Recovery = 47%  Analysis Date = 11/03/13 
 Pct Recovery = 47%  Analysis Date = 11/01/13 
 Pct Recovery = 47%  Analysis Date = 11/01/13 
 Pct Recovery = 47%  Analysis Date = 10/31/13 
 Pct Recovery = 48%  Analysis Date = 10/31/13 
 Pct Recovery = 48%  Analysis Date = 10/29/13 
 Pct Recovery = 49%  Analysis Date = 10/29/13 
 Pct Recovery = 49%  Analysis Date = 10/27/13 
 Pct Recovery = 49%  Analysis Date = 10/27/13 
 Pct Recovery = 49%  Analysis Date = 10/26/13 
 Pct Recovery = 49%  Analysis Date = 10/26/13 
 Pct Recovery = 49%  Analysis Date = 10/24/13 
 Pct Recovery = 49%  Analysis Date = 10/24/13 
 Pct Recovery = 49%  Analysis Date = 10/22/13 
 Pct Recovery = 49%  Analysis Date = 10/22/13 
 Pct Recovery = 49%  Analysis Date = 10/20/13 
 Pct Recovery = 49%  Analysis Date = 10/20/13 
 Pct Recovery = 49%  Analysis Date = 10/19/13 
 Pct Recovery = 49%  Analysis Date = 10/19/13 
 Pct Recovery = 49%  Analysis Date = 10/17/13 
 Pct Recovery = 48%  Analysis Date = 10/17/13 
 Pct Recovery = 48%  Analysis Date = 10/15/13 
 Pct Recovery = 48%  Analysis Date = 10/15/13 
 Pct Recovery = 48%  Analysis Date = 10/14/13 
 Pct Recovery = 48%  Analysis Date = 10/14/13 
 Pct Recovery = 48%  Analysis Date = 10/12/13 
 Pct Recovery = 48%  Analysis Date = 10/12/13 
 Pct Recovery = 48%  Analysis Date = 10/10/13 
 Pct Recovery = 48%  Analysis Date = 10/10/13 
 Pct Recovery = 48%  Analysis Date = 10/09/13 
 Pct Recovery = 48%  Analysis Date = 10/09/13 
 Pct Recovery = 48%  Analysis Date = 10/07/13 
 Pct Recovery = 48%  Analysis Date = 10/07/13 
 Pct Recovery = 48%  Analysis Date = 10/05/13 
 Pct Recovery = 48%  Analysis Date = 10/05/13 
 Pct Recovery = 48%  Analysis Date = 10/03/13 
 Pct Recovery = 48%  Analysis Date = 10/03/13 
 Pct Recovery = 48%  Analysis Date = 10/02/13 
 Pct Recovery = 48%  Analysis Date = 10/02/13 
 Pct Recovery = 48%  Analysis Date = 09/30/13 
 Pct Recovery = 48%  Analysis Date = 09/30/13 
 Pct Recovery = 48%  Analysis Date = 09/28/13 
 Pct Recovery = 48%  Analysis Date = 09/28/13 
 Pct Recovery = 48%  Analysis Date = 09/27/13 
 Pct Recovery = 48%  Analysis Date = 09/27/13 
 Pct Recovery = 48%  Analysis Date = 09/25/13 
 Pct Recovery = 48%  Analysis Date = 09/25/13 
 Pct Recovery = 48%  Analysis Date = 09/23/13 
 Pct Recovery = 48%  Analysis Date = 09/23/13 
 Pct Recovery = 48%  Analysis Date = 09/21/13 
 Pct Recovery = 48%  Analysis Date = 09/21/13 
 Pct Recovery = 48%  Analysis Date = 09/20/13 
 Pct Recovery = 48%  Analysis Date = 09/20/13 
 Pct Recovery = 48%  Analysis Date = 09/18/13 
 Pct Recovery = 48%  Analysis Date = 09/18/13 
 Pct Recovery = 48%  Analysis Date = 09/16/13 
 Pct Recovery = 48%  Analysis Date = 09/16/13 
 Pct Recovery = 48%  Analysis Date = 09/15/13 
 Pct Recovery = 48%  Analysis Date = 09/15/13 
 Pct Recovery = 48%  Analysis Date = 09/13/13 
 Pct Recovery = 48%  Analysis Date = 09/13/13 
 Pct Recovery = 48%  Analysis Date = 09/11/13 
 Pct Recovery = 48%  Analysis Date = 09/11/13 
 Pct Recovery = 48%  Analysis Date = 09/09/13 
 Pct Recovery = 48%  Analysis Date = 09/09/13 
 Pct Recovery = 48%  Analysis Date = 09/08/13 
 Pct Recovery = 48%  Analysis Date = 09/08/13 
 Pct Recovery = 48%  Analysis Date = 09/06/13 
 Pct Recovery = 48%  Analysis Date = 09/06/13 
 Pct Recovery = 48%  Analysis Date = 09/04/13 
 Pct Recovery = 47%  Analysis Date = 09/04/13 
 Pct Recovery = 47%  Analysis Date = 09/03/13 
 Pct Recovery = 47%  Analysis Date = 09/03/13 
 Pct Recovery = 47%  Analysis Date = 09/01/13 
 Pct Recovery = 47%  Analysis Date = 09/01/13 
 Pct Recovery = 47%  Analysis Date = 08/30/13 
 Pct Recovery = 47%  Analysis Date = 08/30/13 
 Pct Recovery = 47%  Analysis Date = 08/28/13 
 Pct Recovery = 47%  Analysis Date = 08/28/13 
 Pct Recovery = 47%  Analysis Date = 08/27/13 
 Pct Recovery = 47%  Analysis Date = 08/27/13 
 Pct Recovery = 47%  Analysis Date = 08/25/13 
 Pct Recovery = 47%  Analysis Date = 08/25/13 
 Pct Recovery = 47%  Analysis Date = 08/23/13 
 Pct Recovery = 47%  Analysis Date = 08/23/13 
 Pct Recovery = 47%  Analysis Date = 08/22/13 
 Pct Recovery = 47%  Analysis Date = 08/22/13 
 Pct Recovery = 47%  Analysis Date = 08/20/13 
 Pct Recovery = 47%  Analysis Date = 08/20/13 
 Pct Recovery = 47%  Analysis Date = 08/18/13 
 Pct Recovery = 47%  Analysis Date = 08/18/13 
 Pct Recovery = 47%  Analysis Date = 08/17/13 
 Pct Recovery = 47%  Analysis Date = 08/17/13 
 Pct Recovery = 47%  Analysis Date = 08/15/13 
 Pct Recovery = 47%  Analysis Date = 08/15/13 
 Pct Recovery = 47%  Analysis Date = 08/13/13 
 Pct Recovery = 47%  Analysis Date = 08/13/13 
 Pct Recovery = 47%  Analysis Date = 08/11/13 
 Pct Recovery = 47%  Analysis Date = 08/11/13 
 Pct Recovery = 47%  Analysis Date = 08/10/13 
 Pct Recovery = 47%  Analysis Date = 08/10/13 
 Pct Recovery = 47%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/08/13 
 Pct Recovery = 47%  Analysis Date = 08/06/13 
 Pct Recovery = 47%  Analysis Date = 08/06/13 
 Pct Recovery = 47%  Analysis Date = 08/05/13 
 Pct Recovery = 47%  Analysis Date = 08/05/13 
 Pct Recovery = 47%  Analysis Date = 08/03/13 
 Pct Recovery = 47%  Analysis Date = 08/03/13 
 Pct Recovery = 47%  Analysis Date = 08/01/13 
 Pct Recovery = 47%  Analysis Date = 08/01/13 
 Pct Recovery = 47%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/29/13 
 Pct Recovery = 46%  Analysis Date = 07/29/13 
 Pct Recovery = 46%  Analysis Date = 07/27/13 
 Pct Recovery = 45%  Analysis Date = 07/27/13 
 Pct Recovery = 45%  Analysis Date = 07/25/13 
 Pct Recovery = 45%  Analysis Date = 07/25/13 
 Pct Recovery = 45%  Analysis Date = 07/24/13 
 Pct Recovery = 45%  Analysis Date = 07/24/13 
 Pct Recovery = 45%  Analysis Date = 07/22/13 
 Pct Recovery = 44%  Analysis Date = 07/22/13 
 Pct Recovery = 44%  Analysis Date = 07/20/13 
 Pct Recovery = 44%  Analysis Date = 07/20/13 
 Pct Recovery = 44%  Analysis Date = 07/18/13 
 Pct Recovery = 43%  Analysis Date = 07/18/13 
 Pct Recovery = 43%  Analysis Date = 07/17/13 
 Pct Recovery = 43%  Analysis Date = 07/17/13 
 Pct Recovery = 43%  Analysis Date = 07/15/13 
 Pct Recovery = 42%  Analysis Date = 07/15/13 
 Pct Recovery = 42%  Analysis Date = 07/13/13 
 Pct Recovery = 42%  Analysis Date = 07/13/13 
 Pct Recovery = 42%  Analysis Date = 07/12/13 
 Pct Recovery = 42%  Analysis Date = 07/12/13 
 Pct Recovery = 42%  Analysis Date = 07/10/13 
 Pct Recovery = 41%  Analysis Date = 07/10/13 
 Pct Recovery = 41%  Analysis Date = 07/08/13 
 Pct Recovery = 41%  Analysis Date = 07/08/13 
 Pct Recovery = 41%  Analysis Date = 07/06/13 
 Pct Recovery = 40%  Analysis Date = 07/06/13 
 Pct Recovery = 40%  Analysis Date = 07/05/13 
 Pct Recovery = 40%  Analysis Date = 07/05/13 
 Pct Recovery = 40%  Analysis Date = 07/03/13 
 Pct Recovery = 40%  Analysis Date = 07/03/13 
 Pct Recovery = 40%  Analysis Date = 07/01/13 
 Pct Recovery = 39%  Analysis Date = 07/01/13 
 Pct Recovery = 39%  Analysis Date = 06/30/13 
 Pct Recovery = 39%  Analysis Date = 06/30/13 
 Pct Recovery = 39%  Analysis Date = 06/28/13 
 Pct Recovery = 38%  Analysis Date = 06/28/13 
 Pct Recovery = 38%  Analysis Date = 06/26/13 
 Pct Recovery = 38%  Analysis Date = 06/26/13 
 Pct Recovery = 38%  Analysis Date = 06/25/13 
 Pct Recovery = 37%  Analysis Date = 06/25/13 
 Pct Recovery = 37%  Analysis Date = 06/23/13 
 Pct Recovery = 37%  Analysis Date = 06/23/13 
 Pct Recovery = 37%  Analysis Date = 06/21/13 
 Pct Recovery = 37%  Analysis Date = 06/21/13 
 Pct Recovery = 37%  Analysis Date = 06/19/13 
 Pct Recovery = 36%  Analysis Date = 06/19/13 
 Pct Recovery = 36%  Analysis Date = 06/18/13 
 Pct Recovery = 36%  Analysis Date = 06/18/13 
 Pct Recovery = 36%  Analysis Date = 06/16/13 
 Pct Recovery = 35%  Analysis Date = 06/16/13 
 Pct Recovery = 35%  Analysis Date = 06/14/13 
 Pct Recovery = 35%  Analysis Date = 06/14/13 
 Pct Recovery = 35%  Analysis Date = 06/13/13 
 Pct Recovery = 35%  Analysis Date = 06/13/13 
 Pct Recovery = 35%  Analysis Date = 06/11/13 
 Pct Recovery = 34%  Analysis Date = 06/11/13 
 Pct Recovery = 34%  Analysis Date = 06/09/13 
 Pct Recovery = 34%  Analysis Date = 06/09/13 
 Pct Recovery = 34%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/07/13 
 Pct Recovery = 33%  Analysis Date = 06/06/13 
 Pct Recovery = 33%  Analysis Date = 06/06/13 
 Pct Recovery = 33%  Analysis Date = 06/04/13 
 Pct Recovery = 32%  Analysis Date = 06/04/13 
 Pct Recovery = 32%  Analysis Date = 06/02/13 
 Pct Recovery = 32%  Analysis Date = 06/02/13 
 Pct Recovery = 32%  Analysis Date = 06/01/13 
 Pct Recovery = 32%  Analysis Date = 06/01/13 
 Pct Recovery = 32%  Analysis Date = 05/30/13 
 Pct Recovery = 31%  Analysis Date = 05/30/13 
 Pct Recovery = 31%  Analysis Date = 05/28/13 
 Pct Recovery = 31%  Analysis Date = 05/28/13 
 Pct Recovery = 31%  Analysis Date = 05/26/13 
 Pct Recovery = 30%  Analysis Date = 05/26/13 
 Pct Recovery = 30%  Analysis Date = 05/25/13 
 Pct Recovery = 30%  Analysis Date = 05/25/13 
 Pct Recovery = 30%  Analysis Date = 05/23/13 
 Pct Recovery = 30%  Analysis Date = 05/23/13 
 Pct Recovery = 30%  Analysis Date = 05/21/13 
 Pct Recovery = 29%  Analysis Date = 05/21/13 
 Pct Recovery = 29%  Analysis Date = 05/20/13 
 Pct Recovery = 29%  Analysis Date = 05/20/13 
 Pct Recovery = 29%  Analysis Date = 05/18/13 
 Pct Recovery = 28%  Analysis Date = 05/18/13 
 Pct Recovery = 28%  Analysis Date = 05/16/13 
 Pct Recovery = 28%  Analysis Date = 05/16/13 
 Pct Recovery = 28%  Analysis Date = 05/14/13 
 Pct Recovery = 28%  Analysis Date = 05/14/13 
 Pct Recovery = 28%  Analysis Date = 05/13/13 
 Pct Recovery = 27%  Analysis Date = 05/13/13 
 Pct Recovery = 27%  Analysis Date = 05/11/13 
 Pct Recovery = 27%  Analysis Date = 05/11/13 
 Pct Recovery = 27%  Analysis Date = 05/09/13 
 Pct Recovery = 26%  Analysis Date = 05/09/13 
 Pct Recovery = 26%  Analysis Date = 05/08/13 
 Pct Recovery = 26%  Analysis Date = 05/08/13 
 Pct Recovery = 26%  Analysis Date = 05/06/13 
 Pct Recovery = 25%  Analysis Date = 05/06/13 
 Pct Recovery = 25%  Analysis Date = 05/04/13 
 Pct Recovery = 25%  Analysis Date = 05/04/13 
 Pct Recovery = 25%  Analysis Date = 05/03/13 
 Pct Recovery = 25%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
RALOXIFENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 9 36% 17% 30% 17%
Total 9 36% 17% 30% 17%

Sample Statistics
RALOXIFENE

Characteristic N % % Basis
Plotted 9 64% Spiked
Estimated Values 9 64% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 5 36% 5 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
RANITIDINE
METHOD: LC9017 , TESTIDCODE: 67452LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 101%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 120%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 92%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 115%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 32%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 8%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 16%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 63%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 81%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 46%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 30%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 51%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 20%  Analysis Date = 04/09/14 
 Pct Recovery = 21%  Analysis Date = 04/07/14 
 Pct Recovery = 21%  Analysis Date = 04/07/14 
 Pct Recovery = 21%  Analysis Date = 04/05/14 
 Pct Recovery = 21%  Analysis Date = 04/05/14 
 Pct Recovery = 21%  Analysis Date = 04/02/14 
 Pct Recovery = 21%  Analysis Date = 04/02/14 
 Pct Recovery = 21%  Analysis Date = 03/31/14 
 Pct Recovery = 21%  Analysis Date = 03/31/14 
 Pct Recovery = 21%  Analysis Date = 03/28/14 
 Pct Recovery = 22%  Analysis Date = 03/28/14 
 Pct Recovery = 22%  Analysis Date = 03/26/14 
 Pct Recovery = 22%  Analysis Date = 03/26/14 
 Pct Recovery = 22%  Analysis Date = 03/24/14 
 Pct Recovery = 22%  Analysis Date = 03/24/14 
 Pct Recovery = 22%  Analysis Date = 03/21/14 
 Pct Recovery = 22%  Analysis Date = 03/21/14 
 Pct Recovery = 22%  Analysis Date = 03/19/14 
 Pct Recovery = 23%  Analysis Date = 03/19/14 
 Pct Recovery = 23%  Analysis Date = 03/16/14 
 Pct Recovery = 23%  Analysis Date = 03/16/14 
 Pct Recovery = 23%  Analysis Date = 03/14/14 
 Pct Recovery = 23%  Analysis Date = 03/14/14 
 Pct Recovery = 23%  Analysis Date = 03/12/14 
 Pct Recovery = 23%  Analysis Date = 03/12/14 
 Pct Recovery = 23%  Analysis Date = 03/09/14 
 Pct Recovery = 24%  Analysis Date = 03/09/14 
 Pct Recovery = 24%  Analysis Date = 03/07/14 
 Pct Recovery = 24%  Analysis Date = 03/07/14 
 Pct Recovery = 24%  Analysis Date = 03/04/14 
 Pct Recovery = 24%  Analysis Date = 03/04/14 
 Pct Recovery = 24%  Analysis Date = 03/02/14 
 Pct Recovery = 24%  Analysis Date = 03/02/14 
 Pct Recovery = 24%  Analysis Date = 02/28/14 
 Pct Recovery = 24%  Analysis Date = 02/28/14 
 Pct Recovery = 24%  Analysis Date = 02/25/14 
 Pct Recovery = 25%  Analysis Date = 02/25/14 
 Pct Recovery = 25%  Analysis Date = 02/23/14 
 Pct Recovery = 25%  Analysis Date = 02/23/14 
 Pct Recovery = 25%  Analysis Date = 02/20/14 
 Pct Recovery = 25%  Analysis Date = 02/20/14 
 Pct Recovery = 25%  Analysis Date = 02/18/14 
 Pct Recovery = 25%  Analysis Date = 02/18/14 
 Pct Recovery = 25%  Analysis Date = 02/15/14 
 Pct Recovery = 26%  Analysis Date = 02/15/14 
 Pct Recovery = 26%  Analysis Date = 02/13/14 
 Pct Recovery = 26%  Analysis Date = 02/13/14 
 Pct Recovery = 26%  Analysis Date = 02/11/14 
 Pct Recovery = 26%  Analysis Date = 02/11/14 
 Pct Recovery = 26%  Analysis Date = 02/08/14 
 Pct Recovery = 26%  Analysis Date = 02/08/14 
 Pct Recovery = 26%  Analysis Date = 02/06/14 
 Pct Recovery = 27%  Analysis Date = 02/06/14 
 Pct Recovery = 27%  Analysis Date = 02/03/14 
 Pct Recovery = 27%  Analysis Date = 02/03/14 
 Pct Recovery = 27%  Analysis Date = 02/01/14 
 Pct Recovery = 27%  Analysis Date = 02/01/14 
 Pct Recovery = 27%  Analysis Date = 01/30/14 
 Pct Recovery = 27%  Analysis Date = 01/30/14 
 Pct Recovery = 27%  Analysis Date = 01/27/14 
 Pct Recovery = 28%  Analysis Date = 01/27/14 
 Pct Recovery = 28%  Analysis Date = 01/25/14 
 Pct Recovery = 28%  Analysis Date = 01/25/14 
 Pct Recovery = 28%  Analysis Date = 01/22/14 
 Pct Recovery = 28%  Analysis Date = 01/22/14 
 Pct Recovery = 28%  Analysis Date = 01/20/14 
 Pct Recovery = 28%  Analysis Date = 01/20/14 
 Pct Recovery = 28%  Analysis Date = 01/18/14 
 Pct Recovery = 28%  Analysis Date = 01/18/14 
 Pct Recovery = 28%  Analysis Date = 01/15/14 
 Pct Recovery = 29%  Analysis Date = 01/15/14 
 Pct Recovery = 29%  Analysis Date = 01/13/14 
 Pct Recovery = 29%  Analysis Date = 01/13/14 
 Pct Recovery = 29%  Analysis Date = 01/10/14 
 Pct Recovery = 29%  Analysis Date = 01/10/14 
 Pct Recovery = 29%  Analysis Date = 01/08/14 
 Pct Recovery = 30%  Analysis Date = 01/08/14 
 Pct Recovery = 30%  Analysis Date = 01/06/14 
 Pct Recovery = 30%  Analysis Date = 01/06/14 
 Pct Recovery = 30%  Analysis Date = 01/03/14 
 Pct Recovery = 30%  Analysis Date = 01/03/14 
 Pct Recovery = 30%  Analysis Date = 01/01/14 
 Pct Recovery = 30%  Analysis Date = 01/01/14 
 Pct Recovery = 30%  Analysis Date = 12/29/13 
 Pct Recovery = 31%  Analysis Date = 12/29/13 
 Pct Recovery = 31%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/27/13 
 Pct Recovery = 31%  Analysis Date = 12/24/13 
 Pct Recovery = 31%  Analysis Date = 12/24/13 
 Pct Recovery = 31%  Analysis Date = 12/22/13 
 Pct Recovery = 32%  Analysis Date = 12/22/13 
 Pct Recovery = 32%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/20/13 
 Pct Recovery = 32%  Analysis Date = 12/17/13 
 Pct Recovery = 32%  Analysis Date = 12/17/13 
 Pct Recovery = 32%  Analysis Date = 12/15/13 
 Pct Recovery = 32%  Analysis Date = 12/15/13 
 Pct Recovery = 32%  Analysis Date = 12/12/13 
 Pct Recovery = 33%  Analysis Date = 12/12/13 
 Pct Recovery = 33%  Analysis Date = 12/10/13 
 Pct Recovery = 33%  Analysis Date = 12/10/13 
 Pct Recovery = 33%  Analysis Date = 12/08/13 
 Pct Recovery = 33%  Analysis Date = 12/08/13 
 Pct Recovery = 33%  Analysis Date = 12/05/13 
 Pct Recovery = 33%  Analysis Date = 12/05/13 
 Pct Recovery = 33%  Analysis Date = 12/03/13 
 Pct Recovery = 34%  Analysis Date = 12/03/13 
 Pct Recovery = 34%  Analysis Date = 11/30/13 
 Pct Recovery = 34%  Analysis Date = 11/30/13 
 Pct Recovery = 34%  Analysis Date = 11/28/13 
 Pct Recovery = 34%  Analysis Date = 11/28/13 
 Pct Recovery = 34%  Analysis Date = 11/26/13 
 Pct Recovery = 35%  Analysis Date = 11/26/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/23/13 
 Pct Recovery = 35%  Analysis Date = 11/21/13 
 Pct Recovery = 35%  Analysis Date = 11/21/13 
 Pct Recovery = 35%  Analysis Date = 11/18/13 
 Pct Recovery = 35%  Analysis Date = 11/18/13 
 Pct Recovery = 35%  Analysis Date = 11/16/13 
 Pct Recovery = 36%  Analysis Date = 11/16/13 
 Pct Recovery = 36%  Analysis Date = 11/13/13 
 Pct Recovery = 36%  Analysis Date = 11/13/13 
 Pct Recovery = 36%  Analysis Date = 11/11/13 
 Pct Recovery = 36%  Analysis Date = 11/11/13 
 Pct Recovery = 36%  Analysis Date = 11/09/13 
 Pct Recovery = 37%  Analysis Date = 11/09/13 
 Pct Recovery = 37%  Analysis Date = 11/06/13 
 Pct Recovery = 37%  Analysis Date = 11/06/13 
 Pct Recovery = 37%  Analysis Date = 11/04/13 
 Pct Recovery = 37%  Analysis Date = 11/04/13 
 Pct Recovery = 37%  Analysis Date = 11/01/13 
 Pct Recovery = 37%  Analysis Date = 11/01/13 
 Pct Recovery = 37%  Analysis Date = 10/30/13 
 Pct Recovery = 38%  Analysis Date = 10/30/13 
 Pct Recovery = 38%  Analysis Date = 10/28/13 
 Pct Recovery = 38%  Analysis Date = 10/28/13 
 Pct Recovery = 38%  Analysis Date = 10/25/13 
 Pct Recovery = 39%  Analysis Date = 10/25/13 
 Pct Recovery = 39%  Analysis Date = 10/23/13 
 Pct Recovery = 39%  Analysis Date = 10/23/13 
 Pct Recovery = 39%  Analysis Date = 10/20/13 
 Pct Recovery = 39%  Analysis Date = 10/20/13 
 Pct Recovery = 39%  Analysis Date = 10/18/13 
 Pct Recovery = 40%  Analysis Date = 10/18/13 
 Pct Recovery = 40%  Analysis Date = 10/16/13 
 Pct Recovery = 40%  Analysis Date = 10/16/13 
 Pct Recovery = 40%  Analysis Date = 10/13/13 
 Pct Recovery = 41%  Analysis Date = 10/13/13 
 Pct Recovery = 41%  Analysis Date = 10/11/13 
 Pct Recovery = 41%  Analysis Date = 10/11/13 
 Pct Recovery = 41%  Analysis Date = 10/08/13 
 Pct Recovery = 42%  Analysis Date = 10/08/13 
 Pct Recovery = 42%  Analysis Date = 10/06/13 
 Pct Recovery = 42%  Analysis Date = 10/06/13 
 Pct Recovery = 42%  Analysis Date = 10/04/13 
 Pct Recovery = 43%  Analysis Date = 10/04/13 
 Pct Recovery = 43%  Analysis Date = 10/01/13 
 Pct Recovery = 43%  Analysis Date = 10/01/13 
 Pct Recovery = 43%  Analysis Date = 09/29/13 
 Pct Recovery = 44%  Analysis Date = 09/29/13 
 Pct Recovery = 44%  Analysis Date = 09/26/13 
 Pct Recovery = 44%  Analysis Date = 09/26/13 
 Pct Recovery = 44%  Analysis Date = 09/24/13 
 Pct Recovery = 45%  Analysis Date = 09/24/13 
 Pct Recovery = 45%  Analysis Date = 09/21/13 
 Pct Recovery = 45%  Analysis Date = 09/21/13 
 Pct Recovery = 45%  Analysis Date = 09/19/13 
 Pct Recovery = 46%  Analysis Date = 09/19/13 
 Pct Recovery = 46%  Analysis Date = 09/17/13 
 Pct Recovery = 46%  Analysis Date = 09/17/13 
 Pct Recovery = 46%  Analysis Date = 09/14/13 
 Pct Recovery = 47%  Analysis Date = 09/14/13 
 Pct Recovery = 47%  Analysis Date = 09/12/13 
 Pct Recovery = 47%  Analysis Date = 09/12/13 
 Pct Recovery = 47%  Analysis Date = 09/09/13 
 Pct Recovery = 48%  Analysis Date = 09/09/13 
 Pct Recovery = 48%  Analysis Date = 09/07/13 
 Pct Recovery = 48%  Analysis Date = 09/07/13 
 Pct Recovery = 48%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/05/13 
 Pct Recovery = 49%  Analysis Date = 09/02/13 
 Pct Recovery = 49%  Analysis Date = 09/02/13 
 Pct Recovery = 49%  Analysis Date = 08/31/13 
 Pct Recovery = 50%  Analysis Date = 08/31/13 
 Pct Recovery = 50%  Analysis Date = 08/28/13 
 Pct Recovery = 50%  Analysis Date = 08/28/13 
 Pct Recovery = 50%  Analysis Date = 08/26/13 
 Pct Recovery = 51%  Analysis Date = 08/26/13 
 Pct Recovery = 51%  Analysis Date = 08/24/13 
 Pct Recovery = 51%  Analysis Date = 08/24/13 
 Pct Recovery = 51%  Analysis Date = 08/21/13 
 Pct Recovery = 52%  Analysis Date = 08/21/13 
 Pct Recovery = 52%  Analysis Date = 08/19/13 
 Pct Recovery = 52%  Analysis Date = 08/19/13 
 Pct Recovery = 52%  Analysis Date = 08/16/13 
 Pct Recovery = 53%  Analysis Date = 08/16/13 
 Pct Recovery = 53%  Analysis Date = 08/14/13 
 Pct Recovery = 53%  Analysis Date = 08/14/13 
 Pct Recovery = 53%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/11/13 
 Pct Recovery = 54%  Analysis Date = 08/09/13 
 Pct Recovery = 55%  Analysis Date = 08/09/13 
 Pct Recovery = 55%  Analysis Date = 08/07/13 
 Pct Recovery = 56%  Analysis Date = 08/07/13 
 Pct Recovery = 56%  Analysis Date = 08/04/13 
 Pct Recovery = 56%  Analysis Date = 08/04/13 
 Pct Recovery = 56%  Analysis Date = 08/02/13 
 Pct Recovery = 57%  Analysis Date = 08/02/13 
 Pct Recovery = 57%  Analysis Date = 07/30/13 
 Pct Recovery = 58%  Analysis Date = 07/30/13 
 Pct Recovery = 58%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/28/13 
 Pct Recovery = 59%  Analysis Date = 07/26/13 
 Pct Recovery = 59%  Analysis Date = 07/26/13 
 Pct Recovery = 59%  Analysis Date = 07/23/13 
 Pct Recovery = 60%  Analysis Date = 07/23/13 
 Pct Recovery = 60%  Analysis Date = 07/21/13 
 Pct Recovery = 61%  Analysis Date = 07/21/13 
 Pct Recovery = 61%  Analysis Date = 07/18/13 
 Pct Recovery = 62%  Analysis Date = 07/18/13 
 Pct Recovery = 62%  Analysis Date = 07/16/13 
 Pct Recovery = 62%  Analysis Date = 07/16/13 
 Pct Recovery = 62%  Analysis Date = 07/14/13 
 Pct Recovery = 63%  Analysis Date = 07/14/13 
 Pct Recovery = 63%  Analysis Date = 07/11/13 
 Pct Recovery = 64%  Analysis Date = 07/11/13 
 Pct Recovery = 64%  Analysis Date = 07/09/13 
 Pct Recovery = 65%  Analysis Date = 07/09/13 
 Pct Recovery = 65%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 07/02/13 
 Pct Recovery = 67%  Analysis Date = 06/29/13 
 Pct Recovery = 68%  Analysis Date = 06/29/13 
 Pct Recovery = 68%  Analysis Date = 06/27/13 
 Pct Recovery = 69%  Analysis Date = 06/27/13 
 Pct Recovery = 69%  Analysis Date = 06/24/13 
 Pct Recovery = 69%  Analysis Date = 06/24/13 
 Pct Recovery = 69%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/22/13 
 Pct Recovery = 70%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/19/13 
 Pct Recovery = 71%  Analysis Date = 06/17/13 
 Pct Recovery = 72%  Analysis Date = 06/17/13 
 Pct Recovery = 72%  Analysis Date = 06/15/13 
 Pct Recovery = 72%  Analysis Date = 06/15/13 
 Pct Recovery = 72%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/12/13 
 Pct Recovery = 73%  Analysis Date = 06/10/13 
 Pct Recovery = 74%  Analysis Date = 06/10/13 
 Pct Recovery = 74%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/07/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/05/13 
 Pct Recovery = 75%  Analysis Date = 06/03/13 
 Pct Recovery = 76%  Analysis Date = 06/03/13 
 Pct Recovery = 76%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 78%  Analysis Date = 05/29/13 
 Pct Recovery = 78%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 80%  Analysis Date = 05/22/13 
 Pct Recovery = 80%  Analysis Date = 05/19/13 
 Pct Recovery = 81%  Analysis Date = 05/19/13 
 Pct Recovery = 81%  Analysis Date = 05/17/13 
 Pct Recovery = 81%  Analysis Date = 05/17/13 
 Pct Recovery = 81%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/12/13 
 Pct Recovery = 83%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/10/13 
 Pct Recovery = 84%  Analysis Date = 05/07/13 
 Pct Recovery = 84%  Analysis Date = 05/07/13 
 Pct Recovery = 84%  Analysis Date = 05/05/13 
 Pct Recovery = 85%  Analysis Date = 05/05/13 
 Pct Recovery = 85%  Analysis Date = 05/02/13 
 Pct Recovery = 86%  Analysis Date = 05/02/13 
 Pct Recovery = 86%  Analysis Date = 04/30/13 
 Pct Recovery = 85%  Analysis Date = 04/30/13 
 Pct Recovery = 85%  Analysis Date = 04/27/13 
 Pct Recovery = 84%  Analysis Date = 04/27/13 
 Pct Recovery = 84%  Analysis Date = 04/25/13 
 Pct Recovery = 83%  Analysis Date = 04/25/13 
 Pct Recovery = 83%  Analysis Date = 04/23/13 
 Pct Recovery = 84%  Analysis Date = 04/23/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/20/13 
 Pct Recovery = 84%  Analysis Date = 04/18/13 
 Pct Recovery = 85%  Analysis Date = 04/18/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/15/13 
 Pct Recovery = 85%  Analysis Date = 04/13/13 
 Pct Recovery = 86%  Analysis Date = 04/13/13 
 Pct Recovery = 86%  Analysis Date = 04/11/13 
 Pct Recovery = 86%  Analysis Date = 04/11/13 
 Pct Recovery = 86%  Analysis Date = 04/08/13 
 Pct Recovery = 87%  Analysis Date = 04/08/13 
 Pct Recovery = 87%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/03/13 
 Pct Recovery = 88%  Analysis Date = 04/03/13 
 Pct Recovery = 88%  Analysis Date = 04/01/13 
 Pct Recovery = 88%  Analysis Date = 04/01/13 
 Pct Recovery = 88%  Analysis Date = 03/30/13 
 Pct Recovery = 89%  Analysis Date = 03/30/13 
 Pct Recovery = 89%  Analysis Date = 03/27/13 
 Pct Recovery = 89%  Analysis Date = 03/27/13 
 Pct Recovery = 89%  Analysis Date = 03/25/13 
 Pct Recovery = 89%  Analysis Date = 03/25/13 
 Pct Recovery = 89%  Analysis Date = 03/22/13 
 Pct Recovery = 89%  Analysis Date = 03/22/13 
 Pct Recovery = 89%  Analysis Date = 03/20/13 
 Pct Recovery = 89%  Analysis Date = 03/20/13 
 Pct Recovery = 89%  Analysis Date = 03/17/13 
 Pct Recovery = 89%  Analysis Date = 03/17/13 
 Pct Recovery = 89%  Analysis Date = 03/15/13 
 Pct Recovery = 89%  Analysis Date = 03/15/13 
 Pct Recovery = 89%  Analysis Date = 03/13/13 
 Pct Recovery = 88%  Analysis Date = 03/13/13 
 Pct Recovery = 88%  Analysis Date = 03/10/13 
 Pct Recovery = 88%  Analysis Date = 03/10/13 
 Pct Recovery = 88%  Analysis Date = 03/08/13 
 Pct Recovery = 88%  Analysis Date = 03/08/13 
 Pct Recovery = 88%  Analysis Date = 03/05/13 
 Pct Recovery = 88%  Analysis Date = 03/05/13 
 Pct Recovery = 88%  Analysis Date = 03/03/13 
 Pct Recovery = 88%  Analysis Date = 03/03/13 
 Pct Recovery = 88%  Analysis Date = 03/01/13 
 Pct Recovery = 88%  Analysis Date = 03/01/13 
 Pct Recovery = 88%  Analysis Date = 02/26/13 
 Pct Recovery = 87%  Analysis Date = 02/26/13 
 Pct Recovery = 87%  Analysis Date = 02/24/13 
 Pct Recovery = 87%  Analysis Date = 02/24/13 
 Pct Recovery = 87%  Analysis Date = 02/21/13 
 Pct Recovery = 87%  Analysis Date = 02/21/13 
 Pct Recovery = 87%  Analysis Date = 02/19/13 
 Pct Recovery = 87%  Analysis Date = 02/19/13 
 Pct Recovery = 87%  Analysis Date = 02/17/13 
 Pct Recovery = 87%  Analysis Date = 02/17/13 
 Pct Recovery = 87%  Analysis Date = 02/14/13 
 Pct Recovery = 87%  Analysis Date = 02/14/13 
 Pct Recovery = 87%  Analysis Date = 02/12/13 
 Pct Recovery = 86%  Analysis Date = 02/12/13 
 Pct Recovery = 86%  Analysis Date = 02/09/13 
 Pct Recovery = 86%  Analysis Date = 02/09/13 
 Pct Recovery = 86%  Analysis Date = 02/07/13 
 Pct Recovery = 86%  Analysis Date = 02/07/13 
 Pct Recovery = 86%  Analysis Date = 02/05/13 
 Pct Recovery = 86%  Analysis Date = 02/05/13 
 Pct Recovery = 86%  Analysis Date = 02/02/13 
 Pct Recovery = 86%  Analysis Date = 02/02/13 
 Pct Recovery = 86%  Analysis Date = 01/31/13 
 Pct Recovery = 85%  Analysis Date = 01/31/13 
 Pct Recovery = 85%  Analysis Date = 01/28/13 
 Pct Recovery = 85%  Analysis Date = 01/28/13 
 Pct Recovery = 85%  Analysis Date = 01/26/13 
 Pct Recovery = 85%  Analysis Date = 01/26/13 
 Pct Recovery = 85%  Analysis Date = 01/23/13 
 Pct Recovery = 85%  Analysis Date = 01/23/13 
 Pct Recovery = 85%  Analysis Date = 01/21/13 
 Pct Recovery = 83%  Analysis Date = 01/21/13 
 Pct Recovery = 83%  Analysis Date = 01/19/13 
 Pct Recovery = 81%  Analysis Date = 01/19/13 
 Pct Recovery = 81%  Analysis Date = 01/16/13 
 Pct Recovery = 80%  Analysis Date = 01/16/13 
 Pct Recovery = 80%  Analysis Date = 01/14/13 
 Pct Recovery = 78%  Analysis Date = 01/14/13 
 Pct Recovery = 78%  Analysis Date = 01/11/13 
 Pct Recovery = 76%  Analysis Date = 01/11/13 
 Pct Recovery = 76%  Analysis Date = 01/09/13 
 Pct Recovery = 74%  Analysis Date = 01/09/13 
 Pct Recovery = 74%  Analysis Date = 01/07/13 
 Pct Recovery = 73%  Analysis Date = 01/07/13 
 Pct Recovery = 73%  Analysis Date = 01/04/13 
 Pct Recovery = 71%  Analysis Date = 01/04/13 
 Pct Recovery = 71%  Analysis Date = 01/02/13 
 Pct Recovery = 69%  Analysis Date = 01/02/13 
 Pct Recovery = 69%  Analysis Date = 12/30/12 
 Pct Recovery = 67%  Analysis Date = 12/30/12 
 Pct Recovery = 67%  Analysis Date = 12/28/12 
 Pct Recovery = 66%  Analysis Date = 12/28/12 
 Pct Recovery = 66%  Analysis Date = 12/26/12 
 Pct Recovery = 64%  Analysis Date = 12/26/12 
 Pct Recovery = 64%  Analysis Date = 12/23/12 
 Pct Recovery = 62%  Analysis Date = 12/23/12 
 Pct Recovery = 62%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/18/12 
 Pct Recovery = 59%  Analysis Date = 12/16/12 
 Pct Recovery = 57%  Analysis Date = 12/16/12 
 Pct Recovery = 57%  Analysis Date = 12/14/12 
 Pct Recovery = 55%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
RANITIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 20% . 20% 0%
>= Reporting Level 13 64% 37% 63% 44%
Total 14 61% 37% 57% 45%

Sample Statistics
RANITIDINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 14 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
SERTRALINE
METHOD: LC9017 , TESTIDCODE: 67528LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 28%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 57%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 28%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 43%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 29%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 42%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 48%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 30%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 22%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 52%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 53%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 26%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 38%  Analysis Date = 04/09/14 
 Pct Recovery = 37%  Analysis Date = 04/07/14 
 Pct Recovery = 37%  Analysis Date = 04/07/14 
 Pct Recovery = 37%  Analysis Date = 04/05/14 
 Pct Recovery = 37%  Analysis Date = 04/05/14 
 Pct Recovery = 37%  Analysis Date = 04/02/14 
 Pct Recovery = 37%  Analysis Date = 04/02/14 
 Pct Recovery = 37%  Analysis Date = 03/31/14 
 Pct Recovery = 37%  Analysis Date = 03/31/14 
 Pct Recovery = 37%  Analysis Date = 03/28/14 
 Pct Recovery = 37%  Analysis Date = 03/28/14 
 Pct Recovery = 37%  Analysis Date = 03/26/14 
 Pct Recovery = 37%  Analysis Date = 03/26/14 
 Pct Recovery = 37%  Analysis Date = 03/24/14 
 Pct Recovery = 38%  Analysis Date = 03/24/14 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 Pct Recovery = 38%  Analysis Date = 03/21/14 
 Pct Recovery = 38%  Analysis Date = 03/19/14 
 Pct Recovery = 38%  Analysis Date = 03/19/14 
 Pct Recovery = 38%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/14/14 
 Pct Recovery = 38%  Analysis Date = 03/14/14 
 Pct Recovery = 38%  Analysis Date = 03/12/14 
 Pct Recovery = 38%  Analysis Date = 03/12/14 
 Pct Recovery = 38%  Analysis Date = 03/09/14 
 Pct Recovery = 38%  Analysis Date = 03/09/14 
 Pct Recovery = 38%  Analysis Date = 03/07/14 
 Pct Recovery = 38%  Analysis Date = 03/07/14 
 Pct Recovery = 38%  Analysis Date = 03/04/14 
 Pct Recovery = 38%  Analysis Date = 03/04/14 
 Pct Recovery = 38%  Analysis Date = 03/02/14 
 Pct Recovery = 38%  Analysis Date = 03/02/14 
 Pct Recovery = 38%  Analysis Date = 02/28/14 
 Pct Recovery = 38%  Analysis Date = 02/28/14 
 Pct Recovery = 38%  Analysis Date = 02/25/14 
 Pct Recovery = 38%  Analysis Date = 02/25/14 
 Pct Recovery = 38%  Analysis Date = 02/23/14 
 Pct Recovery = 38%  Analysis Date = 02/23/14 
 Pct Recovery = 38%  Analysis Date = 02/20/14 
 Pct Recovery = 38%  Analysis Date = 02/20/14 
 Pct Recovery = 38%  Analysis Date = 02/18/14 
 Pct Recovery = 38%  Analysis Date = 02/18/14 
 Pct Recovery = 38%  Analysis Date = 02/15/14 
 Pct Recovery = 38%  Analysis Date = 02/15/14 
 Pct Recovery = 38%  Analysis Date = 02/13/14 
 Pct Recovery = 38%  Analysis Date = 02/13/14 
 Pct Recovery = 38%  Analysis Date = 02/11/14 
 Pct Recovery = 38%  Analysis Date = 02/11/14 
 Pct Recovery = 38%  Analysis Date = 02/08/14 
 Pct Recovery = 38%  Analysis Date = 02/08/14 
 Pct Recovery = 38%  Analysis Date = 02/06/14 
 Pct Recovery = 38%  Analysis Date = 02/06/14 
 Pct Recovery = 38%  Analysis Date = 02/03/14 
 Pct Recovery = 38%  Analysis Date = 02/03/14 
 Pct Recovery = 38%  Analysis Date = 02/01/14 
 Pct Recovery = 38%  Analysis Date = 02/01/14 
 Pct Recovery = 38%  Analysis Date = 01/30/14 
 Pct Recovery = 38%  Analysis Date = 01/30/14 
 Pct Recovery = 38%  Analysis Date = 01/27/14 
 Pct Recovery = 38%  Analysis Date = 01/27/14 
 Pct Recovery = 38%  Analysis Date = 01/25/14 
 Pct Recovery = 38%  Analysis Date = 01/25/14 
 Pct Recovery = 38%  Analysis Date = 01/22/14 
 Pct Recovery = 38%  Analysis Date = 01/22/14 
 Pct Recovery = 38%  Analysis Date = 01/20/14 
 Pct Recovery = 39%  Analysis Date = 01/20/14 
 Pct Recovery = 39%  Analysis Date = 01/18/14 
 Pct Recovery = 39%  Analysis Date = 01/18/14 
 Pct Recovery = 39%  Analysis Date = 01/15/14 
 Pct Recovery = 39%  Analysis Date = 01/15/14 
 Pct Recovery = 39%  Analysis Date = 01/13/14 
 Pct Recovery = 39%  Analysis Date = 01/13/14 
 Pct Recovery = 39%  Analysis Date = 01/10/14 
 Pct Recovery = 39%  Analysis Date = 01/10/14 
 Pct Recovery = 39%  Analysis Date = 01/08/14 
 Pct Recovery = 39%  Analysis Date = 01/08/14 
 Pct Recovery = 39%  Analysis Date = 01/06/14 
 Pct Recovery = 39%  Analysis Date = 01/06/14 
 Pct Recovery = 39%  Analysis Date = 01/03/14 
 Pct Recovery = 39%  Analysis Date = 01/03/14 
 Pct Recovery = 39%  Analysis Date = 01/01/14 
 Pct Recovery = 38%  Analysis Date = 01/01/14 
 Pct Recovery = 38%  Analysis Date = 12/29/13 
 Pct Recovery = 38%  Analysis Date = 12/29/13 
 Pct Recovery = 38%  Analysis Date = 12/27/13 
 Pct Recovery = 38%  Analysis Date = 12/27/13 
 Pct Recovery = 38%  Analysis Date = 12/24/13 
 Pct Recovery = 38%  Analysis Date = 12/24/13 
 Pct Recovery = 38%  Analysis Date = 12/22/13 
 Pct Recovery = 38%  Analysis Date = 12/22/13 
 Pct Recovery = 38%  Analysis Date = 12/20/13 
 Pct Recovery = 38%  Analysis Date = 12/20/13 
 Pct Recovery = 38%  Analysis Date = 12/17/13 
 Pct Recovery = 38%  Analysis Date = 12/17/13 
 Pct Recovery = 38%  Analysis Date = 12/15/13 
 Pct Recovery = 38%  Analysis Date = 12/15/13 
 Pct Recovery = 38%  Analysis Date = 12/12/13 
 Pct Recovery = 38%  Analysis Date = 12/12/13 
 Pct Recovery = 38%  Analysis Date = 12/10/13 
 Pct Recovery = 38%  Analysis Date = 12/10/13 
 Pct Recovery = 38%  Analysis Date = 12/08/13 
 Pct Recovery = 38%  Analysis Date = 12/08/13 
 Pct Recovery = 38%  Analysis Date = 12/05/13 
 Pct Recovery = 38%  Analysis Date = 12/05/13 
 Pct Recovery = 38%  Analysis Date = 12/03/13 
 Pct Recovery = 38%  Analysis Date = 12/03/13 
 Pct Recovery = 38%  Analysis Date = 11/30/13 
 Pct Recovery = 39%  Analysis Date = 11/30/13 
 Pct Recovery = 39%  Analysis Date = 11/28/13 
 Pct Recovery = 39%  Analysis Date = 11/28/13 
 Pct Recovery = 39%  Analysis Date = 11/26/13 
 Pct Recovery = 39%  Analysis Date = 11/26/13 
 Pct Recovery = 39%  Analysis Date = 11/23/13 
 Pct Recovery = 39%  Analysis Date = 11/23/13 
 Pct Recovery = 39%  Analysis Date = 11/21/13 
 Pct Recovery = 39%  Analysis Date = 11/21/13 
 Pct Recovery = 39%  Analysis Date = 11/18/13 
 Pct Recovery = 40%  Analysis Date = 11/18/13 
 Pct Recovery = 40%  Analysis Date = 11/16/13 
 Pct Recovery = 40%  Analysis Date = 11/16/13 
 Pct Recovery = 40%  Analysis Date = 11/13/13 
 Pct Recovery = 40%  Analysis Date = 11/13/13 
 Pct Recovery = 40%  Analysis Date = 11/11/13 
 Pct Recovery = 40%  Analysis Date = 11/11/13 
 Pct Recovery = 40%  Analysis Date = 11/09/13 
 Pct Recovery = 41%  Analysis Date = 11/09/13 
 Pct Recovery = 41%  Analysis Date = 11/06/13 
 Pct Recovery = 41%  Analysis Date = 11/06/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/04/13 
 Pct Recovery = 41%  Analysis Date = 11/01/13 
 Pct Recovery = 42%  Analysis Date = 11/01/13 
 Pct Recovery = 42%  Analysis Date = 10/30/13 
 Pct Recovery = 42%  Analysis Date = 10/30/13 
 Pct Recovery = 42%  Analysis Date = 10/28/13 
 Pct Recovery = 42%  Analysis Date = 10/28/13 
 Pct Recovery = 42%  Analysis Date = 10/25/13 
 Pct Recovery = 42%  Analysis Date = 10/25/13 
 Pct Recovery = 42%  Analysis Date = 10/23/13 
 Pct Recovery = 42%  Analysis Date = 10/23/13 
 Pct Recovery = 42%  Analysis Date = 10/20/13 
 Pct Recovery = 42%  Analysis Date = 10/20/13 
 Pct Recovery = 42%  Analysis Date = 10/18/13 
 Pct Recovery = 42%  Analysis Date = 10/18/13 
 Pct Recovery = 42%  Analysis Date = 10/16/13 
 Pct Recovery = 43%  Analysis Date = 10/16/13 
 Pct Recovery = 43%  Analysis Date = 10/13/13 
 Pct Recovery = 43%  Analysis Date = 10/13/13 
 Pct Recovery = 43%  Analysis Date = 10/11/13 
 Pct Recovery = 43%  Analysis Date = 10/11/13 
 Pct Recovery = 43%  Analysis Date = 10/08/13 
 Pct Recovery = 43%  Analysis Date = 10/08/13 
 Pct Recovery = 43%  Analysis Date = 10/06/13 
 Pct Recovery = 43%  Analysis Date = 10/06/13 
 Pct Recovery = 43%  Analysis Date = 10/04/13 
 Pct Recovery = 43%  Analysis Date = 10/04/13 
 Pct Recovery = 43%  Analysis Date = 10/01/13 
 Pct Recovery = 43%  Analysis Date = 10/01/13 
 Pct Recovery = 43%  Analysis Date = 09/29/13 
 Pct Recovery = 43%  Analysis Date = 09/29/13 
 Pct Recovery = 43%  Analysis Date = 09/26/13 
 Pct Recovery = 43%  Analysis Date = 09/26/13 
 Pct Recovery = 43%  Analysis Date = 09/24/13 
 Pct Recovery = 44%  Analysis Date = 09/24/13 
 Pct Recovery = 44%  Analysis Date = 09/21/13 
 Pct Recovery = 44%  Analysis Date = 09/21/13 
 Pct Recovery = 44%  Analysis Date = 09/19/13 
 Pct Recovery = 44%  Analysis Date = 09/19/13 
 Pct Recovery = 44%  Analysis Date = 09/17/13 
 Pct Recovery = 44%  Analysis Date = 09/17/13 
 Pct Recovery = 44%  Analysis Date = 09/14/13 
 Pct Recovery = 44%  Analysis Date = 09/14/13 
 Pct Recovery = 44%  Analysis Date = 09/12/13 
 Pct Recovery = 44%  Analysis Date = 09/12/13 
 Pct Recovery = 44%  Analysis Date = 09/09/13 
 Pct Recovery = 44%  Analysis Date = 09/09/13 
 Pct Recovery = 44%  Analysis Date = 09/07/13 
 Pct Recovery = 44%  Analysis Date = 09/07/13 
 Pct Recovery = 44%  Analysis Date = 09/05/13 
 Pct Recovery = 44%  Analysis Date = 09/05/13 
 Pct Recovery = 44%  Analysis Date = 09/02/13 
 Pct Recovery = 45%  Analysis Date = 09/02/13 
 Pct Recovery = 45%  Analysis Date = 08/31/13 
 Pct Recovery = 45%  Analysis Date = 08/31/13 
 Pct Recovery = 45%  Analysis Date = 08/28/13 
 Pct Recovery = 45%  Analysis Date = 08/28/13 
 Pct Recovery = 45%  Analysis Date = 08/26/13 
 Pct Recovery = 45%  Analysis Date = 08/26/13 
 Pct Recovery = 45%  Analysis Date = 08/24/13 
 Pct Recovery = 45%  Analysis Date = 08/24/13 
 Pct Recovery = 45%  Analysis Date = 08/21/13 
 Pct Recovery = 45%  Analysis Date = 08/21/13 
 Pct Recovery = 45%  Analysis Date = 08/19/13 
 Pct Recovery = 45%  Analysis Date = 08/19/13 
 Pct Recovery = 45%  Analysis Date = 08/16/13 
 Pct Recovery = 45%  Analysis Date = 08/16/13 
 Pct Recovery = 45%  Analysis Date = 08/14/13 
 Pct Recovery = 45%  Analysis Date = 08/14/13 
 Pct Recovery = 45%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/11/13 
 Pct Recovery = 46%  Analysis Date = 08/09/13 
 Pct Recovery = 46%  Analysis Date = 08/09/13 
 Pct Recovery = 46%  Analysis Date = 08/07/13 
 Pct Recovery = 46%  Analysis Date = 08/07/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/04/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 08/02/13 
 Pct Recovery = 46%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/30/13 
 Pct Recovery = 46%  Analysis Date = 07/28/13 
 Pct Recovery = 46%  Analysis Date = 07/28/13 
 Pct Recovery = 46%  Analysis Date = 07/26/13 
 Pct Recovery = 46%  Analysis Date = 07/26/13 
 Pct Recovery = 46%  Analysis Date = 07/23/13 
 Pct Recovery = 46%  Analysis Date = 07/23/13 
 Pct Recovery = 46%  Analysis Date = 07/21/13 
 Pct Recovery = 46%  Analysis Date = 07/21/13 
 Pct Recovery = 46%  Analysis Date = 07/18/13 
 Pct Recovery = 46%  Analysis Date = 07/18/13 
 Pct Recovery = 46%  Analysis Date = 07/16/13 
 Pct Recovery = 46%  Analysis Date = 07/16/13 
 Pct Recovery = 46%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/14/13 
 Pct Recovery = 46%  Analysis Date = 07/11/13 
 Pct Recovery = 45%  Analysis Date = 07/11/13 
 Pct Recovery = 45%  Analysis Date = 07/09/13 
 Pct Recovery = 45%  Analysis Date = 07/09/13 
 Pct Recovery = 45%  Analysis Date = 07/06/13 
 Pct Recovery = 45%  Analysis Date = 07/06/13 
 Pct Recovery = 45%  Analysis Date = 07/04/13 
 Pct Recovery = 45%  Analysis Date = 07/04/13 
 Pct Recovery = 45%  Analysis Date = 07/02/13 
 Pct Recovery = 45%  Analysis Date = 07/02/13 
 Pct Recovery = 45%  Analysis Date = 06/29/13 
 Pct Recovery = 45%  Analysis Date = 06/29/13 
 Pct Recovery = 45%  Analysis Date = 06/27/13 
 Pct Recovery = 45%  Analysis Date = 06/27/13 
 Pct Recovery = 45%  Analysis Date = 06/24/13 
 Pct Recovery = 45%  Analysis Date = 06/24/13 
 Pct Recovery = 45%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/22/13 
 Pct Recovery = 45%  Analysis Date = 06/19/13 
 Pct Recovery = 45%  Analysis Date = 06/19/13 
 Pct Recovery = 45%  Analysis Date = 06/17/13 
 Pct Recovery = 45%  Analysis Date = 06/17/13 
 Pct Recovery = 45%  Analysis Date = 06/15/13 
 Pct Recovery = 45%  Analysis Date = 06/15/13 
 Pct Recovery = 45%  Analysis Date = 06/12/13 
 Pct Recovery = 45%  Analysis Date = 06/12/13 
 Pct Recovery = 45%  Analysis Date = 06/10/13 
 Pct Recovery = 45%  Analysis Date = 06/10/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/07/13 
 Pct Recovery = 45%  Analysis Date = 06/05/13 
 Pct Recovery = 44%  Analysis Date = 06/05/13 
 Pct Recovery = 44%  Analysis Date = 06/03/13 
 Pct Recovery = 44%  Analysis Date = 06/03/13 
 Pct Recovery = 44%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/31/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/29/13 
 Pct Recovery = 44%  Analysis Date = 05/26/13 
 Pct Recovery = 44%  Analysis Date = 05/26/13 
 Pct Recovery = 44%  Analysis Date = 05/24/13 
 Pct Recovery = 44%  Analysis Date = 05/24/13 
 Pct Recovery = 44%  Analysis Date = 05/22/13 
 Pct Recovery = 44%  Analysis Date = 05/22/13 
 Pct Recovery = 44%  Analysis Date = 05/19/13 
 Pct Recovery = 44%  Analysis Date = 05/19/13 
 Pct Recovery = 44%  Analysis Date = 05/17/13 
 Pct Recovery = 44%  Analysis Date = 05/17/13 
 Pct Recovery = 44%  Analysis Date = 05/14/13 
 Pct Recovery = 44%  Analysis Date = 05/14/13 
 Pct Recovery = 44%  Analysis Date = 05/12/13 
 Pct Recovery = 44%  Analysis Date = 05/12/13 
 Pct Recovery = 44%  Analysis Date = 05/10/13 
 Pct Recovery = 44%  Analysis Date = 05/10/13 
 Pct Recovery = 44%  Analysis Date = 05/07/13 
 Pct Recovery = 44%  Analysis Date = 05/07/13 
 Pct Recovery = 44%  Analysis Date = 05/05/13 
 Pct Recovery = 44%  Analysis Date = 05/05/13 
 Pct Recovery = 44%  Analysis Date = 05/02/13 
 Pct Recovery = 43%  Analysis Date = 05/02/13 
 Pct Recovery = 43%  Analysis Date = 04/30/13 
 Pct Recovery = 43%  Analysis Date = 04/30/13 
 Pct Recovery = 43%  Analysis Date = 04/27/13 
 Pct Recovery = 43%  Analysis Date = 04/27/13 
 Pct Recovery = 43%  Analysis Date = 04/25/13 
 Pct Recovery = 43%  Analysis Date = 04/25/13 
 Pct Recovery = 43%  Analysis Date = 04/23/13 
 Pct Recovery = 42%  Analysis Date = 04/23/13 
 Pct Recovery = 42%  Analysis Date = 04/20/13 
 Pct Recovery = 42%  Analysis Date = 04/20/13 
 Pct Recovery = 42%  Analysis Date = 04/18/13 
 Pct Recovery = 42%  Analysis Date = 04/18/13 
 Pct Recovery = 42%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/15/13 
 Pct Recovery = 41%  Analysis Date = 04/13/13 
 Pct Recovery = 41%  Analysis Date = 04/13/13 
 Pct Recovery = 41%  Analysis Date = 04/11/13 
 Pct Recovery = 41%  Analysis Date = 04/11/13 
 Pct Recovery = 41%  Analysis Date = 04/08/13 
 Pct Recovery = 41%  Analysis Date = 04/08/13 
 Pct Recovery = 41%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/06/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/03/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 04/01/13 
 Pct Recovery = 40%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/30/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/27/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/25/13 
 Pct Recovery = 39%  Analysis Date = 03/22/13 
 Pct Recovery = 38%  Analysis Date = 03/22/13 
 Pct Recovery = 38%  Analysis Date = 03/20/13 
 Pct Recovery = 38%  Analysis Date = 03/20/13 
 Pct Recovery = 38%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/15/13 
 Pct Recovery = 37%  Analysis Date = 03/15/13 
 Pct Recovery = 37%  Analysis Date = 03/13/13 
 Pct Recovery = 37%  Analysis Date = 03/13/13 
 Pct Recovery = 37%  Analysis Date = 03/10/13 
 Pct Recovery = 37%  Analysis Date = 03/10/13 
 Pct Recovery = 37%  Analysis Date = 03/08/13 
 Pct Recovery = 37%  Analysis Date = 03/08/13 
 Pct Recovery = 37%  Analysis Date = 03/05/13 
 Pct Recovery = 36%  Analysis Date = 03/05/13 
 Pct Recovery = 36%  Analysis Date = 03/03/13 
 Pct Recovery = 36%  Analysis Date = 03/03/13 
 Pct Recovery = 36%  Analysis Date = 03/01/13 
 Pct Recovery = 36%  Analysis Date = 03/01/13 
 Pct Recovery = 36%  Analysis Date = 02/26/13 
 Pct Recovery = 35%  Analysis Date = 02/26/13 
 Pct Recovery = 35%  Analysis Date = 02/24/13 
 Pct Recovery = 35%  Analysis Date = 02/24/13 
 Pct Recovery = 35%  Analysis Date = 02/21/13 
 Pct Recovery = 35%  Analysis Date = 02/21/13 
 Pct Recovery = 35%  Analysis Date = 02/19/13 
 Pct Recovery = 34%  Analysis Date = 02/19/13 
 Pct Recovery = 34%  Analysis Date = 02/17/13 
 Pct Recovery = 34%  Analysis Date = 02/17/13 
 Pct Recovery = 34%  Analysis Date = 02/14/13 
 Pct Recovery = 34%  Analysis Date = 02/14/13 
 Pct Recovery = 34%  Analysis Date = 02/12/13 
 Pct Recovery = 34%  Analysis Date = 02/12/13 
 Pct Recovery = 34%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/09/13 
 Pct Recovery = 33%  Analysis Date = 02/07/13 
 Pct Recovery = 33%  Analysis Date = 02/07/13 
 Pct Recovery = 33%  Analysis Date = 02/05/13 
 Pct Recovery = 33%  Analysis Date = 02/05/13 
 Pct Recovery = 33%  Analysis Date = 02/02/13 
 Pct Recovery = 32%  Analysis Date = 02/02/13 
 Pct Recovery = 32%  Analysis Date = 01/31/13 
 Pct Recovery = 32%  Analysis Date = 01/31/13 
 Pct Recovery = 32%  Analysis Date = 01/28/13 
 Pct Recovery = 32%  Analysis Date = 01/28/13 
 Pct Recovery = 32%  Analysis Date = 01/26/13 
 Pct Recovery = 31%  Analysis Date = 01/26/13 
 Pct Recovery = 31%  Analysis Date = 01/23/13 
 Pct Recovery = 31%  Analysis Date = 01/23/13 
 Pct Recovery = 31%  Analysis Date = 01/21/13 
 Pct Recovery = 31%  Analysis Date = 01/21/13 
 Pct Recovery = 31%  Analysis Date = 01/19/13 
 Pct Recovery = 30%  Analysis Date = 01/19/13 
 Pct Recovery = 30%  Analysis Date = 01/16/13 
 Pct Recovery = 30%  Analysis Date = 01/16/13 
 Pct Recovery = 30%  Analysis Date = 01/14/13 
 Pct Recovery = 30%  Analysis Date = 01/14/13 
 Pct Recovery = 30%  Analysis Date = 01/11/13 
 Pct Recovery = 30%  Analysis Date = 01/11/13 
 Pct Recovery = 30%  Analysis Date = 01/09/13 
 Pct Recovery = 29%  Analysis Date = 01/09/13 
 Pct Recovery = 29%  Analysis Date = 01/07/13 
 Pct Recovery = 29%  Analysis Date = 01/07/13 
 Pct Recovery = 29%  Analysis Date = 01/04/13 
 Pct Recovery = 29%  Analysis Date = 01/04/13 
 Pct Recovery = 29%  Analysis Date = 01/02/13 
 Pct Recovery = 28%  Analysis Date = 01/02/13 
 Pct Recovery = 28%  Analysis Date = 12/30/12 
 Pct Recovery = 28%  Analysis Date = 12/30/12 
 Pct Recovery = 28%  Analysis Date = 12/28/12 
 Pct Recovery = 28%  Analysis Date = 12/28/12 
 Pct Recovery = 28%  Analysis Date = 12/26/12 
 Pct Recovery = 27%  Analysis Date = 12/26/12 
 Pct Recovery = 27%  Analysis Date = 12/23/12 
 Pct Recovery = 27%  Analysis Date = 12/23/12 
 Pct Recovery = 27%  Analysis Date = 12/21/12 
 Pct Recovery = 27%  Analysis Date = 12/21/12 
 Pct Recovery = 27%  Analysis Date = 12/18/12 
 Pct Recovery = 26%  Analysis Date = 12/18/12 
 Pct Recovery = 26%  Analysis Date = 12/16/12 
 Pct Recovery = 26%  Analysis Date = 12/16/12 
 Pct Recovery = 26%  Analysis Date = 12/14/12 
 Pct Recovery = 26%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
SERTRALINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 38% . 38% 0%
>= Reporting Level 13 39% 13% 42% 18%
Total 14 39% 12% 40% 18%

Sample Statistics
SERTRALINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 14 100% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
SITAGLIPTIN
METHOD: LC9017 , TESTIDCODE: 67531LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 2%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 3%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 30%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 41%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 35%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 41%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 3%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 2%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 61%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 34%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 82%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 59%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 4%  Analysis Date = 04/09/14 
 Pct Recovery = 38%  Analysis Date = 04/07/14 
 Pct Recovery = 38%  Analysis Date = 04/07/14 
 Pct Recovery = 38%  Analysis Date = 04/05/14 
 Pct Recovery = 39%  Analysis Date = 04/05/14 
 Pct Recovery = 39%  Analysis Date = 04/03/14 
 Pct Recovery = 39%  Analysis Date = 04/03/14 
 Pct Recovery = 39%  Analysis Date = 04/01/14 
 Pct Recovery = 39%  Analysis Date = 04/01/14 
 Pct Recovery = 39%  Analysis Date = 03/30/14 
 Pct Recovery = 39%  Analysis Date = 03/30/14 
 Pct Recovery = 39%  Analysis Date = 03/28/14 
 Pct Recovery = 39%  Analysis Date = 03/28/14 
 Pct Recovery = 39%  Analysis Date = 03/26/14 
 Pct Recovery = 39%  Analysis Date = 03/26/14 
 Pct Recovery = 39%  Analysis Date = 03/24/14 
 Pct Recovery = 40%  Analysis Date = 03/24/14 
 Pct Recovery = 40%  Analysis Date = 03/22/14 
 Pct Recovery = 40%  Analysis Date = 03/22/14 
 Pct Recovery = 40%  Analysis Date = 03/20/14 
 Pct Recovery = 40%  Analysis Date = 03/20/14 
 Pct Recovery = 40%  Analysis Date = 03/18/14 
 Pct Recovery = 40%  Analysis Date = 03/18/14 
 Pct Recovery = 40%  Analysis Date = 03/16/14 
 Pct Recovery = 40%  Analysis Date = 03/16/14 
 Pct Recovery = 40%  Analysis Date = 03/14/14 
 Pct Recovery = 40%  Analysis Date = 03/14/14 
 Pct Recovery = 40%  Analysis Date = 03/12/14 
 Pct Recovery = 41%  Analysis Date = 03/12/14 
 Pct Recovery = 41%  Analysis Date = 03/10/14 
 Pct Recovery = 41%  Analysis Date = 03/10/14 
 Pct Recovery = 41%  Analysis Date = 03/08/14 
 Pct Recovery = 41%  Analysis Date = 03/08/14 
 Pct Recovery = 41%  Analysis Date = 03/06/14 
 Pct Recovery = 41%  Analysis Date = 03/06/14 
 Pct Recovery = 41%  Analysis Date = 03/04/14 
 Pct Recovery = 41%  Analysis Date = 03/04/14 
 Pct Recovery = 41%  Analysis Date = 03/02/14 
 Pct Recovery = 41%  Analysis Date = 03/02/14 
 Pct Recovery = 41%  Analysis Date = 02/28/14 
 Pct Recovery = 42%  Analysis Date = 02/28/14 
 Pct Recovery = 42%  Analysis Date = 02/26/14 
 Pct Recovery = 42%  Analysis Date = 02/26/14 
 Pct Recovery = 42%  Analysis Date = 02/24/14 
 Pct Recovery = 42%  Analysis Date = 02/24/14 
 Pct Recovery = 42%  Analysis Date = 02/22/14 
 Pct Recovery = 42%  Analysis Date = 02/22/14 
 Pct Recovery = 42%  Analysis Date = 02/20/14 
 Pct Recovery = 42%  Analysis Date = 02/20/14 
 Pct Recovery = 42%  Analysis Date = 02/18/14 
 Pct Recovery = 42%  Analysis Date = 02/18/14 
 Pct Recovery = 42%  Analysis Date = 02/16/14 
 Pct Recovery = 42%  Analysis Date = 02/16/14 
 Pct Recovery = 42%  Analysis Date = 02/14/14 
 Pct Recovery = 42%  Analysis Date = 02/14/14 
 Pct Recovery = 42%  Analysis Date = 02/12/14 
 Pct Recovery = 42%  Analysis Date = 02/12/14 
 Pct Recovery = 42%  Analysis Date = 02/10/14 
 Pct Recovery = 43%  Analysis Date = 02/10/14 
 Pct Recovery = 43%  Analysis Date = 02/08/14 
 Pct Recovery = 43%  Analysis Date = 02/08/14 
 Pct Recovery = 43%  Analysis Date = 02/06/14 
 Pct Recovery = 43%  Analysis Date = 02/06/14 
 Pct Recovery = 43%  Analysis Date = 02/04/14 
 Pct Recovery = 43%  Analysis Date = 02/04/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 01/30/14 
 Pct Recovery = 43%  Analysis Date = 01/30/14 
 Pct Recovery = 43%  Analysis Date = 01/28/14 
 Pct Recovery = 43%  Analysis Date = 01/28/14 
 Pct Recovery = 43%  Analysis Date = 01/26/14 
 Pct Recovery = 43%  Analysis Date = 01/26/14 
 Pct Recovery = 43%  Analysis Date = 01/24/14 
 Pct Recovery = 43%  Analysis Date = 01/24/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/22/14 
 Pct Recovery = 43%  Analysis Date = 01/20/14 
 Pct Recovery = 43%  Analysis Date = 01/20/14 
 Pct Recovery = 43%  Analysis Date = 01/18/14 
 Pct Recovery = 43%  Analysis Date = 01/18/14 
 Pct Recovery = 43%  Analysis Date = 01/16/14 
 Pct Recovery = 43%  Analysis Date = 01/16/14 
 Pct Recovery = 43%  Analysis Date = 01/14/14 
 Pct Recovery = 43%  Analysis Date = 01/14/14 
 Pct Recovery = 43%  Analysis Date = 01/12/14 
 Pct Recovery = 44%  Analysis Date = 01/12/14 
 Pct Recovery = 44%  Analysis Date = 01/10/14 
 Pct Recovery = 44%  Analysis Date = 01/10/14 
 Pct Recovery = 44%  Analysis Date = 01/08/14 
 Pct Recovery = 44%  Analysis Date = 01/08/14 
 Pct Recovery = 44%  Analysis Date = 01/06/14 
 Pct Recovery = 45%  Analysis Date = 01/06/14 
 Pct Recovery = 45%  Analysis Date = 01/04/14 
 Pct Recovery = 45%  Analysis Date = 01/04/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 01/02/14 
 Pct Recovery = 45%  Analysis Date = 12/31/13 
 Pct Recovery = 46%  Analysis Date = 12/31/13 
 Pct Recovery = 46%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/29/13 
 Pct Recovery = 46%  Analysis Date = 12/27/13 
 Pct Recovery = 47%  Analysis Date = 12/27/13 
 Pct Recovery = 47%  Analysis Date = 12/25/13 
 Pct Recovery = 47%  Analysis Date = 12/25/13 
 Pct Recovery = 47%  Analysis Date = 12/23/13 
 Pct Recovery = 47%  Analysis Date = 12/23/13 
 Pct Recovery = 47%  Analysis Date = 12/21/13 
 Pct Recovery = 48%  Analysis Date = 12/21/13 
 Pct Recovery = 48%  Analysis Date = 12/19/13 
 Pct Recovery = 48%  Analysis Date = 12/19/13 
 Pct Recovery = 48%  Analysis Date = 12/17/13 
 Pct Recovery = 48%  Analysis Date = 12/17/13 
 Pct Recovery = 48%  Analysis Date = 12/15/13 
 Pct Recovery = 49%  Analysis Date = 12/15/13 
 Pct Recovery = 49%  Analysis Date = 12/13/13 
 Pct Recovery = 49%  Analysis Date = 12/13/13 
 Pct Recovery = 49%  Analysis Date = 12/11/13 
 Pct Recovery = 49%  Analysis Date = 12/11/13 
 Pct Recovery = 49%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/09/13 
 Pct Recovery = 50%  Analysis Date = 12/07/13 
 Pct Recovery = 50%  Analysis Date = 12/07/13 
 Pct Recovery = 50%  Analysis Date = 12/05/13 
 Pct Recovery = 51%  Analysis Date = 12/05/13 
 Pct Recovery = 51%  Analysis Date = 12/03/13 
 Pct Recovery = 51%  Analysis Date = 12/03/13 
 Pct Recovery = 51%  Analysis Date = 12/01/13 
 Pct Recovery = 51%  Analysis Date = 12/01/13 
 Pct Recovery = 51%  Analysis Date = 11/29/13 
 Pct Recovery = 52%  Analysis Date = 11/29/13 
 Pct Recovery = 52%  Analysis Date = 11/27/13 
 Pct Recovery = 52%  Analysis Date = 11/27/13 
 Pct Recovery = 52%  Analysis Date = 11/24/13 
 Pct Recovery = 53%  Analysis Date = 11/24/13 
 Pct Recovery = 53%  Analysis Date = 11/22/13 
 Pct Recovery = 53%  Analysis Date = 11/22/13 
 Pct Recovery = 53%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/16/13 
 Pct Recovery = 54%  Analysis Date = 11/16/13 
 Pct Recovery = 54%  Analysis Date = 11/14/13 
 Pct Recovery = 55%  Analysis Date = 11/14/13 
 Pct Recovery = 55%  Analysis Date = 11/12/13 
 Pct Recovery = 55%  Analysis Date = 11/12/13 
 Pct Recovery = 55%  Analysis Date = 11/10/13 
 Pct Recovery = 56%  Analysis Date = 11/10/13 
 Pct Recovery = 56%  Analysis Date = 11/08/13 
 Pct Recovery = 56%  Analysis Date = 11/08/13 
 Pct Recovery = 56%  Analysis Date = 11/06/13 
 Pct Recovery = 57%  Analysis Date = 11/06/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/04/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/31/13 
 Pct Recovery = 58%  Analysis Date = 10/29/13 
 Pct Recovery = 58%  Analysis Date = 10/29/13 
 Pct Recovery = 58%  Analysis Date = 10/27/13 
 Pct Recovery = 58%  Analysis Date = 10/27/13 
 Pct Recovery = 58%  Analysis Date = 10/25/13 
 Pct Recovery = 58%  Analysis Date = 10/25/13 
 Pct Recovery = 58%  Analysis Date = 10/23/13 
 Pct Recovery = 58%  Analysis Date = 10/23/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 58%  Analysis Date = 10/17/13 
 Pct Recovery = 57%  Analysis Date = 10/17/13 
 Pct Recovery = 57%  Analysis Date = 10/15/13 
 Pct Recovery = 57%  Analysis Date = 10/15/13 
 Pct Recovery = 57%  Analysis Date = 10/13/13 
 Pct Recovery = 57%  Analysis Date = 10/13/13 
 Pct Recovery = 57%  Analysis Date = 10/11/13 
 Pct Recovery = 57%  Analysis Date = 10/11/13 
 Pct Recovery = 57%  Analysis Date = 10/09/13 
 Pct Recovery = 57%  Analysis Date = 10/09/13 
 Pct Recovery = 57%  Analysis Date = 10/07/13 
 Pct Recovery = 56%  Analysis Date = 10/07/13 
 Pct Recovery = 56%  Analysis Date = 10/05/13 
 Pct Recovery = 56%  Analysis Date = 10/05/13 
 Pct Recovery = 56%  Analysis Date = 10/03/13 
 Pct Recovery = 56%  Analysis Date = 10/03/13 
 Pct Recovery = 56%  Analysis Date = 10/01/13 
 Pct Recovery = 56%  Analysis Date = 10/01/13 
 Pct Recovery = 56%  Analysis Date = 09/29/13 
 Pct Recovery = 56%  Analysis Date = 09/29/13 
 Pct Recovery = 56%  Analysis Date = 09/27/13 
 Pct Recovery = 56%  Analysis Date = 09/27/13 
 Pct Recovery = 56%  Analysis Date = 09/25/13 
 Pct Recovery = 55%  Analysis Date = 09/25/13 
 Pct Recovery = 55%  Analysis Date = 09/23/13 
 Pct Recovery = 55%  Analysis Date = 09/23/13 
 Pct Recovery = 55%  Analysis Date = 09/21/13 
 Pct Recovery = 55%  Analysis Date = 09/21/13 
 Pct Recovery = 55%  Analysis Date = 09/18/13 
 Pct Recovery = 55%  Analysis Date = 09/18/13 
 Pct Recovery = 55%  Analysis Date = 09/16/13 
 Pct Recovery = 55%  Analysis Date = 09/16/13 
 Pct Recovery = 55%  Analysis Date = 09/14/13 
 Pct Recovery = 55%  Analysis Date = 09/14/13 
 Pct Recovery = 55%  Analysis Date = 09/12/13 
 Pct Recovery = 54%  Analysis Date = 09/12/13 
 Pct Recovery = 54%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/10/13 
 Pct Recovery = 54%  Analysis Date = 09/08/13 
 Pct Recovery = 54%  Analysis Date = 09/08/13 
 Pct Recovery = 54%  Analysis Date = 09/06/13 
 Pct Recovery = 54%  Analysis Date = 09/06/13 
 Pct Recovery = 54%  Analysis Date = 09/04/13 
 Pct Recovery = 54%  Analysis Date = 09/04/13 
 Pct Recovery = 54%  Analysis Date = 09/02/13 
 Pct Recovery = 53%  Analysis Date = 09/02/13 
 Pct Recovery = 53%  Analysis Date = 08/31/13 
 Pct Recovery = 53%  Analysis Date = 08/31/13 
 Pct Recovery = 53%  Analysis Date = 08/29/13 
 Pct Recovery = 53%  Analysis Date = 08/29/13 
 Pct Recovery = 53%  Analysis Date = 08/27/13 
 Pct Recovery = 53%  Analysis Date = 08/27/13 
 Pct Recovery = 53%  Analysis Date = 08/25/13 
 Pct Recovery = 53%  Analysis Date = 08/25/13 
 Pct Recovery = 53%  Analysis Date = 08/23/13 
 Pct Recovery = 53%  Analysis Date = 08/23/13 
 Pct Recovery = 53%  Analysis Date = 08/21/13 
 Pct Recovery = 52%  Analysis Date = 08/21/13 
 Pct Recovery = 52%  Analysis Date = 08/19/13 
 Pct Recovery = 52%  Analysis Date = 08/19/13 
 Pct Recovery = 52%  Analysis Date = 08/17/13 
 Pct Recovery = 52%  Analysis Date = 08/17/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/15/13 
 Pct Recovery = 52%  Analysis Date = 08/13/13 
 Pct Recovery = 52%  Analysis Date = 08/13/13 
 Pct Recovery = 52%  Analysis Date = 08/11/13 
 Pct Recovery = 51%  Analysis Date = 08/11/13 
 Pct Recovery = 51%  Analysis Date = 08/09/13 
 Pct Recovery = 51%  Analysis Date = 08/09/13 
 Pct Recovery = 51%  Analysis Date = 08/07/13 
 Pct Recovery = 51%  Analysis Date = 08/07/13 
 Pct Recovery = 51%  Analysis Date = 08/05/13 
 Pct Recovery = 51%  Analysis Date = 08/05/13 
 Pct Recovery = 51%  Analysis Date = 08/03/13 
 Pct Recovery = 51%  Analysis Date = 08/03/13 
 Pct Recovery = 51%  Analysis Date = 08/01/13 
 Pct Recovery = 50%  Analysis Date = 08/01/13 
 Pct Recovery = 50%  Analysis Date = 07/30/13 
 Pct Recovery = 49%  Analysis Date = 07/30/13 
 Pct Recovery = 49%  Analysis Date = 07/28/13 
 Pct Recovery = 49%  Analysis Date = 07/28/13 
 Pct Recovery = 49%  Analysis Date = 07/26/13 
 Pct Recovery = 48%  Analysis Date = 07/26/13 
 Pct Recovery = 48%  Analysis Date = 07/24/13 
 Pct Recovery = 47%  Analysis Date = 07/24/13 
 Pct Recovery = 47%  Analysis Date = 07/22/13 
 Pct Recovery = 46%  Analysis Date = 07/22/13 
 Pct Recovery = 46%  Analysis Date = 07/20/13 
 Pct Recovery = 45%  Analysis Date = 07/20/13 
 Pct Recovery = 45%  Analysis Date = 07/18/13 
 Pct Recovery = 44%  Analysis Date = 07/18/13 
 Pct Recovery = 44%  Analysis Date = 07/16/13 
 Pct Recovery = 44%  Analysis Date = 07/16/13 
 Pct Recovery = 44%  Analysis Date = 07/14/13 
 Pct Recovery = 43%  Analysis Date = 07/14/13 
 Pct Recovery = 43%  Analysis Date = 07/11/13 
 Pct Recovery = 42%  Analysis Date = 07/11/13 
 Pct Recovery = 42%  Analysis Date = 07/09/13 
 Pct Recovery = 41%  Analysis Date = 07/09/13 
 Pct Recovery = 41%  Analysis Date = 07/07/13 
 Pct Recovery = 40%  Analysis Date = 07/07/13 
 Pct Recovery = 40%  Analysis Date = 07/05/13 
 Pct Recovery = 39%  Analysis Date = 07/05/13 
 Pct Recovery = 39%  Analysis Date = 07/03/13 
 Pct Recovery = 39%  Analysis Date = 07/03/13 
 Pct Recovery = 39%  Analysis Date = 07/01/13 
 Pct Recovery = 38%  Analysis Date = 07/01/13 
 Pct Recovery = 38%  Analysis Date = 06/29/13 
 Pct Recovery = 37%  Analysis Date = 06/29/13 
 Pct Recovery = 37%  Analysis Date = 06/27/13 
 Pct Recovery = 36%  Analysis Date = 06/27/13 
 Pct Recovery = 36%  Analysis Date = 06/25/13 
 Pct Recovery = 35%  Analysis Date = 06/25/13 
 Pct Recovery = 35%  Analysis Date = 06/23/13 
 Pct Recovery = 34%  Analysis Date = 06/23/13 
 Pct Recovery = 34%  Analysis Date = 06/21/13 
 Pct Recovery = 34%  Analysis Date = 06/21/13 
 Pct Recovery = 34%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/19/13 
 Pct Recovery = 33%  Analysis Date = 06/17/13 
 Pct Recovery = 32%  Analysis Date = 06/17/13 
 Pct Recovery = 32%  Analysis Date = 06/15/13 
 Pct Recovery = 31%  Analysis Date = 06/15/13 
 Pct Recovery = 31%  Analysis Date = 06/13/13 
 Pct Recovery = 30%  Analysis Date = 06/13/13 
 Pct Recovery = 30%  Analysis Date = 06/11/13 
 Pct Recovery = 29%  Analysis Date = 06/11/13 
 Pct Recovery = 29%  Analysis Date = 06/09/13 
 Pct Recovery = 29%  Analysis Date = 06/09/13 
 Pct Recovery = 29%  Analysis Date = 06/07/13 
 Pct Recovery = 28%  Analysis Date = 06/07/13 
 Pct Recovery = 28%  Analysis Date = 06/05/13 
 Pct Recovery = 27%  Analysis Date = 06/05/13 
 Pct Recovery = 27%  Analysis Date = 06/03/13 
 Pct Recovery = 26%  Analysis Date = 06/03/13 
 Pct Recovery = 26%  Analysis Date = 06/01/13 
 Pct Recovery = 25%  Analysis Date = 06/01/13 
 Pct Recovery = 25%  Analysis Date = 05/30/13 
 Pct Recovery = 24%  Analysis Date = 05/30/13 
 Pct Recovery = 24%  Analysis Date = 05/28/13 
 Pct Recovery = 24%  Analysis Date = 05/28/13 
 Pct Recovery = 24%  Analysis Date = 05/26/13 
 Pct Recovery = 23%  Analysis Date = 05/26/13 
 Pct Recovery = 23%  Analysis Date = 05/24/13 
 Pct Recovery = 22%  Analysis Date = 05/24/13 
 Pct Recovery = 22%  Analysis Date = 05/22/13 
 Pct Recovery = 21%  Analysis Date = 05/22/13 
 Pct Recovery = 21%  Analysis Date = 05/20/13 
 Pct Recovery = 20%  Analysis Date = 05/20/13 
 Pct Recovery = 20%  Analysis Date = 05/18/13 
 Pct Recovery = 19%  Analysis Date = 05/18/13 
 Pct Recovery = 19%  Analysis Date = 05/16/13 
 Pct Recovery = 18%  Analysis Date = 05/16/13 
 Pct Recovery = 18%  Analysis Date = 05/14/13 
 Pct Recovery = 18%  Analysis Date = 05/14/13 
 Pct Recovery = 18%  Analysis Date = 05/12/13 
 Pct Recovery = 17%  Analysis Date = 05/12/13 
 Pct Recovery = 17%  Analysis Date = 05/10/13 
 Pct Recovery = 16%  Analysis Date = 05/10/13 
 Pct Recovery = 16%  Analysis Date = 05/08/13 
 Pct Recovery = 15%  Analysis Date = 05/08/13 
 Pct Recovery = 15%  Analysis Date = 05/05/13 
 Pct Recovery = 14%  Analysis Date = 05/05/13 
 Pct Recovery = 14%  Analysis Date = 05/03/13 
 Pct Recovery = 13%  Analysis Date = 05/03/13 
 Pct Recovery = 13%  Analysis Date = 05/01/13 
 Pct Recovery = 13%  Analysis Date = 05/01/13 
 Pct Recovery = 13%  Analysis Date = 04/29/13 
 Pct Recovery = 12%  Analysis Date = 04/29/13 
 Pct Recovery = 12%  Analysis Date = 04/27/13 
 Pct Recovery = 11%  Analysis Date = 04/27/13 
 Pct Recovery = 11%  Analysis Date = 04/25/13 
 Pct Recovery = 11%  Analysis Date = 04/25/13 
 Pct Recovery = 11%  Analysis Date = 04/23/13 
 Pct Recovery = 10%  Analysis Date = 04/23/13 
 Pct Recovery = 10%  Analysis Date = 04/21/13 
 Pct Recovery = 10%  Analysis Date = 04/21/13 
 Pct Recovery = 10%  Analysis Date = 04/19/13 
 Pct Recovery = 9%  Analysis Date = 04/19/13 
 Pct Recovery = 9%  Analysis Date = 04/17/13 
 Pct Recovery = 9%  Analysis Date = 04/17/13 
 Pct Recovery = 9%  Analysis Date = 04/15/13 
 Pct Recovery = 8%  Analysis Date = 04/15/13 
 Pct Recovery = 8%  Analysis Date = 04/13/13 
 Pct Recovery = 8%  Analysis Date = 04/13/13 
 Pct Recovery = 8%  Analysis Date = 04/11/13 
 Pct Recovery = 7%  Analysis Date = 04/11/13 
 Pct Recovery = 7%  Analysis Date = 04/09/13 
 Pct Recovery = 7%  Analysis Date = 04/09/13 
 Pct Recovery = 7%  Analysis Date = 04/07/13 
 Pct Recovery = 6%  Analysis Date = 04/07/13 
 Pct Recovery = 6%  Analysis Date = 04/05/13 
 Pct Recovery = 5%  Analysis Date = 04/05/13 
 Pct Recovery = 5%  Analysis Date = 04/03/13 
 Pct Recovery = 5%  Analysis Date = 04/03/13 
 Pct Recovery = 5%  Analysis Date = 04/01/13 
 Pct Recovery = 4%  Analysis Date = 04/01/13 
 Pct Recovery = 4%  Analysis Date = 03/30/13 
 Pct Recovery = 4%  Analysis Date = 03/30/13 
 Pct Recovery = 4%  Analysis Date = 03/28/13 
 Pct Recovery = 3%  Analysis Date = 03/28/13 
 Pct Recovery = 3%  Analysis Date = 03/26/13 
 Pct Recovery = 3%  Analysis Date = 03/26/13 
 Pct Recovery = 3%  Analysis Date = 03/24/13 
 Pct Recovery = 2%  Analysis Date = 03/24/13 
 Pct Recovery = 2%  Analysis Date = 03/22/13 
 Pct Recovery = 2%  Analysis Date = 03/22/13 
 Pct Recovery = 2%  Analysis Date = 03/20/13 
 Pct Recovery = 1%  Analysis Date = 03/20/13 
 Pct Recovery = 1%  Analysis Date = 03/18/13 
 Pct Recovery = 1%  Analysis Date = 03/18/13 
 Pct Recovery = 1%  Analysis Date = 03/16/13 
 Pct Recovery = 0%  Analysis Date = 03/16/13 
 Pct Recovery = 0%  Analysis Date = 03/14/13 
 Pct Recovery = (    0%)  Analysis Date = 03/14/13 
 Pct Recovery = (    0%)  Analysis Date = 03/12/13 
 Pct Recovery = (    1%)  Analysis Date = 03/12/13 
 Pct Recovery = (    1%)  Analysis Date = 03/10/13 
 Pct Recovery = (    2%)  Analysis Date = 03/10/13 
 Pct Recovery = (    2%)  Analysis Date = 03/08/13 
 Pct Recovery = (    2%)  Analysis Date = 03/08/13 
 Pct Recovery = (    2%)  Analysis Date = 03/06/13 
 Pct Recovery = (    3%)  Analysis Date = 03/06/13 
 Pct Recovery = (    3%)  Analysis Date = 03/04/13 
 Pct Recovery = (    3%)  Analysis Date = 03/04/13 
 Pct Recovery = (    3%)  Analysis Date = 03/02/13 
 Pct Recovery = (    4%)  Analysis Date = 03/02/13 
 Pct Recovery = (    4%)  Analysis Date = 02/28/13 
 Pct Recovery = (    4%)  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
SITAGLIPTIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 4% . 4% 0%
>= Reporting Level 12 33% 26% 35% 35%
Total 13 31% 27% 34% 28%

Sample Statistics
SITAGLIPTIN

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 13 93% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
SULFADIMETHOXINE
METHOD: LC9017 , TESTIDCODE: 67503LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 104%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 98%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 59%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 68%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 82%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 111%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 111%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 84%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 64%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 96%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 110%  Analysis Date = 04/09/14 
 Pct Recovery = 63%  Analysis Date = 04/07/14 
 Pct Recovery = 63%  Analysis Date = 04/07/14 
 Pct Recovery = 63%  Analysis Date = 04/05/14 
 Pct Recovery = 63%  Analysis Date = 04/05/14 
 Pct Recovery = 63%  Analysis Date = 04/02/14 
 Pct Recovery = 64%  Analysis Date = 04/02/14 
 Pct Recovery = 64%  Analysis Date = 03/31/14 
 Pct Recovery = 64%  Analysis Date = 03/31/14 
 Pct Recovery = 64%  Analysis Date = 03/28/14 
 Pct Recovery = 64%  Analysis Date = 03/28/14 
 Pct Recovery = 64%  Analysis Date = 03/26/14 
 Pct Recovery = 65%  Analysis Date = 03/26/14 
 Pct Recovery = 65%  Analysis Date = 03/24/14 
 Pct Recovery = 65%  Analysis Date = 03/24/14 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 Pct Recovery = 65%  Analysis Date = 03/21/14 
 Pct Recovery = 65%  Analysis Date = 03/19/14 
 Pct Recovery = 66%  Analysis Date = 03/19/14 
 Pct Recovery = 66%  Analysis Date = 03/16/14 
 Pct Recovery = 66%  Analysis Date = 03/16/14 
 Pct Recovery = 66%  Analysis Date = 03/14/14 
 Pct Recovery = 66%  Analysis Date = 03/14/14 
 Pct Recovery = 66%  Analysis Date = 03/12/14 
 Pct Recovery = 67%  Analysis Date = 03/12/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/09/14 
 Pct Recovery = 67%  Analysis Date = 03/07/14 
 Pct Recovery = 67%  Analysis Date = 03/07/14 
 Pct Recovery = 67%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/04/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 03/02/14 
 Pct Recovery = 68%  Analysis Date = 02/28/14 
 Pct Recovery = 68%  Analysis Date = 02/28/14 
 Pct Recovery = 68%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/25/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/23/14 
 Pct Recovery = 69%  Analysis Date = 02/20/14 
 Pct Recovery = 69%  Analysis Date = 02/20/14 
 Pct Recovery = 69%  Analysis Date = 02/18/14 
 Pct Recovery = 70%  Analysis Date = 02/18/14 
 Pct Recovery = 70%  Analysis Date = 02/15/14 
 Pct Recovery = 70%  Analysis Date = 02/15/14 
 Pct Recovery = 70%  Analysis Date = 02/13/14 
 Pct Recovery = 70%  Analysis Date = 02/13/14 
 Pct Recovery = 70%  Analysis Date = 02/11/14 
 Pct Recovery = 71%  Analysis Date = 02/11/14 
 Pct Recovery = 71%  Analysis Date = 02/08/14 
 Pct Recovery = 71%  Analysis Date = 02/08/14 
 Pct Recovery = 71%  Analysis Date = 02/06/14 
 Pct Recovery = 71%  Analysis Date = 02/06/14 
 Pct Recovery = 71%  Analysis Date = 02/03/14 
 Pct Recovery = 71%  Analysis Date = 02/03/14 
 Pct Recovery = 71%  Analysis Date = 02/01/14 
 Pct Recovery = 72%  Analysis Date = 02/01/14 
 Pct Recovery = 72%  Analysis Date = 01/30/14 
 Pct Recovery = 72%  Analysis Date = 01/30/14 
 Pct Recovery = 72%  Analysis Date = 01/27/14 
 Pct Recovery = 72%  Analysis Date = 01/27/14 
 Pct Recovery = 72%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 75%  Analysis Date = 01/10/14 
 Pct Recovery = 75%  Analysis Date = 01/08/14 
 Pct Recovery = 75%  Analysis Date = 01/08/14 
 Pct Recovery = 75%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/06/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/03/14 
 Pct Recovery = 75%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 01/01/14 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/29/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/27/13 
 Pct Recovery = 76%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/24/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/22/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/20/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/17/13 
 Pct Recovery = 77%  Analysis Date = 12/15/13 
 Pct Recovery = 78%  Analysis Date = 12/15/13 
 Pct Recovery = 78%  Analysis Date = 12/12/13 
 Pct Recovery = 78%  Analysis Date = 12/12/13 
 Pct Recovery = 78%  Analysis Date = 12/10/13 
 Pct Recovery = 78%  Analysis Date = 12/10/13 
 Pct Recovery = 78%  Analysis Date = 12/08/13 
 Pct Recovery = 78%  Analysis Date = 12/08/13 
 Pct Recovery = 78%  Analysis Date = 12/05/13 
 Pct Recovery = 79%  Analysis Date = 12/05/13 
 Pct Recovery = 79%  Analysis Date = 12/03/13 
 Pct Recovery = 79%  Analysis Date = 12/03/13 
 Pct Recovery = 79%  Analysis Date = 11/30/13 
 Pct Recovery = 79%  Analysis Date = 11/30/13 
 Pct Recovery = 79%  Analysis Date = 11/28/13 
 Pct Recovery = 79%  Analysis Date = 11/28/13 
 Pct Recovery = 79%  Analysis Date = 11/26/13 
 Pct Recovery = 79%  Analysis Date = 11/26/13 
 Pct Recovery = 79%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/23/13 
 Pct Recovery = 78%  Analysis Date = 11/21/13 
 Pct Recovery = 78%  Analysis Date = 11/21/13 
 Pct Recovery = 78%  Analysis Date = 11/18/13 
 Pct Recovery = 78%  Analysis Date = 11/18/13 
 Pct Recovery = 78%  Analysis Date = 11/16/13 
 Pct Recovery = 78%  Analysis Date = 11/16/13 
 Pct Recovery = 78%  Analysis Date = 11/13/13 
 Pct Recovery = 78%  Analysis Date = 11/13/13 
 Pct Recovery = 78%  Analysis Date = 11/11/13 
 Pct Recovery = 77%  Analysis Date = 11/11/13 
 Pct Recovery = 77%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/04/13 
 Pct Recovery = 77%  Analysis Date = 11/04/13 
 Pct Recovery = 77%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 11/01/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/30/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/20/13 
 Pct Recovery = 77%  Analysis Date = 10/20/13 
 Pct Recovery = 77%  Analysis Date = 10/18/13 
 Pct Recovery = 77%  Analysis Date = 10/18/13 
 Pct Recovery = 77%  Analysis Date = 10/16/13 
 Pct Recovery = 77%  Analysis Date = 10/16/13 
 Pct Recovery = 77%  Analysis Date = 10/13/13 
 Pct Recovery = 77%  Analysis Date = 10/13/13 
 Pct Recovery = 77%  Analysis Date = 10/11/13 
 Pct Recovery = 77%  Analysis Date = 10/11/13 
 Pct Recovery = 77%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/08/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/06/13 
 Pct Recovery = 78%  Analysis Date = 10/04/13 
 Pct Recovery = 78%  Analysis Date = 10/04/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 10/01/13 
 Pct Recovery = 78%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/17/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/14/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/12/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/09/13 
 Pct Recovery = 80%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/07/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/05/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 09/02/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/31/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/28/13 
 Pct Recovery = 81%  Analysis Date = 08/26/13 
 Pct Recovery = 82%  Analysis Date = 08/26/13 
 Pct Recovery = 82%  Analysis Date = 08/24/13 
 Pct Recovery = 82%  Analysis Date = 08/24/13 
 Pct Recovery = 82%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/21/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/19/13 
 Pct Recovery = 82%  Analysis Date = 08/16/13 
 Pct Recovery = 83%  Analysis Date = 08/16/13 
 Pct Recovery = 83%  Analysis Date = 08/14/13 
 Pct Recovery = 83%  Analysis Date = 08/14/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/11/13 
 Pct Recovery = 83%  Analysis Date = 08/09/13 
 Pct Recovery = 83%  Analysis Date = 08/09/13 
 Pct Recovery = 83%  Analysis Date = 08/07/13 
 Pct Recovery = 83%  Analysis Date = 08/07/13 
 Pct Recovery = 83%  Analysis Date = 08/04/13 
 Pct Recovery = 84%  Analysis Date = 08/04/13 
 Pct Recovery = 84%  Analysis Date = 08/02/13 
 Pct Recovery = 84%  Analysis Date = 08/02/13 
 Pct Recovery = 84%  Analysis Date = 07/30/13 
 Pct Recovery = 84%  Analysis Date = 07/30/13 
 Pct Recovery = 84%  Analysis Date = 07/28/13 
 Pct Recovery = 85%  Analysis Date = 07/28/13 
 Pct Recovery = 85%  Analysis Date = 07/26/13 
 Pct Recovery = 85%  Analysis Date = 07/26/13 
 Pct Recovery = 85%  Analysis Date = 07/23/13 
 Pct Recovery = 85%  Analysis Date = 07/23/13 
 Pct Recovery = 85%  Analysis Date = 07/21/13 
 Pct Recovery = 86%  Analysis Date = 07/21/13 
 Pct Recovery = 86%  Analysis Date = 07/18/13 
 Pct Recovery = 86%  Analysis Date = 07/18/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 87%  Analysis Date = 07/16/13 
 Pct Recovery = 87%  Analysis Date = 07/14/13 
 Pct Recovery = 87%  Analysis Date = 07/14/13 
 Pct Recovery = 87%  Analysis Date = 07/11/13 
 Pct Recovery = 87%  Analysis Date = 07/11/13 
 Pct Recovery = 87%  Analysis Date = 07/09/13 
 Pct Recovery = 88%  Analysis Date = 07/09/13 
 Pct Recovery = 88%  Analysis Date = 07/06/13 
 Pct Recovery = 88%  Analysis Date = 07/06/13 
 Pct Recovery = 88%  Analysis Date = 07/04/13 
 Pct Recovery = 88%  Analysis Date = 07/04/13 
 Pct Recovery = 88%  Analysis Date = 07/02/13 
 Pct Recovery = 89%  Analysis Date = 07/02/13 
 Pct Recovery = 89%  Analysis Date = 06/29/13 
 Pct Recovery = 89%  Analysis Date = 06/29/13 
 Pct Recovery = 89%  Analysis Date = 06/27/13 
 Pct Recovery = 89%  Analysis Date = 06/27/13 
 Pct Recovery = 89%  Analysis Date = 06/24/13 
 Pct Recovery = 90%  Analysis Date = 06/24/13 
 Pct Recovery = 90%  Analysis Date = 06/22/13 
 Pct Recovery = 90%  Analysis Date = 06/22/13 
 Pct Recovery = 90%  Analysis Date = 06/19/13 
 Pct Recovery = 91%  Analysis Date = 06/19/13 
 Pct Recovery = 91%  Analysis Date = 06/17/13 
 Pct Recovery = 91%  Analysis Date = 06/17/13 
 Pct Recovery = 91%  Analysis Date = 06/15/13 
 Pct Recovery = 91%  Analysis Date = 06/15/13 
 Pct Recovery = 91%  Analysis Date = 06/12/13 
 Pct Recovery = 92%  Analysis Date = 06/12/13 
 Pct Recovery = 92%  Analysis Date = 06/10/13 
 Pct Recovery = 92%  Analysis Date = 06/10/13 
 Pct Recovery = 92%  Analysis Date = 06/07/13 
 Pct Recovery = 92%  Analysis Date = 06/07/13 
 Pct Recovery = 92%  Analysis Date = 06/05/13 
 Pct Recovery = 93%  Analysis Date = 06/05/13 
 Pct Recovery = 93%  Analysis Date = 06/03/13 
 Pct Recovery = 93%  Analysis Date = 06/03/13 
 Pct Recovery = 93%  Analysis Date = 05/31/13 
 Pct Recovery = 94%  Analysis Date = 05/31/13 
 Pct Recovery = 94%  Analysis Date = 05/29/13 
 Pct Recovery = 94%  Analysis Date = 05/29/13 
 Pct Recovery = 94%  Analysis Date = 05/26/13 
 Pct Recovery = 94%  Analysis Date = 05/26/13 
 Pct Recovery = 94%  Analysis Date = 05/24/13 
 Pct Recovery = 95%  Analysis Date = 05/24/13 
 Pct Recovery = 95%  Analysis Date = 05/22/13 
 Pct Recovery = 95%  Analysis Date = 05/22/13 
 Pct Recovery = 95%  Analysis Date = 05/19/13 
 Pct Recovery = 95%  Analysis Date = 05/19/13 
 Pct Recovery = 95%  Analysis Date = 05/17/13 
 Pct Recovery = 96%  Analysis Date = 05/17/13 
 Pct Recovery = 96%  Analysis Date = 05/14/13 
 Pct Recovery = 96%  Analysis Date = 05/14/13 
 Pct Recovery = 96%  Analysis Date = 05/12/13 
 Pct Recovery = 97%  Analysis Date = 05/12/13 
 Pct Recovery = 97%  Analysis Date = 05/10/13 
 Pct Recovery = 97%  Analysis Date = 05/10/13 
 Pct Recovery = 97%  Analysis Date = 05/07/13 
 Pct Recovery = 97%  Analysis Date = 05/07/13 
 Pct Recovery = 97%  Analysis Date = 05/05/13 
 Pct Recovery = 98%  Analysis Date = 05/05/13 
 Pct Recovery = 98%  Analysis Date = 05/02/13 
 Pct Recovery = 98%  Analysis Date = 05/02/13 
 Pct Recovery = 98%  Analysis Date = 04/30/13 
 Pct Recovery = 99%  Analysis Date = 04/30/13 
 Pct Recovery = 99%  Analysis Date = 04/27/13 
 Pct Recovery = 99%  Analysis Date = 04/27/13 
 Pct Recovery = 99%  Analysis Date = 04/25/13 
 Pct Recovery = 99%  Analysis Date = 04/25/13 
 Pct Recovery = 99%  Analysis Date = 04/23/13 
 Pct Recovery = 100%  Analysis Date = 04/23/13 
 Pct Recovery = 100%  Analysis Date = 04/20/13 
 Pct Recovery = 100%  Analysis Date = 04/20/13 
 Pct Recovery = 100%  Analysis Date = 04/18/13 
 Pct Recovery = 100%  Analysis Date = 04/18/13 
 Pct Recovery = 100%  Analysis Date = 04/15/13 
 Pct Recovery = 100%  Analysis Date = 04/15/13 
 Pct Recovery = 100%  Analysis Date = 04/13/13 
 Pct Recovery = 100%  Analysis Date = 04/13/13 
 Pct Recovery = 100%  Analysis Date = 04/11/13 
 Pct Recovery = 101%  Analysis Date = 04/11/13 
 Pct Recovery = 101%  Analysis Date = 04/08/13 
 Pct Recovery = 101%  Analysis Date = 04/08/13 
 Pct Recovery = 101%  Analysis Date = 04/06/13 
 Pct Recovery = 101%  Analysis Date = 04/06/13 
 Pct Recovery = 101%  Analysis Date = 04/03/13 
 Pct Recovery = 101%  Analysis Date = 04/03/13 
 Pct Recovery = 101%  Analysis Date = 04/01/13 
 Pct Recovery = 102%  Analysis Date = 04/01/13 
 Pct Recovery = 102%  Analysis Date = 03/30/13 
 Pct Recovery = 102%  Analysis Date = 03/30/13 
 Pct Recovery = 102%  Analysis Date = 03/27/13 
 Pct Recovery = 102%  Analysis Date = 03/27/13 
 Pct Recovery = 102%  Analysis Date = 03/25/13 
 Pct Recovery = 102%  Analysis Date = 03/25/13 
 Pct Recovery = 102%  Analysis Date = 03/22/13 
 Pct Recovery = 102%  Analysis Date = 03/22/13 
 Pct Recovery = 102%  Analysis Date = 03/20/13 
 Pct Recovery = 103%  Analysis Date = 03/20/13 
 Pct Recovery = 103%  Analysis Date = 03/17/13 
 Pct Recovery = 103%  Analysis Date = 03/17/13 
 Pct Recovery = 103%  Analysis Date = 03/15/13 
 Pct Recovery = 103%  Analysis Date = 03/15/13 
 Pct Recovery = 103%  Analysis Date = 03/13/13 
 Pct Recovery = 103%  Analysis Date = 03/13/13 
 Pct Recovery = 103%  Analysis Date = 03/10/13 
 Pct Recovery = 104%  Analysis Date = 03/10/13 
 Pct Recovery = 104%  Analysis Date = 03/08/13 
 Pct Recovery = 104%  Analysis Date = 03/08/13 
 Pct Recovery = 104%  Analysis Date = 03/05/13 
 Pct Recovery = 104%  Analysis Date = 03/05/13 
 Pct Recovery = 104%  Analysis Date = 03/03/13 
 Pct Recovery = 104%  Analysis Date = 03/03/13 
 Pct Recovery = 104%  Analysis Date = 03/01/13 
 Pct Recovery = 104%  Analysis Date = 03/01/13 
 Pct Recovery = 104%  Analysis Date = 02/26/13 
 Pct Recovery = 105%  Analysis Date = 02/26/13 
 Pct Recovery = 105%  Analysis Date = 02/24/13 
 Pct Recovery = 105%  Analysis Date = 02/24/13 
 Pct Recovery = 105%  Analysis Date = 02/21/13 
 Pct Recovery = 105%  Analysis Date = 02/21/13 
 Pct Recovery = 105%  Analysis Date = 02/19/13 
 Pct Recovery = 105%  Analysis Date = 02/19/13 
 Pct Recovery = 105%  Analysis Date = 02/17/13 
 Pct Recovery = 105%  Analysis Date = 02/17/13 
 Pct Recovery = 105%  Analysis Date = 02/14/13 
 Pct Recovery = 105%  Analysis Date = 02/14/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 105%  Analysis Date = 02/07/13 
 Pct Recovery = 105%  Analysis Date = 02/07/13 
 Pct Recovery = 105%  Analysis Date = 02/05/13 
 Pct Recovery = 105%  Analysis Date = 02/05/13 
 Pct Recovery = 105%  Analysis Date = 02/02/13 
 Pct Recovery = 105%  Analysis Date = 02/02/13 
 Pct Recovery = 105%  Analysis Date = 01/31/13 
 Pct Recovery = 105%  Analysis Date = 01/31/13 
 Pct Recovery = 105%  Analysis Date = 01/28/13 
 Pct Recovery = 106%  Analysis Date = 01/28/13 
 Pct Recovery = 106%  Analysis Date = 01/26/13 
 Pct Recovery = 106%  Analysis Date = 01/26/13 
 Pct Recovery = 106%  Analysis Date = 01/23/13 
 Pct Recovery = 106%  Analysis Date = 01/23/13 
 Pct Recovery = 106%  Analysis Date = 01/21/13 
 Pct Recovery = 106%  Analysis Date = 01/21/13 
 Pct Recovery = 106%  Analysis Date = 01/19/13 
 Pct Recovery = 106%  Analysis Date = 01/19/13 
 Pct Recovery = 106%  Analysis Date = 01/16/13 
 Pct Recovery = 106%  Analysis Date = 01/16/13 
 Pct Recovery = 106%  Analysis Date = 01/14/13 
 Pct Recovery = 106%  Analysis Date = 01/14/13 
 Pct Recovery = 106%  Analysis Date = 01/11/13 
 Pct Recovery = 106%  Analysis Date = 01/11/13 
 Pct Recovery = 106%  Analysis Date = 01/09/13 
 Pct Recovery = 106%  Analysis Date = 01/09/13 
 Pct Recovery = 106%  Analysis Date = 01/07/13 
 Pct Recovery = 106%  Analysis Date = 01/07/13 
 Pct Recovery = 106%  Analysis Date = 01/04/13 
 Pct Recovery = 106%  Analysis Date = 01/04/13 
 Pct Recovery = 106%  Analysis Date = 01/02/13 
 Pct Recovery = 106%  Analysis Date = 01/02/13 
 Pct Recovery = 106%  Analysis Date = 12/30/12 
 Pct Recovery = 107%  Analysis Date = 12/30/12 
 Pct Recovery = 107%  Analysis Date = 12/28/12 
 Pct Recovery = 107%  Analysis Date = 12/28/12 
 Pct Recovery = 107%  Analysis Date = 12/26/12 
 Pct Recovery = 107%  Analysis Date = 12/26/12 
 Pct Recovery = 107%  Analysis Date = 12/23/12 
 Pct Recovery = 107%  Analysis Date = 12/23/12 
 Pct Recovery = 107%  Analysis Date = 12/21/12 
 Pct Recovery = 107%  Analysis Date = 12/21/12 
 Pct Recovery = 107%  Analysis Date = 12/18/12 
 Pct Recovery = 107%  Analysis Date = 12/18/12 
 Pct Recovery = 107%  Analysis Date = 12/16/12 
 Pct Recovery = 107%  Analysis Date = 12/16/12 
 Pct Recovery = 107%  Analysis Date = 12/14/12 
 Pct Recovery = 107%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFADIMETHOXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 110% . 110% 0%
>= Reporting Level 13 85% 18% 82% 18%
Total 14 87% 18% 83% 22%

Sample Statistics
SULFADIMETHOXINE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 3 21% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
SULFAMETHIZOLE
METHOD: LC9017 , TESTIDCODE: 67476LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 75%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 91%  Analysis Date = 05/02/13 
 SpikeMix = ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 80%  Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 189%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 61%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 03/21/14 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 75%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 90%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 85%  Analysis Date = 03/27/13 
 SpikeMix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 77%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 76%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 66%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 70%  Analysis Date = 04/09/14 
 Pct Recovery = 70%  Analysis Date = 04/07/14 
 Pct Recovery = 71%  Analysis Date = 04/07/14 
 Pct Recovery = 71%  Analysis Date = 04/05/14 
 Pct Recovery = 71%  Analysis Date = 04/05/14 
 Pct Recovery = 71%  Analysis Date = 04/02/14 
 Pct Recovery = 71%  Analysis Date = 04/02/14 
 Pct Recovery = 71%  Analysis Date = 03/31/14 
 Pct Recovery = 71%  Analysis Date = 03/31/14 
 Pct Recovery = 71%  Analysis Date = 03/28/14 
 Pct Recovery = 71%  Analysis Date = 03/28/14 
 Pct Recovery = 71%  Analysis Date = 03/26/14 
 Pct Recovery = 71%  Analysis Date = 03/26/14 
 Pct Recovery = 71%  Analysis Date = 03/24/14 
 Pct Recovery = 71%  Analysis Date = 03/24/14 
 Pct Recovery = 71%  Analysis Date = 03/21/14 
 Pct Recovery = 71%  Analysis Date = 03/21/14 
 Pct Recovery = 71%  Analysis Date = 03/19/14 
 Pct Recovery = 71%  Analysis Date = 03/19/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/14/14 
 Pct Recovery = 71%  Analysis Date = 03/14/14 
 Pct Recovery = 71%  Analysis Date = 03/12/14 
 Pct Recovery = 71%  Analysis Date = 03/12/14 
 Pct Recovery = 71%  Analysis Date = 03/09/14 
 Pct Recovery = 72%  Analysis Date = 03/09/14 
 Pct Recovery = 72%  Analysis Date = 03/07/14 
 Pct Recovery = 72%  Analysis Date = 03/07/14 
 Pct Recovery = 72%  Analysis Date = 03/04/14 
 Pct Recovery = 72%  Analysis Date = 03/04/14 
 Pct Recovery = 72%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 02/28/14 
 Pct Recovery = 72%  Analysis Date = 02/28/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/23/14 
 Pct Recovery = 72%  Analysis Date = 02/23/14 
 Pct Recovery = 72%  Analysis Date = 02/20/14 
 Pct Recovery = 72%  Analysis Date = 02/20/14 
 Pct Recovery = 72%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/18/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/15/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/13/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/11/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/08/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/06/14 
 Pct Recovery = 72%  Analysis Date = 02/03/14 
 Pct Recovery = 72%  Analysis Date = 02/03/14 
 Pct Recovery = 72%  Analysis Date = 02/01/14 
 Pct Recovery = 72%  Analysis Date = 02/01/14 
 Pct Recovery = 72%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/30/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/27/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/25/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/22/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/20/14 
 Pct Recovery = 73%  Analysis Date = 01/18/14 
 Pct Recovery = 73%  Analysis Date = 01/18/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/15/14 
 Pct Recovery = 73%  Analysis Date = 01/13/14 
 Pct Recovery = 73%  Analysis Date = 01/13/14 
 Pct Recovery = 73%  Analysis Date = 01/10/14 
 Pct Recovery = 73%  Analysis Date = 01/10/14 
 Pct Recovery = 73%  Analysis Date = 01/08/14 
 Pct Recovery = 73%  Analysis Date = 01/08/14 
 Pct Recovery = 73%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/24/13 
 Pct Recovery = 73%  Analysis Date = 12/24/13 
 Pct Recovery = 73%  Analysis Date = 12/22/13 
 Pct Recovery = 73%  Analysis Date = 12/22/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/20/13 
 Pct Recovery = 73%  Analysis Date = 12/17/13 
 Pct Recovery = 73%  Analysis Date = 12/17/13 
 Pct Recovery = 73%  Analysis Date = 12/15/13 
 Pct Recovery = 73%  Analysis Date = 12/15/13 
 Pct Recovery = 73%  Analysis Date = 12/12/13 
 Pct Recovery = 73%  Analysis Date = 12/12/13 
 Pct Recovery = 73%  Analysis Date = 12/10/13 
 Pct Recovery = 73%  Analysis Date = 12/10/13 
 Pct Recovery = 73%  Analysis Date = 12/08/13 
 Pct Recovery = 73%  Analysis Date = 12/08/13 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 Pct Recovery = 73%  Analysis Date = 12/05/13 
 Pct Recovery = 73%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 12/03/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/30/13 
 Pct Recovery = 73%  Analysis Date = 11/28/13 
 Pct Recovery = 73%  Analysis Date = 11/28/13 
 Pct Recovery = 73%  Analysis Date = 11/26/13 
 Pct Recovery = 73%  Analysis Date = 11/26/13 
 Pct Recovery = 73%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/21/13 
 Pct Recovery = 73%  Analysis Date = 11/21/13 
 Pct Recovery = 73%  Analysis Date = 11/18/13 
 Pct Recovery = 73%  Analysis Date = 11/18/13 
 Pct Recovery = 73%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 73%  Analysis Date = 11/06/13 
 Pct Recovery = 73%  Analysis Date = 11/06/13 
 Pct Recovery = 73%  Analysis Date = 11/04/13 
 Pct Recovery = 73%  Analysis Date = 11/04/13 
 Pct Recovery = 73%  Analysis Date = 11/01/13 
 Pct Recovery = 73%  Analysis Date = 11/01/13 
 Pct Recovery = 73%  Analysis Date = 10/30/13 
 Pct Recovery = 73%  Analysis Date = 10/30/13 
 Pct Recovery = 73%  Analysis Date = 10/28/13 
 Pct Recovery = 73%  Analysis Date = 10/28/13 
 Pct Recovery = 73%  Analysis Date = 10/25/13 
 Pct Recovery = 73%  Analysis Date = 10/25/13 
 Pct Recovery = 73%  Analysis Date = 10/23/13 
 Pct Recovery = 73%  Analysis Date = 10/23/13 
 Pct Recovery = 73%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/20/13 
 Pct Recovery = 73%  Analysis Date = 10/18/13 
 Pct Recovery = 73%  Analysis Date = 10/18/13 
 Pct Recovery = 73%  Analysis Date = 10/16/13 
 Pct Recovery = 73%  Analysis Date = 10/16/13 
 Pct Recovery = 73%  Analysis Date = 10/13/13 
 Pct Recovery = 73%  Analysis Date = 10/13/13 
 Pct Recovery = 73%  Analysis Date = 10/11/13 
 Pct Recovery = 73%  Analysis Date = 10/11/13 
 Pct Recovery = 73%  Analysis Date = 10/08/13 
 Pct Recovery = 73%  Analysis Date = 10/08/13 
 Pct Recovery = 73%  Analysis Date = 10/06/13 
 Pct Recovery = 73%  Analysis Date = 10/06/13 
 Pct Recovery = 73%  Analysis Date = 10/04/13 
 Pct Recovery = 73%  Analysis Date = 10/04/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 10/01/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/29/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/26/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/24/13 
 Pct Recovery = 73%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/21/13 
 Pct Recovery = 72%  Analysis Date = 09/19/13 
 Pct Recovery = 72%  Analysis Date = 09/19/13 
 Pct Recovery = 72%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/17/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/14/13 
 Pct Recovery = 72%  Analysis Date = 09/12/13 
 Pct Recovery = 72%  Analysis Date = 09/12/13 
 Pct Recovery = 72%  Analysis Date = 09/09/13 
 Pct Recovery = 72%  Analysis Date = 09/09/13 
 Pct Recovery = 72%  Analysis Date = 09/07/13 
 Pct Recovery = 72%  Analysis Date = 09/07/13 
 Pct Recovery = 72%  Analysis Date = 09/05/13 
 Pct Recovery = 72%  Analysis Date = 09/05/13 
 Pct Recovery = 72%  Analysis Date = 09/02/13 
 Pct Recovery = 72%  Analysis Date = 09/02/13 
 Pct Recovery = 72%  Analysis Date = 08/31/13 
 Pct Recovery = 72%  Analysis Date = 08/31/13 
 Pct Recovery = 72%  Analysis Date = 08/28/13 
 Pct Recovery = 72%  Analysis Date = 08/28/13 
 Pct Recovery = 72%  Analysis Date = 08/26/13 
 Pct Recovery = 72%  Analysis Date = 08/26/13 
 Pct Recovery = 72%  Analysis Date = 08/24/13 
 Pct Recovery = 72%  Analysis Date = 08/24/13 
 Pct Recovery = 72%  Analysis Date = 08/21/13 
 Pct Recovery = 72%  Analysis Date = 08/21/13 
 Pct Recovery = 72%  Analysis Date = 08/19/13 
 Pct Recovery = 72%  Analysis Date = 08/19/13 
 Pct Recovery = 72%  Analysis Date = 08/16/13 
 Pct Recovery = 72%  Analysis Date = 08/16/13 
 Pct Recovery = 72%  Analysis Date = 08/14/13 
 Pct Recovery = 72%  Analysis Date = 08/14/13 
 Pct Recovery = 72%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/11/13 
 Pct Recovery = 73%  Analysis Date = 08/09/13 
 Pct Recovery = 73%  Analysis Date = 08/09/13 
 Pct Recovery = 73%  Analysis Date = 08/07/13 
 Pct Recovery = 73%  Analysis Date = 08/07/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/04/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 08/02/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/30/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/28/13 
 Pct Recovery = 73%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/26/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/23/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/21/13 
 Pct Recovery = 74%  Analysis Date = 07/18/13 
 Pct Recovery = 74%  Analysis Date = 07/18/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/16/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/14/13 
 Pct Recovery = 74%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/11/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/09/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/06/13 
 Pct Recovery = 75%  Analysis Date = 07/04/13 
 Pct Recovery = 75%  Analysis Date = 07/04/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 07/02/13 
 Pct Recovery = 75%  Analysis Date = 06/29/13 
 Pct Recovery = 75%  Analysis Date = 06/29/13 
 Pct Recovery = 75%  Analysis Date = 06/27/13 
 Pct Recovery = 75%  Analysis Date = 06/27/13 
 Pct Recovery = 75%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/24/13 
 Pct Recovery = 75%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/22/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 76%  Analysis Date = 06/15/13 
 Pct Recovery = 76%  Analysis Date = 06/15/13 
 Pct Recovery = 76%  Analysis Date = 06/12/13 
 Pct Recovery = 76%  Analysis Date = 06/12/13 
 Pct Recovery = 76%  Analysis Date = 06/10/13 
 Pct Recovery = 76%  Analysis Date = 06/10/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/07/13 
 Pct Recovery = 76%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/05/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 06/03/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/31/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/29/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/26/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/24/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/19/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/17/13 
 Pct Recovery = 78%  Analysis Date = 05/14/13 
 Pct Recovery = 78%  Analysis Date = 05/14/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/12/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/10/13 
 Pct Recovery = 78%  Analysis Date = 05/07/13 
 Pct Recovery = 78%  Analysis Date = 05/07/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/05/13 
 Pct Recovery = 78%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/27/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/25/13 
 Pct Recovery = 77%  Analysis Date = 04/23/13 
 Pct Recovery = 78%  Analysis Date = 04/23/13 
 Pct Recovery = 78%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 81%  Analysis Date = 04/18/13 
 Pct Recovery = 81%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/15/13 
 Pct Recovery = 82%  Analysis Date = 04/13/13 
 Pct Recovery = 83%  Analysis Date = 04/13/13 
 Pct Recovery = 83%  Analysis Date = 04/11/13 
 Pct Recovery = 85%  Analysis Date = 04/11/13 
 Pct Recovery = 85%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/08/13 
 Pct Recovery = 86%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/06/13 
 Pct Recovery = 87%  Analysis Date = 04/03/13 
 Pct Recovery = 88%  Analysis Date = 04/03/13 
 Pct Recovery = 88%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/30/13 
 Pct Recovery = 91%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/27/13 
 Pct Recovery = 92%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/25/13 
 Pct Recovery = 93%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/22/13 
 Pct Recovery = 94%  Analysis Date = 03/20/13 
 Pct Recovery = 94%  Analysis Date = 03/20/13 
 Pct Recovery = 94%  Analysis Date = 03/17/13 
 Pct Recovery = 95%  Analysis Date = 03/17/13 
 Pct Recovery = 95%  Analysis Date = 03/15/13 
 Pct Recovery = 96%  Analysis Date = 03/15/13 
 Pct Recovery = 96%  Analysis Date = 03/13/13 
 Pct Recovery = 96%  Analysis Date = 03/13/13 
 Pct Recovery = 96%  Analysis Date = 03/10/13 
 Pct Recovery = 97%  Analysis Date = 03/10/13 
 Pct Recovery = 97%  Analysis Date = 03/08/13 
 Pct Recovery = 98%  Analysis Date = 03/08/13 
 Pct Recovery = 98%  Analysis Date = 03/05/13 
 Pct Recovery = 99%  Analysis Date = 03/05/13 
 Pct Recovery = 99%  Analysis Date = 03/03/13 
 Pct Recovery = 99%  Analysis Date = 03/03/13 
 Pct Recovery = 99%  Analysis Date = 03/01/13 
 Pct Recovery = 100%  Analysis Date = 03/01/13 
 Pct Recovery = 100%  Analysis Date = 02/26/13 
 Pct Recovery = 101%  Analysis Date = 02/26/13 
 Pct Recovery = 101%  Analysis Date = 02/24/13 
 Pct Recovery = 101%  Analysis Date = 02/24/13 
 Pct Recovery = 101%  Analysis Date = 02/21/13 
 Pct Recovery = 102%  Analysis Date = 02/21/13 
 Pct Recovery = 102%  Analysis Date = 02/19/13 
 Pct Recovery = 103%  Analysis Date = 02/19/13 
 Pct Recovery = 103%  Analysis Date = 02/17/13 
 Pct Recovery = 104%  Analysis Date = 02/17/13 
 Pct Recovery = 104%  Analysis Date = 02/14/13 
 Pct Recovery = 104%  Analysis Date = 02/14/13 
 Pct Recovery = 104%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/12/13 
 Pct Recovery = 105%  Analysis Date = 02/09/13 
 Pct Recovery = 106%  Analysis Date = 02/09/13 
 Pct Recovery = 106%  Analysis Date = 02/07/13 
 Pct Recovery = 106%  Analysis Date = 02/07/13 
 Pct Recovery = 106%  Analysis Date = 02/05/13 
 Pct Recovery = 107%  Analysis Date = 02/05/13 
 Pct Recovery = 107%  Analysis Date = 02/02/13 
 Pct Recovery = 108%  Analysis Date = 02/02/13 
 Pct Recovery = 108%  Analysis Date = 01/31/13 
 Pct Recovery = 109%  Analysis Date = 01/31/13 
 Pct Recovery = 109%  Analysis Date = 01/28/13 
 Pct Recovery = 109%  Analysis Date = 01/28/13 
 Pct Recovery = 109%  Analysis Date = 01/26/13 
 Pct Recovery = 110%  Analysis Date = 01/26/13 
 Pct Recovery = 110%  Analysis Date = 01/23/13 
 Pct Recovery = 111%  Analysis Date = 01/23/13 
 Pct Recovery = 111%  Analysis Date = 01/21/13 
 Pct Recovery = 110%  Analysis Date = 01/21/13 
 Pct Recovery = 110%  Analysis Date = 01/19/13 
 Pct Recovery = 110%  Analysis Date = 01/19/13 
 Pct Recovery = 110%  Analysis Date = 01/16/13 
 Pct Recovery = 109%  Analysis Date = 01/16/13 
 Pct Recovery = 109%  Analysis Date = 01/14/13 
 Pct Recovery = 109%  Analysis Date = 01/14/13 
 Pct Recovery = 109%  Analysis Date = 01/11/13 
 Pct Recovery = 108%  Analysis Date = 01/11/13 
 Pct Recovery = 108%  Analysis Date = 01/09/13 
 Pct Recovery = 107%  Analysis Date = 01/09/13 
 Pct Recovery = 107%  Analysis Date = 01/07/13 
 Pct Recovery = 107%  Analysis Date = 01/07/13 
 Pct Recovery = 107%  Analysis Date = 01/04/13 
 Pct Recovery = 106%  Analysis Date = 01/04/13 
 Pct Recovery = 106%  Analysis Date = 01/02/13 
 Pct Recovery = 106%  Analysis Date = 01/02/13 
 Pct Recovery = 106%  Analysis Date = 12/30/12 
 Pct Recovery = 105%  Analysis Date = 12/30/12 
 Pct Recovery = 105%  Analysis Date = 12/28/12 
 Pct Recovery = 105%  Analysis Date = 12/28/12 
 Pct Recovery = 105%  Analysis Date = 12/26/12 
 Pct Recovery = 104%  Analysis Date = 12/26/12 
 Pct Recovery = 104%  Analysis Date = 12/23/12 
 Pct Recovery = 104%  Analysis Date = 12/23/12 
 Pct Recovery = 104%  Analysis Date = 12/21/12 
 Pct Recovery = 103%  Analysis Date = 12/21/12 
 Pct Recovery = 103%  Analysis Date = 12/18/12 
 Pct Recovery = 103%  Analysis Date = 12/18/12 
 Pct Recovery = 103%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/16/12 
 Pct Recovery = 102%  Analysis Date = 12/14/12 
 Pct Recovery = 102%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFAMETHIZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 84% 32% 76% 11%
Total 14 84% 32% 76% 11%

Sample Statistics
SULFAMETHIZOLE

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 14 .  
False Negatives 0 0% 0 out of 14
Not Spiked 18 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
SULFAMETHOXAZOLE
METHOD: LC9017 , TESTIDCODE: 67454LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 61%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 62%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 74%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 91%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 45%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 67%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 79%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 72%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 81%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 112%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 96%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 78%  Analysis Date = 04/09/14 
 Pct Recovery = 74%  Analysis Date = 04/07/14 
 Pct Recovery = 74%  Analysis Date = 04/07/14 
 Pct Recovery = 74%  Analysis Date = 04/05/14 
 Pct Recovery = 74%  Analysis Date = 04/05/14 
 Pct Recovery = 74%  Analysis Date = 04/03/14 
 Pct Recovery = 74%  Analysis Date = 04/03/14 
 Pct Recovery = 74%  Analysis Date = 04/01/14 
 Pct Recovery = 74%  Analysis Date = 04/01/14 
 Pct Recovery = 74%  Analysis Date = 03/30/14 
 Pct Recovery = 74%  Analysis Date = 03/30/14 
 Pct Recovery = 74%  Analysis Date = 03/28/14 
 Pct Recovery = 74%  Analysis Date = 03/28/14 
 Pct Recovery = 74%  Analysis Date = 03/26/14 
 Pct Recovery = 74%  Analysis Date = 03/26/14 
 Pct Recovery = 74%  Analysis Date = 03/24/14 
 Pct Recovery = 74%  Analysis Date = 03/24/14 
 Pct Recovery = 74%  Analysis Date = 03/22/14 
 Pct Recovery = 74%  Analysis Date = 03/22/14 
 Pct Recovery = 74%  Analysis Date = 03/20/14 
 Pct Recovery = 74%  Analysis Date = 03/20/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/18/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/16/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/14/14 
 Pct Recovery = 74%  Analysis Date = 03/12/14 
 Pct Recovery = 74%  Analysis Date = 03/12/14 
 Pct Recovery = 74%  Analysis Date = 03/10/14 
 Pct Recovery = 74%  Analysis Date = 03/10/14 
 Pct Recovery = 74%  Analysis Date = 03/08/14 
 Pct Recovery = 74%  Analysis Date = 03/08/14 
 Pct Recovery = 74%  Analysis Date = 03/06/14 
 Pct Recovery = 74%  Analysis Date = 03/06/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/04/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 03/02/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/28/14 
 Pct Recovery = 74%  Analysis Date = 02/26/14 
 Pct Recovery = 75%  Analysis Date = 02/26/14 
 Pct Recovery = 75%  Analysis Date = 02/24/14 
 Pct Recovery = 75%  Analysis Date = 02/24/14 
 Pct Recovery = 75%  Analysis Date = 02/22/14 
 Pct Recovery = 75%  Analysis Date = 02/22/14 
 Pct Recovery = 75%  Analysis Date = 02/20/14 
 Pct Recovery = 75%  Analysis Date = 02/20/14 
 Pct Recovery = 75%  Analysis Date = 02/18/14 
 Pct Recovery = 75%  Analysis Date = 02/18/14 
 Pct Recovery = 75%  Analysis Date = 02/16/14 
 Pct Recovery = 75%  Analysis Date = 02/16/14 
 Pct Recovery = 75%  Analysis Date = 02/14/14 
 Pct Recovery = 75%  Analysis Date = 02/14/14 
 Pct Recovery = 75%  Analysis Date = 02/12/14 
 Pct Recovery = 75%  Analysis Date = 02/12/14 
 Pct Recovery = 75%  Analysis Date = 02/10/14 
 Pct Recovery = 75%  Analysis Date = 02/10/14 
 Pct Recovery = 75%  Analysis Date = 02/08/14 
 Pct Recovery = 75%  Analysis Date = 02/08/14 
 Pct Recovery = 75%  Analysis Date = 02/06/14 
 Pct Recovery = 76%  Analysis Date = 02/06/14 
 Pct Recovery = 76%  Analysis Date = 02/04/14 
 Pct Recovery = 76%  Analysis Date = 02/04/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 02/02/14 
 Pct Recovery = 76%  Analysis Date = 01/30/14 
 Pct Recovery = 76%  Analysis Date = 01/30/14 
 Pct Recovery = 76%  Analysis Date = 01/28/14 
 Pct Recovery = 76%  Analysis Date = 01/28/14 
 Pct Recovery = 76%  Analysis Date = 01/26/14 
 Pct Recovery = 76%  Analysis Date = 01/26/14 
 Pct Recovery = 76%  Analysis Date = 01/24/14 
 Pct Recovery = 76%  Analysis Date = 01/24/14 
 Pct Recovery = 76%  Analysis Date = 01/22/14 
 Pct Recovery = 77%  Analysis Date = 01/22/14 
 Pct Recovery = 77%  Analysis Date = 01/20/14 
 Pct Recovery = 77%  Analysis Date = 01/20/14 
 Pct Recovery = 77%  Analysis Date = 01/18/14 
 Pct Recovery = 77%  Analysis Date = 01/18/14 
 Pct Recovery = 77%  Analysis Date = 01/16/14 
 Pct Recovery = 77%  Analysis Date = 01/16/14 
 Pct Recovery = 77%  Analysis Date = 01/14/14 
 Pct Recovery = 77%  Analysis Date = 01/14/14 
 Pct Recovery = 77%  Analysis Date = 01/12/14 
 Pct Recovery = 78%  Analysis Date = 01/12/14 
 Pct Recovery = 78%  Analysis Date = 01/10/14 
 Pct Recovery = 78%  Analysis Date = 01/10/14 
 Pct Recovery = 78%  Analysis Date = 01/08/14 
 Pct Recovery = 78%  Analysis Date = 01/08/14 
 Pct Recovery = 78%  Analysis Date = 01/06/14 
 Pct Recovery = 78%  Analysis Date = 01/06/14 
 Pct Recovery = 78%  Analysis Date = 01/04/14 
 Pct Recovery = 79%  Analysis Date = 01/04/14 
 Pct Recovery = 79%  Analysis Date = 01/02/14 
 Pct Recovery = 79%  Analysis Date = 01/02/14 
 Pct Recovery = 79%  Analysis Date = 12/31/13 
 Pct Recovery = 79%  Analysis Date = 12/31/13 
 Pct Recovery = 79%  Analysis Date = 12/29/13 
 Pct Recovery = 79%  Analysis Date = 12/29/13 
 Pct Recovery = 79%  Analysis Date = 12/27/13 
 Pct Recovery = 80%  Analysis Date = 12/27/13 
 Pct Recovery = 80%  Analysis Date = 12/25/13 
 Pct Recovery = 80%  Analysis Date = 12/25/13 
 Pct Recovery = 80%  Analysis Date = 12/23/13 
 Pct Recovery = 80%  Analysis Date = 12/23/13 
 Pct Recovery = 80%  Analysis Date = 12/21/13 
 Pct Recovery = 80%  Analysis Date = 12/21/13 
 Pct Recovery = 80%  Analysis Date = 12/19/13 
 Pct Recovery = 81%  Analysis Date = 12/19/13 
 Pct Recovery = 81%  Analysis Date = 12/17/13 
 Pct Recovery = 81%  Analysis Date = 12/17/13 
 Pct Recovery = 81%  Analysis Date = 12/15/13 
 Pct Recovery = 81%  Analysis Date = 12/15/13 
 Pct Recovery = 81%  Analysis Date = 12/13/13 
 Pct Recovery = 82%  Analysis Date = 12/13/13 
 Pct Recovery = 82%  Analysis Date = 12/11/13 
 Pct Recovery = 82%  Analysis Date = 12/11/13 
 Pct Recovery = 82%  Analysis Date = 12/09/13 
 Pct Recovery = 82%  Analysis Date = 12/09/13 
 Pct Recovery = 82%  Analysis Date = 12/07/13 
 Pct Recovery = 82%  Analysis Date = 12/07/13 
 Pct Recovery = 82%  Analysis Date = 12/05/13 
 Pct Recovery = 83%  Analysis Date = 12/05/13 
 Pct Recovery = 83%  Analysis Date = 12/03/13 
 Pct Recovery = 83%  Analysis Date = 12/03/13 
 Pct Recovery = 83%  Analysis Date = 12/01/13 
 Pct Recovery = 83%  Analysis Date = 12/01/13 
 Pct Recovery = 83%  Analysis Date = 11/29/13 
 Pct Recovery = 83%  Analysis Date = 11/29/13 
 Pct Recovery = 83%  Analysis Date = 11/27/13 
 Pct Recovery = 84%  Analysis Date = 11/27/13 
 Pct Recovery = 84%  Analysis Date = 11/24/13 
 Pct Recovery = 84%  Analysis Date = 11/24/13 
 Pct Recovery = 84%  Analysis Date = 11/22/13 
 Pct Recovery = 84%  Analysis Date = 11/22/13 
 Pct Recovery = 84%  Analysis Date = 11/20/13 
 Pct Recovery = 84%  Analysis Date = 11/20/13 
 Pct Recovery = 84%  Analysis Date = 11/18/13 
 Pct Recovery = 85%  Analysis Date = 11/18/13 
 Pct Recovery = 85%  Analysis Date = 11/16/13 
 Pct Recovery = 85%  Analysis Date = 11/16/13 
 Pct Recovery = 85%  Analysis Date = 11/14/13 
 Pct Recovery = 85%  Analysis Date = 11/14/13 
 Pct Recovery = 85%  Analysis Date = 11/12/13 
 Pct Recovery = 85%  Analysis Date = 11/12/13 
 Pct Recovery = 85%  Analysis Date = 11/10/13 
 Pct Recovery = 86%  Analysis Date = 11/10/13 
 Pct Recovery = 86%  Analysis Date = 11/08/13 
 Pct Recovery = 86%  Analysis Date = 11/08/13 
 Pct Recovery = 86%  Analysis Date = 11/06/13 
 Pct Recovery = 86%  Analysis Date = 11/06/13 
 Pct Recovery = 86%  Analysis Date = 11/04/13 
 Pct Recovery = 87%  Analysis Date = 11/04/13 
 Pct Recovery = 87%  Analysis Date = 11/02/13 
 Pct Recovery = 87%  Analysis Date = 11/02/13 
 Pct Recovery = 87%  Analysis Date = 10/31/13 
 Pct Recovery = 87%  Analysis Date = 10/31/13 
 Pct Recovery = 87%  Analysis Date = 10/29/13 
 Pct Recovery = 87%  Analysis Date = 10/29/13 
 Pct Recovery = 87%  Analysis Date = 10/27/13 
 Pct Recovery = 87%  Analysis Date = 10/27/13 
 Pct Recovery = 87%  Analysis Date = 10/25/13 
 Pct Recovery = 87%  Analysis Date = 10/25/13 
 Pct Recovery = 87%  Analysis Date = 10/23/13 
 Pct Recovery = 87%  Analysis Date = 10/23/13 
 Pct Recovery = 87%  Analysis Date = 10/21/13 
 Pct Recovery = 88%  Analysis Date = 10/21/13 
 Pct Recovery = 88%  Analysis Date = 10/19/13 
 Pct Recovery = 88%  Analysis Date = 10/19/13 
 Pct Recovery = 88%  Analysis Date = 10/17/13 
 Pct Recovery = 88%  Analysis Date = 10/17/13 
 Pct Recovery = 88%  Analysis Date = 10/15/13 
 Pct Recovery = 88%  Analysis Date = 10/15/13 
 Pct Recovery = 88%  Analysis Date = 10/13/13 
 Pct Recovery = 88%  Analysis Date = 10/13/13 
 Pct Recovery = 88%  Analysis Date = 10/11/13 
 Pct Recovery = 88%  Analysis Date = 10/11/13 
 Pct Recovery = 88%  Analysis Date = 10/09/13 
 Pct Recovery = 88%  Analysis Date = 10/09/13 
 Pct Recovery = 88%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/07/13 
 Pct Recovery = 88%  Analysis Date = 10/05/13 
 Pct Recovery = 88%  Analysis Date = 10/05/13 
 Pct Recovery = 88%  Analysis Date = 10/03/13 
 Pct Recovery = 88%  Analysis Date = 10/03/13 
 Pct Recovery = 88%  Analysis Date = 10/01/13 
 Pct Recovery = 88%  Analysis Date = 10/01/13 
 Pct Recovery = 88%  Analysis Date = 09/29/13 
 Pct Recovery = 88%  Analysis Date = 09/29/13 
 Pct Recovery = 88%  Analysis Date = 09/27/13 
 Pct Recovery = 88%  Analysis Date = 09/27/13 
 Pct Recovery = 88%  Analysis Date = 09/25/13 
 Pct Recovery = 88%  Analysis Date = 09/25/13 
 Pct Recovery = 88%  Analysis Date = 09/23/13 
 Pct Recovery = 88%  Analysis Date = 09/23/13 
 Pct Recovery = 88%  Analysis Date = 09/21/13 
 Pct Recovery = 88%  Analysis Date = 09/21/13 
 Pct Recovery = 88%  Analysis Date = 09/18/13 
 Pct Recovery = 88%  Analysis Date = 09/18/13 
 Pct Recovery = 88%  Analysis Date = 09/16/13 
 Pct Recovery = 88%  Analysis Date = 09/16/13 
 Pct Recovery = 88%  Analysis Date = 09/14/13 
 Pct Recovery = 88%  Analysis Date = 09/14/13 
 Pct Recovery = 88%  Analysis Date = 09/12/13 
 Pct Recovery = 88%  Analysis Date = 09/12/13 
 Pct Recovery = 88%  Analysis Date = 09/10/13 
 Pct Recovery = 88%  Analysis Date = 09/10/13 
 Pct Recovery = 88%  Analysis Date = 09/08/13 
 Pct Recovery = 88%  Analysis Date = 09/08/13 
 Pct Recovery = 88%  Analysis Date = 09/06/13 
 Pct Recovery = 88%  Analysis Date = 09/06/13 
 Pct Recovery = 88%  Analysis Date = 09/04/13 
 Pct Recovery = 88%  Analysis Date = 09/04/13 
 Pct Recovery = 88%  Analysis Date = 09/02/13 
 Pct Recovery = 88%  Analysis Date = 09/02/13 
 Pct Recovery = 88%  Analysis Date = 08/31/13 
 Pct Recovery = 88%  Analysis Date = 08/31/13 
 Pct Recovery = 88%  Analysis Date = 08/29/13 
 Pct Recovery = 88%  Analysis Date = 08/29/13 
 Pct Recovery = 88%  Analysis Date = 08/27/13 
 Pct Recovery = 88%  Analysis Date = 08/27/13 
 Pct Recovery = 88%  Analysis Date = 08/25/13 
 Pct Recovery = 88%  Analysis Date = 08/25/13 
 Pct Recovery = 88%  Analysis Date = 08/23/13 
 Pct Recovery = 88%  Analysis Date = 08/23/13 
 Pct Recovery = 88%  Analysis Date = 08/21/13 
 Pct Recovery = 89%  Analysis Date = 08/21/13 
 Pct Recovery = 89%  Analysis Date = 08/19/13 
 Pct Recovery = 89%  Analysis Date = 08/19/13 
 Pct Recovery = 89%  Analysis Date = 08/17/13 
 Pct Recovery = 89%  Analysis Date = 08/17/13 
 Pct Recovery = 89%  Analysis Date = 08/15/13 
 Pct Recovery = 89%  Analysis Date = 08/15/13 
 Pct Recovery = 89%  Analysis Date = 08/13/13 
 Pct Recovery = 89%  Analysis Date = 08/13/13 
 Pct Recovery = 89%  Analysis Date = 08/11/13 
 Pct Recovery = 89%  Analysis Date = 08/11/13 
 Pct Recovery = 89%  Analysis Date = 08/09/13 
 Pct Recovery = 89%  Analysis Date = 08/09/13 
 Pct Recovery = 89%  Analysis Date = 08/07/13 
 Pct Recovery = 89%  Analysis Date = 08/07/13 
 Pct Recovery = 89%  Analysis Date = 08/05/13 
 Pct Recovery = 89%  Analysis Date = 08/05/13 
 Pct Recovery = 89%  Analysis Date = 08/03/13 
 Pct Recovery = 89%  Analysis Date = 08/03/13 
 Pct Recovery = 89%  Analysis Date = 08/01/13 
 Pct Recovery = 89%  Analysis Date = 08/01/13 
 Pct Recovery = 89%  Analysis Date = 07/30/13 
 Pct Recovery = 88%  Analysis Date = 07/30/13 
 Pct Recovery = 88%  Analysis Date = 07/28/13 
 Pct Recovery = 88%  Analysis Date = 07/28/13 
 Pct Recovery = 88%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/26/13 
 Pct Recovery = 88%  Analysis Date = 07/24/13 
 Pct Recovery = 87%  Analysis Date = 07/24/13 
 Pct Recovery = 87%  Analysis Date = 07/22/13 
 Pct Recovery = 87%  Analysis Date = 07/22/13 
 Pct Recovery = 87%  Analysis Date = 07/20/13 
 Pct Recovery = 87%  Analysis Date = 07/20/13 
 Pct Recovery = 87%  Analysis Date = 07/18/13 
 Pct Recovery = 86%  Analysis Date = 07/18/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 86%  Analysis Date = 07/16/13 
 Pct Recovery = 86%  Analysis Date = 07/14/13 
 Pct Recovery = 86%  Analysis Date = 07/14/13 
 Pct Recovery = 86%  Analysis Date = 07/11/13 
 Pct Recovery = 85%  Analysis Date = 07/11/13 
 Pct Recovery = 85%  Analysis Date = 07/09/13 
 Pct Recovery = 85%  Analysis Date = 07/09/13 
 Pct Recovery = 85%  Analysis Date = 07/07/13 
 Pct Recovery = 85%  Analysis Date = 07/07/13 
 Pct Recovery = 85%  Analysis Date = 07/05/13 
 Pct Recovery = 85%  Analysis Date = 07/05/13 
 Pct Recovery = 85%  Analysis Date = 07/03/13 
 Pct Recovery = 84%  Analysis Date = 07/03/13 
 Pct Recovery = 84%  Analysis Date = 07/01/13 
 Pct Recovery = 84%  Analysis Date = 07/01/13 
 Pct Recovery = 84%  Analysis Date = 06/29/13 
 Pct Recovery = 84%  Analysis Date = 06/29/13 
 Pct Recovery = 84%  Analysis Date = 06/27/13 
 Pct Recovery = 83%  Analysis Date = 06/27/13 
 Pct Recovery = 83%  Analysis Date = 06/25/13 
 Pct Recovery = 83%  Analysis Date = 06/25/13 
 Pct Recovery = 83%  Analysis Date = 06/23/13 
 Pct Recovery = 83%  Analysis Date = 06/23/13 
 Pct Recovery = 83%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/21/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/19/13 
 Pct Recovery = 82%  Analysis Date = 06/17/13 
 Pct Recovery = 82%  Analysis Date = 06/17/13 
 Pct Recovery = 82%  Analysis Date = 06/15/13 
 Pct Recovery = 81%  Analysis Date = 06/15/13 
 Pct Recovery = 81%  Analysis Date = 06/13/13 
 Pct Recovery = 81%  Analysis Date = 06/13/13 
 Pct Recovery = 81%  Analysis Date = 06/11/13 
 Pct Recovery = 81%  Analysis Date = 06/11/13 
 Pct Recovery = 81%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/09/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 78%  Analysis Date = 05/28/13 
 Pct Recovery = 78%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 77%  Analysis Date = 05/18/13 
 Pct Recovery = 77%  Analysis Date = 05/18/13 
 Pct Recovery = 77%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/12/13 
 Pct Recovery = 76%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/08/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 75%  Analysis Date = 05/05/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 Pct Recovery = 75%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 05/01/13 
 Pct Recovery = 74%  Analysis Date = 04/29/13 
 Pct Recovery = 74%  Analysis Date = 04/29/13 
 Pct Recovery = 74%  Analysis Date = 04/27/13 
 Pct Recovery = 74%  Analysis Date = 04/27/13 
 Pct Recovery = 74%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/21/13 
 Pct Recovery = 73%  Analysis Date = 04/21/13 
 Pct Recovery = 73%  Analysis Date = 04/19/13 
 Pct Recovery = 73%  Analysis Date = 04/19/13 
 Pct Recovery = 73%  Analysis Date = 04/17/13 
 Pct Recovery = 73%  Analysis Date = 04/17/13 
 Pct Recovery = 73%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/15/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/13/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/09/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/07/13 
 Pct Recovery = 73%  Analysis Date = 04/05/13 
 Pct Recovery = 73%  Analysis Date = 04/05/13 
 Pct Recovery = 73%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/03/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 04/01/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/30/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/28/13 
 Pct Recovery = 72%  Analysis Date = 03/26/13 
 Pct Recovery = 72%  Analysis Date = 03/26/13 
 Pct Recovery = 72%  Analysis Date = 03/24/13 
 Pct Recovery = 72%  Analysis Date = 03/24/13 
 Pct Recovery = 72%  Analysis Date = 03/22/13 
 Pct Recovery = 72%  Analysis Date = 03/22/13 
 Pct Recovery = 72%  Analysis Date = 03/20/13 
 Pct Recovery = 72%  Analysis Date = 03/20/13 
 Pct Recovery = 72%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/18/13 
 Pct Recovery = 71%  Analysis Date = 03/16/13 
 Pct Recovery = 71%  Analysis Date = 03/16/13 
 Pct Recovery = 71%  Analysis Date = 03/14/13 
 Pct Recovery = 71%  Analysis Date = 03/14/13 
 Pct Recovery = 71%  Analysis Date = 03/12/13 
 Pct Recovery = 71%  Analysis Date = 03/12/13 
 Pct Recovery = 71%  Analysis Date = 03/10/13 
 Pct Recovery = 71%  Analysis Date = 03/10/13 
 Pct Recovery = 71%  Analysis Date = 03/08/13 
 Pct Recovery = 71%  Analysis Date = 03/08/13 
 Pct Recovery = 71%  Analysis Date = 03/06/13 
 Pct Recovery = 71%  Analysis Date = 03/06/13 
 Pct Recovery = 71%  Analysis Date = 03/04/13 
 Pct Recovery = 71%  Analysis Date = 03/04/13 
 Pct Recovery = 71%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 03/02/13 
 Pct Recovery = 70%  Analysis Date = 02/28/13 
 Pct Recovery = 70%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFAMETHOXAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 12 76% 18% 76% 16%
Total 12 76% 18% 76% 16%

Sample Statistics
SULFAMETHOXAZOLE

Characteristic N % % Basis
Plotted 12 86% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 2 14% 2 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
TAMOXIFEN
METHOD: LC9017 , TESTIDCODE: 68015LCM56

 Analysis Date = 01/24/13 
 SpikeMix = Abs 053112: 40 µl & ERA 0507-12-06.2: 40 µl 
 Pct Recovery = 7%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 14%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TAMOXIFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 10% 5% 10% 6%
Total 2 10% 5% 10% 6%

Sample Statistics
TAMOXIFEN

Characteristic N % % Basis
Plotted 2 22% Spiked
Estimated Values 2 22% Spiked
Deleted Values 12 38% Spiked + Not Spiked
Spiked, Censored 2 22% Spiked
Spiked 14 .  
False Negatives 5 56% 5 out of 9
Not Spiked 18 .  
False Positives 0 0% 0 out of 11

OBSP Determination:
TEMAZEPAM
METHOD: LC9017 , TESTIDCODE: 67471LCM56

 Analysis Date = 05/02/13 
 SpikeMix = Abs 060112: 40 µl 
 Pct Recovery = 70%  Analysis Date = 01/24/13 
 SpikeMix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl 
 Pct Recovery = 82%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 54%  Analysis Date = 03/27/13 
 SpikeMix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 75%  Analysis Date = 01/16/14 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 70%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/18/13 
 SpikeMix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 54%  Analysis Date = 04/10/14 
 Pct Recovery = 55%  Analysis Date = 04/07/14 
 Pct Recovery = 55%  Analysis Date = 04/07/14 
 Pct Recovery = 55%  Analysis Date = 04/05/14 
 Pct Recovery = 56%  Analysis Date = 04/05/14 
 Pct Recovery = 56%  Analysis Date = 04/03/14 
 Pct Recovery = 56%  Analysis Date = 04/03/14 
 Pct Recovery = 56%  Analysis Date = 04/01/14 
 Pct Recovery = 56%  Analysis Date = 04/01/14 
 Pct Recovery = 56%  Analysis Date = 03/29/14 
 Pct Recovery = 57%  Analysis Date = 03/29/14 
 Pct Recovery = 57%  Analysis Date = 03/27/14 
 Pct Recovery = 57%  Analysis Date = 03/27/14 
 Pct Recovery = 57%  Analysis Date = 03/25/14 
 Pct Recovery = 57%  Analysis Date = 03/25/14 
 Pct Recovery = 57%  Analysis Date = 03/23/14 
 Pct Recovery = 58%  Analysis Date = 03/23/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/18/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 58%  Analysis Date = 03/14/14 
 Pct Recovery = 59%  Analysis Date = 03/14/14 
 Pct Recovery = 59%  Analysis Date = 03/12/14 
 Pct Recovery = 59%  Analysis Date = 03/12/14 
 Pct Recovery = 59%  Analysis Date = 03/10/14 
 Pct Recovery = 59%  Analysis Date = 03/10/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 60%  Analysis Date = 03/07/14 
 Pct Recovery = 60%  Analysis Date = 03/05/14 
 Pct Recovery = 60%  Analysis Date = 03/05/14 
 Pct Recovery = 60%  Analysis Date = 03/03/14 
 Pct Recovery = 60%  Analysis Date = 03/03/14 
 Pct Recovery = 60%  Analysis Date = 03/01/14 
 Pct Recovery = 61%  Analysis Date = 03/01/14 
 Pct Recovery = 61%  Analysis Date = 02/27/14 
 Pct Recovery = 61%  Analysis Date = 02/27/14 
 Pct Recovery = 61%  Analysis Date = 02/24/14 
 Pct Recovery = 61%  Analysis Date = 02/24/14 
 Pct Recovery = 61%  Analysis Date = 02/22/14 
 Pct Recovery = 62%  Analysis Date = 02/22/14 
 Pct Recovery = 62%  Analysis Date = 02/20/14 
 Pct Recovery = 62%  Analysis Date = 02/20/14 
 Pct Recovery = 62%  Analysis Date = 02/18/14 
 Pct Recovery = 62%  Analysis Date = 02/18/14 
 Pct Recovery = 62%  Analysis Date = 02/16/14 
 Pct Recovery = 62%  Analysis Date = 02/16/14 
 Pct Recovery = 62%  Analysis Date = 02/13/14 
 Pct Recovery = 63%  Analysis Date = 02/13/14 
 Pct Recovery = 63%  Analysis Date = 02/11/14 
 Pct Recovery = 63%  Analysis Date = 02/11/14 
 Pct Recovery = 63%  Analysis Date = 02/09/14 
 Pct Recovery = 63%  Analysis Date = 02/09/14 
 Pct Recovery = 63%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/07/14 
 Pct Recovery = 64%  Analysis Date = 02/05/14 
 Pct Recovery = 64%  Analysis Date = 02/05/14 
 Pct Recovery = 64%  Analysis Date = 02/02/14 
 Pct Recovery = 64%  Analysis Date = 02/02/14 
 Pct Recovery = 64%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/31/14 
 Pct Recovery = 65%  Analysis Date = 01/29/14 
 Pct Recovery = 65%  Analysis Date = 01/29/14 
 Pct Recovery = 65%  Analysis Date = 01/27/14 
 Pct Recovery = 65%  Analysis Date = 01/27/14 
 Pct Recovery = 65%  Analysis Date = 01/25/14 
 Pct Recovery = 65%  Analysis Date = 01/25/14 
 Pct Recovery = 65%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/22/14 
 Pct Recovery = 66%  Analysis Date = 01/20/14 
 Pct Recovery = 66%  Analysis Date = 01/20/14 
 Pct Recovery = 66%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 Pct Recovery = 67%  Analysis Date = 01/16/14 
 Pct Recovery = 67%  Analysis Date = 01/14/14 
 Pct Recovery = 67%  Analysis Date = 01/14/14 
 Pct Recovery = 67%  Analysis Date = 01/11/14 
 Pct Recovery = 67%  Analysis Date = 01/11/14 
 Pct Recovery = 67%  Analysis Date = 01/09/14 
 Pct Recovery = 67%  Analysis Date = 01/09/14 
 Pct Recovery = 67%  Analysis Date = 01/07/14 
 Pct Recovery = 67%  Analysis Date = 01/07/14 
 Pct Recovery = 67%  Analysis Date = 01/05/14 
 Pct Recovery = 67%  Analysis Date = 01/05/14 
 Pct Recovery = 67%  Analysis Date = 01/02/14 
 Pct Recovery = 67%  Analysis Date = 01/02/14 
 Pct Recovery = 67%  Analysis Date = 12/31/13 
 Pct Recovery = 67%  Analysis Date = 12/31/13 
 Pct Recovery = 67%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/29/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/27/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/25/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/22/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/20/13 
 Pct Recovery = 67%  Analysis Date = 12/18/13 
 Pct Recovery = 67%  Analysis Date = 12/18/13 
 Pct Recovery = 67%  Analysis Date = 12/16/13 
 Pct Recovery = 67%  Analysis Date = 12/16/13 
 Pct Recovery = 67%  Analysis Date = 12/14/13 
 Pct Recovery = 67%  Analysis Date = 12/14/13 
 Pct Recovery = 67%  Analysis Date = 12/11/13 
 Pct Recovery = 67%  Analysis Date = 12/11/13 
 Pct Recovery = 67%  Analysis Date = 12/09/13 
 Pct Recovery = 67%  Analysis Date = 12/09/13 
 Pct Recovery = 67%  Analysis Date = 12/07/13 
 Pct Recovery = 67%  Analysis Date = 12/07/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/05/13 
 Pct Recovery = 67%  Analysis Date = 12/03/13 
 Pct Recovery = 67%  Analysis Date = 12/03/13 
 Pct Recovery = 67%  Analysis Date = 11/30/13 
 Pct Recovery = 67%  Analysis Date = 11/30/13 
 Pct Recovery = 67%  Analysis Date = 11/28/13 
 Pct Recovery = 66%  Analysis Date = 11/28/13 
 Pct Recovery = 66%  Analysis Date = 11/26/13 
 Pct Recovery = 66%  Analysis Date = 11/26/13 
 Pct Recovery = 66%  Analysis Date = 11/24/13 
 Pct Recovery = 66%  Analysis Date = 11/24/13 
 Pct Recovery = 66%  Analysis Date = 11/22/13 
 Pct Recovery = 66%  Analysis Date = 11/22/13 
 Pct Recovery = 66%  Analysis Date = 11/19/13 
 Pct Recovery = 66%  Analysis Date = 11/19/13 
 Pct Recovery = 66%  Analysis Date = 11/17/13 
 Pct Recovery = 66%  Analysis Date = 11/17/13 
 Pct Recovery = 66%  Analysis Date = 11/15/13 
 Pct Recovery = 66%  Analysis Date = 11/15/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/13/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/11/13 
 Pct Recovery = 66%  Analysis Date = 11/08/13 
 Pct Recovery = 66%  Analysis Date = 11/08/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/06/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/04/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 11/02/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/31/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/28/13 
 Pct Recovery = 66%  Analysis Date = 10/26/13 
 Pct Recovery = 66%  Analysis Date = 10/26/13 
 Pct Recovery = 66%  Analysis Date = 10/24/13 
 Pct Recovery = 66%  Analysis Date = 10/24/13 
 Pct Recovery = 66%  Analysis Date = 10/22/13 
 Pct Recovery = 66%  Analysis Date = 10/22/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/20/13 
 Pct Recovery = 66%  Analysis Date = 10/17/13 
 Pct Recovery = 66%  Analysis Date = 10/17/13 
 Pct Recovery = 66%  Analysis Date = 10/15/13 
 Pct Recovery = 65%  Analysis Date = 10/15/13 
 Pct Recovery = 65%  Analysis Date = 10/13/13 
 Pct Recovery = 65%  Analysis Date = 10/13/13 
 Pct Recovery = 65%  Analysis Date = 10/11/13 
 Pct Recovery = 65%  Analysis Date = 10/11/13 
 Pct Recovery = 65%  Analysis Date = 10/08/13 
 Pct Recovery = 65%  Analysis Date = 10/08/13 
 Pct Recovery = 65%  Analysis Date = 10/06/13 
 Pct Recovery = 65%  Analysis Date = 10/06/13 
 Pct Recovery = 65%  Analysis Date = 10/04/13 
 Pct Recovery = 65%  Analysis Date = 10/04/13 
 Pct Recovery = 65%  Analysis Date = 10/02/13 
 Pct Recovery = 65%  Analysis Date = 10/02/13 
 Pct Recovery = 65%  Analysis Date = 09/30/13 
 Pct Recovery = 64%  Analysis Date = 09/30/13 
 Pct Recovery = 64%  Analysis Date = 09/27/13 
 Pct Recovery = 64%  Analysis Date = 09/27/13 
 Pct Recovery = 64%  Analysis Date = 09/25/13 
 Pct Recovery = 64%  Analysis Date = 09/25/13 
 Pct Recovery = 64%  Analysis Date = 09/23/13 
 Pct Recovery = 64%  Analysis Date = 09/23/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/19/13 
 Pct Recovery = 64%  Analysis Date = 09/16/13 
 Pct Recovery = 64%  Analysis Date = 09/16/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/12/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/10/13 
 Pct Recovery = 63%  Analysis Date = 09/08/13 
 Pct Recovery = 63%  Analysis Date = 09/08/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/05/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/03/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 09/01/13 
 Pct Recovery = 63%  Analysis Date = 08/30/13 
 Pct Recovery = 62%  Analysis Date = 08/30/13 
 Pct Recovery = 62%  Analysis Date = 08/28/13 
 Pct Recovery = 62%  Analysis Date = 08/28/13 
 Pct Recovery = 62%  Analysis Date = 08/25/13 
 Pct Recovery = 62%  Analysis Date = 08/25/13 
 Pct Recovery = 62%  Analysis Date = 08/23/13 
 Pct Recovery = 62%  Analysis Date = 08/23/13 
 Pct Recovery = 62%  Analysis Date = 08/21/13 
 Pct Recovery = 62%  Analysis Date = 08/21/13 
 Pct Recovery = 62%  Analysis Date = 08/19/13 
 Pct Recovery = 62%  Analysis Date = 08/19/13 
 Pct Recovery = 62%  Analysis Date = 08/17/13 
 Pct Recovery = 62%  Analysis Date = 08/17/13 
 Pct Recovery = 62%  Analysis Date = 08/14/13 
 Pct Recovery = 62%  Analysis Date = 08/14/13 
 Pct Recovery = 62%  Analysis Date = 08/12/13 
 Pct Recovery = 62%  Analysis Date = 08/12/13 
 Pct Recovery = 62%  Analysis Date = 08/10/13 
 Pct Recovery = 62%  Analysis Date = 08/10/13 
 Pct Recovery = 62%  Analysis Date = 08/08/13 
 Pct Recovery = 62%  Analysis Date = 08/08/13 
 Pct Recovery = 62%  Analysis Date = 08/06/13 
 Pct Recovery = 62%  Analysis Date = 08/06/13 
 Pct Recovery = 62%  Analysis Date = 08/03/13 
 Pct Recovery = 63%  Analysis Date = 08/03/13 
 Pct Recovery = 63%  Analysis Date = 08/01/13 
 Pct Recovery = 63%  Analysis Date = 08/01/13 
 Pct Recovery = 63%  Analysis Date = 07/30/13 
 Pct Recovery = 63%  Analysis Date = 07/30/13 
 Pct Recovery = 63%  Analysis Date = 07/28/13 
 Pct Recovery = 63%  Analysis Date = 07/28/13 
 Pct Recovery = 63%  Analysis Date = 07/26/13 
 Pct Recovery = 63%  Analysis Date = 07/26/13 
 Pct Recovery = 63%  Analysis Date = 07/23/13 
 Pct Recovery = 63%  Analysis Date = 07/23/13 
 Pct Recovery = 63%  Analysis Date = 07/21/13 
 Pct Recovery = 64%  Analysis Date = 07/21/13 
 Pct Recovery = 64%  Analysis Date = 07/19/13 
 Pct Recovery = 64%  Analysis Date = 07/19/13 
 Pct Recovery = 64%  Analysis Date = 07/17/13 
 Pct Recovery = 64%  Analysis Date = 07/17/13 
 Pct Recovery = 64%  Analysis Date = 07/14/13 
 Pct Recovery = 64%  Analysis Date = 07/14/13 
 Pct Recovery = 64%  Analysis Date = 07/12/13 
 Pct Recovery = 64%  Analysis Date = 07/12/13 
 Pct Recovery = 64%  Analysis Date = 07/10/13 
 Pct Recovery = 64%  Analysis Date = 07/10/13 
 Pct Recovery = 64%  Analysis Date = 07/08/13 
 Pct Recovery = 65%  Analysis Date = 07/08/13 
 Pct Recovery = 65%  Analysis Date = 07/06/13 
 Pct Recovery = 65%  Analysis Date = 07/06/13 
 Pct Recovery = 65%  Analysis Date = 07/03/13 
 Pct Recovery = 65%  Analysis Date = 07/03/13 
 Pct Recovery = 65%  Analysis Date = 07/01/13 
 Pct Recovery = 65%  Analysis Date = 07/01/13 
 Pct Recovery = 65%  Analysis Date = 06/29/13 
 Pct Recovery = 65%  Analysis Date = 06/29/13 
 Pct Recovery = 65%  Analysis Date = 06/27/13 
 Pct Recovery = 65%  Analysis Date = 06/27/13 
 Pct Recovery = 65%  Analysis Date = 06/25/13 
 Pct Recovery = 66%  Analysis Date = 06/25/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/20/13 
 Pct Recovery = 66%  Analysis Date = 06/20/13 
 Pct Recovery = 66%  Analysis Date = 06/18/13 
 Pct Recovery = 66%  Analysis Date = 06/18/13 
 Pct Recovery = 66%  Analysis Date = 06/16/13 
 Pct Recovery = 66%  Analysis Date = 06/16/13 
 Pct Recovery = 66%  Analysis Date = 06/14/13 
 Pct Recovery = 66%  Analysis Date = 06/14/13 
 Pct Recovery = 66%  Analysis Date = 06/11/13 
 Pct Recovery = 67%  Analysis Date = 06/11/13 
 Pct Recovery = 67%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/09/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/07/13 
 Pct Recovery = 67%  Analysis Date = 06/05/13 
 Pct Recovery = 67%  Analysis Date = 06/05/13 
 Pct Recovery = 67%  Analysis Date = 06/03/13 
 Pct Recovery = 67%  Analysis Date = 06/03/13 
 Pct Recovery = 67%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/31/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/29/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/27/13 
 Pct Recovery = 68%  Analysis Date = 05/25/13 
 Pct Recovery = 68%  Analysis Date = 05/25/13 
 Pct Recovery = 68%  Analysis Date = 05/23/13 
 Pct Recovery = 68%  Analysis Date = 05/23/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/20/13 
 Pct Recovery = 68%  Analysis Date = 05/18/13 
 Pct Recovery = 69%  Analysis Date = 05/18/13 
 Pct Recovery = 69%  Analysis Date = 05/16/13 
 Pct Recovery = 69%  Analysis Date = 05/16/13 
 Pct Recovery = 69%  Analysis Date = 05/14/13 
 Pct Recovery = 69%  Analysis Date = 05/14/13 
 Pct Recovery = 69%  Analysis Date = 05/12/13 
 Pct Recovery = 69%  Analysis Date = 05/12/13 
 Pct Recovery = 69%  Analysis Date = 05/09/13 
 Pct Recovery = 69%  Analysis Date = 05/09/13 
 Pct Recovery = 69%  Analysis Date = 05/07/13 
 Pct Recovery = 69%  Analysis Date = 05/07/13 
 Pct Recovery = 69%  Analysis Date = 05/05/13 
 Pct Recovery = 70%  Analysis Date = 05/05/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 05/01/13 
 Pct Recovery = 70%  Analysis Date = 04/28/13 
 Pct Recovery = 70%  Analysis Date = 04/28/13 
 Pct Recovery = 70%  Analysis Date = 04/26/13 
 Pct Recovery = 71%  Analysis Date = 04/26/13 
 Pct Recovery = 71%  Analysis Date = 04/24/13 
 Pct Recovery = 71%  Analysis Date = 04/24/13 
 Pct Recovery = 71%  Analysis Date = 04/22/13 
 Pct Recovery = 71%  Analysis Date = 04/22/13 
 Pct Recovery = 71%  Analysis Date = 04/19/13 
 Pct Recovery = 71%  Analysis Date = 04/19/13 
 Pct Recovery = 71%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/17/13 
 Pct Recovery = 72%  Analysis Date = 04/15/13 
 Pct Recovery = 72%  Analysis Date = 04/15/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/13/13 
 Pct Recovery = 72%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/11/13 
 Pct Recovery = 73%  Analysis Date = 04/08/13 
 Pct Recovery = 73%  Analysis Date = 04/08/13 
 Pct Recovery = 73%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/06/13 
 Pct Recovery = 73%  Analysis Date = 04/04/13 
 Pct Recovery = 74%  Analysis Date = 04/04/13 
 Pct Recovery = 74%  Analysis Date = 04/02/13 
 Pct Recovery = 74%  Analysis Date = 04/02/13 
 Pct Recovery = 74%  Analysis Date = 03/31/13 
 Pct Recovery = 74%  Analysis Date = 03/31/13 
 Pct Recovery = 74%  Analysis Date = 03/28/13 
 Pct Recovery = 74%  Analysis Date = 03/28/13 
 Pct Recovery = 74%  Analysis Date = 03/26/13 
 Pct Recovery = 75%  Analysis Date = 03/26/13 
 Pct Recovery = 75%  Analysis Date = 03/24/13 
 Pct Recovery = 75%  Analysis Date = 03/24/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 76%  Analysis Date = 03/20/13 
 Pct Recovery = 76%  Analysis Date = 03/17/13 
 Pct Recovery = 76%  Analysis Date = 03/17/13 
 Pct Recovery = 76%  Analysis Date = 03/15/13 
 Pct Recovery = 76%  Analysis Date = 03/15/13 
 Pct Recovery = 76%  Analysis Date = 03/13/13 
 Pct Recovery = 76%  Analysis Date = 03/13/13 
 Pct Recovery = 76%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/11/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/09/13 
 Pct Recovery = 77%  Analysis Date = 03/06/13 
 Pct Recovery = 77%  Analysis Date = 03/06/13 
 Pct Recovery = 77%  Analysis Date = 03/04/13 
 Pct Recovery = 78%  Analysis Date = 03/04/13 
 Pct Recovery = 78%  Analysis Date = 03/02/13 
 Pct Recovery = 78%  Analysis Date = 03/02/13 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/23/13 
 Pct Recovery = 79%  Analysis Date = 02/23/13 
 Pct Recovery = 79%  Analysis Date = 02/21/13 
 Pct Recovery = 79%  Analysis Date = 02/21/13 
 Pct Recovery = 79%  Analysis Date = 02/19/13 
 Pct Recovery = 79%  Analysis Date = 02/19/13 
 Pct Recovery = 79%  Analysis Date = 02/17/13 
 Pct Recovery = 79%  Analysis Date = 02/17/13 
 Pct Recovery = 79%  Analysis Date = 02/15/13 
 Pct Recovery = 80%  Analysis Date = 02/15/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 80%  Analysis Date = 02/12/13 
 Pct Recovery = 80%  Analysis Date = 02/10/13 
 Pct Recovery = 80%  Analysis Date = 02/10/13 
 Pct Recovery = 80%  Analysis Date = 02/08/13 
 Pct Recovery = 81%  Analysis Date = 02/08/13 
 Pct Recovery = 81%  Analysis Date = 02/06/13 
 Pct Recovery = 81%  Analysis Date = 02/06/13 
 Pct Recovery = 81%  Analysis Date = 02/04/13 
 Pct Recovery = 81%  Analysis Date = 02/04/13 
 Pct Recovery = 81%  Analysis Date = 02/01/13 
 Pct Recovery = 81%  Analysis Date = 02/01/13 
 Pct Recovery = 81%  Analysis Date = 01/30/13 
 Pct Recovery = 82%  Analysis Date = 01/30/13 
 Pct Recovery = 82%  Analysis Date = 01/28/13 
 Pct Recovery = 82%  Analysis Date = 01/28/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/26/13 
 Pct Recovery = 82%  Analysis Date = 01/24/13 
 Pct Recovery = 83%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEMAZEPAM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 7 68% 11% 70% 16%
Total 7 68% 11% 70% 16%

Sample Statistics
TEMAZEPAM

Characteristic N % % Basis
Plotted 7 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 7 .  
False Negatives 0 0% 0 out of 7
Not Spiked 25 .  
False Positives 1 4% 1 out of 24

OBSP Determination:
THEOPHYLLINE
METHOD: LC9017 , TESTIDCODE: 67494LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 79%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 88%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 33%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 92%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 97%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 80%  Analysis Date = 04/09/14 
 Pct Recovery = 33%  Analysis Date = 04/07/14 
 Pct Recovery = 34%  Analysis Date = 04/07/14 
 Pct Recovery = 34%  Analysis Date = 04/05/14 
 Pct Recovery = 34%  Analysis Date = 04/05/14 
 Pct Recovery = 34%  Analysis Date = 04/03/14 
 Pct Recovery = 34%  Analysis Date = 04/03/14 
 Pct Recovery = 34%  Analysis Date = 04/01/14 
 Pct Recovery = 35%  Analysis Date = 04/01/14 
 Pct Recovery = 35%  Analysis Date = 03/30/14 
 Pct Recovery = 35%  Analysis Date = 03/30/14 
 Pct Recovery = 35%  Analysis Date = 03/28/14 
 Pct Recovery = 35%  Analysis Date = 03/28/14 
 Pct Recovery = 35%  Analysis Date = 03/26/14 
 Pct Recovery = 35%  Analysis Date = 03/26/14 
 Pct Recovery = 35%  Analysis Date = 03/24/14 
 Pct Recovery = 36%  Analysis Date = 03/24/14 
 Pct Recovery = 36%  Analysis Date = 03/22/14 
 Pct Recovery = 36%  Analysis Date = 03/22/14 
 Pct Recovery = 36%  Analysis Date = 03/20/14 
 Pct Recovery = 36%  Analysis Date = 03/20/14 
 Pct Recovery = 36%  Analysis Date = 03/18/14 
 Pct Recovery = 37%  Analysis Date = 03/18/14 
 Pct Recovery = 37%  Analysis Date = 03/16/14 
 Pct Recovery = 37%  Analysis Date = 03/16/14 
 Pct Recovery = 37%  Analysis Date = 03/14/14 
 Pct Recovery = 37%  Analysis Date = 03/14/14 
 Pct Recovery = 37%  Analysis Date = 03/12/14 
 Pct Recovery = 38%  Analysis Date = 03/12/14 
 Pct Recovery = 38%  Analysis Date = 03/10/14 
 Pct Recovery = 38%  Analysis Date = 03/10/14 
 Pct Recovery = 38%  Analysis Date = 03/08/14 
 Pct Recovery = 38%  Analysis Date = 03/08/14 
 Pct Recovery = 38%  Analysis Date = 03/06/14 
 Pct Recovery = 38%  Analysis Date = 03/06/14 
 Pct Recovery = 38%  Analysis Date = 03/04/14 
 Pct Recovery = 39%  Analysis Date = 03/04/14 
 Pct Recovery = 39%  Analysis Date = 03/02/14 
 Pct Recovery = 39%  Analysis Date = 03/02/14 
 Pct Recovery = 39%  Analysis Date = 02/28/14 
 Pct Recovery = 39%  Analysis Date = 02/28/14 
 Pct Recovery = 39%  Analysis Date = 02/26/14 
 Pct Recovery = 40%  Analysis Date = 02/26/14 
 Pct Recovery = 40%  Analysis Date = 02/24/14 
 Pct Recovery = 40%  Analysis Date = 02/24/14 
 Pct Recovery = 40%  Analysis Date = 02/22/14 
 Pct Recovery = 40%  Analysis Date = 02/22/14 
 Pct Recovery = 40%  Analysis Date = 02/20/14 
 Pct Recovery = 41%  Analysis Date = 02/20/14 
 Pct Recovery = 41%  Analysis Date = 02/18/14 
 Pct Recovery = 41%  Analysis Date = 02/18/14 
 Pct Recovery = 41%  Analysis Date = 02/16/14 
 Pct Recovery = 41%  Analysis Date = 02/16/14 
 Pct Recovery = 41%  Analysis Date = 02/14/14 
 Pct Recovery = 41%  Analysis Date = 02/14/14 
 Pct Recovery = 41%  Analysis Date = 02/12/14 
 Pct Recovery = 42%  Analysis Date = 02/12/14 
 Pct Recovery = 42%  Analysis Date = 02/10/14 
 Pct Recovery = 42%  Analysis Date = 02/10/14 
 Pct Recovery = 42%  Analysis Date = 02/08/14 
 Pct Recovery = 42%  Analysis Date = 02/08/14 
 Pct Recovery = 42%  Analysis Date = 02/06/14 
 Pct Recovery = 43%  Analysis Date = 02/06/14 
 Pct Recovery = 43%  Analysis Date = 02/04/14 
 Pct Recovery = 43%  Analysis Date = 02/04/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 02/02/14 
 Pct Recovery = 43%  Analysis Date = 01/30/14 
 Pct Recovery = 44%  Analysis Date = 01/30/14 
 Pct Recovery = 44%  Analysis Date = 01/28/14 
 Pct Recovery = 44%  Analysis Date = 01/28/14 
 Pct Recovery = 44%  Analysis Date = 01/26/14 
 Pct Recovery = 44%  Analysis Date = 01/26/14 
 Pct Recovery = 44%  Analysis Date = 01/24/14 
 Pct Recovery = 44%  Analysis Date = 01/24/14 
 Pct Recovery = 44%  Analysis Date = 01/22/14 
 Pct Recovery = 45%  Analysis Date = 01/22/14 
 Pct Recovery = 45%  Analysis Date = 01/20/14 
 Pct Recovery = 45%  Analysis Date = 01/20/14 
 Pct Recovery = 45%  Analysis Date = 01/18/14 
 Pct Recovery = 45%  Analysis Date = 01/18/14 
 Pct Recovery = 45%  Analysis Date = 01/16/14 
 Pct Recovery = 46%  Analysis Date = 01/16/14 
 Pct Recovery = 46%  Analysis Date = 01/14/14 
 Pct Recovery = 46%  Analysis Date = 01/14/14 
 Pct Recovery = 46%  Analysis Date = 01/12/14 
 Pct Recovery = 46%  Analysis Date = 01/12/14 
 Pct Recovery = 46%  Analysis Date = 01/10/14 
 Pct Recovery = 46%  Analysis Date = 01/10/14 
 Pct Recovery = 46%  Analysis Date = 01/08/14 
 Pct Recovery = 47%  Analysis Date = 01/08/14 
 Pct Recovery = 47%  Analysis Date = 01/06/14 
 Pct Recovery = 47%  Analysis Date = 01/06/14 
 Pct Recovery = 47%  Analysis Date = 01/04/14 
 Pct Recovery = 47%  Analysis Date = 01/04/14 
 Pct Recovery = 47%  Analysis Date = 01/02/14 
 Pct Recovery = 48%  Analysis Date = 01/02/14 
 Pct Recovery = 48%  Analysis Date = 12/31/13 
 Pct Recovery = 48%  Analysis Date = 12/31/13 
 Pct Recovery = 48%  Analysis Date = 12/29/13 
 Pct Recovery = 48%  Analysis Date = 12/29/13 
 Pct Recovery = 48%  Analysis Date = 12/27/13 
 Pct Recovery = 49%  Analysis Date = 12/27/13 
 Pct Recovery = 49%  Analysis Date = 12/25/13 
 Pct Recovery = 49%  Analysis Date = 12/25/13 
 Pct Recovery = 49%  Analysis Date = 12/23/13 
 Pct Recovery = 49%  Analysis Date = 12/23/13 
 Pct Recovery = 49%  Analysis Date = 12/21/13 
 Pct Recovery = 49%  Analysis Date = 12/21/13 
 Pct Recovery = 49%  Analysis Date = 12/19/13 
 Pct Recovery = 50%  Analysis Date = 12/19/13 
 Pct Recovery = 50%  Analysis Date = 12/17/13 
 Pct Recovery = 50%  Analysis Date = 12/17/13 
 Pct Recovery = 50%  Analysis Date = 12/15/13 
 Pct Recovery = 50%  Analysis Date = 12/15/13 
 Pct Recovery = 50%  Analysis Date = 12/13/13 
 Pct Recovery = 51%  Analysis Date = 12/13/13 
 Pct Recovery = 51%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/11/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/09/13 
 Pct Recovery = 51%  Analysis Date = 12/07/13 
 Pct Recovery = 52%  Analysis Date = 12/07/13 
 Pct Recovery = 52%  Analysis Date = 12/05/13 
 Pct Recovery = 52%  Analysis Date = 12/05/13 
 Pct Recovery = 52%  Analysis Date = 12/03/13 
 Pct Recovery = 52%  Analysis Date = 12/03/13 
 Pct Recovery = 52%  Analysis Date = 12/01/13 
 Pct Recovery = 52%  Analysis Date = 12/01/13 
 Pct Recovery = 52%  Analysis Date = 11/29/13 
 Pct Recovery = 53%  Analysis Date = 11/29/13 
 Pct Recovery = 53%  Analysis Date = 11/27/13 
 Pct Recovery = 53%  Analysis Date = 11/27/13 
 Pct Recovery = 53%  Analysis Date = 11/24/13 
 Pct Recovery = 53%  Analysis Date = 11/24/13 
 Pct Recovery = 53%  Analysis Date = 11/22/13 
 Pct Recovery = 54%  Analysis Date = 11/22/13 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/20/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/18/13 
 Pct Recovery = 54%  Analysis Date = 11/16/13 
 Pct Recovery = 55%  Analysis Date = 11/16/13 
 Pct Recovery = 55%  Analysis Date = 11/14/13 
 Pct Recovery = 55%  Analysis Date = 11/14/13 
 Pct Recovery = 55%  Analysis Date = 11/12/13 
 Pct Recovery = 55%  Analysis Date = 11/12/13 
 Pct Recovery = 55%  Analysis Date = 11/10/13 
 Pct Recovery = 55%  Analysis Date = 11/10/13 
 Pct Recovery = 55%  Analysis Date = 11/08/13 
 Pct Recovery = 56%  Analysis Date = 11/08/13 
 Pct Recovery = 56%  Analysis Date = 11/06/13 
 Pct Recovery = 56%  Analysis Date = 11/06/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/04/13 
 Pct Recovery = 56%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 11/02/13 
 Pct Recovery = 57%  Analysis Date = 10/31/13 
 Pct Recovery = 57%  Analysis Date = 10/31/13 
 Pct Recovery = 57%  Analysis Date = 10/29/13 
 Pct Recovery = 57%  Analysis Date = 10/29/13 
 Pct Recovery = 57%  Analysis Date = 10/27/13 
 Pct Recovery = 57%  Analysis Date = 10/27/13 
 Pct Recovery = 57%  Analysis Date = 10/25/13 
 Pct Recovery = 58%  Analysis Date = 10/25/13 
 Pct Recovery = 58%  Analysis Date = 10/23/13 
 Pct Recovery = 58%  Analysis Date = 10/23/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/21/13 
 Pct Recovery = 58%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/19/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/17/13 
 Pct Recovery = 59%  Analysis Date = 10/15/13 
 Pct Recovery = 59%  Analysis Date = 10/15/13 
 Pct Recovery = 59%  Analysis Date = 10/13/13 
 Pct Recovery = 60%  Analysis Date = 10/13/13 
 Pct Recovery = 60%  Analysis Date = 10/11/13 
 Pct Recovery = 60%  Analysis Date = 10/11/13 
 Pct Recovery = 60%  Analysis Date = 10/09/13 
 Pct Recovery = 60%  Analysis Date = 10/09/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/07/13 
 Pct Recovery = 60%  Analysis Date = 10/05/13 
 Pct Recovery = 61%  Analysis Date = 10/05/13 
 Pct Recovery = 61%  Analysis Date = 10/03/13 
 Pct Recovery = 61%  Analysis Date = 10/03/13 
 Pct Recovery = 61%  Analysis Date = 10/01/13 
 Pct Recovery = 61%  Analysis Date = 10/01/13 
 Pct Recovery = 61%  Analysis Date = 09/29/13 
 Pct Recovery = 62%  Analysis Date = 09/29/13 
 Pct Recovery = 62%  Analysis Date = 09/27/13 
 Pct Recovery = 62%  Analysis Date = 09/27/13 
 Pct Recovery = 62%  Analysis Date = 09/25/13 
 Pct Recovery = 62%  Analysis Date = 09/25/13 
 Pct Recovery = 62%  Analysis Date = 09/23/13 
 Pct Recovery = 63%  Analysis Date = 09/23/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/21/13 
 Pct Recovery = 63%  Analysis Date = 09/18/13 
 Pct Recovery = 63%  Analysis Date = 09/18/13 
 Pct Recovery = 63%  Analysis Date = 09/16/13 
 Pct Recovery = 63%  Analysis Date = 09/16/13 
 Pct Recovery = 63%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/14/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/12/13 
 Pct Recovery = 64%  Analysis Date = 09/10/13 
 Pct Recovery = 64%  Analysis Date = 09/10/13 
 Pct Recovery = 64%  Analysis Date = 09/08/13 
 Pct Recovery = 65%  Analysis Date = 09/08/13 
 Pct Recovery = 65%  Analysis Date = 09/06/13 
 Pct Recovery = 65%  Analysis Date = 09/06/13 
 Pct Recovery = 65%  Analysis Date = 09/04/13 
 Pct Recovery = 65%  Analysis Date = 09/04/13 
 Pct Recovery = 65%  Analysis Date = 09/02/13 
 Pct Recovery = 65%  Analysis Date = 09/02/13 
 Pct Recovery = 65%  Analysis Date = 08/31/13 
 Pct Recovery = 66%  Analysis Date = 08/31/13 
 Pct Recovery = 66%  Analysis Date = 08/29/13 
 Pct Recovery = 66%  Analysis Date = 08/29/13 
 Pct Recovery = 66%  Analysis Date = 08/27/13 
 Pct Recovery = 66%  Analysis Date = 08/27/13 
 Pct Recovery = 66%  Analysis Date = 08/25/13 
 Pct Recovery = 67%  Analysis Date = 08/25/13 
 Pct Recovery = 67%  Analysis Date = 08/23/13 
 Pct Recovery = 67%  Analysis Date = 08/23/13 
 Pct Recovery = 67%  Analysis Date = 08/21/13 
 Pct Recovery = 67%  Analysis Date = 08/21/13 
 Pct Recovery = 67%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/17/13 
 Pct Recovery = 68%  Analysis Date = 08/17/13 
 Pct Recovery = 68%  Analysis Date = 08/15/13 
 Pct Recovery = 68%  Analysis Date = 08/15/13 
 Pct Recovery = 68%  Analysis Date = 08/13/13 
 Pct Recovery = 68%  Analysis Date = 08/13/13 
 Pct Recovery = 68%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/11/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/09/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/07/13 
 Pct Recovery = 69%  Analysis Date = 08/05/13 
 Pct Recovery = 70%  Analysis Date = 08/05/13 
 Pct Recovery = 70%  Analysis Date = 08/03/13 
 Pct Recovery = 70%  Analysis Date = 08/03/13 
 Pct Recovery = 70%  Analysis Date = 08/01/13 
 Pct Recovery = 70%  Analysis Date = 08/01/13 
 Pct Recovery = 70%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/30/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/28/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/26/13 
 Pct Recovery = 71%  Analysis Date = 07/24/13 
 Pct Recovery = 71%  Analysis Date = 07/24/13 
 Pct Recovery = 71%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/22/13 
 Pct Recovery = 72%  Analysis Date = 07/20/13 
 Pct Recovery = 72%  Analysis Date = 07/20/13 
 Pct Recovery = 72%  Analysis Date = 07/18/13 
 Pct Recovery = 72%  Analysis Date = 07/18/13 
 Pct Recovery = 72%  Analysis Date = 07/16/13 
 Pct Recovery = 73%  Analysis Date = 07/16/13 
 Pct Recovery = 73%  Analysis Date = 07/14/13 
 Pct Recovery = 73%  Analysis Date = 07/14/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/11/13 
 Pct Recovery = 73%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/09/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/07/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/05/13 
 Pct Recovery = 74%  Analysis Date = 07/03/13 
 Pct Recovery = 74%  Analysis Date = 07/03/13 
 Pct Recovery = 74%  Analysis Date = 07/01/13 
 Pct Recovery = 75%  Analysis Date = 07/01/13 
 Pct Recovery = 75%  Analysis Date = 06/29/13 
 Pct Recovery = 75%  Analysis Date = 06/29/13 
 Pct Recovery = 75%  Analysis Date = 06/27/13 
 Pct Recovery = 75%  Analysis Date = 06/27/13 
 Pct Recovery = 75%  Analysis Date = 06/25/13 
 Pct Recovery = 76%  Analysis Date = 06/25/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/23/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/21/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/19/13 
 Pct Recovery = 76%  Analysis Date = 06/17/13 
 Pct Recovery = 77%  Analysis Date = 06/17/13 
 Pct Recovery = 77%  Analysis Date = 06/15/13 
 Pct Recovery = 77%  Analysis Date = 06/15/13 
 Pct Recovery = 77%  Analysis Date = 06/13/13 
 Pct Recovery = 77%  Analysis Date = 06/13/13 
 Pct Recovery = 77%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/11/13 
 Pct Recovery = 78%  Analysis Date = 06/09/13 
 Pct Recovery = 78%  Analysis Date = 06/09/13 
 Pct Recovery = 78%  Analysis Date = 06/07/13 
 Pct Recovery = 78%  Analysis Date = 06/07/13 
 Pct Recovery = 78%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 06/01/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 80%  Analysis Date = 05/28/13 
 Pct Recovery = 80%  Analysis Date = 05/26/13 
 Pct Recovery = 80%  Analysis Date = 05/26/13 
 Pct Recovery = 80%  Analysis Date = 05/24/13 
 Pct Recovery = 80%  Analysis Date = 05/24/13 
 Pct Recovery = 80%  Analysis Date = 05/22/13 
 Pct Recovery = 81%  Analysis Date = 05/22/13 
 Pct Recovery = 81%  Analysis Date = 05/20/13 
 Pct Recovery = 81%  Analysis Date = 05/20/13 
 Pct Recovery = 81%  Analysis Date = 05/18/13 
 Pct Recovery = 81%  Analysis Date = 05/18/13 
 Pct Recovery = 81%  Analysis Date = 05/16/13 
 Pct Recovery = 82%  Analysis Date = 05/16/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/14/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 82%  Analysis Date = 05/12/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/10/13 
 Pct Recovery = 82%  Analysis Date = 05/08/13 
 Pct Recovery = 83%  Analysis Date = 05/08/13 
 Pct Recovery = 83%  Analysis Date = 05/05/13 
 Pct Recovery = 83%  Analysis Date = 05/05/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/03/13 
 Pct Recovery = 83%  Analysis Date = 05/01/13 
 Pct Recovery = 85%  Analysis Date = 05/01/13 
 Pct Recovery = 85%  Analysis Date = 04/29/13 
 Pct Recovery = 87%  Analysis Date = 04/29/13 
 Pct Recovery = 87%  Analysis Date = 04/27/13 
 Pct Recovery = 90%  Analysis Date = 04/27/13 
 Pct Recovery = 90%  Analysis Date = 04/25/13 
 Pct Recovery = 92%  Analysis Date = 04/25/13 
 Pct Recovery = 92%  Analysis Date = 04/23/13 
 Pct Recovery = 92%  Analysis Date = 04/23/13 
 Pct Recovery = 92%  Analysis Date = 04/21/13 
 Pct Recovery = 92%  Analysis Date = 04/21/13 
 Pct Recovery = 92%  Analysis Date = 04/19/13 
 Pct Recovery = 91%  Analysis Date = 04/19/13 
 Pct Recovery = 91%  Analysis Date = 04/17/13 
 Pct Recovery = 91%  Analysis Date = 04/17/13 
 Pct Recovery = 91%  Analysis Date = 04/15/13 
 Pct Recovery = 91%  Analysis Date = 04/15/13 
 Pct Recovery = 91%  Analysis Date = 04/13/13 
 Pct Recovery = 91%  Analysis Date = 04/13/13 
 Pct Recovery = 91%  Analysis Date = 04/11/13 
 Pct Recovery = 91%  Analysis Date = 04/11/13 
 Pct Recovery = 91%  Analysis Date = 04/09/13 
 Pct Recovery = 91%  Analysis Date = 04/09/13 
 Pct Recovery = 91%  Analysis Date = 04/07/13 
 Pct Recovery = 91%  Analysis Date = 04/07/13 
 Pct Recovery = 91%  Analysis Date = 04/05/13 
 Pct Recovery = 90%  Analysis Date = 04/05/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/03/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 04/01/13 
 Pct Recovery = 90%  Analysis Date = 03/30/13 
 Pct Recovery = 90%  Analysis Date = 03/30/13 
 Pct Recovery = 90%  Analysis Date = 03/28/13 
 Pct Recovery = 90%  Analysis Date = 03/28/13 
 Pct Recovery = 90%  Analysis Date = 03/26/13 
 Pct Recovery = 90%  Analysis Date = 03/26/13 
 Pct Recovery = 90%  Analysis Date = 03/24/13 
 Pct Recovery = 90%  Analysis Date = 03/24/13 
 Pct Recovery = 90%  Analysis Date = 03/22/13 
 Pct Recovery = 90%  Analysis Date = 03/22/13 
 Pct Recovery = 90%  Analysis Date = 03/20/13 
 Pct Recovery = 89%  Analysis Date = 03/20/13 
 Pct Recovery = 89%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/18/13 
 Pct Recovery = 89%  Analysis Date = 03/16/13 
 Pct Recovery = 89%  Analysis Date = 03/16/13 
 Pct Recovery = 89%  Analysis Date = 03/14/13 
 Pct Recovery = 89%  Analysis Date = 03/14/13 
 Pct Recovery = 89%  Analysis Date = 03/12/13 
 Pct Recovery = 89%  Analysis Date = 03/12/13 
 Pct Recovery = 89%  Analysis Date = 03/10/13 
 Pct Recovery = 89%  Analysis Date = 03/10/13 
 Pct Recovery = 89%  Analysis Date = 03/08/13 
 Pct Recovery = 89%  Analysis Date = 03/08/13 
 Pct Recovery = 89%  Analysis Date = 03/06/13 
 Pct Recovery = 88%  Analysis Date = 03/06/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/04/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 03/02/13 
 Pct Recovery = 88%  Analysis Date = 02/28/13 
 Pct Recovery = 88%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
THEOPHYLLINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 80% . 80% 0%
>= Reporting Level 5 78% 26% 88% 9%
Total 6 78% 23% 84% 9%

Sample Statistics
THEOPHYLLINE

Characteristic N % % Basis
Plotted 6 43% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 15 .  
False Negatives 7 50% 7 out of 14
Not Spiked 17 .  
False Positives 1 6% 1 out of 17

OBSP Determination:
THIABENDAZOLE
METHOD: LC9017 , TESTIDCODE: 67455LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 70%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 72%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 23%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 95%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 101%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 80%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 74%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 81%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 76%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 77%  Analysis Date = 04/09/14 
 Pct Recovery = 31%  Analysis Date = 04/07/14 
 Pct Recovery = 31%  Analysis Date = 04/07/14 
 Pct Recovery = 31%  Analysis Date = 04/05/14 
 Pct Recovery = 32%  Analysis Date = 04/05/14 
 Pct Recovery = 32%  Analysis Date = 04/02/14 
 Pct Recovery = 33%  Analysis Date = 04/02/14 
 Pct Recovery = 33%  Analysis Date = 03/31/14 
 Pct Recovery = 34%  Analysis Date = 03/31/14 
 Pct Recovery = 34%  Analysis Date = 03/28/14 
 Pct Recovery = 34%  Analysis Date = 03/28/14 
 Pct Recovery = 34%  Analysis Date = 03/26/14 
 Pct Recovery = 35%  Analysis Date = 03/26/14 
 Pct Recovery = 35%  Analysis Date = 03/24/14 
 Pct Recovery = 36%  Analysis Date = 03/24/14 
 Pct Recovery = 36%  Analysis Date = 03/21/14 
 Pct Recovery = 37%  Analysis Date = 03/21/14 
 Pct Recovery = 37%  Analysis Date = 03/19/14 
 Pct Recovery = 37%  Analysis Date = 03/19/14 
 Pct Recovery = 37%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/16/14 
 Pct Recovery = 38%  Analysis Date = 03/14/14 
 Pct Recovery = 39%  Analysis Date = 03/14/14 
 Pct Recovery = 39%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/12/14 
 Pct Recovery = 40%  Analysis Date = 03/09/14 
 Pct Recovery = 40%  Analysis Date = 03/09/14 
 Pct Recovery = 40%  Analysis Date = 03/07/14 
 Pct Recovery = 41%  Analysis Date = 03/07/14 
 Pct Recovery = 41%  Analysis Date = 03/04/14 
 Pct Recovery = 42%  Analysis Date = 03/04/14 
 Pct Recovery = 42%  Analysis Date = 03/02/14 
 Pct Recovery = 43%  Analysis Date = 03/02/14 
 Pct Recovery = 43%  Analysis Date = 02/28/14 
 Pct Recovery = 43%  Analysis Date = 02/28/14 
 Pct Recovery = 43%  Analysis Date = 02/25/14 
 Pct Recovery = 44%  Analysis Date = 02/25/14 
 Pct Recovery = 44%  Analysis Date = 02/23/14 
 Pct Recovery = 45%  Analysis Date = 02/23/14 
 Pct Recovery = 45%  Analysis Date = 02/20/14 
 Pct Recovery = 46%  Analysis Date = 02/20/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/18/14 
 Pct Recovery = 46%  Analysis Date = 02/15/14 
 Pct Recovery = 47%  Analysis Date = 02/15/14 
 Pct Recovery = 47%  Analysis Date = 02/13/14 
 Pct Recovery = 48%  Analysis Date = 02/13/14 
 Pct Recovery = 48%  Analysis Date = 02/11/14 
 Pct Recovery = 48%  Analysis Date = 02/11/14 
 Pct Recovery = 48%  Analysis Date = 02/08/14 
 Pct Recovery = 49%  Analysis Date = 02/08/14 
 Pct Recovery = 49%  Analysis Date = 02/06/14 
 Pct Recovery = 50%  Analysis Date = 02/06/14 
 Pct Recovery = 50%  Analysis Date = 02/03/14 
 Pct Recovery = 51%  Analysis Date = 02/03/14 
 Pct Recovery = 51%  Analysis Date = 02/01/14 
 Pct Recovery = 51%  Analysis Date = 02/01/14 
 Pct Recovery = 51%  Analysis Date = 01/30/14 
 Pct Recovery = 52%  Analysis Date = 01/30/14 
 Pct Recovery = 52%  Analysis Date = 01/27/14 
 Pct Recovery = 53%  Analysis Date = 01/27/14 
 Pct Recovery = 53%  Analysis Date = 01/25/14 
 Pct Recovery = 54%  Analysis Date = 01/25/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/20/14 
 Pct Recovery = 55%  Analysis Date = 01/20/14 
 Pct Recovery = 55%  Analysis Date = 01/18/14 
 Pct Recovery = 56%  Analysis Date = 01/18/14 
 Pct Recovery = 56%  Analysis Date = 01/15/14 
 Pct Recovery = 57%  Analysis Date = 01/15/14 
 Pct Recovery = 57%  Analysis Date = 01/13/14 
 Pct Recovery = 57%  Analysis Date = 01/13/14 
 Pct Recovery = 57%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/10/14 
 Pct Recovery = 58%  Analysis Date = 01/08/14 
 Pct Recovery = 59%  Analysis Date = 01/08/14 
 Pct Recovery = 59%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/06/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/03/14 
 Pct Recovery = 60%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 01/01/14 
 Pct Recovery = 61%  Analysis Date = 12/29/13 
 Pct Recovery = 62%  Analysis Date = 12/29/13 
 Pct Recovery = 62%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/27/13 
 Pct Recovery = 63%  Analysis Date = 12/24/13 
 Pct Recovery = 63%  Analysis Date = 12/24/13 
 Pct Recovery = 63%  Analysis Date = 12/22/13 
 Pct Recovery = 64%  Analysis Date = 12/22/13 
 Pct Recovery = 64%  Analysis Date = 12/20/13 
 Pct Recovery = 65%  Analysis Date = 12/20/13 
 Pct Recovery = 65%  Analysis Date = 12/17/13 
 Pct Recovery = 66%  Analysis Date = 12/17/13 
 Pct Recovery = 66%  Analysis Date = 12/15/13 
 Pct Recovery = 66%  Analysis Date = 12/15/13 
 Pct Recovery = 66%  Analysis Date = 12/12/13 
 Pct Recovery = 67%  Analysis Date = 12/12/13 
 Pct Recovery = 67%  Analysis Date = 12/10/13 
 Pct Recovery = 68%  Analysis Date = 12/10/13 
 Pct Recovery = 68%  Analysis Date = 12/08/13 
 Pct Recovery = 69%  Analysis Date = 12/08/13 
 Pct Recovery = 69%  Analysis Date = 12/05/13 
 Pct Recovery = 69%  Analysis Date = 12/05/13 
 Pct Recovery = 69%  Analysis Date = 12/03/13 
 Pct Recovery = 70%  Analysis Date = 12/03/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/26/13 
 Pct Recovery = 72%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/23/13 
 Pct Recovery = 73%  Analysis Date = 11/21/13 
 Pct Recovery = 74%  Analysis Date = 11/21/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/18/13 
 Pct Recovery = 74%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/16/13 
 Pct Recovery = 75%  Analysis Date = 11/13/13 
 Pct Recovery = 76%  Analysis Date = 11/13/13 
 Pct Recovery = 76%  Analysis Date = 11/11/13 
 Pct Recovery = 76%  Analysis Date = 11/11/13 
 Pct Recovery = 76%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/09/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/06/13 
 Pct Recovery = 77%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/04/13 
 Pct Recovery = 78%  Analysis Date = 11/01/13 
 Pct Recovery = 78%  Analysis Date = 11/01/13 
 Pct Recovery = 78%  Analysis Date = 10/30/13 
 Pct Recovery = 79%  Analysis Date = 10/30/13 
 Pct Recovery = 79%  Analysis Date = 10/28/13 
 Pct Recovery = 79%  Analysis Date = 10/28/13 
 Pct Recovery = 79%  Analysis Date = 10/25/13 
 Pct Recovery = 79%  Analysis Date = 10/25/13 
 Pct Recovery = 79%  Analysis Date = 10/23/13 
 Pct Recovery = 79%  Analysis Date = 10/23/13 
 Pct Recovery = 79%  Analysis Date = 10/20/13 
 Pct Recovery = 79%  Analysis Date = 10/20/13 
 Pct Recovery = 79%  Analysis Date = 10/18/13 
 Pct Recovery = 79%  Analysis Date = 10/18/13 
 Pct Recovery = 79%  Analysis Date = 10/16/13 
 Pct Recovery = 79%  Analysis Date = 10/16/13 
 Pct Recovery = 79%  Analysis Date = 10/13/13 
 Pct Recovery = 79%  Analysis Date = 10/13/13 
 Pct Recovery = 79%  Analysis Date = 10/11/13 
 Pct Recovery = 79%  Analysis Date = 10/11/13 
 Pct Recovery = 79%  Analysis Date = 10/08/13 
 Pct Recovery = 79%  Analysis Date = 10/08/13 
 Pct Recovery = 79%  Analysis Date = 10/06/13 
 Pct Recovery = 79%  Analysis Date = 10/06/13 
 Pct Recovery = 79%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/04/13 
 Pct Recovery = 79%  Analysis Date = 10/01/13 
 Pct Recovery = 79%  Analysis Date = 10/01/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/29/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/26/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/24/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/21/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/19/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/14/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/12/13 
 Pct Recovery = 79%  Analysis Date = 09/09/13 
 Pct Recovery = 79%  Analysis Date = 09/09/13 
 Pct Recovery = 79%  Analysis Date = 09/07/13 
 Pct Recovery = 79%  Analysis Date = 09/07/13 
 Pct Recovery = 79%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 08/31/13 
 Pct Recovery = 79%  Analysis Date = 08/31/13 
 Pct Recovery = 79%  Analysis Date = 08/28/13 
 Pct Recovery = 79%  Analysis Date = 08/28/13 
 Pct Recovery = 79%  Analysis Date = 08/26/13 
 Pct Recovery = 79%  Analysis Date = 08/26/13 
 Pct Recovery = 79%  Analysis Date = 08/24/13 
 Pct Recovery = 79%  Analysis Date = 08/24/13 
 Pct Recovery = 79%  Analysis Date = 08/21/13 
 Pct Recovery = 79%  Analysis Date = 08/21/13 
 Pct Recovery = 79%  Analysis Date = 08/19/13 
 Pct Recovery = 79%  Analysis Date = 08/19/13 
 Pct Recovery = 79%  Analysis Date = 08/16/13 
 Pct Recovery = 79%  Analysis Date = 08/16/13 
 Pct Recovery = 79%  Analysis Date = 08/14/13 
 Pct Recovery = 79%  Analysis Date = 08/14/13 
 Pct Recovery = 79%  Analysis Date = 08/11/13 
 Pct Recovery = 79%  Analysis Date = 08/11/13 
 Pct Recovery = 79%  Analysis Date = 08/09/13 
 Pct Recovery = 79%  Analysis Date = 08/09/13 
 Pct Recovery = 79%  Analysis Date = 08/07/13 
 Pct Recovery = 79%  Analysis Date = 08/07/13 
 Pct Recovery = 79%  Analysis Date = 08/04/13 
 Pct Recovery = 79%  Analysis Date = 08/04/13 
 Pct Recovery = 79%  Analysis Date = 08/02/13 
 Pct Recovery = 79%  Analysis Date = 08/02/13 
 Pct Recovery = 79%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/30/13 
 Pct Recovery = 79%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 80%  Analysis Date = 07/06/13 
 Pct Recovery = 80%  Analysis Date = 07/06/13 
 Pct Recovery = 80%  Analysis Date = 07/04/13 
 Pct Recovery = 80%  Analysis Date = 07/04/13 
 Pct Recovery = 80%  Analysis Date = 07/02/13 
 Pct Recovery = 80%  Analysis Date = 07/02/13 
 Pct Recovery = 80%  Analysis Date = 06/29/13 
 Pct Recovery = 80%  Analysis Date = 06/29/13 
 Pct Recovery = 80%  Analysis Date = 06/27/13 
 Pct Recovery = 80%  Analysis Date = 06/27/13 
 Pct Recovery = 80%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 80%  Analysis Date = 06/10/13 
 Pct Recovery = 80%  Analysis Date = 06/10/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/07/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/05/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 05/31/13 
 Pct Recovery = 80%  Analysis Date = 05/31/13 
 Pct Recovery = 80%  Analysis Date = 05/29/13 
 Pct Recovery = 80%  Analysis Date = 05/29/13 
 Pct Recovery = 80%  Analysis Date = 05/26/13 
 Pct Recovery = 80%  Analysis Date = 05/26/13 
 Pct Recovery = 80%  Analysis Date = 05/24/13 
 Pct Recovery = 80%  Analysis Date = 05/24/13 
 Pct Recovery = 80%  Analysis Date = 05/22/13 
 Pct Recovery = 80%  Analysis Date = 05/22/13 
 Pct Recovery = 80%  Analysis Date = 05/19/13 
 Pct Recovery = 80%  Analysis Date = 05/19/13 
 Pct Recovery = 80%  Analysis Date = 05/17/13 
 Pct Recovery = 80%  Analysis Date = 05/17/13 
 Pct Recovery = 80%  Analysis Date = 05/14/13 
 Pct Recovery = 80%  Analysis Date = 05/14/13 
 Pct Recovery = 80%  Analysis Date = 05/12/13 
 Pct Recovery = 80%  Analysis Date = 05/12/13 
 Pct Recovery = 80%  Analysis Date = 05/10/13 
 Pct Recovery = 80%  Analysis Date = 05/10/13 
 Pct Recovery = 80%  Analysis Date = 05/07/13 
 Pct Recovery = 80%  Analysis Date = 05/07/13 
 Pct Recovery = 80%  Analysis Date = 05/05/13 
 Pct Recovery = 80%  Analysis Date = 05/05/13 
 Pct Recovery = 80%  Analysis Date = 05/02/13 
 Pct Recovery = 80%  Analysis Date = 05/02/13 
 Pct Recovery = 80%  Analysis Date = 04/30/13 
 Pct Recovery = 80%  Analysis Date = 04/30/13 
 Pct Recovery = 80%  Analysis Date = 04/27/13 
 Pct Recovery = 80%  Analysis Date = 04/27/13 
 Pct Recovery = 80%  Analysis Date = 04/25/13 
 Pct Recovery = 80%  Analysis Date = 04/25/13 
 Pct Recovery = 80%  Analysis Date = 04/23/13 
 Pct Recovery = 80%  Analysis Date = 04/23/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/20/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/18/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/15/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 80%  Analysis Date = 04/13/13 
 Pct Recovery = 80%  Analysis Date = 04/11/13 
 Pct Recovery = 79%  Analysis Date = 04/11/13 
 Pct Recovery = 79%  Analysis Date = 04/08/13 
 Pct Recovery = 79%  Analysis Date = 04/08/13 
 Pct Recovery = 79%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/06/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/03/13 
 Pct Recovery = 79%  Analysis Date = 04/01/13 
 Pct Recovery = 79%  Analysis Date = 04/01/13 
 Pct Recovery = 79%  Analysis Date = 03/30/13 
 Pct Recovery = 79%  Analysis Date = 03/30/13 
 Pct Recovery = 79%  Analysis Date = 03/27/13 
 Pct Recovery = 79%  Analysis Date = 03/27/13 
 Pct Recovery = 79%  Analysis Date = 03/25/13 
 Pct Recovery = 79%  Analysis Date = 03/25/13 
 Pct Recovery = 79%  Analysis Date = 03/22/13 
 Pct Recovery = 79%  Analysis Date = 03/22/13 
 Pct Recovery = 79%  Analysis Date = 03/20/13 
 Pct Recovery = 79%  Analysis Date = 03/20/13 
 Pct Recovery = 79%  Analysis Date = 03/17/13 
 Pct Recovery = 78%  Analysis Date = 03/17/13 
 Pct Recovery = 78%  Analysis Date = 03/15/13 
 Pct Recovery = 78%  Analysis Date = 03/15/13 
 Pct Recovery = 78%  Analysis Date = 03/13/13 
 Pct Recovery = 78%  Analysis Date = 03/13/13 
 Pct Recovery = 78%  Analysis Date = 03/10/13 
 Pct Recovery = 78%  Analysis Date = 03/10/13 
 Pct Recovery = 78%  Analysis Date = 03/08/13 
 Pct Recovery = 78%  Analysis Date = 03/08/13 
 Pct Recovery = 78%  Analysis Date = 03/05/13 
 Pct Recovery = 78%  Analysis Date = 03/05/13 
 Pct Recovery = 78%  Analysis Date = 03/03/13 
 Pct Recovery = 78%  Analysis Date = 03/03/13 
 Pct Recovery = 78%  Analysis Date = 03/01/13 
 Pct Recovery = 78%  Analysis Date = 03/01/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/26/13 
 Pct Recovery = 78%  Analysis Date = 02/24/13 
 Pct Recovery = 78%  Analysis Date = 02/24/13 
 Pct Recovery = 78%  Analysis Date = 02/21/13 
 Pct Recovery = 78%  Analysis Date = 02/21/13 
 Pct Recovery = 78%  Analysis Date = 02/19/13 
 Pct Recovery = 78%  Analysis Date = 02/19/13 
 Pct Recovery = 78%  Analysis Date = 02/17/13 
 Pct Recovery = 78%  Analysis Date = 02/17/13 
 Pct Recovery = 78%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/14/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/12/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/09/13 
 Pct Recovery = 78%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/07/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/05/13 
 Pct Recovery = 77%  Analysis Date = 02/02/13 
 Pct Recovery = 77%  Analysis Date = 02/02/13 
 Pct Recovery = 77%  Analysis Date = 01/31/13 
 Pct Recovery = 77%  Analysis Date = 01/31/13 
 Pct Recovery = 77%  Analysis Date = 01/28/13 
 Pct Recovery = 77%  Analysis Date = 01/28/13 
 Pct Recovery = 77%  Analysis Date = 01/26/13 
 Pct Recovery = 77%  Analysis Date = 01/26/13 
 Pct Recovery = 77%  Analysis Date = 01/23/13 
 Pct Recovery = 77%  Analysis Date = 01/23/13 
 Pct Recovery = 77%  Analysis Date = 01/21/13 
 Pct Recovery = 77%  Analysis Date = 01/21/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/19/13 
 Pct Recovery = 77%  Analysis Date = 01/16/13 
 Pct Recovery = 77%  Analysis Date = 01/16/13 
 Pct Recovery = 77%  Analysis Date = 01/14/13 
 Pct Recovery = 77%  Analysis Date = 01/14/13 
 Pct Recovery = 77%  Analysis Date = 01/11/13 
 Pct Recovery = 77%  Analysis Date = 01/11/13 
 Pct Recovery = 77%  Analysis Date = 01/09/13 
 Pct Recovery = 77%  Analysis Date = 01/09/13 
 Pct Recovery = 77%  Analysis Date = 01/07/13 
 Pct Recovery = 77%  Analysis Date = 01/07/13 
 Pct Recovery = 77%  Analysis Date = 01/04/13 
 Pct Recovery = 77%  Analysis Date = 01/04/13 
 Pct Recovery = 77%  Analysis Date = 01/02/13 
 Pct Recovery = 77%  Analysis Date = 01/02/13 
 Pct Recovery = 77%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/30/12 
 Pct Recovery = 77%  Analysis Date = 12/28/12 
 Pct Recovery = 77%  Analysis Date = 12/28/12 
 Pct Recovery = 77%  Analysis Date = 12/26/12 
 Pct Recovery = 77%  Analysis Date = 12/26/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 77%  Analysis Date = 12/23/12 
 Pct Recovery = 77%  Analysis Date = 12/21/12 
 Pct Recovery = 77%  Analysis Date = 12/21/12 
 Pct Recovery = 77%  Analysis Date = 12/18/12 
 Pct Recovery = 77%  Analysis Date = 12/18/12 
 Pct Recovery = 77%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/16/12 
 Pct Recovery = 77%  Analysis Date = 12/14/12 
 Pct Recovery = 77%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIABENDAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 77% . 77% 0%
>= Reporting Level 10 74% 21% 75% 8%
Total 11 74% 20% 76% 8%

Sample Statistics
THIABENDAZOLE

Characteristic N % % Basis
Plotted 11 79% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 2 14% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
TIOTROPIUM
METHOD: LC9017 , TESTIDCODE: 67508LCM56

The SGPlot Procedure

Sample Statistics
TIOTROPIUM

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 32 .  
False Positives 0 0% 0 out of 31

OBSP Determination:
TRAMADOL
METHOD: LC9017 , TESTIDCODE: 67517LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 75%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 72%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 45%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 66%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 70%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 59%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 85%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 73%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 73%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 69%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 80%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 91%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 69%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 72%  Analysis Date = 04/09/14 
 Pct Recovery = 56%  Analysis Date = 04/07/14 
 Pct Recovery = 56%  Analysis Date = 04/07/14 
 Pct Recovery = 56%  Analysis Date = 04/05/14 
 Pct Recovery = 56%  Analysis Date = 04/05/14 
 Pct Recovery = 56%  Analysis Date = 04/02/14 
 Pct Recovery = 56%  Analysis Date = 04/02/14 
 Pct Recovery = 56%  Analysis Date = 03/31/14 
 Pct Recovery = 57%  Analysis Date = 03/31/14 
 Pct Recovery = 57%  Analysis Date = 03/28/14 
 Pct Recovery = 57%  Analysis Date = 03/28/14 
 Pct Recovery = 57%  Analysis Date = 03/26/14 
 Pct Recovery = 57%  Analysis Date = 03/26/14 
 Pct Recovery = 57%  Analysis Date = 03/24/14 
 Pct Recovery = 58%  Analysis Date = 03/24/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/21/14 
 Pct Recovery = 58%  Analysis Date = 03/19/14 
 Pct Recovery = 58%  Analysis Date = 03/19/14 
 Pct Recovery = 58%  Analysis Date = 03/16/14 
 Pct Recovery = 59%  Analysis Date = 03/16/14 
 Pct Recovery = 59%  Analysis Date = 03/14/14 
 Pct Recovery = 59%  Analysis Date = 03/14/14 
 Pct Recovery = 59%  Analysis Date = 03/12/14 
 Pct Recovery = 59%  Analysis Date = 03/12/14 
 Pct Recovery = 59%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/09/14 
 Pct Recovery = 59%  Analysis Date = 03/07/14 
 Pct Recovery = 60%  Analysis Date = 03/07/14 
 Pct Recovery = 60%  Analysis Date = 03/04/14 
 Pct Recovery = 60%  Analysis Date = 03/04/14 
 Pct Recovery = 60%  Analysis Date = 03/02/14 
 Pct Recovery = 60%  Analysis Date = 03/02/14 
 Pct Recovery = 60%  Analysis Date = 02/28/14 
 Pct Recovery = 61%  Analysis Date = 02/28/14 
 Pct Recovery = 61%  Analysis Date = 02/25/14 
 Pct Recovery = 61%  Analysis Date = 02/25/14 
 Pct Recovery = 61%  Analysis Date = 02/23/14 
 Pct Recovery = 61%  Analysis Date = 02/23/14 
 Pct Recovery = 61%  Analysis Date = 02/20/14 
 Pct Recovery = 62%  Analysis Date = 02/20/14 
 Pct Recovery = 62%  Analysis Date = 02/18/14 
 Pct Recovery = 62%  Analysis Date = 02/18/14 
 Pct Recovery = 62%  Analysis Date = 02/15/14 
 Pct Recovery = 62%  Analysis Date = 02/15/14 
 Pct Recovery = 62%  Analysis Date = 02/13/14 
 Pct Recovery = 63%  Analysis Date = 02/13/14 
 Pct Recovery = 63%  Analysis Date = 02/11/14 
 Pct Recovery = 63%  Analysis Date = 02/11/14 
 Pct Recovery = 63%  Analysis Date = 02/08/14 
 Pct Recovery = 63%  Analysis Date = 02/08/14 
 Pct Recovery = 63%  Analysis Date = 02/06/14 
 Pct Recovery = 63%  Analysis Date = 02/06/14 
 Pct Recovery = 63%  Analysis Date = 02/03/14 
 Pct Recovery = 64%  Analysis Date = 02/03/14 
 Pct Recovery = 64%  Analysis Date = 02/01/14 
 Pct Recovery = 64%  Analysis Date = 02/01/14 
 Pct Recovery = 64%  Analysis Date = 01/30/14 
 Pct Recovery = 64%  Analysis Date = 01/30/14 
 Pct Recovery = 64%  Analysis Date = 01/27/14 
 Pct Recovery = 65%  Analysis Date = 01/27/14 
 Pct Recovery = 65%  Analysis Date = 01/25/14 
 Pct Recovery = 65%  Analysis Date = 01/25/14 
 Pct Recovery = 65%  Analysis Date = 01/22/14 
 Pct Recovery = 65%  Analysis Date = 01/22/14 
 Pct Recovery = 65%  Analysis Date = 01/20/14 
 Pct Recovery = 66%  Analysis Date = 01/20/14 
 Pct Recovery = 66%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/18/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/15/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/13/14 
 Pct Recovery = 66%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/10/14 
 Pct Recovery = 67%  Analysis Date = 01/08/14 
 Pct Recovery = 67%  Analysis Date = 01/08/14 
 Pct Recovery = 67%  Analysis Date = 01/06/14 
 Pct Recovery = 67%  Analysis Date = 01/06/14 
 Pct Recovery = 67%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/03/14 
 Pct Recovery = 67%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 01/01/14 
 Pct Recovery = 68%  Analysis Date = 12/29/13 
 Pct Recovery = 68%  Analysis Date = 12/29/13 
 Pct Recovery = 68%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/27/13 
 Pct Recovery = 68%  Analysis Date = 12/24/13 
 Pct Recovery = 68%  Analysis Date = 12/24/13 
 Pct Recovery = 68%  Analysis Date = 12/22/13 
 Pct Recovery = 68%  Analysis Date = 12/22/13 
 Pct Recovery = 68%  Analysis Date = 12/20/13 
 Pct Recovery = 69%  Analysis Date = 12/20/13 
 Pct Recovery = 69%  Analysis Date = 12/17/13 
 Pct Recovery = 69%  Analysis Date = 12/17/13 
 Pct Recovery = 69%  Analysis Date = 12/15/13 
 Pct Recovery = 69%  Analysis Date = 12/15/13 
 Pct Recovery = 69%  Analysis Date = 12/12/13 
 Pct Recovery = 69%  Analysis Date = 12/12/13 
 Pct Recovery = 69%  Analysis Date = 12/10/13 
 Pct Recovery = 70%  Analysis Date = 12/10/13 
 Pct Recovery = 70%  Analysis Date = 12/08/13 
 Pct Recovery = 70%  Analysis Date = 12/08/13 
 Pct Recovery = 70%  Analysis Date = 12/05/13 
 Pct Recovery = 70%  Analysis Date = 12/05/13 
 Pct Recovery = 70%  Analysis Date = 12/03/13 
 Pct Recovery = 70%  Analysis Date = 12/03/13 
 Pct Recovery = 70%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/23/13 
 Pct Recovery = 71%  Analysis Date = 11/21/13 
 Pct Recovery = 72%  Analysis Date = 11/21/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/18/13 
 Pct Recovery = 72%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/16/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/13/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/11/13 
 Pct Recovery = 73%  Analysis Date = 11/09/13 
 Pct Recovery = 74%  Analysis Date = 11/09/13 
 Pct Recovery = 74%  Analysis Date = 11/06/13 
 Pct Recovery = 74%  Analysis Date = 11/06/13 
 Pct Recovery = 74%  Analysis Date = 11/04/13 
 Pct Recovery = 75%  Analysis Date = 11/04/13 
 Pct Recovery = 75%  Analysis Date = 11/01/13 
 Pct Recovery = 75%  Analysis Date = 11/01/13 
 Pct Recovery = 75%  Analysis Date = 10/30/13 
 Pct Recovery = 75%  Analysis Date = 10/30/13 
 Pct Recovery = 75%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/28/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/25/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/23/13 
 Pct Recovery = 76%  Analysis Date = 10/20/13 
 Pct Recovery = 76%  Analysis Date = 10/20/13 
 Pct Recovery = 76%  Analysis Date = 10/18/13 
 Pct Recovery = 76%  Analysis Date = 10/18/13 
 Pct Recovery = 76%  Analysis Date = 10/16/13 
 Pct Recovery = 76%  Analysis Date = 10/16/13 
 Pct Recovery = 76%  Analysis Date = 10/13/13 
 Pct Recovery = 76%  Analysis Date = 10/13/13 
 Pct Recovery = 76%  Analysis Date = 10/11/13 
 Pct Recovery = 77%  Analysis Date = 10/11/13 
 Pct Recovery = 77%  Analysis Date = 10/08/13 
 Pct Recovery = 77%  Analysis Date = 10/08/13 
 Pct Recovery = 77%  Analysis Date = 10/06/13 
 Pct Recovery = 77%  Analysis Date = 10/06/13 
 Pct Recovery = 77%  Analysis Date = 10/04/13 
 Pct Recovery = 77%  Analysis Date = 10/04/13 
 Pct Recovery = 77%  Analysis Date = 10/01/13 
 Pct Recovery = 77%  Analysis Date = 10/01/13 
 Pct Recovery = 77%  Analysis Date = 09/29/13 
 Pct Recovery = 77%  Analysis Date = 09/29/13 
 Pct Recovery = 77%  Analysis Date = 09/26/13 
 Pct Recovery = 77%  Analysis Date = 09/26/13 
 Pct Recovery = 77%  Analysis Date = 09/24/13 
 Pct Recovery = 78%  Analysis Date = 09/24/13 
 Pct Recovery = 78%  Analysis Date = 09/21/13 
 Pct Recovery = 78%  Analysis Date = 09/21/13 
 Pct Recovery = 78%  Analysis Date = 09/19/13 
 Pct Recovery = 78%  Analysis Date = 09/19/13 
 Pct Recovery = 78%  Analysis Date = 09/17/13 
 Pct Recovery = 78%  Analysis Date = 09/17/13 
 Pct Recovery = 78%  Analysis Date = 09/14/13 
 Pct Recovery = 78%  Analysis Date = 09/14/13 
 Pct Recovery = 78%  Analysis Date = 09/12/13 
 Pct Recovery = 78%  Analysis Date = 09/12/13 
 Pct Recovery = 78%  Analysis Date = 09/09/13 
 Pct Recovery = 78%  Analysis Date = 09/09/13 
 Pct Recovery = 78%  Analysis Date = 09/07/13 
 Pct Recovery = 78%  Analysis Date = 09/07/13 
 Pct Recovery = 78%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/05/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 08/31/13 
 Pct Recovery = 79%  Analysis Date = 08/31/13 
 Pct Recovery = 79%  Analysis Date = 08/28/13 
 Pct Recovery = 79%  Analysis Date = 08/28/13 
 Pct Recovery = 79%  Analysis Date = 08/26/13 
 Pct Recovery = 79%  Analysis Date = 08/26/13 
 Pct Recovery = 79%  Analysis Date = 08/24/13 
 Pct Recovery = 79%  Analysis Date = 08/24/13 
 Pct Recovery = 79%  Analysis Date = 08/21/13 
 Pct Recovery = 79%  Analysis Date = 08/21/13 
 Pct Recovery = 79%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/19/13 
 Pct Recovery = 80%  Analysis Date = 08/16/13 
 Pct Recovery = 80%  Analysis Date = 08/16/13 
 Pct Recovery = 80%  Analysis Date = 08/14/13 
 Pct Recovery = 80%  Analysis Date = 08/14/13 
 Pct Recovery = 80%  Analysis Date = 08/11/13 
 Pct Recovery = 80%  Analysis Date = 08/11/13 
 Pct Recovery = 80%  Analysis Date = 08/09/13 
 Pct Recovery = 80%  Analysis Date = 08/09/13 
 Pct Recovery = 80%  Analysis Date = 08/07/13 
 Pct Recovery = 80%  Analysis Date = 08/07/13 
 Pct Recovery = 80%  Analysis Date = 08/04/13 
 Pct Recovery = 80%  Analysis Date = 08/04/13 
 Pct Recovery = 80%  Analysis Date = 08/02/13 
 Pct Recovery = 80%  Analysis Date = 08/02/13 
 Pct Recovery = 80%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/30/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/28/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/26/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/23/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/21/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/18/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/16/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/14/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/11/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 80%  Analysis Date = 07/09/13 
 Pct Recovery = 80%  Analysis Date = 07/06/13 
 Pct Recovery = 80%  Analysis Date = 07/06/13 
 Pct Recovery = 80%  Analysis Date = 07/04/13 
 Pct Recovery = 80%  Analysis Date = 07/04/13 
 Pct Recovery = 80%  Analysis Date = 07/02/13 
 Pct Recovery = 80%  Analysis Date = 07/02/13 
 Pct Recovery = 80%  Analysis Date = 06/29/13 
 Pct Recovery = 80%  Analysis Date = 06/29/13 
 Pct Recovery = 80%  Analysis Date = 06/27/13 
 Pct Recovery = 80%  Analysis Date = 06/27/13 
 Pct Recovery = 80%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/24/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/22/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/19/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/17/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/15/13 
 Pct Recovery = 80%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/12/13 
 Pct Recovery = 79%  Analysis Date = 06/10/13 
 Pct Recovery = 79%  Analysis Date = 06/10/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/07/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/05/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 06/03/13 
 Pct Recovery = 79%  Analysis Date = 05/31/13 
 Pct Recovery = 79%  Analysis Date = 05/31/13 
 Pct Recovery = 79%  Analysis Date = 05/29/13 
 Pct Recovery = 79%  Analysis Date = 05/29/13 
 Pct Recovery = 79%  Analysis Date = 05/26/13 
 Pct Recovery = 79%  Analysis Date = 05/26/13 
 Pct Recovery = 79%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/24/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/22/13 
 Pct Recovery = 79%  Analysis Date = 05/19/13 
 Pct Recovery = 79%  Analysis Date = 05/19/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/17/13 
 Pct Recovery = 79%  Analysis Date = 05/14/13 
 Pct Recovery = 79%  Analysis Date = 05/14/13 
 Pct Recovery = 79%  Analysis Date = 05/12/13 
 Pct Recovery = 79%  Analysis Date = 05/12/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/10/13 
 Pct Recovery = 79%  Analysis Date = 05/07/13 
 Pct Recovery = 79%  Analysis Date = 05/07/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/05/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 05/02/13 
 Pct Recovery = 79%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/30/13 
 Pct Recovery = 78%  Analysis Date = 04/27/13 
 Pct Recovery = 78%  Analysis Date = 04/27/13 
 Pct Recovery = 78%  Analysis Date = 04/25/13 
 Pct Recovery = 78%  Analysis Date = 04/25/13 
 Pct Recovery = 78%  Analysis Date = 04/23/13 
 Pct Recovery = 78%  Analysis Date = 04/23/13 
 Pct Recovery = 78%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/20/13 
 Pct Recovery = 77%  Analysis Date = 04/18/13 
 Pct Recovery = 77%  Analysis Date = 04/18/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/15/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/13/13 
 Pct Recovery = 77%  Analysis Date = 04/11/13 
 Pct Recovery = 77%  Analysis Date = 04/11/13 
 Pct Recovery = 77%  Analysis Date = 04/08/13 
 Pct Recovery = 76%  Analysis Date = 04/08/13 
 Pct Recovery = 76%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/06/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/03/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 04/01/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/30/13 
 Pct Recovery = 76%  Analysis Date = 03/27/13 
 Pct Recovery = 75%  Analysis Date = 03/27/13 
 Pct Recovery = 75%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/25/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/22/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/20/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/17/13 
 Pct Recovery = 75%  Analysis Date = 03/15/13 
 Pct Recovery = 74%  Analysis Date = 03/15/13 
 Pct Recovery = 74%  Analysis Date = 03/13/13 
 Pct Recovery = 74%  Analysis Date = 03/13/13 
 Pct Recovery = 74%  Analysis Date = 03/10/13 
 Pct Recovery = 74%  Analysis Date = 03/10/13 
 Pct Recovery = 74%  Analysis Date = 03/08/13 
 Pct Recovery = 74%  Analysis Date = 03/08/13 
 Pct Recovery = 74%  Analysis Date = 03/05/13 
 Pct Recovery = 74%  Analysis Date = 03/05/13 
 Pct Recovery = 74%  Analysis Date = 03/03/13 
 Pct Recovery = 73%  Analysis Date = 03/03/13 
 Pct Recovery = 73%  Analysis Date = 03/01/13 
 Pct Recovery = 73%  Analysis Date = 03/01/13 
 Pct Recovery = 73%  Analysis Date = 02/26/13 
 Pct Recovery = 73%  Analysis Date = 02/26/13 
 Pct Recovery = 73%  Analysis Date = 02/24/13 
 Pct Recovery = 73%  Analysis Date = 02/24/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/21/13 
 Pct Recovery = 73%  Analysis Date = 02/19/13 
 Pct Recovery = 73%  Analysis Date = 02/19/13 
 Pct Recovery = 73%  Analysis Date = 02/17/13 
 Pct Recovery = 72%  Analysis Date = 02/17/13 
 Pct Recovery = 72%  Analysis Date = 02/14/13 
 Pct Recovery = 72%  Analysis Date = 02/14/13 
 Pct Recovery = 72%  Analysis Date = 02/12/13 
 Pct Recovery = 72%  Analysis Date = 02/12/13 
 Pct Recovery = 72%  Analysis Date = 02/09/13 
 Pct Recovery = 72%  Analysis Date = 02/09/13 
 Pct Recovery = 72%  Analysis Date = 02/07/13 
 Pct Recovery = 72%  Analysis Date = 02/07/13 
 Pct Recovery = 72%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/05/13 
 Pct Recovery = 71%  Analysis Date = 02/02/13 
 Pct Recovery = 71%  Analysis Date = 02/02/13 
 Pct Recovery = 71%  Analysis Date = 01/31/13 
 Pct Recovery = 71%  Analysis Date = 01/31/13 
 Pct Recovery = 71%  Analysis Date = 01/28/13 
 Pct Recovery = 71%  Analysis Date = 01/28/13 
 Pct Recovery = 71%  Analysis Date = 01/26/13 
 Pct Recovery = 71%  Analysis Date = 01/26/13 
 Pct Recovery = 71%  Analysis Date = 01/23/13 
 Pct Recovery = 71%  Analysis Date = 01/23/13 
 Pct Recovery = 71%  Analysis Date = 01/21/13 
 Pct Recovery = 70%  Analysis Date = 01/21/13 
 Pct Recovery = 70%  Analysis Date = 01/19/13 
 Pct Recovery = 70%  Analysis Date = 01/19/13 
 Pct Recovery = 70%  Analysis Date = 01/16/13 
 Pct Recovery = 70%  Analysis Date = 01/16/13 
 Pct Recovery = 70%  Analysis Date = 01/14/13 
 Pct Recovery = 70%  Analysis Date = 01/14/13 
 Pct Recovery = 70%  Analysis Date = 01/11/13 
 Pct Recovery = 70%  Analysis Date = 01/11/13 
 Pct Recovery = 70%  Analysis Date = 01/09/13 
 Pct Recovery = 70%  Analysis Date = 01/09/13 
 Pct Recovery = 70%  Analysis Date = 01/07/13 
 Pct Recovery = 69%  Analysis Date = 01/07/13 
 Pct Recovery = 69%  Analysis Date = 01/04/13 
 Pct Recovery = 69%  Analysis Date = 01/04/13 
 Pct Recovery = 69%  Analysis Date = 01/02/13 
 Pct Recovery = 69%  Analysis Date = 01/02/13 
 Pct Recovery = 69%  Analysis Date = 12/30/12 
 Pct Recovery = 69%  Analysis Date = 12/30/12 
 Pct Recovery = 69%  Analysis Date = 12/28/12 
 Pct Recovery = 69%  Analysis Date = 12/28/12 
 Pct Recovery = 69%  Analysis Date = 12/26/12 
 Pct Recovery = 68%  Analysis Date = 12/26/12 
 Pct Recovery = 68%  Analysis Date = 12/23/12 
 Pct Recovery = 68%  Analysis Date = 12/23/12 
 Pct Recovery = 68%  Analysis Date = 12/21/12 
 Pct Recovery = 68%  Analysis Date = 12/21/12 
 Pct Recovery = 68%  Analysis Date = 12/18/12 
 Pct Recovery = 68%  Analysis Date = 12/18/12 
 Pct Recovery = 68%  Analysis Date = 12/16/12 
 Pct Recovery = 68%  Analysis Date = 12/16/12 
 Pct Recovery = 68%  Analysis Date = 12/14/12 
 Pct Recovery = 68%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRAMADOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 70% 2% 70% 2%
>= Reporting Level 12 72% 12% 72% 7%
Total 14 71% 11% 72% 4%

Sample Statistics
TRAMADOL

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 1 7% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
TRIAMTERENE
METHOD: LC9017 , TESTIDCODE: 67475LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 76%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 78%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 69%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 124%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 102%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 76%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 64%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 73%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 101%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 100%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 94%  Analysis Date = 04/09/14 
 Pct Recovery = 89%  Analysis Date = 04/07/14 
 Pct Recovery = 89%  Analysis Date = 04/07/14 
 Pct Recovery = 89%  Analysis Date = 04/05/14 
 Pct Recovery = 89%  Analysis Date = 04/05/14 
 Pct Recovery = 89%  Analysis Date = 04/03/14 
 Pct Recovery = 90%  Analysis Date = 04/03/14 
 Pct Recovery = 90%  Analysis Date = 04/01/14 
 Pct Recovery = 90%  Analysis Date = 04/01/14 
 Pct Recovery = 90%  Analysis Date = 03/30/14 
 Pct Recovery = 90%  Analysis Date = 03/30/14 
 Pct Recovery = 90%  Analysis Date = 03/28/14 
 Pct Recovery = 90%  Analysis Date = 03/28/14 
 Pct Recovery = 90%  Analysis Date = 03/26/14 
 Pct Recovery = 90%  Analysis Date = 03/26/14 
 Pct Recovery = 90%  Analysis Date = 03/24/14 
 Pct Recovery = 90%  Analysis Date = 03/24/14 
 Pct Recovery = 90%  Analysis Date = 03/22/14 
 Pct Recovery = 91%  Analysis Date = 03/22/14 
 Pct Recovery = 91%  Analysis Date = 03/20/14 
 Pct Recovery = 91%  Analysis Date = 03/20/14 
 Pct Recovery = 91%  Analysis Date = 03/18/14 
 Pct Recovery = 91%  Analysis Date = 03/18/14 
 Pct Recovery = 91%  Analysis Date = 03/16/14 
 Pct Recovery = 91%  Analysis Date = 03/16/14 
 Pct Recovery = 91%  Analysis Date = 03/14/14 
 Pct Recovery = 91%  Analysis Date = 03/14/14 
 Pct Recovery = 91%  Analysis Date = 03/12/14 
 Pct Recovery = 91%  Analysis Date = 03/12/14 
 Pct Recovery = 91%  Analysis Date = 03/10/14 
 Pct Recovery = 92%  Analysis Date = 03/10/14 
 Pct Recovery = 92%  Analysis Date = 03/08/14 
 Pct Recovery = 92%  Analysis Date = 03/08/14 
 Pct Recovery = 92%  Analysis Date = 03/06/14 
 Pct Recovery = 92%  Analysis Date = 03/06/14 
 Pct Recovery = 92%  Analysis Date = 03/04/14 
 Pct Recovery = 92%  Analysis Date = 03/04/14 
 Pct Recovery = 92%  Analysis Date = 03/02/14 
 Pct Recovery = 92%  Analysis Date = 03/02/14 
 Pct Recovery = 92%  Analysis Date = 02/28/14 
 Pct Recovery = 92%  Analysis Date = 02/28/14 
 Pct Recovery = 92%  Analysis Date = 02/26/14 
 Pct Recovery = 93%  Analysis Date = 02/26/14 
 Pct Recovery = 93%  Analysis Date = 02/24/14 
 Pct Recovery = 93%  Analysis Date = 02/24/14 
 Pct Recovery = 93%  Analysis Date = 02/22/14 
 Pct Recovery = 93%  Analysis Date = 02/22/14 
 Pct Recovery = 93%  Analysis Date = 02/20/14 
 Pct Recovery = 93%  Analysis Date = 02/20/14 
 Pct Recovery = 93%  Analysis Date = 02/18/14 
 Pct Recovery = 93%  Analysis Date = 02/18/14 
 Pct Recovery = 93%  Analysis Date = 02/16/14 
 Pct Recovery = 93%  Analysis Date = 02/16/14 
 Pct Recovery = 93%  Analysis Date = 02/14/14 
 Pct Recovery = 94%  Analysis Date = 02/14/14 
 Pct Recovery = 94%  Analysis Date = 02/12/14 
 Pct Recovery = 94%  Analysis Date = 02/12/14 
 Pct Recovery = 94%  Analysis Date = 02/10/14 
 Pct Recovery = 94%  Analysis Date = 02/10/14 
 Pct Recovery = 94%  Analysis Date = 02/08/14 
 Pct Recovery = 94%  Analysis Date = 02/08/14 
 Pct Recovery = 94%  Analysis Date = 02/06/14 
 Pct Recovery = 94%  Analysis Date = 02/06/14 
 Pct Recovery = 94%  Analysis Date = 02/04/14 
 Pct Recovery = 94%  Analysis Date = 02/04/14 
 Pct Recovery = 94%  Analysis Date = 02/02/14 
 Pct Recovery = 95%  Analysis Date = 02/02/14 
 Pct Recovery = 95%  Analysis Date = 01/30/14 
 Pct Recovery = 95%  Analysis Date = 01/30/14 
 Pct Recovery = 95%  Analysis Date = 01/28/14 
 Pct Recovery = 95%  Analysis Date = 01/28/14 
 Pct Recovery = 95%  Analysis Date = 01/26/14 
 Pct Recovery = 95%  Analysis Date = 01/26/14 
 Pct Recovery = 95%  Analysis Date = 01/24/14 
 Pct Recovery = 95%  Analysis Date = 01/24/14 
 Pct Recovery = 95%  Analysis Date = 01/22/14 
 Pct Recovery = 95%  Analysis Date = 01/22/14 
 Pct Recovery = 95%  Analysis Date = 01/20/14 
 Pct Recovery = 96%  Analysis Date = 01/20/14 
 Pct Recovery = 96%  Analysis Date = 01/18/14 
 Pct Recovery = 96%  Analysis Date = 01/18/14 
 Pct Recovery = 96%  Analysis Date = 01/16/14 
 Pct Recovery = 96%  Analysis Date = 01/16/14 
 Pct Recovery = 96%  Analysis Date = 01/14/14 
 Pct Recovery = 96%  Analysis Date = 01/14/14 
 Pct Recovery = 96%  Analysis Date = 01/12/14 
 Pct Recovery = 96%  Analysis Date = 01/12/14 
 Pct Recovery = 96%  Analysis Date = 01/10/14 
 Pct Recovery = 96%  Analysis Date = 01/10/14 
 Pct Recovery = 96%  Analysis Date = 01/08/14 
 Pct Recovery = 96%  Analysis Date = 01/08/14 
 Pct Recovery = 96%  Analysis Date = 01/06/14 
 Pct Recovery = 96%  Analysis Date = 01/06/14 
 Pct Recovery = 96%  Analysis Date = 01/04/14 
 Pct Recovery = 96%  Analysis Date = 01/04/14 
 Pct Recovery = 96%  Analysis Date = 01/02/14 
 Pct Recovery = 96%  Analysis Date = 01/02/14 
 Pct Recovery = 96%  Analysis Date = 12/31/13 
 Pct Recovery = 95%  Analysis Date = 12/31/13 
 Pct Recovery = 95%  Analysis Date = 12/29/13 
 Pct Recovery = 95%  Analysis Date = 12/29/13 
 Pct Recovery = 95%  Analysis Date = 12/27/13 
 Pct Recovery = 95%  Analysis Date = 12/27/13 
 Pct Recovery = 95%  Analysis Date = 12/25/13 
 Pct Recovery = 95%  Analysis Date = 12/25/13 
 Pct Recovery = 95%  Analysis Date = 12/23/13 
 Pct Recovery = 95%  Analysis Date = 12/23/13 
 Pct Recovery = 95%  Analysis Date = 12/21/13 
 Pct Recovery = 95%  Analysis Date = 12/21/13 
 Pct Recovery = 95%  Analysis Date = 12/19/13 
 Pct Recovery = 95%  Analysis Date = 12/19/13 
 Pct Recovery = 95%  Analysis Date = 12/17/13 
 Pct Recovery = 95%  Analysis Date = 12/17/13 
 Pct Recovery = 95%  Analysis Date = 12/15/13 
 Pct Recovery = 95%  Analysis Date = 12/15/13 
 Pct Recovery = 95%  Analysis Date = 12/13/13 
 Pct Recovery = 95%  Analysis Date = 12/13/13 
 Pct Recovery = 95%  Analysis Date = 12/11/13 
 Pct Recovery = 95%  Analysis Date = 12/11/13 
 Pct Recovery = 95%  Analysis Date = 12/09/13 
 Pct Recovery = 95%  Analysis Date = 12/09/13 
 Pct Recovery = 95%  Analysis Date = 12/07/13 
 Pct Recovery = 95%  Analysis Date = 12/07/13 
 Pct Recovery = 95%  Analysis Date = 12/05/13 
 Pct Recovery = 95%  Analysis Date = 12/05/13 
 Pct Recovery = 95%  Analysis Date = 12/03/13 
 Pct Recovery = 95%  Analysis Date = 12/03/13 
 Pct Recovery = 95%  Analysis Date = 12/01/13 
 Pct Recovery = 95%  Analysis Date = 12/01/13 
 Pct Recovery = 95%  Analysis Date = 11/29/13 
 Pct Recovery = 95%  Analysis Date = 11/29/13 
 Pct Recovery = 95%  Analysis Date = 11/27/13 
 Pct Recovery = 95%  Analysis Date = 11/27/13 
 Pct Recovery = 95%  Analysis Date = 11/24/13 
 Pct Recovery = 95%  Analysis Date = 11/24/13 
 Pct Recovery = 95%  Analysis Date = 11/22/13 
 Pct Recovery = 95%  Analysis Date = 11/22/13 
 Pct Recovery = 95%  Analysis Date = 11/20/13 
 Pct Recovery = 95%  Analysis Date = 11/20/13 
 Pct Recovery = 95%  Analysis Date = 11/18/13 
 Pct Recovery = 95%  Analysis Date = 11/18/13 
 Pct Recovery = 95%  Analysis Date = 11/16/13 
 Pct Recovery = 95%  Analysis Date = 11/16/13 
 Pct Recovery = 95%  Analysis Date = 11/14/13 
 Pct Recovery = 95%  Analysis Date = 11/14/13 
 Pct Recovery = 95%  Analysis Date = 11/12/13 
 Pct Recovery = 95%  Analysis Date = 11/12/13 
 Pct Recovery = 95%  Analysis Date = 11/10/13 
 Pct Recovery = 95%  Analysis Date = 11/10/13 
 Pct Recovery = 95%  Analysis Date = 11/08/13 
 Pct Recovery = 95%  Analysis Date = 11/08/13 
 Pct Recovery = 95%  Analysis Date = 11/06/13 
 Pct Recovery = 95%  Analysis Date = 11/06/13 
 Pct Recovery = 95%  Analysis Date = 11/04/13 
 Pct Recovery = 95%  Analysis Date = 11/04/13 
 Pct Recovery = 95%  Analysis Date = 11/02/13 
 Pct Recovery = 95%  Analysis Date = 11/02/13 
 Pct Recovery = 95%  Analysis Date = 10/31/13 
 Pct Recovery = 96%  Analysis Date = 10/31/13 
 Pct Recovery = 96%  Analysis Date = 10/29/13 
 Pct Recovery = 96%  Analysis Date = 10/29/13 
 Pct Recovery = 96%  Analysis Date = 10/27/13 
 Pct Recovery = 96%  Analysis Date = 10/27/13 
 Pct Recovery = 96%  Analysis Date = 10/25/13 
 Pct Recovery = 96%  Analysis Date = 10/25/13 
 Pct Recovery = 96%  Analysis Date = 10/23/13 
 Pct Recovery = 96%  Analysis Date = 10/23/13 
 Pct Recovery = 96%  Analysis Date = 10/21/13 
 Pct Recovery = 96%  Analysis Date = 10/21/13 
 Pct Recovery = 96%  Analysis Date = 10/19/13 
 Pct Recovery = 95%  Analysis Date = 10/19/13 
 Pct Recovery = 95%  Analysis Date = 10/17/13 
 Pct Recovery = 95%  Analysis Date = 10/17/13 
 Pct Recovery = 95%  Analysis Date = 10/15/13 
 Pct Recovery = 95%  Analysis Date = 10/15/13 
 Pct Recovery = 95%  Analysis Date = 10/13/13 
 Pct Recovery = 95%  Analysis Date = 10/13/13 
 Pct Recovery = 95%  Analysis Date = 10/11/13 
 Pct Recovery = 95%  Analysis Date = 10/11/13 
 Pct Recovery = 95%  Analysis Date = 10/09/13 
 Pct Recovery = 95%  Analysis Date = 10/09/13 
 Pct Recovery = 95%  Analysis Date = 10/07/13 
 Pct Recovery = 95%  Analysis Date = 10/07/13 
 Pct Recovery = 95%  Analysis Date = 10/05/13 
 Pct Recovery = 95%  Analysis Date = 10/05/13 
 Pct Recovery = 95%  Analysis Date = 10/03/13 
 Pct Recovery = 95%  Analysis Date = 10/03/13 
 Pct Recovery = 95%  Analysis Date = 10/01/13 
 Pct Recovery = 95%  Analysis Date = 10/01/13 
 Pct Recovery = 95%  Analysis Date = 09/29/13 
 Pct Recovery = 95%  Analysis Date = 09/29/13 
 Pct Recovery = 95%  Analysis Date = 09/27/13 
 Pct Recovery = 95%  Analysis Date = 09/27/13 
 Pct Recovery = 95%  Analysis Date = 09/25/13 
 Pct Recovery = 95%  Analysis Date = 09/25/13 
 Pct Recovery = 95%  Analysis Date = 09/23/13 
 Pct Recovery = 95%  Analysis Date = 09/23/13 
 Pct Recovery = 95%  Analysis Date = 09/21/13 
 Pct Recovery = 95%  Analysis Date = 09/21/13 
 Pct Recovery = 95%  Analysis Date = 09/18/13 
 Pct Recovery = 95%  Analysis Date = 09/18/13 
 Pct Recovery = 95%  Analysis Date = 09/16/13 
 Pct Recovery = 95%  Analysis Date = 09/16/13 
 Pct Recovery = 95%  Analysis Date = 09/14/13 
 Pct Recovery = 95%  Analysis Date = 09/14/13 
 Pct Recovery = 95%  Analysis Date = 09/12/13 
 Pct Recovery = 95%  Analysis Date = 09/12/13 
 Pct Recovery = 95%  Analysis Date = 09/10/13 
 Pct Recovery = 95%  Analysis Date = 09/10/13 
 Pct Recovery = 95%  Analysis Date = 09/08/13 
 Pct Recovery = 95%  Analysis Date = 09/08/13 
 Pct Recovery = 95%  Analysis Date = 09/06/13 
 Pct Recovery = 95%  Analysis Date = 09/06/13 
 Pct Recovery = 95%  Analysis Date = 09/04/13 
 Pct Recovery = 95%  Analysis Date = 09/04/13 
 Pct Recovery = 95%  Analysis Date = 09/02/13 
 Pct Recovery = 95%  Analysis Date = 09/02/13 
 Pct Recovery = 95%  Analysis Date = 08/31/13 
 Pct Recovery = 95%  Analysis Date = 08/31/13 
 Pct Recovery = 95%  Analysis Date = 08/29/13 
 Pct Recovery = 95%  Analysis Date = 08/29/13 
 Pct Recovery = 95%  Analysis Date = 08/27/13 
 Pct Recovery = 95%  Analysis Date = 08/27/13 
 Pct Recovery = 95%  Analysis Date = 08/25/13 
 Pct Recovery = 95%  Analysis Date = 08/25/13 
 Pct Recovery = 95%  Analysis Date = 08/23/13 
 Pct Recovery = 95%  Analysis Date = 08/23/13 
 Pct Recovery = 95%  Analysis Date = 08/21/13 
 Pct Recovery = 95%  Analysis Date = 08/21/13 
 Pct Recovery = 95%  Analysis Date = 08/19/13 
 Pct Recovery = 95%  Analysis Date = 08/19/13 
 Pct Recovery = 95%  Analysis Date = 08/17/13 
 Pct Recovery = 95%  Analysis Date = 08/17/13 
 Pct Recovery = 95%  Analysis Date = 08/15/13 
 Pct Recovery = 95%  Analysis Date = 08/15/13 
 Pct Recovery = 95%  Analysis Date = 08/13/13 
 Pct Recovery = 95%  Analysis Date = 08/13/13 
 Pct Recovery = 95%  Analysis Date = 08/11/13 
 Pct Recovery = 95%  Analysis Date = 08/11/13 
 Pct Recovery = 95%  Analysis Date = 08/09/13 
 Pct Recovery = 95%  Analysis Date = 08/09/13 
 Pct Recovery = 95%  Analysis Date = 08/07/13 
 Pct Recovery = 95%  Analysis Date = 08/07/13 
 Pct Recovery = 95%  Analysis Date = 08/05/13 
 Pct Recovery = 95%  Analysis Date = 08/05/13 
 Pct Recovery = 95%  Analysis Date = 08/03/13 
 Pct Recovery = 95%  Analysis Date = 08/03/13 
 Pct Recovery = 95%  Analysis Date = 08/01/13 
 Pct Recovery = 95%  Analysis Date = 08/01/13 
 Pct Recovery = 95%  Analysis Date = 07/30/13 
 Pct Recovery = 94%  Analysis Date = 07/30/13 
 Pct Recovery = 94%  Analysis Date = 07/28/13 
 Pct Recovery = 94%  Analysis Date = 07/28/13 
 Pct Recovery = 94%  Analysis Date = 07/26/13 
 Pct Recovery = 93%  Analysis Date = 07/26/13 
 Pct Recovery = 93%  Analysis Date = 07/24/13 
 Pct Recovery = 93%  Analysis Date = 07/24/13 
 Pct Recovery = 93%  Analysis Date = 07/22/13 
 Pct Recovery = 92%  Analysis Date = 07/22/13 
 Pct Recovery = 92%  Analysis Date = 07/20/13 
 Pct Recovery = 92%  Analysis Date = 07/20/13 
 Pct Recovery = 92%  Analysis Date = 07/18/13 
 Pct Recovery = 91%  Analysis Date = 07/18/13 
 Pct Recovery = 91%  Analysis Date = 07/16/13 
 Pct Recovery = 91%  Analysis Date = 07/16/13 
 Pct Recovery = 91%  Analysis Date = 07/14/13 
 Pct Recovery = 90%  Analysis Date = 07/14/13 
 Pct Recovery = 90%  Analysis Date = 07/11/13 
 Pct Recovery = 90%  Analysis Date = 07/11/13 
 Pct Recovery = 90%  Analysis Date = 07/09/13 
 Pct Recovery = 89%  Analysis Date = 07/09/13 
 Pct Recovery = 89%  Analysis Date = 07/07/13 
 Pct Recovery = 89%  Analysis Date = 07/07/13 
 Pct Recovery = 89%  Analysis Date = 07/05/13 
 Pct Recovery = 88%  Analysis Date = 07/05/13 
 Pct Recovery = 88%  Analysis Date = 07/03/13 
 Pct Recovery = 88%  Analysis Date = 07/03/13 
 Pct Recovery = 88%  Analysis Date = 07/01/13 
 Pct Recovery = 87%  Analysis Date = 07/01/13 
 Pct Recovery = 87%  Analysis Date = 06/29/13 
 Pct Recovery = 87%  Analysis Date = 06/29/13 
 Pct Recovery = 87%  Analysis Date = 06/27/13 
 Pct Recovery = 86%  Analysis Date = 06/27/13 
 Pct Recovery = 86%  Analysis Date = 06/25/13 
 Pct Recovery = 86%  Analysis Date = 06/25/13 
 Pct Recovery = 86%  Analysis Date = 06/23/13 
 Pct Recovery = 85%  Analysis Date = 06/23/13 
 Pct Recovery = 85%  Analysis Date = 06/21/13 
 Pct Recovery = 85%  Analysis Date = 06/21/13 
 Pct Recovery = 85%  Analysis Date = 06/19/13 
 Pct Recovery = 84%  Analysis Date = 06/19/13 
 Pct Recovery = 84%  Analysis Date = 06/17/13 
 Pct Recovery = 84%  Analysis Date = 06/17/13 
 Pct Recovery = 84%  Analysis Date = 06/15/13 
 Pct Recovery = 83%  Analysis Date = 06/15/13 
 Pct Recovery = 83%  Analysis Date = 06/13/13 
 Pct Recovery = 83%  Analysis Date = 06/13/13 
 Pct Recovery = 83%  Analysis Date = 06/11/13 
 Pct Recovery = 82%  Analysis Date = 06/11/13 
 Pct Recovery = 82%  Analysis Date = 06/09/13 
 Pct Recovery = 82%  Analysis Date = 06/09/13 
 Pct Recovery = 82%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/07/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/05/13 
 Pct Recovery = 81%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 06/03/13 
 Pct Recovery = 80%  Analysis Date = 06/01/13 
 Pct Recovery = 80%  Analysis Date = 06/01/13 
 Pct Recovery = 80%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/30/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 79%  Analysis Date = 05/28/13 
 Pct Recovery = 79%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/26/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/24/13 
 Pct Recovery = 78%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/22/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 77%  Analysis Date = 05/20/13 
 Pct Recovery = 77%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/18/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/16/13 
 Pct Recovery = 76%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/14/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/12/13 
 Pct Recovery = 75%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/10/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/08/13 
 Pct Recovery = 74%  Analysis Date = 05/05/13 
 Pct Recovery = 74%  Analysis Date = 05/05/13 
 Pct Recovery = 74%  Analysis Date = 05/03/13 
 Pct Recovery = 73%  Analysis Date = 05/03/13 
 Pct Recovery = 73%  Analysis Date = 05/01/13 
 Pct Recovery = 73%  Analysis Date = 05/01/13 
 Pct Recovery = 73%  Analysis Date = 04/29/13 
 Pct Recovery = 73%  Analysis Date = 04/29/13 
 Pct Recovery = 73%  Analysis Date = 04/27/13 
 Pct Recovery = 74%  Analysis Date = 04/27/13 
 Pct Recovery = 74%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/25/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/23/13 
 Pct Recovery = 74%  Analysis Date = 04/21/13 
 Pct Recovery = 74%  Analysis Date = 04/21/13 
 Pct Recovery = 74%  Analysis Date = 04/19/13 
 Pct Recovery = 75%  Analysis Date = 04/19/13 
 Pct Recovery = 75%  Analysis Date = 04/17/13 
 Pct Recovery = 75%  Analysis Date = 04/17/13 
 Pct Recovery = 75%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/15/13 
 Pct Recovery = 75%  Analysis Date = 04/13/13 
 Pct Recovery = 76%  Analysis Date = 04/13/13 
 Pct Recovery = 76%  Analysis Date = 04/11/13 
 Pct Recovery = 76%  Analysis Date = 04/11/13 
 Pct Recovery = 76%  Analysis Date = 04/09/13 
 Pct Recovery = 76%  Analysis Date = 04/09/13 
 Pct Recovery = 76%  Analysis Date = 04/07/13 
 Pct Recovery = 77%  Analysis Date = 04/07/13 
 Pct Recovery = 77%  Analysis Date = 04/05/13 
 Pct Recovery = 77%  Analysis Date = 04/05/13 
 Pct Recovery = 77%  Analysis Date = 04/03/13 
 Pct Recovery = 77%  Analysis Date = 04/03/13 
 Pct Recovery = 77%  Analysis Date = 04/01/13 
 Pct Recovery = 78%  Analysis Date = 04/01/13 
 Pct Recovery = 78%  Analysis Date = 03/30/13 
 Pct Recovery = 78%  Analysis Date = 03/30/13 
 Pct Recovery = 78%  Analysis Date = 03/28/13 
 Pct Recovery = 78%  Analysis Date = 03/28/13 
 Pct Recovery = 78%  Analysis Date = 03/26/13 
 Pct Recovery = 79%  Analysis Date = 03/26/13 
 Pct Recovery = 79%  Analysis Date = 03/24/13 
 Pct Recovery = 79%  Analysis Date = 03/24/13 
 Pct Recovery = 79%  Analysis Date = 03/22/13 
 Pct Recovery = 79%  Analysis Date = 03/22/13 
 Pct Recovery = 79%  Analysis Date = 03/20/13 
 Pct Recovery = 80%  Analysis Date = 03/20/13 
 Pct Recovery = 80%  Analysis Date = 03/18/13 
 Pct Recovery = 80%  Analysis Date = 03/18/13 
 Pct Recovery = 80%  Analysis Date = 03/16/13 
 Pct Recovery = 80%  Analysis Date = 03/16/13 
 Pct Recovery = 80%  Analysis Date = 03/14/13 
 Pct Recovery = 81%  Analysis Date = 03/14/13 
 Pct Recovery = 81%  Analysis Date = 03/12/13 
 Pct Recovery = 81%  Analysis Date = 03/12/13 
 Pct Recovery = 81%  Analysis Date = 03/10/13 
 Pct Recovery = 81%  Analysis Date = 03/10/13 
 Pct Recovery = 81%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/08/13 
 Pct Recovery = 82%  Analysis Date = 03/06/13 
 Pct Recovery = 82%  Analysis Date = 03/06/13 
 Pct Recovery = 82%  Analysis Date = 03/04/13 
 Pct Recovery = 82%  Analysis Date = 03/04/13 
 Pct Recovery = 82%  Analysis Date = 03/02/13 
 Pct Recovery = 82%  Analysis Date = 03/02/13 
 Pct Recovery = 82%  Analysis Date = 02/28/13 
 Pct Recovery = 83%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIAMTERENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 87% 18% 78% 21%
Total 11 87% 18% 78% 21%

Sample Statistics
TRIAMTERENE

Characteristic N % % Basis
Plotted 11 79% Spiked
Estimated Values 5 36% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 2 14% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
TRIMETHOPRIM
METHOD: LC9017 , TESTIDCODE: 67456LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 49%  Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 54%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 43%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 92%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 64%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 65%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 57%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 102%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 88%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 56%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 81%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 58%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 76%  Analysis Date = 04/09/14 
 Pct Recovery = 70%  Analysis Date = 04/07/14 
 Pct Recovery = 70%  Analysis Date = 04/07/14 
 Pct Recovery = 70%  Analysis Date = 04/05/14 
 Pct Recovery = 71%  Analysis Date = 04/05/14 
 Pct Recovery = 71%  Analysis Date = 04/02/14 
 Pct Recovery = 71%  Analysis Date = 04/02/14 
 Pct Recovery = 71%  Analysis Date = 03/31/14 
 Pct Recovery = 71%  Analysis Date = 03/31/14 
 Pct Recovery = 71%  Analysis Date = 03/28/14 
 Pct Recovery = 71%  Analysis Date = 03/28/14 
 Pct Recovery = 71%  Analysis Date = 03/26/14 
 Pct Recovery = 71%  Analysis Date = 03/26/14 
 Pct Recovery = 71%  Analysis Date = 03/24/14 
 Pct Recovery = 71%  Analysis Date = 03/24/14 
 Pct Recovery = 71%  Analysis Date = 03/21/14 
 Pct Recovery = 71%  Analysis Date = 03/21/14 
 Pct Recovery = 71%  Analysis Date = 03/19/14 
 Pct Recovery = 71%  Analysis Date = 03/19/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/16/14 
 Pct Recovery = 71%  Analysis Date = 03/14/14 
 Pct Recovery = 72%  Analysis Date = 03/14/14 
 Pct Recovery = 72%  Analysis Date = 03/12/14 
 Pct Recovery = 72%  Analysis Date = 03/12/14 
 Pct Recovery = 72%  Analysis Date = 03/09/14 
 Pct Recovery = 72%  Analysis Date = 03/09/14 
 Pct Recovery = 72%  Analysis Date = 03/07/14 
 Pct Recovery = 72%  Analysis Date = 03/07/14 
 Pct Recovery = 72%  Analysis Date = 03/04/14 
 Pct Recovery = 72%  Analysis Date = 03/04/14 
 Pct Recovery = 72%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 03/02/14 
 Pct Recovery = 72%  Analysis Date = 02/28/14 
 Pct Recovery = 72%  Analysis Date = 02/28/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/25/14 
 Pct Recovery = 72%  Analysis Date = 02/23/14 
 Pct Recovery = 73%  Analysis Date = 02/23/14 
 Pct Recovery = 73%  Analysis Date = 02/20/14 
 Pct Recovery = 73%  Analysis Date = 02/20/14 
 Pct Recovery = 73%  Analysis Date = 02/18/14 
 Pct Recovery = 73%  Analysis Date = 02/18/14 
 Pct Recovery = 73%  Analysis Date = 02/15/14 
 Pct Recovery = 73%  Analysis Date = 02/15/14 
 Pct Recovery = 73%  Analysis Date = 02/13/14 
 Pct Recovery = 73%  Analysis Date = 02/13/14 
 Pct Recovery = 73%  Analysis Date = 02/11/14 
 Pct Recovery = 73%  Analysis Date = 02/11/14 
 Pct Recovery = 73%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/08/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/06/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/03/14 
 Pct Recovery = 73%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 02/01/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/30/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/27/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/25/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/22/14 
 Pct Recovery = 74%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/20/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/18/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/15/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/13/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/10/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/08/14 
 Pct Recovery = 74%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/06/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/03/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 01/01/14 
 Pct Recovery = 73%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/29/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/27/13 
 Pct Recovery = 73%  Analysis Date = 12/24/13 
 Pct Recovery = 72%  Analysis Date = 12/24/13 
 Pct Recovery = 72%  Analysis Date = 12/22/13 
 Pct Recovery = 72%  Analysis Date = 12/22/13 
 Pct Recovery = 72%  Analysis Date = 12/20/13 
 Pct Recovery = 72%  Analysis Date = 12/20/13 
 Pct Recovery = 72%  Analysis Date = 12/17/13 
 Pct Recovery = 72%  Analysis Date = 12/17/13 
 Pct Recovery = 72%  Analysis Date = 12/15/13 
 Pct Recovery = 72%  Analysis Date = 12/15/13 
 Pct Recovery = 72%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/12/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/10/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/08/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/05/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 12/03/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/30/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/28/13 
 Pct Recovery = 71%  Analysis Date = 11/26/13 
 Pct Recovery = 70%  Analysis Date = 11/26/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/23/13 
 Pct Recovery = 70%  Analysis Date = 11/21/13 
 Pct Recovery = 70%  Analysis Date = 11/21/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/18/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/16/13 
 Pct Recovery = 70%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/13/13 
 Pct Recovery = 71%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/11/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/09/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/06/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/04/13 
 Pct Recovery = 71%  Analysis Date = 11/01/13 
 Pct Recovery = 72%  Analysis Date = 11/01/13 
 Pct Recovery = 72%  Analysis Date = 10/30/13 
 Pct Recovery = 72%  Analysis Date = 10/30/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/28/13 
 Pct Recovery = 72%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/25/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/23/13 
 Pct Recovery = 72%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/20/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/18/13 
 Pct Recovery = 71%  Analysis Date = 10/16/13 
 Pct Recovery = 71%  Analysis Date = 10/16/13 
 Pct Recovery = 71%  Analysis Date = 10/13/13 
 Pct Recovery = 71%  Analysis Date = 10/13/13 
 Pct Recovery = 71%  Analysis Date = 10/11/13 
 Pct Recovery = 71%  Analysis Date = 10/11/13 
 Pct Recovery = 71%  Analysis Date = 10/08/13 
 Pct Recovery = 71%  Analysis Date = 10/08/13 
 Pct Recovery = 71%  Analysis Date = 10/06/13 
 Pct Recovery = 71%  Analysis Date = 10/06/13 
 Pct Recovery = 71%  Analysis Date = 10/04/13 
 Pct Recovery = 70%  Analysis Date = 10/04/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 10/01/13 
 Pct Recovery = 70%  Analysis Date = 09/29/13 
 Pct Recovery = 70%  Analysis Date = 09/29/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/26/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/24/13 
 Pct Recovery = 70%  Analysis Date = 09/21/13 
 Pct Recovery = 70%  Analysis Date = 09/21/13 
 Pct Recovery = 70%  Analysis Date = 09/19/13 
 Pct Recovery = 70%  Analysis Date = 09/19/13 
 Pct Recovery = 70%  Analysis Date = 09/17/13 
 Pct Recovery = 70%  Analysis Date = 09/17/13 
 Pct Recovery = 70%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/14/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/12/13 
 Pct Recovery = 69%  Analysis Date = 09/09/13 
 Pct Recovery = 69%  Analysis Date = 09/09/13 
 Pct Recovery = 69%  Analysis Date = 09/07/13 
 Pct Recovery = 69%  Analysis Date = 09/07/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/05/13 
 Pct Recovery = 69%  Analysis Date = 09/02/13 
 Pct Recovery = 69%  Analysis Date = 09/02/13 
 Pct Recovery = 69%  Analysis Date = 08/31/13 
 Pct Recovery = 69%  Analysis Date = 08/31/13 
 Pct Recovery = 69%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/28/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/26/13 
 Pct Recovery = 68%  Analysis Date = 08/24/13 
 Pct Recovery = 68%  Analysis Date = 08/24/13 
 Pct Recovery = 68%  Analysis Date = 08/21/13 
 Pct Recovery = 68%  Analysis Date = 08/21/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/19/13 
 Pct Recovery = 68%  Analysis Date = 08/16/13 
 Pct Recovery = 68%  Analysis Date = 08/16/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/14/13 
 Pct Recovery = 68%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/09/13 
 Pct Recovery = 67%  Analysis Date = 08/09/13 
 Pct Recovery = 67%  Analysis Date = 08/07/13 
 Pct Recovery = 67%  Analysis Date = 08/07/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/23/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/21/13 
 Pct Recovery = 66%  Analysis Date = 07/18/13 
 Pct Recovery = 66%  Analysis Date = 07/18/13 
 Pct Recovery = 66%  Analysis Date = 07/16/13 
 Pct Recovery = 66%  Analysis Date = 07/16/13 
 Pct Recovery = 66%  Analysis Date = 07/14/13 
 Pct Recovery = 66%  Analysis Date = 07/14/13 
 Pct Recovery = 66%  Analysis Date = 07/11/13 
 Pct Recovery = 66%  Analysis Date = 07/11/13 
 Pct Recovery = 66%  Analysis Date = 07/09/13 
 Pct Recovery = 66%  Analysis Date = 07/09/13 
 Pct Recovery = 66%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 06/29/13 
 Pct Recovery = 65%  Analysis Date = 06/29/13 
 Pct Recovery = 65%  Analysis Date = 06/27/13 
 Pct Recovery = 65%  Analysis Date = 06/27/13 
 Pct Recovery = 65%  Analysis Date = 06/24/13 
 Pct Recovery = 65%  Analysis Date = 06/24/13 
 Pct Recovery = 65%  Analysis Date = 06/22/13 
 Pct Recovery = 65%  Analysis Date = 06/22/13 
 Pct Recovery = 65%  Analysis Date = 06/19/13 
 Pct Recovery = 65%  Analysis Date = 06/19/13 
 Pct Recovery = 65%  Analysis Date = 06/17/13 
 Pct Recovery = 65%  Analysis Date = 06/17/13 
 Pct Recovery = 65%  Analysis Date = 06/15/13 
 Pct Recovery = 65%  Analysis Date = 06/15/13 
 Pct Recovery = 65%  Analysis Date = 06/12/13 
 Pct Recovery = 65%  Analysis Date = 06/12/13 
 Pct Recovery = 65%  Analysis Date = 06/10/13 
 Pct Recovery = 65%  Analysis Date = 06/10/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 64%  Analysis Date = 06/05/13 
 Pct Recovery = 64%  Analysis Date = 06/03/13 
 Pct Recovery = 64%  Analysis Date = 06/03/13 
 Pct Recovery = 64%  Analysis Date = 05/31/13 
 Pct Recovery = 64%  Analysis Date = 05/31/13 
 Pct Recovery = 64%  Analysis Date = 05/29/13 
 Pct Recovery = 64%  Analysis Date = 05/29/13 
 Pct Recovery = 64%  Analysis Date = 05/26/13 
 Pct Recovery = 64%  Analysis Date = 05/26/13 
 Pct Recovery = 64%  Analysis Date = 05/24/13 
 Pct Recovery = 64%  Analysis Date = 05/24/13 
 Pct Recovery = 64%  Analysis Date = 05/22/13 
 Pct Recovery = 64%  Analysis Date = 05/22/13 
 Pct Recovery = 64%  Analysis Date = 05/19/13 
 Pct Recovery = 64%  Analysis Date = 05/19/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/17/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/14/13 
 Pct Recovery = 64%  Analysis Date = 05/12/13 
 Pct Recovery = 63%  Analysis Date = 05/12/13 
 Pct Recovery = 63%  Analysis Date = 05/10/13 
 Pct Recovery = 63%  Analysis Date = 05/10/13 
 Pct Recovery = 63%  Analysis Date = 05/07/13 
 Pct Recovery = 63%  Analysis Date = 05/07/13 
 Pct Recovery = 63%  Analysis Date = 05/05/13 
 Pct Recovery = 63%  Analysis Date = 05/05/13 
 Pct Recovery = 63%  Analysis Date = 05/02/13 
 Pct Recovery = 63%  Analysis Date = 05/02/13 
 Pct Recovery = 63%  Analysis Date = 04/30/13 
 Pct Recovery = 63%  Analysis Date = 04/30/13 
 Pct Recovery = 63%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/27/13 
 Pct Recovery = 63%  Analysis Date = 04/25/13 
 Pct Recovery = 63%  Analysis Date = 04/25/13 
 Pct Recovery = 63%  Analysis Date = 04/23/13 
 Pct Recovery = 63%  Analysis Date = 04/23/13 
 Pct Recovery = 63%  Analysis Date = 04/20/13 
 Pct Recovery = 62%  Analysis Date = 04/20/13 
 Pct Recovery = 62%  Analysis Date = 04/18/13 
 Pct Recovery = 62%  Analysis Date = 04/18/13 
 Pct Recovery = 62%  Analysis Date = 04/15/13 
 Pct Recovery = 62%  Analysis Date = 04/15/13 
 Pct Recovery = 62%  Analysis Date = 04/13/13 
 Pct Recovery = 62%  Analysis Date = 04/13/13 
 Pct Recovery = 62%  Analysis Date = 04/11/13 
 Pct Recovery = 62%  Analysis Date = 04/11/13 
 Pct Recovery = 62%  Analysis Date = 04/08/13 
 Pct Recovery = 62%  Analysis Date = 04/08/13 
 Pct Recovery = 62%  Analysis Date = 04/06/13 
 Pct Recovery = 62%  Analysis Date = 04/06/13 
 Pct Recovery = 62%  Analysis Date = 04/03/13 
 Pct Recovery = 62%  Analysis Date = 04/03/13 
 Pct Recovery = 62%  Analysis Date = 04/01/13 
 Pct Recovery = 62%  Analysis Date = 04/01/13 
 Pct Recovery = 62%  Analysis Date = 03/30/13 
 Pct Recovery = 62%  Analysis Date = 03/30/13 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 Pct Recovery = 62%  Analysis Date = 03/25/13 
 Pct Recovery = 62%  Analysis Date = 03/25/13 
 Pct Recovery = 62%  Analysis Date = 03/22/13 
 Pct Recovery = 61%  Analysis Date = 03/22/13 
 Pct Recovery = 61%  Analysis Date = 03/20/13 
 Pct Recovery = 61%  Analysis Date = 03/20/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/15/13 
 Pct Recovery = 61%  Analysis Date = 03/15/13 
 Pct Recovery = 61%  Analysis Date = 03/13/13 
 Pct Recovery = 61%  Analysis Date = 03/13/13 
 Pct Recovery = 61%  Analysis Date = 03/10/13 
 Pct Recovery = 61%  Analysis Date = 03/10/13 
 Pct Recovery = 61%  Analysis Date = 03/08/13 
 Pct Recovery = 61%  Analysis Date = 03/08/13 
 Pct Recovery = 61%  Analysis Date = 03/05/13 
 Pct Recovery = 61%  Analysis Date = 03/05/13 
 Pct Recovery = 61%  Analysis Date = 03/03/13 
 Pct Recovery = 61%  Analysis Date = 03/03/13 
 Pct Recovery = 61%  Analysis Date = 03/01/13 
 Pct Recovery = 61%  Analysis Date = 03/01/13 
 Pct Recovery = 61%  Analysis Date = 02/26/13 
 Pct Recovery = 61%  Analysis Date = 02/26/13 
 Pct Recovery = 61%  Analysis Date = 02/24/13 
 Pct Recovery = 61%  Analysis Date = 02/24/13 
 Pct Recovery = 61%  Analysis Date = 02/21/13 
 Pct Recovery = 61%  Analysis Date = 02/21/13 
 Pct Recovery = 61%  Analysis Date = 02/19/13 
 Pct Recovery = 61%  Analysis Date = 02/19/13 
 Pct Recovery = 61%  Analysis Date = 02/17/13 
 Pct Recovery = 61%  Analysis Date = 02/17/13 
 Pct Recovery = 61%  Analysis Date = 02/14/13 
 Pct Recovery = 61%  Analysis Date = 02/14/13 
 Pct Recovery = 61%  Analysis Date = 02/12/13 
 Pct Recovery = 61%  Analysis Date = 02/12/13 
 Pct Recovery = 61%  Analysis Date = 02/09/13 
 Pct Recovery = 61%  Analysis Date = 02/09/13 
 Pct Recovery = 61%  Analysis Date = 02/07/13 
 Pct Recovery = 60%  Analysis Date = 02/07/13 
 Pct Recovery = 60%  Analysis Date = 02/05/13 
 Pct Recovery = 60%  Analysis Date = 02/05/13 
 Pct Recovery = 60%  Analysis Date = 02/02/13 
 Pct Recovery = 60%  Analysis Date = 02/02/13 
 Pct Recovery = 60%  Analysis Date = 01/31/13 
 Pct Recovery = 60%  Analysis Date = 01/31/13 
 Pct Recovery = 60%  Analysis Date = 01/28/13 
 Pct Recovery = 60%  Analysis Date = 01/28/13 
 Pct Recovery = 60%  Analysis Date = 01/26/13 
 Pct Recovery = 60%  Analysis Date = 01/26/13 
 Pct Recovery = 60%  Analysis Date = 01/23/13 
 Pct Recovery = 60%  Analysis Date = 01/23/13 
 Pct Recovery = 60%  Analysis Date = 01/21/13 
 Pct Recovery = 60%  Analysis Date = 01/21/13 
 Pct Recovery = 60%  Analysis Date = 01/19/13 
 Pct Recovery = 60%  Analysis Date = 01/19/13 
 Pct Recovery = 60%  Analysis Date = 01/16/13 
 Pct Recovery = 60%  Analysis Date = 01/16/13 
 Pct Recovery = 60%  Analysis Date = 01/14/13 
 Pct Recovery = 60%  Analysis Date = 01/14/13 
 Pct Recovery = 60%  Analysis Date = 01/11/13 
 Pct Recovery = 60%  Analysis Date = 01/11/13 
 Pct Recovery = 60%  Analysis Date = 01/09/13 
 Pct Recovery = 60%  Analysis Date = 01/09/13 
 Pct Recovery = 60%  Analysis Date = 01/07/13 
 Pct Recovery = 60%  Analysis Date = 01/07/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/02/13 
 Pct Recovery = 60%  Analysis Date = 01/02/13 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/28/12 
 Pct Recovery = 60%  Analysis Date = 12/28/12 
 Pct Recovery = 60%  Analysis Date = 12/26/12 
 Pct Recovery = 60%  Analysis Date = 12/26/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 60%  Analysis Date = 12/16/12 
 Pct Recovery = 60%  Analysis Date = 12/16/12 
 Pct Recovery = 60%  Analysis Date = 12/14/12 
 Pct Recovery = 60%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIMETHOPRIM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 76% . 76% 0%
>= Reporting Level 13 67% 18% 60% 18%
Total 14 68% 18% 62% 18%

Sample Statistics
TRIMETHOPRIM

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
VALACYCLOVIR
METHOD: LC9017 , TESTIDCODE: 67507LCM56

 Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 9%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 4%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
VALACYCLOVIR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 6% 4% 6% 4%
Total 2 6% 4% 6% 4%

Sample Statistics
VALACYCLOVIR

Characteristic N % % Basis
Plotted 2 14% Spiked
Estimated Values 2 14% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 12 86% 12 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
VENLAFAXINE
METHOD: LC9017 , TESTIDCODE: 67534LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 60%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 63%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 58%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 38%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 54%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 65%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 78%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 57%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 64%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 70%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 55%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 45%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 67%  Analysis Date = 04/09/14 
 Pct Recovery = 43%  Analysis Date = 04/07/14 
 Pct Recovery = 43%  Analysis Date = 04/07/14 
 Pct Recovery = 43%  Analysis Date = 04/05/14 
 Pct Recovery = 44%  Analysis Date = 04/05/14 
 Pct Recovery = 44%  Analysis Date = 04/02/14 
 Pct Recovery = 44%  Analysis Date = 04/02/14 
 Pct Recovery = 44%  Analysis Date = 03/31/14 
 Pct Recovery = 44%  Analysis Date = 03/31/14 
 Pct Recovery = 44%  Analysis Date = 03/28/14 
 Pct Recovery = 45%  Analysis Date = 03/28/14 
 Pct Recovery = 45%  Analysis Date = 03/26/14 
 Pct Recovery = 45%  Analysis Date = 03/26/14 
 Pct Recovery = 45%  Analysis Date = 03/24/14 
 Pct Recovery = 45%  Analysis Date = 03/24/14 
 Pct Recovery = 45%  Analysis Date = 03/21/14 
 Pct Recovery = 46%  Analysis Date = 03/21/14 
 Pct Recovery = 46%  Analysis Date = 03/19/14 
 Pct Recovery = 46%  Analysis Date = 03/19/14 
 Pct Recovery = 46%  Analysis Date = 03/16/14 
 Pct Recovery = 46%  Analysis Date = 03/16/14 
 Pct Recovery = 46%  Analysis Date = 03/14/14 
 Pct Recovery = 47%  Analysis Date = 03/14/14 
 Pct Recovery = 47%  Analysis Date = 03/12/14 
 Pct Recovery = 47%  Analysis Date = 03/12/14 
 Pct Recovery = 47%  Analysis Date = 03/09/14 
 Pct Recovery = 48%  Analysis Date = 03/09/14 
 Pct Recovery = 48%  Analysis Date = 03/07/14 
 Pct Recovery = 48%  Analysis Date = 03/07/14 
 Pct Recovery = 48%  Analysis Date = 03/04/14 
 Pct Recovery = 48%  Analysis Date = 03/04/14 
 Pct Recovery = 48%  Analysis Date = 03/02/14 
 Pct Recovery = 49%  Analysis Date = 03/02/14 
 Pct Recovery = 49%  Analysis Date = 02/28/14 
 Pct Recovery = 49%  Analysis Date = 02/28/14 
 Pct Recovery = 49%  Analysis Date = 02/25/14 
 Pct Recovery = 49%  Analysis Date = 02/25/14 
 Pct Recovery = 49%  Analysis Date = 02/23/14 
 Pct Recovery = 50%  Analysis Date = 02/23/14 
 Pct Recovery = 50%  Analysis Date = 02/20/14 
 Pct Recovery = 50%  Analysis Date = 02/20/14 
 Pct Recovery = 50%  Analysis Date = 02/18/14 
 Pct Recovery = 50%  Analysis Date = 02/18/14 
 Pct Recovery = 50%  Analysis Date = 02/15/14 
 Pct Recovery = 51%  Analysis Date = 02/15/14 
 Pct Recovery = 51%  Analysis Date = 02/13/14 
 Pct Recovery = 51%  Analysis Date = 02/13/14 
 Pct Recovery = 51%  Analysis Date = 02/11/14 
 Pct Recovery = 51%  Analysis Date = 02/11/14 
 Pct Recovery = 51%  Analysis Date = 02/08/14 
 Pct Recovery = 52%  Analysis Date = 02/08/14 
 Pct Recovery = 52%  Analysis Date = 02/06/14 
 Pct Recovery = 52%  Analysis Date = 02/06/14 
 Pct Recovery = 52%  Analysis Date = 02/03/14 
 Pct Recovery = 52%  Analysis Date = 02/03/14 
 Pct Recovery = 52%  Analysis Date = 02/01/14 
 Pct Recovery = 53%  Analysis Date = 02/01/14 
 Pct Recovery = 53%  Analysis Date = 01/30/14 
 Pct Recovery = 53%  Analysis Date = 01/30/14 
 Pct Recovery = 53%  Analysis Date = 01/27/14 
 Pct Recovery = 53%  Analysis Date = 01/27/14 
 Pct Recovery = 53%  Analysis Date = 01/25/14 
 Pct Recovery = 54%  Analysis Date = 01/25/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/22/14 
 Pct Recovery = 54%  Analysis Date = 01/20/14 
 Pct Recovery = 54%  Analysis Date = 01/20/14 
 Pct Recovery = 54%  Analysis Date = 01/18/14 
 Pct Recovery = 55%  Analysis Date = 01/18/14 
 Pct Recovery = 55%  Analysis Date = 01/15/14 
 Pct Recovery = 55%  Analysis Date = 01/15/14 
 Pct Recovery = 55%  Analysis Date = 01/13/14 
 Pct Recovery = 55%  Analysis Date = 01/13/14 
 Pct Recovery = 55%  Analysis Date = 01/10/14 
 Pct Recovery = 55%  Analysis Date = 01/10/14 
 Pct Recovery = 55%  Analysis Date = 01/08/14 
 Pct Recovery = 56%  Analysis Date = 01/08/14 
 Pct Recovery = 56%  Analysis Date = 01/06/14 
 Pct Recovery = 56%  Analysis Date = 01/06/14 
 Pct Recovery = 56%  Analysis Date = 01/03/14 
 Pct Recovery = 56%  Analysis Date = 01/03/14 
 Pct Recovery = 56%  Analysis Date = 01/01/14 
 Pct Recovery = 57%  Analysis Date = 01/01/14 
 Pct Recovery = 57%  Analysis Date = 12/29/13 
 Pct Recovery = 57%  Analysis Date = 12/29/13 
 Pct Recovery = 57%  Analysis Date = 12/27/13 
 Pct Recovery = 57%  Analysis Date = 12/27/13 
 Pct Recovery = 57%  Analysis Date = 12/24/13 
 Pct Recovery = 57%  Analysis Date = 12/24/13 
 Pct Recovery = 57%  Analysis Date = 12/22/13 
 Pct Recovery = 58%  Analysis Date = 12/22/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/20/13 
 Pct Recovery = 58%  Analysis Date = 12/17/13 
 Pct Recovery = 58%  Analysis Date = 12/17/13 
 Pct Recovery = 58%  Analysis Date = 12/15/13 
 Pct Recovery = 58%  Analysis Date = 12/15/13 
 Pct Recovery = 58%  Analysis Date = 12/12/13 
 Pct Recovery = 59%  Analysis Date = 12/12/13 
 Pct Recovery = 59%  Analysis Date = 12/10/13 
 Pct Recovery = 59%  Analysis Date = 12/10/13 
 Pct Recovery = 59%  Analysis Date = 12/08/13 
 Pct Recovery = 59%  Analysis Date = 12/08/13 
 Pct Recovery = 59%  Analysis Date = 12/05/13 
 Pct Recovery = 60%  Analysis Date = 12/05/13 
 Pct Recovery = 60%  Analysis Date = 12/03/13 
 Pct Recovery = 60%  Analysis Date = 12/03/13 
 Pct Recovery = 60%  Analysis Date = 11/30/13 
 Pct Recovery = 60%  Analysis Date = 11/30/13 
 Pct Recovery = 60%  Analysis Date = 11/28/13 
 Pct Recovery = 60%  Analysis Date = 11/28/13 
 Pct Recovery = 60%  Analysis Date = 11/26/13 
 Pct Recovery = 60%  Analysis Date = 11/26/13 
 Pct Recovery = 60%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/23/13 
 Pct Recovery = 61%  Analysis Date = 11/21/13 
 Pct Recovery = 61%  Analysis Date = 11/21/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/18/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/16/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/13/13 
 Pct Recovery = 61%  Analysis Date = 11/11/13 
 Pct Recovery = 61%  Analysis Date = 11/11/13 
 Pct Recovery = 61%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/09/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/06/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/04/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 11/01/13 
 Pct Recovery = 62%  Analysis Date = 10/30/13 
 Pct Recovery = 62%  Analysis Date = 10/30/13 
 Pct Recovery = 62%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/28/13 
 Pct Recovery = 63%  Analysis Date = 10/25/13 
 Pct Recovery = 63%  Analysis Date = 10/25/13 
 Pct Recovery = 63%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/23/13 
 Pct Recovery = 63%  Analysis Date = 10/20/13 
 Pct Recovery = 63%  Analysis Date = 10/20/13 
 Pct Recovery = 63%  Analysis Date = 10/18/13 
 Pct Recovery = 63%  Analysis Date = 10/18/13 
 Pct Recovery = 63%  Analysis Date = 10/16/13 
 Pct Recovery = 63%  Analysis Date = 10/16/13 
 Pct Recovery = 63%  Analysis Date = 10/13/13 
 Pct Recovery = 63%  Analysis Date = 10/13/13 
 Pct Recovery = 63%  Analysis Date = 10/11/13 
 Pct Recovery = 64%  Analysis Date = 10/11/13 
 Pct Recovery = 64%  Analysis Date = 10/08/13 
 Pct Recovery = 64%  Analysis Date = 10/08/13 
 Pct Recovery = 64%  Analysis Date = 10/06/13 
 Pct Recovery = 64%  Analysis Date = 10/06/13 
 Pct Recovery = 64%  Analysis Date = 10/04/13 
 Pct Recovery = 64%  Analysis Date = 10/04/13 
 Pct Recovery = 64%  Analysis Date = 10/01/13 
 Pct Recovery = 64%  Analysis Date = 10/01/13 
 Pct Recovery = 64%  Analysis Date = 09/29/13 
 Pct Recovery = 64%  Analysis Date = 09/29/13 
 Pct Recovery = 64%  Analysis Date = 09/26/13 
 Pct Recovery = 64%  Analysis Date = 09/26/13 
 Pct Recovery = 64%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/24/13 
 Pct Recovery = 64%  Analysis Date = 09/21/13 
 Pct Recovery = 65%  Analysis Date = 09/21/13 
 Pct Recovery = 65%  Analysis Date = 09/19/13 
 Pct Recovery = 65%  Analysis Date = 09/19/13 
 Pct Recovery = 65%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/17/13 
 Pct Recovery = 65%  Analysis Date = 09/14/13 
 Pct Recovery = 65%  Analysis Date = 09/14/13 
 Pct Recovery = 65%  Analysis Date = 09/12/13 
 Pct Recovery = 65%  Analysis Date = 09/12/13 
 Pct Recovery = 65%  Analysis Date = 09/09/13 
 Pct Recovery = 65%  Analysis Date = 09/09/13 
 Pct Recovery = 65%  Analysis Date = 09/07/13 
 Pct Recovery = 65%  Analysis Date = 09/07/13 
 Pct Recovery = 65%  Analysis Date = 09/05/13 
 Pct Recovery = 65%  Analysis Date = 09/05/13 
 Pct Recovery = 65%  Analysis Date = 09/02/13 
 Pct Recovery = 66%  Analysis Date = 09/02/13 
 Pct Recovery = 66%  Analysis Date = 08/31/13 
 Pct Recovery = 66%  Analysis Date = 08/31/13 
 Pct Recovery = 66%  Analysis Date = 08/28/13 
 Pct Recovery = 66%  Analysis Date = 08/28/13 
 Pct Recovery = 66%  Analysis Date = 08/26/13 
 Pct Recovery = 66%  Analysis Date = 08/26/13 
 Pct Recovery = 66%  Analysis Date = 08/24/13 
 Pct Recovery = 66%  Analysis Date = 08/24/13 
 Pct Recovery = 66%  Analysis Date = 08/21/13 
 Pct Recovery = 66%  Analysis Date = 08/21/13 
 Pct Recovery = 66%  Analysis Date = 08/19/13 
 Pct Recovery = 66%  Analysis Date = 08/19/13 
 Pct Recovery = 66%  Analysis Date = 08/16/13 
 Pct Recovery = 66%  Analysis Date = 08/16/13 
 Pct Recovery = 66%  Analysis Date = 08/14/13 
 Pct Recovery = 67%  Analysis Date = 08/14/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/11/13 
 Pct Recovery = 67%  Analysis Date = 08/09/13 
 Pct Recovery = 67%  Analysis Date = 08/09/13 
 Pct Recovery = 67%  Analysis Date = 08/07/13 
 Pct Recovery = 67%  Analysis Date = 08/07/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/04/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 08/02/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/30/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/28/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/26/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/23/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/21/13 
 Pct Recovery = 67%  Analysis Date = 07/18/13 
 Pct Recovery = 67%  Analysis Date = 07/18/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/16/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/14/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/11/13 
 Pct Recovery = 67%  Analysis Date = 07/09/13 
 Pct Recovery = 66%  Analysis Date = 07/09/13 
 Pct Recovery = 66%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/06/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/04/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 07/02/13 
 Pct Recovery = 66%  Analysis Date = 06/29/13 
 Pct Recovery = 66%  Analysis Date = 06/29/13 
 Pct Recovery = 66%  Analysis Date = 06/27/13 
 Pct Recovery = 66%  Analysis Date = 06/27/13 
 Pct Recovery = 66%  Analysis Date = 06/24/13 
 Pct Recovery = 66%  Analysis Date = 06/24/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/22/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/19/13 
 Pct Recovery = 66%  Analysis Date = 06/17/13 
 Pct Recovery = 66%  Analysis Date = 06/17/13 
 Pct Recovery = 66%  Analysis Date = 06/15/13 
 Pct Recovery = 66%  Analysis Date = 06/15/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/12/13 
 Pct Recovery = 66%  Analysis Date = 06/10/13 
 Pct Recovery = 65%  Analysis Date = 06/10/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/07/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/05/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 06/03/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/31/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/29/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/26/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/24/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/22/13 
 Pct Recovery = 65%  Analysis Date = 05/19/13 
 Pct Recovery = 65%  Analysis Date = 05/19/13 
 Pct Recovery = 65%  Analysis Date = 05/17/13 
 Pct Recovery = 65%  Analysis Date = 05/17/13 
 Pct Recovery = 65%  Analysis Date = 05/14/13 
 Pct Recovery = 65%  Analysis Date = 05/14/13 
 Pct Recovery = 65%  Analysis Date = 05/12/13 
 Pct Recovery = 65%  Analysis Date = 05/12/13 
 Pct Recovery = 65%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/10/13 
 Pct Recovery = 64%  Analysis Date = 05/07/13 
 Pct Recovery = 64%  Analysis Date = 05/07/13 
 Pct Recovery = 64%  Analysis Date = 05/05/13 
 Pct Recovery = 64%  Analysis Date = 05/05/13 
 Pct Recovery = 64%  Analysis Date = 05/02/13 
 Pct Recovery = 64%  Analysis Date = 05/02/13 
 Pct Recovery = 64%  Analysis Date = 04/30/13 
 Pct Recovery = 64%  Analysis Date = 04/30/13 
 Pct Recovery = 64%  Analysis Date = 04/27/13 
 Pct Recovery = 64%  Analysis Date = 04/27/13 
 Pct Recovery = 64%  Analysis Date = 04/25/13 
 Pct Recovery = 64%  Analysis Date = 04/25/13 
 Pct Recovery = 64%  Analysis Date = 04/23/13 
 Pct Recovery = 63%  Analysis Date = 04/23/13 
 Pct Recovery = 63%  Analysis Date = 04/20/13 
 Pct Recovery = 63%  Analysis Date = 04/20/13 
 Pct Recovery = 63%  Analysis Date = 04/18/13 
 Pct Recovery = 63%  Analysis Date = 04/18/13 
 Pct Recovery = 63%  Analysis Date = 04/15/13 
 Pct Recovery = 63%  Analysis Date = 04/15/13 
 Pct Recovery = 63%  Analysis Date = 04/13/13 
 Pct Recovery = 63%  Analysis Date = 04/13/13 
 Pct Recovery = 63%  Analysis Date = 04/11/13 
 Pct Recovery = 63%  Analysis Date = 04/11/13 
 Pct Recovery = 63%  Analysis Date = 04/08/13 
 Pct Recovery = 62%  Analysis Date = 04/08/13 
 Pct Recovery = 62%  Analysis Date = 04/06/13 
 Pct Recovery = 62%  Analysis Date = 04/06/13 
 Pct Recovery = 62%  Analysis Date = 04/03/13 
 Pct Recovery = 62%  Analysis Date = 04/03/13 
 Pct Recovery = 62%  Analysis Date = 04/01/13 
 Pct Recovery = 62%  Analysis Date = 04/01/13 
 Pct Recovery = 62%  Analysis Date = 03/30/13 
 Pct Recovery = 62%  Analysis Date = 03/30/13 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 Pct Recovery = 62%  Analysis Date = 03/27/13 
 Pct Recovery = 62%  Analysis Date = 03/25/13 
 Pct Recovery = 61%  Analysis Date = 03/25/13 
 Pct Recovery = 61%  Analysis Date = 03/22/13 
 Pct Recovery = 61%  Analysis Date = 03/22/13 
 Pct Recovery = 61%  Analysis Date = 03/20/13 
 Pct Recovery = 61%  Analysis Date = 03/20/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/17/13 
 Pct Recovery = 61%  Analysis Date = 03/15/13 
 Pct Recovery = 61%  Analysis Date = 03/15/13 
 Pct Recovery = 61%  Analysis Date = 03/13/13 
 Pct Recovery = 61%  Analysis Date = 03/13/13 
 Pct Recovery = 61%  Analysis Date = 03/10/13 
 Pct Recovery = 60%  Analysis Date = 03/10/13 
 Pct Recovery = 60%  Analysis Date = 03/08/13 
 Pct Recovery = 60%  Analysis Date = 03/08/13 
 Pct Recovery = 60%  Analysis Date = 03/05/13 
 Pct Recovery = 60%  Analysis Date = 03/05/13 
 Pct Recovery = 60%  Analysis Date = 03/03/13 
 Pct Recovery = 60%  Analysis Date = 03/03/13 
 Pct Recovery = 60%  Analysis Date = 03/01/13 
 Pct Recovery = 60%  Analysis Date = 03/01/13 
 Pct Recovery = 60%  Analysis Date = 02/26/13 
 Pct Recovery = 60%  Analysis Date = 02/26/13 
 Pct Recovery = 60%  Analysis Date = 02/24/13 
 Pct Recovery = 60%  Analysis Date = 02/24/13 
 Pct Recovery = 60%  Analysis Date = 02/21/13 
 Pct Recovery = 60%  Analysis Date = 02/21/13 
 Pct Recovery = 60%  Analysis Date = 02/19/13 
 Pct Recovery = 60%  Analysis Date = 02/19/13 
 Pct Recovery = 60%  Analysis Date = 02/17/13 
 Pct Recovery = 60%  Analysis Date = 02/17/13 
 Pct Recovery = 60%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/14/13 
 Pct Recovery = 60%  Analysis Date = 02/12/13 
 Pct Recovery = 60%  Analysis Date = 02/12/13 
 Pct Recovery = 60%  Analysis Date = 02/09/13 
 Pct Recovery = 60%  Analysis Date = 02/09/13 
 Pct Recovery = 60%  Analysis Date = 02/07/13 
 Pct Recovery = 60%  Analysis Date = 02/07/13 
 Pct Recovery = 60%  Analysis Date = 02/05/13 
 Pct Recovery = 60%  Analysis Date = 02/05/13 
 Pct Recovery = 60%  Analysis Date = 02/02/13 
 Pct Recovery = 60%  Analysis Date = 02/02/13 
 Pct Recovery = 60%  Analysis Date = 01/31/13 
 Pct Recovery = 60%  Analysis Date = 01/31/13 
 Pct Recovery = 60%  Analysis Date = 01/28/13 
 Pct Recovery = 60%  Analysis Date = 01/28/13 
 Pct Recovery = 60%  Analysis Date = 01/26/13 
 Pct Recovery = 60%  Analysis Date = 01/26/13 
 Pct Recovery = 60%  Analysis Date = 01/23/13 
 Pct Recovery = 60%  Analysis Date = 01/23/13 
 Pct Recovery = 60%  Analysis Date = 01/21/13 
 Pct Recovery = 60%  Analysis Date = 01/21/13 
 Pct Recovery = 60%  Analysis Date = 01/19/13 
 Pct Recovery = 60%  Analysis Date = 01/19/13 
 Pct Recovery = 60%  Analysis Date = 01/16/13 
 Pct Recovery = 60%  Analysis Date = 01/16/13 
 Pct Recovery = 60%  Analysis Date = 01/14/13 
 Pct Recovery = 60%  Analysis Date = 01/14/13 
 Pct Recovery = 60%  Analysis Date = 01/11/13 
 Pct Recovery = 60%  Analysis Date = 01/11/13 
 Pct Recovery = 60%  Analysis Date = 01/09/13 
 Pct Recovery = 60%  Analysis Date = 01/09/13 
 Pct Recovery = 60%  Analysis Date = 01/07/13 
 Pct Recovery = 60%  Analysis Date = 01/07/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/04/13 
 Pct Recovery = 60%  Analysis Date = 01/02/13 
 Pct Recovery = 60%  Analysis Date = 01/02/13 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/30/12 
 Pct Recovery = 60%  Analysis Date = 12/28/12 
 Pct Recovery = 60%  Analysis Date = 12/28/12 
 Pct Recovery = 60%  Analysis Date = 12/26/12 
 Pct Recovery = 60%  Analysis Date = 12/26/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/23/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/21/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 60%  Analysis Date = 12/18/12 
 Pct Recovery = 60%  Analysis Date = 12/16/12 
 Pct Recovery = 60%  Analysis Date = 12/16/12 
 Pct Recovery = 60%  Analysis Date = 12/14/12 
 Pct Recovery = 60%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
VENLAFAXINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 59% 10% 60% 8%
Total 13 59% 10% 60% 8%

Sample Statistics
VENLAFAXINE

Characteristic N % % Basis
Plotted 13 93% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 1 7% 1 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
VERAPAMIL
METHOD: LC9017 , TESTIDCODE: 67472LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 37%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 20%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 13%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 23%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 26%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 8%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 21%  Analysis Date = 04/26/13 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 36%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 15%  Analysis Date = 11/20/13 
 SpikeMix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl 
 Pct Recovery = 10%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 47%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 37%  Analysis Date = 02/28/13 
 SpikeMix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl 
 Pct Recovery = 7%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 10%  Analysis Date = 04/09/14 
 Pct Recovery = 15%  Analysis Date = 04/07/14 
 Pct Recovery = 15%  Analysis Date = 04/07/14 
 Pct Recovery = 15%  Analysis Date = 04/05/14 
 Pct Recovery = 15%  Analysis Date = 04/05/14 
 Pct Recovery = 15%  Analysis Date = 04/02/14 
 Pct Recovery = 16%  Analysis Date = 04/02/14 
 Pct Recovery = 16%  Analysis Date = 03/31/14 
 Pct Recovery = 16%  Analysis Date = 03/31/14 
 Pct Recovery = 16%  Analysis Date = 03/28/14 
 Pct Recovery = 16%  Analysis Date = 03/28/14 
 Pct Recovery = 16%  Analysis Date = 03/26/14 
 Pct Recovery = 16%  Analysis Date = 03/26/14 
 Pct Recovery = 16%  Analysis Date = 03/24/14 
 Pct Recovery = 16%  Analysis Date = 03/24/14 
 Pct Recovery = 16%  Analysis Date = 03/21/14 
 Pct Recovery = 16%  Analysis Date = 03/21/14 
 Pct Recovery = 16%  Analysis Date = 03/19/14 
 Pct Recovery = 16%  Analysis Date = 03/19/14 
 Pct Recovery = 16%  Analysis Date = 03/16/14 
 Pct Recovery = 16%  Analysis Date = 03/16/14 
 Pct Recovery = 16%  Analysis Date = 03/14/14 
 Pct Recovery = 17%  Analysis Date = 03/14/14 
 Pct Recovery = 17%  Analysis Date = 03/12/14 
 Pct Recovery = 17%  Analysis Date = 03/12/14 
 Pct Recovery = 17%  Analysis Date = 03/09/14 
 Pct Recovery = 17%  Analysis Date = 03/09/14 
 Pct Recovery = 17%  Analysis Date = 03/07/14 
 Pct Recovery = 17%  Analysis Date = 03/07/14 
 Pct Recovery = 17%  Analysis Date = 03/04/14 
 Pct Recovery = 17%  Analysis Date = 03/04/14 
 Pct Recovery = 17%  Analysis Date = 03/02/14 
 Pct Recovery = 17%  Analysis Date = 03/02/14 
 Pct Recovery = 17%  Analysis Date = 02/28/14 
 Pct Recovery = 17%  Analysis Date = 02/28/14 
 Pct Recovery = 17%  Analysis Date = 02/25/14 
 Pct Recovery = 17%  Analysis Date = 02/25/14 
 Pct Recovery = 17%  Analysis Date = 02/23/14 
 Pct Recovery = 18%  Analysis Date = 02/23/14 
 Pct Recovery = 18%  Analysis Date = 02/20/14 
 Pct Recovery = 18%  Analysis Date = 02/20/14 
 Pct Recovery = 18%  Analysis Date = 02/18/14 
 Pct Recovery = 18%  Analysis Date = 02/18/14 
 Pct Recovery = 18%  Analysis Date = 02/15/14 
 Pct Recovery = 18%  Analysis Date = 02/15/14 
 Pct Recovery = 18%  Analysis Date = 02/13/14 
 Pct Recovery = 18%  Analysis Date = 02/13/14 
 Pct Recovery = 18%  Analysis Date = 02/11/14 
 Pct Recovery = 18%  Analysis Date = 02/11/14 
 Pct Recovery = 18%  Analysis Date = 02/08/14 
 Pct Recovery = 19%  Analysis Date = 02/08/14 
 Pct Recovery = 19%  Analysis Date = 02/06/14 
 Pct Recovery = 19%  Analysis Date = 02/06/14 
 Pct Recovery = 19%  Analysis Date = 02/03/14 
 Pct Recovery = 19%  Analysis Date = 02/03/14 
 Pct Recovery = 19%  Analysis Date = 02/01/14 
 Pct Recovery = 19%  Analysis Date = 02/01/14 
 Pct Recovery = 19%  Analysis Date = 01/30/14 
 Pct Recovery = 19%  Analysis Date = 01/30/14 
 Pct Recovery = 19%  Analysis Date = 01/27/14 
 Pct Recovery = 19%  Analysis Date = 01/27/14 
 Pct Recovery = 19%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/25/14 
 Pct Recovery = 20%  Analysis Date = 01/22/14 
 Pct Recovery = 20%  Analysis Date = 01/22/14 
 Pct Recovery = 20%  Analysis Date = 01/20/14 
 Pct Recovery = 20%  Analysis Date = 01/20/14 
 Pct Recovery = 20%  Analysis Date = 01/18/14 
 Pct Recovery = 20%  Analysis Date = 01/18/14 
 Pct Recovery = 20%  Analysis Date = 01/15/14 
 Pct Recovery = 20%  Analysis Date = 01/15/14 
 Pct Recovery = 20%  Analysis Date = 01/13/14 
 Pct Recovery = 20%  Analysis Date = 01/13/14 
 Pct Recovery = 20%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/10/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/08/14 
 Pct Recovery = 21%  Analysis Date = 01/06/14 
 Pct Recovery = 21%  Analysis Date = 01/06/14 
 Pct Recovery = 21%  Analysis Date = 01/03/14 
 Pct Recovery = 21%  Analysis Date = 01/03/14 
 Pct Recovery = 21%  Analysis Date = 01/01/14 
 Pct Recovery = 21%  Analysis Date = 01/01/14 
 Pct Recovery = 21%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/29/13 
 Pct Recovery = 22%  Analysis Date = 12/27/13 
 Pct Recovery = 22%  Analysis Date = 12/27/13 
 Pct Recovery = 22%  Analysis Date = 12/24/13 
 Pct Recovery = 22%  Analysis Date = 12/24/13 
 Pct Recovery = 22%  Analysis Date = 12/22/13 
 Pct Recovery = 22%  Analysis Date = 12/22/13 
 Pct Recovery = 22%  Analysis Date = 12/20/13 
 Pct Recovery = 22%  Analysis Date = 12/20/13 
 Pct Recovery = 22%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/17/13 
 Pct Recovery = 23%  Analysis Date = 12/15/13 
 Pct Recovery = 23%  Analysis Date = 12/15/13 
 Pct Recovery = 23%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/12/13 
 Pct Recovery = 23%  Analysis Date = 12/10/13 
 Pct Recovery = 23%  Analysis Date = 12/10/13 
 Pct Recovery = 23%  Analysis Date = 12/08/13 
 Pct Recovery = 23%  Analysis Date = 12/08/13 
 Pct Recovery = 23%  Analysis Date = 12/05/13 
 Pct Recovery = 24%  Analysis Date = 12/05/13 
 Pct Recovery = 24%  Analysis Date = 12/03/13 
 Pct Recovery = 24%  Analysis Date = 12/03/13 
 Pct Recovery = 24%  Analysis Date = 11/30/13 
 Pct Recovery = 24%  Analysis Date = 11/30/13 
 Pct Recovery = 24%  Analysis Date = 11/28/13 
 Pct Recovery = 25%  Analysis Date = 11/28/13 
 Pct Recovery = 25%  Analysis Date = 11/26/13 
 Pct Recovery = 25%  Analysis Date = 11/26/13 
 Pct Recovery = 25%  Analysis Date = 11/23/13 
 Pct Recovery = 25%  Analysis Date = 11/23/13 
 Pct Recovery = 25%  Analysis Date = 11/21/13 
 Pct Recovery = 26%  Analysis Date = 11/21/13 
 Pct Recovery = 26%  Analysis Date = 11/18/13 
 Pct Recovery = 26%  Analysis Date = 11/18/13 
 Pct Recovery = 26%  Analysis Date = 11/16/13 
 Pct Recovery = 26%  Analysis Date = 11/16/13 
 Pct Recovery = 26%  Analysis Date = 11/13/13 
 Pct Recovery = 26%  Analysis Date = 11/13/13 
 Pct Recovery = 26%  Analysis Date = 11/11/13 
 Pct Recovery = 27%  Analysis Date = 11/11/13 
 Pct Recovery = 27%  Analysis Date = 11/09/13 
 Pct Recovery = 27%  Analysis Date = 11/09/13 
 Pct Recovery = 27%  Analysis Date = 11/06/13 
 Pct Recovery = 27%  Analysis Date = 11/06/13 
 Pct Recovery = 27%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/25/13 
 Pct Recovery = 28%  Analysis Date = 10/23/13 
 Pct Recovery = 29%  Analysis Date = 10/23/13 
 Pct Recovery = 29%  Analysis Date = 10/20/13 
 Pct Recovery = 29%  Analysis Date = 10/20/13 
 Pct Recovery = 29%  Analysis Date = 10/18/13 
 Pct Recovery = 29%  Analysis Date = 10/18/13 
 Pct Recovery = 29%  Analysis Date = 10/16/13 
 Pct Recovery = 29%  Analysis Date = 10/16/13 
 Pct Recovery = 29%  Analysis Date = 10/13/13 
 Pct Recovery = 29%  Analysis Date = 10/13/13 
 Pct Recovery = 29%  Analysis Date = 10/11/13 
 Pct Recovery = 29%  Analysis Date = 10/11/13 
 Pct Recovery = 29%  Analysis Date = 10/08/13 
 Pct Recovery = 29%  Analysis Date = 10/08/13 
 Pct Recovery = 29%  Analysis Date = 10/06/13 
 Pct Recovery = 30%  Analysis Date = 10/06/13 
 Pct Recovery = 30%  Analysis Date = 10/04/13 
 Pct Recovery = 30%  Analysis Date = 10/04/13 
 Pct Recovery = 30%  Analysis Date = 10/01/13 
 Pct Recovery = 30%  Analysis Date = 10/01/13 
 Pct Recovery = 30%  Analysis Date = 09/29/13 
 Pct Recovery = 30%  Analysis Date = 09/29/13 
 Pct Recovery = 30%  Analysis Date = 09/26/13 
 Pct Recovery = 30%  Analysis Date = 09/26/13 
 Pct Recovery = 30%  Analysis Date = 09/24/13 
 Pct Recovery = 30%  Analysis Date = 09/24/13 
 Pct Recovery = 30%  Analysis Date = 09/21/13 
 Pct Recovery = 30%  Analysis Date = 09/21/13 
 Pct Recovery = 30%  Analysis Date = 09/19/13 
 Pct Recovery = 31%  Analysis Date = 09/19/13 
 Pct Recovery = 31%  Analysis Date = 09/17/13 
 Pct Recovery = 31%  Analysis Date = 09/17/13 
 Pct Recovery = 31%  Analysis Date = 09/14/13 
 Pct Recovery = 31%  Analysis Date = 09/14/13 
 Pct Recovery = 31%  Analysis Date = 09/12/13 
 Pct Recovery = 31%  Analysis Date = 09/12/13 
 Pct Recovery = 31%  Analysis Date = 09/09/13 
 Pct Recovery = 31%  Analysis Date = 09/09/13 
 Pct Recovery = 31%  Analysis Date = 09/07/13 
 Pct Recovery = 31%  Analysis Date = 09/07/13 
 Pct Recovery = 31%  Analysis Date = 09/05/13 
 Pct Recovery = 31%  Analysis Date = 09/05/13 
 Pct Recovery = 31%  Analysis Date = 09/02/13 
 Pct Recovery = 32%  Analysis Date = 09/02/13 
 Pct Recovery = 32%  Analysis Date = 08/31/13 
 Pct Recovery = 32%  Analysis Date = 08/31/13 
 Pct Recovery = 32%  Analysis Date = 08/28/13 
 Pct Recovery = 32%  Analysis Date = 08/28/13 
 Pct Recovery = 32%  Analysis Date = 08/26/13 
 Pct Recovery = 32%  Analysis Date = 08/26/13 
 Pct Recovery = 32%  Analysis Date = 08/24/13 
 Pct Recovery = 32%  Analysis Date = 08/24/13 
 Pct Recovery = 32%  Analysis Date = 08/21/13 
 Pct Recovery = 32%  Analysis Date = 08/21/13 
 Pct Recovery = 32%  Analysis Date = 08/19/13 
 Pct Recovery = 32%  Analysis Date = 08/19/13 
 Pct Recovery = 32%  Analysis Date = 08/16/13 
 Pct Recovery = 33%  Analysis Date = 08/16/13 
 Pct Recovery = 33%  Analysis Date = 08/14/13 
 Pct Recovery = 33%  Analysis Date = 08/14/13 
 Pct Recovery = 33%  Analysis Date = 08/11/13 
 Pct Recovery = 33%  Analysis Date = 08/11/13 
 Pct Recovery = 33%  Analysis Date = 08/09/13 
 Pct Recovery = 33%  Analysis Date = 08/09/13 
 Pct Recovery = 33%  Analysis Date = 08/07/13 
 Pct Recovery = 33%  Analysis Date = 08/07/13 
 Pct Recovery = 33%  Analysis Date = 08/04/13 
 Pct Recovery = 33%  Analysis Date = 08/04/13 
 Pct Recovery = 33%  Analysis Date = 08/02/13 
 Pct Recovery = 33%  Analysis Date = 08/02/13 
 Pct Recovery = 33%  Analysis Date = 07/30/13 
 Pct Recovery = 33%  Analysis Date = 07/30/13 
 Pct Recovery = 33%  Analysis Date = 07/28/13 
 Pct Recovery = 33%  Analysis Date = 07/28/13 
 Pct Recovery = 33%  Analysis Date = 07/26/13 
 Pct Recovery = 33%  Analysis Date = 07/26/13 
 Pct Recovery = 33%  Analysis Date = 07/23/13 
 Pct Recovery = 33%  Analysis Date = 07/23/13 
 Pct Recovery = 33%  Analysis Date = 07/21/13 
 Pct Recovery = 33%  Analysis Date = 07/21/13 
 Pct Recovery = 33%  Analysis Date = 07/18/13 
 Pct Recovery = 33%  Analysis Date = 07/18/13 
 Pct Recovery = 33%  Analysis Date = 07/16/13 
 Pct Recovery = 32%  Analysis Date = 07/16/13 
 Pct Recovery = 32%  Analysis Date = 07/14/13 
 Pct Recovery = 32%  Analysis Date = 07/14/13 
 Pct Recovery = 32%  Analysis Date = 07/11/13 
 Pct Recovery = 32%  Analysis Date = 07/11/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/09/13 
 Pct Recovery = 32%  Analysis Date = 07/06/13 
 Pct Recovery = 32%  Analysis Date = 07/06/13 
 Pct Recovery = 32%  Analysis Date = 07/04/13 
 Pct Recovery = 32%  Analysis Date = 07/04/13 
 Pct Recovery = 32%  Analysis Date = 07/02/13 
 Pct Recovery = 31%  Analysis Date = 07/02/13 
 Pct Recovery = 31%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/27/13 
 Pct Recovery = 31%  Analysis Date = 06/27/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/22/13 
 Pct Recovery = 31%  Analysis Date = 06/22/13 
 Pct Recovery = 31%  Analysis Date = 06/19/13 
 Pct Recovery = 31%  Analysis Date = 06/19/13 
 Pct Recovery = 31%  Analysis Date = 06/17/13 
 Pct Recovery = 31%  Analysis Date = 06/17/13 
 Pct Recovery = 31%  Analysis Date = 06/15/13 
 Pct Recovery = 30%  Analysis Date = 06/15/13 
 Pct Recovery = 30%  Analysis Date = 06/12/13 
 Pct Recovery = 30%  Analysis Date = 06/12/13 
 Pct Recovery = 30%  Analysis Date = 06/10/13 
 Pct Recovery = 30%  Analysis Date = 06/10/13 
 Pct Recovery = 30%  Analysis Date = 06/07/13 
 Pct Recovery = 30%  Analysis Date = 06/07/13 
 Pct Recovery = 30%  Analysis Date = 06/05/13 
 Pct Recovery = 30%  Analysis Date = 06/05/13 
 Pct Recovery = 30%  Analysis Date = 06/03/13 
 Pct Recovery = 30%  Analysis Date = 06/03/13 
 Pct Recovery = 30%  Analysis Date = 05/31/13 
 Pct Recovery = 29%  Analysis Date = 05/31/13 
 Pct Recovery = 29%  Analysis Date = 05/29/13 
 Pct Recovery = 29%  Analysis Date = 05/29/13 
 Pct Recovery = 29%  Analysis Date = 05/26/13 
 Pct Recovery = 29%  Analysis Date = 05/26/13 
 Pct Recovery = 29%  Analysis Date = 05/24/13 
 Pct Recovery = 29%  Analysis Date = 05/24/13 
 Pct Recovery = 29%  Analysis Date = 05/22/13 
 Pct Recovery = 29%  Analysis Date = 05/22/13 
 Pct Recovery = 29%  Analysis Date = 05/19/13 
 Pct Recovery = 29%  Analysis Date = 05/19/13 
 Pct Recovery = 29%  Analysis Date = 05/17/13 
 Pct Recovery = 28%  Analysis Date = 05/17/13 
 Pct Recovery = 28%  Analysis Date = 05/14/13 
 Pct Recovery = 28%  Analysis Date = 05/14/13 
 Pct Recovery = 28%  Analysis Date = 05/12/13 
 Pct Recovery = 28%  Analysis Date = 05/12/13 
 Pct Recovery = 28%  Analysis Date = 05/10/13 
 Pct Recovery = 28%  Analysis Date = 05/10/13 
 Pct Recovery = 28%  Analysis Date = 05/07/13 
 Pct Recovery = 28%  Analysis Date = 05/07/13 
 Pct Recovery = 28%  Analysis Date = 05/05/13 
 Pct Recovery = 28%  Analysis Date = 05/05/13 
 Pct Recovery = 28%  Analysis Date = 05/02/13 
 Pct Recovery = 28%  Analysis Date = 05/02/13 
 Pct Recovery = 28%  Analysis Date = 04/30/13 
 Pct Recovery = 27%  Analysis Date = 04/30/13 
 Pct Recovery = 27%  Analysis Date = 04/27/13 
 Pct Recovery = 27%  Analysis Date = 04/27/13 
 Pct Recovery = 27%  Analysis Date = 04/25/13 
 Pct Recovery = 26%  Analysis Date = 04/25/13 
 Pct Recovery = 26%  Analysis Date = 04/23/13 
 Pct Recovery = 26%  Analysis Date = 04/23/13 
 Pct Recovery = 26%  Analysis Date = 04/20/13 
 Pct Recovery = 26%  Analysis Date = 04/20/13 
 Pct Recovery = 26%  Analysis Date = 04/18/13 
 Pct Recovery = 25%  Analysis Date = 04/18/13 
 Pct Recovery = 25%  Analysis Date = 04/15/13 
 Pct Recovery = 25%  Analysis Date = 04/15/13 
 Pct Recovery = 25%  Analysis Date = 04/13/13 
 Pct Recovery = 24%  Analysis Date = 04/13/13 
 Pct Recovery = 24%  Analysis Date = 04/11/13 
 Pct Recovery = 24%  Analysis Date = 04/11/13 
 Pct Recovery = 24%  Analysis Date = 04/08/13 
 Pct Recovery = 24%  Analysis Date = 04/08/13 
 Pct Recovery = 24%  Analysis Date = 04/06/13 
 Pct Recovery = 23%  Analysis Date = 04/06/13 
 Pct Recovery = 23%  Analysis Date = 04/03/13 
 Pct Recovery = 23%  Analysis Date = 04/03/13 
 Pct Recovery = 23%  Analysis Date = 04/01/13 
 Pct Recovery = 23%  Analysis Date = 04/01/13 
 Pct Recovery = 23%  Analysis Date = 03/30/13 
 Pct Recovery = 22%  Analysis Date = 03/30/13 
 Pct Recovery = 22%  Analysis Date = 03/27/13 
 Pct Recovery = 22%  Analysis Date = 03/27/13 
 Pct Recovery = 22%  Analysis Date = 03/25/13 
 Pct Recovery = 21%  Analysis Date = 03/25/13 
 Pct Recovery = 21%  Analysis Date = 03/22/13 
 Pct Recovery = 21%  Analysis Date = 03/22/13 
 Pct Recovery = 21%  Analysis Date = 03/20/13 
 Pct Recovery = 21%  Analysis Date = 03/20/13 
 Pct Recovery = 21%  Analysis Date = 03/17/13 
 Pct Recovery = 20%  Analysis Date = 03/17/13 
 Pct Recovery = 20%  Analysis Date = 03/15/13 
 Pct Recovery = 20%  Analysis Date = 03/15/13 
 Pct Recovery = 20%  Analysis Date = 03/13/13 
 Pct Recovery = 20%  Analysis Date = 03/13/13 
 Pct Recovery = 20%  Analysis Date = 03/10/13 
 Pct Recovery = 19%  Analysis Date = 03/10/13 
 Pct Recovery = 19%  Analysis Date = 03/08/13 
 Pct Recovery = 19%  Analysis Date = 03/08/13 
 Pct Recovery = 19%  Analysis Date = 03/05/13 
 Pct Recovery = 18%  Analysis Date = 03/05/13 
 Pct Recovery = 18%  Analysis Date = 03/03/13 
 Pct Recovery = 18%  Analysis Date = 03/03/13 
 Pct Recovery = 18%  Analysis Date = 03/01/13 
 Pct Recovery = 18%  Analysis Date = 03/01/13 
 Pct Recovery = 18%  Analysis Date = 02/26/13 
 Pct Recovery = 17%  Analysis Date = 02/26/13 
 Pct Recovery = 17%  Analysis Date = 02/24/13 
 Pct Recovery = 17%  Analysis Date = 02/24/13 
 Pct Recovery = 17%  Analysis Date = 02/21/13 
 Pct Recovery = 17%  Analysis Date = 02/21/13 
 Pct Recovery = 17%  Analysis Date = 02/19/13 
 Pct Recovery = 16%  Analysis Date = 02/19/13 
 Pct Recovery = 16%  Analysis Date = 02/17/13 
 Pct Recovery = 16%  Analysis Date = 02/17/13 
 Pct Recovery = 16%  Analysis Date = 02/14/13 
 Pct Recovery = 15%  Analysis Date = 02/14/13 
 Pct Recovery = 15%  Analysis Date = 02/12/13 
 Pct Recovery = 15%  Analysis Date = 02/12/13 
 Pct Recovery = 15%  Analysis Date = 02/09/13 
 Pct Recovery = 15%  Analysis Date = 02/09/13 
 Pct Recovery = 15%  Analysis Date = 02/07/13 
 Pct Recovery = 14%  Analysis Date = 02/07/13 
 Pct Recovery = 14%  Analysis Date = 02/05/13 
 Pct Recovery = 14%  Analysis Date = 02/05/13 
 Pct Recovery = 14%  Analysis Date = 02/02/13 
 Pct Recovery = 13%  Analysis Date = 02/02/13 
 Pct Recovery = 13%  Analysis Date = 01/31/13 
 Pct Recovery = 13%  Analysis Date = 01/31/13 
 Pct Recovery = 13%  Analysis Date = 01/28/13 
 Pct Recovery = 13%  Analysis Date = 01/28/13 
 Pct Recovery = 13%  Analysis Date = 01/26/13 
 Pct Recovery = 12%  Analysis Date = 01/26/13 
 Pct Recovery = 12%  Analysis Date = 01/23/13 
 Pct Recovery = 12%  Analysis Date = 01/23/13 
 Pct Recovery = 12%  Analysis Date = 01/21/13 
 Pct Recovery = 12%  Analysis Date = 01/21/13 
 Pct Recovery = 12%  Analysis Date = 01/19/13 
 Pct Recovery = 11%  Analysis Date = 01/19/13 
 Pct Recovery = 11%  Analysis Date = 01/16/13 
 Pct Recovery = 11%  Analysis Date = 01/16/13 
 Pct Recovery = 11%  Analysis Date = 01/14/13 
 Pct Recovery = 10%  Analysis Date = 01/14/13 
 Pct Recovery = 10%  Analysis Date = 01/11/13 
 Pct Recovery = 10%  Analysis Date = 01/11/13 
 Pct Recovery = 10%  Analysis Date = 01/09/13 
 Pct Recovery = 10%  Analysis Date = 01/09/13 
 Pct Recovery = 10%  Analysis Date = 01/07/13 
 Pct Recovery = 9%  Analysis Date = 01/07/13 
 Pct Recovery = 9%  Analysis Date = 01/04/13 
 Pct Recovery = 9%  Analysis Date = 01/04/13 
 Pct Recovery = 9%  Analysis Date = 01/02/13 
 Pct Recovery = 8%  Analysis Date = 01/02/13 
 Pct Recovery = 8%  Analysis Date = 12/30/12 
 Pct Recovery = 8%  Analysis Date = 12/30/12 
 Pct Recovery = 8%  Analysis Date = 12/28/12 
 Pct Recovery = 8%  Analysis Date = 12/28/12 
 Pct Recovery = 8%  Analysis Date = 12/26/12 
 Pct Recovery = 7%  Analysis Date = 12/26/12 
 Pct Recovery = 7%  Analysis Date = 12/23/12 
 Pct Recovery = 7%  Analysis Date = 12/23/12 
 Pct Recovery = 7%  Analysis Date = 12/21/12 
 Pct Recovery = 6%  Analysis Date = 12/21/12 
 Pct Recovery = 6%  Analysis Date = 12/18/12 
 Pct Recovery = 6%  Analysis Date = 12/18/12 
 Pct Recovery = 6%  Analysis Date = 12/16/12 
 Pct Recovery = 6%  Analysis Date = 12/16/12 
 Pct Recovery = 6%  Analysis Date = 12/14/12 
 Pct Recovery = 5%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
VERAPAMIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 22% 13% 21% 20%
Total 14 22% 13% 21% 20%

Sample Statistics
VERAPAMIL

Characteristic N % % Basis
Plotted 14 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 15 .  
False Negatives 0 0% 0 out of 14
Not Spiked 17 .  
False Positives 0 0% 0 out of 17

OBSP Determination:
WARFARIN
METHOD: LC9017 , TESTIDCODE: 67457LCM56

 Analysis Date = 05/03/13 
 SpikeMix = ERA 0823-11-05.2: 40 µl 
 Pct Recovery = 31%  Analysis Date = 05/03/13 
 SpikeMix = Abs 071112: 40 µl 
 Pct Recovery = 48%  Analysis Date = 02/20/14 
 SpikeMix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 33%  Analysis Date = 04/10/14 
 SpikeMix = Abs 071112: 20 µl & Abs 060112: 20 µl 
 Pct Recovery = 23%  Analysis Date = 02/20/14 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 45%  Analysis Date = 01/16/14 
 SpikeMix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Pct Recovery = 49%  Analysis Date = 12/05/13 
 SpikeMix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Pct Recovery = 25%  Analysis Date = 02/28/13 
 SpikeMix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl 
 Pct Recovery = 31%  Analysis Date = 10/29/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl 
 Pct Recovery = 29%  Analysis Date = 08/02/13 
 SpikeMix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl 
 Pct Recovery = 20%  Analysis Date = 12/14/12 
 SpikeMix = Abs 071112: 10 µl & ERA 0507-12-06.2: 10 µl 
 Pct Recovery = 49%  Analysis Date = 04/09/14 
 Pct Recovery = 27%  Analysis Date = 04/07/14 
 Pct Recovery = 27%  Analysis Date = 04/07/14 
 Pct Recovery = 27%  Analysis Date = 04/05/14 
 Pct Recovery = 28%  Analysis Date = 04/05/14 
 Pct Recovery = 28%  Analysis Date = 04/02/14 
 Pct Recovery = 28%  Analysis Date = 04/02/14 
 Pct Recovery = 28%  Analysis Date = 03/31/14 
 Pct Recovery = 29%  Analysis Date = 03/31/14 
 Pct Recovery = 29%  Analysis Date = 03/28/14 
 Pct Recovery = 29%  Analysis Date = 03/28/14 
 Pct Recovery = 29%  Analysis Date = 03/26/14 
 Pct Recovery = 30%  Analysis Date = 03/26/14 
 Pct Recovery = 30%  Analysis Date = 03/24/14 
 Pct Recovery = 30%  Analysis Date = 03/24/14 
 Pct Recovery = 30%  Analysis Date = 03/21/14 
 Pct Recovery = 31%  Analysis Date = 03/21/14 
 Pct Recovery = 31%  Analysis Date = 03/19/14 
 Pct Recovery = 31%  Analysis Date = 03/19/14 
 Pct Recovery = 31%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/16/14 
 Pct Recovery = 32%  Analysis Date = 03/14/14 
 Pct Recovery = 32%  Analysis Date = 03/14/14 
 Pct Recovery = 32%  Analysis Date = 03/12/14 
 Pct Recovery = 33%  Analysis Date = 03/12/14 
 Pct Recovery = 33%  Analysis Date = 03/09/14 
 Pct Recovery = 33%  Analysis Date = 03/09/14 
 Pct Recovery = 33%  Analysis Date = 03/07/14 
 Pct Recovery = 34%  Analysis Date = 03/07/14 
 Pct Recovery = 34%  Analysis Date = 03/04/14 
 Pct Recovery = 34%  Analysis Date = 03/04/14 
 Pct Recovery = 34%  Analysis Date = 03/02/14 
 Pct Recovery = 34%  Analysis Date = 03/02/14 
 Pct Recovery = 34%  Analysis Date = 02/28/14 
 Pct Recovery = 35%  Analysis Date = 02/28/14 
 Pct Recovery = 35%  Analysis Date = 02/25/14 
 Pct Recovery = 35%  Analysis Date = 02/25/14 
 Pct Recovery = 35%  Analysis Date = 02/23/14 
 Pct Recovery = 36%  Analysis Date = 02/23/14 
 Pct Recovery = 36%  Analysis Date = 02/20/14 
 Pct Recovery = 36%  Analysis Date = 02/20/14 
 Pct Recovery = 36%  Analysis Date = 02/18/14 
 Pct Recovery = 37%  Analysis Date = 02/18/14 
 Pct Recovery = 37%  Analysis Date = 02/15/14 
 Pct Recovery = 37%  Analysis Date = 02/15/14 
 Pct Recovery = 37%  Analysis Date = 02/13/14 
 Pct Recovery = 37%  Analysis Date = 02/13/14 
 Pct Recovery = 37%  Analysis Date = 02/11/14 
 Pct Recovery = 37%  Analysis Date = 02/11/14 
 Pct Recovery = 37%  Analysis Date = 02/08/14 
 Pct Recovery = 37%  Analysis Date = 02/08/14 
 Pct Recovery = 37%  Analysis Date = 02/06/14 
 Pct Recovery = 37%  Analysis Date = 02/06/14 
 Pct Recovery = 37%  Analysis Date = 02/03/14 
 Pct Recovery = 37%  Analysis Date = 02/03/14 
 Pct Recovery = 37%  Analysis Date = 02/01/14 
 Pct Recovery = 37%  Analysis Date = 02/01/14 
 Pct Recovery = 37%  Analysis Date = 01/30/14 
 Pct Recovery = 38%  Analysis Date = 01/30/14 
 Pct Recovery = 38%  Analysis Date = 01/27/14 
 Pct Recovery = 38%  Analysis Date = 01/27/14 
 Pct Recovery = 38%  Analysis Date = 01/25/14 
 Pct Recovery = 38%  Analysis Date = 01/25/14 
 Pct Recovery = 38%  Analysis Date = 01/22/14 
 Pct Recovery = 38%  Analysis Date = 01/22/14 
 Pct Recovery = 38%  Analysis Date = 01/20/14 
 Pct Recovery = 38%  Analysis Date = 01/20/14 
 Pct Recovery = 38%  Analysis Date = 01/18/14 
 Pct Recovery = 38%  Analysis Date = 01/18/14 
 Pct Recovery = 38%  Analysis Date = 01/15/14 
 Pct Recovery = 38%  Analysis Date = 01/15/14 
 Pct Recovery = 38%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/13/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/10/14 
 Pct Recovery = 38%  Analysis Date = 01/08/14 
 Pct Recovery = 37%  Analysis Date = 01/08/14 
 Pct Recovery = 37%  Analysis Date = 01/06/14 
 Pct Recovery = 37%  Analysis Date = 01/06/14 
 Pct Recovery = 37%  Analysis Date = 01/03/14 
 Pct Recovery = 37%  Analysis Date = 01/03/14 
 Pct Recovery = 37%  Analysis Date = 01/01/14 
 Pct Recovery = 36%  Analysis Date = 01/01/14 
 Pct Recovery = 36%  Analysis Date = 12/29/13 
 Pct Recovery = 36%  Analysis Date = 12/29/13 
 Pct Recovery = 36%  Analysis Date = 12/27/13 
 Pct Recovery = 36%  Analysis Date = 12/27/13 
 Pct Recovery = 36%  Analysis Date = 12/24/13 
 Pct Recovery = 35%  Analysis Date = 12/24/13 
 Pct Recovery = 35%  Analysis Date = 12/22/13 
 Pct Recovery = 35%  Analysis Date = 12/22/13 
 Pct Recovery = 35%  Analysis Date = 12/20/13 
 Pct Recovery = 35%  Analysis Date = 12/20/13 
 Pct Recovery = 35%  Analysis Date = 12/17/13 
 Pct Recovery = 34%  Analysis Date = 12/17/13 
 Pct Recovery = 34%  Analysis Date = 12/15/13 
 Pct Recovery = 34%  Analysis Date = 12/15/13 
 Pct Recovery = 34%  Analysis Date = 12/12/13 
 Pct Recovery = 34%  Analysis Date = 12/12/13 
 Pct Recovery = 34%  Analysis Date = 12/10/13 
 Pct Recovery = 33%  Analysis Date = 12/10/13 
 Pct Recovery = 33%  Analysis Date = 12/08/13 
 Pct Recovery = 33%  Analysis Date = 12/08/13 
 Pct Recovery = 33%  Analysis Date = 12/05/13 
 Pct Recovery = 33%  Analysis Date = 12/05/13 
 Pct Recovery = 33%  Analysis Date = 12/03/13 
 Pct Recovery = 32%  Analysis Date = 12/03/13 
 Pct Recovery = 32%  Analysis Date = 11/30/13 
 Pct Recovery = 32%  Analysis Date = 11/30/13 
 Pct Recovery = 32%  Analysis Date = 11/28/13 
 Pct Recovery = 32%  Analysis Date = 11/28/13 
 Pct Recovery = 32%  Analysis Date = 11/26/13 
 Pct Recovery = 31%  Analysis Date = 11/26/13 
 Pct Recovery = 31%  Analysis Date = 11/23/13 
 Pct Recovery = 31%  Analysis Date = 11/23/13 
 Pct Recovery = 31%  Analysis Date = 11/21/13 
 Pct Recovery = 31%  Analysis Date = 11/21/13 
 Pct Recovery = 31%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/18/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/16/13 
 Pct Recovery = 30%  Analysis Date = 11/13/13 
 Pct Recovery = 30%  Analysis Date = 11/13/13 
 Pct Recovery = 30%  Analysis Date = 11/11/13 
 Pct Recovery = 29%  Analysis Date = 11/11/13 
 Pct Recovery = 29%  Analysis Date = 11/09/13 
 Pct Recovery = 29%  Analysis Date = 11/09/13 
 Pct Recovery = 29%  Analysis Date = 11/06/13 
 Pct Recovery = 29%  Analysis Date = 11/06/13 
 Pct Recovery = 29%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/04/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 11/01/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/30/13 
 Pct Recovery = 28%  Analysis Date = 10/28/13 
 Pct Recovery = 27%  Analysis Date = 10/28/13 
 Pct Recovery = 27%  Analysis Date = 10/25/13 
 Pct Recovery = 27%  Analysis Date = 10/25/13 
 Pct Recovery = 27%  Analysis Date = 10/23/13 
 Pct Recovery = 27%  Analysis Date = 10/23/13 
 Pct Recovery = 27%  Analysis Date = 10/20/13 
 Pct Recovery = 27%  Analysis Date = 10/20/13 
 Pct Recovery = 27%  Analysis Date = 10/18/13 
 Pct Recovery = 27%  Analysis Date = 10/18/13 
 Pct Recovery = 27%  Analysis Date = 10/16/13 
 Pct Recovery = 28%  Analysis Date = 10/16/13 
 Pct Recovery = 28%  Analysis Date = 10/13/13 
 Pct Recovery = 28%  Analysis Date = 10/13/13 
 Pct Recovery = 28%  Analysis Date = 10/11/13 
 Pct Recovery = 28%  Analysis Date = 10/11/13 
 Pct Recovery = 28%  Analysis Date = 10/08/13 
 Pct Recovery = 28%  Analysis Date = 10/08/13 
 Pct Recovery = 28%  Analysis Date = 10/06/13 
 Pct Recovery = 28%  Analysis Date = 10/06/13 
 Pct Recovery = 28%  Analysis Date = 10/04/13 
 Pct Recovery = 28%  Analysis Date = 10/04/13 
 Pct Recovery = 28%  Analysis Date = 10/01/13 
 Pct Recovery = 28%  Analysis Date = 10/01/13 
 Pct Recovery = 28%  Analysis Date = 09/29/13 
 Pct Recovery = 28%  Analysis Date = 09/29/13 
 Pct Recovery = 28%  Analysis Date = 09/26/13 
 Pct Recovery = 28%  Analysis Date = 09/26/13 
 Pct Recovery = 28%  Analysis Date = 09/24/13 
 Pct Recovery = 28%  Analysis Date = 09/24/13 
 Pct Recovery = 28%  Analysis Date = 09/21/13 
 Pct Recovery = 28%  Analysis Date = 09/21/13 
 Pct Recovery = 28%  Analysis Date = 09/19/13 
 Pct Recovery = 28%  Analysis Date = 09/19/13 
 Pct Recovery = 28%  Analysis Date = 09/17/13 
 Pct Recovery = 28%  Analysis Date = 09/17/13 
 Pct Recovery = 28%  Analysis Date = 09/14/13 
 Pct Recovery = 28%  Analysis Date = 09/14/13 
 Pct Recovery = 28%  Analysis Date = 09/12/13 
 Pct Recovery = 28%  Analysis Date = 09/12/13 
 Pct Recovery = 28%  Analysis Date = 09/09/13 
 Pct Recovery = 28%  Analysis Date = 09/09/13 
 Pct Recovery = 28%  Analysis Date = 09/07/13 
 Pct Recovery = 28%  Analysis Date = 09/07/13 
 Pct Recovery = 28%  Analysis Date = 09/05/13 
 Pct Recovery = 28%  Analysis Date = 09/05/13 
 Pct Recovery = 28%  Analysis Date = 09/02/13 
 Pct Recovery = 28%  Analysis Date = 09/02/13 
 Pct Recovery = 28%  Analysis Date = 08/31/13 
 Pct Recovery = 28%  Analysis Date = 08/31/13 
 Pct Recovery = 28%  Analysis Date = 08/28/13 
 Pct Recovery = 28%  Analysis Date = 08/28/13 
 Pct Recovery = 28%  Analysis Date = 08/26/13 
 Pct Recovery = 28%  Analysis Date = 08/26/13 
 Pct Recovery = 28%  Analysis Date = 08/24/13 
 Pct Recovery = 28%  Analysis Date = 08/24/13 
 Pct Recovery = 28%  Analysis Date = 08/21/13 
 Pct Recovery = 28%  Analysis Date = 08/21/13 
 Pct Recovery = 28%  Analysis Date = 08/19/13 
 Pct Recovery = 28%  Analysis Date = 08/19/13 
 Pct Recovery = 28%  Analysis Date = 08/16/13 
 Pct Recovery = 28%  Analysis Date = 08/16/13 
 Pct Recovery = 28%  Analysis Date = 08/14/13 
 Pct Recovery = 28%  Analysis Date = 08/14/13 
 Pct Recovery = 28%  Analysis Date = 08/11/13 
 Pct Recovery = 28%  Analysis Date = 08/11/13 
 Pct Recovery = 28%  Analysis Date = 08/09/13 
 Pct Recovery = 29%  Analysis Date = 08/09/13 
 Pct Recovery = 29%  Analysis Date = 08/07/13 
 Pct Recovery = 29%  Analysis Date = 08/07/13 
 Pct Recovery = 29%  Analysis Date = 08/04/13 
 Pct Recovery = 29%  Analysis Date = 08/04/13 
 Pct Recovery = 29%  Analysis Date = 08/02/13 
 Pct Recovery = 29%  Analysis Date = 08/02/13 
 Pct Recovery = 29%  Analysis Date = 07/30/13 
 Pct Recovery = 29%  Analysis Date = 07/30/13 
 Pct Recovery = 29%  Analysis Date = 07/28/13 
 Pct Recovery = 29%  Analysis Date = 07/28/13 
 Pct Recovery = 29%  Analysis Date = 07/26/13 
 Pct Recovery = 29%  Analysis Date = 07/26/13 
 Pct Recovery = 29%  Analysis Date = 07/23/13 
 Pct Recovery = 29%  Analysis Date = 07/23/13 
 Pct Recovery = 29%  Analysis Date = 07/21/13 
 Pct Recovery = 29%  Analysis Date = 07/21/13 
 Pct Recovery = 29%  Analysis Date = 07/18/13 
 Pct Recovery = 29%  Analysis Date = 07/18/13 
 Pct Recovery = 29%  Analysis Date = 07/16/13 
 Pct Recovery = 30%  Analysis Date = 07/16/13 
 Pct Recovery = 30%  Analysis Date = 07/14/13 
 Pct Recovery = 30%  Analysis Date = 07/14/13 
 Pct Recovery = 30%  Analysis Date = 07/11/13 
 Pct Recovery = 30%  Analysis Date = 07/11/13 
 Pct Recovery = 30%  Analysis Date = 07/09/13 
 Pct Recovery = 30%  Analysis Date = 07/09/13 
 Pct Recovery = 30%  Analysis Date = 07/06/13 
 Pct Recovery = 30%  Analysis Date = 07/06/13 
 Pct Recovery = 30%  Analysis Date = 07/04/13 
 Pct Recovery = 30%  Analysis Date = 07/04/13 
 Pct Recovery = 30%  Analysis Date = 07/02/13 
 Pct Recovery = 30%  Analysis Date = 07/02/13 
 Pct Recovery = 30%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/29/13 
 Pct Recovery = 31%  Analysis Date = 06/27/13 
 Pct Recovery = 31%  Analysis Date = 06/27/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/24/13 
 Pct Recovery = 31%  Analysis Date = 06/22/13 
 Pct Recovery = 31%  Analysis Date = 06/22/13 
 Pct Recovery = 31%  Analysis Date = 06/19/13 
 Pct Recovery = 31%  Analysis Date = 06/19/13 
 Pct Recovery = 31%  Analysis Date = 06/17/13 
 Pct Recovery = 31%  Analysis Date = 06/17/13 
 Pct Recovery = 31%  Analysis Date = 06/15/13 
 Pct Recovery = 31%  Analysis Date = 06/15/13 
 Pct Recovery = 31%  Analysis Date = 06/12/13 
 Pct Recovery = 32%  Analysis Date = 06/12/13 
 Pct Recovery = 32%  Analysis Date = 06/10/13 
 Pct Recovery = 32%  Analysis Date = 06/10/13 
 Pct Recovery = 32%  Analysis Date = 06/07/13 
 Pct Recovery = 32%  Analysis Date = 06/07/13 
 Pct Recovery = 32%  Analysis Date = 06/05/13 
 Pct Recovery = 32%  Analysis Date = 06/05/13 
 Pct Recovery = 32%  Analysis Date = 06/03/13 
 Pct Recovery = 32%  Analysis Date = 06/03/13 
 Pct Recovery = 32%  Analysis Date = 05/31/13 
 Pct Recovery = 32%  Analysis Date = 05/31/13 
 Pct Recovery = 32%  Analysis Date = 05/29/13 
 Pct Recovery = 32%  Analysis Date = 05/29/13 
 Pct Recovery = 32%  Analysis Date = 05/26/13 
 Pct Recovery = 32%  Analysis Date = 05/26/13 
 Pct Recovery = 32%  Analysis Date = 05/24/13 
 Pct Recovery = 33%  Analysis Date = 05/24/13 
 Pct Recovery = 33%  Analysis Date = 05/22/13 
 Pct Recovery = 33%  Analysis Date = 05/22/13 
 Pct Recovery = 33%  Analysis Date = 05/19/13 
 Pct Recovery = 33%  Analysis Date = 05/19/13 
 Pct Recovery = 33%  Analysis Date = 05/17/13 
 Pct Recovery = 33%  Analysis Date = 05/17/13 
 Pct Recovery = 33%  Analysis Date = 05/14/13 
 Pct Recovery = 33%  Analysis Date = 05/14/13 
 Pct Recovery = 33%  Analysis Date = 05/12/13 
 Pct Recovery = 33%  Analysis Date = 05/12/13 
 Pct Recovery = 33%  Analysis Date = 05/10/13 
 Pct Recovery = 33%  Analysis Date = 05/10/13 
 Pct Recovery = 33%  Analysis Date = 05/07/13 
 Pct Recovery = 34%  Analysis Date = 05/07/13 
 Pct Recovery = 34%  Analysis Date = 05/05/13 
 Pct Recovery = 34%  Analysis Date = 05/05/13 
 Pct Recovery = 34%  Analysis Date = 05/02/13 
 Pct Recovery = 34%  Analysis Date = 05/02/13 
 Pct Recovery = 34%  Analysis Date = 04/30/13 
 Pct Recovery = 34%  Analysis Date = 04/30/13 
 Pct Recovery = 34%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/27/13 
 Pct Recovery = 34%  Analysis Date = 04/25/13 
 Pct Recovery = 35%  Analysis Date = 04/25/13 
 Pct Recovery = 35%  Analysis Date = 04/23/13 
 Pct Recovery = 35%  Analysis Date = 04/23/13 
 Pct Recovery = 35%  Analysis Date = 04/20/13 
 Pct Recovery = 35%  Analysis Date = 04/20/13 
 Pct Recovery = 35%  Analysis Date = 04/18/13 
 Pct Recovery = 35%  Analysis Date = 04/18/13 
 Pct Recovery = 35%  Analysis Date = 04/15/13 
 Pct Recovery = 35%  Analysis Date = 04/15/13 
 Pct Recovery = 35%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/13/13 
 Pct Recovery = 36%  Analysis Date = 04/11/13 
 Pct Recovery = 36%  Analysis Date = 04/11/13 
 Pct Recovery = 36%  Analysis Date = 04/08/13 
 Pct Recovery = 36%  Analysis Date = 04/08/13 
 Pct Recovery = 36%  Analysis Date = 04/06/13 
 Pct Recovery = 36%  Analysis Date = 04/06/13 
 Pct Recovery = 36%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/03/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 04/01/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/30/13 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 Pct Recovery = 37%  Analysis Date = 03/27/13 
 Pct Recovery = 37%  Analysis Date = 03/25/13 
 Pct Recovery = 38%  Analysis Date = 03/25/13 
 Pct Recovery = 38%  Analysis Date = 03/22/13 
 Pct Recovery = 38%  Analysis Date = 03/22/13 
 Pct Recovery = 38%  Analysis Date = 03/20/13 
 Pct Recovery = 38%  Analysis Date = 03/20/13 
 Pct Recovery = 38%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/17/13 
 Pct Recovery = 38%  Analysis Date = 03/15/13 
 Pct Recovery = 38%  Analysis Date = 03/15/13 
 Pct Recovery = 38%  Analysis Date = 03/13/13 
 Pct Recovery = 39%  Analysis Date = 03/13/13 
 Pct Recovery = 39%  Analysis Date = 03/10/13 
 Pct Recovery = 39%  Analysis Date = 03/10/13 
 Pct Recovery = 39%  Analysis Date = 03/08/13 
 Pct Recovery = 39%  Analysis Date = 03/08/13 
 Pct Recovery = 39%  Analysis Date = 03/05/13 
 Pct Recovery = 39%  Analysis Date = 03/05/13 
 Pct Recovery = 39%  Analysis Date = 03/03/13 
 Pct Recovery = 40%  Analysis Date = 03/03/13 
 Pct Recovery = 40%  Analysis Date = 03/01/13 
 Pct Recovery = 40%  Analysis Date = 03/01/13 
 Pct Recovery = 40%  Analysis Date = 02/26/13 
 Pct Recovery = 40%  Analysis Date = 02/26/13 
 Pct Recovery = 40%  Analysis Date = 02/24/13 
 Pct Recovery = 40%  Analysis Date = 02/24/13 
 Pct Recovery = 40%  Analysis Date = 02/21/13 
 Pct Recovery = 40%  Analysis Date = 02/21/13 
 Pct Recovery = 40%  Analysis Date = 02/19/13 
 Pct Recovery = 41%  Analysis Date = 02/19/13 
 Pct Recovery = 41%  Analysis Date = 02/17/13 
 Pct Recovery = 41%  Analysis Date = 02/17/13 
 Pct Recovery = 41%  Analysis Date = 02/14/13 
 Pct Recovery = 41%  Analysis Date = 02/14/13 
 Pct Recovery = 41%  Analysis Date = 02/12/13 
 Pct Recovery = 41%  Analysis Date = 02/12/13 
 Pct Recovery = 41%  Analysis Date = 02/09/13 
 Pct Recovery = 41%  Analysis Date = 02/09/13 
 Pct Recovery = 41%  Analysis Date = 02/07/13 
 Pct Recovery = 42%  Analysis Date = 02/07/13 
 Pct Recovery = 42%  Analysis Date = 02/05/13 
 Pct Recovery = 42%  Analysis Date = 02/05/13 
 Pct Recovery = 42%  Analysis Date = 02/02/13 
 Pct Recovery = 42%  Analysis Date = 02/02/13 
 Pct Recovery = 42%  Analysis Date = 01/31/13 
 Pct Recovery = 42%  Analysis Date = 01/31/13 
 Pct Recovery = 42%  Analysis Date = 01/28/13 
 Pct Recovery = 42%  Analysis Date = 01/28/13 
 Pct Recovery = 42%  Analysis Date = 01/26/13 
 Pct Recovery = 43%  Analysis Date = 01/26/13 
 Pct Recovery = 43%  Analysis Date = 01/23/13 
 Pct Recovery = 43%  Analysis Date = 01/23/13 
 Pct Recovery = 43%  Analysis Date = 01/21/13 
 Pct Recovery = 43%  Analysis Date = 01/21/13 
 Pct Recovery = 43%  Analysis Date = 01/19/13 
 Pct Recovery = 43%  Analysis Date = 01/19/13 
 Pct Recovery = 43%  Analysis Date = 01/16/13 
 Pct Recovery = 44%  Analysis Date = 01/16/13 
 Pct Recovery = 44%  Analysis Date = 01/14/13 
 Pct Recovery = 44%  Analysis Date = 01/14/13 
 Pct Recovery = 44%  Analysis Date = 01/11/13 
 Pct Recovery = 44%  Analysis Date = 01/11/13 
 Pct Recovery = 44%  Analysis Date = 01/09/13 
 Pct Recovery = 44%  Analysis Date = 01/09/13 
 Pct Recovery = 44%  Analysis Date = 01/07/13 
 Pct Recovery = 44%  Analysis Date = 01/07/13 
 Pct Recovery = 44%  Analysis Date = 01/04/13 
 Pct Recovery = 45%  Analysis Date = 01/04/13 
 Pct Recovery = 45%  Analysis Date = 01/02/13 
 Pct Recovery = 45%  Analysis Date = 01/02/13 
 Pct Recovery = 45%  Analysis Date = 12/30/12 
 Pct Recovery = 45%  Analysis Date = 12/30/12 
 Pct Recovery = 45%  Analysis Date = 12/28/12 
 Pct Recovery = 45%  Analysis Date = 12/28/12 
 Pct Recovery = 45%  Analysis Date = 12/26/12 
 Pct Recovery = 45%  Analysis Date = 12/26/12 
 Pct Recovery = 45%  Analysis Date = 12/23/12 
 Pct Recovery = 46%  Analysis Date = 12/23/12 
 Pct Recovery = 46%  Analysis Date = 12/21/12 
 Pct Recovery = 46%  Analysis Date = 12/21/12 
 Pct Recovery = 46%  Analysis Date = 12/18/12 
 Pct Recovery = 46%  Analysis Date = 12/18/12 
 Pct Recovery = 46%  Analysis Date = 12/16/12 
 Pct Recovery = 46%  Analysis Date = 12/16/12 
 Pct Recovery = 46%  Analysis Date = 12/14/12 
 Pct Recovery = 46%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
WARFARIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 49% . 49% 0%
>= Reporting Level 10 33% 10% 31% 14%
Total 11 35% 11% 31% 17%

Sample Statistics
WARFARIN

Characteristic N % % Basis
Plotted 11 79% Spiked
Estimated Values 5 36% Spiked
Deleted Values 1 3% Spiked + Not Spiked
Spiked, Censored 1 7% Spiked
Spiked 15 .  
False Negatives 2 14% 2 out of 14
Not Spiked 17 .  
False Positives 1 6% 1 out of 17