BQS OBSP Determination:
SITAGLIPTIN
METHOD: 2440 , TESTIDCODE: 67531LCM56
DATES: 05/17/14 - 01/19/17
Open Data Set

 Expected Conc. = 609 
 Median Pct Recovery = 74%  Expected Conc. = 609 
 Median Pct Recovery = 74%  Expected Conc. = 609 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 585.44 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 489.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 487.2 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390.98 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 390 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 292.72 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 244.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 243.6 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208.52 
 Median Pct Recovery = 74%  Expected Conc. = 208 
 Median Pct Recovery = 74%  Expected Conc. = 208 
 Median Pct Recovery = 74%  Expected Conc. = 208 
 Median Pct Recovery = 74%  Expected Conc. = 208 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195.49 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 195 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 146.36 
 Median Pct Recovery = 74%  Expected Conc. = 73.18 
 Median Pct Recovery = 74%  Expected Conc. = 73.18 
 Median Pct Recovery = 74%  Expected Conc. = 73.18 
 Median Pct Recovery = 74%  Analysis Date = 01/19/17 
 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Pct Recovery = 89%  Analysis Date = 01/19/17 
 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Pct Recovery = 82%  Analysis Date = 11/24/15 
 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl 
 Pct Recovery = 74%  Analysis Date = 10/01/15 
 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl 
 Pct Recovery = 69%  Analysis Date = 10/01/15 
 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl 
 Pct Recovery = 19%  Analysis Date = 09/09/16 
 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Pct Recovery = 83%  Analysis Date = 09/09/16 
 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Pct Recovery = 82%  Analysis Date = 07/23/16 
 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl 
 Pct Recovery = 76%  Analysis Date = 07/23/16 
 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl 
 Pct Recovery = 82%  Analysis Date = 11/18/16 
 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl 
 Pct Recovery = 70%  Analysis Date = 11/18/16 
 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl 
 Pct Recovery = 75%  Analysis Date = 11/18/16 
 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl 
 Pct Recovery = 65%  Analysis Date = 11/18/16 
 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl 
 Pct Recovery = 67%  Analysis Date = 03/10/15 
 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Pct Recovery = 70%  Analysis Date = 12/07/14 
 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Pct Recovery = 80%  Analysis Date = 10/25/14 
 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl 
 Pct Recovery = 86%  Analysis Date = 06/22/14 
 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl 
 Pct Recovery = 79%  Analysis Date = 06/11/14 
 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl 
 Pct Recovery = 50%  Analysis Date = 04/29/15 
 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl 
 Pct Recovery = 117%  Analysis Date = 03/11/15 
 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl 
 Pct Recovery = 113%  Analysis Date = 02/06/15 
 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl 
 Pct Recovery = 99%  Analysis Date = 12/06/14 
 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl 
 Pct Recovery = 82%  Analysis Date = 10/11/14 
 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl 
 Pct Recovery = 84%  Analysis Date = 08/21/14 
 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl 
 Pct Recovery = 54%  Analysis Date = 07/26/14 
 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl 
 Pct Recovery = 69%  Analysis Date = 04/27/16 
 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl 
 Pct Recovery = 61%  Analysis Date = 04/27/16 
 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl 
 Pct Recovery = 58%  Analysis Date = 12/15/15 
 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl 
 Pct Recovery = 69%  Analysis Date = 07/31/15 
 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl 
 Pct Recovery = 54%  Analysis Date = 07/30/15 
 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl 
 Pct Recovery = 66%  Analysis Date = 01/05/17 
 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 121%  Analysis Date = 01/05/17 
 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 137%  Analysis Date = 10/28/16 
 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 83%  Analysis Date = 10/28/16 
 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 73%  Analysis Date = 09/23/16 
 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl 
 Pct Recovery = 84%  Analysis Date = 09/23/16 
 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl 
 Pct Recovery = 99%  Analysis Date = 08/17/16 
 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 63%  Analysis Date = 08/17/16 
 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl 
 Pct Recovery = 70%  Analysis Date = 08/11/16 
 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl 
 Pct Recovery = 74%  Analysis Date = 08/11/16 
 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl 
 Pct Recovery = 82%  Analysis Date = 10/29/16 
 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Pct Recovery = 65%  Analysis Date = 10/29/16 
 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Pct Recovery = 82%  Analysis Date = 09/17/16 
 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl 
 Pct Recovery = 63%  Analysis Date = 09/17/16 
 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl 
 Pct Recovery = 68%  Analysis Date = 04/30/15 
 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Pct Recovery = 86%  Analysis Date = 02/10/15 
 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Pct Recovery = 76%  Analysis Date = 10/24/14 
 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl 
 Pct Recovery = 75%  Analysis Date = 12/07/14 
 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl 
 Pct Recovery = 98%  Analysis Date = 11/04/14 
 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl 
 Pct Recovery = 98%  Analysis Date = 09/12/14 
 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl 
 Pct Recovery = 62%  Analysis Date = 07/13/14 
 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Pct Recovery = 44%  Analysis Date = 06/28/14 
 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Pct Recovery = 45%  Analysis Date = 05/30/14 
 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Pct Recovery = 42%  Analysis Date = 05/17/14 
 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Pct Recovery = 54%  Analysis Date = 10/10/14 
 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl 
 Pct Recovery = 99%  Analysis Date = 08/30/14 
 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl 
 Pct Recovery = 76%  Analysis Date = 07/20/14 
 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl 
 Pct Recovery = 49%  Analysis Date = 02/23/16 
 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Pct Recovery = 50%  Analysis Date = 08/11/15 
 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl 
 Pct Recovery = 55%  Analysis Date = 06/26/15 
 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Pct Recovery = 55%  Analysis Date = 06/09/15 
 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl 
 Pct Recovery = 55%  Analysis Date = 04/09/16 
 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl 
 Pct Recovery = 80%  Analysis Date = 04/09/16 
 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl 
 Pct Recovery = 128%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Median Pct Recovery = 74%  Y = 1
The SGPlot Procedure